scheme and detailed syllabusjnec.org/syllabus/chem/se-chemical-engineering-syllabus-2017-18.pdf ·...

2

SCHEME AND DETAILED SYLLABUS

of

SE (Chemical Engineering)

Under Choice Based Credit & Grading System

(w.e.f. academic year 2017-18 & onwards/-)

FOUR YEAR DEGREE COURSE IN SCIENCE& TECHNOLOGY

Dr. BABASAHEB AMBEDKAR MARATHWADA UNIVERSITY,

AURANGABAD

3

Faculty of Science and Technology

Curriculum structure of S.E. (Chemical Engineering)

With effect from Academic Year: 2017-18 & onwards/-

PART-I

Sub Code Semester-I Contact Hrs/Week Examination Scheme Duration of The

Theory

Examination Subject L T P Total CT TH TW PR Total credits

BSH201 Engineering

Mathematics -III 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE202 Process Instrumentation

and Analytical

Techniques

4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE203 Mechanical Operation 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE204 Chemical Process

Calculation 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE205 Fluid Mechanics 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE221 Lab 1: Process

Instrumentation and

Analytical Techniques

-- -- 2 2 -- -- 50 -- 50 1

CHE222 Lab 2: Mechanical

Operation -- -- 2 2 -- -- -- 50 50 1

CHE223 Lab 3: Fluid Mechanics -- -- 2 2 -- -- -- 50 50 1

CHE224 Lab 4: Theory and

Drawing of Equipment -- -- 4 4 -- -- 50 -- 50 2

CHE225 Lab 5: Computer

Laboratory -- -- 2 2 -- -- -- 50 50 1

Total 20 -- 12 32 100 400 100 150 750 26

PART - II

Sub Code Semester-II Contact Hrs/Week Examination Scheme

Duration of

The Theory

Examination

Subject L T P Total CT TH TW PR Total Credits

BSH206 Engineering

Mathematics-IV 4 -- -- 4 20 80 -- -- 100 4 3 Hr

BSH207 Engineering chemistry 4 -- -- 4 20 80 -- -- 100 4 3 Hr

BSH208 Physical Chemistry and

Thermodynamics 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE209 Heat Transfer 4 -- -- 4 20 80 -- -- 100 4 3 Hr

CHE210 Strength of Material 4 -- -- 4 20 80 -- -- 100 4 3 Hr

BSH226 Lab 6: Engineering

chemistry -- -- 4 4 -- -- -- 50 50 2

BSH227 Lab 7: Physical

Chemistry and

Thermodynamics

-- -- 2 2 -- -- -- 50 50 1

CHE228 Lab 8: Heat Transfer -- -- 2 2 -- -- -- 50 50 1

CHE229 Lab 9: Strength of

Material -- -- 2 2 -- -- 50 -- 50 1

CHE230 Lab 10: Communication

Skills- I -- -- 2 2 -- -- 50 -- 50 1

Total 20 -- 12 32 100 400 100 150 750 26

Total of Semester I & II 40 24 64 200 800 200 300 1500 52

L: Lecture hours per week T: Tutorial hours per week P: Practical hours per week

CT: Class Test, TH: University Theory Examination,TW: Term Work, PR: Practical/Oral Examination

4

BSH-201: ENGINEERING MATHEMATICS-III

Teaching Scheme Examination Scheme

Lectures: 4 Hrs/week Theory: 80 Marks

Credits: 04 Class Test: 20 Marks

Duration of Theory paper: 3Hrs

Objectives:

• TodevelopLogicalunderstandingofthesubject.

• Todevelopmathematical skill sothatstudentsareabletoapply

mathematicalmethods&Principle’sinsolving problemsfrom Engineeringfields.

• Toproducegraduateswithmathematicalknowledge&computationalskill.

Unit1 [8 Hrs]

LinearDifferentialEquations:

LinearDifferential Equationswithconstant coefficients Generalmethod, shortcutmethods

tofindparticularintegral,

HomogenousLineardifferentialequations(Cauchy’s&Legendre’sform),methodofvariation

ofparameters.

Unit2 [6Hrs]

Application o fL i n e a r DifferentialEquations:

Application o fL i n e a r DifferentialEquations to Electrical circuits & to Mechanical system

(Analogous study of two systems), to Civil Engineering, Free oscillations/vibrations, forced

oscillation /vibrations, Damped Free oscillations / vibrations, Damped Forced oscillations /

vibrations.

Unit3 [6Hrs]

Fourier Transform:

Fourier Transform, Fourier sine and cosine transform, Fourier integral, Fourier sine and cosine

integral.

Unit4 [8 Hrs]

Statistics&Probability: Measures of central

Tendency and Measures of Dispersion (for grouped data only), Karl Pearson’s coefficient of

skewness, Probability distribution for random variables, Binomial and Normal Distributions

Regression and Correlation.

Unit 5 [6 Hrs]

VectorDifferentiation Differentiation of

vectors, Gradient of scalar point function, Directional derivative, Divergence of vector point

function, Curl of a vector point function. Irrotational and solenoidal vector field.

Unit6: [6Hrs]

5

VectorCalculus(Integralcalculus)

The line integral, Surface integral, volume integral, Gauss Divergence theorem, Stoke’s theorem,

Green’s theorem (All theorem without proof).

Note:

SectionA:Unit1,2,3

SectionB:Unit4,5,6

Text Books:

1. P.N.WartikarandJ.N.Wartikar,“ATextBookofEngineering Mathematics”(Volume-I, II,III)

PuneVidyarthi GrihaPrakashan,Pune.

