study of a pressure in masses of particles

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    ChE 30

    Chemical engineering laboratory - II

    Experiment No. Group No. 03 (A2)

    Name of the experiment:

    STUDY OF APRESSUREIN MASSES OF PARTICLES

    Submitted by:

    Md. Hasib Al Mahbub

    Student Id: 0902045

    Level: 3; Term: 2

    Section: A2

    Date of performance:11/02/2014

    Date of submission:25/02/2014

    Partners Student Id.0902041

    0902042

    0902043

    0902044

    Department of Chemical Engineering.

    Bangladesh University of engineering and technology, Dhaka.

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    Experimental Setup

    Figure 1. Schematic diagram of the experimental setup

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    Observed data

    Table 1: Observed data for weight and height.

    Obs. no. Mass of sand added(Kg)

    Mass of sand in

    column(Kg)

    Height of sand in

    column(inch)

    1 1 1 0.5

    2 2 1.7 2

    3 3 2.3 2.8

    4 4 3.3 4.5

    5 5 3.75 6

    6 6 4.15 7.5

    7 7 4.5 8.8

    8 8 4.8 10.5

    9 9 4.95 12

    10 10 5.1 13

    11 11 5.2 14.7

    12 12 5.35 15.7

    13 13 5.5 17.3

    14 14 5.55 19

    15 15 5.6 20.4

    16 16 5.65 21.8

    17 17 5.7 23.5

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    Table 2: Data for calculation of mass flow rate.

    Observation

    No.

    Mass of

    particle,

    Kg

    Time of

    collection,

    sec

    Mass flow

    rate, m

    Kg/sec

    Average mass

    flow rate, m

    Kg/sec

    1 0.4 10 0.04

    0.0427

    2 0.4 10 0.04

    3 0.4 10 0.04

    4 0.4 10 0.04

    5 0.4 10 0.04

    6 0.45 10 0.045

    7 0.45 10 0.045

    8 0.45 10 0.045

    9 0.45 10 0.045

    10 0.45 10 0.045

    11 0.45 10 0.045

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    Calculated data

    Table 1.03 : Calculated data for ( PB) Th & ( PB) expt .

    Obs

    .no.

    Volume

    occupied bysand , V

    ft 3

    Bulk density,

    blbm/ ft 3

    angle of

    internalfriction

    of solids

    m ( 0)

    1 - Sin mK=

    1 + Sin m

    Theoretical

    basepressure

    ( PB) Thlbf/ft2

    Expt.

    basepressure

    ( PB) expt.

    lbf/ft2

    1 0.00818571 269.3230031

    23.020.43776

    10.88944128 11.23076923

    2 0.03274284 134.6615016 19.89112387 19.09230769

    3 0.045839976 144.2801803 28.46173276 25.83076923

    4 0.07367139 119.6991125 34.42197814 37.06153846

    5 0.09822852 112.217918 39.59887257 42.11538462

    6 0.12278565 107.7292013 43.85516383 46.60769231

    7 0.144068496 107.1171035 47.83462617 50.53846154

    8 0.17189991 102.5992393 50.21743195 53.90769231

    9 0.19645704 100.9961262 52.5651913 55.59230769

    10 0.21282846 103.5857704 55.74561057 57.27692308

    11 0.240659874 100.76711 56.79499699 58.4

    12 0.257031294 102.9259885 59.31429435 60.08461538

    13 0.283225566 101.1907237 60.0596509 61.76923077

    14 0.31105698 99.22426431 60.3745286 62.33076923

    15 0.333976968 99.01580998 61.25190768 62.89230769

    16 0.356896956 98.83412959 61.98203392 63.45384615

    17 0.38472837 97.41470326 61.92427968 64.01538462

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    Results and discussions

    For one Kg mass of particle the experimental base pressure is 11.23 lbf/ft2, whereas using the

    Janssen equation we got it 10.89 lbf/ft2. After a certain height 1.7 ft the pressure becomes

    practically constant. And at this height the experimentally observed pressure is 64.01 lbf/ft2

    and pressure using the Janssen equation is 61.9 lbf/ft2.

    Graph 1 shows the behavior of both the experimental and theoretical base pressure with the

    increment of the bed height. The two curves are very close. This indicates that the values of

    experimental and theoretical pressures are almost same. The experimental values were little

    higher than theoretical one. These discrepancies might be occurred due to improper addition of

    sand particle. That means when sand was added into the column it was not possible to add thesand particle uniformly into the column.

    Solid particle handling or storage is a regular requirement in our day-to-day life or in the

    industries. It is a huge challenge for all sorts of people ranging from the plant engineer to the

    food grain dealers or the sea-line operators. The challenge as clear from this experiment is the

    pressure exerted by the masses of particles. This pressure has profound impact on the design

    of bin, vessels, hoppers or silos as economics is always involved in building such storage tanks.

    This experiment helps to determine the maximum pressure exerted by the solid particles.

    Knowing this limit, the capacity or the size of the storage tank can be determined. Proper

    materials of construction can be selected as well. It can save the storage tanks from being over

    pressurized and being collapsed. Hence, this experiment is very important and gets a wide

    range of application where design of storage tank is concerned.

    Some of the fields of application of this experiment are as follows:

    Food grain storage tank design. Design of vessels carrying various grains. Design of reactor handling solid particles. Design of silos in cement industries, etc.

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    When granular solids are stored in a bin or hopper, the lateral pressure exerted on the walls at

    any point is less than predicted from the head of material above that point. Furthermore there

    usually is friction between the wall and the solid grains, and because of the interlocking of the

    particles; the effect of this friction is felt throughout the mass. The frictional force at the wall

    tends to offset the weight of the solid and reduces the pressure exerted by the mass on the floor

    of the container. With many solids, when the height reaches about three times the diameter of

    the bin, additional material has virtually no effect on the pressure at the base. The total mass of

    bin plus material continues to increase, but the additional mass is carried by the wall and not

    by the floor of the bin. In the extreme case this force causes the mass to arch, or bridge, so that

    it does not fall, even when the material below is removed.

    In solids the pressure is not the same in all directions. In general, a pressure applied in one

    direction creates some pressure in other directions, but it is always smaller than the applied

    pressure. It is a minimum in the direction at right angles to the applied pressure.

    It has been observed that when the height reaches a certain limit, additional sand has virtually

    no effect on the pressure at the base. The total mass of the column plus material continues to

    increase, but the additional mass is carried by the wall and foundation, not by the floor of the

    column.

    From the readings, it is clear that after a certain height the pressure exerted by the solid grains

    became constant. Nevertheless, the result could be improved by taking care to take the readings

    of height. The top edge of the materials in the cylindrical glass tube was no at horizontal level

    so that we had to take the average height reading. As a result the parallax error was introduced

    in the experiment. Moreover, the weighing machines were not highly calibrated to take more

    precisely weigh readings.

    The experimental results revealed two concepts, which are, the lateral pressure that acts at

    right angle with the applied pressure is always the minimum pressure; at a certain applied

    pressure, base pressure of the column is constant.

    This knowledge of pressure (exerted by the masses of particles) distribution characteristics will

    help us to design the structure of bins, hoppers or silos to preserve the too valuable or too

    soluble solids.

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    Graphical comparison between experimental and theoretical base pressure

    Graph 1: experimental base pressure vs. theoretical base pressure

    10

    20

    30

    40

    50

    60

    70

    0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2

    Base

    Pressure

    Height

    Experimental

    Theoretical