study of spray dryer

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    Summary

    The main objective of this experiment was to study about the spray dryers and the mechanism

    of the spray drying process. The experiment was carried with mixed flow spray dryer which

    contains a two-flow atomizer. A cyclone separator was used for the separation of solid. In our

    experiment, a solution of known amount of powder milk was spray dried to observe the

    performance of the spray dryer. In this experiment, 1000.1 gm liquor milk was taken which

    contains 50 gm milk powder. And after the drying process 12.4 gm milk powder was

    recovered from the solution. Hence, 24.8% milk powder was recovered. The probable reasons

    for the poor recovery are highlighted in the discussion.

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    Experimental Setup

    Figure 2: Schematic diagram of experimental setup of a spray drying system

    Air blower

    Chamber Tem .

    Heater

    Drying chamber

    Air

    Compressor

    Powder milk

    container

    Cyclone separatorHot air

    Thermometer

    Exhaust pipe

    Air water vapor

    Feed milk container

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    Observed data

    Working pressure, P = 20 psig

    Inlet temperature, Ti = 150 C

    Initial outlet temperature of air, To = 78.5 C

    Final outlet temperature of air, To = 64 C

    Total time required for drying, t = 38 min

    = 2280 sec

    Weight of milk powder, m = 50 gm

    Weight of water, mw = 950.1 gm

    Weight of liquid milk, Mt = (mw + ms) = (950.1+50) gm

    = 1000.1 gm

    Weight of empty beaker, m1 = 554.1 gm

    Weight of beaker with recovered milk powder, m2 = 566.5 mg

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    Calculated data

    Weight of solid recovered, MR = (Weight of beaker + recovered milk powder) Weight of

    empty beaker

    = m2m1

    = (566.5554.1) gm

    = 12.4 gm

    %100akenintially tsolidtheofweight

    recoveredsolidtheofweight

    recoveryPercentage

    %100m

    M

    R

    %24.8

    %10050

    12.4

    dryingoftimeTotal

    waterofweightrateDrying

    t

    m

    W

    gm/sec0.42

    gm/sec0.41671

    gm/sec2280

    950.1

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    Result

    Weight of solid recovered, MR= 12.4 gm

    Percentage recovery of milk powder = 24.8%

    Drying rate = 0.42 gm/sec

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    Discussion

    From the experiment result the percentages recovery of milk indicates some losses in the

    system. Probable reason behind such low recovery are stated below

    1. Some milk powder may accumulate in the apparatus.2. Air is exhausted from the cyclone separator which may contain milk powder.3. A considerable portion of milk was stuck on the separator wall, which also reduced

    the milk powder recovery.

    4. The experiment was done in a very small scale and the dryer had been used forseveral years. So, the depreciation factor of the pilot plant has caused lower recovery

    of milk powder.

    5. The milk that is supplied has some moisture content but after drying only dry milkpowder was obtained. So loss in the weight of milk powder was found.

    6. If the paste was not prepared perfectly, then some powder might clot. Clotted powdermight create problem while flowing throw pipe and spraying.

    7. The feed had been entered the dryer at a quite high flow rate to conduct the dryingprocess quickly, if the rate was lower the drying process would be more efficient

    8. Before the experiment there were some water in the nozzle for some operatingproblem. That is why dried powder may again dissolved in the water. It may be a

    reason for low percentage recovery.

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    Process Block Diagram (PBD)

    Figure 2: Process block diagram of a spray drying system

    Compressed air

    P= 20 psig

    Milk powder solution

    Milk powder=4.9995%

    Water=95.0005%

    Air

    Blower

    Heater

    Hot air, T=150

    Spray

    Dryer

    Cyclone

    Separator

    Recovered milk

    powder

    Air

    Milk powder

    Water vapor

    Air and Water

    vapor

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    Process Flow Diagram

    Figure 3: Process flow diagram of a spray drying system

    Air

    Air

    Hot air, T=150

    Air

    Compressed air

    P= 20 psig

    Feed

    Milk powder=4.9995%

    Water=95.0005%

    Air and Water

    vapor

    Recovered milk

    powder

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    Modification

    It is essential for both economic and environmental reasons to recover as much powder as

    possible from the system. Three modifications are available-

    1. Bag filters2. Wet scrubber3. Electrostatic precipitator (ESP)

    Bag filters

    Bag filters are in general frequently used for dust removal in industrial applications. So as it

    is used for recovery of particle in spray drying of solid. The flow can be from the outside to

    the inside of the filter or the other way around, depending on the application. The particles

    are normally captured on the internal surface of the bag filter. Bag filters are in general not

    designed for replacement when they are clogged, but some bag filters, like particle removers,

    can be cleaned, for example by mechanical shaking or by backwashing with compressed air

    (so called reverse-flow bag filters). Bag filters are mostly surface-type filters.

    Figure 4: Bag filter

    Wet scrubber

    Wet scrubbers are the most economical outlet air cleaner. It can be used in spray drying for

    higher recovery of solid dust powder. The principle of a wet scrubber is to dissolve any dust

    powder left in the air stream into either water or the feed stream by spraying the wash stream

    through the air. This also recovers heat from the exiting air and evaporates some of the water

    in the feed stream (if used as the wash water).

    Made of fabrics

    (Holds milk powder but

    removes gases)

    Exhaust Air

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    Figure 5: Scrubber

    Electrostatic precipitator

    An electrostatic precipitator (ESP) or electrostatic air cleaner is a particulate collection device

    that removes particles from a flowing gas (such as air) using the force of an induced

    electrostatic charge. Electrostatic precipitators are highly efficient filtration devices that can

    easily remove fine particulate matter such as dust and smoke from the air stream. In contrast

    to wet scrubbers which apply energy directly to the flowing fluid medium, an ESP applies

    energy only to the particulate matter being collected and therefore is very efficient in its

    consumption of energy (in the form of electricity).

    Figure 6: Electrostatic precipitator

    Exhaust air

    Water

    Li uid milk

    Charged collecting

    plate

    Collected particle

    Exhaust gas

    containing particle

    Exhaust gas

    Without particle