sampling and analysis report for dredge sediment ...€¦ · 3.1 sampling and analysis methods...
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SAMPLING AND ANALYSIS REPORT FOR DREDGE SEDIMENT CHARACTERIZATION: SEWARD MARINE INDUSTRIAL CENTER IMPROVEMENTS SEWARD, ALASKA
Prepared for: City of Seward P.O. Box 167 Seward, Alaska 99664 September 3, 2013
Prepared by: R&M Consultants, Inc. 9101 Vanguard Drive Anchorage, Alaska 99507
Dredge Sediment Sampling Report i SMIC Improvements R&M Consultants, Inc. Seward, Alaska
SAMPLING AND ANALYSIS REPORT for DREDGE SEDIMENT CHARACTERIZATION:
SEWARD MARINE INDUSTRIAL CENTER IMPROVEMENTS SEWARD, ALASKA
TABLE OF CONTENTS TABLE OF CONTENTS ............................................................................................................. i LIST OF TABLES ...................................................................................................................... ii LIST OF APPENDICES ............................................................................................................. ii ACRONYMS & ABBREVIATIONS ....................................................................................... iii 1.0 INTRODUCTION .............................................................................................................. 1
1.1 Background and Objectives .................................................................................... 1 1.2 Purpose and Scope of Work .................................................................................... 1
2.0 REGIONAL SETTING AND SITE CONDITIONS .......................................................... 3 2.1 Location and Legal Description .............................................................................. 3
2.1.1 Geology and Subsurface Conditions ........................................................... 3 2.1.2 Dredge Sediment Characterization ............................................................. 3 2.1.3 Groundwater ................................................................................................ 4
3.0 ENVIRONMENTAL SAMPLING ..................................................................................... 5 3.1 Sampling and Analysis Methods ............................................................................ 5
3.1.1 Decontamination ......................................................................................... 6 3.1.2 Investigation Derived Wastes ..................................................................... 7
4.0 LABORATORY ANALYSIS ............................................................................................ 8 4.1 Soil Analysis ........................................................................................................... 8 4.2 Quality Assurance ................................................................................................... 8
5.0 LABORATORY ANALYTICAL RESULTS .................................................................. 10 5.1 Offshore Samples .................................................................................................. 10 5.2 Upland Samples .................................................................................................... 10
6.0 DISCUSSION AND RECOMMENDATIONS ................................................................ 11 7.0 REFERENCES .................................................................................................................. 13
Dredge Sediment Sampling Report ii SMIC Improvements R&M Consultants, Inc. Seward, Alaska
LIST OF TABLES Table 1 PID Readings (In PPM) From Upland Samples ............................................................ 6 Table 2 Laboratory Analytical Results, Soil Samples (May 2013) ............................................ 9
LIST OF APPENDICES APPENDIX A - SITE MAPS Location and Vicinity Map .......................................................................... Figure 1 Environmental Sample Location Map ......................................................... Figure 2
APPENDIX B - FIELD PHOTOGRAPHS Photographs of Environmental Sampling ................................... B-01 through B-03 APPENDIX C - LABORATORY ANALYTICAL RESULTS Offshore Samples SGS Laboratory Data Report #1132031 ..................................................... 76 Pages ADEC Laboratory Data Checklist ................................................................ 7 Pages Upland Samples SGS Laboratory Data Report #1132110 ................................................... 130 Pages ADEC Laboratory Data Checklist ................................................................ 7 Pages APPENDIX D -2013 SAMPLING AND ANALYSIS PLAN
Sampling and Analysis Plan For Dredge Sediment Characterization: Seward Marine Industrial Center Improvements, Seward, Alaska; Prepared by R&M Consultants, Inc., May 2013 ............................................................................................ 11 Pages
Dredge Sediment Sampling Report iii SMIC Improvements R&M Consultants, Inc. Seward, Alaska
ACRONYMS & ABBREVIATIONS AAC Alaska Administrative Code ADEC Alaska Department of Environmental Conservation ASTM American Society for Testing and Materials BGS Below Ground Surface BTEX Benzene, Toluene, Ethylbenzene, and Total Xylenes DMMP Dredged Material Management Program DRO Diesel Range Organics EPA U.S. Environmental Protection Agency GRO Gasoline Range Organics kg Kilograms mg Milligrams PID Photoionization Detector PPM Parts Per Million R&M R&M Consultants, Inc. RCRA Resource Conservation and Recovery Act RRO Residual Range Organics SAP Sampling and Analysis Plan SVOC Semi-Volatile Organic Compound TBT Tributyltin USACE United States Army Corps of Engineers USGS U.S. Geological Survey VOC Volatile Organic Compounds
Dredge Sediment Sampling Report 1 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
SAMPLING AND ANALYSIS REPORT for DREDGE SEDIMENT CHARACTERIZATION:
SEWARD MARINE INDUSTRIAL CENTER IMPROVEMENTS
SEWARD, ALASKA
1.0 INTRODUCTION
1.1 Background and Objectives R&M Consultants, Inc. (R&M) has been retained by the City of Seward to design and permit improvements to the existing Seward Marine Industrial Center (SMIC). The existing SMIC is a fairly open industrial harbor on the east side of Resurrection Bay (Figures 1 and 2); it was constructed in the early 1980s, and has been in operation since. The Seward Ships Drydock Inc. (SSDI) is a lessee at SMIC who offers upland storage and maintenance/repair areas for vessels and a 5,000-ton Syncrolift vessel haul out facility. The SMIC also hosts Polar Seafoods (a seafood processor) and the City’s 250-ton marine TraveLift. The North Dock, which is a sheetpile cargo dock, has a fuel header (owned/operated by Shoreside Petroleum, Inc.) that is connected via subsurface 6-inch diameter pipeline to an aboveground fuel storage tank (AST), (Figure 2). The existing SMIC basin has an approximate depth of -20 feet to -24 feet mean lower low water (MLLW). Proposed SMIC improvements generally include partially enclosing the harbor with a new breakwater on the west side, extending both the existing North Dock and East Dock, significantly enlarging the harbor basin by excavating/dredging inland, and adding moorage floats, gangways, utilities, and associated amenities (Figure 2).
A sampling and analysis plan (SAP) was prepared to set forth the dredge sediment characterization efforts that were performed for this project, to inform both the permitting process and disposal considerations (R&M, 2013a). Given the industrial character of the area, there is sufficient “reason to believe” that contaminants may be present in the discharge material to warrant sampling and chemical testing for the possible presence of petroleum constituents (DRO, GRO, RRO), VOC’s, and SVOC’s. TBT and metals have the greatest potential for being carried (e.g. in sandblast grit) by wind and water at the SMIC. Sampling for these constituents was conducted at a screening level. Previous sampling efforts within the project vicinity indicate that PCBs are not a contaminant of concern for this project (R&M, 2013a).
Two disposal scenarios are being considered for this project, offshore disposal (offshore area to be determined) and upland disposal (location or locations to be determined), or a combination thereof. The complete 2013 SAP is included in as Appendix D to this report for reference.
1.2 Purpose and Scope of Work The purpose of this Sampling Analysis Report is to characterize the upland and offshore soils proposed for dredging under the SMIC Improvements Project. The information contained in this report has been compiled to inform the City of Seward and the regulatory agencies of physical and environmental characteristics of sediment within the SMIC basin proposed for dredging and
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to guide the permitting and dredged sediment disposal efforts. More detailed information on the geotechnical characteristics of the SMIC subsurface may be found in R&M’s 2013 geotechnical report for the SMIC Improvement project (R&M, 2013b).
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2.0 REGIONAL SETTING AND SITE CONDITIONS
2.1 Location and Legal Description
Seward is situated along the southeastern coast of Alaska’s Kenai Peninsula at the head of Resurrection Bay (Figure 1). The SMIC is located on the east side of Resurrection Bay opposite the City of Seward off of Nash Road. The SMIC lies between Fourth of July Creek and Spring Creek. The legal description of the project study area is Section 18, Township 1 South, Range 1 East, Seward Meridian, USGS Quadrangle Seward A-7 SE (USGS, 1983). A 2011 aerial photograph-based site map of the project study area and surrounding areas is included as Figure 2 in Appendix A.
2.1.1 Geology and Subsurface Conditions The site is located on the fan-delta of Fourth of July Creek. Fan-deltas are complex deposits consisting of sand, gravel and cobbles with minor amounts of fines. The deposits grade to finer sand and silt farther from shore. The density of the material is typically loose to medium dense. Fan-deltas are produced by rapid deposition of material on a steep slope at the angle-of-repose (R&M, 2013a). The angle-of-repose is by definition at the limiting natural angle of gravitational stability. A number of geotechnical studies previously conducted in the vicinity of the SMIC site were reviewed to further characterize localized subsurface conditions. The boreholes from these references confirm that the deposits at the site generally consist of poorly graded gravel with sand interlayered with silty sand and silty gravel. Scattered thin layers of silt containing organic material were noted on some borehole logs (H4M, 1981; Tetratech, 1985; PND, 1987). Naturally-occurring heavy metal concentrations are common in the soils of the Seward area. High concentrations of naturally occurring arsenic, barium, chromium, and lead are expected in the soil analysis (E&E, 2007).
2.1.2 Dredge Sediment Characterization
Proposed dredging would occur to an approximate depth of -30 feet MLLW for offshore areas where deep draft vessel access is required and to a depth of -20 feet MLLW for expanded basin areas that may be created from excavating the nearby uplands. Gradation and material type is variable across the site but consists mostly of coarse-grained soils with minimal fine-grained soils (ASTM, 2000). Offshore surface material (to -30 feet MLLW) generally consists of silt (ML), well-graded sand with silt (SW-SM), poorly graded sand with gravel (SP), poorly graded gravel (GP), and well-graded gravel (GW). Geotechnical samples collected from upland boreholes to approximately 20 feet below MLLW consisted of poorly graded gravel with silt and sand (SP-SM), well-graded sand with silt (SW-SM), and well-graded gravel with silt (GW-GM). A full profile of the subsurface conditions is presented in R&M’s 2013 geotechnical report for the SMIC Improvement project (R&M, 2013b).
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2.1.3 Groundwater Groundwater levels in the upland portions of the project study area are variable as a result of the geology and tidal influences. The water table was encountered at the upland sample locations K through O, generally between 13 and 14.5 feet below ground surface (BGS); the water table at sample location M was notably deeper at 20.2 feet BGS.
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3.0 ENVIRONMENTAL SAMPLING
3.1 Sampling and Analysis Methods Environmental sampling and analysis was conducted in conjunction with the geotechnical drilling and sampling program. A truck-mounted drill rig was used to advance borings, both offshore (from a large landing craft) and onshore (Appendix B, Photo 1). In addition, a Petersen grab sampler (clamshell-style) was used from the landing craft to gather seafloor surface sediments (Appendix B, Photo 3). Sampling and decontamination methods were previously presented in the 2013 SAP (R&M, 2013a). Field work and sampling was conducted in general accordance with that document, as detailed herein. Offshore sampling was conducted from 24 to 26 May 2013. All soil samples were physically screened for visual and olfactory signs of contamination. No soil samples exhibited a hydrocarbon odor or displayed visual signs that contaminants were present. Sample locations R and T were accessible from the beach at low tide; samples were obtained with stainless steel spoons directly from the beach surface (Appendix B, Photo 2). Analytical samples for the remaining offshore sample locations (E, F, S, P, and Q) were collected from the landing craft. Seafloor surface sediment samples were collected with a Petersen grab sampler (Appendix B, Photo 4). For sample locations E and F, split-spoon soil samples were collected as close as possible (depending on wind/wave/tidal action) to five and ten feet below the seafloor per the sampling scheme presented in the 2013 SAP (R&M, 2013a). Upland sampling was conducted from 30 to 31 May 2013. All soil samples were physically screened for visual and olfactory signs of contamination. No soil samples exhibited a hydrocarbon odor or displayed visual signs that contaminants were present. Surface soil samples were collected by hand from approximately 0 to 6 inches below grade, after the surface soil was broken by the drill auger. Split-spoon soil samples were obtained at 1.5 feet below ground surface, then at five-foot increments to 40 feet below ground surface. Soil from each sample depth was first placed in the laboratory jars; remaining soil was used for field screening. Field screening with a MiniRAE photoionization detector (PID) was conducted by sealing soil within a zip-top bag, agitating it, and warming it to a minimum of five degrees Celsius. Field screening took place after volatile organic compounds, if present, were released from the soil for ten minutes but no longer than one hour. PID readings for each sample are presented in Table 1. Field screening results were intended to identify which samples were to be submitted for laboratory analysis. PID readings were all below 1.0 ppm and did not reveal any areas of contamination. Therefore sample depths were assigned to ensure a relatively even distribution of sample depths across the site. Samples were collected and submitted from saturated soils just above the groundwater table at each sample location (Table 1). Upland sample locations were generally located in open, sparsely-vegetated areas. The exception to this standard was sample site L which was located adjacent to a material stockpile near Nash Road (Appendix B, Photo 5). During the sampling effort, multiple loaders and construction equipment were observed loading and hauling away material from the stockpile. In addition, sample location M is located within the storage area leased by Polar Seafoods. Stored and stockpiled items consisted of trailers, tires, boats, appliances, fishing equipment, etc. (Appendix B, Photo 6).
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TABLE 1 - PID READINGS (IN PPM) FROM UPLAND SAMPLES Depth BGS
(feet) Upland Sample Locations (Figure 2)
K L M N O 0 (surface) 0.3* 0.0* 0.2* 0.1* 0.2*
1.5 0.3* 0.3* 0.2* 0.0* 0.3* 5 0.0 0.6 0.1* 0.0 0.2
10 0.0* 0.0 0.1 0.3* 0.1* - WT = 13' BGS WT = 13' BGS - WT = 14' BGS WT = 14.5' BGS
15 0.3 0.5* 0.0 0.1 0.1 20 0.0 0.3 0.1* 0.1 0.0 - - - WT = 20.2' BGS - -
25 0.0 0.2 0.0 0.1 0.2* 30 0.0 0.2 0.0 0.0* 0.0 35 0.0 0.4* 0.0 0.1 0.2 40 0* 0.0 0.0 0.0 0.0
Notes: WT = Water Table BGS = Below Ground Surface * Indicates sample was submitted to lab for analysis
For all locations, analytical soil samples were collected immediately after opening the split-spoon sampler, in order of decreasing volatility, beginning with gasoline range organics (GRO) and volatile organic compounds (VOC), followed by diesel range organics/residual range organics (DRO/RRO) and semi-volatile organic compounds (SVOC) and Resource Conservation and Recovery Act (RCRA) Metals, then tributyltin (TBT). The soil samples were collected from the spilt-spoon samplers with nitrile gloves and a clean, disposable stainless steel spoon. Soil samples were placed in new laboratory-grade glass jars, and sealed with Teflon-lined (as appropriate) screw caps. Methanol was used as a sample-covering preservative for soil samples intended for analysis for volatile fuel constituents (GRO and VOC). All sample containers were labeled immediately upon or prior to filling, and placed in a cooler on frozen gel packs along with a Chain-of Custody form, which identified the sample location, date, time, and collection personnel for all samples. Samples were maintained at a temperature of two to six degrees Celsius by R&M until delivery to SGS Laboratories in Anchorage. All holding time requirements were met.
3.1.1 Decontamination For the offshore sampling, the stainless steel tub used (for handling larger Petersen grab samples) and the split-spoon samplers were decontaminated in a three-step process. First the item was washed with sea water to remove soil and residue, then washed with a 1% Alconox/seawater solution, then rinsed with seawater. The grab sampler was rinsed off between sample locations by submersing it back into the seawater as many times as was needed to remove any residual sediment. For the upland sampling, the split-spoon samplers were decontaminated by a similar three-step process, only potable water was used in lieu of seawater. First the item was washed with fresh potable water to remove soil and residue, then washed with a 1% Alconox solution in potable water, then the item was rinsed with deionized water.
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3.1.2 Investigation Derived Wastes
Most soil was collected for either environmental sampling or geotechnical analysis. Any unused soil was discarded over the side of the vessel or spread on uplands adjacent to each sampling site. Decontamination water was discharged either over the side of the vessel or onsite and allowed to infiltrate near the borehole. Solid waste was bagged and placed in an appropriate dumpster or refuse container. There were no other excess potentially contaminated materials that required special disposal.
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4.0 LABORATORY ANALYSIS
The methods of the laboratory analysis portion of this sampling effort are presented below. The raw analytical data are presented in Appendix C.
4.1 Soil Analysis Based on “Reason to Believe” research on previous contaminant sources in the area, which is prescribed in the 2013 SAP (R&M, 2013a), soil samples were analyzed for DRO by test method AK102, GRO by test method AK101, VOC by test method 8260B, RRO by test method AK103, SVOC by test method 8270, RCRA Metals by test method 6020, and tributyltin by test method Krone 1989. RCRA metals include: arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver. The specific suite of analytical tests varied by borehole location and depth based on site history and the “reason to believe” analysis included in the 2013 SAP (R&M, 2013a). The samples were submitted for analysis to SGS Environmental Services, Inc. of Anchorage, Alaska, an Environmental Protection Agency (EPA) and Alaska Department of Environmental Conservation (ADEC) approved laboratory. A summary of sample analysis results is presented below in Table 2. The complete SGS lab reports and ADEC Laboratory Data Review Checklists are included in Appendix C. 4.2 Quality Assurance Samples were collected and submitted for laboratory analysis in a timely manner, well within the published hold times associated with each analytical method. Each analytical soil sample was given a unique identifier with the site ID (SMIC), location (borehole/sample letter), and sample depth in feet, namely SMIC-E (5’). Duplicate samples were collected at the rate of one duplicate per 10 samples, and were submitted for laboratory analysis in a manner identical to regular samples. Duplicate samples were collected in the same place and at the same depth as the regular sample with the same identifier, but noted with a “D”. Results of duplicate samples were examined for variation in analytical results by completing an ADEC Laboratory Data Review Checklist (Appendix C). Samples were found to be in generally good agreement. Silver was identified in the sample for SMIC-S(0) but not in the duplicate, and DRO was detected in the sample for SMIC-M(1.5) but not in its duplicate. As a result these samples had relative percent differences (RPD) of 200%. A roughly 140% difference was noted in the RRO results between sample SMIC-M (1.5) and its duplicate as well. DRO and RRO can be highly variable within a given quantity of soil obtained as grab samples, and this level of change between samples for this level of investigation is not considered noteworthy. All other RPDs were far below the ADEC-suggested 50% RPD threshold. Soil trip blanks preserved in methanol were transported in coolers containing samples to be analyzed for GRO and VOC. Trip blanks were analyzed for these constituents in conjunction with the collected samples. Trip blanks were all non-detect for GRO and VOCs. Chain-of-Custody documents accompanied all laboratory samples throughout the analytical process; they are included at the end of the laboratory reports in Appendix C. There were no deviations from quality control procedures during this investigation.
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TABLE 2: LABORATORY ANALYTICAL RESULTS, SOIL SAMPLES (MAY 2013) SAMPLE ID1 RRO (mg/kg) DRO (mg/kg) VOC (mg/kg) RCRA METALS (mg/kg) TBT (mg/kg) Toluene Arsenic Barium Chromium Lead Mercury Silver
OFF
SHO
RE
SAM
PLES
SMIC-E(0) 34.8 ND ND 9.50 62.0 41.0 11.0 ND ND ND SMIC-E(5) ND ND ND 3.83 26.6 25.2 5.42 ND ND ND SMIC-E(5)D ND ND ND 4.35 25.9 32.3 5.46 ND ND ND SMIC-E(10) ND ND ND 7.15 38.2 35.7 7.13 ND ND ND SMIC-F(0) ND ND ND 3.60 21.6 26.8 5.43 ND ND ND SMIC-F(4.5) ND ND ND 3.92 30.2 30.4 5.12 ND ND ND SMIC-F(8.5) ND ND ND 5.08 38.0 34.0 5.08 ND ND - SMIC-P(0) - - ND 15.2 64.0 47.2 13.8 0.0793 ND ND SMIC-Q(0) - - ND 8.99 47.0 38.7 9.40 0.0571 ND ND SMIC-R(0) - - ND 3.72 23.2 29.6 4.64 ND ND ND SMIC-S(0) 49.9 ND ND 22.0 81.4 57.5 20.0 0.1270 0.158 ND SMIC-S(0)D 66.4 ND ND 20.2 78.3 54.8 19.6 0.0950 ND ND SMIC-T(0) - - - 3.98 38.4 32.2 7.51 ND ND ND
UPL
AN
D S
AM
PLES
SMIC-K(0) 65.2 ND ND 4.31 35.3 35.3 5.87 ND ND ND SMIC-K(1.5) ND ND ND 3.69 29.5 31.3 4.72 ND ND ND SMIC-K(10) ND ND ND 6.14 50.1 37.2 5.80 ND ND - SMIC-K(40) ND ND ND 5.66 46.2 32.5 6.45 ND ND - SMIC-L(0) 267 45.1 ND 4.02 37.4 31.9 7.18 ND ND 0.0014 SMIC-L(1.5) ND ND ND 4.73 33.0 47.1 4.78 ND ND ND SMIC-L(15) ND ND ND 4.04 40.7 34.8 6.24 ND ND - SMIC-L(35) ND ND ND 6.57 46.2 35.3 7.27 ND ND - SMIC-M(0) 146 24.3 ND 4.19 33.9 32.0 5.05 ND ND 0.0033 SMIC-M(1.5) 184 32.6 ND 4.44 37.0 32.7 5.56 ND ND ND SMIC-M(1.5)D 36.3 ND ND 4.34 44.3 34.2 5.05 ND ND ND SMIC-M(5) ND ND ND 4.06 31.5 27.3 5.55 ND ND - SMIC-M(20) ND ND ND 4.66 43.0 34.2 5.59 ND ND - SMIC-N(0) 23.7 ND 50.5 14.3 32.9 39.3 7.88 0.0749 ND ND SMIC-N(1.5) 44.7 ND ND 17.3 30.0 36.6 9.04 0.0561 ND ND SMIC-N(10) ND ND ND 6.34 35.1 37.9 4.39 ND ND - SMIC-N(30) ND ND ND 8.08 50.3 29.2 7.48 ND ND - SMIC-O(0) ND ND 68.0 7.43 28.7 41.3 8.46 0.0745 ND ND SMIC-O(0)D ND ND 64.7 7.46 30.3 44.1 8.33 0.0861 ND ND SMIC-O(1.5) 39.2 ND ND 6.77 34.2 39.8 9.30 0.0591 ND ND SMIC-O(10) ND ND ND 4.46 36.3 33.4 4.71 ND ND - SMIC-O(25) ND ND ND 4.64 32.5 32.9 5.30 ND ND -
ADEC MIGRATION TO GROUNDWATER CLEANUP LEVELS2 9,700 230 6.5 3.9 1,100 25 NA 3 0.012 11.2 1,502 4
ADEC DIRECT CONTACT CLEANUP LEVELS2 8,3005 8,2505 6,600 3.7 16,600 250 400 25 410 1,502 4 DMMP SCREENING LEVELS6 NA7 NA7 NA7 5.7 NA7 260 450 0.410 6.10 0.0758 REPRESENTATIVE BACKGROUND LEVELS9 53.2 3.52 ND 9.8 218 34.8 6.2 0.11 0.58 - Notes:
ND = Analyte was not detected. (-) Indicates analyte was not sampled for. 1. Sample depths presented parenthetically in each sample name. 2. Method Two Cleanup Standards for migration to groundwater are the most stringent.; Cleanup levels for direct contact within the ‘over 40-inch zone’ (18 AAC 75 Table B) are less stringent and provide a more appropriate comparison for upland disposal options. 3. Migration to groundwater cleanup levels for lead have not been established. 4. Cleanup levels for tributyltin are currently under revision. The current cleanup level is 5,500 mg/kg; the proposed revised cleanup level is 1,502 mg/kg. 5. Direct contact cleanup levels are not presented in 18 AAC 75 Table B; cleanup levels for ingestion within the ‘over 40-inch zone’ are included here. 6. Screening levels identified in Table 8-2 DMMP Chemicals Of Concern and Regulatory Guidelines (DMMP, 2013) are being used to analyzed offshore disposal options. 7. Screening level for this analyte was not included in the DMMP guidance (DMMP, 2013). 8. Screening level for TBT was not included in the DMMP guidance; 0.075 mg/kg represents the bioaccumulation trigger (DMMP, 2013). 9. Background levels from similar studies used for comparison (E&E, 2007).
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5.0 LABORATORY ANALYTICAL RESULTS
Detectable contaminants have been summarized in Table 2. Various cleanup standards and criteria are listed at the bottom of the table for comparison purposes. These are discussed in more detail in Section 6.0.
5.1 Offshore Samples
The analytical results for the samples acquired offshore were generally non-detect (ND), and any detectable contaminants were found in seafloor surface samples. RRO was detected in relatively low concentrations at sample locations E at 34.8 mg/kg (surface) and S at 66.4 mg/kg (duplicate surface sample). Mercury was detected at sample locations P at 0.0793 mg/kg (surface), Q at 0.0571 mg/kg (surface), and S at 0.127 mg/kg (surface) and 0.0950 mg/kg (duplicate surface sample). Silver only was detected at sample location S at 0.158 mg/kg (surface). Arsenic, barium, chromium, and lead were detected in every sample. Arsenic levels ranged between 3.60 mg/kg (surface) at sample location F to 22.0 mg/kg (surface) at sample location S; barium ranged from 21.6 mg/kg (surface) at sample location F to 81.4 mg/kg (surface) at sample location S; chromium levels ranged from 25.2 mg/kg (5 feet BGS) at sample location E to 57.5 mg/kg (surface) at sample location S; lead levels ranged from 4.64 mg/kg (surface) at sample location R to 20.0 mg/kg (surface) at sample location S. Cadmium and selenium (remaining RCRA metals), TBT, VOC, and SVOC were not detected in any of the offshore samples (Table 2). 5.2 Upland Samples
The analytical results for the samples acquired from the upland locations reveal low concentrations of contaminants at the surface to 1.5 feet BGS. DRO was detected at sample locations L at 45.1 mg/kg (surface) and M at 24.3 mg/kg (surface) and 32.6 mg/kg (1.5 feet BGS). RRO was detected at each upland sample location either at the surface or at 1.5 feet BGS; concentrations ranged from 23.7 mg/kg at sample location N (surface) to 267 mg/kg at sample location L (surface). Toluene was the only VOC detected; it was encountered sample location N at 50.5 mg/kg (surface) and sample location O at 68.0 mg/kg (surface). Mercury was detected at sample locations N and O to 1.5 feet BGS; concentrations ranged from 0.0561 at sample location N (1.5 feet BGS) to 0.0861 at sample location O (surface). Arsenic, barium, chromium, and lead were detected in every sample. Arsenic levels ranged between 3.69 mg/kg at sample location K (1.5 feet BGS) to 17.3 mg/kg at sample location N (1.5 feet BGS); barium ranged from 28.7 mg/kg at sample location O (surface) to 50.3 mg/kg at sample location N (30 feet BGS); chromium levels ranged from 27.3 mg/kg at sample location M (5 feet BGS) to 47.1 mg/kg at sample location L (1.5 feet BGS); lead levels ranged from 4.39 mg/kg at sample location N (10 feet BGS) to 9.3 mg/kg at sample location O (1.5 feet BGS). TBT was detected at sample locations L and M at 0.0014 mg/kg (surface) and 0.0033 mg/kg (surface), respectively. Cadmium and selenium (remaining RCRA metals) and SVOC were not detected in any of the upland samples (Table 2).
Dredge Sediment Sampling Report 11 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
6.0 DISCUSSION AND RECOMMENDATIONS Based on the results of the environmental sampling effort, both offshore and upland disposal scenarios would be feasible. Soil sample analysis did not reveal any evidence of discrete contamination that would be of concern for offshore or upland disposal of dredged sediment. ADEC maintains permitting authority for upland disposal options of dredged sediment. ADEC Method Two cleanup levels are included in Table 2 for migration to groundwater (most stringent) and direct contact (18 AAC 75 Table B). ADEC has indicated that cleanup levels for migration to groundwater should be included in the preliminary assessment of analytical results; however, the direct contact levels represent a more appropriate comparison for upland disposal given the industrial nature and history of the SMIC facility. The USACE and the Environmental Protection Agency (EPA) provide oversight and permitting authority over offshore disposal of dredged sediment. There currently are no dredged material disposal criteria levels designated for Alaskan waters. For this reason, screening levels presented in guidance established by the Dredged Material Management Program (DMMP) of Washington State have been used to provide an analytical comparison for this sampling effort (DMMP, 2013). Multiple cleanup levels are presented in the Dredged Material Evaluation and Disposal Procedures, User Manual (July, 2013). Screening levels (SL) represent values defined for typical chemicals of concern; concentrations at or below the SL indicate there is no reason to believe that offshore disposal of dredged material would result in adverse effects. SL values are presented in Table 2 and used as a tool to assess the appropriateness and feasibility for offshore disposal. Petroleum hydrocarbon detections (DRO and RRO) are minimal and restricted to surface soils, and are significantly below ADEC cleanup levels; the DMMP has not established screening levels for petroleum hydrocarbons. Surface soil RRO, DRO, and toluene detections appear to reflect the industrial nature of the facility and area, and do not indicate an existing contamination issue. Detected RCRA metals include arsenic, barium, chromium, lead, mercury, and silver. With the exception of arsenic, all metals were detected at levels below ADEC direct contact cleanup levels and DMMP screening levels. Therefore, the presence of these metals would not be a concern for upland or offshore disposal of dredged sediment. Note that barium was not included as a chemical of concern in the DMMP guidance. Arsenic concentrations exceeded ADEC cleanup levels in every sample and exceeded DMMP screening levels in approximately half of the samples (Table 2). The ADEC cleanup levels and out of state DMMP Guidance do not account for naturally occurring metals found in the project area soils. Previous studies and current literature indicate that detection of arsenic, chromium, and mercury is anticipated and that the detected levels are generally consistent with naturally-occurring concentrations (E&E, 2007; USGS, 1997). In consideration of these naturally-occurring levels, the analytical results for arsenic (as well as chromium and mercury) are comparable to background levels even though they exceed standardized ADEC cleanup and DMMP screening levels. TBT is commonly used in marine paints. TBT was detected at only two upland surface sample locations at levels significantly below current and proposed ADEC cleanup levels. A screening
Dredge Sediment Sampling Report 12 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
level for TBT was not included in the DMMP guidance, but detectable results were below identified bioaccumulation trigger levels (DMMP, 2013).As a result, TBT is not anticipated to pose a risk of contamination for either upland or offshore disposal options (Table 2).
Dredge Sediment Sampling Report 13 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
7.0 REFERENCES
Alaska Department of Environmental Conservation (18 AAC 75), Oil and Other Hazardous Substances Pollution Control, 18 AAC 75.340 Soil Cleanup Levels, General Requirements, Amended as of 8 April 2012.
American Society for Testing and Materials (ASTM, 2000), “Standard Practice for Classification
of Soils for Engineering Purposes (Unified Classification System)”, Designation D 2487-00.
Dredged Material Management Program (DMMP, 2013), “Dredged Material Evaluation and
Disposal Procedures User Manual” Prepared by U.S. Army Corps of Engineers-Seattle District and Environmental Protection Agency- Region 10, July 2013.
Ecology and Environment, Inc. (E&E, 2007), “Seward Ship’s Dry Dock Site Inspection, Seward,
Alaska,” Prepared for the U.S. Environmental Protection Agency, September, 2007. H4M Corporation (H4M, 1981), “Preliminary Report Soils Exploration, Fourth of July Creek,
Seward, Alaska”, August 17, 1981.
Peratrovich, Nottingham & Drage, Inc. (PND, 1987), “Seward Marine Industrial Center, North Dock Geotechnical Study” November, 1987.
R&M Consultants, Inc. (R&M, 2013a), “Sampling and Analysis Plan for Dredge Sediment
Characterization: Seward Marine Industrial Center Improvements, Seward, Alaska”, Prepared for City of Seward, May 15, 2013.
R&M Consultants, Inc. (R&M, 2013b), “Geotechnical Analysis: Seward Marine Industrial
Center Improvements, Seward, Alaska”, Prepared for City of Seward, (currently in production).
Tetratech Limited (Tetratech, 1985), “Report of Geotechnical Investigations, Fourth of July
Creek Marine Industrial Park, Seward, Alaska”, October 4, 1985. U.S. Geological Survey (USGS, 1983), “Seward A-7 SE Quadrangle, Alaska”, As viewed on
National Geographic’s TOPO!, Version 4.2.6. U.S. Geological Survey (USGS, 1997), Environmental Studies of Mineral Deposits in Alaska,
U.S. Geological Survey Bulletin 2156, 1997.
APPENDIX A
SITE MAPS Location and Vicinity Map .......................................................................... Figure 1 Environmental Sample Location Map ......................................................... Figure 2
PROJECT
AREA
P
A
C
IF
IC
O
C
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A
N
B
E
R
IN
G
S
E
A
A
R
C
T
I
C
O
C
E
A
N
PROJECT
LOCATION
NOME
FAIRBANKS
ANCHORAGE
KODIAK
00 60003000
SCALE IN FEET
SEWARD
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1
0
0
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9
0
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0
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9
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-10
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0
'
-20.0'
-20.0'
-2
0.0
'
NO
RTH
D
OCK
APPROX. LOCATION
BURIED PIPELINE
SHORESIDE
PETROLEUM AST
M
SPRIN
G CREEK
TRAVEL
LIFT
RESURRECTION
BAY
ANALYTICAL SAMPLES
COLLECTED FROM
BEACH AT LOW TIDE
POLAR
SEAFOODS
K
O
LEGEND
SURFACE AND SUBSURFACE SAMPLES OBTAINED
SURFACE SAMPLE ONLY
PROPOSED DREDGE LIMITS
2
X
X
APPENDIX B
FIELD PHOTOGRAPHS Photographs of Environmental Sampling ................................... B-01 through B-03
Dredge Sediment Sampling Report B-01 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
Photo 1: Landing craft with truck mounted drill-rig at rear of vessel (24 May 2013).
Photo 2: Surface sample R collected from beach at low tide (24 May 2013).
Dredge Sediment Sampling Report B-02 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
Photo 3: Obtaining surface sample from seafloor using Peterson Grab Sampler (24 May 2013).
Photo 4: Surface sample collected at location Q (25 May 2013).
Dredge Sediment Sampling Report B-03 SMIC Improvements R&M Consultants, Inc. Seward, Alaska
Photo 5: Typical upland sample area; sample location O is shown in photo looking northeast.
Note material stockpile in background (31 May 2013).
Photo 6: Sample location M within Polar Seafoods leased storage area. Note type and quantity of stored material in background (31 May 2013)
APPENDIX C
LABORATORY ANALYTICAL RESULTS Offshore Samples SGS Laboratory Data Report #1132031 ....................................................................... C1 - C151 ADEC Laboratory Data Checklist ............................................................................ C152 - C158 Upland Samples SGS Laboratory Data Report #1132110 ................................................................... C159 - C418 ADEC Laboratory Data Checklist ............................................................................ C419 - C425
Report Number: 1132031
Client Project: SMIC Improvements 1770.01
Laboratory Report of Analysis
Dear Kevin Pendergast,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of fourteen (14) days from the date of this
report unless other archiving requirements were included in the quote.
If there are any questions about the report or services performed during this project, please call Steve at (907)
562-2343. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Steve Crupi Date
Project [email protected]
To: R & M Consultants Inc
9101 Vanguard Dr
Anchorage, AK 99507
(907)522-1707
Print Date: 06/18/2013 11:16:51AM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C1
Case NarrativeRNMCONP R & M Consultants Inc1132031 SMIC Improvements 1770.01
Customer:Project:
SGS North America Inc.
Refer to the sample receipt form for information on sample condition.
1132031001 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031002 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031003 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031004 PS 4.5Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031006 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
1132031007 PS 5Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031008 PS 10Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031009 PS 5) Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031010 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
1132031011 PS 0) Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
1132031012 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1132031013 PS 0Krone 1989 - TBT was analyzed by ALS of Kelso, WA.
1150322 LCS XXX/290748270D - LCS recovery for dimethylphthalate, di-n-butylphthalate and chrysene is outside of QC criteria (biased high). These analytes were not detected above the LOQ in the associated samples.
1150436 MS 0)(1132031013MS6020 - Metals - MS recoveries for barium and chromium were outside of acceptance criteria . Post digestion spike was successful.
1150437 MSD 0)(1132031013MSD6020 - Metals - MSD recovery for barium was outside of acceptance criteria. Post digestion spike was successful.
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to the associated field samples.
C2
Laboratory ID Client Sample ID Analytical Batch Analyte Reason
Report of Manual Integrations
SW8270D
SMIC-E (0) XMS7348 Benzo[k]fluoranthene RP1132031006
SMIC-E (0) XMS7348 Benzoic acid RP1132031006
LCS for HBN 1452070 [XXX/29074 XMS7345 1-Chloronaphthalene RSP1150322
LCS for HBN 1452070 [XXX/29074 XMS7345 2-Chloronaphthalene RSP1150322
1132031006MS XMS7348 1-Chloronaphthalene RSP1150324
1132031006MS XMS7348 2-Chloronaphthalene RSP1150324
1132031006MSD XMS7348 1-Chloronaphthalene RP1150325
CCV for HBN 1453101 [XMS/7348] XMS7348 1-Chloronaphthalene BLC1150959
Manual Integration Reason Code Descriptions
Code Description
O Original Chromatogram
M Modified Chromatogram
SS Skimmed surrogate
BLG Closed baseline gap
RP Reassign peak name
PIR Pattern integration required
IT Included tail
SP Split peak
RSP Removed split peak
FPS Forced peak start/stop
BLC Baseline correction
PNF Peak not found by software
All DRO/RRO analysis are integrated per SOP.
Print Date: 06/18/2013 11:16:52AM
Member of SGS Group
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C3
Laboratory Qualifiers
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their
entirety and SGS is not responsible for use of less than the complete report. If you have any questions regarding this
report, or if we can be of any other assistance, please contact your SGS Project Manager at 907-562-2343. All work is
provided under SGS general terms and conditions (<http://www.sgs.com/terms_and_conditions.htm>), unless other
written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan
(QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971
(DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and 2944.01 for DOD ELAP/ISO17025 (RCRA methods:
1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6020, 7470A, 7471B, 8021B, 8082A, 8260B, 8270D,
8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and
data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, other regulatory
authorities.