2. B.S.Grewal,“Higher EngineeringMathematics,”Khanna Publications,NewDelhi.

3. H. K.Das,“AdvancedEngineeringMathematics,” S.Chand&Company.

ReferenceBooks:

1. B.V.Ramana,“HigherEngineeringMathematics,”(Tata McGraw- Hill).

2. ErwinKreyszig, “AdvancedEngineeringMathematics,”Wiley EasternLtd.

3. RavishR Singh,MukulBhat,“EngineeringMathematics,”ATutorial Approach,McGrawHill

4. S.C. Gupta and V.K. Kapoor,“Fundamentals of Mathematical Statistics” byS. Chand and

Sons

PatternofQuestionPaper:

Theunitsinthesyllabusshallbedividedintwoequalsections.Questionpapershallbesethavingtwosectio

nsAandB.SectionAquestionsshallbeset onfirstthreeunits(1,2,3)

andSectionBquestionsonremainingthreeunits(4,5,6). Questionpapershouldcovertheentiresyllabus.

For80marksPaper:

1. Minimumtenquestions

2. Fivequestionsineachsection

3. Question no1and6bemadecompulsoryandshouldhaveatleast EIGHTbits

oftwomarksoutofwhichFIVEtobesolved.

4. Twoquestionsfromremainingquestionsfromeachsectionbe

askedtosolvehavingweightageof15marks.

6

CHE-202: PROCESS INSTRUMENTATION AND ANALYTICAL TECHNIQUES





Objectives:

1) To develop understanding of the principles of measurement.

2) To understand the instruments and analytical method using in process industries.

Unit I [6 Hrs]

Principles of measurement, elements of instruments, static and dynamic characteristics, response

of first and second order instruments. Process Instrumentation. Recording, indicating, signaling

instruments. Principles of transductions, Transducers & their classification. Elastic, Resistance,

Capacitive & Inductive transducers for temperature, level, flow and pressure measurements.

Instrumentation diagrams.

UnitII [8 Hrs]

Constructional details, working principles and response characteristics of, temperature measuring

instruments like expansion thermometers, thermocouples,thermister, resistance thermometer,

pyrometers, etc.

Unit III [6 Hrs]

Constructional details, working principles and response characteristics of, pressure and vacuum

measuring devices (instruments) like pressure gauge, McLeod gauge, etc. Head and Level

measuring devices. Review of flow meters (orifice meter, venturi meter, rotameter.

Unit IV [8 Hrs]

Importance, scope & methods of sampling of solids, liquids, gaseous materials, industrial &

laboratory techniques. Tools of the analyst, general procedures, preliminaries to the analyst.

Theory of indicators. Gas analysis,Introduction theory, instrumentation and application of

Visible Spectrophotometry, Colorimetry, Infrared Spectroscopy, Conductometry &

conductometric titration, Potentiometry.

Unit V [6 Hrs]

Introduction theory, instrumentation and application of Flame Photometry, Polarography,

Amperometric titration, Coulometric technique & titration.

Unit VI [6 Hrs]

Introduction theory, instrumentation and application of Karl-Fischer titrimetry, Gas

chromatography, thin layer chromatography.

7

Reference Book:

1. Industrial Instrumentation by Donald P. Eckrnan, Wiley Eastern Ltd.

2. Principles of Industrial Instrumentation by D. Patranabis, Tata -McGraw Hill Co.

3. Instrumental Methods in Chemical Analysis by G.W.Ewing, Mc Graw Hill Co.

4. Instrumental Methods in Chemical Analysis by Chatwal and Anand.

5. Instrumental Methods in Chemical Analysis by B.K.Sharma

6. Quantitative Inorganic Analysis by A. I. Vogel

Pattern of Question Paper:

The units in the syllabus shall be divided in two equal sections. Question paper shall be set

having two sections A and B. Section A questions shall be set on first three units (1,2,3) and

Section B questions on remaining three units (4,5,6) Question paper should cover the entire

syllabus.

For 80 marks Paper:

1. Minimum ten questions

2. Five questions in each section

3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out of

which FIVE to be solved.

4. Two questions from remaining questions from each section be asked to solve

havingweightage of 15 marks

8

CHE-203: MECHANICAL OPERATIONS





Objectives:

1) To develop understanding of the principles of unit operations.

2) To understand calculations and principles related to chemical processes.

Unit 1 [6 Hrs]

Size Reduction:

Law of Size reduction, types of equipment used and their selection. Open and Closed Circuit

Operation, Crushers, Ball Mill, Rod Mill etc. Energy relationship in size reduction.

Unit 2 [8 Hrs]

Particle size analysis and Separation:

Methods of representation of size analysis, sub sieve methods of analysis, surface area

determination. Theory of screening and size distribution, different type of screening equipments,

mesh number, cumulative screening, effectiveness factor, screening effectiveness.

Unit 3 [6 Hrs]

Storage and Transportation of Solids:

Storage of solids; Bunkers, Silos, Bins, Hoppers and handling of solids. Transportation of solids,

conveying, types of conveyors and performances.

Unit 4 [8 Hrs]

Sorting:

Separation of solids, Gravity concentrationmethods. Jigging, Principles of jigging, types of jiggs,

their performances, characteristics. Froth flotation- Principles and Theories of collection,

flotation cell, typical circuits, magnetic and electrical separation.

Unit 5 [10 Hrs]

Solid-Liquid Separation:

Filtration- filtration theory, equipments for filtration, constant pressure and constant rate

filtration, optimum cycle, use of filter aids, equipment for liquid solid filtration. Agitated

Nutsche filters. Micro and ultrailtration, reverse osmosis. Centrifugal separations - Principle.

