session 13 ic2011 bonigut

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Bonigut, Krug Forest Products Society 65 th International Convention Portland, OR, June 2011 Properties of thermally modified oriented strandboards (OSB) Juergen Bonigut, Dr. Detlef Krug Institute of Wood Technology Dresden, Dresden, Germany

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Page 1: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Properties of thermally modified oriented strandboards (OSB)

Juergen Bonigut, Dr. Detlef KrugInstitute of Wood Technology Dresden, Dresden, Germany

Page 2: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Outline

1. Current situation2. Research goals3. Material and method4. Selected results5. Summary

Page 3: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Current situation - TMT

Thermal modification of solid wood is at the centre of R & DDegree of modification depends on the parameters

temperature

ambient pressure

oxygen content

duration of modification

Page 4: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Advantages

reduced moisture uptake

increased biological durability

improved dimensional stability by reducing swelling and shrinking

Disadvantages

decreased density

reduced physical properties

increased brittleness

forming of cracks, halos (softwoods)

Current situation - TMT

Page 5: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Current situation - PF WBM

Phenol formaldehyde resin bonded wood-based materials:

industry: storage of PF-bonded wbm in a (hot-) stack

during hot-stacking further and complete adhesive curing takes place due to high temperatures of panels right after hot-press

results in enhanced mechanical strength properties and improved hygroscopic properties

Page 6: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

OSB production

logs / solid wood stranding strands resination forming hot-pressingOSB panels

Page 7: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

logs / solid wood stranding strands resination forming hot-pressingOSB panels

Treatment types

Page 8: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

logs / solid wood stranding strands resination forming hot-pressingOSB panels

Treatment types

Page 9: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

logs / solid wood stranding strands resination hot-pressingOSB panels

Treatment types

Page 10: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Goals

Thermal post-treatment of PF-bonded oriented strandboards (OSB)

reduction of equilibrium moisture content (EMC),

reduction of thickness swelling,

improvement of internal bond strength (IB) after 2 h boiling,

reduction of creep behaviour.

Exploratory investigations with MUF-bonded SWP and PF-bonded MDF showed promising results

Page 11: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Material

PF-bonded industrial OSB

type: OSB/3 (acc. to EN 300)

density: 620 kg/m3 (38.7 lbs/cu.ft),

thickness: 16 mm (0.63 in.),

adhesive content: 7 % PF (solids/oven-dry wood)

content hydrophobing agent: 1.5 % paraffin (solids/oven-dry wood)

Page 12: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Thermal post-treatment

Post-treatment of OSB took place according to Mühlböck- procedure in a partner company‘s treatment chamber

Heating up and cooling down of the chamber: 3 min/KMaximum temperatures:

160 °C (320 F)

170 °C (338 F)

180 °C (356 F)

Holding time: 4 h

Page 13: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

In analogy to thermally modified solid wood (TMT), OSB showed darker colouration over whole cross-section

Thermal post-treatment

Page 14: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Testing of properties

Short-term properties

IB (dry & 2 h boiling) (EN 300, EN 319),

MOR & MOE (EN 310),

TS (EN 317),

WA,

EMC (EN 323).

Long-term property

creep behaviour testing climate: 20 °C (68 F) / 85 % humidity

Page 15: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

IB

Requirements for load-bearing boards for use in humid conditions (type OSB/3) according to EN 300: 0.32 MPa and 0.13 Mpa, respectively

Page 16: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

MOR & MOE (main axis)

Requirements for load-bearing boards for use in humid conditions (type OSB/3) according to EN 300 (main axis): 20 MPa (MOR) and 3,500 MPA (MOE), respect.

Page 17: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

TS

Requirements for load-bearing boards for use in humid conditions (type OSB/3) according to EN 300: max. 15 % after 24 h immersion in water

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Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

WA

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Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

EMC

Climate: 20 °C (68 F) / 65 % humidity

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Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Creep behaviour

Creep factor describes relation between time-dependent increase of deflection under load and elastic initial deflection

Tested in accordance with ENV 1156

Wood-based panels – Determination of duration of load and creep factors

Page 21: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Creep behaviour

Creep behaviour is dependent on:

duration

stress level

climate

Duration of testing: 105 days

Stress level: 25 % of Fmax

Test climate: 20 °C (68 F) / 85 % humidity

Page 22: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Creep behaviour

Page 23: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Summary

Influence of thermal post-treatment on PF-bonded OSB

Property strongly positive

slightly positive

hardly / minor

slightly negative

strongly negative

IB (dry & after 2h boiling)

X

MOR & MOE X TS & WA (2 h & 24 h) X

EMC X creep behaviour X

Page 24: Session 13 ic2011 bonigut

Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

Summary

Conclusion: by thermally post-treating PF-bonded OSB very positive effects could be shown, i. e. improvemements of most physical properties

Research into thermal post-treatment of wbm will be continued

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Bonigut, KrugForest Products Society 65th International Convention Portland, OR, June 2011

[email protected]