The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
IB Instrument Blank
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 06/18/2013 11:16:52AM
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SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
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C4
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
SMIC-R-(0) 1132031001 05/24/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-T-(0) 1132031002 05/24/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-F-(0) 1132031003 05/24/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-F (4.5) 1132031004 05/24/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-F (8.5) 1132031005 05/24/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-E (0) 1132031006 05/25/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-E (5) 1132031007 05/25/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-E (10) 1132031008 05/25/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-E (5) D 1132031009 05/25/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-S-(0) 1132031010 05/26/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-S (0) D 1132031011 05/26/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-P (0) 1132031012 05/26/2013 05/28/2013 Soil/Solid (dry weight)
SMIC-Q (0) 1132031013 05/26/2013 05/28/2013 Soil/Solid (dry weight)
Trip Blank 1 1132031014 05/24/2013 05/28/2013 Soil/Solid (dry weight)
Trip Blank 2 1132031015 05/24/2013 05/28/2013 Soil/Solid (dry weight)
Method DescriptionMethod
Diesel/Residual Range OrganicsAK103
Diesel/Residual Range OrganicsAK102
Gasoline Range Organics (S)AK101
Percent Solids SM2540GSM21 2540G
RCRA Metals by ICP-MSSW6020
SW846 8270 Semi-Volatiles by GC/MS (S)SW8270D
VOC 8260 (S) Field ExtractedSW8260B
Print Date: 06/18/2013 11:16:53AM
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SGS North America Inc.200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C5
Detectable Results Summary
Client Sample ID: SMIC-R-(0)
Lab Sample ID: 1132031001 UnitsParameter Result
Arsenic mg/Kg3.72Metals by ICP/MS
Barium mg/Kg23.2
Chromium mg/Kg29.6
Lead mg/Kg4.64
Client Sample ID: SMIC-T-(0)
Lab Sample ID: 1132031002 UnitsParameter Result
Arsenic mg/Kg3.98Metals by ICP/MS
Barium mg/Kg38.4
Chromium mg/Kg32.2
Lead mg/Kg7.51
Client Sample ID: SMIC-F-(0)
Lab Sample ID: 1132031003 UnitsParameter Result
Arsenic mg/Kg3.60Metals by ICP/MS
Barium mg/Kg21.6
Chromium mg/Kg26.8
Lead mg/Kg5.43
Client Sample ID: SMIC-F (4.5)
Lab Sample ID: 1132031004 UnitsParameter Result
Arsenic mg/Kg3.92Metals by ICP/MS
Barium mg/Kg30.2
Chromium mg/Kg30.4
Lead mg/Kg5.12
Client Sample ID: SMIC-F (8.5)
Lab Sample ID: 1132031005 UnitsParameter Result
Arsenic mg/Kg5.08Metals by ICP/MS
Barium mg/Kg38.0
Chromium mg/Kg34.0
Lead mg/Kg5.08
Client Sample ID: SMIC-E (0)
Lab Sample ID: 1132031006 UnitsParameter Result
Arsenic mg/Kg9.50Metals by ICP/MS
Barium mg/Kg62.0
Chromium mg/Kg41.0
Lead mg/Kg11.0
Residual Range Organics mg/Kg34.8Semivolatile Organic Fuels
Client Sample ID: SMIC-E (5)
Lab Sample ID: 1132031007 UnitsParameter Result
Arsenic mg/Kg3.83Metals by ICP/MS
Barium mg/Kg26.6
Chromium mg/Kg25.2
Lead mg/Kg5.42
Print Date: 06/18/2013 11:16:53AM
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SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
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C6
Detectable Results Summary
Client Sample ID: SMIC-E (10)
Lab Sample ID: 1132031008 UnitsParameter Result
Arsenic mg/Kg7.15Metals by ICP/MS
Barium mg/Kg38.2
Chromium mg/Kg35.7
Lead mg/Kg7.13
Client Sample ID: SMIC-E (5) D
Lab Sample ID: 1132031009 UnitsParameter Result
Arsenic mg/Kg4.35Metals by ICP/MS
Barium mg/Kg25.9
Chromium mg/Kg32.3
Lead mg/Kg5.46
Client Sample ID: SMIC-S-(0)
Lab Sample ID: 1132031010 UnitsParameter Result
Arsenic mg/Kg22.0Metals by ICP/MS
Barium mg/Kg81.4
Chromium mg/Kg57.5
Lead mg/Kg20.0
Mercury mg/Kg0.127
Silver mg/Kg0.158
Residual Range Organics mg/Kg49.9Semivolatile Organic Fuels
Client Sample ID: SMIC-S (0) D
Lab Sample ID: 1132031011 UnitsParameter Result
Arsenic mg/Kg20.2Metals by ICP/MS
Barium mg/Kg78.3
Chromium mg/Kg54.8
Lead mg/Kg19.6
Mercury mg/Kg0.0950
Residual Range Organics mg/Kg66.4Semivolatile Organic Fuels
Client Sample ID: SMIC-P (0)
Lab Sample ID: 1132031012 UnitsParameter Result
Arsenic mg/Kg15.2Metals by ICP/MS
Barium mg/Kg64.0
Chromium mg/Kg47.2
Lead mg/Kg13.8
Mercury mg/Kg0.0793
Client Sample ID: SMIC-Q (0)
Lab Sample ID: 1132031013 UnitsParameter Result
Arsenic mg/Kg8.99Metals by ICP/MS
Barium mg/Kg47.0
Chromium mg/Kg38.7
Lead mg/Kg9.40
Mercury mg/Kg0.0571
Print Date: 06/18/2013 11:16:53AM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
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C7
Client Sample ID: SMIC-R-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031001
Lab Project ID: 1132031
Collection Date: 05/24/13 07:34
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Metals by ICP/MS
Results of SMIC-R-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.72 mg/Kg 101.09 0.339 05/31/13 12:51
Barium 23.2 mg/Kg 100.328 0.103 05/31/13 12:51
Cadmium 0.219 mg/Kg 10U 0.219 0.0678 05/31/13 12:51
Chromium 29.6 mg/Kg 100.437 0.131 05/31/13 12:51
Lead 4.64 mg/Kg 100.219 0.0678 05/31/13 12:51
Mercury 0.0437 mg/Kg 10U 0.0437 0.0131 05/31/13 12:51
Selenium 0.547 mg/Kg 10U 0.547 0.164 05/31/13 12:51
Silver 0.109 mg/Kg 10U 0.109 0.0339 05/31/13 12:51
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.088 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 12:51
Container ID: 1132031001-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C8
Client Sample ID: SMIC-R-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031001
Lab Project ID: 1132031
Collection Date: 05/24/13 07:34
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Semivolatile Organic GC/MS
Results of SMIC-R-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
1,2-Dichlorobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
1,3-Dichlorobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
1,4-Dichlorobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
1-Chloronaphthalene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,4,5-Trichlorophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,4,6-Trichlorophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,4-Dichlorophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,4-Dimethylphenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,4-Dinitrophenol 3.57 mg/Kg 1U 3.57 1.12 05/31/13 01:00
2,4-Dinitrotoluene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,6-Dichlorophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2,6-Dinitrotoluene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Chloronaphthalene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Chlorophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Methyl-4,6-dinitrophenol 2.38 mg/Kg 1U 2.38 0.739 05/31/13 01:00
2-Methylnaphthalene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Methylphenol (o-Cresol) 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Nitroaniline 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
2-Nitrophenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
3&4-Methylphenol (p&m-Cresol) 1.19 mg/Kg 1U 1.19 0.369 05/31/13 01:00
3,3-Dichlorobenzidine 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
3-Nitroaniline 0.596 mg/Kg 1U 0.596 0.179 05/31/13 01:00
4-Bromophenyl-phenylether 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
4-Chloro-3-methylphenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
4-Chloroaniline 0.596 mg/Kg 1U 0.596 0.179 05/31/13 01:00
4-Chlorophenyl-phenylether 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
4-Nitroaniline 3.57 mg/Kg 1U 3.57 1.12 05/31/13 01:00
4-Nitrophenol 1.19 mg/Kg 1U 1.19 0.369 05/31/13 01:00
Acenaphthene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Acenaphthylene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Aniline 2.38 mg/Kg 1U 2.38 0.739 05/31/13 01:00
Anthracene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Azobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzo(a)Anthracene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzo[a]pyrene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzo[b]Fluoranthene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzo[g,h,i]perylene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzo[k]fluoranthene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Benzoic acid 1.79 mg/Kg 1U 1.79 0.893 05/31/13 01:00
Benzyl alcohol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Bis(2-Chloroethoxy)methane 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Bis(2-Chloroethyl)ether 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
bis(2-Ethylhexyl)phthalate 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C9
Client Sample ID: SMIC-R-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031001
Lab Project ID: 1132031
Collection Date: 05/24/13 07:34
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Semivolatile Organic GC/MS
Results of SMIC-R-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Butylbenzylphthalate 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Carbazole 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Chrysene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Di-n-butylphthalate 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
di-n-Octylphthalate 0.596 mg/Kg 1U 0.596 0.179 05/31/13 01:00
Dibenzo[a,h]anthracene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Dibenzofuran 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Diethylphthalate 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Dimethylphthalate 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Fluoranthene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Fluorene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Hexachlorobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Hexachlorobutadiene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Hexachlorocyclopentadiene 0.834 mg/Kg 1U 0.834 0.238 05/31/13 01:00
Hexachloroethane 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Indeno[1,2,3-c,d] pyrene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Isophorone 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
N-Nitroso-di-n-propylamine 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
N-Nitrosodimethylamine 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
N-Nitrosodiphenylamine 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Naphthalene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Nitrobenzene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Pentachlorophenol 2.38 mg/Kg 1U 2.38 0.739 05/31/13 01:00
Phenanthrene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Phenol 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Pyrene 0.298 mg/Kg 1U 0.298 0.0929 05/31/13 01:00
Surrogates
2,4,6-Tribromophenol 94 % 135-125 05/31/13 01:00
2-Fluorobiphenyl 87 % 145-105 05/31/13 01:00
2-Fluorophenol 72.7 % 135-105 05/31/13 01:00
Nitrobenzene-d5 75.2 % 135-100 05/31/13 01:00
Phenol-d6 78.6 % 140-100 05/31/13 01:00
Terphenyl-d14 106 % 130-125 05/31/13 01:00
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.462 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 01:00
Container ID: 1132031001-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C10
Client Sample ID: SMIC-T-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031002
Lab Project ID: 1132031
Collection Date: 05/24/13 07:53
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Metals by ICP/MS
Results of SMIC-T-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.98 mg/Kg 100.999 0.310 05/31/13 12:53
Barium 38.4 mg/Kg 100.300 0.0939 05/31/13 12:53
Cadmium 0.200 mg/Kg 10U 0.200 0.0619 05/31/13 12:53
Chromium 32.2 mg/Kg 100.399 0.120 05/31/13 12:53
Lead 7.51 mg/Kg 100.200 0.0619 05/31/13 12:53
Mercury 0.0399 mg/Kg 10U 0.0399 0.0120 05/31/13 12:53
Selenium 0.499 mg/Kg 10U 0.499 0.150 05/31/13 12:53
Silver 0.0999 mg/Kg 10U 0.0999 0.0310 05/31/13 12:53
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.091 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 12:53
Container ID: 1132031002-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C11
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Metals by ICP/MS
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.60 mg/Kg 101.08 0.335 05/31/13 12:55
Barium 21.6 mg/Kg 100.324 0.102 05/31/13 12:55
Cadmium 0.216 mg/Kg 10U 0.216 0.0670 05/31/13 12:55
Chromium 26.8 mg/Kg 100.432 0.130 05/31/13 12:55
Lead 5.43 mg/Kg 100.216 0.0670 05/31/13 12:55
Mercury 0.0432 mg/Kg 10U 0.0432 0.0130 05/31/13 12:55
Selenium 0.541 mg/Kg 10U 0.541 0.162 05/31/13 12:55
Silver 0.108 mg/Kg 10U 0.108 0.0335 05/31/13 12:55
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.058 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 12:55
Container ID: 1132031003-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C12
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Semivolatile Organic Fuels
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.6 mg/Kg 1U 22.6 7.00 06/04/13 12:02
Surrogates
5a Androstane 93.6 % 150-150 06/04/13 12:02
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.376 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:02
Container ID: 1132031003-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.6 mg/Kg 1U 22.6 7.00 06/04/13 12:02
Surrogates
n-Triacontane-d62 99.3 % 150-150 06/04/13 12:02
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.376 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:02
Container ID: 1132031003-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C13
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Semivolatile Organic GC/MS
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
1,2-Dichlorobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
1,3-Dichlorobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
1,4-Dichlorobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
1-Chloronaphthalene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,4,5-Trichlorophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,4,6-Trichlorophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,4-Dichlorophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,4-Dimethylphenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,4-Dinitrophenol 3.42 mg/Kg 1U 3.42 1.07 05/31/13 01:17
2,4-Dinitrotoluene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,6-Dichlorophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2,6-Dinitrotoluene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Chloronaphthalene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Chlorophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Methyl-4,6-dinitrophenol 2.28 mg/Kg 1U 2.28 0.707 05/31/13 01:17
2-Methylnaphthalene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Methylphenol (o-Cresol) 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Nitroaniline 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
2-Nitrophenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
3&4-Methylphenol (p&m-Cresol) 1.14 mg/Kg 1U 1.14 0.353 05/31/13 01:17
3,3-Dichlorobenzidine 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
3-Nitroaniline 0.570 mg/Kg 1U 0.570 0.171 05/31/13 01:17
4-Bromophenyl-phenylether 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
4-Chloro-3-methylphenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
4-Chloroaniline 0.570 mg/Kg 1U 0.570 0.171 05/31/13 01:17
4-Chlorophenyl-phenylether 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
4-Nitroaniline 3.42 mg/Kg 1U 3.42 1.07 05/31/13 01:17
4-Nitrophenol 1.14 mg/Kg 1U 1.14 0.353 05/31/13 01:17
Acenaphthene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Acenaphthylene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Aniline 2.28 mg/Kg 1U 2.28 0.707 05/31/13 01:17
Anthracene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Azobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzo(a)Anthracene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzo[a]pyrene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzo[b]Fluoranthene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzo[g,h,i]perylene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzo[k]fluoranthene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Benzoic acid 1.71 mg/Kg 1U 1.71 0.855 05/31/13 01:17
Benzyl alcohol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Bis(2-Chloroethoxy)methane 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Bis(2-Chloroethyl)ether 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
bis(2-Ethylhexyl)phthalate 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C14
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Semivolatile Organic GC/MS
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Butylbenzylphthalate 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Carbazole 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Chrysene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Di-n-butylphthalate 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
di-n-Octylphthalate 0.570 mg/Kg 1U 0.570 0.171 05/31/13 01:17
Dibenzo[a,h]anthracene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Dibenzofuran 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Diethylphthalate 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Dimethylphthalate 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Fluoranthene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Fluorene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Hexachlorobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Hexachlorobutadiene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Hexachlorocyclopentadiene 0.798 mg/Kg 1U 0.798 0.228 05/31/13 01:17
Hexachloroethane 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Indeno[1,2,3-c,d] pyrene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Isophorone 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
N-Nitroso-di-n-propylamine 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
N-Nitrosodimethylamine 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
N-Nitrosodiphenylamine 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Naphthalene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Nitrobenzene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Pentachlorophenol 2.28 mg/Kg 1U 2.28 0.707 05/31/13 01:17
Phenanthrene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Phenol 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Pyrene 0.285 mg/Kg 1U 0.285 0.0889 05/31/13 01:17
Surrogates
2,4,6-Tribromophenol 94 % 135-125 05/31/13 01:17
2-Fluorobiphenyl 91.6 % 145-105 05/31/13 01:17
2-Fluorophenol 70.6 % 135-105 05/31/13 01:17
Nitrobenzene-d5 72.9 % 135-100 05/31/13 01:17
Phenol-d6 77.7 % 140-100 05/31/13 01:17
Terphenyl-d14 108 % 130-125 05/31/13 01:17
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.569 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 01:17
Container ID: 1132031003-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C15
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Volatile Fuels
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.08 mg/Kg 1U 2.08 0.624 06/05/13 12:33
Surrogates
4-Bromofluorobenzene 94.6 % 150-150 06/05/13 12:33
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/24/13 12:58
Prep Initial Wt./Vol.: 104.996 g
Prep Extract Vol: 38.1955 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 12:33
Container ID: 1132031003-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C16
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Volatile GC/MS
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,1,1-Trichloroethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,1,2,2-Tetrachloroethane 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
1,1,2-Trichloroethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,1-Dichloroethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,1-Dichloroethene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,1-Dichloropropene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2,3-Trichlorobenzene 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
1,2,3-Trichloropropane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2,4-Trichlorobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2,4-Trimethylbenzene 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
1,2-Dibromo-3-chloropropane 83.2 ug/Kg 1U 83.2 25.8 05/30/13 23:27
1,2-Dibromoethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2-Dichlorobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2-Dichloroethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,2-Dichloropropane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,3,5-Trimethylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,3-Dichlorobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,3-Dichloropropane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
1,4-Dichlorobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
2,2-Dichloropropane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
2-Butanone (MEK) 208 ug/Kg 1U 208 64.9 05/30/13 23:27
2-Chlorotoluene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
2-Hexanone 208 ug/Kg 1U 208 64.9 05/30/13 23:27
4-Chlorotoluene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
4-Isopropyltoluene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
4-Methyl-2-pentanone (MIBK) 208 ug/Kg 1U 208 64.9 05/30/13 23:27
Benzene 10.4 ug/Kg 1U 10.4 3.25 05/30/13 23:27
Bromobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Bromochloromethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Bromodichloromethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Bromoform 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Bromomethane 166 ug/Kg 1U 166 51.6 05/30/13 23:27
Carbon disulfide 83.2 ug/Kg 1U 83.2 25.8 05/30/13 23:27
Carbon tetrachloride 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Chlorobenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Chloroethane 166 ug/Kg 1U 166 51.6 05/30/13 23:27
Chloroform 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Chloromethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
cis-1,2-Dichloroethene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
cis-1,3-Dichloropropene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Dibromochloromethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Dibromomethane 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Dichlorodifluoromethane 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C17
Client Sample ID: SMIC-F-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031003
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 87.4
Results by Volatile GC/MS
Results of SMIC-F-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Hexachlorobutadiene 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
Isopropylbenzene (Cumene) 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Methyl-t-butyl ether 83.2 ug/Kg 1U 83.2 25.8 05/30/13 23:27
Methylene chloride 83.2 ug/Kg 1U 83.2 25.8 05/30/13 23:27
n-Butylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
n-Propylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Naphthalene 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
o-Xylene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
P & M -Xylene 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
sec-Butylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Styrene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
tert-Butylbenzene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Tetrachloroethene 10.4 ug/Kg 1U 10.4 3.25 05/30/13 23:27
Toluene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
trans-1,2-Dichloroethene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
trans-1,3-Dichloropropene 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Trichloroethene 10.4 ug/Kg 1U 10.4 3.25 05/30/13 23:27
Trichlorofluoromethane 41.6 ug/Kg 1U 41.6 12.5 05/30/13 23:27
Vinyl chloride 20.8 ug/Kg 1U 20.8 6.49 05/30/13 23:27
Xylenes (total) 83.2 ug/Kg 1U 83.2 25.8 05/30/13 23:27
Surrogates
1,2-Dichloroethane-D4 99.2 % 179-118 05/30/13 23:27
4-Bromofluorobenzene 94.1 % 167-138 05/30/13 23:27
Toluene-d8 94.7 % 185-115 05/30/13 23:27
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/24/13 12:58
Prep Initial Wt./Vol.: 104.996 g
Prep Extract Vol: 38.1955 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/30/13 23:27
Container ID: 1132031003-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C18
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Metals by ICP/MS
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.92 mg/Kg 101.18 0.366 05/31/13 12:58
Barium 30.2 mg/Kg 100.354 0.111 05/31/13 12:58
Cadmium 0.236 mg/Kg 10U 0.236 0.0731 05/31/13 12:58
Chromium 30.4 mg/Kg 100.472 0.142 05/31/13 12:58
Lead 5.12 mg/Kg 100.236 0.0731 05/31/13 12:58
Mercury 0.0472 mg/Kg 10U 0.0472 0.0142 05/31/13 12:58
Selenium 0.590 mg/Kg 10U 0.590 0.177 05/31/13 12:58
Silver 0.118 mg/Kg 10U 0.118 0.0366 05/31/13 12:58
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.008 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 12:58
Container ID: 1132031004-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C19
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Semivolatile Organic Fuels
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 23.5 mg/Kg 1U 23.5 7.27 06/04/13 12:11
Surrogates
5a Androstane 78.9 % 150-150 06/04/13 12:11
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.411 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:11
Container ID: 1132031004-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 23.5 mg/Kg 1U 23.5 7.27 06/04/13 12:11
Surrogates
n-Triacontane-d62 86.9 % 150-150 06/04/13 12:11
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.411 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:11
Container ID: 1132031004-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C20
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Semivolatile Organic GC/MS
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
1,2-Dichlorobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
1,3-Dichlorobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
1,4-Dichlorobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
1-Chloronaphthalene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,4,5-Trichlorophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,4,6-Trichlorophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,4-Dichlorophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,4-Dimethylphenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,4-Dinitrophenol 3.51 mg/Kg 1U 3.51 1.10 05/31/13 01:34
2,4-Dinitrotoluene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,6-Dichlorophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2,6-Dinitrotoluene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Chloronaphthalene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Chlorophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Methyl-4,6-dinitrophenol 2.34 mg/Kg 1U 2.34 0.725 05/31/13 01:34
2-Methylnaphthalene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Methylphenol (o-Cresol) 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Nitroaniline 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
2-Nitrophenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
3&4-Methylphenol (p&m-Cresol) 1.17 mg/Kg 1U 1.17 0.362 05/31/13 01:34
3,3-Dichlorobenzidine 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
3-Nitroaniline 0.585 mg/Kg 1U 0.585 0.175 05/31/13 01:34
4-Bromophenyl-phenylether 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
4-Chloro-3-methylphenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
4-Chloroaniline 0.585 mg/Kg 1U 0.585 0.175 05/31/13 01:34
4-Chlorophenyl-phenylether 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
4-Nitroaniline 3.51 mg/Kg 1U 3.51 1.10 05/31/13 01:34
4-Nitrophenol 1.17 mg/Kg 1U 1.17 0.362 05/31/13 01:34
Acenaphthene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Acenaphthylene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Aniline 2.34 mg/Kg 1U 2.34 0.725 05/31/13 01:34
Anthracene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Azobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzo(a)Anthracene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzo[a]pyrene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzo[b]Fluoranthene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzo[g,h,i]perylene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzo[k]fluoranthene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Benzoic acid 1.75 mg/Kg 1U 1.75 0.877 05/31/13 01:34
Benzyl alcohol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Bis(2-Chloroethoxy)methane 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Bis(2-Chloroethyl)ether 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
bis(2-Ethylhexyl)phthalate 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C21
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Semivolatile Organic GC/MS
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Butylbenzylphthalate 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Carbazole 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Chrysene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Di-n-butylphthalate 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
di-n-Octylphthalate 0.585 mg/Kg 1U 0.585 0.175 05/31/13 01:34
Dibenzo[a,h]anthracene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Dibenzofuran 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Diethylphthalate 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Dimethylphthalate 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Fluoranthene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Fluorene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Hexachlorobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Hexachlorobutadiene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Hexachlorocyclopentadiene 0.818 mg/Kg 1U 0.818 0.234 05/31/13 01:34
Hexachloroethane 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Indeno[1,2,3-c,d] pyrene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Isophorone 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
N-Nitroso-di-n-propylamine 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
N-Nitrosodimethylamine 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
N-Nitrosodiphenylamine 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Naphthalene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Nitrobenzene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Pentachlorophenol 2.34 mg/Kg 1U 2.34 0.725 05/31/13 01:34
Phenanthrene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Phenol 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Pyrene 0.292 mg/Kg 1U 0.292 0.0912 05/31/13 01:34
Surrogates
2,4,6-Tribromophenol 88.1 % 135-125 05/31/13 01:34
2-Fluorobiphenyl 83.5 % 145-105 05/31/13 01:34
2-Fluorophenol 68.8 % 135-105 05/31/13 01:34
Nitrobenzene-d5 71.7 % 135-100 05/31/13 01:34
Phenol-d6 74.5 % 140-100 05/31/13 01:34
Terphenyl-d14 103 % 130-125 05/31/13 01:34
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.877 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 01:34
Container ID: 1132031004-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C22
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Volatile Fuels
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 4.44 mg/Kg 1U 4.44 1.33 06/05/13 12:51
Surrogates
4-Bromofluorobenzene 91.7 % 150-150 06/05/13 12:51
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/24/13 13:44
Prep Initial Wt./Vol.: 42.445 g
Prep Extract Vol: 31.7381 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 12:51
Container ID: 1132031004-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C23
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Volatile GC/MS
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,1,1-Trichloroethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,1,2,2-Tetrachloroethane 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
1,1,2-Trichloroethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,1-Dichloroethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,1-Dichloroethene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,1-Dichloropropene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2,3-Trichlorobenzene 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
1,2,3-Trichloropropane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2,4-Trichlorobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2,4-Trimethylbenzene 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
1,2-Dibromo-3-chloropropane 178 ug/Kg 1U 178 55.1 05/30/13 23:44
1,2-Dibromoethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2-Dichlorobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2-Dichloroethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,2-Dichloropropane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,3,5-Trimethylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,3-Dichlorobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,3-Dichloropropane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
1,4-Dichlorobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
2,2-Dichloropropane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
2-Butanone (MEK) 444 ug/Kg 1U 444 139 05/30/13 23:44
2-Chlorotoluene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
2-Hexanone 444 ug/Kg 1U 444 139 05/30/13 23:44
4-Chlorotoluene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
4-Isopropyltoluene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
4-Methyl-2-pentanone (MIBK) 444 ug/Kg 1U 444 139 05/30/13 23:44
Benzene 22.2 ug/Kg 1U 22.2 6.93 05/30/13 23:44
Bromobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Bromochloromethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Bromodichloromethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Bromoform 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Bromomethane 356 ug/Kg 1U 356 110 05/30/13 23:44
Carbon disulfide 178 ug/Kg 1U 178 55.1 05/30/13 23:44
Carbon tetrachloride 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Chlorobenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Chloroethane 356 ug/Kg 1U 356 110 05/30/13 23:44
Chloroform 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Chloromethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
cis-1,2-Dichloroethene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
cis-1,3-Dichloropropene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Dibromochloromethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Dibromomethane 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Dichlorodifluoromethane 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C24
Client Sample ID: SMIC-F (4.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031004
Lab Project ID: 1132031
Collection Date: 05/24/13 13:44
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 84.1
Results by Volatile GC/MS
Results of SMIC-F (4.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Hexachlorobutadiene 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
Isopropylbenzene (Cumene) 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Methyl-t-butyl ether 178 ug/Kg 1U 178 55.1 05/30/13 23:44
Methylene chloride 178 ug/Kg 1U 178 55.1 05/30/13 23:44
n-Butylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
n-Propylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Naphthalene 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
o-Xylene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
P & M -Xylene 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
sec-Butylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Styrene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
tert-Butylbenzene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Tetrachloroethene 22.2 ug/Kg 1U 22.2 6.93 05/30/13 23:44
Toluene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
trans-1,2-Dichloroethene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
trans-1,3-Dichloropropene 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Trichloroethene 22.2 ug/Kg 1U 22.2 6.93 05/30/13 23:44
Trichlorofluoromethane 88.9 ug/Kg 1U 88.9 26.7 05/30/13 23:44
Vinyl chloride 44.4 ug/Kg 1U 44.4 13.9 05/30/13 23:44
Xylenes (total) 178 ug/Kg 1U 178 55.1 05/30/13 23:44
Surrogates
1,2-Dichloroethane-D4 108 % 179-118 05/30/13 23:44
4-Bromofluorobenzene 96.7 % 167-138 05/30/13 23:44
Toluene-d8 102 % 185-115 05/30/13 23:44
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/24/13 13:44
Prep Initial Wt./Vol.: 42.445 g
Prep Extract Vol: 31.7381 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/30/13 23:44
Container ID: 1132031004-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C25
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Metals by ICP/MS
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 5.08 mg/Kg 101.18 0.367 05/31/13 13:00
Barium 38.0 mg/Kg 100.355 0.111 05/31/13 13:00
Cadmium 0.237 mg/Kg 10U 0.237 0.0734 05/31/13 13:00
Chromium 34.0 mg/Kg 100.474 0.142 05/31/13 13:00
Lead 5.08 mg/Kg 100.237 0.0734 05/31/13 13:00
Mercury 0.0474 mg/Kg 10U 0.0474 0.0142 05/31/13 13:00
Selenium 0.592 mg/Kg 10U 0.592 0.178 05/31/13 13:00
Silver 0.118 mg/Kg 10U 0.118 0.0367 05/31/13 13:00
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.024 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:00
Container ID: 1132031005-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C26
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Semivolatile Organic Fuels
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 24.2 mg/Kg 1U 24.2 7.51 06/04/13 12:21
Surrogates
5a Androstane 82.1 % 150-150 06/04/13 12:21
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.048 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:21
Container ID: 1132031005-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 24.2 mg/Kg 1U 24.2 7.51 06/04/13 12:21
Surrogates
n-Triacontane-d62 85.6 % 150-150 06/04/13 12:21
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.048 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:21
Container ID: 1132031005-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C27
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Semivolatile Organic GC/MS
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
1,2-Dichlorobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
1,3-Dichlorobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
1,4-Dichlorobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
1-Chloronaphthalene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,4,5-Trichlorophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,4,6-Trichlorophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,4-Dichlorophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,4-Dimethylphenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,4-Dinitrophenol 3.62 mg/Kg 1U 3.62 1.14 05/31/13 01:52
2,4-Dinitrotoluene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,6-Dichlorophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2,6-Dinitrotoluene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Chloronaphthalene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Chlorophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Methyl-4,6-dinitrophenol 2.42 mg/Kg 1U 2.42 0.749 05/31/13 01:52
2-Methylnaphthalene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Methylphenol (o-Cresol) 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Nitroaniline 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
2-Nitrophenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
3&4-Methylphenol (p&m-Cresol) 1.21 mg/Kg 1U 1.21 0.375 05/31/13 01:52
3,3-Dichlorobenzidine 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
3-Nitroaniline 0.604 mg/Kg 1U 0.604 0.181 05/31/13 01:52
4-Bromophenyl-phenylether 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
4-Chloro-3-methylphenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
4-Chloroaniline 0.604 mg/Kg 1U 0.604 0.181 05/31/13 01:52
4-Chlorophenyl-phenylether 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
4-Nitroaniline 3.62 mg/Kg 1U 3.62 1.14 05/31/13 01:52
4-Nitrophenol 1.21 mg/Kg 1U 1.21 0.375 05/31/13 01:52
Acenaphthene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Acenaphthylene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Aniline 2.42 mg/Kg 1U 2.42 0.749 05/31/13 01:52
Anthracene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Azobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzo(a)Anthracene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzo[a]pyrene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzo[b]Fluoranthene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzo[g,h,i]perylene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzo[k]fluoranthene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Benzoic acid 1.81 mg/Kg 1U 1.81 0.906 05/31/13 01:52
Benzyl alcohol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Bis(2-Chloroethoxy)methane 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Bis(2-Chloroethyl)ether 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
bis(2-Ethylhexyl)phthalate 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C28
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Semivolatile Organic GC/MS
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Butylbenzylphthalate 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Carbazole 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Chrysene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Di-n-butylphthalate 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
di-n-Octylphthalate 0.604 mg/Kg 1U 0.604 0.181 05/31/13 01:52
Dibenzo[a,h]anthracene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Dibenzofuran 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Diethylphthalate 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Dimethylphthalate 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Fluoranthene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Fluorene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Hexachlorobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Hexachlorobutadiene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Hexachlorocyclopentadiene 0.846 mg/Kg 1U 0.846 0.242 05/31/13 01:52
Hexachloroethane 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Indeno[1,2,3-c,d] pyrene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Isophorone 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
N-Nitroso-di-n-propylamine 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
N-Nitrosodimethylamine 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
N-Nitrosodiphenylamine 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Naphthalene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Nitrobenzene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Pentachlorophenol 2.42 mg/Kg 1U 2.42 0.749 05/31/13 01:52
Phenanthrene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Phenol 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Pyrene 0.302 mg/Kg 1U 0.302 0.0942 05/31/13 01:52
Surrogates
2,4,6-Tribromophenol 88.8 % 135-125 05/31/13 01:52
2-Fluorobiphenyl 83.2 % 145-105 05/31/13 01:52
2-Fluorophenol 67.5 % 135-105 05/31/13 01:52
Nitrobenzene-d5 71.8 % 135-100 05/31/13 01:52
Phenol-d6 73.7 % 140-100 05/31/13 01:52
Terphenyl-d14 108 % 130-125 05/31/13 01:52
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.579 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 01:52
Container ID: 1132031005-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C29
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Volatile Fuels
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.63 mg/Kg 1U 2.63 0.790 06/05/13 13:10
Surrogates
4-Bromofluorobenzene 106 % 150-150 06/05/13 13:10
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/24/13 14:21
Prep Initial Wt./Vol.: 96.507 g
Prep Extract Vol: 41.911 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 13:10
Container ID: 1132031005-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C30
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Volatile GC/MS
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,1,1-Trichloroethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,1,2,2-Tetrachloroethane 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
1,1,2-Trichloroethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,1-Dichloroethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,1-Dichloroethene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,1-Dichloropropene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2,3-Trichlorobenzene 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
1,2,3-Trichloropropane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2,4-Trichlorobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2,4-Trimethylbenzene 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
1,2-Dibromo-3-chloropropane 105 ug/Kg 1U 105 32.6 05/31/13 00:01
1,2-Dibromoethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2-Dichlorobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2-Dichloroethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,2-Dichloropropane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,3,5-Trimethylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,3-Dichlorobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,3-Dichloropropane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
1,4-Dichlorobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
2,2-Dichloropropane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
2-Butanone (MEK) 263 ug/Kg 1U 263 82.1 05/31/13 00:01
2-Chlorotoluene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
2-Hexanone 263 ug/Kg 1U 263 82.1 05/31/13 00:01
4-Chlorotoluene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
4-Isopropyltoluene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
4-Methyl-2-pentanone (MIBK) 263 ug/Kg 1U 263 82.1 05/31/13 00:01
Benzene 13.2 ug/Kg 1U 13.2 4.11 05/31/13 00:01
Bromobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Bromochloromethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Bromodichloromethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Bromoform 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Bromomethane 211 ug/Kg 1U 211 65.3 05/31/13 00:01
Carbon disulfide 105 ug/Kg 1U 105 32.6 05/31/13 00:01
Carbon tetrachloride 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Chlorobenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Chloroethane 211 ug/Kg 1U 211 65.3 05/31/13 00:01
Chloroform 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Chloromethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
cis-1,2-Dichloroethene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
cis-1,3-Dichloropropene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Dibromochloromethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Dibromomethane 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Dichlorodifluoromethane 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C31
Client Sample ID: SMIC-F (8.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031005
Lab Project ID: 1132031
Collection Date: 05/24/13 14:21
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 82.5
Results by Volatile GC/MS
Results of SMIC-F (8.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Hexachlorobutadiene 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
Isopropylbenzene (Cumene) 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Methyl-t-butyl ether 105 ug/Kg 1U 105 32.6 05/31/13 00:01
Methylene chloride 105 ug/Kg 1U 105 32.6 05/31/13 00:01
n-Butylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
n-Propylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Naphthalene 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
o-Xylene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
P & M -Xylene 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
sec-Butylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Styrene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
tert-Butylbenzene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Tetrachloroethene 13.2 ug/Kg 1U 13.2 4.11 05/31/13 00:01
Toluene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
trans-1,2-Dichloroethene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
trans-1,3-Dichloropropene 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Trichloroethene 13.2 ug/Kg 1U 13.2 4.11 05/31/13 00:01
Trichlorofluoromethane 52.7 ug/Kg 1U 52.7 15.8 05/31/13 00:01
Vinyl chloride 26.3 ug/Kg 1U 26.3 8.21 05/31/13 00:01
Xylenes (total) 105 ug/Kg 1U 105 32.6 05/31/13 00:01
Surrogates
1,2-Dichloroethane-D4 98.8 % 179-118 05/31/13 00:01
4-Bromofluorobenzene 103 % 167-138 05/31/13 00:01
Toluene-d8 92.5 % 185-115 05/31/13 00:01
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/24/13 14:21
Prep Initial Wt./Vol.: 96.507 g
Prep Extract Vol: 41.911 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 00:01
Container ID: 1132031005-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C32
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Metals by ICP/MS
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 9.50 mg/Kg 101.40 0.433 05/31/13 13:02
Barium 62.0 mg/Kg 100.419 0.131 05/31/13 13:02
Cadmium 0.279 mg/Kg 10U 0.279 0.0865 05/31/13 13:02
Chromium 41.0 mg/Kg 100.558 0.168 05/31/13 13:02
Lead 11.0 mg/Kg 100.279 0.0865 05/31/13 13:02
Mercury 0.0558 mg/Kg 10U 0.0558 0.0168 05/31/13 13:02
Selenium 0.698 mg/Kg 10U 0.698 0.209 05/31/13 13:02
Silver 0.140 mg/Kg 10U 0.140 0.0433 05/31/13 13:02
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.012 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:02
Container ID: 1132031006-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C33
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Semivolatile Organic Fuels
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 27.8 mg/Kg 1U 27.8 8.63 06/04/13 12:30
Surrogates
5a Androstane 84.9 % 150-150 06/04/13 12:30
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.456 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:30
Container ID: 1132031006-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 34.8 mg/Kg 127.8 8.63 06/04/13 12:30
Surrogates
n-Triacontane-d62 95.8 % 150-150 06/04/13 12:30
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.456 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:30