Thickening - Batch and Continuous thickeners Classification, types of classifiers, mechanical

and non mechanical, pneumatic, Cyclone separation, theory, principle.

Unit 6 [4 Hrs]

Mixing :

Mixers & mixing, Agitators & agitation, Flow patters in agitated vessels, flow numbers, power

consumption and mixing index.

9

Reference Books:

1. Unit Operations of Chemical Engineering, W. L. McCabe & J.M. Smith, et al McGraw Hill

Publication.

2. Chemical Engineering Vol.-I & II, J. F. Richardson J. M. Coulson, Pergamon Press

Publication.

3. Introduction to Chemical Engineering, W. L. Badger and J. T. Banchero McGraw Hill

Publication.

4. Principles of Unit Operations, A. S. Foust et al John Wiley & Sons Publications.

5. Chemical Engineers Hand book, R. H. Perry, McGraw Hill Publication.

6. Chemical Engineering mechanical operations by Hiramath and A.P. Kulkarni.




Section B questions on remaining three units (4,5,6) . Question paper should cover the entire

syllabus.

For 80 marks Paper:





4. Two questions from remaining questions from each section be asked to solve having

weightage of 15 marks

10

CHE-204: CHEMICAL PROCESS CALCULATIONS


Lectures 4 Hrs/week Theory: 80 Marks

Credits: 04 Class Test 20 Marks


Objectives:

1) To develop Logical understanding of the subject

2) To understand fundamental calculations and principles related to chemical processes.

3) To produce graduates with knowledge of making basic chemical engineering calculations.

UNIT 1 [6 Hrs]

Introduction to Process Calculations. Basic & derived units, Stoichiometric relations, different

ways of expressing the composition of mixtures and solutions. Properties of Gases Liquids &

Solids: Ideal & real gas laws. Critical properties, properties of mixtures & solution, phase

Equilibria, phase rule. Laws of Dalton & Amagat and their applications. Vapor pressure:

vaporization, effect of temperature on vapor pressure, vapor pressure plot, Estimation of critical

properties. vapor pressure of immiscible liquids solutions, Raoult’s law.

UNIT 2 [6 Hrs]

Humidity & Saturation:Humidity, Saturation, Dew point, Vaporization & Condensation

processes, Wet & Dry bulb thermometry. Psychometric chart, Solubility diagrams. Thermo

physics: Heat capacity of gases, liquids, solids & solutions. Kopp’s rule, Latent heats, heat of

fusion & vaporization.

UNIT 3 [6 Hrs]

Material Balance: Concepts of limiting & excess reactants, recycle, purging, bypass in batch,

stage wise & continues operations in systems with & without chemical reaction in unit operation.

UNIT 4 [6 Hrs]

Thermo chemistry: Heats of formation, combustion, reaction, neutralization and their

applications. Heats of mixing solution. Dilution, the effect of pressure & temperature on them.

Temperature of reaction. Use of enthalpy concentration charts. Energy balances for system with

& without chemical reaction. Process efficiency.

UNIT 5 [8 Hrs]

Fuels and Combustion: Basic concepts. Types of fuels, heating values of fuels, theoretical &

excess air. Material and Energy balances- heat & combustion calculations.

UNIT 6 [6 Hrs]

Applications: Application of material and energy balance to typical chemical industrial

processes. Unsteady material balance & energy balances & its applications. (06 Hr)

11

Reference Books

1. Stoichiometry by Bhat B I & Vora S.M, Tata McGraw Hill Co. Ltd.

2. Basic Principles & Calculations in Chemical Engineering by Himmelblau D M. Prentice Hall

of India Ltd.

3. Chemical Process Principles Part I by Hougen D A & Watson K M John Wiley & Sons.

4. Chemical Engineering Vol 6, by Richardson & Coulson




Section B questions on remaining three units (4,5,6). Question paper should cover the entire

syllabus.

For 80 marks Paper:







12

CHE-205: FLUID MECHANICS





Objectives:

1) To develop Logical understanding of the subject.

2) To understand fundamental calculations and principles related to fluid flow in chemical

processes.

3) To produce graduates with knowledge of dynamics of fluid flow.

Unit 1 [8 Hrs]

Fluid Statics: Nature and properties of fluids, static fluid properties, hydrostatic equation,

barometric equation, hydrostatic equation in centrifugal fields, hydrostatic forces on plane and

curved surfaces, Buoyancy. Measurement of fluid pressure – manometers, Fluid flow

phenomenon: Types of fluid flow–shear stress and shear rate fields, viscosity and momentum

flux. Viscosity of gases and liquids, eddy viscosity.

Unit 2 [4 Hrs]

Flow of compressible fluids: Continuity equation, Total energy balance equation, mechanical

energy balance equation, Ideal gas equation, Velocity of sound, Sonic velocity, Mach Number.

Unit 3 [8 Hrs]

Basic equations of fluid flow: Basic equations of incompressible flow- conservation of mass

momentum and energy. Turbulence and nature of turbulence, Reynolds number, flow in

boundary layers. Boundary layer formation in straight tubes/ pipes, Boundary layer separation &

wake formation. One-dimensional flow, Euler’s equation and Bernoulli equation. Application of

basic equations of fluid flow.

Unit 4 [8 Hrs]

Flow of fluids: Flow of incompressible fluids through circular conduits, shear stress distribution,

and relation between skin friction and wall shear. The friction factor, relation between skin

friction parameters, laminar flow in pipes. Laminar and turbulent flow equations – average

velocity kinetic, energy correction factor. Hagen– Poiseuille equation. Turbulent flow in pipes

and closed channel, velocity distribution equation for laminar, sub layer, buffer layer and

turbulent core. Maximum and average velocity. Effect of roughness parameter. The friction

factor chart (Mood’s diagram), friction factor in flow through channels of non-circular cross

section, friction from changes in velocity or direction, effect of fittings and valves. Flow through

coils. Non –Newtonian fluid flow.

