sge gc inlet liner range - available from kinesis
DESCRIPTION
Choosing the right inlet liner and injection parameter can increase peak areas and reduce detection limits by up to 300%1. Customer research conducted by SGE found that a significant number of GC users don’t understand the importance of inlet liner selection, or how it contributes to their analysis. The SGE inlet liner range aims to make it simple for all gas chromatographers to select the right liner.TRANSCRIPT
Spot the difference in the SGE lineup!
SGE GC inlet liner range:
•Easytochoose.•Easytouse.•Confidenceinyouranalysis.
1.Kende,Aetal.Chromatographia,2006;63(3/4):181-7
Easy to chooseForeaseofselectionsoyoucanoptimizeyourresults,SGEhascolorcodedthelinersbygeometry.Colorcodingandsampletypesarelistedinthetablebelow.
Color Injection Technique
Sample Types Liner Geometry
Dar
k G
reen
Splitless•Tracelevelanalyses.
•Activecompounds.
Taper / Gooseneck
Blu
e
Split
•Generalpurpose.
•Concentratedsamples.
•Dirtysamples.
FocusLiner™
Aq
ua
Splitless
•Tracelevelanalyses.
•Dirtysamples.
•Wideboilingpointrange.
Taper Focus
Ora
ng
e
Direct•Tracelevelanalyses.
•Activecompounds.
ConnecTite™
Purp
le
SplitSplitless
•Generalpurpose.
•Concentratedsamples.
•Dirtysamples(onlyifquartzwool is present)
•Gaseous samples (also Purge andTrap,Headspace).
Straight
Yel
low
SplitlessLVI
•Tracelevelanalyses.
•Lowboilingpointcompounds.
•Activecompounds.
Double Taper
Gre
y
PTVLVI
•Tracelevelanalyses.
•Largevolumeinjections.
PTV/LVI
Easy to choose•Color coded by geometry to
simplifyyourselection.
Easy to use•Containo-ringssoyou’reready
togo.
Confidence in your analysis•Certified deactivation gives you
confidenceinyouranalysis.
Spot the difference in the SGE lineup!
Choosing the right inlet liner and injection parameter can increase peakareasandreducedetectionlimitsbyupto300%1.
Customer research conducted by SGE found that a significant number ofGCusersdon’tunderstandtheimportanceofinletlinerselection,orhowitcontributestotheiranalysis.TheSGEinletlinerrangeaimstomakeitsimpleforallgaschromatographerstoselecttherightliner.
SGE has also created a liner selection tool that can be found on our website: www.sge.com/linertool
Whetherforroutineanalysis,difficultprobesortraceanalysishaveconfidenceinyouranalysiswithSGE’sinletliners.Whilebottomtaperwithwoolisconsideredthebestgeometryfortraceanalysis,theSGEFocusLiner™ delivers optimal performanceinallapplications.
Confidence in your analysis
SGE standard inlet liner deactivation
SGEtestseverybatchofinletlinersforactivityusingtheEPA8081Bmethod.Thisstandardmethodensuresthateachbatchofinletlinershaslessthana3%Endrinbreakdown(5ppmstandard).SGEvalidatesthisqualityassurancebyincludingabatchcertificatewitheverypack.
5 7 9 11 13 15 17 19 21 23
InjectionNoinjection–gasflowfor5min
InjectorTemp 350 °C Purgeflow 20 ml/min
Ovenprogram50 °C to 350 °C (20/min)hold2.2mins
Carrier gas He(1.2ml/min)Detector(MS) 50-650mzInstrument Agilent 6890
MS scan for Siloxane bleed - thick vs thin film deactivation
Confidence in your trace analysis
14000000
12000000
10000000
8000000
6000000
4000000
2000000
0
SGE
Brand X
Brand Y
• Low siloxane bleed due toSGE’sthinfilmdeactivation.