Container ID: 1132031006-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C34
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Semivolatile Organic GC/MS
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
1,2-Dichlorobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
1,3-Dichlorobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
1,4-Dichlorobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
1-Chloronaphthalene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,4,5-Trichlorophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,4,6-Trichlorophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,4-Dichlorophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,4-Dimethylphenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,4-Dinitrophenol 4.16 mg/Kg 1U 4.16 1.30 06/03/13 19:47
2,4-Dinitrotoluene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,6-Dichlorophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2,6-Dinitrotoluene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Chloronaphthalene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Chlorophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Methyl-4,6-dinitrophenol 2.77 mg/Kg 1U 2.77 0.859 06/03/13 19:47
2-Methylnaphthalene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Methylphenol (o-Cresol) 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Nitroaniline 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
2-Nitrophenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
3&4-Methylphenol (p&m-Cresol) 1.39 mg/Kg 1U 1.39 0.430 06/03/13 19:47
3,3-Dichlorobenzidine 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
3-Nitroaniline 0.693 mg/Kg 1U 0.693 0.208 06/03/13 19:47
4-Bromophenyl-phenylether 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
4-Chloro-3-methylphenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
4-Chloroaniline 0.693 mg/Kg 1U 0.693 0.208 06/03/13 19:47
4-Chlorophenyl-phenylether 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
4-Nitroaniline 4.16 mg/Kg 1U 4.16 1.30 06/03/13 19:47
4-Nitrophenol 1.39 mg/Kg 1U 1.39 0.430 06/03/13 19:47
Acenaphthene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Acenaphthylene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Aniline 2.77 mg/Kg 1U 2.77 0.859 06/03/13 19:47
Anthracene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Azobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzo(a)Anthracene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzo[a]pyrene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzo[b]Fluoranthene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzo[g,h,i]perylene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzo[k]fluoranthene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Benzoic acid 2.08 mg/Kg 1U 2.08 1.04 06/03/13 19:47
Benzyl alcohol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Bis(2-Chloroethoxy)methane 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Bis(2-Chloroethyl)ether 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
bis(2-Ethylhexyl)phthalate 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C35
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Semivolatile Organic GC/MS
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Butylbenzylphthalate 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Carbazole 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Chrysene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Di-n-butylphthalate 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
di-n-Octylphthalate 0.693 mg/Kg 1U 0.693 0.208 06/03/13 19:47
Dibenzo[a,h]anthracene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Dibenzofuran 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Diethylphthalate 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Dimethylphthalate 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Fluoranthene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Fluorene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Hexachlorobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Hexachlorobutadiene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Hexachlorocyclopentadiene 0.970 mg/Kg 1U 0.970 0.277 06/03/13 19:47
Hexachloroethane 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Indeno[1,2,3-c,d] pyrene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Isophorone 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
N-Nitroso-di-n-propylamine 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
N-Nitrosodimethylamine 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
N-Nitrosodiphenylamine 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Naphthalene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Nitrobenzene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Pentachlorophenol 2.77 mg/Kg 1U 2.77 0.859 06/03/13 19:47
Phenanthrene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Phenol 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Pyrene 0.346 mg/Kg 1U 0.346 0.108 06/03/13 19:47
Surrogates
2,4,6-Tribromophenol 91.8 % 135-125 06/03/13 19:47
2-Fluorobiphenyl 87.5 % 145-105 06/03/13 19:47
2-Fluorophenol 73 % 135-105 06/03/13 19:47
Nitrobenzene-d5 77.8 % 135-100 06/03/13 19:47
Phenol-d6 80.4 % 140-100 06/03/13 19:47
Terphenyl-d14 100 % 130-125 06/03/13 19:47
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.938 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/03/13 19:47
Container ID: 1132031006-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C36
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Volatile Fuels
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 4.37 mg/Kg 1U 4.37 1.31 06/05/13 13:28
Surrogates
4-Bromofluorobenzene 84.9 % 150-150 06/05/13 13:28
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/25/13 20:11
Prep Initial Wt./Vol.: 76.58 g
Prep Extract Vol: 47.3686 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 13:28
Container ID: 1132031006-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C37
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Volatile GC/MS
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,1,1-Trichloroethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,1,2,2-Tetrachloroethane 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
1,1,2-Trichloroethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,1-Dichloroethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,1-Dichloroethene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,1-Dichloropropene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2,3-Trichlorobenzene 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
1,2,3-Trichloropropane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2,4-Trichlorobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2,4-Trimethylbenzene 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
1,2-Dibromo-3-chloropropane 175 ug/Kg 1U 175 54.2 05/31/13 00:17
1,2-Dibromoethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2-Dichlorobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2-Dichloroethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,2-Dichloropropane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,3,5-Trimethylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,3-Dichlorobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,3-Dichloropropane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
1,4-Dichlorobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
2,2-Dichloropropane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
2-Butanone (MEK) 437 ug/Kg 1U 437 136 05/31/13 00:17
2-Chlorotoluene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
2-Hexanone 437 ug/Kg 1U 437 136 05/31/13 00:17
4-Chlorotoluene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
4-Isopropyltoluene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
4-Methyl-2-pentanone (MIBK) 437 ug/Kg 1U 437 136 05/31/13 00:17
Benzene 21.8 ug/Kg 1U 21.8 6.82 05/31/13 00:17
Bromobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Bromochloromethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Bromodichloromethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Bromoform 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Bromomethane 350 ug/Kg 1U 350 108 05/31/13 00:17
Carbon disulfide 175 ug/Kg 1U 175 54.2 05/31/13 00:17
Carbon tetrachloride 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Chlorobenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Chloroethane 350 ug/Kg 1U 350 108 05/31/13 00:17
Chloroform 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Chloromethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
cis-1,2-Dichloroethene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
cis-1,3-Dichloropropene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Dibromochloromethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Dibromomethane 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Dichlorodifluoromethane 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C38
Client Sample ID: SMIC-E (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031006
Lab Project ID: 1132031
Collection Date: 05/25/13 20:11
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 70.8
Results by Volatile GC/MS
Results of SMIC-E (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Hexachlorobutadiene 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
Isopropylbenzene (Cumene) 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Methyl-t-butyl ether 175 ug/Kg 1U 175 54.2 05/31/13 00:17
Methylene chloride 175 ug/Kg 1U 175 54.2 05/31/13 00:17
n-Butylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
n-Propylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Naphthalene 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
o-Xylene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
P & M -Xylene 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
sec-Butylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Styrene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
tert-Butylbenzene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Tetrachloroethene 21.8 ug/Kg 1U 21.8 6.82 05/31/13 00:17
Toluene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
trans-1,2-Dichloroethene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
trans-1,3-Dichloropropene 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Trichloroethene 21.8 ug/Kg 1U 21.8 6.82 05/31/13 00:17
Trichlorofluoromethane 87.4 ug/Kg 1U 87.4 26.2 05/31/13 00:17
Vinyl chloride 43.7 ug/Kg 1U 43.7 13.6 05/31/13 00:17
Xylenes (total) 175 ug/Kg 1U 175 54.2 05/31/13 00:17
Surrogates
1,2-Dichloroethane-D4 103 % 179-118 05/31/13 00:17
4-Bromofluorobenzene 102 % 167-138 05/31/13 00:17
Toluene-d8 97.3 % 185-115 05/31/13 00:17
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/25/13 20:11
Prep Initial Wt./Vol.: 76.58 g
Prep Extract Vol: 47.3686 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 00:17
Container ID: 1132031006-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C39
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Metals by ICP/MS
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.83 mg/Kg 101.03 0.320 05/31/13 13:04
Barium 26.6 mg/Kg 100.309 0.0969 05/31/13 13:04
Cadmium 0.206 mg/Kg 10U 0.206 0.0639 05/31/13 13:04
Chromium 25.2 mg/Kg 100.412 0.124 05/31/13 13:04
Lead 5.42 mg/Kg 100.206 0.0639 05/31/13 13:04
Mercury 0.0412 mg/Kg 10U 0.0412 0.0124 05/31/13 13:04
Selenium 0.515 mg/Kg 10U 0.515 0.155 05/31/13 13:04
Silver 0.103 mg/Kg 10U 0.103 0.0320 05/31/13 13:04
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.077 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:04
Container ID: 1132031007-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C40
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Semivolatile Organic Fuels
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.2 mg/Kg 1U 22.2 6.87 06/04/13 12:40
Surrogates
5a Androstane 73.4 % 150-150 06/04/13 12:40
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.046 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:40
Container ID: 1132031007-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.2 mg/Kg 1U 22.2 6.87 06/04/13 12:40
Surrogates
n-Triacontane-d62 79.7 % 150-150 06/04/13 12:40
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.046 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:40
Container ID: 1132031007-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C41
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Semivolatile Organic GC/MS
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
1,2-Dichlorobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
1,3-Dichlorobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
1,4-Dichlorobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
1-Chloronaphthalene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,4,5-Trichlorophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,4,6-Trichlorophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,4-Dichlorophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,4-Dimethylphenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,4-Dinitrophenol 3.30 mg/Kg 1U 3.30 1.04 05/31/13 03:01
2,4-Dinitrotoluene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,6-Dichlorophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2,6-Dinitrotoluene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Chloronaphthalene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Chlorophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Methyl-4,6-dinitrophenol 2.20 mg/Kg 1U 2.20 0.683 05/31/13 03:01
2-Methylnaphthalene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Methylphenol (o-Cresol) 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Nitroaniline 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
2-Nitrophenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
3&4-Methylphenol (p&m-Cresol) 1.10 mg/Kg 1U 1.10 0.341 05/31/13 03:01
3,3-Dichlorobenzidine 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
3-Nitroaniline 0.551 mg/Kg 1U 0.551 0.165 05/31/13 03:01
4-Bromophenyl-phenylether 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
4-Chloro-3-methylphenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
4-Chloroaniline 0.551 mg/Kg 1U 0.551 0.165 05/31/13 03:01
4-Chlorophenyl-phenylether 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
4-Nitroaniline 3.30 mg/Kg 1U 3.30 1.04 05/31/13 03:01
4-Nitrophenol 1.10 mg/Kg 1U 1.10 0.341 05/31/13 03:01
Acenaphthene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Acenaphthylene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Aniline 2.20 mg/Kg 1U 2.20 0.683 05/31/13 03:01
Anthracene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Azobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzo(a)Anthracene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzo[a]pyrene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzo[b]Fluoranthene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzo[g,h,i]perylene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzo[k]fluoranthene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Benzoic acid 1.65 mg/Kg 1U 1.65 0.826 05/31/13 03:01
Benzyl alcohol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Bis(2-Chloroethoxy)methane 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Bis(2-Chloroethyl)ether 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
bis(2-Ethylhexyl)phthalate 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C42
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Semivolatile Organic GC/MS
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Butylbenzylphthalate 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Carbazole 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Chrysene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Di-n-butylphthalate 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
di-n-Octylphthalate 0.551 mg/Kg 1U 0.551 0.165 05/31/13 03:01
Dibenzo[a,h]anthracene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Dibenzofuran 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Diethylphthalate 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Dimethylphthalate 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Fluoranthene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Fluorene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Hexachlorobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Hexachlorobutadiene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Hexachlorocyclopentadiene 0.771 mg/Kg 1U 0.771 0.220 05/31/13 03:01
Hexachloroethane 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Indeno[1,2,3-c,d] pyrene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Isophorone 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
N-Nitroso-di-n-propylamine 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
N-Nitrosodimethylamine 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
N-Nitrosodiphenylamine 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Naphthalene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Nitrobenzene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Pentachlorophenol 2.20 mg/Kg 1U 2.20 0.683 05/31/13 03:01
Phenanthrene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Phenol 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Pyrene 0.275 mg/Kg 1U 0.275 0.0859 05/31/13 03:01
Surrogates
2,4,6-Tribromophenol 87 % 135-125 05/31/13 03:01
2-Fluorobiphenyl 84.6 % 145-105 05/31/13 03:01
2-Fluorophenol 72.9 % 135-105 05/31/13 03:01
Nitrobenzene-d5 75.7 % 135-100 05/31/13 03:01
Phenol-d6 78.3 % 140-100 05/31/13 03:01
Terphenyl-d14 104 % 130-125 05/31/13 03:01
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.683 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 03:01
Container ID: 1132031007-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C43
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Volatile Fuels
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.19 mg/Kg 1U 2.19 0.656 06/05/13 13:47
Surrogates
4-Bromofluorobenzene 98.9 % 150-150 06/05/13 13:47
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/25/13 21:07
Prep Initial Wt./Vol.: 84.972 g
Prep Extract Vol: 33.4447 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 13:47
Container ID: 1132031007-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C44
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Volatile GC/MS
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,1,1-Trichloroethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,1,2,2-Tetrachloroethane 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
1,1,2-Trichloroethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,1-Dichloroethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,1-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,1-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2,3-Trichlorobenzene 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
1,2,3-Trichloropropane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2,4-Trichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2,4-Trimethylbenzene 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
1,2-Dibromo-3-chloropropane 87.4 ug/Kg 1U 87.4 27.1 05/31/13 00:34
1,2-Dibromoethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2-Dichloroethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,2-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,3,5-Trimethylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,3-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,3-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
1,4-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
2,2-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
2-Butanone (MEK) 219 ug/Kg 1U 219 68.2 05/31/13 00:34
2-Chlorotoluene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
2-Hexanone 219 ug/Kg 1U 219 68.2 05/31/13 00:34
4-Chlorotoluene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
4-Isopropyltoluene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
4-Methyl-2-pentanone (MIBK) 219 ug/Kg 1U 219 68.2 05/31/13 00:34
Benzene 10.9 ug/Kg 1U 10.9 3.41 05/31/13 00:34
Bromobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Bromochloromethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Bromodichloromethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Bromoform 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Bromomethane 175 ug/Kg 1U 175 54.2 05/31/13 00:34
Carbon disulfide 87.4 ug/Kg 1U 87.4 27.1 05/31/13 00:34
Carbon tetrachloride 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Chlorobenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Chloroethane 175 ug/Kg 1U 175 54.2 05/31/13 00:34
Chloroform 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Chloromethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
cis-1,2-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
cis-1,3-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Dibromochloromethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Dibromomethane 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Dichlorodifluoromethane 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C45
Client Sample ID: SMIC-E (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031007
Lab Project ID: 1132031
Collection Date: 05/25/13 21:07
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 90.1
Results by Volatile GC/MS
Results of SMIC-E (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Hexachlorobutadiene 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
Isopropylbenzene (Cumene) 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Methyl-t-butyl ether 87.4 ug/Kg 1U 87.4 27.1 05/31/13 00:34
Methylene chloride 87.4 ug/Kg 1U 87.4 27.1 05/31/13 00:34
n-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
n-Propylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Naphthalene 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
o-Xylene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
P & M -Xylene 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
sec-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Styrene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
tert-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Tetrachloroethene 10.9 ug/Kg 1U 10.9 3.41 05/31/13 00:34
Toluene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
trans-1,2-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
trans-1,3-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Trichloroethene 10.9 ug/Kg 1U 10.9 3.41 05/31/13 00:34
Trichlorofluoromethane 43.7 ug/Kg 1U 43.7 13.1 05/31/13 00:34
Vinyl chloride 21.9 ug/Kg 1U 21.9 6.82 05/31/13 00:34
Xylenes (total) 87.4 ug/Kg 1U 87.4 27.1 05/31/13 00:34
Surrogates
1,2-Dichloroethane-D4 105 % 179-118 05/31/13 00:34
4-Bromofluorobenzene 99 % 167-138 05/31/13 00:34
Toluene-d8 97.3 % 185-115 05/31/13 00:34
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/25/13 21:07
Prep Initial Wt./Vol.: 84.972 g
Prep Extract Vol: 33.4447 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 00:34
Container ID: 1132031007-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C46
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Metals by ICP/MS
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 7.15 mg/Kg 101.05 0.326 05/31/13 13:06
Barium 38.2 mg/Kg 100.316 0.0989 05/31/13 13:06
Cadmium 0.210 mg/Kg 10U 0.210 0.0652 05/31/13 13:06
Chromium 35.7 mg/Kg 100.421 0.126 05/31/13 13:06
Lead 7.13 mg/Kg 100.210 0.0652 05/31/13 13:06
Mercury 0.0421 mg/Kg 10U 0.0421 0.0126 05/31/13 13:06
Selenium 0.526 mg/Kg 10U 0.526 0.158 05/31/13 13:06
Silver 0.105 mg/Kg 10U 0.105 0.0326 05/31/13 13:06
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.077 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:06
Container ID: 1132031008-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C47
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Semivolatile Organic Fuels
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.4 mg/Kg 1U 22.4 6.93 06/04/13 12:49
Surrogates
5a Androstane 78.9 % 150-150 06/04/13 12:49
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.388 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:49
Container ID: 1132031008-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.4 mg/Kg 1U 22.4 6.93 06/04/13 12:49
Surrogates
n-Triacontane-d62 85.1 % 150-150 06/04/13 12:49
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.388 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:49
Container ID: 1132031008-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C48
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Semivolatile Organic GC/MS
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
1,2-Dichlorobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
1,3-Dichlorobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
1,4-Dichlorobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
1-Chloronaphthalene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,4,5-Trichlorophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,4,6-Trichlorophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,4-Dichlorophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,4-Dimethylphenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,4-Dinitrophenol 3.37 mg/Kg 1U 3.37 1.06 05/31/13 03:19
2,4-Dinitrotoluene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,6-Dichlorophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2,6-Dinitrotoluene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Chloronaphthalene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Chlorophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Methyl-4,6-dinitrophenol 2.25 mg/Kg 1U 2.25 0.697 05/31/13 03:19
2-Methylnaphthalene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Methylphenol (o-Cresol) 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Nitroaniline 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
2-Nitrophenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
3&4-Methylphenol (p&m-Cresol) 1.12 mg/Kg 1U 1.12 0.349 05/31/13 03:19
3,3-Dichlorobenzidine 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
3-Nitroaniline 0.562 mg/Kg 1U 0.562 0.169 05/31/13 03:19
4-Bromophenyl-phenylether 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
4-Chloro-3-methylphenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
4-Chloroaniline 0.562 mg/Kg 1U 0.562 0.169 05/31/13 03:19
4-Chlorophenyl-phenylether 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
4-Nitroaniline 3.37 mg/Kg 1U 3.37 1.06 05/31/13 03:19
4-Nitrophenol 1.12 mg/Kg 1U 1.12 0.349 05/31/13 03:19
Acenaphthene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Acenaphthylene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Aniline 2.25 mg/Kg 1U 2.25 0.697 05/31/13 03:19
Anthracene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Azobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzo(a)Anthracene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzo[a]pyrene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzo[b]Fluoranthene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzo[g,h,i]perylene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzo[k]fluoranthene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Benzoic acid 1.69 mg/Kg 1U 1.69 0.843 05/31/13 03:19
Benzyl alcohol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Bis(2-Chloroethoxy)methane 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Bis(2-Chloroethyl)ether 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
bis(2-Ethylhexyl)phthalate 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C49
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Semivolatile Organic GC/MS
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Butylbenzylphthalate 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Carbazole 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Chrysene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Di-n-butylphthalate 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
di-n-Octylphthalate 0.562 mg/Kg 1U 0.562 0.169 05/31/13 03:19
Dibenzo[a,h]anthracene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Dibenzofuran 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Diethylphthalate 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Dimethylphthalate 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Fluoranthene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Fluorene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Hexachlorobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Hexachlorobutadiene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Hexachlorocyclopentadiene 0.787 mg/Kg 1U 0.787 0.225 05/31/13 03:19
Hexachloroethane 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Indeno[1,2,3-c,d] pyrene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Isophorone 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
N-Nitroso-di-n-propylamine 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
N-Nitrosodimethylamine 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
N-Nitrosodiphenylamine 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Naphthalene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Nitrobenzene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Pentachlorophenol 2.25 mg/Kg 1U 2.25 0.697 05/31/13 03:19
Phenanthrene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Phenol 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Pyrene 0.281 mg/Kg 1U 0.281 0.0877 05/31/13 03:19
Surrogates
2,4,6-Tribromophenol 88.2 % 135-125 05/31/13 03:19
2-Fluorobiphenyl 89.5 % 145-105 05/31/13 03:19
2-Fluorophenol 73.8 % 135-105 05/31/13 03:19
Nitrobenzene-d5 74.8 % 135-100 05/31/13 03:19
Phenol-d6 80.2 % 140-100 05/31/13 03:19
Terphenyl-d14 105 % 130-125 05/31/13 03:19
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.661 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 03:19
Container ID: 1132031008-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C50
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Volatile Fuels
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.37 mg/Kg 1U 2.37 0.712 06/05/13 14:06
Surrogates
4-Bromofluorobenzene 98.6 % 150-150 06/05/13 14:06
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/25/13 22:14
Prep Initial Wt./Vol.: 82.832 g
Prep Extract Vol: 34.7023 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 14:06
Container ID: 1132031008-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C51
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Volatile GC/MS
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,1,1-Trichloroethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,1,2,2-Tetrachloroethane 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
1,1,2-Trichloroethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,1-Dichloroethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,1-Dichloroethene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,1-Dichloropropene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2,3-Trichlorobenzene 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
1,2,3-Trichloropropane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2,4-Trichlorobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2,4-Trimethylbenzene 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
1,2-Dibromo-3-chloropropane 94.9 ug/Kg 1U 94.9 29.4 05/31/13 00:51
1,2-Dibromoethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2-Dichlorobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2-Dichloroethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,2-Dichloropropane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,3,5-Trimethylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,3-Dichlorobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,3-Dichloropropane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
1,4-Dichlorobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
2,2-Dichloropropane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
2-Butanone (MEK) 237 ug/Kg 1U 237 74.0 05/31/13 00:51
2-Chlorotoluene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
2-Hexanone 237 ug/Kg 1U 237 74.0 05/31/13 00:51
4-Chlorotoluene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
4-Isopropyltoluene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
4-Methyl-2-pentanone (MIBK) 237 ug/Kg 1U 237 74.0 05/31/13 00:51
Benzene 11.9 ug/Kg 1U 11.9 3.70 05/31/13 00:51
Bromobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Bromochloromethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Bromodichloromethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Bromoform 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Bromomethane 190 ug/Kg 1U 190 58.8 05/31/13 00:51
Carbon disulfide 94.9 ug/Kg 1U 94.9 29.4 05/31/13 00:51
Carbon tetrachloride 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Chlorobenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Chloroethane 190 ug/Kg 1U 190 58.8 05/31/13 00:51
Chloroform 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Chloromethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
cis-1,2-Dichloroethene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
cis-1,3-Dichloropropene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Dibromochloromethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Dibromomethane 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Dichlorodifluoromethane 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C52
Client Sample ID: SMIC-E (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031008
Lab Project ID: 1132031
Collection Date: 05/25/13 22:14
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.3
Results by Volatile GC/MS
Results of SMIC-E (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Hexachlorobutadiene 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
Isopropylbenzene (Cumene) 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Methyl-t-butyl ether 94.9 ug/Kg 1U 94.9 29.4 05/31/13 00:51
Methylene chloride 94.9 ug/Kg 1U 94.9 29.4 05/31/13 00:51
n-Butylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
n-Propylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Naphthalene 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
o-Xylene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
P & M -Xylene 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
sec-Butylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Styrene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
tert-Butylbenzene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Tetrachloroethene 11.9 ug/Kg 1U 11.9 3.70 05/31/13 00:51
Toluene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
trans-1,2-Dichloroethene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
trans-1,3-Dichloropropene 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Trichloroethene 11.9 ug/Kg 1U 11.9 3.70 05/31/13 00:51
Trichlorofluoromethane 47.5 ug/Kg 1U 47.5 14.2 05/31/13 00:51
Vinyl chloride 23.7 ug/Kg 1U 23.7 7.40 05/31/13 00:51
Xylenes (total) 94.9 ug/Kg 1U 94.9 29.4 05/31/13 00:51
Surrogates
1,2-Dichloroethane-D4 107 % 179-118 05/31/13 00:51
4-Bromofluorobenzene 104 % 167-138 05/31/13 00:51
Toluene-d8 99.4 % 185-115 05/31/13 00:51
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/25/13 22:14
Prep Initial Wt./Vol.: 82.832 g
Prep Extract Vol: 34.7023 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 00:51
Container ID: 1132031008-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C53
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Metals by ICP/MS
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.35 mg/Kg 101.09 0.339 05/31/13 13:09
Barium 25.9 mg/Kg 100.328 0.103 05/31/13 13:09
Cadmium 0.219 mg/Kg 10U 0.219 0.0678 05/31/13 13:09
Chromium 32.3 mg/Kg 100.438 0.131 05/31/13 13:09
Lead 5.46 mg/Kg 100.219 0.0678 05/31/13 13:09
Mercury 0.0438 mg/Kg 10U 0.0438 0.0131 05/31/13 13:09
Selenium 0.547 mg/Kg 10U 0.547 0.164 05/31/13 13:09
Silver 0.109 mg/Kg 10U 0.109 0.0339 05/31/13 13:09
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.032 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:09
Container ID: 1132031009-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C54
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Semivolatile Organic Fuels
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.2 mg/Kg 1U 22.2 6.89 06/04/13 12:59
Surrogates
5a Androstane 74.3 % 150-150 06/04/13 12:59
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.46 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 12:59
Container ID: 1132031009-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.2 mg/Kg 1U 22.2 6.89 06/04/13 12:59
Surrogates
n-Triacontane-d62 80.3 % 150-150 06/04/13 12:59
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.46 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 12:59
Container ID: 1132031009-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C55
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Semivolatile Organic GC/MS
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
1,2-Dichlorobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
1,3-Dichlorobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
1,4-Dichlorobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
1-Chloronaphthalene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,4,5-Trichlorophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,4,6-Trichlorophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,4-Dichlorophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,4-Dimethylphenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,4-Dinitrophenol 3.36 mg/Kg 1U 3.36 1.05 05/31/13 03:36
2,4-Dinitrotoluene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,6-Dichlorophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2,6-Dinitrotoluene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Chloronaphthalene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Chlorophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Methyl-4,6-dinitrophenol 2.24 mg/Kg 1U 2.24 0.693 05/31/13 03:36
2-Methylnaphthalene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Methylphenol (o-Cresol) 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Nitroaniline 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
2-Nitrophenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
3&4-Methylphenol (p&m-Cresol) 1.12 mg/Kg 1U 1.12 0.347 05/31/13 03:36
3,3-Dichlorobenzidine 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
3-Nitroaniline 0.559 mg/Kg 1U 0.559 0.168 05/31/13 03:36
4-Bromophenyl-phenylether 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
4-Chloro-3-methylphenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
4-Chloroaniline 0.559 mg/Kg 1U 0.559 0.168 05/31/13 03:36
4-Chlorophenyl-phenylether 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
4-Nitroaniline 3.36 mg/Kg 1U 3.36 1.05 05/31/13 03:36
4-Nitrophenol 1.12 mg/Kg 1U 1.12 0.347 05/31/13 03:36
Acenaphthene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Acenaphthylene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Aniline 2.24 mg/Kg 1U 2.24 0.693 05/31/13 03:36
Anthracene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Azobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzo(a)Anthracene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzo[a]pyrene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzo[b]Fluoranthene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzo[g,h,i]perylene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzo[k]fluoranthene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Benzoic acid 1.68 mg/Kg 1U 1.68 0.839 05/31/13 03:36
Benzyl alcohol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Bis(2-Chloroethoxy)methane 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Bis(2-Chloroethyl)ether 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
bis(2-Ethylhexyl)phthalate 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C56
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Semivolatile Organic GC/MS
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Butylbenzylphthalate 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Carbazole 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Chrysene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Di-n-butylphthalate 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
di-n-Octylphthalate 0.559 mg/Kg 1U 0.559 0.168 05/31/13 03:36
Dibenzo[a,h]anthracene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Dibenzofuran 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Diethylphthalate 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Dimethylphthalate 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Fluoranthene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Fluorene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Hexachlorobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Hexachlorobutadiene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Hexachlorocyclopentadiene 0.783 mg/Kg 1U 0.783 0.224 05/31/13 03:36
Hexachloroethane 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Indeno[1,2,3-c,d] pyrene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Isophorone 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
N-Nitroso-di-n-propylamine 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
N-Nitrosodimethylamine 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
N-Nitrosodiphenylamine 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Naphthalene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Nitrobenzene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Pentachlorophenol 2.24 mg/Kg 1U 2.24 0.693 05/31/13 03:36
Phenanthrene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Phenol 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Pyrene 0.280 mg/Kg 1U 0.280 0.0872 05/31/13 03:36
Surrogates
2,4,6-Tribromophenol 87.8 % 135-125 05/31/13 03:36
2-Fluorobiphenyl 89.9 % 145-105 05/31/13 03:36
2-Fluorophenol 75.3 % 135-105 05/31/13 03:36
Nitrobenzene-d5 77.9 % 135-100 05/31/13 03:36
Phenol-d6 81.4 % 140-100 05/31/13 03:36
Terphenyl-d14 108 % 130-125 05/31/13 03:36
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.707 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7345
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 05/31/13 03:36
Container ID: 1132031009-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C57
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Volatile Fuels
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.65 mg/Kg 1U 2.65 0.796 06/05/13 14:24
Surrogates
4-Bromofluorobenzene 98.7 % 150-150 06/05/13 14:24
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/25/13 21:10
Prep Initial Wt./Vol.: 70.187 g
Prep Extract Vol: 33.0078 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 14:24
Container ID: 1132031009-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C58
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Volatile GC/MS
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,1,1-Trichloroethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,1,2,2-Tetrachloroethane 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
1,1,2-Trichloroethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,1-Dichloroethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,1-Dichloroethene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,1-Dichloropropene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2,3-Trichlorobenzene 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
1,2,3-Trichloropropane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2,4-Trichlorobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2,4-Trimethylbenzene 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
1,2-Dibromo-3-chloropropane 106 ug/Kg 1U 106 32.9 05/31/13 01:08
1,2-Dibromoethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2-Dichlorobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2-Dichloroethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,2-Dichloropropane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,3,5-Trimethylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,3-Dichlorobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,3-Dichloropropane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
1,4-Dichlorobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
2,2-Dichloropropane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
2-Butanone (MEK) 265 ug/Kg 1U 265 82.8 05/31/13 01:08
2-Chlorotoluene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
2-Hexanone 265 ug/Kg 1U 265 82.8 05/31/13 01:08
4-Chlorotoluene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
4-Isopropyltoluene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
4-Methyl-2-pentanone (MIBK) 265 ug/Kg 1U 265 82.8 05/31/13 01:08
Benzene 13.3 ug/Kg 1U 13.3 4.14 05/31/13 01:08
Bromobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Bromochloromethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Bromodichloromethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Bromoform 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Bromomethane 212 ug/Kg 1U 212 65.8 05/31/13 01:08
Carbon disulfide 106 ug/Kg 1U 106 32.9 05/31/13 01:08
Carbon tetrachloride 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Chlorobenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Chloroethane 212 ug/Kg 1U 212 65.8 05/31/13 01:08
Chloroform 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Chloromethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
cis-1,2-Dichloroethene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
cis-1,3-Dichloropropene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Dibromochloromethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Dibromomethane 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Dichlorodifluoromethane 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C59
Client Sample ID: SMIC-E (5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031009
Lab Project ID: 1132031
Collection Date: 05/25/13 21:10
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 88.6
Results by Volatile GC/MS
Results of SMIC-E (5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Hexachlorobutadiene 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
Isopropylbenzene (Cumene) 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Methyl-t-butyl ether 106 ug/Kg 1U 106 32.9 05/31/13 01:08
Methylene chloride 106 ug/Kg 1U 106 32.9 05/31/13 01:08
n-Butylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
n-Propylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Naphthalene 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
o-Xylene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
P & M -Xylene 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
sec-Butylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Styrene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
tert-Butylbenzene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Tetrachloroethene 13.3 ug/Kg 1U 13.3 4.14 05/31/13 01:08
Toluene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
trans-1,2-Dichloroethene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
trans-1,3-Dichloropropene 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Trichloroethene 13.3 ug/Kg 1U 13.3 4.14 05/31/13 01:08
Trichlorofluoromethane 53.1 ug/Kg 1U 53.1 15.9 05/31/13 01:08
Vinyl chloride 26.5 ug/Kg 1U 26.5 8.28 05/31/13 01:08
Xylenes (total) 106 ug/Kg 1U 106 32.9 05/31/13 01:08
Surrogates
1,2-Dichloroethane-D4 110 % 179-118 05/31/13 01:08
4-Bromofluorobenzene 106 % 167-138 05/31/13 01:08
Toluene-d8 106 % 185-115 05/31/13 01:08
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/25/13 21:10
Prep Initial Wt./Vol.: 70.187 g
Prep Extract Vol: 33.0078 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 01:08
Container ID: 1132031009-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C60
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Metals by ICP/MS
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 22.0 mg/Kg 101.51 0.468 05/31/13 13:22
Barium 81.4 mg/Kg 100.453 0.142 05/31/13 13:22
Cadmium 0.302 mg/Kg 10U 0.302 0.0936 05/31/13 13:22
Chromium 57.5 mg/Kg 100.604 0.181 05/31/13 13:22
Lead 20.0 mg/Kg 100.302 0.0936 05/31/13 13:22
Mercury 0.127 mg/Kg 100.0604 0.0181 05/31/13 13:22
Selenium 0.755 mg/Kg 10U 0.755 0.227 05/31/13 13:22
Silver 0.158 mg/Kg 100.151 0.0468 05/31/13 13:22
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.042 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:22
Container ID: 1132031010-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C61
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Semivolatile Organic Fuels
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 31.0 mg/Kg 1U 31.0 9.61 06/04/13 13:08
Surrogates
5a Androstane 72.7 % 150-150 06/04/13 13:08
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.457 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 13:08
Container ID: 1132031010-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 49.9 mg/Kg 131.0 9.61 06/04/13 13:08
Surrogates
n-Triacontane-d62 83.7 % 150-150 06/04/13 13:08
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.457 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 13:08
Container ID: 1132031010-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C62
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Semivolatile Organic GC/MS
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
1,2-Dichlorobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
1,3-Dichlorobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
1,4-Dichlorobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
1-Chloronaphthalene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,4,5-Trichlorophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,4,6-Trichlorophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,4-Dichlorophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,4-Dimethylphenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,4-Dinitrophenol 4.71 mg/Kg 1U 4.71 1.48 06/03/13 20:38
2,4-Dinitrotoluene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,6-Dichlorophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2,6-Dinitrotoluene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Chloronaphthalene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Chlorophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Methyl-4,6-dinitrophenol 3.14 mg/Kg 1U 3.14 0.973 06/03/13 20:38
2-Methylnaphthalene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Methylphenol (o-Cresol) 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Nitroaniline 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