Unit 5 [6 Hrs]

Flow past immersed bodies: Boundary layer formation -Laminar and turbulent boundary layers.

Types of drag, drag coefficient and stream lining. Flow through solids, Ergun’s equation,

Kozney- Carmen equation, Blake Plummer equation. Mechanism of fluidization, types of

13

fluidization, minimum fluidization velocity. Applications of fluidization, Motion of particles

through fluids- free and hindered settling. Measurement of fluid flow by pitot tube, orifice meter,

venturimeter, rotameter

Unit 6 [6 Hrs]

Fluid flow machinery: Developed head, power requirement, suction lift & cavitation, NPSH.

Pumps & Compressors for chemical plants- reciprocating, rotary, centrifugal, airlift pumps,

blowers (their performance & characteristics. Pipeline in series and parallel flow problems.

Reference Books

1. Unit operations in Chemical Engineering by McCabe W L & Smith J C McGraw Hill Co.

2. Chemical Engineering Vol I by Richardson & Coulson

3. Fluid and Particle mechanics by Michele S J

4. Fluid Mechanics by A K Jain Khanna Publication





syllabus.

For 80 marks Paper:



3. Question no 1 and 6 be made compulsory and should have at least ten bits of two marks out

of which FIVE to be solved.



14

CHE221 LAB-I PROCESS INSTRUMENTATION AND ANALYTICAL TECHNIQUES


Practical: 2Hrs/Week Term work: 50 Marks

Credit: 01

Term Work:

Term work shall consist of a Journal containing record of any eight experiments, at least four

from each section, performed from the following list of suggested experiments:

Section-A

1. Characteristics of thermocouple

2.Calculation of time constant of thermometer.

3. Characteristics of thermister

4. Characteristics of Resistance Temperature Detector.

5. Calculation of time constant of single liquid level tank.

6. Characteristic of Pressure gauge.

Section-B

1.Detennination of iron/ nickel spectrophotometrically.

2. Determination of sodium / calcium / potassium by flame photometer. ,

3. Determination of KMnO4 or acetic acid potentiometrically.

4. Identification and quantification of cadmium in a mixture by polarigraphy.

5. Separation of some amines by TLC or paper chromatography.

6. Identification and quantification of an organic compound by gas chromatography.

7. Determination of moisture content by Karl-fisher apparatus.

8. Determination of percentage of sugar / camphor / lactic acid in a solution by polarometer.

9. Analysis of fertilizer / drugs / milk by colorimeter.

15

CHE222 LAB-II MECHANICAL OPERATIONS


Practical: 2Hrs/Week Practical: 50 Marks

Credit: 01

Practical Work

Minimum eight experiments, based on the syllabus, should be conducted during the course and

record (Journal) for the same shall be submitted.

The practical examination shall consist of performing an experiment based on the practical work

done during the course, the record of the experiments to be submitted by the candidate and viva-

voce based on the syllabus.

Suggested List of Experiments:

1. The experiment be based on following list:

1. Sieve analysis.

2. Double deck Vibrating Screen.

3. Jaw crusher.

4. Pulveriser.

5. Ball mill.

6. Plate and frame filter.

7. Vacuum filter.

8. Batch settling.

9. Cyclone Separator.

10. Sigma mixer.

16

CHE223 LAB-III FLUID MECHANICS



Credit: 01

The term work syllabus consists of a record of minimum eight (laboratory experiments)

performed & completed during the term

Suggested list of experiments/studies:

1. To perform an experiment on venturimeter.

2. To perform an experiment on orifice meter.

3. To perform an experiment on flow of water through pipe.

4. To perform an experiment on flow of water through helical coil.

5. To perform an experiment on flow of water through spiral coil

6. To study the characteristics of centrifugal pump.

7. To study the characteristics of reciprocating pump.

8. To determine reflux time of a tank and funnel.

9. To study the velocity profile of fluid in pipe/duct.

10. To study flow of fluid through packed bed.

11. To study flow of fluid through fluidized bed.

12. Determination of viscosity

13. Verification of Bernoulli's theorem

17

CHE224 LAB-IV THEORY AND DRAWING OF EQUIPMENT


Practical: 4 Hrs/Week Term work: 50 Marks

Credit: 02

Note:

1. The theoretical concepts and design in this subject is to be taught in the practical class.

2. The practical classes are to be conducted in a drawing hall.

3. The duration for each batch of students attending the practical class is 04 (four) hours, out of

which 01(one) hour is to be spent on teaching the theoretical concepts and 03 (three) hours

are to be given to the students to complete the drawings on a drawing sheet.

4. Along with the theory & design, drawing of simple parts of machines and ability of supply

additional views is expected.

5. Stress should be given with reference to chemical industry applications.

List of Practical:

Total five sheets should be completed based on the following topics.

1. Standard equipment symbol

2. Standard instrumentation symbol

3. Process flow-sheet based on 1.and 2.

4. Pipe joints and pipe fittings.

5. Types of valves – Gate valve, Globe valve, etc.

6. Types of Joints

7. Types of threads and fastenings

8. Keys and Coupling

The practical examination shall consist of a viva-voce based on theory and drawing work done

during the course and on the syllabus.

18

CHE225 LAB-IV COMPUTER LABORATORIES



Credit: 01

Term work shall consist of a record of minimum eight executable programming assignments

using C or C++ language dedicated to "Applications in Chemical Engineering" and based on

following numerical techniques.

