size and structure of the pilot plant

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    EXPERIMENTATION

    IN PILOT PLANT

    By : Sri Kumalaningsih

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    INTRODUCTION

    Pilot plant studies are physicalsimulation studies

    The pilot plant is a physical model and

    should be a copy of the correspondingindustrial unit, with equipment scaleddown in size to approximately 1/100

    1/10 of the modeled unit

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    1. Market Survey A determined new product amount can be

    produced in the pilot plant, to test its acceptanceand to decide whether it would be economicallyprofitable

    2. Design Data

    A pilot plant permits the acquisition of accuratedata on processing system energy and massbalances

    3. Products and Raw Material

    Usually needed to characterize food products andto evaluate the development of certain rawmaterials into spesific products

    4. Optimization data of a Running Plant

    Can be used to optimize running of equipment andfood plants, in order to study possible

    modifications of the original food processings stem deemed im racticable or uneconomical at

    Pilot plant experiments serve toobtain more information and datain the following areas :

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    Basic Principles of Scaling

    If fluids are handled in the pilot plant,three types of similarities involved influid dynamics must be included :

    1. Geometric similarity

    2. Kinematic similarity

    3. Dynamic similarity

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    1. Geometric Similarity

    Both the pilot plant and food processing plantshould have the same physical form or atleast the same geometric dimensionrelationships.

    This similarity can be partial

    2. Kinematic SimilarityThe same velocity relationships should exist

    in both the pilot and food processing plants

    3. Dynamic Similarity In both the pilot and food processing plants,

    the same force relationships should exist. For example, the turbulence regime should be

    similar on both scales when fluids are handled

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    If the process simulated in a pilot plantinvolves chemical or biochemical reactions,as frequently occurs in food processing

    systems, the following similarities apply :a.Thermal similarity

    In addition to geometric and kinematicsimilarity, the pilot and processing plant

    should present similar temperaturedifferences among the various points in thesystem, simulated at both plant and industriallevels

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    b. Chemical and biochemical similarity

    There should be parallel differences in concentration(of products or components in the studied system) inthe pilot plant and food processing plant.

    In addition, the chemical and biochemical kineticsmust be similar on both scales

    Generally, the thermal, chemical and biochemical

    similarities (including kinetics) are complete at bothpilot plant and industrial level (with scale factor = 1)

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    Minimum and MaximumSize The minimum size is set by the minimum

    product amount required for quality analiticalcontrol

    Ex : if the aim of pilot plant experimentation isto study the influence of process conditions onproduct quality, the minimum amount ofprocessed product in the pilot plant shouldpermit the necessary physical-chemicalanalysis to evaluate product quality

    The maximum size is set by the amount ofprocessed product needed in order to testmarket acceptance

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    Types and Applications

    When product production in amounts large enoughto conduct market acceptance tests is required, thepilot plant is called a semicommercial plant

    In any case, reduced-scale pilot plant studies arethe most often employed studies used to obtaininformation and data on production engineering(running of food processing plants) and design

    engineering (new food processing plants)

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    1. Product Studies

    Quality characterization

    Influence of process conditions on productquality Development of new product Studies of market acceptance2. Raw Material Studies

    Raw material characterization Evaluation of aptitude for industrializatio

    of diferent raw material

    The most common applications of a pilot plant are as follow :

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    3. Process Technology andEngineering Studies Setting the most suitable process conditions

    from an economic point of view Study of process equipment alterntives to

    carry out given food processing steps or unit

    operations Development of new process technology and

    new process engineering/process equipmentAuxiliary system requirement studies

    Reliable evaluation of mass and energy

    balances and food physical properties Study of energy recovery possibilities in

    process systems Improvement and evaluation of alternatives

    for control systems

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    PILOT PLANT DESIGN

    An appropriate pilot plant design isessential in order to achieve reliableresults during pilot plant experimental

    programsTaking into consideration the similarity

    principles, the factors that will becontrolled or changed duringexperimentation are evaluated first

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    Example :

    A study on drying fruits and vegetables with hot aircrossing over the drying bed.

    Controlled factors are :

    - Air velocity between 0,2 and 3 m/s

    - Air temperature between 50 and 100C

    - Load density of drying bed between 40 and 50 kg/m

    - Air relative humidity between 20 and 100%

    - Hot air recycling between 0% and 100%

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    Thus, the controlled factors are established aswell as the interval of variation considered

    Other aspects to take into account in the

    design of a pilot plant are availability ofauxiliary systems, raw materials andspesifications of the product

    The location of the pilot plant usually depends

    on plant size, utilities and laboratoryrequirements to assist in pilot plant operation

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    ExperimentationStrategiesThe profits from experimentation in the pilot plant

    should be greater than the costsThus, it is very important to establish an appropriate

    experimental design for the pilot plant, since it will save

    time and money All controlled process parameters (experimental

    variables) are usually known as factorsThe value of each factor is the variation level of the

    factor A combination of factors used in a particular

    experimental run is called the treatment

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    The result of factor variation in an experimentalrun is designated as the effect

    If the raw material used in experiments is

    limited in quantity, it may be necessary to useseveral batches of raw material that are similarbut not identical in characteristics

    Each batch is called a block and repetitions of

    the same experiment are known as replications

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    Factorial design requires an appropriateexperimental design procedure in the pilotplant.

    It is useful in discovering the influence ofdifferent factors on process development orfinal quality of the product

    Once the effects of the different factors have

    been studied, a regression analysis can becompleted to develop quantitative relationshipsamong the different factors, processparameters, or product quality parameters

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    Capital Investment and Operation Cost

    The cost of experimentation in the pilotplants is determined as follows :

    a. Capital investment costs for process

    equipment and auxiliary systems inthe pilot plant, as well as unexpectedexpenses common duringconstruction

    b. Cost of buildings and structures toconstruct and operate pilot plant

    c. Cost of raw materials and

    consumptions of auxiliary systems

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    d. Cost of staff during experimentation,considering direct labor as well assupervision, analysis and interpretation of

    resultse. Cost of laboratory fungible material to

    control product quality and process

    f. Estimated cost of instrumental equipment

    use, needed to control process, productquality and raw materials.

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    Thank You