2-Nitrophenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
3&4-Methylphenol (p&m-Cresol) 1.57 mg/Kg 1U 1.57 0.487 06/03/13 20:38
3,3-Dichlorobenzidine 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
3-Nitroaniline 0.785 mg/Kg 1U 0.785 0.235 06/03/13 20:38
4-Bromophenyl-phenylether 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
4-Chloro-3-methylphenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
4-Chloroaniline 0.785 mg/Kg 1U 0.785 0.235 06/03/13 20:38
4-Chlorophenyl-phenylether 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
4-Nitroaniline 4.71 mg/Kg 1U 4.71 1.48 06/03/13 20:38
4-Nitrophenol 1.57 mg/Kg 1U 1.57 0.487 06/03/13 20:38
Acenaphthene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Acenaphthylene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Aniline 3.14 mg/Kg 1U 3.14 0.973 06/03/13 20:38
Anthracene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Azobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzo(a)Anthracene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzo[a]pyrene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzo[b]Fluoranthene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzo[g,h,i]perylene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzo[k]fluoranthene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Benzoic acid 2.35 mg/Kg 1U 2.35 1.18 06/03/13 20:38
Benzyl alcohol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Bis(2-Chloroethoxy)methane 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Bis(2-Chloroethyl)ether 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
bis(2-Ethylhexyl)phthalate 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C63
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Semivolatile Organic GC/MS
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Butylbenzylphthalate 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Carbazole 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Chrysene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Di-n-butylphthalate 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
di-n-Octylphthalate 0.785 mg/Kg 1U 0.785 0.235 06/03/13 20:38
Dibenzo[a,h]anthracene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Dibenzofuran 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Diethylphthalate 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Dimethylphthalate 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Fluoranthene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Fluorene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Hexachlorobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Hexachlorobutadiene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Hexachlorocyclopentadiene 1.10 mg/Kg 1U 1.10 0.314 06/03/13 20:38
Hexachloroethane 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Indeno[1,2,3-c,d] pyrene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Isophorone 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
N-Nitroso-di-n-propylamine 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
N-Nitrosodimethylamine 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
N-Nitrosodiphenylamine 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Naphthalene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Nitrobenzene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Pentachlorophenol 3.14 mg/Kg 1U 3.14 0.973 06/03/13 20:38
Phenanthrene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Phenol 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Pyrene 0.392 mg/Kg 1U 0.392 0.122 06/03/13 20:38
Surrogates
2,4,6-Tribromophenol 94.8 % 135-125 06/03/13 20:38
2-Fluorobiphenyl 86.7 % 145-105 06/03/13 20:38
2-Fluorophenol 72.7 % 135-105 06/03/13 20:38
Nitrobenzene-d5 80.4 % 135-100 06/03/13 20:38
Phenol-d6 80.3 % 140-100 06/03/13 20:38
Terphenyl-d14 111 % 130-125 06/03/13 20:38
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.554 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/03/13 20:38
Container ID: 1132031010-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C64
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Volatile Fuels
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 5.84 mg/Kg 1U 5.84 1.75 06/05/13 14:43
Surrogates
4-Bromofluorobenzene 73.3 % 150-150 06/05/13 14:43
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/26/13 13:15
Prep Initial Wt./Vol.: 66.183 g
Prep Extract Vol: 49.12 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 14:43
Container ID: 1132031010-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C65
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Volatile GC/MS
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,1,1-Trichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,1,2,2-Tetrachloroethane 117 ug/Kg 1U 117 35.0 05/31/13 01:24
1,1,2-Trichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,1-Dichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,1-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,1-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2,3-Trichlorobenzene 117 ug/Kg 1U 117 35.0 05/31/13 01:24
1,2,3-Trichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2,4-Trichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2,4-Trimethylbenzene 117 ug/Kg 1U 117 35.0 05/31/13 01:24
1,2-Dibromo-3-chloropropane 234 ug/Kg 1U 234 72.4 05/31/13 01:24
1,2-Dibromoethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2-Dichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,2-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,3,5-Trimethylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,3-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,3-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
1,4-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
2,2-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
2-Butanone (MEK) 584 ug/Kg 1U 584 182 05/31/13 01:24
2-Chlorotoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
2-Hexanone 584 ug/Kg 1U 584 182 05/31/13 01:24
4-Chlorotoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
4-Isopropyltoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
4-Methyl-2-pentanone (MIBK) 584 ug/Kg 1U 584 182 05/31/13 01:24
Benzene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:24
Bromobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Bromochloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Bromodichloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Bromoform 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Bromomethane 467 ug/Kg 1U 467 145 05/31/13 01:24
Carbon disulfide 234 ug/Kg 1U 234 72.4 05/31/13 01:24
Carbon tetrachloride 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Chlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Chloroethane 467 ug/Kg 1U 467 145 05/31/13 01:24
Chloroform 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Chloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
cis-1,2-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
cis-1,3-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Dibromochloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Dibromomethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Dichlorodifluoromethane 117 ug/Kg 1U 117 35.0 05/31/13 01:24
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C66
Client Sample ID: SMIC-S-(0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031010
Lab Project ID: 1132031
Collection Date: 05/26/13 13:15
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 63.6
Results by Volatile GC/MS
Results of SMIC-S-(0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Hexachlorobutadiene 117 ug/Kg 1U 117 35.0 05/31/13 01:24
Isopropylbenzene (Cumene) 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Methyl-t-butyl ether 234 ug/Kg 1U 234 72.4 05/31/13 01:24
Methylene chloride 234 ug/Kg 1U 234 72.4 05/31/13 01:24
n-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
n-Propylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Naphthalene 117 ug/Kg 1U 117 35.0 05/31/13 01:24
o-Xylene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
P & M -Xylene 117 ug/Kg 1U 117 35.0 05/31/13 01:24
sec-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Styrene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
tert-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Tetrachloroethene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:24
Toluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
trans-1,2-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
trans-1,3-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Trichloroethene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:24
Trichlorofluoromethane 117 ug/Kg 1U 117 35.0 05/31/13 01:24
Vinyl chloride 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:24
Xylenes (total) 234 ug/Kg 1U 234 72.4 05/31/13 01:24
Surrogates
1,2-Dichloroethane-D4 105 % 179-118 05/31/13 01:24
4-Bromofluorobenzene 102 % 167-138 05/31/13 01:24
Toluene-d8 98.2 % 185-115 05/31/13 01:24
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/26/13 13:15
Prep Initial Wt./Vol.: 66.183 g
Prep Extract Vol: 49.12 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 01:24
Container ID: 1132031010-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C67
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Metals by ICP/MS
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 20.2 mg/Kg 101.54 0.479 05/31/13 13:24
Barium 78.3 mg/Kg 100.463 0.145 05/31/13 13:24
Cadmium 0.309 mg/Kg 10U 0.309 0.0958 05/31/13 13:24
Chromium 54.8 mg/Kg 100.618 0.185 05/31/13 13:24
Lead 19.6 mg/Kg 100.309 0.0958 05/31/13 13:24
Mercury 0.0950 mg/Kg 100.0618 0.0185 05/31/13 13:24
Selenium 0.772 mg/Kg 10U 0.772 0.232 05/31/13 13:24
Silver 0.154 mg/Kg 10U 0.154 0.0479 05/31/13 13:24
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.056 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:24
Container ID: 1132031011-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C68
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Semivolatile Organic Fuels
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 32.3 mg/Kg 1U 32.3 10.0 06/04/13 13:18
Surrogates
5a Androstane 83.2 % 150-150 06/04/13 13:18
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.261 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/04/13 13:18
Container ID: 1132031011-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 66.4 mg/Kg 132.3 10.0 06/04/13 13:18
Surrogates
n-Triacontane-d62 93.5 % 150-150 06/04/13 13:18
Batch Information
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/13 13:30
Prep Initial Wt./Vol.: 30.261 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10912
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/04/13 13:18
Container ID: 1132031011-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C69
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Semivolatile Organic GC/MS
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
1,2-Dichlorobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
1,3-Dichlorobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
1,4-Dichlorobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
1-Chloronaphthalene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,4,5-Trichlorophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,4,6-Trichlorophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,4-Dichlorophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,4-Dimethylphenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,4-Dinitrophenol 4.81 mg/Kg 1U 4.81 1.51 06/03/13 20:55
2,4-Dinitrotoluene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,6-Dichlorophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2,6-Dinitrotoluene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Chloronaphthalene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Chlorophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Methyl-4,6-dinitrophenol 3.21 mg/Kg 1U 3.21 0.994 06/03/13 20:55
2-Methylnaphthalene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Methylphenol (o-Cresol) 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Nitroaniline 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
2-Nitrophenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
3&4-Methylphenol (p&m-Cresol) 1.60 mg/Kg 1U 1.60 0.497 06/03/13 20:55
3,3-Dichlorobenzidine 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
3-Nitroaniline 0.802 mg/Kg 1U 0.802 0.241 06/03/13 20:55
4-Bromophenyl-phenylether 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
4-Chloro-3-methylphenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
4-Chloroaniline 0.802 mg/Kg 1U 0.802 0.241 06/03/13 20:55
4-Chlorophenyl-phenylether 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
4-Nitroaniline 4.81 mg/Kg 1U 4.81 1.51 06/03/13 20:55
4-Nitrophenol 1.60 mg/Kg 1U 1.60 0.497 06/03/13 20:55
Acenaphthene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Acenaphthylene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Aniline 3.21 mg/Kg 1U 3.21 0.994 06/03/13 20:55
Anthracene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Azobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzo(a)Anthracene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzo[a]pyrene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzo[b]Fluoranthene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzo[g,h,i]perylene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzo[k]fluoranthene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Benzoic acid 2.41 mg/Kg 1U 2.41 1.20 06/03/13 20:55
Benzyl alcohol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Bis(2-Chloroethoxy)methane 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Bis(2-Chloroethyl)ether 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
bis(2-Ethylhexyl)phthalate 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C70
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Semivolatile Organic GC/MS
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Butylbenzylphthalate 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Carbazole 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Chrysene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Di-n-butylphthalate 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
di-n-Octylphthalate 0.802 mg/Kg 1U 0.802 0.241 06/03/13 20:55
Dibenzo[a,h]anthracene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Dibenzofuran 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Diethylphthalate 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Dimethylphthalate 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Fluoranthene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Fluorene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Hexachlorobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Hexachlorobutadiene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Hexachlorocyclopentadiene 1.12 mg/Kg 1U 1.12 0.321 06/03/13 20:55
Hexachloroethane 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Indeno[1,2,3-c,d] pyrene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Isophorone 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
N-Nitroso-di-n-propylamine 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
N-Nitrosodimethylamine 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
N-Nitrosodiphenylamine 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Naphthalene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Nitrobenzene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Pentachlorophenol 3.21 mg/Kg 1U 3.21 0.994 06/03/13 20:55
Phenanthrene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Phenol 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Pyrene 0.401 mg/Kg 1U 0.401 0.125 06/03/13 20:55
Surrogates
2,4,6-Tribromophenol 84.4 % 135-125 06/03/13 20:55
2-Fluorobiphenyl 75.5 % 145-105 06/03/13 20:55
2-Fluorophenol 64.5 % 135-105 06/03/13 20:55
Nitrobenzene-d5 69.9 % 135-100 06/03/13 20:55
Phenol-d6 71.2 % 140-100 06/03/13 20:55
Terphenyl-d14 96 % 130-125 06/03/13 20:55
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.879 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/03/13 20:55
Container ID: 1132031011-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C71
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Volatile Fuels
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 5.84 mg/Kg 1U 5.84 1.75 06/05/13 15:02
Surrogates
4-Bromofluorobenzene 99.5 % 150-150 06/05/13 15:02
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/26/13 13:18
Prep Initial Wt./Vol.: 75.967 g
Prep Extract Vol: 54.3885 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 15:02
Container ID: 1132031011-B
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C72
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Volatile GC/MS
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,1,1-Trichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,1,2,2-Tetrachloroethane 117 ug/Kg 1U 117 35.0 05/31/13 01:41
1,1,2-Trichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,1-Dichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,1-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,1-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2,3-Trichlorobenzene 117 ug/Kg 1U 117 35.0 05/31/13 01:41
1,2,3-Trichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2,4-Trichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2,4-Trimethylbenzene 117 ug/Kg 1U 117 35.0 05/31/13 01:41
1,2-Dibromo-3-chloropropane 234 ug/Kg 1U 234 72.4 05/31/13 01:41
1,2-Dibromoethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2-Dichloroethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,2-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,3,5-Trimethylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,3-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,3-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
1,4-Dichlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
2,2-Dichloropropane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
2-Butanone (MEK) 584 ug/Kg 1U 584 182 05/31/13 01:41
2-Chlorotoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
2-Hexanone 584 ug/Kg 1U 584 182 05/31/13 01:41
4-Chlorotoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
4-Isopropyltoluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
4-Methyl-2-pentanone (MIBK) 584 ug/Kg 1U 584 182 05/31/13 01:41
Benzene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:41
Bromobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Bromochloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Bromodichloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Bromoform 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Bromomethane 467 ug/Kg 1U 467 145 05/31/13 01:41
Carbon disulfide 234 ug/Kg 1U 234 72.4 05/31/13 01:41
Carbon tetrachloride 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Chlorobenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Chloroethane 467 ug/Kg 1U 467 145 05/31/13 01:41
Chloroform 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Chloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
cis-1,2-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
cis-1,3-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Dibromochloromethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Dibromomethane 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Dichlorodifluoromethane 117 ug/Kg 1U 117 35.0 05/31/13 01:41
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C73
Client Sample ID: SMIC-S (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031011
Lab Project ID: 1132031
Collection Date: 05/26/13 13:18
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 61.3
Results by Volatile GC/MS
Results of SMIC-S (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Hexachlorobutadiene 117 ug/Kg 1U 117 35.0 05/31/13 01:41
Isopropylbenzene (Cumene) 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Methyl-t-butyl ether 234 ug/Kg 1U 234 72.4 05/31/13 01:41
Methylene chloride 234 ug/Kg 1U 234 72.4 05/31/13 01:41
n-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
n-Propylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Naphthalene 117 ug/Kg 1U 117 35.0 05/31/13 01:41
o-Xylene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
P & M -Xylene 117 ug/Kg 1U 117 35.0 05/31/13 01:41
sec-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Styrene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
tert-Butylbenzene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Tetrachloroethene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:41
Toluene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
trans-1,2-Dichloroethene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
trans-1,3-Dichloropropene 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Trichloroethene 29.2 ug/Kg 1U 29.2 9.11 05/31/13 01:41
Trichlorofluoromethane 117 ug/Kg 1U 117 35.0 05/31/13 01:41
Vinyl chloride 58.4 ug/Kg 1U 58.4 18.2 05/31/13 01:41
Xylenes (total) 234 ug/Kg 1U 234 72.4 05/31/13 01:41
Surrogates
1,2-Dichloroethane-D4 101 % 179-118 05/31/13 01:41
4-Bromofluorobenzene 115 % 167-138 05/31/13 01:41
Toluene-d8 95 % 185-115 05/31/13 01:41
Batch Information
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/26/13 13:18
Prep Initial Wt./Vol.: 75.967 g
Prep Extract Vol: 54.3885 mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 01:41
Container ID: 1132031011-C
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C74
Client Sample ID: SMIC-P (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031012
Lab Project ID: 1132031
Collection Date: 05/26/13 13:52
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 67.1
Results by Metals by ICP/MS
Results of SMIC-P (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 15.2 mg/Kg 101.36 0.421 05/31/13 13:27
Barium 64.0 mg/Kg 100.407 0.128 05/31/13 13:27
Cadmium 0.272 mg/Kg 10U 0.272 0.0842 05/31/13 13:27
Chromium 47.2 mg/Kg 100.543 0.163 05/31/13 13:27
Lead 13.8 mg/Kg 100.272 0.0842 05/31/13 13:27
Mercury 0.0793 mg/Kg 100.0543 0.0163 05/31/13 13:27
Selenium 0.679 mg/Kg 10U 0.679 0.204 05/31/13 13:27
Silver 0.136 mg/Kg 10U 0.136 0.0421 05/31/13 13:27
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.097 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 13:27
Container ID: 1132031012-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C75
Client Sample ID: SMIC-P (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031012
Lab Project ID: 1132031
Collection Date: 05/26/13 13:52
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 67.1
Results by Semivolatile Organic GC/MS
Results of SMIC-P (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
1,2-Dichlorobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
1,3-Dichlorobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
1,4-Dichlorobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
1-Chloronaphthalene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,4,5-Trichlorophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,4,6-Trichlorophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,4-Dichlorophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,4-Dimethylphenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,4-Dinitrophenol 4.42 mg/Kg 1U 4.42 1.39 06/03/13 21:12
2,4-Dinitrotoluene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,6-Dichlorophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2,6-Dinitrotoluene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Chloronaphthalene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Chlorophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Methyl-4,6-dinitrophenol 2.95 mg/Kg 1U 2.95 0.914 06/03/13 21:12
2-Methylnaphthalene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Methylphenol (o-Cresol) 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Nitroaniline 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
2-Nitrophenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
3&4-Methylphenol (p&m-Cresol) 1.47 mg/Kg 1U 1.47 0.457 06/03/13 21:12
3,3-Dichlorobenzidine 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
3-Nitroaniline 0.737 mg/Kg 1U 0.737 0.221 06/03/13 21:12
4-Bromophenyl-phenylether 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
4-Chloro-3-methylphenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
4-Chloroaniline 0.737 mg/Kg 1U 0.737 0.221 06/03/13 21:12
4-Chlorophenyl-phenylether 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
4-Nitroaniline 4.42 mg/Kg 1U 4.42 1.39 06/03/13 21:12
4-Nitrophenol 1.47 mg/Kg 1U 1.47 0.457 06/03/13 21:12
Acenaphthene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Acenaphthylene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Aniline 2.95 mg/Kg 1U 2.95 0.914 06/03/13 21:12
Anthracene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Azobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzo(a)Anthracene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzo[a]pyrene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzo[b]Fluoranthene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzo[g,h,i]perylene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzo[k]fluoranthene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Benzoic acid 2.21 mg/Kg 1U 2.21 1.11 06/03/13 21:12
Benzyl alcohol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Bis(2-Chloroethoxy)methane 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Bis(2-Chloroethyl)ether 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
bis(2-Ethylhexyl)phthalate 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C76
Client Sample ID: SMIC-P (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031012
Lab Project ID: 1132031
Collection Date: 05/26/13 13:52
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 67.1
Results by Semivolatile Organic GC/MS
Results of SMIC-P (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Butylbenzylphthalate 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Carbazole 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Chrysene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Di-n-butylphthalate 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
di-n-Octylphthalate 0.737 mg/Kg 1U 0.737 0.221 06/03/13 21:12
Dibenzo[a,h]anthracene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Dibenzofuran 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Diethylphthalate 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Dimethylphthalate 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Fluoranthene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Fluorene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Hexachlorobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Hexachlorobutadiene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Hexachlorocyclopentadiene 1.03 mg/Kg 1U 1.03 0.295 06/03/13 21:12
Hexachloroethane 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Indeno[1,2,3-c,d] pyrene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Isophorone 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
N-Nitroso-di-n-propylamine 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
N-Nitrosodimethylamine 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
N-Nitrosodiphenylamine 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Naphthalene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Nitrobenzene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Pentachlorophenol 2.95 mg/Kg 1U 2.95 0.914 06/03/13 21:12
Phenanthrene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Phenol 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Pyrene 0.369 mg/Kg 1U 0.369 0.115 06/03/13 21:12
Surrogates
2,4,6-Tribromophenol 86.5 % 135-125 06/03/13 21:12
2-Fluorobiphenyl 74.9 % 145-105 06/03/13 21:12
2-Fluorophenol 59.2 % 135-105 06/03/13 21:12
Nitrobenzene-d5 64.8 % 135-100 06/03/13 21:12
Phenol-d6 67.2 % 140-100 06/03/13 21:12
Terphenyl-d14 101 % 130-125 06/03/13 21:12
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.729 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/03/13 21:12
Container ID: 1132031012-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C77
Client Sample ID: SMIC-Q (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031013
Lab Project ID: 1132031
Collection Date: 05/26/13 14:02
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 73.2
Results by Metals by ICP/MS
Results of SMIC-Q (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 8.99 mg/Kg 101.26 0.392 05/31/13 12:26
Barium 47.0 mg/Kg 100.379 0.119 05/31/13 12:26
Cadmium 0.253 mg/Kg 10U 0.253 0.0784 05/31/13 12:26
Chromium 38.7 mg/Kg 100.506 0.152 05/31/13 12:26
Lead 9.40 mg/Kg 100.253 0.0784 05/31/13 12:26
Mercury 0.0571 mg/Kg 100.0506 0.0152 05/31/13 12:26
Selenium 0.632 mg/Kg 10U 0.632 0.190 05/31/13 12:26
Silver 0.126 mg/Kg 10U 0.126 0.0392 05/31/13 12:26
Batch Information
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/13 08:20
Prep Initial Wt./Vol.: 1.081 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Analyst: ACF
Analytical Date/Time: 05/31/13 12:26
Container ID: 1132031013-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C78
Client Sample ID: SMIC-Q (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031013
Lab Project ID: 1132031
Collection Date: 05/26/13 14:02
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 73.2
Results by Semivolatile Organic GC/MS
Results of SMIC-Q (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
1,2-Dichlorobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
1,3-Dichlorobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
1,4-Dichlorobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
1-Chloronaphthalene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,4,5-Trichlorophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,4,6-Trichlorophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,4-Dichlorophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,4-Dimethylphenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,4-Dinitrophenol 4.06 mg/Kg 1U 4.06 1.27 06/03/13 21:29
2,4-Dinitrotoluene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,6-Dichlorophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2,6-Dinitrotoluene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Chloronaphthalene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Chlorophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Methyl-4,6-dinitrophenol 2.71 mg/Kg 1U 2.71 0.839 06/03/13 21:29
2-Methylnaphthalene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Methylphenol (o-Cresol) 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Nitroaniline 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
2-Nitrophenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
3&4-Methylphenol (p&m-Cresol) 1.35 mg/Kg 1U 1.35 0.419 06/03/13 21:29
3,3-Dichlorobenzidine 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
3-Nitroaniline 0.676 mg/Kg 1U 0.676 0.203 06/03/13 21:29
4-Bromophenyl-phenylether 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
4-Chloro-3-methylphenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
4-Chloroaniline 0.676 mg/Kg 1U 0.676 0.203 06/03/13 21:29
4-Chlorophenyl-phenylether 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
4-Nitroaniline 4.06 mg/Kg 1U 4.06 1.27 06/03/13 21:29
4-Nitrophenol 1.35 mg/Kg 1U 1.35 0.419 06/03/13 21:29
Acenaphthene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Acenaphthylene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Aniline 2.71 mg/Kg 1U 2.71 0.839 06/03/13 21:29
Anthracene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Azobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzo(a)Anthracene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzo[a]pyrene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzo[b]Fluoranthene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzo[g,h,i]perylene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzo[k]fluoranthene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Benzoic acid 2.03 mg/Kg 1U 2.03 1.01 06/03/13 21:29
Benzyl alcohol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Bis(2-Chloroethoxy)methane 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Bis(2-Chloroethyl)ether 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
bis(2-Ethylhexyl)phthalate 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C79
Client Sample ID: SMIC-Q (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031013
Lab Project ID: 1132031
Collection Date: 05/26/13 14:02
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%): 73.2
Results by Semivolatile Organic GC/MS
Results of SMIC-Q (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Butylbenzylphthalate 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Carbazole 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Chrysene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Di-n-butylphthalate 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
di-n-Octylphthalate 0.676 mg/Kg 1U 0.676 0.203 06/03/13 21:29
Dibenzo[a,h]anthracene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Dibenzofuran 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Diethylphthalate 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Dimethylphthalate 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Fluoranthene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Fluorene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Hexachlorobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Hexachlorobutadiene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Hexachlorocyclopentadiene 0.947 mg/Kg 1U 0.947 0.271 06/03/13 21:29
Hexachloroethane 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Indeno[1,2,3-c,d] pyrene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Isophorone 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
N-Nitroso-di-n-propylamine 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
N-Nitrosodimethylamine 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
N-Nitrosodiphenylamine 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Naphthalene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Nitrobenzene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Pentachlorophenol 2.71 mg/Kg 1U 2.71 0.839 06/03/13 21:29
Phenanthrene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Phenol 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Pyrene 0.338 mg/Kg 1U 0.338 0.106 06/03/13 21:29
Surrogates
2,4,6-Tribromophenol 88.9 % 135-125 06/03/13 21:29
2-Fluorobiphenyl 81.3 % 145-105 06/03/13 21:29
2-Fluorophenol 68.7 % 135-105 06/03/13 21:29
Nitrobenzene-d5 74.5 % 135-100 06/03/13 21:29
Phenol-d6 75.2 % 140-100 06/03/13 21:29
Terphenyl-d14 103 % 130-125 06/03/13 21:29
Batch Information
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/13 11:00
Prep Initial Wt./Vol.: 22.735 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/03/13 21:29
Container ID: 1132031013-A
Print Date: 06/18/2013 11:16:54AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C80
Client Sample ID: Trip Blank 1
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031014
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile Fuels
Results of Trip Blank 1
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.51 mg/Kg 1U 2.51 0.752 06/05/13 15:39
Surrogates
4-Bromofluorobenzene 97.3 % 150-150 06/05/13 15:39
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/24/13 12:58
Prep Initial Wt./Vol.: 49.835 g
Prep Extract Vol: 25 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 15:39
Container ID: 1132031014-A
Print Date: 06/18/2013 11:16:54AM
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C81
Client Sample ID: Trip Blank 2
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031015
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile GC/MS
Results of Trip Blank 2
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,1,1-Trichloroethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,1,2,2-Tetrachloroethane 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
1,1,2-Trichloroethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,1-Dichloroethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,1-Dichloroethene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,1-Dichloropropene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2,3-Trichlorobenzene 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
1,2,3-Trichloropropane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2,4-Trichlorobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2,4-Trimethylbenzene 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
1,2-Dibromo-3-chloropropane 100 ug/Kg 1U 100 31.1 05/31/13 14:21
1,2-Dibromoethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2-Dichlorobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2-Dichloroethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,2-Dichloropropane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,3,5-Trimethylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,3-Dichlorobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,3-Dichloropropane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
1,4-Dichlorobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
2,2-Dichloropropane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
2-Butanone (MEK) 250 ug/Kg 1U 250 78.2 05/31/13 14:21
2-Chlorotoluene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
2-Hexanone 250 ug/Kg 1U 250 78.2 05/31/13 14:21
4-Chlorotoluene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
4-Isopropyltoluene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
4-Methyl-2-pentanone (MIBK) 250 ug/Kg 1U 250 78.2 05/31/13 14:21
Benzene 12.5 ug/Kg 1U 12.5 3.91 05/31/13 14:21
Bromobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Bromochloromethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Bromodichloromethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Bromoform 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Bromomethane 200 ug/Kg 1U 200 62.1 05/31/13 14:21
Carbon disulfide 100 ug/Kg 1U 100 31.1 05/31/13 14:21
Carbon tetrachloride 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Chlorobenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Chloroethane 200 ug/Kg 1U 200 62.1 05/31/13 14:21
Chloroform 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Chloromethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
cis-1,2-Dichloroethene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
cis-1,3-Dichloropropene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Dibromochloromethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Dibromomethane 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Dichlorodifluoromethane 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
Print Date: 06/18/2013 11:16:54AM
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C82
Client Sample ID: Trip Blank 2
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132031015
Lab Project ID: 1132031
Collection Date: 05/24/13 12:58
Received Date: 05/28/13 12:04
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile GC/MS
Results of Trip Blank 2
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Hexachlorobutadiene 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
Isopropylbenzene (Cumene) 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Methyl-t-butyl ether 100 ug/Kg 1U 100 31.1 05/31/13 14:21
Methylene chloride 100 ug/Kg 1U 100 31.1 05/31/13 14:21
n-Butylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
n-Propylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Naphthalene 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
o-Xylene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
P & M -Xylene 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
sec-Butylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Styrene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
tert-Butylbenzene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Tetrachloroethene 12.5 ug/Kg 1U 12.5 3.91 05/31/13 14:21
Toluene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
trans-1,2-Dichloroethene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
trans-1,3-Dichloropropene 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Trichloroethene 12.5 ug/Kg 1U 12.5 3.91 05/31/13 14:21
Trichlorofluoromethane 50.1 ug/Kg 1U 50.1 15.0 05/31/13 14:21
Vinyl chloride 25.0 ug/Kg 1U 25.0 7.82 05/31/13 14:21
Xylenes (total) 100 ug/Kg 1U 100 31.1 05/31/13 14:21
Surrogates
1,2-Dichloroethane-D4 105 % 179-118 05/31/13 14:21
4-Bromofluorobenzene 93.5 % 167-138 05/31/13 14:21
Toluene-d8 101 % 185-115 05/31/13 14:21
Batch Information
Prep Batch: VXX24762
Prep Method: SW5035A
Prep Date/Time: 05/24/13 12:58
Prep Initial Wt./Vol.: 49.902 g
Prep Extract Vol: 25 mL
Analytical Batch: VMS13528
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 05/31/13 14:21
Container ID: 1132031015-A
Print Date: 06/18/2013 11:16:54AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C83
Blank ID: MB for HBN 1452181 [MXX/26513]
Blank Lab ID: 1150434
QC for Samples:
1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031012, 1132031013
Matrix: Soil/Solid (dry weight)
Results by SW6020
DL UnitsLOQ/CLResultsParameter
Method Blank
Arsenic 0.990 mg/Kg0.3070.614U
Barium 0.297 mg/Kg0.09310.186U
Cadmium 0.198 mg/Kg0.06140.123U
Chromium 0.396 mg/Kg0.1190.238U
Lead 0.198 mg/Kg0.06140.123U
Mercury 0.0396 mg/Kg0.01190.0238U
Selenium 0.495 mg/Kg0.1490.298U
Silver 0.0990 mg/Kg0.03070.0614U
Batch Information
Analytical Batch: MMS7977
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: ACF
Analytical Date/Time: 5/31/2013 1:16:23PM
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 5/30/2013 8:20:00AM
Prep Initial Wt./Vol.: 1.01 g
Prep Extract Vol: 50 mL
Print Date: 06/18/2013 11:16:58AM
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C84
Blank Spike ID: LCS for HBN 1132031 [MXX26513]
Blank Spike Lab ID: 1150435
Date Analyzed: 05/31/2013 13:18
Results by SW6020
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007,
1132031008, 1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Result
Arsenic 48.4 102 ( 80-120 )49.4
Barium 48.4 111 ( 80-120 )53.9
Cadmium 4.84 103 ( 80-120 )5.00
Chromium 19.4 109 ( 80-120 )21.1
Lead 48.4 117 ( 80-120 )56.5
Mercury 0.484 100 ( 80-120 )0.485
Selenium 48.4 106 ( 80-120 )51.3
Silver 4.84 104 ( 80-120 )5.03
Batch Information
Analytical Batch: MMS7977
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: ACF
Prep Batch: MXX26513
Prep Method: SW3050B
Prep Date/Time: 05/30/2013 08:20
Spike Init Wt./Vol.: 48.4 mg/Kg Extract Vol: 50 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/18/2013 11:16:59AM
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C85
Original Sample ID: 1132031013
MS Sample ID: 1150436 MS
MSD Sample ID: 1150437 MSD
Analysis Date: 05/31/2013 12:26
Analysis Date: 05/31/2013 17:50
Analysis Date: 05/31/2013 17:52
Matrix: Soil/Solid (dry weight)
Results by SW6020
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007,
1132031008, 1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Matrix Spike Summary
RPD CL
Arsenic 61.58.99 73.4 105 67.2 78.6 104 80-120 6.82 (< 20 )
Barium 61.547.0 129 134 67.2 136 132 80-120 4.88 (< 20 )* *
Cadmium 6.150.253U 6.46 105 6.72 7.23 108 80-120 11.20 (< 20 )
Chromium 24.638.7 68.6 122 26.9 70.8 119 80-120 3.11 (< 20 )*
Lead 61.59.40 78.0 112 67.2 85.2 113 80-120 8.82 (< 20 )
Mercury 0.6150.0571 0.672 100 0.672 0.721 99 80-120 7.13 (< 20 )
Selenium 61.50.632U 67.9 110 67.2 71.9 107 80-120 5.65 (< 20 )
Silver 6.150.126U 6.49 106 6.72 7.08 105 80-120 8.57 (< 20 )
Batch Information
Prep Batch: MXX26513
Prep Method: Soils/Solids Digest for Metals by ICP-MS
Prep Date/Time: 5/30/2013 8:20:00AM
Prep Initial Wt./Vol.: 1.11g
Prep Extract Vol: 50.00mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: ACF
Analytical Date/Time: 5/31/2013 5:50:35PM
Print Date: 06/18/2013 11:17:00AM
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C86
Original Sample ID: 1132031013
MS Sample ID: 1150438 BND
MSD Sample ID:
Analysis Date: 05/31/2013 12:26
Analysis Date: 05/31/2013 17:55
Analysis Date:
Matrix: Soil/Solid (dry weight)
Results by SW6020
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007,
1132031008, 1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Bench Spike Summary
RPD CL
Barium 31647.0 385 107 75-125
Chromium 15838.7 205 105 75-125
Batch Information
Prep Batch: MXX26513
Prep Method: Soils/Solids Digest for Metals by ICP-MS
Prep Date/Time: 5/30/2013 8:20:00AM
Prep Initial Wt./Vol.: 1.08g
Prep Extract Vol: 50.00mL
Analytical Batch: MMS7977
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: ACF
Analytical Date/Time: 5/31/2013 5:55:02PM
Print Date: 06/18/2013 11:17:00AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C87
Blank ID: MB for HBN 1452059 [SPT/9029]
Blank Lab ID: 1150286
QC for Samples:
1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031012, 1132031013
Matrix: Soil/Solid (dry weight)
Results by SM21 2540G
DL UnitsLOQ/CLResultsParameter
Method Blank
Total Solids %100
Batch Information
Analytical Batch: SPT9029
Analytical Method: SM21 2540G
Instrument:
Analyst: ACE
Analytical Date/Time: 5/29/2013 5:13:00PM
Print Date: 06/18/2013 11:17:00AM
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C88
Original Sample ID: 1132031010
Duplicate Sample ID: 1150287
Analysis Date: 05/29/2013 17:13
Matrix: Soil/Solid (dry weight)
Results by SM21 2540G
Duplicate Sample Summary
NAME Original (15.00) Duplicate (15.00)
QC for Samples:
RPD CL
1132031001, 1132031002, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031012, 1132031013
RPD (%)
Total Solids 63.6 63.6 15.000.03
Analytical Batch: SPT9029
Analytical Method: SM21 2540G
Instrument:
Analyst: ACE
Batch Information
Print Date: 06/18/2013 11:17:01AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C89
Blank ID: MB for HBN 1452362 [VXX/24760]
Blank Lab ID: 1150457
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011,
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
1,1,1,2-Tetrachloroethane 25.0 ug/Kg7.8015.6U
1,1,1-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1,2,2-Tetrachloroethane 50.0 ug/Kg15.030.0U
1,1,2-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethene 25.0 ug/Kg7.8015.6U
1,1-Dichloropropene 25.0 ug/Kg7.8015.6U
1,2,3-Trichlorobenzene 50.0 ug/Kg15.030.0U
1,2,3-Trichloropropane 25.0 ug/Kg7.8015.6U
1,2,4-Trichlorobenzene 25.0 ug/Kg7.8015.6U
1,2,4-Trimethylbenzene 50.0 ug/Kg15.030.0U
1,2-Dibromo-3-chloropropane 100 ug/Kg31.062.0U
1,2-Dibromoethane 25.0 ug/Kg7.8015.6U
1,2-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,2-Dichloroethane 25.0 ug/Kg7.8015.6U
1,2-Dichloropropane 25.0 ug/Kg7.8015.6U
1,3,5-Trimethylbenzene 25.0 ug/Kg7.8015.6U
1,3-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,3-Dichloropropane 25.0 ug/Kg7.8015.6U
1,4-Dichlorobenzene 25.0 ug/Kg7.8015.6U
2,2-Dichloropropane 25.0 ug/Kg7.8015.6U
2-Butanone (MEK) 250 ug/Kg78.0156U
2-Chlorotoluene 25.0 ug/Kg7.8015.6U
2-Hexanone 250 ug/Kg78.0156U
4-Chlorotoluene 25.0 ug/Kg7.8015.6U
4-Isopropyltoluene 25.0 ug/Kg7.8015.6U
4-Methyl-2-pentanone (MIBK) 250 ug/Kg78.0156U
Benzene 12.5 ug/Kg3.907.80U
Bromobenzene 25.0 ug/Kg7.8015.6U
Bromochloromethane 25.0 ug/Kg7.8015.6U
Bromodichloromethane 25.0 ug/Kg7.8015.6U
Bromoform 25.0 ug/Kg7.8015.6U
Bromomethane 200 ug/Kg62.0124U
Carbon disulfide 100 ug/Kg31.062.0U
Carbon tetrachloride 25.0 ug/Kg7.8015.6U
Chlorobenzene 25.0 ug/Kg7.8015.6U
Chloroethane 200 ug/Kg62.0124U
Chloroform 25.0 ug/Kg7.8015.6U
Print Date: 06/18/2013 11:17:02AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C90
Blank ID: MB for HBN 1452362 [VXX/24760]
Blank Lab ID: 1150457
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011,
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Chloromethane 25.0 ug/Kg7.8015.6U
cis-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
cis-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Dibromochloromethane 25.0 ug/Kg7.8015.6U
Dibromomethane 25.0 ug/Kg7.8015.6U
Dichlorodifluoromethane 50.0 ug/Kg15.030.0U
Ethylbenzene 25.0 ug/Kg7.8015.6U
Hexachlorobutadiene 50.0 ug/Kg15.030.0U
Isopropylbenzene (Cumene) 25.0 ug/Kg7.8015.6U
Methylene chloride 100 ug/Kg31.062.0U
Methyl-t-butyl ether 100 ug/Kg31.062.0U
Naphthalene 50.0 ug/Kg15.030.0U
n-Butylbenzene 25.0 ug/Kg7.8015.6U
n-Propylbenzene 25.0 ug/Kg7.8015.6U
o-Xylene 25.0 ug/Kg7.8015.6U
P & M -Xylene 50.0 ug/Kg15.030.0U
sec-Butylbenzene 25.0 ug/Kg7.8015.6U
Styrene 25.0 ug/Kg7.8015.6U
tert-Butylbenzene 25.0 ug/Kg7.8015.6U
Tetrachloroethene 12.5 ug/Kg3.907.80U
Toluene 25.0 ug/Kg7.8015.6U
trans-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
trans-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Trichloroethene 12.5 ug/Kg3.907.80U
Trichlorofluoromethane 50.0 ug/Kg15.030.0U
Vinyl chloride 25.0 ug/Kg7.8015.6U
Xylenes (total) 100 ug/Kg31.062.0U
Surrogates
1,2-Dichloroethane-D4 79-118 %104
4-Bromofluorobenzene 67-138 %95.9
Toluene-d8 85-115 %99.8
Print Date: 06/18/2013 11:17:02AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C91
Blank ID: MB for HBN 1452362 [VXX/24760]
Blank Lab ID: 1150457
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011,
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Batch Information
Analytical Batch: VMS13526
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 5/30/2013 6:49:01PM
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 5/30/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/18/2013 11:17:02AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C92
Blank Spike ID: LCS for HBN 1132031 [VXX24760]
Blank Spike Lab ID: 1150458
Date Analyzed: 05/30/2013 19:06
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Result
1,1,1,2-Tetrachloroethane 750 110 ( 75-125 )829
1,1,1-Trichloroethane 750 111 ( 70-135 )834
1,1,2,2-Tetrachloroethane 750 115 ( 55-130 )862
1,1,2-Trichloroethane 750 115 ( 60-125 )862
1,1-Dichloroethane 750 111 ( 75-125 )831
1,1-Dichloroethene 750 111 ( 65-135 )831
1,1-Dichloropropene 750 112 ( 70-135 )838
1,2,3-Trichlorobenzene 750 111 ( 60-135 )834
1,2,3-Trichloropropane 750 111 ( 65-130 )834
1,2,4-Trichlorobenzene 750 110 ( 65-130 )826
1,2,4-Trimethylbenzene 750 111 ( 65-135 )830
1,2-Dibromo-3-chloropropane 750 112 ( 40-135 )838
1,2-Dibromoethane 750 111 ( 70-125 )834
1,2-Dichlorobenzene 750 109 ( 75-120 )818
1,2-Dichloroethane 750 110 ( 70-135 )825
1,2-Dichloropropane 750 111 ( 70-120 )832
1,3,5-Trimethylbenzene 750 111 ( 65-135 )834
1,3-Dichlorobenzene 750 110 ( 70-125 )825
1,3-Dichloropropane 750 112 ( 75-125 )839