1. Root finding methods (bisection, secant, regular-false, Newton Raphson), for algebraic and

transcendental equations.

2. Interpolation and extrapolation.

3. Numerical Integration and differentiation.

4. Curve fitting.

5. Matrix operations (Addition, subtraction, multiplication, inverse) for solution of

simultaneous linear algebraic equation arising in chemical engineering.

Emphasis is to be given on numerical techniques. Students should be made aware of advantages

and disadvantages of One method over other, wherever possible.

The term work will be a continuous assessment based on: 1. Program compiled by the student in

the computer laboratory. 2. The record of the experiments submitted by the student. 3. An oral

examination / viva-voce (conducted internally) on the syllabus and the term work mentioned

above.

The practical examination shall consist of a viva-voce based on numerical techniques done

during the course and on the syllabus.

Reference Books

For Numerical Methods:

1. Computer oriented numerical methods by Rajaraman V.

2. Numerical methods by Balchandra R.S.

3. Numerical methods with C++ programming by Somasundaram R.M.

4. Numerical methods for Engineering problems by Krishna R.N.

5. Lean Lapidus. "Digital Computation for Chemical Engineers". McGrawHill Publication,

1962.

For C Programming:

1. Let us C by Yeshwant Kanitkar

2. The C programming language by Karnighan B.W.

3. Programming in C by Stepken G. Kochan

For C++ Programming:

1. The complete reference in C++ 3rd

edition by Herbert Schidlt, Tata McGraw hill.

2. Object oriented programming in turbo C++ by Robert Lafore.

19

BSH-251: ENGINEERING MATHEMATICS-IV





Objectives:

• To develop Logical understanding of the subject

• To developmathematical skill so that students are able to apply mathematical methods &

Principal’s in solving problems from Engineering fields

• To produce graduates with mathematical knowledge & computational skill.

Unit1 [6 Hrs]

Laplace Transform:

Definition,Transfor

mofelementaryfunctions, Properties& theorems of Laplace transforms (without proof),

transforms of periodic function,

Heavisideunitstepfunction,displacedunitstepfunction,Diracdeltafunction,errorfunction,

Bessel’functionofzeroorder.

Unit2 [6 Hrs]

InverseLaplace TransformanditsApplications:

Inverse Laplace transforms by using (i) properties, ii) partial fractions, iii) Convolution theorem,

Applications to solve linear differential equations with constant coefficients (Initial value

problems), Simultaneous Linear differential equations.

Unit3 [8 Hrs]

Z Transform:

Definition,Ztransformofelementaryfunctions,propertiesofZ transform,InverseZtransform by

using partial fraction and residues theorem,SolutionofdifferenceequationbyZtransform.

Unit4 [8 Hrs]

NumericalMethods and Curve Fitting:

Solution of transdental equations by Newton Raphson method, Gauss Seidel method to solve

simultaneous linear equations, Lagranges interpolation formula for unequal intervals, numerical

differentiation: Newton’s forward and Newton’s Backward difference formulae, Solution of

ordinary differential equation by Eular modified Method and Runge-Kutta IVth order method,

Curve fitting: Principle of least squares, Fitting of linear curve, parabola, exponential curve.

Unit5 [6 Hrs]

FunctionofComplexVariable(Differentialcalculus):

Introduction,AnalyticfunctionCauchy Riemann equationsinCartesian andPolarform,Harmonic

function,Laurent’sseries (withoutproof),Conformalmapping: Translation, Magnification,

Rotation and inversionbilinear transformation.

20

Unit6 [6 Hrs]

Function ofComplex Variable(Integral calculus):

Line integral, contour

integral:Cauchy’sintegraltheorem,Cauchy’sintegralformulaResidues,Cauchy’sresiduetheorem(Al

l theorems withoutproof).

Note:

SectionA:Unit1,2,3

SectionB:Unit4,5,6

Text Books:

1. P.N.WartikarandJ.N.Wartikar,“ATextBookofEngineering Mathematics(Volume-I, II,III)

PuneVidyarthi GrihaPrakashan,Pune.

2. B.S.Grewal,“HigherEngineeringMathematics,”Khanna Publications,NewDelhi.

3. H. K.Das,“AdvancedEngineeringMathematics,” S.Chand&Company.

ReferenceBooks:

1. B.V.Ramana,“HigherEngineeringMathematics,”(Tata McGraw-Hill).

2. Erwin Kreyszig,“AdvancedEngineeringMathematics,”WileyEastern Ltd.

3. RavishR Singh, Mukul Bhat, “Engineering MathematicsATutorial

Approach,”by,McGrawHill

PatternofQuestionPaper:

Theunitsinthesyllabusshallbedividedintwoequalsections.Questionpapershallbesethavingtwosectio

nsAandB.SectionAquestionsshallbesetonfirstthreeunits(1,2,3)andSectionBquestionsonremaining

threeunits(4,5,6).Questionpapershouldcoverthe entiresyllabus.

For80marksPaper:

1. Minimumtenquestions

2. Fivequestionsineachsection

3. Questionno1and6bemadecompulsoryandshouldhaveatleastEIGHTbitsoftwomarksout

ofwhichFIVEtobesolved.

4. Twoquestionsfromremainingquestionsfromeachsectionbeaskedtosolvehaving weightageof

15marks

21

BSH-207: ENGINEERING CHEMISTRY





Objectives:

1) To develop understanding related to synthesis of organics

2) To produce graduates with knowledge of reaction mechanism & synthetic chemistry.