Liner Comparison -0.5 ng 2, 4-dinitrophenol
Instrument: 5973inertMSDand6890GC
Oven:40 °C to 80 °C at 10 °C a minute 20 °C a minuteto190°Choldfor2minutes30°Caminuteto350°Choldforoneminute
Inlet: 4.9psi200°CHeColumn: 30mBPX50.25mmx0.25µm(PN:054101)GCMS: Scan 50 to 550InjectionVolume:
1µL
TestMix:CustomSVOCstandardmixfromAccuStandard S-23011 2000 ug/mL (diluted to0.5ppm)
Confidence with difficult probes
• Reproducibleperformancewiththerightchoiceinlinergeometry.
-10000
40000
90000
140000
190000
240000
10.12 10.14 10.16 10.18 10.2 10.22 10.24 10.26 10.28 10.3
Time (min)
SGE Tapered Focus 1
SGE Tapered Focus 2
SGE Tapered Focus 3
BrandXBottomTaperwithwool1
BrandXBottomTaperwithwool2
BrandXBottomTaperwithwool3
Confidence for routine analysis - injection after injection
50 ppb 100 Repeat injections comparison Endrin and DDT % breakdown
Testing Parameters
50 ppm Endrin and DDT test mix1µLSplitlessinjection@250°CHT grade Septa (PN: 041898)
• SGE’s Tapered FocusLiner™ shows improved performancecompared with competitor’spremiumdeactivatedliner.
• ChoosetheTaperedFocusLiner™ to ensure your analysis is uncompromised injection afterinjection.
0
5
10
15
20
25
30
35
0 20 40 60 80 100
%B
reak
dow
n
NumberofInjections
BrandXEndrinKetoneandEndrinAldehyde(Bottomtaperwithwool)
Brand X DDD and DDE (Bottomtaperwithwool)
SGEEndrinKetoneandEndrinAldehyde (Tapered FocusLiner)
SGE DDD and DDE (Tapered FocusLiner)
BR-0
359-
A_R
evC
© S
GE
Ana
lytic
al S
cien
ce P
ty L
td 0
4/20
12
Easy to useSGE’s inlet liners come as a complete, packaged solution:•1,5and25packs.•Complete with instrument
appropriateo-ringsorsealingrings.•Each pack supplied with quality
assurancetestresults.•SGE blister packs are perforated
enablingeasydivisionofthe5and25packswhilemaintainingblisterintegrity.
•25 packs come in a re-usablecontainer,witharangeofattractivedesigns, thatwill behandy aroundthelab.
Easy to chooseEasy to use Confidence in your analysis
SGE inlet liners, spot the difference.
To select the right inlet liner for your instrument, injection and sample – use our selection tool: www.sge.com/linertool
When deactivation REALLY matters
Singlepackdeactivationcertificationoptions:•CustomerswhoareISOaccreditedorfollowGLPwillbenefitfromSGE’scertifiedsinglepacks. Add CERT when ordering.•MSreadylinersinsinglepacksconditionedandMStestedpostdeactivationsotheyarereadyforusestraight
outofthepack.Add MS when ordering.
AUSTRALIA & PACIFIC REGIONSGE Analytical Science Pty LtdToll Free: 1800 800 167Tel: +61 (0) 3 9837 4200Fax: +61 (0) 3 9874 5672Email: [email protected]
JAPANSGEJapanIncTel: +81 45 222 2885Fax: +81 45 222 2887Email: [email protected]
EUROPESGE Europe LtdEuropeanHeadOfficeToll Free: 00800 2790 8999Toll Free Fax: 00800 2626 2609Tel: +44 1908 568 844Fax: +44 1908 566 790Tel France: +33 1 69 29 80 90Fax France: +33 1 69 29 09 25Tel Germany: +49 (0) 6155 / 60746 0Fax Germany: +49 (0) 6155 / 60746 50Email: [email protected]
UNITED STATES OF AMERICASGEIncorporatedToll Free: (800) 945 6154Tel: +1 512 837 7190Fax: +1 512 836 9159Email: [email protected]
www.sge.com