1,4-Dichlorobenzene 750 110 ( 70-125 )824
2,2-Dichloropropane 750 106 ( 65-135 )796
2-Butanone (MEK) 2250 105 ( 30-160 )2360
2-Chlorotoluene 750 112 ( 70-130 )840
2-Hexanone 2250 115 ( 45-145 )2590
4-Chlorotoluene 750 110 ( 75-125 )828
4-Isopropyltoluene 750 111 ( 75-135 )836
4-Methyl-2-pentanone (MIBK) 2250 114 ( 45-145 )2560
Benzene 750 104 ( 75-125 )782
Bromobenzene 750 110 ( 65-120 )823
Bromochloromethane 750 109 ( 70-125 )815
Bromodichloromethane 750 110 ( 70-130 )828
Bromoform 750 112 ( 55-135 )843
Bromomethane 750 110 ( 30-160 )827
Print Date: 06/18/2013 11:17:03AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C93
Blank Spike ID: LCS for HBN 1132031 [VXX24760]
Blank Spike Lab ID: 1150458
Date Analyzed: 05/30/2013 19:06
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Result
Carbon disulfide 1130 107 ( 45-160 )1200
Carbon tetrachloride 750 103 ( 65-135 )774
Chlorobenzene 750 110 ( 75-125 )827
Chloroethane 750 115 ( 40-155 )860
Chloroform 750 111 ( 70-125 )830
Chloromethane 750 111 ( 50-130 )833
cis-1,2-Dichloroethene 750 110 ( 65-125 )826
cis-1,3-Dichloropropene 750 109 ( 70-125 )819
Dibromochloromethane 750 113 ( 65-130 )845
Dibromomethane 750 110 ( 75-130 )822
Dichlorodifluoromethane 750 104 ( 35-135 )777
Ethylbenzene 750 113 ( 75-125 )848
Hexachlorobutadiene 750 110 ( 55-140 )822
Isopropylbenzene (Cumene) 750 112 ( 75-130 )838
Methyl-t-butyl ether 1130 110 ( 63-149 )1240
Methylene chloride 750 101 ( 55-140 )757
n-Butylbenzene 750 109 ( 65-140 )820
n-Propylbenzene 750 112 ( 65-135 )837
Naphthalene 750 111 ( 40-125 )836
o-Xylene 750 110 ( 75-125 )827
P & M -Xylene 1500 111 ( 80-125 )1660
sec-Butylbenzene 750 112 ( 65-130 )836
Styrene 750 110 ( 75-125 )828
tert-Butylbenzene 750 110 ( 65-130 )826
Tetrachloroethene 750 115 ( 65-140 )865
Toluene 750 118 ( 70-125 )885
trans-1,2-Dichloroethene 750 110 ( 65-135 )827
trans-1,3-Dichloropropene 750 112 ( 65-125 )841
Trichloroethene 750 103 ( 75-125 )774
Trichlorofluoromethane 750 105 ( 25-185 )790
Vinyl chloride 750 113 ( 60-125 )848
Xylenes (total) 2250 111 ( 80-125 )2490
Surrogates
Print Date: 06/18/2013 11:17:03AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C94
Blank Spike ID: LCS for HBN 1132031 [VXX24760]
Blank Spike Lab ID: 1150458
Date Analyzed: 05/30/2013 19:06
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (%)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Result
1,2-Dichloroethane-D4 750 109 ( 79-118 )109
4-Bromofluorobenzene 750 106 ( 67-138 )106
Toluene-d8 750 109 ( 85-115 )109
Batch Information
Analytical Batch: VMS13526
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Prep Batch: VXX24760
Prep Method: SW5035A
Prep Date/Time: 05/30/2013 08:00
Spike Init Wt./Vol.: 750 ug/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/18/2013 11:17:03AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C95
Original Sample ID: 1150460
MS Sample ID: 1150461 MS
MSD Sample ID: 1150462 MSD
Analysis Date: 05/30/2013 21:13
Analysis Date: 05/30/2013 20:23
Analysis Date: 05/30/2013 20:40
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Matrix Spike Summary
RPD CL
1,1,1,2-Tetrachloroethane 49010.2U 466 95 490 464 95 75-125 0.46 (< 20 )
1,1,1-Trichloroethane 49010.2U 473 97 490 469 96 70-135 0.90 (< 20 )
1,1,2,2-Tetrachloroethane 49019.6U 494 101 490 485 99 55-130 1.70 (< 20 )
1,1,2-Trichloroethane 49010.2U 477 97 490 476 97 60-125 0.27 (< 20 )
1,1-Dichloroethane 49010.2U 470 96 490 464 95 75-125 1.30 (< 20 )
1,1-Dichloroethene 49010.2U 469 96 490 464 95 65-135 1.10 (< 20 )
1,1-Dichloropropene 49010.2U 474 97 490 477 97 70-135 0.58 (< 20 )
1,2,3-Trichlorobenzene 49019.6U 468 96 490 480 98 60-135 2.60 (< 20 )
1,2,3-Trichloropropane 49010.2U 487 99 490 471 96 65-130 3.30 (< 20 )
1,2,4-Trichlorobenzene 49010.2U 475 97 490 477 97 65-130 0.38 (< 20 )
1,2,4-Trimethylbenzene 49019.6U 471 96 490 464 95 65-135 1.50 (< 20 )
1,2-Dibromo-3-chloropropane 49040.6U 505 103 490 505 103 40-135 0.10 (< 20 )
1,2-Dibromoethane 49010.2U 464 95 490 459 94 70-125 1.20 (< 20 )
1,2-Dichlorobenzene 49010.2U 465 95 490 461 94 75-120 0.78 (< 20 )
1,2-Dichloroethane 49010.2U 461 94 490 455 93 70-135 1.30 (< 20 )
1,2-Dichloropropane 49010.2U 469 96 490 462 94 70-120 1.40 (< 20 )
1,3,5-Trimethylbenzene 49010.2U 472 96 490 466 95 65-135 1.30 (< 20 )
1,3-Dichlorobenzene 49010.2U 462 94 490 459 94 70-125 0.67 (< 20 )
1,3-Dichloropropane 49010.2U 466 95 490 456 93 75-125 2.20 (< 20 )
1,4-Dichlorobenzene 49010.2U 471 96 490 461 94 70-125 2.30 (< 20 )
2,2-Dichloropropane 49010.2U 496 101 490 492 100 65-135 0.73 (< 20 )
2-Butanone (MEK) 1470102U 1500 102 1470 1490 102 30-160 0.68 (< 20 )
2-Chlorotoluene 49010.2U 473 97 490 466 95 70-130 1.40 (< 20 )
2-Hexanone 1470102U 1550 106 1470 1560 106 45-145 0.12 (< 20 )
4-Chlorotoluene 49010.2U 470 96 490 464 95 75-125 1.30 (< 20 )
4-Isopropyltoluene 49010.2U 472 96 490 473 96 75-135 0.17 (< 20 )
4-Methyl-2-pentanone (MIBK) 1470102U 1530 104 1470 1530 104 45-145 0.28 (< 20 )
Benzene 4905.10U 438 89 490 433 88 75-125 1.00 (< 20 )
Bromobenzene 49010.2U 464 95 490 461 94 65-120 0.53 (< 20 )
Bromochloromethane 49010.2U 461 94 490 455 93 70-125 1.30 (< 20 )
Bromodichloromethane 49010.2U 472 96 490 461 94 70-130 2.30 (< 20 )
Bromoform 49010.2U 463 95 490 468 96 55-135 1.10 (< 20 )
Bromomethane 49081.0U 563 115 490 493 101 30-160 13.20 (< 20 )
Carbon disulfide 73534.8J 681 88 735 712 92 45-160 4.40 (< 20 )
Carbon tetrachloride 49010.2U 440 90 490 434 89 65-135 1.20 (< 20 )
Chlorobenzene 49010.2U 462 94 490 460 94 75-125 0.57 (< 20 )
Chloroethane 49081.0U 507 103 490 475 97 40-155 6.60 (< 20 )
Print Date: 06/18/2013 11:17:03AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C96
Original Sample ID: 1150460
MS Sample ID: 1150461 MS
MSD Sample ID: 1150462 MSD
Analysis Date: 05/30/2013 21:13
Analysis Date: 05/30/2013 20:23
Analysis Date: 05/30/2013 20:40
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Matrix Spike Summary
RPD CL
Chloroform 49010.2U 469 96 490 462 94 70-125 1.60 (< 20 )
Chloromethane 4905.88J 472 95 490 467 94 50-130 1.00 (< 20 )
cis-1,2-Dichloroethene 49010.2U 466 95 490 463 94 65-125 0.63 (< 20 )
cis-1,3-Dichloropropene 49010.2U 470 96 490 467 95 70-125 0.59 (< 20 )
Dibromochloromethane 49010.2U 472 96 490 464 95 65-130 1.80 (< 20 )
Dibromomethane 49010.2U 464 95 490 457 93 75-130 1.50 (< 20 )
Dichlorodifluoromethane 49019.6U 443 90 490 430 88 35-135 3.00 (< 20 )
Ethylbenzene 49010.2U 468 96 490 466 95 75-125 0.56 (< 20 )
Hexachlorobutadiene 49013.1J 480 95 490 487 97 55-140 1.50 (< 20 )
Isopropylbenzene (Cumene) 49010.2U 474 97 490 471 96 75-130 0.62 (< 20 )
Methyl-t-butyl ether 73540.6U 694 94 735 682 93 63-149 1.70 (< 20 )
Methylene chloride 49040.6U 427 87 490 415 85 55-140 2.90 (< 20 )
n-Butylbenzene 49010.2U 477 97 490 480 98 65-140 0.55 (< 20 )
n-Propylbenzene 49010.2U 469 96 490 469 96 65-135 0.04 (< 20 )
Naphthalene 49019.6U 477 97 490 487 99 40-125 2.10 (< 20 )
o-Xylene 49010.2U 466 95 490 463 94 75-125 0.67 (< 20 )
P & M -Xylene 98019.6U 928 95 980 919 94 80-125 1.00 (< 20 )
sec-Butylbenzene 49010.2U 472 96 490 474 97 65-130 0.35 (< 20 )
Styrene 49010.2U 462 94 490 466 95 75-125 0.85 (< 20 )
tert-Butylbenzene 49010.2U 466 95 490 464 95 65-130 0.39 (< 20 )
Tetrachloroethene 49011.8 484 96 490 487 97 65-140 0.44 (< 20 )
Toluene 49010.2U 485 99 490 485 99 70-125 0.10 (< 20 )
trans-1,2-Dichloroethene 4907.84J 468 94 490 472 95 65-135 0.94 (< 20 )
trans-1,3-Dichloropropene 49010.2U 467 95 490 464 95 65-125 0.74 (< 20 )
Trichloroethene 4905.10U 438 89 490 438 89 75-125 0.00 (< 20 )
Trichlorofluoromethane 49019.6U 447 91 490 441 90 25-185 1.40 (< 20 )
Vinyl chloride 49010.2U 486 99 490 484 99 60-125 0.40 (< 20 )
Xylenes (total) 147040.6U 1390 95 1470 1380 94 80-125 0.91 (< 20 )
Surrogates
1,2-Dichloroethane-D4 490 451 92 490 470 96 79-118 4.00
4-Bromofluorobenzene 1310 1070 82 1310 1080 83 67-138 1.40
Toluene-d8 490 436 89 490 466 95 85-115 6.60
Print Date: 06/18/2013 11:17:03AM
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C97
Original Sample ID: 1150460
MS Sample ID: 1150461 MS
MSD Sample ID: 1150462 MSD
Analysis Date:
Analysis Date: 05/30/2013 20:23
Analysis Date: 05/30/2013 20:40
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031015
Matrix Spike Summary
RPD CL
Batch Information
Prep Batch: VXX24760
Prep Method: Vol. Extraction SW8260 Field Extracted L
Prep Date/Time: 5/30/2013 8:00:00AM
Prep Initial Wt./Vol.: 76.50g
Prep Extract Vol: 25.00mL
Analytical Batch: VMS13526
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 5/30/2013 8:23:00PM
Print Date: 06/18/2013 11:17:03AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C98
Blank ID: MB for HBN 1452659 [VXX/24762]
Blank Lab ID: 1150551
QC for Samples:
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
1,1,1,2-Tetrachloroethane 25.0 ug/Kg7.8015.6U
1,1,1-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1,2,2-Tetrachloroethane 50.0 ug/Kg15.030.0U
1,1,2-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethene 25.0 ug/Kg7.8015.6U
1,1-Dichloropropene 25.0 ug/Kg7.8015.6U
1,2,3-Trichlorobenzene 50.0 ug/Kg15.030.0U
1,2,3-Trichloropropane 25.0 ug/Kg7.8015.6U
1,2,4-Trichlorobenzene 25.0 ug/Kg7.8015.6U
1,2,4-Trimethylbenzene 50.0 ug/Kg15.030.0U
1,2-Dibromo-3-chloropropane 100 ug/Kg31.062.0U
1,2-Dibromoethane 25.0 ug/Kg7.8015.6U
1,2-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,2-Dichloroethane 25.0 ug/Kg7.8015.6U
1,2-Dichloropropane 25.0 ug/Kg7.8015.6U
1,3,5-Trimethylbenzene 25.0 ug/Kg7.8015.6U
1,3-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,3-Dichloropropane 25.0 ug/Kg7.8015.6U
1,4-Dichlorobenzene 25.0 ug/Kg7.8015.6U
2,2-Dichloropropane 25.0 ug/Kg7.8015.6U
2-Butanone (MEK) 250 ug/Kg78.0156U
2-Chlorotoluene 25.0 ug/Kg7.8015.6U
2-Hexanone 250 ug/Kg78.0156U
4-Chlorotoluene 25.0 ug/Kg7.8015.6U
4-Isopropyltoluene 25.0 ug/Kg7.8015.6U
4-Methyl-2-pentanone (MIBK) 250 ug/Kg78.0156U
Benzene 12.5 ug/Kg3.907.80U
Bromobenzene 25.0 ug/Kg7.8015.6U
Bromochloromethane 25.0 ug/Kg7.8015.6U
Bromodichloromethane 25.0 ug/Kg7.8015.6U
Bromoform 25.0 ug/Kg7.8015.6U
Bromomethane 200 ug/Kg62.0124U
Carbon disulfide 100 ug/Kg31.062.0U
Carbon tetrachloride 25.0 ug/Kg7.8015.6U
Chlorobenzene 25.0 ug/Kg7.8015.6U
Chloroethane 200 ug/Kg62.0124U
Chloroform 25.0 ug/Kg7.8015.6U
Print Date: 06/18/2013 11:17:04AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C99
Blank ID: MB for HBN 1452659 [VXX/24762]
Blank Lab ID: 1150551
QC for Samples:
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Chloromethane 25.0 ug/Kg7.8015.6U
cis-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
cis-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Dibromochloromethane 25.0 ug/Kg7.8015.6U
Dibromomethane 25.0 ug/Kg7.8015.6U
Dichlorodifluoromethane 50.0 ug/Kg15.030.0U
Ethylbenzene 25.0 ug/Kg7.8015.6U
Hexachlorobutadiene 50.0 ug/Kg15.030.0U
Isopropylbenzene (Cumene) 25.0 ug/Kg7.8015.6U
Methylene chloride 100 ug/Kg31.062.0U
Methyl-t-butyl ether 100 ug/Kg31.062.0U
Naphthalene 50.0 ug/Kg15.030.0U
n-Butylbenzene 25.0 ug/Kg7.8015.6U
n-Propylbenzene 25.0 ug/Kg7.8015.6U
o-Xylene 25.0 ug/Kg7.8015.6U
P & M -Xylene 50.0 ug/Kg15.030.0U
sec-Butylbenzene 25.0 ug/Kg7.8015.6U
Styrene 25.0 ug/Kg7.8015.6U
tert-Butylbenzene 25.0 ug/Kg7.8015.6U
Tetrachloroethene 12.5 ug/Kg3.907.80U
Toluene 25.0 ug/Kg7.8015.6U
trans-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
trans-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Trichloroethene 12.5 ug/Kg3.907.80U
Trichlorofluoromethane 50.0 ug/Kg15.030.0U
Vinyl chloride 25.0 ug/Kg7.8015.6U
Xylenes (total) 100 ug/Kg31.062.0U
Surrogates
1,2-Dichloroethane-D4 79-118 %113
4-Bromofluorobenzene 67-138 %104
Toluene-d8 85-115 %109
Print Date: 06/18/2013 11:17:04AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C100
Blank ID: MB for HBN 1452659 [VXX/24762]
Blank Lab ID: 1150551
QC for Samples:
1132031015
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Batch Information
Analytical Batch: VMS13528
Analytical Method: SW8260B
Instrument: HP 5890 Series II MS3 VNA
Analyst: HM
Analytical Date/Time: 5/31/2013 11:40:01AM
Prep Batch: VXX24762
Prep Method: SW5035A
Prep Date/Time: 5/31/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/18/2013 11:17:04AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C101
Blank Spike ID: LCS for HBN 1132031 [VXX24762]
Blank Spike Lab ID: 1150552
Date Analyzed: 05/31/2013 12:00
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132031015
Result
1,1,1,2-Tetrachloroethane 750 90 ( 75-125 )677
1,1,1-Trichloroethane 750 93 ( 70-135 )698
1,1,2,2-Tetrachloroethane 750 99 ( 55-130 )740
1,1,2-Trichloroethane 750 103 ( 60-125 )776
1,1-Dichloroethane 750 99 ( 75-125 )741
1,1-Dichloroethene 750 100 ( 65-135 )753
1,1-Dichloropropene 750 102 ( 70-135 )762
1,2,3-Trichlorobenzene 750 98 ( 60-135 )731
1,2,3-Trichloropropane 750 94 ( 65-130 )705
1,2,4-Trichlorobenzene 750 100 ( 65-130 )747
1,2,4-Trimethylbenzene 750 96 ( 65-135 )723
1,2-Dibromo-3-chloropropane 750 84 ( 40-135 )630
1,2-Dibromoethane 750 102 ( 70-125 )764
1,2-Dichlorobenzene 750 100 ( 75-120 )751
1,2-Dichloroethane 750 99 ( 70-135 )743
1,2-Dichloropropane 750 97 ( 70-120 )729
1,3,5-Trimethylbenzene 750 98 ( 65-135 )733
1,3-Dichlorobenzene 750 96 ( 70-125 )719
1,3-Dichloropropane 750 100 ( 75-125 )746
1,4-Dichlorobenzene 750 94 ( 70-125 )706
2,2-Dichloropropane 750 103 ( 65-135 )775
2-Butanone (MEK) 2250 96 ( 30-160 )2170
2-Chlorotoluene 750 96 ( 70-130 )717
2-Hexanone 2250 106 ( 45-145 )2380
4-Chlorotoluene 750 97 ( 75-125 )724
4-Isopropyltoluene 750 99 ( 75-135 )743
4-Methyl-2-pentanone (MIBK) 2250 95 ( 45-145 )2130
Benzene 750 94 ( 75-125 )702
Bromobenzene 750 96 ( 65-120 )722
Bromochloromethane 750 100 ( 70-125 )746
Bromodichloromethane 750 87 ( 70-130 )652
Bromoform 750 83 ( 55-135 )624
Bromomethane 750 98 ( 30-160 )736
Print Date: 06/18/2013 11:17:04AM
Member of SGS Group
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C102
Blank Spike ID: LCS for HBN 1132031 [VXX24762]
Blank Spike Lab ID: 1150552
Date Analyzed: 05/31/2013 12:00
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132031015
Result
Carbon disulfide 1130 95 ( 45-160 )1070
Carbon tetrachloride 750 87 ( 65-135 )656
Chlorobenzene 750 99 ( 75-125 )744
Chloroethane 750 101 ( 40-155 )759
Chloroform 750 96 ( 70-125 )723
Chloromethane 750 103 ( 50-130 )770
cis-1,2-Dichloroethene 750 94 ( 65-125 )704
cis-1,3-Dichloropropene 750 88 ( 70-125 )663
Dibromochloromethane 750 86 ( 65-130 )646
Dibromomethane 750 97 ( 75-130 )731
Dichlorodifluoromethane 750 102 ( 35-135 )762
Ethylbenzene 750 100 ( 75-125 )751
Hexachlorobutadiene 750 97 ( 55-140 )729
Isopropylbenzene (Cumene) 750 102 ( 75-130 )765
Methyl-t-butyl ether 1130 100 ( 63-149 )1130
Methylene chloride 750 98 ( 55-140 )737
n-Butylbenzene 750 100 ( 65-140 )751
n-Propylbenzene 750 99 ( 65-135 )739
Naphthalene 750 100 ( 40-125 )753
o-Xylene 750 99 ( 75-125 )746
P & M -Xylene 1500 101 ( 80-125 )1510
sec-Butylbenzene 750 98 ( 65-130 )731
Styrene 750 101 ( 75-125 )755
tert-Butylbenzene 750 98 ( 65-130 )732
Tetrachloroethene 750 96 ( 65-140 )716
Toluene 750 100 ( 70-125 )747
trans-1,2-Dichloroethene 750 100 ( 65-135 )749
trans-1,3-Dichloropropene 750 93 ( 65-125 )696
Trichloroethene 750 94 ( 75-125 )708
Trichlorofluoromethane 750 81 ( 25-185 )610
Vinyl chloride 750 107 ( 60-125 )806
Xylenes (total) 2250 100 ( 80-125 )2260
Surrogates
Print Date: 06/18/2013 11:17:04AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
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C103
Blank Spike ID: LCS for HBN 1132031 [VXX24762]
Blank Spike Lab ID: 1150552
Date Analyzed: 05/31/2013 12:00
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (%)
QC for Samples: 1132031015
Result
1,2-Dichloroethane-D4 750 105 ( 79-118 )105
4-Bromofluorobenzene 750 97 ( 67-138 )96.7
Toluene-d8 750 104 ( 85-115 )104
Batch Information
Analytical Batch: VMS13528
Analytical Method: SW8260B
Instrument: HP 5890 Series II MS3 VNA
Analyst: HM
Prep Batch: VXX24762
Prep Method: SW5035A
Prep Date/Time: 05/31/2013 08:00
Spike Init Wt./Vol.: 750 ug/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/18/2013 11:17:04AM
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C104
Original Sample ID: 1150553
MS Sample ID: 1150554 MS
MSD Sample ID: 1150555 MSD
Analysis Date: 05/31/2013 14:56
Analysis Date: 05/31/2013 12:39
Analysis Date: 05/31/2013 12:56
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031015
Matrix Spike Summary
RPD CL
1,1,1,2-Tetrachloroethane 2685.56U 265 99 268 250 94 75-125 5.80 (< 20 )
1,1,1-Trichloroethane 2685.56U 278 104 268 276 103 70-135 0.93 (< 20 )
1,1,2,2-Tetrachloroethane 26810.7U 302 113 268 284 106 55-130 6.10 (< 20 )
1,1,2-Trichloroethane 2685.56U 305 114 268 284 106 60-125 7.20 (< 20 )
1,1-Dichloroethane 2685.56U 292 109 268 285 107 75-125 2.50 (< 20 )
1,1-Dichloroethene 2685.56U 309 116 268 307 115 65-135 0.55 (< 20 )
1,1-Dichloropropene 2685.56U 301 112 268 296 111 70-135 1.70 (< 20 )
1,2,3-Trichlorobenzene 26810.7U 279 104 268 270 101 60-135 3.40 (< 20 )
1,2,3-Trichloropropane 2685.56U 288 108 268 270 101 65-130 6.50 (< 20 )
1,2,4-Trichlorobenzene 2685.56U 285 107 268 274 103 65-130 3.80 (< 20 )
1,2,4-Trimethylbenzene 2687.76J 291 106 268 277 101 65-135 4.90 (< 20 )
1,2-Dibromo-3-chloropropane 26822.2U 270 101 268 247 92 40-135 9.00 (< 20 )
1,2-Dibromoethane 2685.56U 305 114 268 288 108 70-125 5.90 (< 20 )
1,2-Dichlorobenzene 2685.56U 288 108 268 280 105 75-120 2.90 (< 20 )
1,2-Dichloroethane 2685.56U 298 112 268 293 109 70-135 2.00 (< 20 )
1,2-Dichloropropane 2685.56U 291 109 268 289 108 70-120 0.92 (< 20 )
1,3,5-Trimethylbenzene 2683.48J 291 108 268 279 103 65-135 4.10 (< 20 )
1,3-Dichlorobenzene 2685.56U 279 104 268 269 100 70-125 3.70 (< 20 )
1,3-Dichloropropane 2685.56U 295 110 268 277 104 75-125 6.20 (< 20 )
1,4-Dichlorobenzene 2685.56U 277 104 268 269 101 70-125 3.20 (< 20 )
2,2-Dichloropropane 2685.56U 305 114 268 302 113 65-135 1.10 (< 20 )
2-Butanone (MEK) 80355.6U 921 115 803 848 106 30-160 8.20 (< 20 )
2-Chlorotoluene 2685.56U 283 106 268 273 102 70-130 3.40 (< 20 )
2-Hexanone 80355.6U 1000 125 803 914 114 45-145 9.40 (< 20 )
4-Chlorotoluene 2685.56U 282 105 268 268 100 75-125 5.20 (< 20 )
4-Isopropyltoluene 2686.15J 292 107 268 282 103 75-135 3.70 (< 20 )
4-Methyl-2-pentanone (MIBK) 80355.6U 908 113 803 843 105 45-145 7.40 (< 20 )
Benzene 2682.78U 276 103 268 271 101 75-125 1.60 (< 20 )
Bromobenzene 2685.56U 285 107 268 274 103 65-120 4.00 (< 20 )
Bromochloromethane 2685.56U 301 113 268 290 109 70-125 3.60 (< 20 )
Bromodichloromethane 2685.56U 265 99 268 262 98 70-130 1.30 (< 20 )
Bromoform 2685.56U 255 95 268 238 89 55-135 6.80 (< 20 )
Bromomethane 26844.2U 318 119 268 323 121 30-160 1.60 (< 20 )
Carbon disulfide 40122.2U 433 108 401 425 106 45-160 1.70 (< 20 )
Carbon tetrachloride 2685.56U 254 95 268 255 95 65-135 0.28 (< 20 )
Chlorobenzene 2685.56U 290 109 268 275 103 75-125 5.50 (< 20 )
Chloroethane 26844.2U 316 118 268 321 120 40-155 1.80 (< 20 )
Print Date: 06/18/2013 11:17:05AM
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C105
Original Sample ID: 1150553
MS Sample ID: 1150554 MS
MSD Sample ID: 1150555 MSD
Analysis Date: 05/31/2013 14:56
Analysis Date: 05/31/2013 12:39
Analysis Date: 05/31/2013 12:56
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031015
Matrix Spike Summary
RPD CL
Chloroform 2685.56U 288 108 268 282 106 70-125 2.10 (< 20 )
Chloromethane 2685.56U 301 112 268 300 112 50-130 0.15 (< 20 )
cis-1,2-Dichloroethene 2685.56U 293 110 268 286 107 65-125 2.70 (< 20 )
cis-1,3-Dichloropropene 2685.56U 270 101 268 263 98 70-125 2.80 (< 20 )
Dibromochloromethane 2685.56U 254 95 268 244 91 65-130 4.30 (< 20 )
Dibromomethane 2685.56U 296 111 268 289 108 75-130 2.30 (< 20 )
Dichlorodifluoromethane 26810.7U 281 105 268 274 102 35-135 2.50 (< 20 )
Ethylbenzene 2685.56U 297 111 268 277 104 75-125 6.60 (< 20 )
Hexachlorobutadiene 26810.7U 299 112 268 287 107 55-140 3.90 (< 20 )
Isopropylbenzene (Cumene) 2685.56U 296 111 268 278 104 75-130 6.10 (< 20 )
Methyl-t-butyl ether 40122.2U 454 113 401 442 110 63-149 2.60 (< 20 )
Methylene chloride 26822.2U 282 105 268 272 102 55-140 3.60 (< 20 )
n-Butylbenzene 2685.56U 289 108 268 282 105 65-140 2.60 (< 20 )
n-Propylbenzene 2685.56U 291 109 268 279 104 65-135 4.10 (< 20 )
Naphthalene 26810.7U 308 115 268 292 109 40-125 5.30 (< 20 )
o-Xylene 2685.56U 291 109 268 275 103 75-125 5.60 (< 20 )
P & M -Xylene 53510.7U 593 111 535 563 105 80-125 5.20 (< 20 )
sec-Butylbenzene 2685.56U 284 106 268 271 101 65-130 4.40 (< 20 )
Styrene 2685.56U 292 109 268 277 104 75-125 5.00 (< 20 )
tert-Butylbenzene 2685.56U 286 107 268 274 102 65-130 4.20 (< 20 )
Tetrachloroethene 2682.78U 278 104 268 262 98 65-140 6.10 (< 20 )
Toluene 2685.56U 287 107 268 276 103 70-125 4.10 (< 20 )
trans-1,2-Dichloroethene 2685.56U 291 109 268 286 107 65-135 1.90 (< 20 )
trans-1,3-Dichloropropene 2685.56U 272 102 268 259 97 65-125 4.80 (< 20 )
Trichloroethene 2682.78U 275 103 268 272 102 75-125 1.30 (< 20 )
Trichlorofluoromethane 26810.7U 332 124 268 366 137 25-185 9.70 (< 20 )
Vinyl chloride 2685.56U 293 110 268 289 108 60-125 1.40 (< 20 )
Xylenes (total) 80322.2U 884 110 803 838 104 80-125 5.30 (< 20 )
Surrogates
1,2-Dichloroethane-D4 268 287 107 268 295 110 79-118 2.60
4-Bromofluorobenzene 713 494 69 713 492 69 67-138 0.47
Toluene-d8 268 275 103 268 268 100 85-115 2.60
Print Date: 06/18/2013 11:17:05AM
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C106
Original Sample ID: 1150553
MS Sample ID: 1150554 MS
MSD Sample ID: 1150555 MSD
Analysis Date:
Analysis Date: 05/31/2013 12:39
Analysis Date: 05/31/2013 12:56
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031015
Matrix Spike Summary
RPD CL
Batch Information
Prep Batch: VXX24762
Prep Method: Vol. Extraction SW8260 Field Extracted L
Prep Date/Time: 5/31/2013 8:00:00AM
Prep Initial Wt./Vol.: 140.19g
Prep Extract Vol: 25.00mL
Analytical Batch: VMS13528
Analytical Method: SW8260B
Instrument: HP 5890 Series II MS3 VNA
Analyst: HM
Analytical Date/Time: 5/31/2013 12:39:00PM
Print Date: 06/18/2013 11:17:05AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C107
Blank ID: MB for HBN 1453288 [VXX/24775]
Blank Lab ID: 1151394
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011,
1132031014
Matrix: Soil/Solid (dry weight)
Results by AK101
DL UnitsLOQ/CLResultsParameter
Method Blank
Gasoline Range Organics 2.50 mg/Kg0.7500.936J
Surrogates
4-Bromofluorobenzene 50-150 %82.3
Batch Information
Analytical Batch: VFC11449
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Analytical Date/Time: 6/5/2013 10:40:00AM
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 6/5/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/18/2013 11:17:05AM
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C108
Blank Spike ID: LCS for HBN 1132031 [VXX24775]
Blank Spike Lab ID: 1151395
Date Analyzed: 06/05/2013 11:36
Spike Duplicate ID: LCSD for HBN 1132031
[VXX24775]
Spike Duplicate Lab ID: 1151396
Results by AK101
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011, 1132031014
Result
Gasoline Range Organics 10.0 98 10.0 9.50 95 ( 60-120 ) (< 20 ) 3.009.80
Surrogates
4-Bromofluorobenzene 1.25 83 1.25 82.9 83 ( 50-150 ) 0.4683.3
Batch Information
Analytical Batch: VFC11449
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 06/05/2013 08:00
Spike Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Print Date: 06/18/2013 11:17:06AM
Member of SGS Group
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C109
Blank ID: MB for HBN 1452070 [XXX/29074]
Blank Lab ID: 1150320
QC for Samples:
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010,
1132031011, 1132031012, 1132031013
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
1,2,4-Trichlorobenzene 0.250 mg/Kg0.07800.156U
1,2-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,3-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,4-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2,4,5-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4,6-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dimethylphenol 0.250 mg/Kg0.07800.156U
2,4-Dinitrophenol 3.00 mg/Kg0.9401.88U
2,4-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2,6-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,6-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2-Chlorophenol 0.250 mg/Kg0.07800.156U
2-Methyl-4,6-dinitrophenol 2.00 mg/Kg0.6201.24U
2-Methylnaphthalene 0.250 mg/Kg0.07800.156U
2-Methylphenol (o-Cresol) 0.250 mg/Kg0.07800.156U
2-Nitroaniline 0.250 mg/Kg0.07800.156U
2-Nitrophenol 0.250 mg/Kg0.07800.156U
3&4-Methylphenol (p&m-Cresol) 1.00 mg/Kg0.3100.620U
3,3-Dichlorobenzidine 0.250 mg/Kg0.07800.156U
3-Nitroaniline 0.500 mg/Kg0.1500.300U
4-Bromophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Chloro-3-methylphenol 0.250 mg/Kg0.07800.156U
4-Chloroaniline 0.500 mg/Kg0.1500.300U
4-Chlorophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Nitroaniline 3.00 mg/Kg0.9401.88U
4-Nitrophenol 1.00 mg/Kg0.3100.620U
Acenaphthene 0.250 mg/Kg0.07800.156U
Acenaphthylene 0.250 mg/Kg0.07800.156U
Aniline 2.00 mg/Kg0.6201.24U
Anthracene 0.250 mg/Kg0.07800.156U
Azobenzene 0.250 mg/Kg0.07800.156U
Benzo(a)Anthracene 0.250 mg/Kg0.07800.156U
Benzo[a]pyrene 0.250 mg/Kg0.07800.156U
Benzo[b]Fluoranthene 0.250 mg/Kg0.07800.156U
Benzo[g,h,i]perylene 0.250 mg/Kg0.07800.156U
Print Date: 06/18/2013 11:17:07AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C110
Blank ID: MB for HBN 1452070 [XXX/29074]
Blank Lab ID: 1150320
QC for Samples:
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010,
1132031011, 1132031012, 1132031013
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Benzo[k]fluoranthene 0.250 mg/Kg0.07800.156U
Benzoic acid 1.50 mg/Kg0.7501.50U
Benzyl alcohol 0.250 mg/Kg0.07800.156U
Bis(2chloro1methylethyl)Ether 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethoxy)methane 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethyl)ether 0.250 mg/Kg0.07800.156U
bis(2-Ethylhexyl)phthalate 0.250 mg/Kg0.07800.156U
Butylbenzylphthalate 0.250 mg/Kg0.07800.156U
Carbazole 0.250 mg/Kg0.07800.156U
Chrysene 0.250 mg/Kg0.07800.156U
Dibenzo[a,h]anthracene 0.250 mg/Kg0.07800.156U
Dibenzofuran 0.250 mg/Kg0.07800.156U
Diethylphthalate 0.250 mg/Kg0.07800.156U
Dimethylphthalate 0.250 mg/Kg0.07800.156U
Di-n-butylphthalate 0.250 mg/Kg0.07800.156U
di-n-Octylphthalate 0.500 mg/Kg0.1500.300U
Fluoranthene 0.250 mg/Kg0.07800.156U
Fluorene 0.250 mg/Kg0.07800.156U
Hexachlorobenzene 0.250 mg/Kg0.07800.156U
Hexachlorobutadiene 0.250 mg/Kg0.07800.156U
Hexachlorocyclopentadiene 0.700 mg/Kg0.2000.400U
Hexachloroethane 0.250 mg/Kg0.07800.156U
Indeno[1,2,3-c,d] pyrene 0.250 mg/Kg0.07800.156U
Isophorone 0.250 mg/Kg0.07800.156U
Naphthalene 0.250 mg/Kg0.07800.156U
Nitrobenzene 0.250 mg/Kg0.07800.156U
N-Nitrosodimethylamine 0.250 mg/Kg0.07800.156U
N-Nitroso-di-n-propylamine 0.250 mg/Kg0.07800.156U
N-Nitrosodiphenylamine 0.250 mg/Kg0.07800.156U
Pentachlorophenol 2.00 mg/Kg0.6201.24U
Phenanthrene 0.250 mg/Kg0.07800.156U
Phenol 0.250 mg/Kg0.07800.156U
Pyrene 0.250 mg/Kg0.07800.156U
Surrogates
2,4,6-Tribromophenol 35-125 %86
2-Fluorobiphenyl 45-105 %85
2-Fluorophenol 35-105 %71
Nitrobenzene-d5 35-100 %72.5
Print Date: 06/18/2013 11:17:07AM
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C111
Blank ID: MB for HBN 1452070 [XXX/29074]
Blank Lab ID: 1150320
QC for Samples:
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010,
1132031011, 1132031012, 1132031013
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Phenol-d6 40-100 %76.4
Terphenyl-d14 30-125 %99.6
Batch Information
Analytical Batch: XMS7345
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Analytical Date/Time: 5/30/2013 7:14:00PM
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 5/30/2013 11:00:00AM
Prep Initial Wt./Vol.: 22.5 g
Prep Extract Vol: 1 mL
Print Date: 06/18/2013 11:17:07AM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C112
Blank Spike ID: LCS for HBN 1132031 [XXX29074]
Blank Spike Lab ID: 1150322
Date Analyzed: 05/30/2013 19:32
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Result
1,2,4-Trichlorobenzene 4.44 81 ( 45-110 )3.59
1,2-Dichlorobenzene 4.44 72 ( 45-100 )3.20
1,3-Dichlorobenzene 4.44 74 ( 40-100 )3.27
1,4-Dichlorobenzene 4.44 73 ( 35-105 )3.25
1-Chloronaphthalene 1.78 95 ( 44-105 )1.69
2,4,5-Trichlorophenol 4.44 102 ( 50-110 )4.54
2,4,6-Trichlorophenol 4.44 94 ( 45-110 )4.18
2,4-Dichlorophenol 4.44 90 ( 45-110 )3.98
2,4-Dimethylphenol 4.44 88 ( 30-105 )3.91
2,4-Dinitrophenol 8 98 ( 15-130 )7.84
2,4-Dinitrotoluene 4.44 107 ( 50-115 )4.76
2,6-Dichlorophenol 1.78 90 ( 52-102 )1.59
2,6-Dinitrotoluene 4.44 99 ( 50-110 )4.40
2-Chloronaphthalene 4.44 97 ( 45-105 )4.31
2-Chlorophenol 4.44 76 ( 45-105 )3.38
2-Methyl-4,6-dinitrophenol 8 120 ( 30-135 )9.58
2-Methylnaphthalene 4.44 88 ( 45-105 )3.92
2-Methylphenol (o-Cresol) 4.44 80 ( 40-105 )3.56
2-Nitroaniline 4.44 110 ( 45-120 )4.88
2-Nitrophenol 4.44 93 ( 40-110 )4.13
3&4-Methylphenol (p&m-Cresol) 6.22 94 ( 40-105 )5.88
3,3-Dichlorobenzidine 4.44 93 ( 10-130 )4.13
3-Nitroaniline 4.44 105 ( 25-110 )4.65
4-Bromophenyl-phenylether 4.44 107 ( 45-115 )4.76
4-Chloro-3-methylphenol 4.44 99 ( 45-115 )4.39
4-Chloroaniline 4.44 85 ( 10-100 )3.79
4-Chlorophenyl-phenylether 4.44 107 ( 45-110 )4.76
4-Nitroaniline 4.44 109 ( 35-115 )4.84
4-Nitrophenol 6.22 97 ( 15-140 )6.05
Acenaphthene 4.44 96 ( 45-110 )4.24
Acenaphthylene 4.44 101 ( 45-105 )4.51
Aniline 4.44 64 ( 20-84 )2.85
Anthracene 4.44 97 ( 55-105 )4.31
Print Date: 06/18/2013 11:17:07AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C113
Blank Spike ID: LCS for HBN 1132031 [XXX29074]
Blank Spike Lab ID: 1150322
Date Analyzed: 05/30/2013 19:32
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Result
Azobenzene 4.44 99 ( 63-117 )4.39
Benzo(a)Anthracene 4.44 105 ( 50-110 )4.68
Benzo[a]pyrene 4.44 101 ( 50-110 )4.50
Benzo[b]Fluoranthene 4.44 112 ( 45-115 )4.96
Benzo[g,h,i]perylene 4.44 96 ( 40-125 )4.25
Benzo[k]fluoranthene 4.44 100 ( 45-125 )4.44
Benzoic acid 6.22 103 ( 10-110 )6.42
Benzyl alcohol 4.44 87 ( 20-125 )3.86
Bis(2-Chloroethoxy)methane 4.44 95 ( 45-110 )4.21
Bis(2-Chloroethyl)ether 4.44 91 ( 40-105 )4.06
bis(2-Ethylhexyl)phthalate 4.44 115 ( 45-125 )5.11
Bis(2chloro1methylethyl)Ether 4.44 79 ( 20-115 )3.50
Butylbenzylphthalate 4.44 116 ( 50-125 )5.14
Carbazole 4.44 103 ( 45-115 )4.57
Chrysene 4.44 111 ( 55-110 )4.92 *
Di-n-butylphthalate 4.44 112 ( 55-110 )4.98 *
di-n-Octylphthalate 4.44 117 ( 40-130 )5.20
Dibenzo[a,h]anthracene 4.44 102 ( 40-125 )4.51
Dibenzofuran 4.44 102 ( 50-105 )4.55
Diethylphthalate 4.44 110 ( 50-115 )4.89
Dimethylphthalate 4.44 111 ( 50-110 )4.93 *
Fluoranthene 4.44 104 ( 55-115 )4.63
Fluorene 4.44 99 ( 50-110 )4.41
Hexachlorobenzene 4.44 100 ( 45-120 )4.46
Hexachlorobutadiene 4.44 89 ( 40-115 )3.95
Hexachlorocyclopentadiene 4.44 97 ( 48-108 )4.32
Hexachloroethane 4.44 74 ( 35-110 )3.28
Indeno[1,2,3-c,d] pyrene 4.44 98 ( 40-120 )4.34
Isophorone 4.44 95 ( 45-110 )4.20
N-Nitroso-di-n-propylamine 4.44 93 ( 40-115 )4.12
N-Nitrosodimethylamine 4.44 80 ( 20-115 )3.57
N-Nitrosodiphenylamine 4.44 85 ( 50-115 )3.77
Naphthalene 4.44 82 ( 40-105 )3.65
Print Date: 06/18/2013 11:17:07AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C114
Blank Spike ID: LCS for HBN 1132031 [XXX29074]
Blank Spike Lab ID: 1150322
Date Analyzed: 05/30/2013 19:32
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Result
Nitrobenzene 4.44 89 ( 40-115 )3.94
Pentachlorophenol 6.22 100 ( 25-120 )6.22
Phenanthrene 4.44 100 ( 50-110 )4.42
Phenol 4.44 80 ( 40-100 )3.56
Pyrene 4.44 104 ( 45-125 )4.62
Surrogates
2,4,6-Tribromophenol 8.89 93 ( 35-125 )93.2
2-Fluorobiphenyl 4.44 94 ( 45-105 )93.7
2-Fluorophenol 8.89 73 ( 35-105 )72.7
Nitrobenzene-d5 4.44 81 ( 35-100 )80.7
Phenol-d6 8.89 79 ( 40-100 )78.9
Terphenyl-d14 4.44 101 ( 30-125 )101
Batch Information
Analytical Batch: XMS7345
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Prep Batch: XXX29074
Prep Method: SW3550C
Prep Date/Time: 05/30/2013 11:00
Spike Init Wt./Vol.: 4.44 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/18/2013 11:17:07AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C115
Original Sample ID: 1132031006
MS Sample ID: 1150324 MS
MSD Sample ID: 1150325 MSD
Analysis Date: 06/03/2013 19:47
Analysis Date: 06/03/2013 20:04
Analysis Date: 06/03/2013 20:21
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Matrix Spike Summary
RPD CL
1,2,4-Trichlorobenzene 6.120.346U 4.58 75 6.27 4.58 73 45-110 0.17 (< 30 )
1,2-Dichlorobenzene 6.120.346U 4.45 73 6.27 4.15 66 45-100 7.00 (< 30 )
1,3-Dichlorobenzene 6.120.346U 4.39 72 6.27 4.11 66 40-100 6.50 (< 30 )
1,4-Dichlorobenzene 6.120.346U 4.36 71 6.27 4.11 66 35-105 6.00 (< 30 )
1-Chloronaphthalene 2.440.346U 2.18 89 2.51 1.92 77 44-105 12.10 (< 30 )
2,4,5-Trichlorophenol 6.120.346U 5.89 96 6.27 6.24 100 50-110 5.80 (< 30 )
2,4,6-Trichlorophenol 6.120.346U 5.56 91 6.27 5.96 95 45-110 6.70 (< 30 )
2,4-Dichlorophenol 6.120.346U 5.07 83 6.27 5.38 86 45-110 6.10 (< 30 )
2,4-Dimethylphenol 6.120.346U 5.08 83 6.27 5.32 85 30-105 4.70 (< 30 )
2,4-Dinitrophenol 11.04.16U 9.04 82 11.3 10.1 89 15-130 10.70 (< 30 )
2,4-Dinitrotoluene 6.120.346U 6.07 99 6.27 6.44 103 50-115 5.80 (< 30 )
2,6-Dichlorophenol 2.440.346U 2.02 82 2.51 2.08 83 52-102 2.80 (< 30 )
2,6-Dinitrotoluene 6.120.346U 5.55 91 6.27 5.86 94 50-110 5.40 (< 30 )
2-Chloronaphthalene 6.120.346U 5.13 84 6.27 5.75 92 45-105 11.40 (< 30 )
2-Chlorophenol 6.120.346U 4.62 76 6.27 4.46 71 45-105 3.60 (< 30 )
2-Methyl-4,6-dinitrophenol 11.02.77U 12.6 115 11.3 13.4 119 30-135 6.10 (< 30 )
2-Methylnaphthalene 6.120.346U 4.84 79 6.27 5.13 82 45-105 5.50 (< 30 )
2-Methylphenol (o-Cresol) 6.120.346U 4.80 79 6.27 4.79 76 40-105 0.29 (< 30 )
2-Nitroaniline 6.120.346U 6.10 100 6.27 6.48 103 45-120 6.20 (< 30 )
2-Nitrophenol 6.120.346U 5.42 89 6.27 5.52 88 40-110 1.70 (< 30 )
3&4-Methylphenol (p&m-Cresol) 8.561.39U 7.92 93 8.79 8.11 92 40-105 2.30 (< 30 )
3,3-Dichlorobenzidine 6.120.346U 5.42 89 6.27 5.79 92 10-130 6.80 (< 30 )
3-Nitroaniline 6.120.693U 5.78 95 6.27 6.17 98 25-110 6.50 (< 30 )
4-Bromophenyl-phenylether 6.120.346U 5.99 98 6.27 6.13 98 45-115 2.20 (< 30 )
4-Chloro-3-methylphenol 6.120.346U 5.54 91 6.27 5.93 95 45-115 6.90 (< 30 )
4-Chloroaniline 6.120.693U 4.94 81 6.27 5.08 81 10-100 2.60 (< 30 )
4-Chlorophenyl-phenylether 6.120.346U 5.73 94 6.27 5.89 94 45-110 2.50 (< 30 )
4-Nitroaniline 6.124.16U 6.02 98 6.27 6.34 101 35-115 5.30 (< 30 )
4-Nitrophenol 8.561.39U 7.88 92 8.79 8.31 95 15-140 5.40 (< 30 )
Acenaphthene 6.120.346U 5.38 88 6.27 5.52 88 45-110 2.50 (< 30 )
Acenaphthylene 6.120.346U 5.59 91 6.27 5.79 92 45-105 3.70 (< 30 )
Aniline 6.122.77U 4.12 68 6.27 4.03 64 20-84 2.40 (< 30 )
Anthracene 6.120.346U 5.88 96 6.27 5.83 93 55-105 0.81 (< 30 )
Azobenzene 6.120.346U 5.96 98 6.27 6.21 99 63-117 4.10 (< 30 )
Benzo(a)Anthracene 6.120.346U 5.83 96 6.27 6.23 99 50-110 6.60 (< 30 )
Benzo[a]pyrene 6.120.346U 5.92 97 6.27 6.03 96 50-110 1.80 (< 30 )
Benzo[b]Fluoranthene 6.120.346U 6.29 103 6.27 6.79 108 45-115 7.90 (< 30 )
Print Date: 06/18/2013 11:17:08AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C116
Original Sample ID: 1132031006
MS Sample ID: 1150324 MS
MSD Sample ID: 1150325 MSD
Analysis Date: 06/03/2013 19:47
Analysis Date: 06/03/2013 20:04
Analysis Date: 06/03/2013 20:21
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Matrix Spike Summary
RPD CL
Benzo[g,h,i]perylene 6.120.346U 5.10 83 6.27 5.08 81 40-125 0.34 (< 30 )
Benzo[k]fluoranthene 6.120.346U 6.38 104 6.27 6.26 100 45-125 2.00 (< 30 )
Benzoic acid 8.562.08U 5.88 69 8.79 7.25 83 10-110 20.90 (< 30 )
Benzyl alcohol 6.120.346U 5.08 83 6.27 5.13 82 20-125 0.85 (< 30 )
Bis(2-Chloroethoxy)methane 6.120.346U 5.37 88 6.27 5.48 87 45-110 2.10 (< 30 )
Bis(2-Chloroethyl)ether 6.120.346U 5.38 88 6.27 5.44 87 40-105 0.96 (< 30 )
bis(2-Ethylhexyl)phthalate 6.120.346U 6.34 104 6.27 6.78 108 45-125 6.60 (< 30 )
Bis(2chloro1methylethyl)Ether 6.120.346U 4.92 80 6.27 4.68 75 20-115 5.00 (< 30 )
Butylbenzylphthalate 6.120.346U 6.57 107 6.27 7.01 112 50-125 6.50 (< 30 )
Carbazole 6.120.346U 6.20 101 6.27 6.43 103 45-115 3.60 (< 30 )
Chrysene 6.120.346U 5.99 98 6.27 6.40 102 55-110 6.50 (< 30 )
Di-n-butylphthalate 6.120.346U 6.17 101 6.27 6.36 101 55-110 3.10 (< 30 )
di-n-Octylphthalate 6.120.693U 6.33 103 6.27 6.72 107 40-130 6.10 (< 30 )
Dibenzo[a,h]anthracene 6.120.346U 5.10 83 6.27 5.23 83 40-125 2.40 (< 30 )
Dibenzofuran 6.120.346U 5.64 92 6.27 5.82 93 50-105 3.10 (< 30 )
Diethylphthalate 6.120.346U 6.26 102 6.27 6.38 102 50-115 2.10 (< 30 )
Dimethylphthalate 6.120.346U 6.17 101 6.27 6.38 102 50-110 3.20 (< 30 )
Fluoranthene 6.120.346U 5.95 97 6.27 6.20 99 55-115 4.20 (< 30 )
Fluorene 6.120.346U 5.51 90 6.27 5.79 92 50-110 5.10 (< 30 )
Hexachlorobenzene 6.120.346U 5.78 94 6.27 6.16 98 45-120 6.40 (< 30 )
Hexachlorobutadiene 6.120.346U 4.86 79 6.27 4.80 77 40-115 1.10 (< 30 )
Hexachlorocyclopentadiene 6.120.970U 4.42 72 6.27 4.41 70 48-108 0.35 (< 30 )
Hexachloroethane 6.120.346U 4.34 71 6.27 4.05 65 35-110 6.60 (< 30 )
Indeno[1,2,3-c,d] pyrene 6.120.346U 5.11 84 6.27 5.17 82 40-120 1.20 (< 30 )
Isophorone 6.120.346U 5.27 86 6.27 5.61 89 45-110 6.20 (< 30 )
N-Nitroso-di-n-propylamine 6.120.346U 5.35 88 6.27 5.49 88 40-115 2.70 (< 30 )
N-Nitrosodimethylamine 6.120.346U 4.90 80 6.27 4.63 74 20-115 5.80 (< 30 )
N-Nitrosodiphenylamine 6.120.346U 5.08 83 6.27 5.21 83 50-115 2.50 (< 30 )
Naphthalene 6.120.346U 4.72 77 6.27 4.70 75 40-105 0.14 (< 30 )
Nitrobenzene 6.120.346U 5.04 83 6.27 5.18 83 40-115 2.90 (< 30 )
Pentachlorophenol 8.562.77U 7.98 93 8.79 8.66 99 25-120 8.00 (< 30 )
Phenanthrene 6.120.346U 6.03 99 6.27 6.21 99 50-110 3.00 (< 30 )
Phenol 6.120.346U 4.82 79 6.27 4.83 77 40-100 0.41 (< 30 )
Pyrene 6.120.346U 5.82 95 6.27 6.30 100 45-125 8.00 (< 30 )
Surrogates
2,4,6-Tribromophenol 12.2 11.3 92 12.5 11.8 94 35-125 4.70
2-Fluorobiphenyl 6.12 4.80 79 6.27 5.11 81 45-105 6.00
Print Date: 06/18/2013 11:17:08AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C117
Original Sample ID: 1132031006
MS Sample ID: 1150324 MS
MSD Sample ID: 1150325 MSD
Analysis Date:
Analysis Date: 06/03/2013 20:04
Analysis Date: 06/03/2013 20:21
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132031001, 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008,
1132031009, 1132031010, 1132031011, 1132031012, 1132031013
Matrix Spike Summary
RPD CL
2-Fluorophenol 12.2 8.53 70 12.5 7.99 64 35-105 6.60
Nitrobenzene-d5 6.12 4.79 78 6.27 4.92 78 35-100 2.40
Phenol-d6 12.2 9.32 76 12.5 9.36 75 40-100 0.39
Terphenyl-d14 6.12 5.86 96 6.27 6.34 101 30-125 7.90
Batch Information
Prep Batch: XXX29074
Prep Method: Sonication Extraction Soil SW8270
Prep Date/Time: 5/30/2013 11:00:00AM
Prep Initial Wt./Vol.: 23.11g
Prep Extract Vol: 1.00mL
Analytical Batch: XMS7348
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Analytical Date/Time: 6/3/2013 8:04:00PM
Print Date: 06/18/2013 11:17:08AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C118
Blank ID: MB for HBN 1452170 [XXX/29075]
Blank Lab ID: 1150389
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011
Matrix: Soil/Solid (dry weight)
Results by AK102
DL UnitsLOQ/CLResultsParameter
Method Blank
Diesel Range Organics 20.0 mg/Kg6.2012.4U
Surrogates
5a Androstane 60-120 %83.5
Batch Information
Analytical Batch: XFC10912
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/4/2013 11:24:00AM
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 5/30/2013 1:30:00PM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/18/2013 11:17:08AM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C119
Blank Spike ID: LCS for HBN 1132031 [XXX29075]
Blank Spike Lab ID: 1150390
Date Analyzed: 06/04/2013 11:33
Spike Duplicate ID: LCSD for HBN 1132031
[XXX29075]
Spike Duplicate Lab ID: 1150391
Results by AK102
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011
Result
Diesel Range Organics 167 92 167 134 81 ( 75-125 ) (< 20 ) 13.50154
Surrogates
5a Androstane 3.33 104 3.33 88 88 ( 60-120 ) 17.20104
Batch Information
Analytical Batch: XFC10912
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/2013 13:30
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/18/2013 11:17:09AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C120
Blank ID: MB for HBN 1452170 [XXX/29075]
Blank Lab ID: 1150389
QC for Samples:
1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009, 1132031010, 1132031011
Matrix: Soil/Solid (dry weight)
Results by AK103
DL UnitsLOQ/CLResultsParameter
Method Blank
Residual Range Organics 20.0 mg/Kg6.2012.4U
Surrogates
n-Triacontane-d62 60-120 %87.1
Batch Information
Analytical Batch: XFC10912
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/4/2013 11:24:00AM
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 5/30/2013 1:30:00PM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/18/2013 11:17:10AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C121
Blank Spike ID: LCS for HBN 1132031 [XXX29075]
Blank Spike Lab ID: 1150390
Date Analyzed: 06/04/2013 11:33
Spike Duplicate ID: LCSD for HBN 1132031
[XXX29075]
Spike Duplicate Lab ID: 1150391
Results by AK103
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132031003, 1132031004, 1132031005, 1132031006, 1132031007, 1132031008, 1132031009,
1132031010, 1132031011
Result
Residual Range Organics 167 107 167 156 94 ( 60-120 ) (< 20 ) 13.80179
Surrogates
n-Triacontane-d62 3.33 111 3.33 93.4 93 ( 60-120 ) 17.60111
Batch Information
Analytical Batch: XFC10912
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29075
Prep Method: SW3550C
Prep Date/Time: 05/30/2013 13:30
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/18/2013 11:17:10AM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C122
C123
C124
C125
ADDRESS 1317 S. 13th Avenue, Kelso, WA 98626 USA PHONE +1 360 577 7222 FAX +1 360 636 1068
ALS Group USA, Corp. Part of the ALS Group An ALS Limited Company
June 17, 2013 Analytical Report for Service Request No: K1305064 Julie Shumway SGS Environmental Services, Inc. 200 West Potter Drive Anchorage, AK 99518 RE: 1132031 Dear Julie: Enclosed are the results of the samples submitted to our laboratory on May 30, 2013. For your reference, these analyses have been assigned our service request number K1305064. Analyses were performed according to our laboratory’s NELAP-approved quality assurance program. The test results meet requirements of the current NELAP standards, where applicable, and except as noted in the laboratory case narrative provided. For a specific list of NELAP-accredited analytes, refer to the certifications section at www.alsglobal.com. All results are intended to be considered in their entirety, and ALS Group USA Corp. dba ALS Environmental (ALS) is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report. Please call if you have any questions. My extension is 3364. You may also contact me via Email at [email protected].
Respectfully submitted, ALS Group USA Corp. dba ALS Environmental Howard Holmes Project Manager HH/ln Page 1 of _______
C126
Acronyms ASTM American Society for Testing and Materials A2LA American Association for Laboratory Accreditation CARB California Air Resources Board CAS Number Chemical Abstract Service registry Number CFC Chlorofluorocarbon CFU Colony-Forming Unit DEC Department of Environmental Conservation DEQ Department of Environmental Quality DHS Department of Health Services DOE Department of Ecology DOH Department of Health EPA U. S. Environmental Protection Agency ELAP Environmental Laboratory Accreditation Program GC Gas Chromatography GC/MS Gas Chromatography/Mass Spectrometry LOD Limit of Detection LOQ Limit of Quantitation LUFT Leaking Underground Fuel Tank M Modified MCL Maximum Contaminant Level is the highest permissible concentration of a substance
allowed in drinking water as established by the USEPA. MDL Method Detection Limit MPN Most Probable Number MRL Method Reporting Limit NA Not Applicable NC Not Calculated NCASI National Council of the Paper Industry for Air and Stream Improvement ND Not Detected NIOSH National Institute for Occupational Safety and Health PQL Practical Quantitation Limit RCRA Resource Conservation and Recovery Act SIM Selected Ion Monitoring TPH Total Petroleum Hydrocarbons tr Trace level is the concentration of an analyte that is less than the PQL but greater
than or equal to the MDL.
C127
Inorganic Data Qualifiers* The result is an outlier. See case narrative.
# The control limit criteria is not applicable. See case narrative.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
E The result is an estimate amount because the value exceeded the instrument calibration range.
J The result is an estimated value.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
H The holding time for this test is immediately following sample collection. The samples were analyzed as soon as possible afterreceipt by the laboratory.
Metals Data Qualifiers# The control limit criteria is not applicable. See case narrative.
J The result is an estimated value.
E The percent difference for the serial dilution was greater than 10%, indicating a possible matrix interference in the sample.
M The duplicate injection precision was not met.
N The Matrix Spike sample recovery is not within control limits. See case narrative.
S The reported value was determined by the Method of Standard Additions (MSA).
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
W The post-digestion spike for furnace AA analysis is out of control limits, while sample absorbance is less than 50% of spike absorbance.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
+ The correlation coefficient for the MSA is less than 0.995.
Q See case narrative. One or more quality control criteria was outside the limits.
Organic Data Qualifiers* The result is an outlier. See case narrative.
# The control limit criteria is not applicable. See case narrative.
A A tentatively identified compound, a suspected aldol-condensation product.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
C The analyte was qualitatively confirmed using GC/MS techniques, pattern recognition, or by comparing to historical data.
D The reported result is from a dilution.
E The result is an estimated value.
J The result is an estimated value.
N The result is presumptive. The analyte was tentatively identified, but a confirmation analysis was not performed.
P The GC or HPLC confirmation criteria was exceeded. The relative percent difference is greater than 40% between the two analytical results.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a chromatographic interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
Additional Petroleum Hydrocarbon Specific QualifiersF The chromatographic fingerprint of the sample matches the elution pattern of the calibration standard.
L The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of lighter molecular weight constituents than the calibration standard.
H The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of heavier molecular weight constituents than the calibration standard.
O The chromatographic fingerprint of the sample resembles an oil, but does not match the calibration standard.Y The chromatographic fingerprint of the sample resembles a petroleum product eluting in approximately the correct carbon range,
but the elution pattern does not match the calibration standard.
Z The chromatographic fingerprint does not resemble a petroleum product.
C128
Agency Web Site Number
Alaska DEC UST http://dec.alaska.gov/applications/eh/ehllabreports/USTLabs.aspx UST-040
Arizona DHS http://www.azdhs.gov/lab/license/env.htm AZ0339
Arkansas - DEQ http://www.adeq.state.ar.us/techsvs/labcert.htm 88-0637
California DHS (ELAP) http://www.cdph.ca.gov/certlic/labs/Pages/ELAP.aspx 2286
DOD ELAP http://www.denix.osd.mil/edqw/Accreditation/AccreditedLabs.cfm L12-28
Florida DOH http://www.doh.state.fl.us/lab/EnvLabCert/WaterCert.htm E87412
Georgia DNR http://www.gaepd.org/Documents/techguide_pcb.html#cel 881
Hawaii DOH Not available -
Idaho DHWhttp://www.healthandwelfare.idaho.gov/Health/Labs/CertificationDrinkingWaterLabs/tabid/1833/Default.aspx -
Indiana DOH http://www.in.gov/isdh/24859.htm C-WA-01
ISO 17025 http://www.pjlabs.com/ L12-27
Louisiana DEQhttp://www.deq.louisiana.gov/portal/DIVISIONS/PublicParticipationandPermitSupport/LouisianaLaboratoryAccreditationProgram.aspx 3016
Louisiana DHH Not available LA110003
Maine DHS Not available WA0035
Michigan DEQ http://www.michigan.gov/deq/0,1607,7-135-3307_4131_4156---,00.html 9949
Minnesota DOH http://www.health.state.mn.us/accreditation 053-999-368
Montana DPHHS http://www.dphhs.mt.gov/publichealth/ CERT0047
Nevada DEP http://ndep.nv.gov/bsdw/labservice.htm WA35
New Jersey DEP http://www.nj.gov/dep/oqa/ WA005
New Mexico ED http://www.nmenv.state.nm.us/dwb/Index.htm -
North Carolina DWQ http://www.dwqlab.org/ 605
Oklahoma DEQ http://www.deq.state.ok.us/CSDnew/labcert.htm 9801
Oregon – DEQ (NELAP)http://public.health.oregon.gov/LaboratoryServices/EnvironmentalLaboratoryAccreditation/Pages/index.aspx WA200001
South Carolina DHEC http://www.scdhec.gov/environment/envserv/ 61002
Texas CEQ http://www.tceq.texas.gov/field/qa/env_lab_accreditation.html 4704427-08-TX
Washington DOE http://www.ecy.wa.gov/programs/eap/labs/lab-accreditation.html C1203
Wisconsin DNR http://dnr.wi.gov/ 998386840
Wyoming (EPA Region 8) http://www.epa.gov/region8/water/dwhome/wyomingdi.html -
Kelso Laboratory Website www.caslab.com NA
Columbia Analytical Services, Inc. dba ALS Environmental (ALS) - KelsoState Certifications, Accreditations, and Licenses
Analyses were performed according to our laboratory’s NELAP-approved quality assurance program. A complete listing of specific NELAP-certified analytes, can be found in the certification section at www.caslab.com or at the accreditation bodies web sitePlease refer to the certification and/or accreditation body's web site if samples are submitted for compliance purposes. The states highlighted above, require the analysis be listed on the state certification if used for compliance purposes and if the method/anlayte is offered by that state.
C129
1.JUENT: SGS-AK
CONTACT: Julie Shumway PHONE NO:
America Inc,
CHAIN OF CUSTODY RECORD
SGS Reference:
Additional Comments:
(907) 562-2343
ALS Kelso
Locations Nationwide
Alaska
New Jersey
North Carolina
West Virgina
Maryland
New York
Indiana
Kentucky WWW us SQS com
Page
PROJECT "'U"""v # Preservl :3 ) L/ 1132031 PWSIDI ative "-=-/ '$7~ NAME: PERMIT#: C Used: ~o
REPORTS TO: Julie Shumway E-MAIL: Julie,Shumway@sgs,com 0 TYPE
N c= a;-T COMP 00 A G= ...