Unit 1 [8 Hrs]

AromaticHydrocarbons:

Preparation, Properties and uses of Benzene, Naphthalene and Anthracene, Structure

determination of benzene. Heterocyclic Compounds: Preparation, properties and uses of: Pyrrole,

Thiophene, Furan, Pyridine and Quinolene.

Unit 2 [8 Hrs]

Carbohydrates & Dyes:

Manufacture of Sucrose and Glucose, their reaction and structure determination and industrial

use.Dyes: Introduction, dyeing, isolation, constitution, synthesis and properties of (1) Indigotin

(2) Methyl Orange, (3) Alizarin. (4) Congored.

Unit3 [6 Hrs]

Amines:

Mono, Di and Tri amines, their general preparations, separations and reactions. Aniline and

diazotization reaction. General properties of diazonium salts.

Unit 4 [8 Hrs]

Study of the following unit processes: Nitration:

Nitrating agents, Mechanism of nitration of aromatics, process equipments typical nitration

process for making nitrobenzene and chloronitrobenzene Sulphonation: Reagents for

sulphonation, mechanism of sulphonation of aromatics, preparation of aliphatic and aromatic

sulphonates and sulphates. Sulphonation of lauryl alcohol, dimethyl ether etc. Halogenation:

Reagents for halogenation, mechanism of halogenations of aromatics, preparation of

chlorobenzene, DDT, BHC etc. Uses of LiAIH4 and peracids.

Unit 5 [6 Hrs]

Reactions, mechanisms and Industrial applications:

Knoevanagel's reaction, Gatterman Koch reaction, Claisen rearrangement, Pinacol-Pinacolone

rearrangement, Michel reaction, Deckmann Condensation, Benzil-Benzilic acid rearrangement,

Beckmann Rearrangement.

22

Unit 6 [4 Hrs]

Chemistry of Natural products:

Simple turpines. General methods of extraction and separation, their physical and chemical

properties, Geranial and alpha-pinene

Reference Books:

1. Organic chemistry Vol-I & II by Finar IL

2. Text book of organic chemistry by Soni PI.

3. Unit processes in synthesis by Groggin P.H.

4. Organic chemistry by Morrison and Boyd.

5. Textbook on quantitative and qualitative organic chemistry by Vogel A. I

6. Organic Chemistry by O.P. Agrawal.

7. Pitter Sykes, Organic reactions and mechanism, Orient Longman-1986

8. Reaction, rearrangements and reagents by S.N. Sanyal

9. Chemistry of Organic natural products Vol-I & II by O.P. Agrawal.

10. Heterocyclic chemistry by Raj K. Bansal.



having two sections A and B. Section A questions shall be set on first three units (1,2,3)and


syllabus.

For 80 marks Paper:







23

BSH-208: PHYSICAL CHEMISTRY AND THERMODYNAMICS





Objectives:

1) Physical Chemistry is the base of all the Chemical Industries.

2) To develop practical skill which helps the students in Chemical Industries?

Unit 1 [6 Hrs]

Electrolyte:

Conductance, Ionic mobility’s, Galvanic Cells, Classification of electrodes, determination of

Standard EMF, and its application, Cell reaction, Thermodynamics of electrolytes solutions,

Dehye and Hackle theory.

Unit 2 [10 Hrs]

Colloidal state, Adsorption,Molecular structure & properties:

Relation between molecular structure and properties such as surface tension, viscosity,

refractivity and dipole moments. Introduction, Types of colloidal states. Classification,

preparation, properties of colloidal Systems (hydrophobic & hydrophilic). Emulsifiers, gels,

foams, etc. and their applications.Adsorption Heat of adsorption, factors influencing adsorption,

adsorption isobar and adsorption isotherms Langmuir's umimolecular adsorption and limitations.

BET Theory and verification of BET equation and related problems

Unit 3 [4 Hrs]

Photochemistry:

Laws of photochemistry, quantum efficiency, kinetics of photochemical reactions.

Photochemical equilibrium, photosensitized reactions, photochemical phenomena. Radiation

chemistry, ionization radiation and electron impact process.

Unit 4 [6 Hrs]

Introduction:

Basic concepts of work., energy, heat, internal energy. The first law of thermodynamics,

thermodynamic state & state functions. Enthalpy, the steady state flow process. Equilibrium,

the reversible process. Heat capacities & specific heat. Numerical based on the above.

Unit 5 [10 Hrs]

The Phase rule:

Phase, degree of freedom of a system, the phase rule & its thermodynamic derivation.

Application of phase rule to one and two component systems. Numerical based on the above.

Volumetric properties of pure fluids: The PVT behavior. The Virial equations & its applications.

Ideal gas, Cubic equations of state, Accentric factor. The behavior of liquids. Numerical based

on the above.

24

Unit 6 [4 Hrs]

The Second law of Thermodynamic:

The Second law of Thermodynamic, heat engines, the thermodynamic temperature scale. The

concept of entropy. Entropy changes & irreversibility. The third law of thermodynamics.

Numerical based on the above.

Reference Books:

1. Principles of Physical Chemistry by Puri & Sharma

2. Physical Chemistry by Peter Atkin.

3. Advanced Physical Chemistry by Gurdeep, Raj.

4. Introduction to Chemical Engineering Thermodynamics by J M Smith & Van Ness

5. Chemical Engineering Thermodynamics, T. E. Daubert McGraw Hill Publication.

6. Chemical Process Principles Part - II O. A. Hougen et al John Wiley Publication.





syllabus.

For 80 marks Paper:







25

CHE-209: HEAT TRANSFER





Objectives:

1) To develop understanding of the principles and modes of heat transfer.