~
INVOICE TO: QUOTE#: ( GRAB '" I I I I I N Multi c I 1 P.O.#: 1132031 2
2(RESERVEO E Incre~ x:
SAMPLE IDENTIFICATION DATE TIME MATRIXI R mental i='
for lab use mm/ddlvv HH:MM MATRIX s Soils III MS MSD SGS lab# LoclD REMARKS I-
SMIC-R-(O) 05124/13 734 S 1 GRAB x 1132031001
SMIC-T-(O) 05/24/13 753 S 1 GRAB x 1132031002
SMIC-F-(O) 05124113 1258 S 1 GRAB )( 1132031003
SMIC-F-(4.5) 05/24/13 1344 S 1 GRAB x 1132031004
SMIC-E-(O) 05/25/13 2011 S 1 GRAB x 1132031006
SMIC-E-(5) 05/25/13 2107 S 1 GRAB x 1132031007
SMIC-E-(10) 05/25/13 2214 S 1 GRAB x 1132031008
SMIC-E-(5)D 05/25113 2110 S 1 GRAB x 1132031009
SMIC-S-(Ol 05/26/13 1315 S 1 GRAB x 1132031010
SMIC-(O)D f} 05/26/13 1318 S 1 GRAB x 1132031011
5~el!~!!J~-n ~y~~lp~,l~ Date Time Received By: ~~DOD Project? YES Data Deliverable Requirements:
/7;J'/t« 05/29/13 loe4fy L'Ely~1 n l'~ort'+ csv Excel EDD Cooler ID:
,R~!illquished Byf (2) LJ Date Time I Received By: Requested Turnaround Time and-or special instructions: I Relinquished By: (3) Date Time Received By:
Temp Blank ·C: Chain of Custody Seal: (Circle)
IRelinquished By: (4) Date Time Received for Laboratory By: INTACT BROKEN ABSENT
16"; or Ambient [ 1
(See attached Sample Receipt fOf/fl) (See attached Sample Receipt forml ~
1 200 W. Potter Drive Anchorage, AK 995111 Tel: (S07) 562-2343 Fax: (907)561-5301 http://www.sgs.comltermsandcomiitions.htm
1 5500 Business Drive Wilmington, !IIC 28405 Tel: (910)350-1903 Fax: (9101350-1551
1132031 TBTl
C130
locations Nationwide
North America Inc. Alaska Maryland
CHAIN OF CUSTODY RECORD New Jersey
North Carolina
West Virgina
New York
Indiana
Kentucky www us sos com
'1~lIENT: SGS-AK SGS Reference: AlS Kelso
Additional Comments: Page PHONE NO:
CONTACT: Julie Shumway (907) 562-2343 UJE:ul # PROJECT 1132031 PWSIDI
NAME: PERMIT#: C
REPORTS TO: Julie Shumway E-MAil: [email protected] 0 N T A
INVOICE TO: QUOTE#: I
'1 P.O.#.: 1132031 N E
2r'RESERVED SAMPLE IDENTIFICATION
DATE TIME MATRIX! R
for lab use mm/dd/vv HH:MM MATRIX s SMIC-P-(O) 05/26113 1652 S 1
SMIC-Q-(O) 05126113 1402 S 1
I
"- FO
&'tf! Date Time Received By: 05129/13
O~ 't~~~ished By/(2) 6 Date Time Received By:
Relinquished By: (3) Date Time Received By:
Relinquished By: (4) Date Time Received for
I~I I "C6\._~, .A
fJ ] 200 W. Potter Drive Anchorage, AI< 99518 Tei: (9071562-2343 Fax: (907) 561-5301
5500 Business Drive Wilmington, !lie 28405 Tei: (910) 350-1903 Fax: (910) 350-1557
I Preserv~ atlve $;>'1(.;
Used: ~a // 1 TYPE
I c= m COMP IX)
G= '" I I I ... GRAB ., I I I I I I I
'" I Multi e Incre- :.::
mental i=' Soils III MS MSD SGS lab# loclD REMARKS I-
GRAB x 1132031012
GRAB x 1132031013
~~OD Project? YES Data Deliverable Requirements:
l.eyeUI.rElPort '" csv Excel EDD Cooler 10:
Requested Turnaround Time and-or Special Instructions:
Temp BlanK Chain of Custody Seal: (Circle)
'1 By: or Ambient [ J INTACT BROKEN ABSENT - ItSee attached Sample (See attached Sampie Receipt Form)
hrtp:llwww.sgs.com/terms and cOl1ditiol1s.htrn
1132031 TBTL
C131
PC .
Cooler Receipt and J~reservation F'orm
Client / Service Request K13
Opened: 5 I SCI' 3 By: -'---"-__ Unloaded: 5/10 II .:?I By: ~'-r
1. Samples were received via? Mail Fed Ex @ DHL PDX Courier Hand Delivered
2. Samples were received in: (circle) CBJ Box Envelope Other ______ --,-____ _
3. Were custody seals on coolers? NA If yes, how many and
If present, were custody seals intact?
N
N If present, were they signed and dated?
Raw Cooler/COC ID
4. Packing material: Inserts Baggies B~ap ~ks Wet lee Dry Ice Sleeves
5. Were custody papers properly filled out (ink, signed, etc.)?
6. Did all bottles arrive in good condition (unbroken)? Indicate in the table below.
7. Were all sample labels complete (i.e analysis, preservation, etc.)?
8. Did all sample labels and tags agree with custody papers? Indicate major discrepancies in the table on page 2.
9. Were appropriate bottles/containers and volumes received for the tests indicated?
10. Were the pH-preserved bottles (see SMO GEN SOP) received at the appropriate pH? Indicate in the table below
11. Were VOA vials received without headspace? Indicate in the table below.
12. Was C12IRes negative?
I F-... ~.mpl' ID 00 BottJ! Sampl.,D on CDC Identified by:
,--I Bottle Count Out of Head- Volume Reagent Lot I I Sample 10 Bottle Type Temp space Broke pH Reagent added Number
-
--
-Notes, Discrepancies, & Resolutions:
NA
NA
NA
NA
NA
y
y
y
Initials
N
Filed
N
N
N
N
N
N
N
Time
Page __ ().f~ __ C132
ALS Group USA, Corp. dba ALS Environmental
Sample Name
Date
Collected
Date
Received
Date
AnalyzedLab Code Result
Result Notes
Test Notes:
Analysis Method: Basis: 160.3M Wet
Prep Method: Units: NONE PERCENT
Total Solids
Sample Matrix: Soil
Project: 1132031
Service Request: Client: SGS Environmental Services, Inc. K1305064
Analytical Results
K1305064-001 86.506/06/201305/24/2013 05/30/2013SMIC-R-(0)
K1305064-002 93.606/06/201305/24/2013 05/30/2013SMIC-T-(0)
K1305064-003 87.306/06/201305/24/2013 05/30/2013SMIC-F-(0)
K1305064-004 82.906/06/201305/24/2013 05/30/2013SMIC-F-(4.5)
K1305064-005 68.606/06/201305/25/2013 05/30/2013SMIC-E-(0)
K1305064-006 87.606/06/201305/25/2013 05/30/2013SMIC-E-(5)
K1305064-007 93.006/06/201305/25/2013 05/30/2013SMIC-E-(10)
K1305064-008 88.106/06/201305/25/2013 05/30/2013SMIC-E-(5)D
K1305064-009 62.506/06/201305/26/2013 05/30/2013SMIC-S-(0)
K1305064-010 62.506/06/201305/26/2013 05/30/2013SMIC-(0)D
K1305064-011 68.806/06/201305/26/2013 05/30/2013SMIC-P-(0)
K1305064-012 78.806/06/201305/26/2013 05/30/2013SMIC-Q-(0)
SuperSet Reference: W1305486
Printed: 06/14/2013 08:34 1of1Page
u:\Stealth\Crystal.rpt\Solids.rpt
C133
ALS Group USA, Corp. dba ALS Environmental
QA/QC Report
Service Request:
Date Collected:
Date Received:
Date Analyzed:
05/24/2013
05/30/2013
06/06/2013
Client:
Project:
Sample Matrix:
1132031
Soil
Total Solids
Duplicate Sample Summary
Prep Method:
Analysis Method:
Test Notes:
NONE
160.3M
PERCENT
Wet
Units:
Basis:
Sample Name Lab Code
Result NotesSample
Result
Duplicate
Sample
Result Average
Relative
Percent
Difference
SGS Environmental Services, Inc. K1305064
88.486.5 87.5 2SMIC-R-(0) K1305064-001
SuperSet Reference: W1305486
Printed: 06/14/2013 08:34 2of1Page
u:\Stealth\Crystal.rpt\Solids.rpt
C134
ALS Group USA, Corp. dba ALS Environmental
QA/QC Report
Service Request:
Date Collected:
Date Received:
Date Analyzed:
05/26/2013
05/30/2013
06/06/2013
Client:
Project:
Sample Matrix:
1132031
Soil
Total Solids
Duplicate Sample Summary
Prep Method:
Analysis Method:
Test Notes:
NONE
160.3M
PERCENT
Wet
Units:
Basis:
Sample Name Lab Code
Result NotesSample
Result
Duplicate
Sample
Result Average
Relative
Percent
Difference
SGS Environmental Services, Inc. K1305064
71.868.8 70.3 4SMIC-P-(0) K1305064-011
SuperSet Reference: W1305486
Printed: 06/14/2013 08:34 2of2Page
u:\Stealth\Crystal.rpt\Solids.rpt
C135
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-001
ug/Kg
Dry
SMIC-R-(0)
05/24/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.2 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1385
Comments:
1of1Page20:07:0006/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C136
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-002
ug/Kg
Dry
SMIC-T-(0)
05/24/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1378
Comments:
1of1Page20:07:0406/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C137
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-003
ug/Kg
Dry
SMIC-F-(0)
05/24/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.2 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1381
Comments:
1of1Page20:07:0706/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C138
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-004
ug/Kg
Dry
SMIC-F-(4.5)
05/24/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.2 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1381
Comments:
1of1Page20:07:1006/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C139
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-005
ug/Kg
Dry
SMIC-E-(0)
05/25/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.5 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1385
Comments:
1of1Page20:07:1306/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C140
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-006
ug/Kg
Dry
SMIC-E-(5)
05/25/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.2 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1369
Comments:
1of1Page20:07:1606/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C141
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-007
ug/Kg
Dry
SMIC-E-(10)
05/25/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1358
Comments:
1of1Page20:07:1906/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C142
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-008
ug/Kg
Dry
SMIC-E-(5)D
05/25/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.2 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1380
Comments:
1of1Page20:07:2206/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C143
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-009
ug/Kg
Dry
SMIC-S-(0)
05/26/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.6 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1379
Comments:
1of1Page20:07:2506/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C144
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-010
ug/Kg
Dry
SMIC-(0)D
05/26/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.6 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1371
Comments:
1of1Page20:07:2806/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C145
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-011
ug/Kg
Dry
SMIC-P-(0)
05/26/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.5 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1387
Comments:
1of1Page20:07:3106/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C146
Analytical Results
SGS Environmental Services, Inc. K1305064
K1305064-012
ug/Kg
Dry
SMIC-Q-(0)
05/26/2013
05/30/2013
1132031
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.3 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1377
Comments:
1of1Page20:07:3406/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C147
Analytical Results
SGS Environmental Services, Inc. K1305064
KWG1305527-4
ug/Kg
Dry
Method Blank
NA
NA
1132031
Sediment
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
0.98 06/04/131 KWG130552706/10/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/10/1361
Comments:
1of1Page20:07:3706/12/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR155906u:\Stealth\Crystal.rpt\Form1mNew.rpt
C148
ALS Group USA, Corp. dba ALS Environmental
Extraction Method:
QA/QC Report
Surrogate Recovery Summary
SGS Environmental Services, Inc. K1305064
Low
Sediment
1132031
Client:
Project:
Sample Matrix:
Service Request:
Units:
Level:
Sample Name Lab Code
Butyltins (as cation)
Method
Analysis Method: Krone
Sur1
Percent
K1305034-001Batch QC 93
K1305064-001SMIC-R-(0) 85
K1305064-002SMIC-T-(0) 78
K1305064-003SMIC-F-(0) 81
K1305064-004SMIC-F-(4.5) 81
K1305064-005SMIC-E-(0) 85
K1305064-006SMIC-E-(5) 69
K1305064-007SMIC-E-(10) 58
K1305064-008SMIC-E-(5)D 80
K1305064-009SMIC-S-(0) 79
K1305064-010SMIC-(0)D 71
K1305064-011SMIC-P-(0) 87
K1305064-012SMIC-Q-(0) 77
KWG1305527-4Method Blank 61
KWG1305527-1Batch QCMS 97
KWG1305527-2Batch QCDMS 101
KWG1305527-3Lab Control Sample 83
Form 2A - OrganicPrinted: 06/12/2013 20:07:41 1 of 1
Surrogate Recovery Control Limits (%)
10-120Tri-n-propyltin
Results flagged with an asterisk (*) indicate values outside control criteria.
Page
Results flagged with a pound (#) indicate the control criteria is not applicable.
RR155906SuperSet Reference:
Sur1 =
u:\Stealth\Crystal.rpt\Form2.rpt
C149
Matrix Spike/Duplicate Matrix Spike Summary
Sample
Result %Rec
Matrix Spike
%Rec
Limits
Duplicate Matrix Spike
%Rec RPD
RPD
Limit
QA/QC Report
SGS Environmental Services, Inc.
Batch QC
K1305034-001
Krone
K1305064
ug/Kg
Dry
Butyltins (as cation)
Sediment
Low
1132031
Client:
Project:
Sample Matrix:
Service Request:
Sample Name:
Lab Code:
Extraction Method:
Analysis Method:
Units:
Basis:
Level:
Extraction Lot:
Analyte Name Result Result
ALS Group USA, Corp. dba ALS Environmental
Date Extracted:
Date Analyzed:
06/04/2013
06/10/2013
Method
KWG1305527
KWG1305527-2KWG1305527-1
Batch QCMS Batch QCDMS
Spike
Amount
Spike
Amount
10-115ND 22.0 68Tri-n-butyltin Cation 22.0 83 401918.2 15.0
Form 3A - OrganicPrinted: 06/12/2013 20:07:45 Page 1 of 1
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
RR155906SuperSet Reference:
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
u:\Stealth\Crystal.rpt\Form3DMS.rpt
C150
Lab Control Spike Summary
%Rec
Lab Control Spike
%Rec
Limits
QA/QC Report
SGS Environmental Services, Inc. K1305064
Krone
ug/Kg
Dry
Lab Control Sample
KWG1305527-3
Butyltins (as cation)
KWG1305527
Sediment
Low
1132031
Client:
Project:
Sample Matrix:
Service Request:
Units:
Basis:
Level:
Extraction Lot:
Analyte Name Result
Extraction Method:
Analysis Method:
ALS Group USA, Corp. dba ALS Environmental
Date Extracted:
Date Analyzed: 06/10/2013
06/04/2013
Method
Spike
Amount
10-122Tri-n-butyltin Cation 22.2 5111.3
Form 3C - OrganicPrinted: 06/12/2013 20:07:48 Page 1 of 1
Results flagged with an asterisk (*) indicate values outside control criteria.
RR155906SuperSet Reference:
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
u:\Stealth\Crystal.rpt\Form3LCS.rpt
C151
Page 1 of 7Version 2.7 01/10
Laboratory Data Review Checklist
Completed by: Kristi McLean
Title: Environmental Specialist Date: 24 July 2013
CS Report Name: SMIC Improvements 1770.01 Report Date: 19 June 2013
Consultant Firm: R&M Consultants, Inc.
Laboratory Name: SGS North America, Inc. Laboratory Report Number: 1132031
ADEC File Number: NA ADEC RecKey Number: NA
1. Laboratory
a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample analyses?
Comments:Yes No NA (Please explain.)
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS approved?
Comments:
Columbia Analytical Services, Inc. dba ALS Environmental is certified by the State of Alaska
NA (Please explain)Yes No
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)?
Comments:NA (Please explain)Yes No
b. Correct analyses requested? Comments:NA (Please explain)Yes No
3. Laboratory Sample Receipt Documentation
a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Comments:NA (Please explain)Yes No
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Page 2 of 7Version 2.7 01/10
b. Sample preservation acceptable - acidified waters, Methanol preserved VOC soil (GRO, BTEX, Volatile Chlorinated Solvents, etc.)?
Comments:NA (Please explain)Yes No
c. Sample condition documented - broken, leaking (Methanol), zero headspace (VOC vials)?
Comments:
All samples were received in good condition
NA (Please explain)Yes No
d. If there were any discrepancies, were they documented? - For example, incorrect sample containers/preservation, sample temperature outside of acceptance range, insufficient or missing samples, etc.?
Comments:
No discrepancies were documented.
NA (Please explain)Yes No
e. Data quality or usability affected? (Please explain)
Comments:
NA
a. Present and understandable?
4. Case Narrative
Comments:NA (Please explain)Yes No
b. Discrepancies, errors or QC failures identified by the lab?
Comments:NA (Please explain)Yes No
c. Were all corrective actions documented? Comments:
No corrective actions were identified.
NA (Please explain)Yes No
d. What is the effect on data quality/usability according to the case narrative? Comments:
NA
C153
Page 3 of 7Version 2.7 01/10
a. Correct analyses performed/reported as requested on COC?
5. Samples Results
Comments:NA (Please explain)Yes No
b. All applicable holding times met?
Comments:NA (Please explain)Yes No
c. All soils reported on a dry weight basis?
Comments:NA (Please explain)Yes No
Comments:
d. Are the reported PQLs less than the Cleanup Level or the minimum required detection level for the project?
NA (Please explain)Yes No
e. Data quality or usability affected? (Please explain) Comments:
Sample handling and results did not result in an issue that would have affected data quality or usability.
a. Method Blank6. QC Samples
i. One method blank reported per matrix, analysis and 20 samples?
Comments:NA (Please explain)Yes No
ii. All method blank results less than PQL? Comments:NA (Please explain)Yes No
iii. If above PQL, what samples are affected? Comments:
NA
C154
Page 4 of 7Version 2.7 01/10
iv. Do the affected sample(s) have data flags? If so, are the data flags clearly defined? Comments:
No samples were affected
NA (Please explain)Yes No
v. Data quality or usability affected? (Please explain) Comments:
No samples were affected; data quality and usability was not compromised.
i. Organics - One LCS/LCSD reported per matrix, analysis and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846)
Comments:
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
Yes No NA (Please explain)
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples?
Comments:NA (Please explain)Yes No
iii. Accuracy - All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK Petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages)
Comments:
LCS recovery for demethylphthalate, di-n-butyphthalate, and chrysene is outside of QC criteria in one sample.
NA (Please explain)Yes No
iv. Precision - All relative percent differences (RPD) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/DMSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages)
Comments:NA (Please explain)Yes No
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments:
No samples were affected.
C155
Page 5 of 7Version 2.7 01/10
vi. Do the affected samples(s) have data flags? If so, are the data flags clearly defined?
Comments:
The samples were not affected and therefore not flagged.
NA (Please explain)Yes No
vii. Data quality or usability affected? (Please explain) Comments:
QC criteria was biased high and the identified analytes were not detected in the associated samples.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses - field, QC and laboratory samples?
Comments:NA (Please explain)Yes No
ii. Accuracy - All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages)
Comments:NA (Please explain)NoYes
iii. Do the sample results with failed surrogate recoveries have data flags? If so, are the data flags clearly defined?
Comments:
No samples had failed surrogate recoveries
NA (Please explain)Yes No
iv. Data quality or usability affected? (Use the comment box to explain.). Comments:
NA, see above
d. Trip Blank - Volatile analyses only (GRO, BTEX, Volatile Chlorinated Solvents, etc.): Water and Soil
i. One trip blank reported per matrix, analysis and for each cooler containing volatile samples? (If not, enter explanation below.)
Comments:Yes No NA (Please explain.)
ii. Is the cooler used to transport the trip blank and VOA samples clearly indicated on the COC? (If not, a comment explaining why must be entered below)
Comments:
Only one cooler with samples and trip blank was submitted to the lab.
Yes No NA (Please explain.)
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Page 6 of 7Version 2.7 01/10
iii. All results less than PQL?
Comments:Yes No NA (Please explain.)
Comments:
NA
iv. If above PQL, what samples are affected?
v. Data quality or usability affected? (Please explain.)
Comments:
NA
e. Field Duplicatei. One field duplicate submitted per matrix, analysis and 10 project samples?
Comments:NA (Please explain)NoYes
ii. Submitted blind to lab?
Comments:Yes No NA (Please explain.)
iii. Precision - All relative percent differences (RPD) less than specified DQOs? (Recommended: 30% water, 50% soil) RPD (%) = Absolute Value of: (R1- R2) x 100 ((R1+ R2)/2) Where R1 = Sample Concentration R2 = Field Duplicate Concentration
Comments:
The RPD for sample SMIC-S(0) was 200% for silver; it was not detected in the duplicate sample.
NA (Please explain)Yes No
iv. Data quality or usability affected? (Use the comment box to explain why or why not.) Comments:
There is often discrepancies with grab samples.
Yes No NA (Please explain)
C157
Page 7 of 7Version 2.7 01/10
Comments:
No decontamination sample was submitted to the lab.
f. Decontamination or Equipment Blank (if applicable)
i. All results less than PQL?
Comments:NA (Please explain)NoYes
NA (Please explain)Yes No
ii. If above PQL, what samples are affected? Comments:
NA
iii. Data quality or usability affected? (Please explain.) Comments:
NA
a. Defined and appropriate?
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab Specific, etc.)
Comments:
No data flags/qualifiers were associated with the samples.
Yes No NA (Please explain)
Reset Form
C158
Report Number: 1132110
Client Project: SMIC Improvements 1770.01
Laboratory Report of Analysis
Dear Kevin Pendergast,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. All results are
intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any
samples submitted to our laboratory will be retained for a maximum of fourteen (14) days from the date of this
report unless other archiving requirements were included in the quote.
If there are any questions about the report or services performed during this project, please call Steve at (907)
562-2343. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America Inc.
__________________________________________________________________
Steve Crupi Date
Project [email protected]
To: R & M Consultants Inc
9101 Vanguard Dr
Anchorage, AK 99507
(907)522-1707
Print Date: 06/27/2013 5:39:04PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C159
Case Narrative
SGS Client: R & M Consultants Inc
SGS Project: 1132110
Project Name/Site: SMIC Improvements 1770.01
Project Contact: Kevin Pendergast
Refer to sample receipt form for information on sample condition.
SMIC-K (0) (1132110001) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
8270D - Surrogate (terphenyl-d14) recovery is outside of QC criteria (biased high). No analytes were detected above
the LOQ in the sample.
AK103 - Unknown hydrocarbon with several peaks is present.
SMIC-K (1.5) (1132110002) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
8270D - Surrogate (terphenyl-d14) recovery is outside of QC criteria (biased high). No analytes were detected above
the LOQ in the sample.
SMIC-K (10) (1132110003) PS
8270D - Surrogate (terphenyl-d14) recovery is outside of QC criteria (biased high). No analytes were detected above
the LOQ in the sample.
SMIC-K (40) (1132110004) PS
8270D - Surrogate (terphenyl-d14) recovery is outside of QC criteria (biased high). No analytes were detected above
the LOQ in the sample.
SMIC-L (0) (1132110005) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK103 - Unknown hydrocarbon with several peaks is present.
SMIC-L (1.5) (1132110006) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
8260B - Sample surrogate recovery for 1,2-dichloroethane-D4 does not meet QC criteria (biased high). All analytes
associated with this surrogate were not detected above the LOQ.
SMIC-O (0) (1132110009) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
SMIC-O (0) D (1132110010) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
SMIC-O (1.5) (1132110011) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK103 - Unknown hydrocarbon with several peaks is present.
SMIC-M (0) (1132110014) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
SMIC-M (1.5) (1132110015) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
SMIC-M (1.5) D (1132110018) PS
Print Date: 06/27/2013 5:39:04PM
Member of SGS Group
SGS North America Inc.
200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C160
Case Narrative
SGS Client: R & M Consultants Inc
SGS Project: 1132110
Project Name/Site: SMIC Improvements 1770.01
Project Contact: Kevin Pendergast
Refer to sample receipt form for information on sample condition.
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
8260B - Sample surrogate recovery for 1,2-dichloroethane-D4 does not meet QC criteria (biased high). All analytes
associated with this surrogate were not detected above the LOQ.
AK102/103 - Unknown hydrocarbon with several peaks is present.
SMIC-N (0) (1132110019) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
SMIC-N (1.5) (1132110020) PS
Krone - Tributyl tin was analyzed by ALS of Kelso, WA.
AK102/103 - Unknown hydrocarbon with several peaks is present.
SMIC-N (30) (1132110022) PS
8260B - Sample surrogate recovery for 1,2-dichloroethane-D4 does not meet QC criteria (biased high). All analytes
associated with this surrogate were not detected above the LOQ.
CCV for HBN 1453192 (VMS/13531 (1151211) CCV
8260B - CCV recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected
above the LOQ in the associated samples.
CCV for HBN 1453194 (VMS/13532 (1151226) CCV
8260B - CCV recovery for 2-butanone (MEK) does not meet QC criteria (biased high). This analyte was not detected
above the LOQ in the associated samples.
LCS for HBN 1453077 [XXX/29091 (1150864) LCS
AK103 - LCS n-Triacontane (surrogate) recovery is outside QC criteria (biased high). Associated samples met criteria
for this surrogate.
MB for HBN 1453077 [XXX/29091] (1150863) MB
AK103 - MB n-Triacontane (surrogate) recovery is outside QC criteria (biased high). Associated samples met criteria for
this surrogate.
1132110006MS (1150931) MS
6020 - Metals - MS/MSD recoveries for chromium and barium were outside of acceptance criteria. Post digestion spike
was successful.
1131859001MS (1150937) MS
6020 - Metals - MS/MSD recoveries for chromium were outside of acceptance criteria. Post digestion spike was
successful.
1132110006MSD (1150932) MSD
6020 - Metals - MS/MSD recoveries for chromium and barium were outside of acceptance criteria. Post digestion spike
was successful.
1131859001MSD (1150938) MSD
6020 - Metals - MS/MSD recoveries for chromium were outside of acceptance criteria. Post digestion spike was
successful.
1132110020(1151214MSD) (1151216) MSD
Print Date: 06/27/2013 5:39:04PM
Member of SGS Group
SGS North America Inc.
200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C161
Case Narrative
SGS Client: R & M Consultants Inc
SGS Project: 1132110
Project Name/Site: SMIC Improvements 1770.01
Project Contact: Kevin Pendergast
Refer to sample receipt form for information on sample condition.
8260B - MS/MSD RPDs for several analytes does not meet QC criteria. These analytes were not detected above the
LOQ in the original sample.
8260B - Sample surrogate recovery for 1,2-dichloroethane-D4 does not meet QC criteria (biased high). All analytes
associated with this surrogate were not detected above the LOQ.
*QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
Print Date: 06/27/2013 5:39:04PM
Member of SGS Group
SGS North America Inc.
200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C162
Laboratory ID Client Sample ID Analytical Batch Analyte Reason
Report of Manual Integrations
SW8270D
LCS for HBN 1453106 [XXX/29094 XMS7354 1-Chloronaphthalene SP1150982
LCS for HBN 1453106 [XXX/29094 XMS7354 2-Chloronaphthalene SP1150982
1132110021MS XMS7354 1-Chloronaphthalene RP1150984
1132110021MSD XMS7354 1-Chloronaphthalene SP1150985
1132110021MSD XMS7354 2-Chloronaphthalene SP1150985
LCS for HBN 1453190 [XXX/29103 XMS7361 2-Chloronaphthalene BLC1151198
1132110020MS XMS7361 1-Chloronaphthalene RSP1151201
1132110020MS XMS7361 2-Chloronaphthalene RSP1151201
1132110020MSD XMS7361 1-Chloronaphthalene PNF1151202
1132110020MSD XMS7361 2-Chloronaphthalene BLC1151202
Manual Integration Reason Code Descriptions
Code Description
O Original Chromatogram
M Modified Chromatogram
SS Skimmed surrogate
BLG Closed baseline gap
RP Reassign peak name
PIR Pattern integration required
IT Included tail
SP Split peak
RSP Removed split peak
FPS Forced peak start/stop
BLC Baseline correction
PNF Peak not found by software
All DRO/RRO analysis are integrated per SOP.
Print Date: 06/27/2013 5:39:05PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C163
Laboratory Qualifiers
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their
entirety and SGS is not responsible for use of less than the complete report. If you have any questions regarding this
report, or if we can be of any other assistance, please contact your SGS Project Manager at 907-562-2343. All work is
provided under SGS general terms and conditions (<http://www.sgs.com/terms_and_conditions.htm>), unless other
written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan
(QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971
(DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and 2944.01 for DOD ELAP/ISO17025 (RCRA methods:
1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6020, 7470A, 7471B, 8021B, 8082A, 8260B, 8270D,
8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and
data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, other regulatory
authorities.
The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
IB Instrument Blank
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 06/27/2013 5:39:06PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C164
Sample Summary
Client Sample ID Lab Sample ID Collected Received Matrix
SMIC-K (0) 1132110001 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-K (1.5) 1132110002 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-K (10) 1132110003 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-K (40) 1132110004 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-L (0) 1132110005 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-L (1.5) 1132110006 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-L (15) 1132110007 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-L (35) 1132110008 05/30/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-O (0) 1132110009 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-O (0) D 1132110010 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-O (1.5) 1132110011 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-O (10) 1132110012 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-O (25) 1132110013 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-M (0) 1132110014 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-M (1.5) 1132110015 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-M (5) 1132110016 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-M (20) 1132110017 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-M (1.5) D 1132110018 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-N (0) 1132110019 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-N (1.5) 1132110020 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-N (10) 1132110021 05/31/2013 06/03/2013 Soil/Solid (dry weight)
SMIC-N (30) 1132110022 05/31/2013 06/03/2013 Soil/Solid (dry weight)
Trip Blank 1132110023 05/30/2013 06/03/2013 Soil/Solid (dry weight)
Method DescriptionMethod
Diesel/Residual Range OrganicsAK103
Diesel/Residual Range OrganicsAK102
Gasoline Range Organics (S)AK101
Percent Solids SM2540GSM21 2540G
RCRA Metals by ICP-MSSW6020
SW846 8270 Semi-Volatiles by GC/MS (S)SW8270D
VOC 8260 (S) Field ExtractedSW8260B
Print Date: 06/27/2013 5:39:06PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C165
Detectable Results Summary
Client Sample ID: SMIC-K (0)
Lab Sample ID: 1132110001 UnitsParameter Result
Arsenic mg/Kg4.31Metals by ICP/MS
Barium mg/Kg35.3
Chromium mg/Kg35.3
Lead mg/Kg5.87
Residual Range Organics mg/Kg65.2Semivolatile Organic Fuels
Client Sample ID: SMIC-K (1.5)
Lab Sample ID: 1132110002 UnitsParameter Result
Arsenic mg/Kg3.69Metals by ICP/MS
Barium mg/Kg29.5
Chromium mg/Kg31.3
Lead mg/Kg4.72
Client Sample ID: SMIC-K (10)
Lab Sample ID: 1132110003 UnitsParameter Result
Arsenic mg/Kg6.14Metals by ICP/MS
Barium mg/Kg50.1
Chromium mg/Kg37.2
Lead mg/Kg5.80
Client Sample ID: SMIC-K (40)
Lab Sample ID: 1132110004 UnitsParameter Result
Arsenic mg/Kg5.66Metals by ICP/MS
Barium mg/Kg46.2
Chromium mg/Kg32.5
Lead mg/Kg6.45
Client Sample ID: SMIC-L (0)
Lab Sample ID: 1132110005 UnitsParameter Result
Arsenic mg/Kg4.02Metals by ICP/MS
Barium mg/Kg37.4
Chromium mg/Kg31.9
Lead mg/Kg7.18
Diesel Range Organics mg/Kg45.1Semivolatile Organic Fuels
Residual Range Organics mg/Kg267
Client Sample ID: SMIC-L (1.5)
Lab Sample ID: 1132110006 UnitsParameter Result
Arsenic mg/Kg4.73Metals by ICP/MS
Barium mg/Kg33.0
Chromium mg/Kg47.1
Lead mg/Kg4.78
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C166
Detectable Results Summary
Client Sample ID: SMIC-L (15)
Lab Sample ID: 1132110007 UnitsParameter Result
Arsenic mg/Kg4.04Metals by ICP/MS
Barium mg/Kg40.7
Chromium mg/Kg34.8
Lead mg/Kg6.24
Client Sample ID: SMIC-L (35)
Lab Sample ID: 1132110008 UnitsParameter Result
Arsenic mg/Kg6.57Metals by ICP/MS
Barium mg/Kg46.2
Chromium mg/Kg35.3
Lead mg/Kg7.27
Client Sample ID: SMIC-O (0)
Lab Sample ID: 1132110009 UnitsParameter Result
Arsenic mg/Kg7.43Metals by ICP/MS
Barium mg/Kg28.7
Chromium mg/Kg41.3
Lead mg/Kg8.46
Mercury mg/Kg0.0745
Toluene ug/Kg68.0Volatile GC/MS
Client Sample ID: SMIC-O (0) D
Lab Sample ID: 1132110010 UnitsParameter Result
Arsenic mg/Kg7.46Metals by ICP/MS
Barium mg/Kg30.3
Chromium mg/Kg44.1
Lead mg/Kg8.33
Mercury mg/Kg0.0861
Toluene ug/Kg64.7Volatile GC/MS
Client Sample ID: SMIC-O (1.5)
Lab Sample ID: 1132110011 UnitsParameter Result
Arsenic mg/Kg6.77Metals by ICP/MS
Barium mg/Kg34.2
Chromium mg/Kg39.8
Lead mg/Kg9.30
Mercury mg/Kg0.0591
Residual Range Organics mg/Kg39.2Semivolatile Organic Fuels
Client Sample ID: SMIC-O (10)
Lab Sample ID: 1132110012 UnitsParameter Result
Arsenic mg/Kg4.46Metals by ICP/MS
Barium mg/Kg36.3
Chromium mg/Kg33.4
Lead mg/Kg4.71
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C167
Detectable Results Summary
Client Sample ID: SMIC-O (25)
Lab Sample ID: 1132110013 UnitsParameter Result
Arsenic mg/Kg4.64Metals by ICP/MS
Barium mg/Kg32.5
Chromium mg/Kg32.9
Lead mg/Kg5.30
Client Sample ID: SMIC-M (0)
Lab Sample ID: 1132110014 UnitsParameter Result
Arsenic mg/Kg4.19Metals by ICP/MS
Barium mg/Kg33.9
Chromium mg/Kg32.0
Lead mg/Kg5.05
Diesel Range Organics mg/Kg24.3Semivolatile Organic Fuels
Residual Range Organics mg/Kg146
Client Sample ID: SMIC-M (1.5)
Lab Sample ID: 1132110015 UnitsParameter Result
Arsenic mg/Kg4.44Metals by ICP/MS
Barium mg/Kg37.0
Chromium mg/Kg32.7
Lead mg/Kg5.56
Diesel Range Organics mg/Kg32.6Semivolatile Organic Fuels
Residual Range Organics mg/Kg184
Client Sample ID: SMIC-M (5)
Lab Sample ID: 1132110016 UnitsParameter Result
Arsenic mg/Kg4.06Metals by ICP/MS
Barium mg/Kg31.5
Chromium mg/Kg27.3
Lead mg/Kg5.55
Client Sample ID: SMIC-M (20)
Lab Sample ID: 1132110017 UnitsParameter Result
Arsenic mg/Kg4.66Metals by ICP/MS
Barium mg/Kg43.0
Chromium mg/Kg34.2
Lead mg/Kg5.59
Client Sample ID: SMIC-M (1.5) D
Lab Sample ID: 1132110018 UnitsParameter Result
Arsenic mg/Kg4.34Metals by ICP/MS
Barium mg/Kg44.3
Chromium mg/Kg34.2
Lead mg/Kg5.05
Residual Range Organics mg/Kg36.3Semivolatile Organic Fuels
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C168
Detectable Results Summary
Client Sample ID: SMIC-N (0)
Lab Sample ID: 1132110019 UnitsParameter Result
Arsenic mg/Kg14.3Metals by ICP/MS
Barium mg/Kg32.9
Chromium mg/Kg39.3
Lead mg/Kg7.88
Mercury mg/Kg0.0749
Residual Range Organics mg/Kg23.7Semivolatile Organic Fuels
Toluene ug/Kg50.5Volatile GC/MS
Client Sample ID: SMIC-N (1.5)
Lab Sample ID: 1132110020 UnitsParameter Result
Arsenic mg/Kg17.3Metals by ICP/MS
Barium mg/Kg30.0
Chromium mg/Kg36.6
Lead mg/Kg9.04
Mercury mg/Kg0.0561
Residual Range Organics mg/Kg44.7Semivolatile Organic Fuels
Client Sample ID: SMIC-N (10)
Lab Sample ID: 1132110021 UnitsParameter Result
Arsenic mg/Kg6.34Metals by ICP/MS
Barium mg/Kg35.1
Chromium mg/Kg37.9
Lead mg/Kg4.39
Client Sample ID: SMIC-N (30)
Lab Sample ID: 1132110022 UnitsParameter Result
Arsenic mg/Kg8.08Metals by ICP/MS
Barium mg/Kg50.3
Chromium mg/Kg29.2
Lead mg/Kg7.48
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C169
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Metals by ICP/MS
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.31 mg/Kg 100.933 0.289 06/04/13 17:41
Barium 35.3 mg/Kg 100.280 0.0877 06/04/13 17:41
Cadmium 0.187 mg/Kg 10U 0.187 0.0579 06/04/13 17:41
Chromium 35.3 mg/Kg 100.373 0.112 06/04/13 17:41
Lead 5.87 mg/Kg 100.187 0.0579 06/04/13 17:41
Mercury 0.0373 mg/Kg 10U 0.0373 0.0112 06/04/13 17:41
Selenium 0.467 mg/Kg 10U 0.467 0.140 06/04/13 17:41
Silver 0.0933 mg/Kg 10U 0.0933 0.0289 06/04/13 17:41
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.113 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:41
Container ID: 1132110001-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C170
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Semivolatile Organic Fuels
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.0 mg/Kg 1U 20.0 6.20 06/08/13 19:51
Surrogates
5a Androstane 103 % 150-150 06/08/13 19:51
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 31.155 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 19:51
Container ID: 1132110001-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 65.2 mg/Kg 120.0 6.20 06/08/13 19:51
Surrogates
n-Triacontane-d62 128 % 150-150 06/08/13 19:51
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 31.155 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 19:51
Container ID: 1132110001-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C171
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Semivolatile Organic GC/MS
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
1,2-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
1,3-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
1,4-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
1-Chloronaphthalene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,4,5-Trichlorophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,4,6-Trichlorophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,4-Dichlorophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,4-Dimethylphenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,4-Dinitrophenol 3.09 mg/Kg 1U 3.09 0.967 06/06/13 03:20
2,4-Dinitrotoluene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,6-Dichlorophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2,6-Dinitrotoluene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Chloronaphthalene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Chlorophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Methyl-4,6-dinitrophenol 2.06 mg/Kg 1U 2.06 0.638 06/06/13 03:20
2-Methylnaphthalene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Methylphenol (o-Cresol) 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Nitroaniline 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
2-Nitrophenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
3&4-Methylphenol (p&m-Cresol) 1.03 mg/Kg 1U 1.03 0.319 06/06/13 03:20
3,3-Dichlorobenzidine 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
3-Nitroaniline 0.514 mg/Kg 1U 0.514 0.154 06/06/13 03:20
4-Bromophenyl-phenylether 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
4-Chloro-3-methylphenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
4-Chloroaniline 0.514 mg/Kg 1U 0.514 0.154 06/06/13 03:20
4-Chlorophenyl-phenylether 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
4-Nitroaniline 3.09 mg/Kg 1U 3.09 0.967 06/06/13 03:20
4-Nitrophenol 1.03 mg/Kg 1U 1.03 0.319 06/06/13 03:20
Acenaphthene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Acenaphthylene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Aniline 2.06 mg/Kg 1U 2.06 0.638 06/06/13 03:20
Anthracene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Azobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzo(a)Anthracene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzo[a]pyrene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzo[b]Fluoranthene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzo[g,h,i]perylene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzo[k]fluoranthene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Benzoic acid 1.54 mg/Kg 1U 1.54 0.771 06/06/13 03:20
Benzyl alcohol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Bis(2-Chloroethoxy)methane 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Bis(2-Chloroethyl)ether 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
bis(2-Ethylhexyl)phthalate 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C172
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Semivolatile Organic GC/MS
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Butylbenzylphthalate 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Carbazole 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Chrysene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Di-n-butylphthalate 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
di-n-Octylphthalate 0.514 mg/Kg 1U 0.514 0.154 06/06/13 03:20
Dibenzo[a,h]anthracene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Dibenzofuran 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Diethylphthalate 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Dimethylphthalate 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Fluoranthene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Fluorene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Hexachlorobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Hexachlorobutadiene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Hexachlorocyclopentadiene 0.720 mg/Kg 1U 0.720 0.206 06/06/13 03:20
Hexachloroethane 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Indeno[1,2,3-c,d] pyrene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Isophorone 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
N-Nitroso-di-n-propylamine 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
N-Nitrosodimethylamine 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
N-Nitrosodiphenylamine 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Naphthalene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Nitrobenzene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Pentachlorophenol 2.06 mg/Kg 1U 2.06 0.638 06/06/13 03:20
Phenanthrene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Phenol 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Pyrene 0.257 mg/Kg 1U 0.257 0.0802 06/06/13 03:20
Surrogates
2,4,6-Tribromophenol 94.7 % 135-125 06/06/13 03:20
2-Fluorobiphenyl 90.2 % 145-105 06/06/13 03:20
2-Fluorophenol 70.9 % 135-105 06/06/13 03:20
Nitrobenzene-d5 78.6 % 135-100 06/06/13 03:20
Phenol-d6 79.4 % 140-100 06/06/13 03:20
Terphenyl-d14 139 % 130-125 06/06/13 03:20*
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.726 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Analyst: RTS
Analytical Date/Time: 06/06/13 03:20
Container ID: 1132110001-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C173
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Volatile Fuels
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.76 mg/Kg 1U 2.76 0.829 06/05/13 18:17
Surrogates
4-Bromofluorobenzene 97.2 % 150-150 06/05/13 18:17
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:29
Prep Initial Wt./Vol.: 50.514 g
Prep Extract Vol: 26.8826 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 18:17
Container ID: 1132110001-C
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C174
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Volatile GC/MS
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,1,1-Trichloroethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,1,2,2-Tetrachloroethane 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
1,1,2-Trichloroethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,1-Dichloroethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,1-Dichloroethene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,1-Dichloropropene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2,3-Trichlorobenzene 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
1,2,3-Trichloropropane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2,4-Trichlorobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2,4-Trimethylbenzene 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
1,2-Dibromo-3-chloropropane 111 ug/Kg 1U 111 34.3 06/03/13 15:04
1,2-Dibromoethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2-Dichloroethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,2-Dichloropropane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,3,5-Trimethylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,3-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,3-Dichloropropane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
1,4-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
2,2-Dichloropropane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
2-Butanone (MEK) 276 ug/Kg 1U 276 86.2 06/03/13 15:04
2-Chlorotoluene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
2-Hexanone 276 ug/Kg 1U 276 86.2 06/03/13 15:04
4-Chlorotoluene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
4-Isopropyltoluene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
4-Methyl-2-pentanone (MIBK) 276 ug/Kg 1U 276 86.2 06/03/13 15:04
Benzene 13.8 ug/Kg 1U 13.8 4.31 06/03/13 15:04
Bromobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Bromochloromethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Bromodichloromethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Bromoform 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Bromomethane 221 ug/Kg 1U 221 68.5 06/03/13 15:04
Carbon disulfide 111 ug/Kg 1U 111 34.3 06/03/13 15:04
Carbon tetrachloride 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Chlorobenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Chloroethane 221 ug/Kg 1U 221 68.5 06/03/13 15:04
Chloroform 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Chloromethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
cis-1,2-Dichloroethene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
cis-1,3-Dichloropropene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Dibromochloromethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Dibromomethane 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Dichlorodifluoromethane 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C175
Client Sample ID: SMIC-K (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110001
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.3
Results by Volatile GC/MS
Results of SMIC-K (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Hexachlorobutadiene 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
Isopropylbenzene (Cumene) 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Methyl-t-butyl ether 111 ug/Kg 1U 111 34.3 06/03/13 15:04
Methylene chloride 111 ug/Kg 1U 111 34.3 06/03/13 15:04
n-Butylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
n-Propylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Naphthalene 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
o-Xylene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
P & M -Xylene 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
sec-Butylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Styrene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
tert-Butylbenzene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Tetrachloroethene 13.8 ug/Kg 1U 13.8 4.31 06/03/13 15:04
Toluene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
trans-1,2-Dichloroethene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
trans-1,3-Dichloropropene 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Trichloroethene 13.8 ug/Kg 1U 13.8 4.31 06/03/13 15:04
Trichlorofluoromethane 55.3 ug/Kg 1U 55.3 16.6 06/03/13 15:04
Vinyl chloride 27.6 ug/Kg 1U 27.6 8.62 06/03/13 15:04
Xylenes (total) 111 ug/Kg 1U 111 34.3 06/03/13 15:04
Surrogates
1,2-Dichloroethane-D4 111 % 179-118 06/03/13 15:04
4-Bromofluorobenzene 97.3 % 167-138 06/03/13 15:04
Toluene-d8 103 % 185-115 06/03/13 15:04
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:29
Prep Initial Wt./Vol.: 50.514 g
Prep Extract Vol: 26.8826 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 15:04
Container ID: 1132110001-C
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C176
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Metals by ICP/MS
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 3.69 mg/Kg 100.944 0.293 06/04/13 17:43
Barium 29.5 mg/Kg 100.283 0.0888 06/04/13 17:43
Cadmium 0.189 mg/Kg 10U 0.189 0.0585 06/04/13 17:43
Chromium 31.3 mg/Kg 100.378 0.113 06/04/13 17:43
Lead 4.72 mg/Kg 100.189 0.0585 06/04/13 17:43
Mercury 0.0378 mg/Kg 10U 0.0378 0.0113 06/04/13 17:43
Selenium 0.472 mg/Kg 10U 0.472 0.142 06/04/13 17:43
Silver 0.0944 mg/Kg 10U 0.0944 0.0293 06/04/13 17:43
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.086 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:43
Container ID: 1132110002-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C177
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic Fuels
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 19.9 mg/Kg 1U 19.9 6.18 06/08/13 20:01
Surrogates
5a Androstane 106 % 150-150 06/08/13 20:01
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.883 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:01
Container ID: 1132110002-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 19.9 mg/Kg 1U 19.9 6.18 06/08/13 20:01
Surrogates
n-Triacontane-d62 130 % 150-150 06/08/13 20:01
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.883 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:01
Container ID: 1132110002-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C178
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic GC/MS
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,4-Dinitrophenol 3.04 mg/Kg 1U 3.04 0.954 06/06/13 03:37
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.629 06/06/13 03:37
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
3&4-Methylphenol (p&m-Cresol) 1.01 mg/Kg 1U 1.01 0.314 06/06/13 03:37
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
3-Nitroaniline 0.507 mg/Kg 1U 0.507 0.152 06/06/13 03:37
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
4-Chloroaniline 0.507 mg/Kg 1U 0.507 0.152 06/06/13 03:37
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
4-Nitroaniline 3.04 mg/Kg 1U 3.04 0.954 06/06/13 03:37
4-Nitrophenol 1.01 mg/Kg 1U 1.01 0.314 06/06/13 03:37
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Aniline 2.03 mg/Kg 1U 2.03 0.629 06/06/13 03:37
Anthracene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Azobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Benzoic acid 1.52 mg/Kg 1U 1.52 0.761 06/06/13 03:37
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C179
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic GC/MS
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Carbazole 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Chrysene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
di-n-Octylphthalate 0.507 mg/Kg 1U 0.507 0.152 06/06/13 03:37
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Fluorene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Hexachlorocyclopentadiene 0.710 mg/Kg 1U 0.710 0.203 06/06/13 03:37
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Isophorone 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Naphthalene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.629 06/06/13 03:37
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Phenol 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Pyrene 0.254 mg/Kg 1U 0.254 0.0791 06/06/13 03:37
Surrogates
2,4,6-Tribromophenol 86.7 % 135-125 06/06/13 03:37
2-Fluorobiphenyl 85.1 % 145-105 06/06/13 03:37
2-Fluorophenol 70.7 % 135-105 06/06/13 03:37
Nitrobenzene-d5 78.1 % 135-100 06/06/13 03:37
Phenol-d6 79.8 % 140-100 06/06/13 03:37
Terphenyl-d14 128 % 130-125 06/06/13 03:37*
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.745 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Analyst: RTS
Analytical Date/Time: 06/06/13 03:37
Container ID: 1132110002-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C180
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile Fuels
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.76 mg/Kg 1U 2.76 0.827 06/05/13 18:36
Surrogates
4-Bromofluorobenzene 97.4 % 150-150 06/05/13 18:36
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:37
Prep Initial Wt./Vol.: 48.735 g
Prep Extract Vol: 26.2146 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 18:36
Container ID: 1132110002-C
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C181
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile GC/MS
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,1,1-Trichloroethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,1,2,2-Tetrachloroethane 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
1,1,2-Trichloroethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,1-Dichloroethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,1-Dichloroethene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,1-Dichloropropene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2,3-Trichlorobenzene 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
1,2,3-Trichloropropane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2,4-Trichlorobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2,4-Trimethylbenzene 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
1,2-Dibromo-3-chloropropane 110 ug/Kg 1U 110 34.2 06/03/13 15:21
1,2-Dibromoethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2-Dichloroethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,2-Dichloropropane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,3,5-Trimethylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,3-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,3-Dichloropropane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
1,4-Dichlorobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
2,2-Dichloropropane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
2-Butanone (MEK) 276 ug/Kg 1U 276 86.1 06/03/13 15:21
2-Chlorotoluene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
2-Hexanone 276 ug/Kg 1U 276 86.1 06/03/13 15:21
4-Chlorotoluene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
4-Isopropyltoluene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
4-Methyl-2-pentanone (MIBK) 276 ug/Kg 1U 276 86.1 06/03/13 15:21
Benzene 13.8 ug/Kg 1U 13.8 4.30 06/03/13 15:21
Bromobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Bromochloromethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Bromodichloromethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Bromoform 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Bromomethane 221 ug/Kg 1U 221 68.4 06/03/13 15:21
Carbon disulfide 110 ug/Kg 1U 110 34.2 06/03/13 15:21
Carbon tetrachloride 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Chlorobenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Chloroethane 221 ug/Kg 1U 221 68.4 06/03/13 15:21
Chloroform 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Chloromethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
cis-1,2-Dichloroethene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
cis-1,3-Dichloropropene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Dibromochloromethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Dibromomethane 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Dichlorodifluoromethane 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C182
Client Sample ID: SMIC-K (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110002
Lab Project ID: 1132110
Collection Date: 05/30/13 10:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile GC/MS
Results of SMIC-K (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Hexachlorobutadiene 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
Isopropylbenzene (Cumene) 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Methyl-t-butyl ether 110 ug/Kg 1U 110 34.2 06/03/13 15:21
Methylene chloride 110 ug/Kg 1U 110 34.2 06/03/13 15:21
n-Butylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
n-Propylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Naphthalene 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
o-Xylene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
P & M -Xylene 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
sec-Butylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Styrene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
tert-Butylbenzene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Tetrachloroethene 13.8 ug/Kg 1U 13.8 4.30 06/03/13 15:21
Toluene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
trans-1,2-Dichloroethene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