2) To understand calculations and principles related to heat transfer in chemical processes.

Unit 1 [6 Hrs]

Heat Transfer Media and Conduction:

Heat Transfer Media: Characteristic properties, classification, selection and application. Nature

of heat flow, modes of heat transfer, Fourier’s Law, steady state and unsteady state conduction in

plane wall, cylindrical wall, spherical wall, multilayer walls, lumped parameter analysis,

transient heat flow in a semi-infinite solid.

Unit 2 [8 Hrs]

Insulation, Fins and Heat Transfer Augmentation:

Thermal insulation, types and selection, optimum and economic thickness of insulation for high

and low temperatures. Heat transfer in extended surfaces,effectiveness of fins, areas of

application. Heat transfer by convection, concept, of film and overall heat transfer coefficient,

resistance concept, coefficients for scale deposits, Augmentation Techniques.

Unit 3 [6 Hrs]

Convection:

Convective heat transfers for flow through and outside pipes, laminar heat transfer on a flat plate,

dimensionless numbers in heat transfer. Dittus-Boltzer Equation, Sieder-Tate Equation, Colburn

Equation. Natural convection, fluid flow and heat transfer across cylinders and spheres.

Unit 4 [6 Hrs]

Convection with Phase Change and Analogy:

Heat transfer with phase change, heat transfer in boiling liquids and condensation of vapors.

Reynolds Analogy between Heat Transfer and Momentum Transfer, Colburn’s Analogy in

convective flow. Heat Transfer in Packed Bed and Fluidized Bed Systems.

Unit 5 [6 Hrs]

Radiation:

Heat transfer by radiation, Absorptivity, Reflectivity, Transimitivity, Kickoff’s Law, Stefan

Boatman’s Law, Black and Gray body radiations, Opaque Body, view factors, radiant heat

exchange between non-black surfaces. Radiation between different surfaces, radiation shield,

radiation from flames and gases. Combined heat transfers by conduction-convection and

radiation.

26

Unit 6 [8 Hrs]

Heat Transfer Equipment:

Heat transfer equipments, double pipe heat exchangers, single and multi-pass shell and tube heat

exchangers, LMTD and effectiveness-NTU method. Spiral coil and plate type heat exchangers,

heat transfer in evaporators – single and multiple effects, heat transfer in agitated vessels, coils,

jacketed vessels, transient heating and cooling, Heat pipe.

Reference Books:

1. Unit Operations of Chemical Engineering, W. L. McCabe & J.M. Smith, et al McGraw Hill

Publication.

2. Process Heat Transfer, D. Q. Kern McGraw Hill Publication.

3. Chemical Engineering Vol.-I J. F. Richardson J. M. Coulson, Pergamon Press Publication.

4. Heat Transfer by J P Holman, McGraw Hill Publication.

5. Fundamentals of Heat Transfer F. Krieth, M. S. Bohn et al Harper & Row Publishers, New

York.

6. Heat Transmission W. H. Mc Adams McGraw Hill Publication.

7. Engineering Heat Transfer Gupta and Prakash.

8. Heat and Mass Transfer:Fundamentals & Applications by Yunus Cengel, McGraw Hill

Publication





syllabus.

For 80 marks Paper:







27

CHE-210:STRENGTH OF MATERIAL





Unit 1 [10 Hrs]

Shear force & Bending moment:

Relation between load intensity, shear force and bending moment. Shear force & Bending

moment diagrams for simply supported, cantilever & overhanging beams with point loads &

UDL. Theory of simple bending & bending stress distribution. Shear stresses & shear stress

distribution in beam sections

Unit 2 [6 Hrs]

Simple Stresses & Strain:

Simple stress & strain due to tension, compression and. shear. Temperature stresses for section

of one material & more than one material.

Unit 3 [4 Hrs]

Principle Stresses & Strain:

Principle stresses & planes. Analysis of stresses on different planes in a material, two-

dimensional stress system. Mohr’s circle diagram for stress.

Unit 4 [6 Hrs]

Eccentric Loading:

Bending combined with axial loads. Eccentrically loaded short columns & chimneys. Axially

loaded long & short columns with different support conditions. Euler’s & Ranking’s method.

Unit 5 [8 Hrs]

Theory of Torsion:

Circular shafts subjected to torque- stress distribution & power transmission. Torsion combined

with bending & axial force. Strain Energy: Strain energy due to axial loads, bending, shear,

torsion & axial impact load.

Unit 6 [6 Hrs]

Thin & Thick Cylinders & Spheres:

Thin cylinders & spheres subjected to internal fluid pressure. Lame’s theory, design of thick

cylinders & spheres.

Reference Books

1. Mechanics of structure vol I by S. B. Junnarkar

2. Strength of materials by Singer F L

3. Strength of materials by Ramamurtham

4. Strength of materials by B C Punmia

5. Elements of strength of materials by Timoshenko & Young

28





syllabus.

For 80 marks Paper:







29

BSH226LAB-VI ENGINEERING CHEMISTRY


Practical: 4 Hrs/Week Practical: 50 Marks

Credit: 02

Practical Work

Minimum ten experiments, based on the syllabus, should be conducted during the course and



done during the course, the record of the experiments submitted by the candidate and viva-voce

based on the syllabus.


The experiment be based onfollowing list:

1. Identification of organic compounds based on functional group analysis. Physical

constants and derivatives. (at least 4 compounds)

2. Preparation of organic compounds (any three)

a) Preparation of acetanilide from aniline.

b) Preparation of meta-dinitrobenzene from benzene.

c) Preparation of iodoform from acetone.

d) Preparation of benzoic acid from benzaldehyde.

e) Preparation of aspirin form salicylic acid.

3. Estimation of following compounds (any three)

a) Carboxylic acid by titration method. Acetic acid.

b) Phenol by bromination.

c) Glucose by iodiometry method.

d) Esters by hydrolysis (ethyl acetate)

e) Aniline by bromination

f) Amide by hydrolysis (amide group) (acetamide)

30

BSH227 LAB-VII PHYSICAL CHEMISTRY AND THERMODYNAMICS



Credit: 01

Practical Work






Suggested list of experiments/studies

To determine the viscosity of the liquid.

1. To determine the specific and molecular refractions of unknown liquid by refractrometer.

2. To determine the normality of acetic acid and hydrochloric acid.

3. To determine the dissociation constants of acetic acids by pH meter.

4. To verify the Lambert-Beer law for Potassium dichromate, Potassium per magnet

and to prove the principal of additives.

5. To determine the energy of activation of liquid phase reaction.

6. To determine the unknown composition of Acetic acid in three-component system.

7. To determine the red ox potential in Ferrous-ferric system using potentiometer

8. Hydrolysis of ester in presence of hydrochloric acid.

9. Saponification of ester by sodium hydroxide.

10. Determination of rate of reaction in Zero order kinetics.

31

CHE228 LAB-VIII HEAT TRANSFER



Credit: 01

Practical Work







The experiment be based onfollowing list:

1. Thermal conductivity of composite wall.

2. Pin fins.

3. Forced convection apparatus.

4. Natural convective apparatus.

5. Emmisivity of test plate.

6. Dropwise and filmwise condensation

6. Stefan Boltzman apparatus.

7. Parallel flow /counter flow heat exchanger.

8. Pool boiling phenomena and critical heat flux.

9. Heat transfer on evaporator.

10. Thermal conductivity of insulating material.

11. Temperature profile in a metal rod.

12. Heat Transfer in Agitated Vessel.

13. Heat Transfer through Shell and Tube heat exchanger.

32

CHE229 LAB-IX: STRENGTH OF MATERIAL


Practical: 2Hrs/Week Term work: 50 Marks

Credit: 01

The term work will consist of a record of laboratory experiments and studies on following:

Part A (Any Five)

1. Tension test on ductile materials.

2. Bending test.

3. Shear test.

4. Torsion test.

5. Hardness test - Brinell & Rockwell.

6. Impact test.

Part B: Two exercises (each) on following

1. Shear Force & Bending Moment Diagram

2. Theory of bending.

3. Mohr’s circle for principal stresses.

4. Deflection of beams.

The term work will be a continuous assessment based on the experiments performed by the

student in the laboratory. The record of the experiments submitted by the student.

33

BSH 275: COMMUNICATION SKILLS-I


Practical: 2Hrs/Week Term work/Oral: 50 Marks

Credit: 01

The teacher shall explain in detail, the gist and techniques involved in the following work units

to the students. The teacher shall subsequently formulate the exercises to adjudge the skill sets

acquired by the students.

Unit 1 [04 Hrs]

Time Management:

Value of time, Diagnosing Time Management, Weekly Planner to do list and Prioritizing work.

Unit 2 [08 Hrs]

Grammar and Usage:

Overview of basic Mid-level English Grammar, Parts of speech, Preparations and Conditions,

Tense and Concept of time, Sentence Construction (Concord), Vocabulary: Words, Idioms,

Phrases, Antonyms and Synonyms

Unit 3 [08 Hrs]

Speaking Skills:

Training in Sound Recognition, the speech process, message, audience, speech style, feedback,

conversation and oral skills, fluency and self-expression body language phonetics and spoken

English, speaking techniques, word stress, correct stress patterns, voice quality, correct tone,

types of tones, Presentation skills-planning, preparation, organization, Stress and Intonation

pattern in spoken communication, Sound Recording Exercise (Language Lab Exercise),

Communication Errors in English

Unit 4 [08 Hrs]

Listening and Reading Skills:

Active and Passive Listening, the reading process, purpose, different kinds of texts, reference

material, scientific and technical texts, active and passive reading, strategies-vocabulary skills,

eye reading and visual perception, Skimming and scanning reading, drawing inferences and

conclusions, comprehension of technical material- scientific and technical texts, instructions and

technical manuals, graphic information. Note making- tool for study skills.

Unit 5 [06 Hrs]

Writing Skills:

Identification of different writing styles (Four Writing Style), Types of reports, information and

analytical reports, oral and written reports, formal and non-formal reports, printed forms, letter

and memo format, manuscript format, proposals, technical articles, journal articles and

conference papers, Drafting: Memo, Circulars, Notices, agendas etc. E-mails, Business Memos /

Letters, Employment Communication- resume design, resume style.

34

Unit 6 [08 Hrs]

Developing Skills and Presentations:

Developing key traits 1: creativity, critical thinking and problem solving. Effective

Presentations- Gathering Information and Building Presentation. Presentation by students in

team.

Text Books:

1. ‘Effective Technical Communication’ by M Ashraf Rizvi, Tata McGraw Hill Publishing

Company Ltd.

2. ‘Basic Managerial Skills for all’ E. H. McGrath, Eastern Economy Edition, Prentice

hall India.

3. ‘Developing Communication Skills’ Krishna Mohan, Meera Banerji, McMillan India Ltd.

4. Skills’ Krishna Mohan, Meera Banerji, McMillan India Ltd.

Term Work:

Term work marks should be given on the basis of online test conducted internally at college level.

scheme and detailed syllabusjnec.org/syllabus/chem/se-chemical-engineering-syllabus-2017-18.pdf ·...

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