trans-1,3-Dichloropropene 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Trichloroethene 13.8 ug/Kg 1U 13.8 4.30 06/03/13 15:21
Trichlorofluoromethane 55.2 ug/Kg 1U 55.2 16.5 06/03/13 15:21
Vinyl chloride 27.6 ug/Kg 1U 27.6 8.61 06/03/13 15:21
Xylenes (total) 110 ug/Kg 1U 110 34.2 06/03/13 15:21
Surrogates
1,2-Dichloroethane-D4 113 % 179-118 06/03/13 15:21
4-Bromofluorobenzene 97.5 % 167-138 06/03/13 15:21
Toluene-d8 104 % 185-115 06/03/13 15:21
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:37
Prep Initial Wt./Vol.: 48.735 g
Prep Extract Vol: 26.2146 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 15:21
Container ID: 1132110002-C
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C183
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Metals by ICP/MS
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 6.14 mg/Kg 101.08 0.334 06/04/13 17:50
Barium 50.1 mg/Kg 100.323 0.101 06/04/13 17:50
Cadmium 0.215 mg/Kg 10U 0.215 0.0667 06/04/13 17:50
Chromium 37.2 mg/Kg 100.431 0.129 06/04/13 17:50
Lead 5.80 mg/Kg 100.215 0.0667 06/04/13 17:50
Mercury 0.0431 mg/Kg 10U 0.0431 0.0129 06/04/13 17:50
Selenium 0.538 mg/Kg 10U 0.538 0.161 06/04/13 17:50
Silver 0.108 mg/Kg 10U 0.108 0.0334 06/04/13 17:50
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.012 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:50
Container ID: 1132110003-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C184
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Semivolatile Organic Fuels
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 21.4 mg/Kg 1U 21.4 6.64 06/08/13 20:10
Surrogates
5a Androstane 94.2 % 150-150 06/08/13 20:10
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.51 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:10
Container ID: 1132110003-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 21.4 mg/Kg 1U 21.4 6.64 06/08/13 20:10
Surrogates
n-Triacontane-d62 113 % 150-150 06/08/13 20:10
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.51 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:10
Container ID: 1132110003-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C185
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Semivolatile Organic GC/MS
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
1,2-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
1,3-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
1,4-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
1-Chloronaphthalene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,4,5-Trichlorophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,4,6-Trichlorophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,4-Dichlorophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,4-Dimethylphenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,4-Dinitrophenol 3.26 mg/Kg 1U 3.26 1.02 06/06/13 03:54
2,4-Dinitrotoluene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,6-Dichlorophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2,6-Dinitrotoluene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Chloronaphthalene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Chlorophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Methyl-4,6-dinitrophenol 2.17 mg/Kg 1U 2.17 0.674 06/06/13 03:54
2-Methylnaphthalene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Methylphenol (o-Cresol) 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Nitroaniline 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
2-Nitrophenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
3&4-Methylphenol (p&m-Cresol) 1.09 mg/Kg 1U 1.09 0.337 06/06/13 03:54
3,3-Dichlorobenzidine 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
3-Nitroaniline 0.543 mg/Kg 1U 0.543 0.163 06/06/13 03:54
4-Bromophenyl-phenylether 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
4-Chloro-3-methylphenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
4-Chloroaniline 0.543 mg/Kg 1U 0.543 0.163 06/06/13 03:54
4-Chlorophenyl-phenylether 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
4-Nitroaniline 3.26 mg/Kg 1U 3.26 1.02 06/06/13 03:54
4-Nitrophenol 1.09 mg/Kg 1U 1.09 0.337 06/06/13 03:54
Acenaphthene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Acenaphthylene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Aniline 2.17 mg/Kg 1U 2.17 0.674 06/06/13 03:54
Anthracene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Azobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzo(a)Anthracene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzo[a]pyrene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzo[b]Fluoranthene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzo[g,h,i]perylene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzo[k]fluoranthene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Benzoic acid 1.63 mg/Kg 1U 1.63 0.815 06/06/13 03:54
Benzyl alcohol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Bis(2-Chloroethoxy)methane 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Bis(2-Chloroethyl)ether 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
bis(2-Ethylhexyl)phthalate 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C186
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Semivolatile Organic GC/MS
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Butylbenzylphthalate 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Carbazole 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Chrysene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Di-n-butylphthalate 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
di-n-Octylphthalate 0.543 mg/Kg 1U 0.543 0.163 06/06/13 03:54
Dibenzo[a,h]anthracene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Dibenzofuran 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Diethylphthalate 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Dimethylphthalate 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Fluoranthene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Fluorene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Hexachlorobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Hexachlorobutadiene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Hexachlorocyclopentadiene 0.761 mg/Kg 1U 0.761 0.217 06/06/13 03:54
Hexachloroethane 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Indeno[1,2,3-c,d] pyrene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Isophorone 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
N-Nitroso-di-n-propylamine 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
N-Nitrosodimethylamine 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
N-Nitrosodiphenylamine 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Naphthalene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Nitrobenzene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Pentachlorophenol 2.17 mg/Kg 1U 2.17 0.674 06/06/13 03:54
Phenanthrene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Phenol 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Pyrene 0.272 mg/Kg 1U 0.272 0.0848 06/06/13 03:54
Surrogates
2,4,6-Tribromophenol 77.6 % 135-125 06/06/13 03:54
2-Fluorobiphenyl 73.8 % 145-105 06/06/13 03:54
2-Fluorophenol 53.7 % 135-105 06/06/13 03:54
Nitrobenzene-d5 59.8 % 135-100 06/06/13 03:54
Phenol-d6 62.2 % 140-100 06/06/13 03:54
Terphenyl-d14 126 % 130-125 06/06/13 03:54*
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.552 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Analyst: RTS
Analytical Date/Time: 06/06/13 03:54
Container ID: 1132110003-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C187
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Volatile Fuels
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.86 mg/Kg 1U 2.86 0.859 06/05/13 18:54
Surrogates
4-Bromofluorobenzene 103 % 150-150 06/05/13 18:54
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:58
Prep Initial Wt./Vol.: 56.362 g
Prep Extract Vol: 29.6194 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 18:54
Container ID: 1132110003-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C188
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Volatile GC/MS
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,1,1-Trichloroethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,1,2,2-Tetrachloroethane 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
1,1,2-Trichloroethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,1-Dichloroethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,1-Dichloroethene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,1-Dichloropropene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2,3-Trichlorobenzene 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
1,2,3-Trichloropropane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2,4-Trichlorobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2,4-Trimethylbenzene 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
1,2-Dibromo-3-chloropropane 114 ug/Kg 1U 114 35.5 06/03/13 15:37
1,2-Dibromoethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2-Dichlorobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2-Dichloroethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,2-Dichloropropane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,3,5-Trimethylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,3-Dichlorobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,3-Dichloropropane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
1,4-Dichlorobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
2,2-Dichloropropane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
2-Butanone (MEK) 286 ug/Kg 1U 286 89.3 06/03/13 15:37
2-Chlorotoluene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
2-Hexanone 286 ug/Kg 1U 286 89.3 06/03/13 15:37
4-Chlorotoluene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
4-Isopropyltoluene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
4-Methyl-2-pentanone (MIBK) 286 ug/Kg 1U 286 89.3 06/03/13 15:37
Benzene 14.3 ug/Kg 1U 14.3 4.47 06/03/13 15:37
Bromobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Bromochloromethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Bromodichloromethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Bromoform 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Bromomethane 229 ug/Kg 1U 229 71.0 06/03/13 15:37
Carbon disulfide 114 ug/Kg 1U 114 35.5 06/03/13 15:37
Carbon tetrachloride 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Chlorobenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Chloroethane 229 ug/Kg 1U 229 71.0 06/03/13 15:37
Chloroform 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Chloromethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
cis-1,2-Dichloroethene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
cis-1,3-Dichloropropene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Dibromochloromethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Dibromomethane 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Dichlorodifluoromethane 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C189
Client Sample ID: SMIC-K (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110003
Lab Project ID: 1132110
Collection Date: 05/30/13 10:58
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 91.8
Results by Volatile GC/MS
Results of SMIC-K (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Hexachlorobutadiene 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
Isopropylbenzene (Cumene) 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Methyl-t-butyl ether 114 ug/Kg 1U 114 35.5 06/03/13 15:37
Methylene chloride 114 ug/Kg 1U 114 35.5 06/03/13 15:37
n-Butylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
n-Propylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Naphthalene 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
o-Xylene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
P & M -Xylene 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
sec-Butylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Styrene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
tert-Butylbenzene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Tetrachloroethene 14.3 ug/Kg 1U 14.3 4.47 06/03/13 15:37
Toluene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
trans-1,2-Dichloroethene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
trans-1,3-Dichloropropene 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Trichloroethene 14.3 ug/Kg 1U 14.3 4.47 06/03/13 15:37
Trichlorofluoromethane 57.2 ug/Kg 1U 57.2 17.2 06/03/13 15:37
Vinyl chloride 28.6 ug/Kg 1U 28.6 8.93 06/03/13 15:37
Xylenes (total) 114 ug/Kg 1U 114 35.5 06/03/13 15:37
Surrogates
1,2-Dichloroethane-D4 109 % 179-118 06/03/13 15:37
4-Bromofluorobenzene 101 % 167-138 06/03/13 15:37
Toluene-d8 101 % 185-115 06/03/13 15:37
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:58
Prep Initial Wt./Vol.: 56.362 g
Prep Extract Vol: 29.6194 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 15:37
Container ID: 1132110003-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C190
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Metals by ICP/MS
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 5.66 mg/Kg 101.08 0.334 06/04/13 17:52
Barium 46.2 mg/Kg 100.324 0.101 06/04/13 17:52
Cadmium 0.216 mg/Kg 10U 0.216 0.0669 06/04/13 17:52
Chromium 32.5 mg/Kg 100.431 0.129 06/04/13 17:52
Lead 6.45 mg/Kg 100.216 0.0669 06/04/13 17:52
Mercury 0.0431 mg/Kg 10U 0.0431 0.0129 06/04/13 17:52
Selenium 0.539 mg/Kg 10U 0.539 0.162 06/04/13 17:52
Silver 0.108 mg/Kg 10U 0.108 0.0334 06/04/13 17:52
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.06 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:52
Container ID: 1132110004-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C191
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Semivolatile Organic Fuels
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.3 mg/Kg 1U 22.3 6.92 06/08/13 20:19
Surrogates
5a Androstane 106 % 150-150 06/08/13 20:19
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.722 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:19
Container ID: 1132110004-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.3 mg/Kg 1U 22.3 6.92 06/08/13 20:19
Surrogates
n-Triacontane-d62 126 % 150-150 06/08/13 20:19
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.722 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:19
Container ID: 1132110004-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C192
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Semivolatile Organic GC/MS
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
1,2-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
1,3-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
1,4-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
1-Chloronaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,4,5-Trichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,4,6-Trichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,4-Dichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,4-Dimethylphenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,4-Dinitrophenol 3.39 mg/Kg 1U 3.39 1.06 06/06/13 04:10
2,4-Dinitrotoluene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,6-Dichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2,6-Dinitrotoluene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Chloronaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Chlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Methyl-4,6-dinitrophenol 2.26 mg/Kg 1U 2.26 0.701 06/06/13 04:10
2-Methylnaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Methylphenol (o-Cresol) 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Nitroaniline 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
2-Nitrophenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
3&4-Methylphenol (p&m-Cresol) 1.13 mg/Kg 1U 1.13 0.350 06/06/13 04:10
3,3-Dichlorobenzidine 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
3-Nitroaniline 0.565 mg/Kg 1U 0.565 0.170 06/06/13 04:10
4-Bromophenyl-phenylether 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
4-Chloro-3-methylphenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
4-Chloroaniline 0.565 mg/Kg 1U 0.565 0.170 06/06/13 04:10
4-Chlorophenyl-phenylether 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
4-Nitroaniline 3.39 mg/Kg 1U 3.39 1.06 06/06/13 04:10
4-Nitrophenol 1.13 mg/Kg 1U 1.13 0.350 06/06/13 04:10
Acenaphthene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Acenaphthylene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Aniline 2.26 mg/Kg 1U 2.26 0.701 06/06/13 04:10
Anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Azobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzo(a)Anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzo[a]pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzo[b]Fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzo[g,h,i]perylene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzo[k]fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Benzoic acid 1.70 mg/Kg 1U 1.70 0.848 06/06/13 04:10
Benzyl alcohol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Bis(2-Chloroethoxy)methane 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Bis(2-Chloroethyl)ether 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
bis(2-Ethylhexyl)phthalate 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C193
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Semivolatile Organic GC/MS
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Butylbenzylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Carbazole 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Chrysene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Di-n-butylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
di-n-Octylphthalate 0.565 mg/Kg 1U 0.565 0.170 06/06/13 04:10
Dibenzo[a,h]anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Dibenzofuran 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Diethylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Dimethylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Fluorene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Hexachlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Hexachlorobutadiene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Hexachlorocyclopentadiene 0.791 mg/Kg 1U 0.791 0.226 06/06/13 04:10
Hexachloroethane 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Indeno[1,2,3-c,d] pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Isophorone 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
N-Nitroso-di-n-propylamine 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
N-Nitrosodimethylamine 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
N-Nitrosodiphenylamine 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Naphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Nitrobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Pentachlorophenol 2.26 mg/Kg 1U 2.26 0.701 06/06/13 04:10
Phenanthrene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Phenol 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/06/13 04:10
Surrogates
2,4,6-Tribromophenol 77.1 % 135-125 06/06/13 04:10
2-Fluorobiphenyl 72.9 % 145-105 06/06/13 04:10
2-Fluorophenol 57.3 % 135-105 06/06/13 04:10
Nitrobenzene-d5 62 % 135-100 06/06/13 04:10
Phenol-d6 65.9 % 140-100 06/06/13 04:10
Terphenyl-d14 128 % 130-125 06/06/13 04:10*
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.752 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Analyst: RTS
Analytical Date/Time: 06/06/13 04:10
Container ID: 1132110004-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C194
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Volatile Fuels
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 3.17 mg/Kg 1U 3.17 0.951 06/05/13 19:13
Surrogates
4-Bromofluorobenzene 103 % 150-150 06/05/13 19:13
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 12:28
Prep Initial Wt./Vol.: 58.255 g
Prep Extract Vol: 32.2962 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 19:13
Container ID: 1132110004-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C195
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Volatile GC/MS
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,1,1-Trichloroethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,1,2,2-Tetrachloroethane 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
1,1,2-Trichloroethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,1-Dichloroethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,1-Dichloroethene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,1-Dichloropropene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2,3-Trichlorobenzene 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
1,2,3-Trichloropropane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2,4-Trichlorobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2,4-Trimethylbenzene 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
1,2-Dibromo-3-chloropropane 127 ug/Kg 1U 127 39.3 06/03/13 15:54
1,2-Dibromoethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2-Dichlorobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2-Dichloroethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,2-Dichloropropane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,3,5-Trimethylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,3-Dichlorobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,3-Dichloropropane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
1,4-Dichlorobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
2,2-Dichloropropane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
2-Butanone (MEK) 317 ug/Kg 1U 317 98.9 06/03/13 15:54
2-Chlorotoluene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
2-Hexanone 317 ug/Kg 1U 317 98.9 06/03/13 15:54
4-Chlorotoluene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
4-Isopropyltoluene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
4-Methyl-2-pentanone (MIBK) 317 ug/Kg 1U 317 98.9 06/03/13 15:54
Benzene 15.8 ug/Kg 1U 15.8 4.94 06/03/13 15:54
Bromobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Bromochloromethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Bromodichloromethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Bromoform 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Bromomethane 254 ug/Kg 1U 254 78.6 06/03/13 15:54
Carbon disulfide 127 ug/Kg 1U 127 39.3 06/03/13 15:54
Carbon tetrachloride 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Chlorobenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Chloroethane 254 ug/Kg 1U 254 78.6 06/03/13 15:54
Chloroform 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Chloromethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
cis-1,2-Dichloroethene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
cis-1,3-Dichloropropene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Dibromochloromethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Dibromomethane 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Dichlorodifluoromethane 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C196
Client Sample ID: SMIC-K (40)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110004
Lab Project ID: 1132110
Collection Date: 05/30/13 12:28
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 87.5
Results by Volatile GC/MS
Results of SMIC-K (40)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Hexachlorobutadiene 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
Isopropylbenzene (Cumene) 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Methyl-t-butyl ether 127 ug/Kg 1U 127 39.3 06/03/13 15:54
Methylene chloride 127 ug/Kg 1U 127 39.3 06/03/13 15:54
n-Butylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
n-Propylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Naphthalene 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
o-Xylene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
P & M -Xylene 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
sec-Butylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Styrene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
tert-Butylbenzene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Tetrachloroethene 15.8 ug/Kg 1U 15.8 4.94 06/03/13 15:54
Toluene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
trans-1,2-Dichloroethene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
trans-1,3-Dichloropropene 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Trichloroethene 15.8 ug/Kg 1U 15.8 4.94 06/03/13 15:54
Trichlorofluoromethane 63.4 ug/Kg 1U 63.4 19.0 06/03/13 15:54
Vinyl chloride 31.7 ug/Kg 1U 31.7 9.89 06/03/13 15:54
Xylenes (total) 127 ug/Kg 1U 127 39.3 06/03/13 15:54
Surrogates
1,2-Dichloroethane-D4 115 % 179-118 06/03/13 15:54
4-Bromofluorobenzene 103 % 167-138 06/03/13 15:54
Toluene-d8 105 % 185-115 06/03/13 15:54
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 12:28
Prep Initial Wt./Vol.: 58.255 g
Prep Extract Vol: 32.2962 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 15:54
Container ID: 1132110004-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C197
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Metals by ICP/MS
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.02 mg/Kg 100.973 0.302 06/04/13 17:54
Barium 37.4 mg/Kg 100.292 0.0914 06/04/13 17:54
Cadmium 0.195 mg/Kg 10U 0.195 0.0603 06/04/13 17:54
Chromium 31.9 mg/Kg 100.389 0.117 06/04/13 17:54
Lead 7.18 mg/Kg 100.195 0.0603 06/04/13 17:54
Mercury 0.0389 mg/Kg 10U 0.0389 0.0117 06/04/13 17:54
Selenium 0.486 mg/Kg 10U 0.486 0.146 06/04/13 17:54
Silver 0.0973 mg/Kg 10U 0.0973 0.0302 06/04/13 17:54
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.078 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:54
Container ID: 1132110005-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C198
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Semivolatile Organic Fuels
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 45.1 mg/Kg 120.5 6.34 06/08/13 20:29
Surrogates
5a Androstane 116 % 150-150 06/08/13 20:29
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.74 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:29
Container ID: 1132110005-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 267 mg/Kg 120.5 6.34 06/08/13 20:29
Surrogates
n-Triacontane-d62 146 % 150-150 06/08/13 20:29
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.74 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:29
Container ID: 1132110005-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C199
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Semivolatile Organic GC/MS
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
1,2-Dichlorobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
1,3-Dichlorobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
1,4-Dichlorobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
1-Chloronaphthalene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,4,5-Trichlorophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,4,6-Trichlorophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,4-Dichlorophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,4-Dimethylphenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,4-Dinitrophenol 3.10 mg/Kg 1U 3.10 0.972 06/11/13 21:39
2,4-Dinitrotoluene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,6-Dichlorophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2,6-Dinitrotoluene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Chloronaphthalene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Chlorophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Methyl-4,6-dinitrophenol 2.07 mg/Kg 1U 2.07 0.641 06/11/13 21:39
2-Methylnaphthalene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Methylphenol (o-Cresol) 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Nitroaniline 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
2-Nitrophenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
3&4-Methylphenol (p&m-Cresol) 1.03 mg/Kg 1U 1.03 0.320 06/11/13 21:39
3,3-Dichlorobenzidine 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
3-Nitroaniline 0.517 mg/Kg 1U 0.517 0.155 06/11/13 21:39
4-Bromophenyl-phenylether 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
4-Chloro-3-methylphenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
4-Chloroaniline 0.517 mg/Kg 1U 0.517 0.155 06/11/13 21:39
4-Chlorophenyl-phenylether 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
4-Nitroaniline 3.10 mg/Kg 1U 3.10 0.972 06/11/13 21:39
4-Nitrophenol 1.03 mg/Kg 1U 1.03 0.320 06/11/13 21:39
Acenaphthene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Acenaphthylene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Aniline 2.07 mg/Kg 1U 2.07 0.641 06/11/13 21:39
Anthracene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Azobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzo(a)Anthracene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzo[a]pyrene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzo[b]Fluoranthene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzo[g,h,i]perylene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzo[k]fluoranthene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Benzoic acid 1.55 mg/Kg 1U 1.55 0.775 06/11/13 21:39
Benzyl alcohol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Bis(2-Chloroethoxy)methane 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Bis(2-Chloroethyl)ether 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
bis(2-Ethylhexyl)phthalate 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C200
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Semivolatile Organic GC/MS
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Butylbenzylphthalate 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Carbazole 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Chrysene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Di-n-butylphthalate 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
di-n-Octylphthalate 0.517 mg/Kg 1U 0.517 0.155 06/11/13 21:39
Dibenzo[a,h]anthracene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Dibenzofuran 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Diethylphthalate 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Dimethylphthalate 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Fluoranthene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Fluorene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Hexachlorobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Hexachlorobutadiene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Hexachlorocyclopentadiene 0.724 mg/Kg 1U 0.724 0.207 06/11/13 21:39
Hexachloroethane 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Indeno[1,2,3-c,d] pyrene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Isophorone 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
N-Nitroso-di-n-propylamine 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
N-Nitrosodimethylamine 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
N-Nitrosodiphenylamine 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Naphthalene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Nitrobenzene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Pentachlorophenol 2.07 mg/Kg 1U 2.07 0.641 06/11/13 21:39
Phenanthrene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Phenol 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Pyrene 0.258 mg/Kg 1U 0.258 0.0806 06/11/13 21:39
Surrogates
2,4,6-Tribromophenol 113 % 135-125 06/11/13 21:39
2-Fluorobiphenyl 95.7 % 145-105 06/11/13 21:39
2-Fluorophenol 65.7 % 135-105 06/11/13 21:39
Nitrobenzene-d5 67.1 % 135-100 06/11/13 21:39
Phenol-d6 76.3 % 140-100 06/11/13 21:39
Terphenyl-d14 110 % 130-125 06/11/13 21:39
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.824 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 21:39
Container ID: 1132110005-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C201
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Volatile Fuels
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.70 mg/Kg 1U 2.70 0.811 06/05/13 19:32
Surrogates
4-Bromofluorobenzene 96.9 % 150-150 06/05/13 19:32
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 15:44
Prep Initial Wt./Vol.: 53.265 g
Prep Extract Vol: 27.4662 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 19:32
Container ID: 1132110005-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C202
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Volatile GC/MS
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,1,1-Trichloroethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,1,2,2-Tetrachloroethane 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
1,1,2-Trichloroethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,1-Dichloroethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,1-Dichloroethene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,1-Dichloropropene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2,3-Trichlorobenzene 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
1,2,3-Trichloropropane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2,4-Trichlorobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2,4-Trimethylbenzene 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
1,2-Dibromo-3-chloropropane 108 ug/Kg 1U 108 33.5 06/03/13 16:11
1,2-Dibromoethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2-Dichlorobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2-Dichloroethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,2-Dichloropropane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,3,5-Trimethylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,3-Dichlorobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,3-Dichloropropane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
1,4-Dichlorobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
2,2-Dichloropropane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
2-Butanone (MEK) 270 ug/Kg 1U 270 84.3 06/03/13 16:11
2-Chlorotoluene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
2-Hexanone 270 ug/Kg 1U 270 84.3 06/03/13 16:11
4-Chlorotoluene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
4-Isopropyltoluene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
4-Methyl-2-pentanone (MIBK) 270 ug/Kg 1U 270 84.3 06/03/13 16:11
Benzene 13.5 ug/Kg 1U 13.5 4.22 06/03/13 16:11
Bromobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Bromochloromethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Bromodichloromethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Bromoform 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Bromomethane 216 ug/Kg 1U 216 67.0 06/03/13 16:11
Carbon disulfide 108 ug/Kg 1U 108 33.5 06/03/13 16:11
Carbon tetrachloride 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Chlorobenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Chloroethane 216 ug/Kg 1U 216 67.0 06/03/13 16:11
Chloroform 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Chloromethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
cis-1,2-Dichloroethene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
cis-1,3-Dichloropropene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Dibromochloromethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Dibromomethane 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Dichlorodifluoromethane 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C203
Client Sample ID: SMIC-L (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110005
Lab Project ID: 1132110
Collection Date: 05/30/13 15:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 95.4
Results by Volatile GC/MS
Results of SMIC-L (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Hexachlorobutadiene 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
Isopropylbenzene (Cumene) 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Methyl-t-butyl ether 108 ug/Kg 1U 108 33.5 06/03/13 16:11
Methylene chloride 108 ug/Kg 1U 108 33.5 06/03/13 16:11
n-Butylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
n-Propylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Naphthalene 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
o-Xylene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
P & M -Xylene 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
sec-Butylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Styrene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
tert-Butylbenzene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Tetrachloroethene 13.5 ug/Kg 1U 13.5 4.22 06/03/13 16:11
Toluene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
trans-1,2-Dichloroethene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
trans-1,3-Dichloropropene 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Trichloroethene 13.5 ug/Kg 1U 13.5 4.22 06/03/13 16:11
Trichlorofluoromethane 54.1 ug/Kg 1U 54.1 16.2 06/03/13 16:11
Vinyl chloride 27.0 ug/Kg 1U 27.0 8.43 06/03/13 16:11
Xylenes (total) 108 ug/Kg 1U 108 33.5 06/03/13 16:11
Surrogates
1,2-Dichloroethane-D4 109 % 179-118 06/03/13 16:11
4-Bromofluorobenzene 94.5 % 167-138 06/03/13 16:11
Toluene-d8 98.8 % 185-115 06/03/13 16:11
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 15:44
Prep Initial Wt./Vol.: 53.265 g
Prep Extract Vol: 27.4662 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 16:11
Container ID: 1132110005-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C204
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Metals by ICP/MS
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.73 mg/Kg 100.959 0.297 06/04/13 17:27
Barium 33.0 mg/Kg 100.288 0.0901 06/04/13 17:27
Cadmium 0.192 mg/Kg 10U 0.192 0.0595 06/04/13 17:27
Chromium 47.1 mg/Kg 100.384 0.115 06/04/13 17:27
Lead 4.78 mg/Kg 100.192 0.0595 06/04/13 17:27
Mercury 0.0384 mg/Kg 10U 0.0384 0.0115 06/04/13 17:27
Selenium 0.480 mg/Kg 10U 0.480 0.144 06/04/13 17:27
Silver 0.0959 mg/Kg 10U 0.0959 0.0297 06/04/13 17:27
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.062 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:27
Container ID: 1132110006-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C205
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Semivolatile Organic Fuels
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.1 mg/Kg 1U 20.1 6.24 06/08/13 20:38
Surrogates
5a Androstane 110 % 150-150 06/08/13 20:38
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.338 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:38
Container ID: 1132110006-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 20.1 mg/Kg 1U 20.1 6.24 06/08/13 20:38
Surrogates
n-Triacontane-d62 130 % 150-150 06/08/13 20:38
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.338 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:38
Container ID: 1132110006-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C206
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Semivolatile Organic GC/MS
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
1,2-Dichlorobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
1,3-Dichlorobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
1,4-Dichlorobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
1-Chloronaphthalene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,4,5-Trichlorophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,4,6-Trichlorophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,4-Dichlorophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,4-Dimethylphenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,4-Dinitrophenol 3.03 mg/Kg 1U 3.03 0.951 06/11/13 21:57
2,4-Dinitrotoluene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,6-Dichlorophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2,6-Dinitrotoluene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Chloronaphthalene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Chlorophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Methyl-4,6-dinitrophenol 2.02 mg/Kg 1U 2.02 0.627 06/11/13 21:57
2-Methylnaphthalene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Methylphenol (o-Cresol) 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Nitroaniline 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
2-Nitrophenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
3&4-Methylphenol (p&m-Cresol) 1.01 mg/Kg 1U 1.01 0.314 06/11/13 21:57
3,3-Dichlorobenzidine 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
3-Nitroaniline 0.506 mg/Kg 1U 0.506 0.152 06/11/13 21:57
4-Bromophenyl-phenylether 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
4-Chloro-3-methylphenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
4-Chloroaniline 0.506 mg/Kg 1U 0.506 0.152 06/11/13 21:57
4-Chlorophenyl-phenylether 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
4-Nitroaniline 3.03 mg/Kg 1U 3.03 0.951 06/11/13 21:57
4-Nitrophenol 1.01 mg/Kg 1U 1.01 0.314 06/11/13 21:57
Acenaphthene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Acenaphthylene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Aniline 2.02 mg/Kg 1U 2.02 0.627 06/11/13 21:57
Anthracene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Azobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzo(a)Anthracene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzo[a]pyrene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzo[b]Fluoranthene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzo[g,h,i]perylene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzo[k]fluoranthene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Benzoic acid 1.52 mg/Kg 1U 1.52 0.759 06/11/13 21:57
Benzyl alcohol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Bis(2-Chloroethoxy)methane 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Bis(2-Chloroethyl)ether 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
bis(2-Ethylhexyl)phthalate 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C207
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Semivolatile Organic GC/MS
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Butylbenzylphthalate 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Carbazole 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Chrysene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Di-n-butylphthalate 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
di-n-Octylphthalate 0.506 mg/Kg 1U 0.506 0.152 06/11/13 21:57
Dibenzo[a,h]anthracene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Dibenzofuran 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Diethylphthalate 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Dimethylphthalate 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Fluoranthene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Fluorene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Hexachlorobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Hexachlorobutadiene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Hexachlorocyclopentadiene 0.708 mg/Kg 1U 0.708 0.202 06/11/13 21:57
Hexachloroethane 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Indeno[1,2,3-c,d] pyrene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Isophorone 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
N-Nitroso-di-n-propylamine 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
N-Nitrosodimethylamine 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
N-Nitrosodiphenylamine 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Naphthalene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Nitrobenzene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Pentachlorophenol 2.02 mg/Kg 1U 2.02 0.627 06/11/13 21:57
Phenanthrene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Phenol 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Pyrene 0.253 mg/Kg 1U 0.253 0.0789 06/11/13 21:57
Surrogates
2,4,6-Tribromophenol 98.3 % 135-125 06/11/13 21:57
2-Fluorobiphenyl 89.6 % 145-105 06/11/13 21:57
2-Fluorophenol 65.4 % 135-105 06/11/13 21:57
Nitrobenzene-d5 65.4 % 135-100 06/11/13 21:57
Phenol-d6 77.5 % 140-100 06/11/13 21:57
Terphenyl-d14 102 % 130-125 06/11/13 21:57
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.658 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 21:57
Container ID: 1132110006-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C208
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Volatile Fuels
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.61 mg/Kg 1U 2.61 0.784 06/05/13 19:50
Surrogates
4-Bromofluorobenzene 93.6 % 150-150 06/05/13 19:50
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 15:52
Prep Initial Wt./Vol.: 50.488 g
Prep Extract Vol: 25.9151 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 19:50
Container ID: 1132110006-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C209
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Volatile GC/MS
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,1,1-Trichloroethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,1,2,2-Tetrachloroethane 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
1,1,2-Trichloroethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,1-Dichloroethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,1-Dichloroethene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,1-Dichloropropene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2,3-Trichlorobenzene 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
1,2,3-Trichloropropane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2,4-Trichlorobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2,4-Trimethylbenzene 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
1,2-Dibromo-3-chloropropane 105 ug/Kg 1U 105 32.4 06/03/13 16:28
1,2-Dibromoethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2-Dichlorobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2-Dichloroethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,2-Dichloropropane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,3,5-Trimethylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,3-Dichlorobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,3-Dichloropropane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
1,4-Dichlorobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
2,2-Dichloropropane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
2-Butanone (MEK) 261 ug/Kg 1U 261 81.6 06/03/13 16:28
2-Chlorotoluene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
2-Hexanone 261 ug/Kg 1U 261 81.6 06/03/13 16:28
4-Chlorotoluene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
4-Isopropyltoluene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
4-Methyl-2-pentanone (MIBK) 261 ug/Kg 1U 261 81.6 06/03/13 16:28
Benzene 13.1 ug/Kg 1U 13.1 4.08 06/03/13 16:28
Bromobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Bromochloromethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Bromodichloromethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Bromoform 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Bromomethane 209 ug/Kg 1U 209 64.8 06/03/13 16:28
Carbon disulfide 105 ug/Kg 1U 105 32.4 06/03/13 16:28
Carbon tetrachloride 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Chlorobenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Chloroethane 209 ug/Kg 1U 209 64.8 06/03/13 16:28
Chloroform 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Chloromethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
cis-1,2-Dichloroethene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
cis-1,3-Dichloropropene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Dibromochloromethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Dibromomethane 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Dichlorodifluoromethane 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C210
Client Sample ID: SMIC-L (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110006
Lab Project ID: 1132110
Collection Date: 05/30/13 15:52
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.2
Results by Volatile GC/MS
Results of SMIC-L (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Hexachlorobutadiene 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
Isopropylbenzene (Cumene) 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Methyl-t-butyl ether 105 ug/Kg 1U 105 32.4 06/03/13 16:28
Methylene chloride 105 ug/Kg 1U 105 32.4 06/03/13 16:28
n-Butylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
n-Propylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Naphthalene 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
o-Xylene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
P & M -Xylene 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
sec-Butylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Styrene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
tert-Butylbenzene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Tetrachloroethene 13.1 ug/Kg 1U 13.1 4.08 06/03/13 16:28
Toluene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
trans-1,2-Dichloroethene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
trans-1,3-Dichloropropene 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Trichloroethene 13.1 ug/Kg 1U 13.1 4.08 06/03/13 16:28
Trichlorofluoromethane 52.3 ug/Kg 1U 52.3 15.7 06/03/13 16:28
Vinyl chloride 26.1 ug/Kg 1U 26.1 8.16 06/03/13 16:28
Xylenes (total) 105 ug/Kg 1U 105 32.4 06/03/13 16:28
Surrogates
1,2-Dichloroethane-D4 119 % 179-118 06/03/13 16:28*4-Bromofluorobenzene 104 % 167-138 06/03/13 16:28
Toluene-d8 109 % 185-115 06/03/13 16:28
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 15:52
Prep Initial Wt./Vol.: 50.488 g
Prep Extract Vol: 25.9151 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 16:28
Container ID: 1132110006-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C211
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Metals by ICP/MS
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.04 mg/Kg 101.14 0.355 06/04/13 17:56
Barium 40.7 mg/Kg 100.343 0.108 06/04/13 17:56
Cadmium 0.229 mg/Kg 10U 0.229 0.0709 06/04/13 17:56
Chromium 34.8 mg/Kg 100.458 0.137 06/04/13 17:56
Lead 6.24 mg/Kg 100.229 0.0709 06/04/13 17:56
Mercury 0.0458 mg/Kg 10U 0.0458 0.0137 06/04/13 17:56
Selenium 0.572 mg/Kg 10U 0.572 0.172 06/04/13 17:56
Silver 0.114 mg/Kg 10U 0.114 0.0355 06/04/13 17:56
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.042 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:56
Container ID: 1132110007-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C212
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Semivolatile Organic Fuels
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 23.3 mg/Kg 1U 23.3 7.21 06/08/13 20:48
Surrogates
5a Androstane 112 % 150-150 06/08/13 20:48
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.726 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:48
Container ID: 1132110007-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 23.3 mg/Kg 1U 23.3 7.21 06/08/13 20:48
Surrogates
n-Triacontane-d62 133 % 150-150 06/08/13 20:48
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.726 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:48
Container ID: 1132110007-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C213
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Semivolatile Organic GC/MS
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
1,2-Dichlorobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
1,3-Dichlorobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
1,4-Dichlorobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
1-Chloronaphthalene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,4,5-Trichlorophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,4,6-Trichlorophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,4-Dichlorophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,4-Dimethylphenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,4-Dinitrophenol 3.55 mg/Kg 1U 3.55 1.11 06/11/13 22:14
2,4-Dinitrotoluene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,6-Dichlorophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2,6-Dinitrotoluene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Chloronaphthalene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Chlorophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Methyl-4,6-dinitrophenol 2.36 mg/Kg 1U 2.36 0.733 06/11/13 22:14
2-Methylnaphthalene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Methylphenol (o-Cresol) 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Nitroaniline 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
2-Nitrophenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
3&4-Methylphenol (p&m-Cresol) 1.18 mg/Kg 1U 1.18 0.366 06/11/13 22:14
3,3-Dichlorobenzidine 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
3-Nitroaniline 0.591 mg/Kg 1U 0.591 0.177 06/11/13 22:14
4-Bromophenyl-phenylether 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
4-Chloro-3-methylphenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
4-Chloroaniline 0.591 mg/Kg 1U 0.591 0.177 06/11/13 22:14
4-Chlorophenyl-phenylether 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
4-Nitroaniline 3.55 mg/Kg 1U 3.55 1.11 06/11/13 22:14
4-Nitrophenol 1.18 mg/Kg 1U 1.18 0.366 06/11/13 22:14
Acenaphthene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Acenaphthylene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Aniline 2.36 mg/Kg 1U 2.36 0.733 06/11/13 22:14
Anthracene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Azobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzo(a)Anthracene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzo[a]pyrene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzo[b]Fluoranthene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzo[g,h,i]perylene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzo[k]fluoranthene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Benzoic acid 1.77 mg/Kg 1U 1.77 0.887 06/11/13 22:14
Benzyl alcohol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Bis(2-Chloroethoxy)methane 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Bis(2-Chloroethyl)ether 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
bis(2-Ethylhexyl)phthalate 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C214
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Semivolatile Organic GC/MS
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Butylbenzylphthalate 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Carbazole 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Chrysene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Di-n-butylphthalate 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
di-n-Octylphthalate 0.591 mg/Kg 1U 0.591 0.177 06/11/13 22:14
Dibenzo[a,h]anthracene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Dibenzofuran 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Diethylphthalate 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Dimethylphthalate 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Fluoranthene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Fluorene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Hexachlorobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Hexachlorobutadiene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Hexachlorocyclopentadiene 0.828 mg/Kg 1U 0.828 0.236 06/11/13 22:14
Hexachloroethane 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Indeno[1,2,3-c,d] pyrene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Isophorone 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
N-Nitroso-di-n-propylamine 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
N-Nitrosodimethylamine 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
N-Nitrosodiphenylamine 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Naphthalene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Nitrobenzene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Pentachlorophenol 2.36 mg/Kg 1U 2.36 0.733 06/11/13 22:14
Phenanthrene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Phenol 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Pyrene 0.296 mg/Kg 1U 0.296 0.0922 06/11/13 22:14
Surrogates
2,4,6-Tribromophenol 95.9 % 135-125 06/11/13 22:14
2-Fluorobiphenyl 89.1 % 145-105 06/11/13 22:14
2-Fluorophenol 64.1 % 135-105 06/11/13 22:14
Nitrobenzene-d5 64 % 135-100 06/11/13 22:14
Phenol-d6 72.7 % 140-100 06/11/13 22:14
Terphenyl-d14 102 % 130-125 06/11/13 22:14
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.683 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 22:14
Container ID: 1132110007-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C215
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Volatile Fuels
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.87 mg/Kg 1U 2.87 0.862 06/05/13 20:09
Surrogates
4-Bromofluorobenzene 104 % 150-150 06/05/13 20:09
Batch Information
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 05/30/13 16:13
Prep Initial Wt./Vol.: 77.886 g
Prep Extract Vol: 37.5343 mL
Analytical Batch: VFC11449
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 20:09
Container ID: 1132110007-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C216
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Volatile GC/MS
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,1,1-Trichloroethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,1,2,2-Tetrachloroethane 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
1,1,2-Trichloroethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,1-Dichloroethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,1-Dichloroethene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,1-Dichloropropene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2,3-Trichlorobenzene 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
1,2,3-Trichloropropane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2,4-Trichlorobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2,4-Trimethylbenzene 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
1,2-Dibromo-3-chloropropane 115 ug/Kg 1U 115 35.6 06/03/13 16:44
1,2-Dibromoethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2-Dichlorobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2-Dichloroethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,2-Dichloropropane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,3,5-Trimethylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,3-Dichlorobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,3-Dichloropropane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
1,4-Dichlorobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
2,2-Dichloropropane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
2-Butanone (MEK) 287 ug/Kg 1U 287 89.6 06/03/13 16:44
2-Chlorotoluene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
2-Hexanone 287 ug/Kg 1U 287 89.6 06/03/13 16:44
4-Chlorotoluene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
4-Isopropyltoluene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
4-Methyl-2-pentanone (MIBK) 287 ug/Kg 1U 287 89.6 06/03/13 16:44
Benzene 14.4 ug/Kg 1U 14.4 4.48 06/03/13 16:44
Bromobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Bromochloromethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Bromodichloromethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Bromoform 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Bromomethane 230 ug/Kg 1U 230 71.2 06/03/13 16:44
Carbon disulfide 115 ug/Kg 1U 115 35.6 06/03/13 16:44
Carbon tetrachloride 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Chlorobenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Chloroethane 230 ug/Kg 1U 230 71.2 06/03/13 16:44
Chloroform 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Chloromethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
cis-1,2-Dichloroethene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
cis-1,3-Dichloropropene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Dibromochloromethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Dibromomethane 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Dichlorodifluoromethane 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C217
Client Sample ID: SMIC-L (15)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110007
Lab Project ID: 1132110
Collection Date: 05/30/13 16:13
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 83.9
Results by Volatile GC/MS
Results of SMIC-L (15)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Hexachlorobutadiene 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
Isopropylbenzene (Cumene) 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Methyl-t-butyl ether 115 ug/Kg 1U 115 35.6 06/03/13 16:44
Methylene chloride 115 ug/Kg 1U 115 35.6 06/03/13 16:44
n-Butylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
n-Propylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Naphthalene 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
o-Xylene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
P & M -Xylene 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
sec-Butylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Styrene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
tert-Butylbenzene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Tetrachloroethene 14.4 ug/Kg 1U 14.4 4.48 06/03/13 16:44
Toluene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
trans-1,2-Dichloroethene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
trans-1,3-Dichloropropene 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Trichloroethene 14.4 ug/Kg 1U 14.4 4.48 06/03/13 16:44
Trichlorofluoromethane 57.4 ug/Kg 1U 57.4 17.2 06/03/13 16:44
Vinyl chloride 28.7 ug/Kg 1U 28.7 8.96 06/03/13 16:44
Xylenes (total) 115 ug/Kg 1U 115 35.6 06/03/13 16:44
Surrogates
1,2-Dichloroethane-D4 114 % 179-118 06/03/13 16:44
4-Bromofluorobenzene 103 % 167-138 06/03/13 16:44
Toluene-d8 104 % 185-115 06/03/13 16:44
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 16:13
Prep Initial Wt./Vol.: 77.886 g
Prep Extract Vol: 37.5343 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 16:44
Container ID: 1132110007-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C218
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Metals by ICP/MS
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 6.57 mg/Kg 101.07 0.332 06/04/13 17:59
Barium 46.2 mg/Kg 100.321 0.101 06/04/13 17:59
Cadmium 0.214 mg/Kg 10U 0.214 0.0664 06/04/13 17:59
Chromium 35.3 mg/Kg 100.428 0.128 06/04/13 17:59
Lead 7.27 mg/Kg 100.214 0.0664 06/04/13 17:59
Mercury 0.0428 mg/Kg 10U 0.0428 0.0128 06/04/13 17:59
Selenium 0.535 mg/Kg 10U 0.535 0.161 06/04/13 17:59
Silver 0.107 mg/Kg 10U 0.107 0.0332 06/04/13 17:59
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.055 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 17:59
Container ID: 1132110008-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C219
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Semivolatile Organic Fuels
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.4 mg/Kg 1U 22.4 6.94 06/08/13 20:57
Surrogates
5a Androstane 104 % 150-150 06/08/13 20:57
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.266 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 20:57
Container ID: 1132110008-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.4 mg/Kg 1U 22.4 6.94 06/08/13 20:57
Surrogates
n-Triacontane-d62 122 % 150-150 06/08/13 20:57
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.266 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 20:57
Container ID: 1132110008-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C220
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Semivolatile Organic GC/MS
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
1,2-Dichlorobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
1,3-Dichlorobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
1,4-Dichlorobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
1-Chloronaphthalene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,4,5-Trichlorophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,4,6-Trichlorophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,4-Dichlorophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,4-Dimethylphenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,4-Dinitrophenol 3.34 mg/Kg 1U 3.34 1.05 06/11/13 22:31
2,4-Dinitrotoluene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,6-Dichlorophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2,6-Dinitrotoluene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Chloronaphthalene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Chlorophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Methyl-4,6-dinitrophenol 2.23 mg/Kg 1U 2.23 0.690 06/11/13 22:31
2-Methylnaphthalene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Methylphenol (o-Cresol) 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Nitroaniline 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
2-Nitrophenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
3&4-Methylphenol (p&m-Cresol) 1.11 mg/Kg 1U 1.11 0.345 06/11/13 22:31
3,3-Dichlorobenzidine 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
3-Nitroaniline 0.556 mg/Kg 1U 0.556 0.167 06/11/13 22:31
4-Bromophenyl-phenylether 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
4-Chloro-3-methylphenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
4-Chloroaniline 0.556 mg/Kg 1U 0.556 0.167 06/11/13 22:31
4-Chlorophenyl-phenylether 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
4-Nitroaniline 3.34 mg/Kg 1U 3.34 1.05 06/11/13 22:31
4-Nitrophenol 1.11 mg/Kg 1U 1.11 0.345 06/11/13 22:31
Acenaphthene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Acenaphthylene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Aniline 2.23 mg/Kg 1U 2.23 0.690 06/11/13 22:31
Anthracene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Azobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzo(a)Anthracene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzo[a]pyrene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzo[b]Fluoranthene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzo[g,h,i]perylene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzo[k]fluoranthene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Benzoic acid 1.67 mg/Kg 1U 1.67 0.834 06/11/13 22:31
Benzyl alcohol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Bis(2-Chloroethoxy)methane 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Bis(2-Chloroethyl)ether 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
bis(2-Ethylhexyl)phthalate 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C221
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Semivolatile Organic GC/MS
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Butylbenzylphthalate 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Carbazole 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Chrysene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Di-n-butylphthalate 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
di-n-Octylphthalate 0.556 mg/Kg 1U 0.556 0.167 06/11/13 22:31
Dibenzo[a,h]anthracene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Dibenzofuran 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Diethylphthalate 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Dimethylphthalate 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Fluoranthene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Fluorene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Hexachlorobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Hexachlorobutadiene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Hexachlorocyclopentadiene 0.779 mg/Kg 1U 0.779 0.223 06/11/13 22:31
Hexachloroethane 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Indeno[1,2,3-c,d] pyrene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Isophorone 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
N-Nitroso-di-n-propylamine 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
N-Nitrosodimethylamine 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
N-Nitrosodiphenylamine 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Naphthalene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Nitrobenzene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Pentachlorophenol 2.23 mg/Kg 1U 2.23 0.690 06/11/13 22:31
Phenanthrene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Phenol 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Pyrene 0.278 mg/Kg 1U 0.278 0.0868 06/11/13 22:31
Surrogates
2,4,6-Tribromophenol 101 % 135-125 06/11/13 22:31
2-Fluorobiphenyl 88.6 % 145-105 06/11/13 22:31
2-Fluorophenol 63.3 % 135-105 06/11/13 22:31
Nitrobenzene-d5 67.6 % 135-100 06/11/13 22:31
Phenol-d6 73.3 % 140-100 06/11/13 22:31
Terphenyl-d14 102 % 130-125 06/11/13 22:31
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.844 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 22:31
Container ID: 1132110008-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C222
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Volatile Fuels
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.74 mg/Kg 1U 2.74 0.822 06/06/13 21:06
Surrogates
4-Bromofluorobenzene 105 % 150-150 06/06/13 21:06
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/30/13 16:54
Prep Initial Wt./Vol.: 67.516 g
Prep Extract Vol: 32.7421 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 21:06
Container ID: 1132110008-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C223
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Volatile GC/MS
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,1,1-Trichloroethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,1,2,2-Tetrachloroethane 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
1,1,2-Trichloroethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,1-Dichloroethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,1-Dichloroethene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,1-Dichloropropene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2,3-Trichlorobenzene 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
1,2,3-Trichloropropane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2,4-Trichlorobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2,4-Trimethylbenzene 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
1,2-Dibromo-3-chloropropane 110 ug/Kg 1U 110 34.0 06/03/13 17:01
1,2-Dibromoethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2-Dichlorobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2-Dichloroethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,2-Dichloropropane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,3,5-Trimethylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,3-Dichlorobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,3-Dichloropropane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
1,4-Dichlorobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
2,2-Dichloropropane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
2-Butanone (MEK) 274 ug/Kg 1U 274 85.5 06/03/13 17:01
2-Chlorotoluene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
2-Hexanone 274 ug/Kg 1U 274 85.5 06/03/13 17:01
4-Chlorotoluene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
4-Isopropyltoluene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
4-Methyl-2-pentanone (MIBK) 274 ug/Kg 1U 274 85.5 06/03/13 17:01
Benzene 13.7 ug/Kg 1U 13.7 4.27 06/03/13 17:01
Bromobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Bromochloromethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Bromodichloromethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Bromoform 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Bromomethane 219 ug/Kg 1U 219 67.9 06/03/13 17:01
Carbon disulfide 110 ug/Kg 1U 110 34.0 06/03/13 17:01
Carbon tetrachloride 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Chlorobenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Chloroethane 219 ug/Kg 1U 219 67.9 06/03/13 17:01
Chloroform 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Chloromethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
cis-1,2-Dichloroethene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
cis-1,3-Dichloropropene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Dibromochloromethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Dibromomethane 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Dichlorodifluoromethane 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C224
Client Sample ID: SMIC-L (35)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110008
Lab Project ID: 1132110
Collection Date: 05/30/13 16:54
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 88.5
Results by Volatile GC/MS
Results of SMIC-L (35)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Hexachlorobutadiene 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
Isopropylbenzene (Cumene) 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Methyl-t-butyl ether 110 ug/Kg 1U 110 34.0 06/03/13 17:01
Methylene chloride 110 ug/Kg 1U 110 34.0 06/03/13 17:01
n-Butylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
n-Propylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Naphthalene 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
o-Xylene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
P & M -Xylene 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
sec-Butylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Styrene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
tert-Butylbenzene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Tetrachloroethene 13.7 ug/Kg 1U 13.7 4.27 06/03/13 17:01
Toluene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
trans-1,2-Dichloroethene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
trans-1,3-Dichloropropene 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Trichloroethene 13.7 ug/Kg 1U 13.7 4.27 06/03/13 17:01
Trichlorofluoromethane 54.8 ug/Kg 1U 54.8 16.4 06/03/13 17:01
Vinyl chloride 27.4 ug/Kg 1U 27.4 8.55 06/03/13 17:01
Xylenes (total) 110 ug/Kg 1U 110 34.0 06/03/13 17:01
Surrogates
1,2-Dichloroethane-D4 116 % 179-118 06/03/13 17:01
4-Bromofluorobenzene 105 % 167-138 06/03/13 17:01
Toluene-d8 105 % 185-115 06/03/13 17:01
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 16:54
Prep Initial Wt./Vol.: 67.516 g
Prep Extract Vol: 32.7421 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 17:01
Container ID: 1132110008-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C225
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Metals by ICP/MS
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 7.43 mg/Kg 100.941 0.292 06/04/13 18:01
Barium 28.7 mg/Kg 100.282 0.0885 06/04/13 18:01
Cadmium 0.188 mg/Kg 10U 0.188 0.0584 06/04/13 18:01
Chromium 41.3 mg/Kg 100.377 0.113 06/04/13 18:01
Lead 8.46 mg/Kg 100.188 0.0584 06/04/13 18:01
Mercury 0.0745 mg/Kg 100.0377 0.0113 06/04/13 18:01
Selenium 0.471 mg/Kg 10U 0.471 0.141 06/04/13 18:01
Silver 0.0941 mg/Kg 10U 0.0941 0.0292 06/04/13 18:01
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.091 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:01
Container ID: 1132110009-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C226
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic Fuels
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.3 mg/Kg 1U 20.3 6.30 06/08/13 21:07
Surrogates
5a Androstane 125 % 150-150 06/08/13 21:07
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.317 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:07
Container ID: 1132110009-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 20.3 mg/Kg 1U 20.3 6.30 06/08/13 21:07
Surrogates
n-Triacontane-d62 148 % 150-150 06/08/13 21:07
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.317 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:07
Container ID: 1132110009-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C227
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,4-Dinitrophenol 3.05 mg/Kg 1U 3.05 0.955 06/11/13 22:48
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 22:48
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.315 06/11/13 22:48
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
3-Nitroaniline 0.508 mg/Kg 1U 0.508 0.152 06/11/13 22:48
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
4-Chloroaniline 0.508 mg/Kg 1U 0.508 0.152 06/11/13 22:48
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
4-Nitroaniline 3.05 mg/Kg 1U 3.05 0.955 06/11/13 22:48
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.315 06/11/13 22:48
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Aniline 2.03 mg/Kg 1U 2.03 0.630 06/11/13 22:48
Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Azobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Benzoic acid 1.52 mg/Kg 1U 1.52 0.762 06/11/13 22:48
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C228
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Carbazole 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Chrysene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
di-n-Octylphthalate 0.508 mg/Kg 1U 0.508 0.152 06/11/13 22:48
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Fluorene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Hexachlorocyclopentadiene 0.711 mg/Kg 1U 0.711 0.203 06/11/13 22:48
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Isophorone 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Naphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 22:48
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Phenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 22:48
Surrogates
2,4,6-Tribromophenol 89.9 % 135-125 06/11/13 22:48
2-Fluorobiphenyl 88 % 145-105 06/11/13 22:48
2-Fluorophenol 61.5 % 135-105 06/11/13 22:48
Nitrobenzene-d5 66.8 % 135-100 06/11/13 22:48
Phenol-d6 70.2 % 140-100 06/11/13 22:48
Terphenyl-d14 101 % 130-125 06/11/13 22:48
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.749 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 22:48
Container ID: 1132110009-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C229
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile Fuels
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.19 mg/Kg 1U 2.19 0.656 06/06/13 21:25
Surrogates
4-Bromofluorobenzene 89.4 % 150-150 06/06/13 21:25
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:44
Prep Initial Wt./Vol.: 62.588 g
Prep Extract Vol: 26.642 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 21:25
Container ID: 1132110009-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C230
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,1,1-Trichloroethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,1,2,2-Tetrachloroethane 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
1,1,2-Trichloroethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,1-Dichloroethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,1-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,1-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2,3-Trichlorobenzene 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
1,2,3-Trichloropropane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2,4-Trichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2,4-Trimethylbenzene 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
1,2-Dibromo-3-chloropropane 87.4 ug/Kg 1U 87.4 27.1 06/03/13 17:18
1,2-Dibromoethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2-Dichloroethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,2-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,3,5-Trimethylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,3-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,3-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
1,4-Dichlorobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
2,2-Dichloropropane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
2-Butanone (MEK) 219 ug/Kg 1U 219 68.2 06/03/13 17:18
2-Chlorotoluene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
2-Hexanone 219 ug/Kg 1U 219 68.2 06/03/13 17:18
4-Chlorotoluene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
4-Isopropyltoluene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
4-Methyl-2-pentanone (MIBK) 219 ug/Kg 1U 219 68.2 06/03/13 17:18
Benzene 10.9 ug/Kg 1U 10.9 3.41 06/03/13 17:18
Bromobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Bromochloromethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Bromodichloromethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Bromoform 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Bromomethane 175 ug/Kg 1U 175 54.2 06/03/13 17:18
Carbon disulfide 87.4 ug/Kg 1U 87.4 27.1 06/03/13 17:18
Carbon tetrachloride 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Chlorobenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Chloroethane 175 ug/Kg 1U 175 54.2 06/03/13 17:18
Chloroform 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Chloromethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
cis-1,2-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
cis-1,3-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Dibromochloromethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Dibromomethane 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Dichlorodifluoromethane 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C231
Client Sample ID: SMIC-O (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110009
Lab Project ID: 1132110
Collection Date: 05/31/13 08:44
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-O (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Hexachlorobutadiene 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
Isopropylbenzene (Cumene) 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Methyl-t-butyl ether 87.4 ug/Kg 1U 87.4 27.1 06/03/13 17:18
Methylene chloride 87.4 ug/Kg 1U 87.4 27.1 06/03/13 17:18
n-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
n-Propylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Naphthalene 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
o-Xylene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
P & M -Xylene 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
sec-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Styrene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
tert-Butylbenzene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Tetrachloroethene 10.9 ug/Kg 1U 10.9 3.41 06/03/13 17:18
Toluene 68.0 ug/Kg 121.9 6.82 06/03/13 17:18
trans-1,2-Dichloroethene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
trans-1,3-Dichloropropene 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Trichloroethene 10.9 ug/Kg 1U 10.9 3.41 06/03/13 17:18
Trichlorofluoromethane 43.7 ug/Kg 1U 43.7 13.1 06/03/13 17:18
Vinyl chloride 21.9 ug/Kg 1U 21.9 6.82 06/03/13 17:18
Xylenes (total) 87.4 ug/Kg 1U 87.4 27.1 06/03/13 17:18
Surrogates
1,2-Dichloroethane-D4 116 % 179-118 06/03/13 17:18
4-Bromofluorobenzene 93.1 % 167-138 06/03/13 17:18
Toluene-d8 104 % 185-115 06/03/13 17:18
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:44
Prep Initial Wt./Vol.: 62.588 g
Prep Extract Vol: 26.642 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 17:18
Container ID: 1132110009-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C232
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Metals by ICP/MS
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 7.46 mg/Kg 100.970 0.301 06/04/13 18:03
Barium 30.3 mg/Kg 100.291 0.0912 06/04/13 18:03
Cadmium 0.194 mg/Kg 10U 0.194 0.0602 06/04/13 18:03
Chromium 44.1 mg/Kg 100.388 0.116 06/04/13 18:03
Lead 8.33 mg/Kg 100.194 0.0602 06/04/13 18:03
Mercury 0.0861 mg/Kg 100.0388 0.0116 06/04/13 18:03
Selenium 0.485 mg/Kg 10U 0.485 0.146 06/04/13 18:03
Silver 0.0970 mg/Kg 10U 0.0970 0.0301 06/04/13 18:03
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.058 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:03
Container ID: 1132110010-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C233
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic Fuels
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.2 mg/Kg 1U 20.2 6.28 06/08/13 21:16
Surrogates
5a Androstane 101 % 150-150 06/08/13 21:16
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.423 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:16
Container ID: 1132110010-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 20.2 mg/Kg 1U 20.2 6.28 06/08/13 21:16
Surrogates
n-Triacontane-d62 117 % 150-150 06/08/13 21:16
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.423 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:16
Container ID: 1132110010-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C234
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
1,2-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
1,3-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
1,4-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
1-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,4,5-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,4,6-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,4-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,4-Dimethylphenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,4-Dinitrophenol 3.06 mg/Kg 1U 3.06 0.960 06/11/13 23:05
2,4-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,6-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2,6-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Chlorophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Methyl-4,6-dinitrophenol 2.04 mg/Kg 1U 2.04 0.633 06/11/13 23:05
2-Methylnaphthalene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Methylphenol (o-Cresol) 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Nitroaniline 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
2-Nitrophenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.317 06/11/13 23:05
3,3-Dichlorobenzidine 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
3-Nitroaniline 0.511 mg/Kg 1U 0.511 0.153 06/11/13 23:05
4-Bromophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
4-Chloro-3-methylphenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
4-Chloroaniline 0.511 mg/Kg 1U 0.511 0.153 06/11/13 23:05
4-Chlorophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
4-Nitroaniline 3.06 mg/Kg 1U 3.06 0.960 06/11/13 23:05
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.317 06/11/13 23:05
Acenaphthene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Acenaphthylene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Aniline 2.04 mg/Kg 1U 2.04 0.633 06/11/13 23:05
Anthracene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Azobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzo(a)Anthracene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzo[a]pyrene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzo[b]Fluoranthene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzo[g,h,i]perylene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzo[k]fluoranthene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Benzoic acid 1.53 mg/Kg 1U 1.53 0.766 06/11/13 23:05
Benzyl alcohol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Bis(2-Chloroethoxy)methane 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Bis(2-Chloroethyl)ether 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
bis(2-Ethylhexyl)phthalate 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C235
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Butylbenzylphthalate 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Carbazole 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Chrysene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Di-n-butylphthalate 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
di-n-Octylphthalate 0.511 mg/Kg 1U 0.511 0.153 06/11/13 23:05
Dibenzo[a,h]anthracene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Dibenzofuran 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Diethylphthalate 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Dimethylphthalate 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Fluoranthene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Fluorene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Hexachlorobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Hexachlorobutadiene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Hexachlorocyclopentadiene 0.715 mg/Kg 1U 0.715 0.204 06/11/13 23:05
Hexachloroethane 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Indeno[1,2,3-c,d] pyrene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Isophorone 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
N-Nitroso-di-n-propylamine 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
N-Nitrosodimethylamine 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
N-Nitrosodiphenylamine 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Naphthalene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Nitrobenzene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Pentachlorophenol 2.04 mg/Kg 1U 2.04 0.633 06/11/13 23:05
Phenanthrene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Phenol 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Pyrene 0.255 mg/Kg 1U 0.255 0.0797 06/11/13 23:05
Surrogates
2,4,6-Tribromophenol 89.6 % 135-125 06/11/13 23:05
2-Fluorobiphenyl 90.4 % 145-105 06/11/13 23:05
2-Fluorophenol 61.1 % 135-105 06/11/13 23:05
Nitrobenzene-d5 67.7 % 135-100 06/11/13 23:05
Phenol-d6 72 % 140-100 06/11/13 23:05
Terphenyl-d14 100 % 130-125 06/11/13 23:05
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.608 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 23:05
Container ID: 1132110010-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C236
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile Fuels
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.80 mg/Kg 1U 2.80 0.840 06/06/13 21:44
Surrogates
4-Bromofluorobenzene 91.1 % 150-150 06/06/13 21:44
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:47
Prep Initial Wt./Vol.: 48.087 g
Prep Extract Vol: 26.2386 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 21:44
Container ID: 1132110010-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C237
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,1,1-Trichloroethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,1,2,2-Tetrachloroethane 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
1,1,2-Trichloroethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,1-Dichloroethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,1-Dichloroethene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,1-Dichloropropene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2,3-Trichlorobenzene 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
1,2,3-Trichloropropane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2,4-Trichlorobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2,4-Trimethylbenzene 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
1,2-Dibromo-3-chloropropane 112 ug/Kg 1U 112 34.7 06/03/13 17:35
1,2-Dibromoethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2-Dichloroethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,2-Dichloropropane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,3,5-Trimethylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,3-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,3-Dichloropropane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
1,4-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
2,2-Dichloropropane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
2-Butanone (MEK) 280 ug/Kg 1U 280 87.4 06/03/13 17:35
2-Chlorotoluene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
2-Hexanone 280 ug/Kg 1U 280 87.4 06/03/13 17:35
4-Chlorotoluene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
4-Isopropyltoluene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
4-Methyl-2-pentanone (MIBK) 280 ug/Kg 1U 280 87.4 06/03/13 17:35
Benzene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 17:35
Bromobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Bromochloromethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Bromodichloromethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Bromoform 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Bromomethane 224 ug/Kg 1U 224 69.4 06/03/13 17:35
Carbon disulfide 112 ug/Kg 1U 112 34.7 06/03/13 17:35
Carbon tetrachloride 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Chlorobenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Chloroethane 224 ug/Kg 1U 224 69.4 06/03/13 17:35
Chloroform 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Chloromethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
cis-1,2-Dichloroethene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
cis-1,3-Dichloropropene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Dibromochloromethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Dibromomethane 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Dichlorodifluoromethane 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C238
Client Sample ID: SMIC-O (0) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110010
Lab Project ID: 1132110
Collection Date: 05/31/13 08:47
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-O (0) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Hexachlorobutadiene 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
Isopropylbenzene (Cumene) 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Methyl-t-butyl ether 112 ug/Kg 1U 112 34.7 06/03/13 17:35
Methylene chloride 112 ug/Kg 1U 112 34.7 06/03/13 17:35
n-Butylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
n-Propylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Naphthalene 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
o-Xylene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
P & M -Xylene 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
sec-Butylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Styrene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
tert-Butylbenzene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Tetrachloroethene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 17:35
Toluene 64.7 ug/Kg 128.0 8.74 06/03/13 17:35
trans-1,2-Dichloroethene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
trans-1,3-Dichloropropene 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Trichloroethene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 17:35
Trichlorofluoromethane 56.0 ug/Kg 1U 56.0 16.8 06/03/13 17:35
Vinyl chloride 28.0 ug/Kg 1U 28.0 8.74 06/03/13 17:35
Xylenes (total) 112 ug/Kg 1U 112 34.7 06/03/13 17:35
Surrogates
1,2-Dichloroethane-D4 115 % 179-118 06/03/13 17:35
4-Bromofluorobenzene 94.7 % 167-138 06/03/13 17:35
Toluene-d8 105 % 185-115 06/03/13 17:35
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:47
Prep Initial Wt./Vol.: 48.087 g
Prep Extract Vol: 26.2386 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 17:35
Container ID: 1132110010-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C239
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Metals by ICP/MS
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 6.77 mg/Kg 101.01 0.314 06/04/13 18:05
Barium 34.2 mg/Kg 100.304 0.0952 06/04/13 18:05
Cadmium 0.203 mg/Kg 10U 0.203 0.0628 06/04/13 18:05
Chromium 39.8 mg/Kg 100.405 0.122 06/04/13 18:05
Lead 9.30 mg/Kg 100.203 0.0628 06/04/13 18:05
Mercury 0.0591 mg/Kg 100.0405 0.0122 06/04/13 18:05
Selenium 0.506 mg/Kg 10U 0.506 0.152 06/04/13 18:05
Silver 0.101 mg/Kg 10U 0.101 0.0314 06/04/13 18:05
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.02 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:05
Container ID: 1132110011-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C240
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Semivolatile Organic Fuels
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.6 mg/Kg 1U 20.6 6.39 06/08/13 21:26
Surrogates
5a Androstane 111 % 150-150 06/08/13 21:26
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.054 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:26
Container ID: 1132110011-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 39.2 mg/Kg 120.6 6.39 06/08/13 21:26
Surrogates
n-Triacontane-d62 134 % 150-150 06/08/13 21:26
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.054 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:26
Container ID: 1132110011-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C241
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Semivolatile Organic GC/MS
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,4-Dinitrophenol 3.05 mg/Kg 1U 3.05 0.955 06/11/13 23:22
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 23:22
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.315 06/11/13 23:22
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
3-Nitroaniline 0.508 mg/Kg 1U 0.508 0.152 06/11/13 23:22
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
4-Chloroaniline 0.508 mg/Kg 1U 0.508 0.152 06/11/13 23:22
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
4-Nitroaniline 3.05 mg/Kg 1U 3.05 0.955 06/11/13 23:22
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.315 06/11/13 23:22
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Aniline 2.03 mg/Kg 1U 2.03 0.630 06/11/13 23:22
Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Azobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Benzoic acid 1.52 mg/Kg 1U 1.52 0.762 06/11/13 23:22
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C242
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Semivolatile Organic GC/MS
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Carbazole 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Chrysene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
di-n-Octylphthalate 0.508 mg/Kg 1U 0.508 0.152 06/11/13 23:22
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Fluorene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Hexachlorocyclopentadiene 0.711 mg/Kg 1U 0.711 0.203 06/11/13 23:22
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Isophorone 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Naphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 23:22
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Phenol 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/11/13 23:22
Surrogates
2,4,6-Tribromophenol 93.4 % 135-125 06/11/13 23:22
2-Fluorobiphenyl 87.7 % 145-105 06/11/13 23:22
2-Fluorophenol 62.3 % 135-105 06/11/13 23:22
Nitrobenzene-d5 65.9 % 135-100 06/11/13 23:22
Phenol-d6 71.3 % 140-100 06/11/13 23:22
Terphenyl-d14 100 % 130-125 06/11/13 23:22
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.888 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 23:22
Container ID: 1132110011-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C243
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Volatile Fuels
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.94 mg/Kg 1U 2.94 0.883 06/06/13 22:02
Surrogates
4-Bromofluorobenzene 86.9 % 150-150 06/06/13 22:02
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:55
Prep Initial Wt./Vol.: 46.486 g
Prep Extract Vol: 26.4963 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 22:02
Container ID: 1132110011-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C244
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Volatile GC/MS
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,1,1-Trichloroethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,1,2,2-Tetrachloroethane 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
1,1,2-Trichloroethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,1-Dichloroethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,1-Dichloroethene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,1-Dichloropropene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2,3-Trichlorobenzene 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
1,2,3-Trichloropropane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2,4-Trichlorobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2,4-Trimethylbenzene 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
1,2-Dibromo-3-chloropropane 118 ug/Kg 1U 118 36.5 06/03/13 17:51
1,2-Dibromoethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2-Dichlorobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2-Dichloroethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,2-Dichloropropane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,3,5-Trimethylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,3-Dichlorobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,3-Dichloropropane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
1,4-Dichlorobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
2,2-Dichloropropane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
2-Butanone (MEK) 294 ug/Kg 1U 294 91.9 06/03/13 17:51
2-Chlorotoluene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
2-Hexanone 294 ug/Kg 1U 294 91.9 06/03/13 17:51
4-Chlorotoluene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
4-Isopropyltoluene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
4-Methyl-2-pentanone (MIBK) 294 ug/Kg 1U 294 91.9 06/03/13 17:51
Benzene 14.7 ug/Kg 1U 14.7 4.59 06/03/13 17:51
Bromobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Bromochloromethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Bromodichloromethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Bromoform 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Bromomethane 236 ug/Kg 1U 236 73.0 06/03/13 17:51
Carbon disulfide 118 ug/Kg 1U 118 36.5 06/03/13 17:51
Carbon tetrachloride 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Chlorobenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Chloroethane 236 ug/Kg 1U 236 73.0 06/03/13 17:51
Chloroform 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Chloromethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
cis-1,2-Dichloroethene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
cis-1,3-Dichloropropene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Dibromochloromethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Dibromomethane 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Dichlorodifluoromethane 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C245
Client Sample ID: SMIC-O (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110011
Lab Project ID: 1132110
Collection Date: 05/31/13 08:55
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.8
Results by Volatile GC/MS
Results of SMIC-O (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Hexachlorobutadiene 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
Isopropylbenzene (Cumene) 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Methyl-t-butyl ether 118 ug/Kg 1U 118 36.5 06/03/13 17:51
Methylene chloride 118 ug/Kg 1U 118 36.5 06/03/13 17:51
n-Butylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
n-Propylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Naphthalene 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
o-Xylene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
P & M -Xylene 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
sec-Butylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Styrene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
tert-Butylbenzene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Tetrachloroethene 14.7 ug/Kg 1U 14.7 4.59 06/03/13 17:51
Toluene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
trans-1,2-Dichloroethene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
trans-1,3-Dichloropropene 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Trichloroethene 14.7 ug/Kg 1U 14.7 4.59 06/03/13 17:51
Trichlorofluoromethane 58.9 ug/Kg 1U 58.9 17.7 06/03/13 17:51
Vinyl chloride 29.4 ug/Kg 1U 29.4 9.19 06/03/13 17:51
Xylenes (total) 118 ug/Kg 1U 118 36.5 06/03/13 17:51
Surrogates
1,2-Dichloroethane-D4 111 % 179-118 06/03/13 17:51
4-Bromofluorobenzene 89.2 % 167-138 06/03/13 17:51
Toluene-d8 101 % 185-115 06/03/13 17:51
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 08:55
Prep Initial Wt./Vol.: 46.486 g
Prep Extract Vol: 26.4963 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 17:51
Container ID: 1132110011-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C246
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Metals by ICP/MS
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.46 mg/Kg 100.991 0.307 06/04/13 18:07
Barium 36.3 mg/Kg 100.297 0.0932 06/04/13 18:07
Cadmium 0.198 mg/Kg 10U 0.198 0.0614 06/04/13 18:07
Chromium 33.4 mg/Kg 100.396 0.119 06/04/13 18:07
Lead 4.71 mg/Kg 100.198 0.0614 06/04/13 18:07
Mercury 0.0396 mg/Kg 10U 0.0396 0.0119 06/04/13 18:07
Selenium 0.496 mg/Kg 10U 0.496 0.149 06/04/13 18:07
Silver 0.0991 mg/Kg 10U 0.0991 0.0307 06/04/13 18:07
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.043 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:07
Container ID: 1132110012-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C247
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Semivolatile Organic Fuels
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.4 mg/Kg 1U 20.4 6.33 06/08/13 21:35
Surrogates
5a Androstane 102 % 150-150 06/08/13 21:35
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.376 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:35
Container ID: 1132110012-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 20.4 mg/Kg 1U 20.4 6.33 06/08/13 21:35
Surrogates
n-Triacontane-d62 120 % 150-150 06/08/13 21:35
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.376 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:35
Container ID: 1132110012-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C248
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Semivolatile Organic GC/MS
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
1,2-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
1,3-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
1,4-Dichlorobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
1-Chloronaphthalene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,4,5-Trichlorophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,4,6-Trichlorophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,4-Dichlorophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,4-Dimethylphenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,4-Dinitrophenol 3.09 mg/Kg 1U 3.09 0.968 06/11/13 23:39
2,4-Dinitrotoluene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,6-Dichlorophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2,6-Dinitrotoluene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Chloronaphthalene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Chlorophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Methyl-4,6-dinitrophenol 2.06 mg/Kg 1U 2.06 0.638 06/11/13 23:39
2-Methylnaphthalene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Methylphenol (o-Cresol) 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Nitroaniline 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
2-Nitrophenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
3&4-Methylphenol (p&m-Cresol) 1.03 mg/Kg 1U 1.03 0.319 06/11/13 23:39
3,3-Dichlorobenzidine 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
3-Nitroaniline 0.515 mg/Kg 1U 0.515 0.154 06/11/13 23:39
4-Bromophenyl-phenylether 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
4-Chloro-3-methylphenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
4-Chloroaniline 0.515 mg/Kg 1U 0.515 0.154 06/11/13 23:39
4-Chlorophenyl-phenylether 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
4-Nitroaniline 3.09 mg/Kg 1U 3.09 0.968 06/11/13 23:39
4-Nitrophenol 1.03 mg/Kg 1U 1.03 0.319 06/11/13 23:39
Acenaphthene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Acenaphthylene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Aniline 2.06 mg/Kg 1U 2.06 0.638 06/11/13 23:39
Anthracene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Azobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzo(a)Anthracene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzo[a]pyrene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzo[b]Fluoranthene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzo[g,h,i]perylene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzo[k]fluoranthene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Benzoic acid 1.54 mg/Kg 1U 1.54 0.772 06/11/13 23:39
Benzyl alcohol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Bis(2-Chloroethoxy)methane 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Bis(2-Chloroethyl)ether 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
bis(2-Ethylhexyl)phthalate 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C249
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Semivolatile Organic GC/MS
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Butylbenzylphthalate 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Carbazole 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Chrysene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Di-n-butylphthalate 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
di-n-Octylphthalate 0.515 mg/Kg 1U 0.515 0.154 06/11/13 23:39
Dibenzo[a,h]anthracene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Dibenzofuran 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Diethylphthalate 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Dimethylphthalate 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Fluoranthene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Fluorene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Hexachlorobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Hexachlorobutadiene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Hexachlorocyclopentadiene 0.721 mg/Kg 1U 0.721 0.206 06/11/13 23:39
Hexachloroethane 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Indeno[1,2,3-c,d] pyrene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Isophorone 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
N-Nitroso-di-n-propylamine 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
N-Nitrosodimethylamine 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
N-Nitrosodiphenylamine 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Naphthalene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Nitrobenzene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Pentachlorophenol 2.06 mg/Kg 1U 2.06 0.638 06/11/13 23:39
Phenanthrene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Phenol 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Pyrene 0.257 mg/Kg 1U 0.257 0.0803 06/11/13 23:39
Surrogates
2,4,6-Tribromophenol 94.4 % 135-125 06/11/13 23:39
2-Fluorobiphenyl 86.7 % 145-105 06/11/13 23:39
2-Fluorophenol 62.8 % 135-105 06/11/13 23:39
Nitrobenzene-d5 64.2 % 135-100 06/11/13 23:39
Phenol-d6 70.4 % 140-100 06/11/13 23:39
Terphenyl-d14 94.2 % 130-125 06/11/13 23:39
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.587 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 23:39
Container ID: 1132110012-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C250
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Volatile Fuels
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 3.49 mg/Kg 1U 3.49 1.05 06/06/13 22:21
Surrogates
4-Bromofluorobenzene 101 % 150-150 06/06/13 22:21
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 09:06
Prep Initial Wt./Vol.: 38.921 g
Prep Extract Vol: 26.2675 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 22:21
Container ID: 1132110012-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C251
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Volatile GC/MS
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,1,1-Trichloroethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,1,2,2-Tetrachloroethane 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
1,1,2-Trichloroethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,1-Dichloroethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,1-Dichloroethene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,1-Dichloropropene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2,3-Trichlorobenzene 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
1,2,3-Trichloropropane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2,4-Trichlorobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2,4-Trimethylbenzene 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
1,2-Dibromo-3-chloropropane 140 ug/Kg 1U 140 43.3 06/03/13 18:08
1,2-Dibromoethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2-Dichlorobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2-Dichloroethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,2-Dichloropropane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,3,5-Trimethylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,3-Dichlorobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,3-Dichloropropane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
1,4-Dichlorobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
2,2-Dichloropropane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
2-Butanone (MEK) 349 ug/Kg 1U 349 109 06/03/13 18:08
2-Chlorotoluene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
2-Hexanone 349 ug/Kg 1U 349 109 06/03/13 18:08
4-Chlorotoluene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
4-Isopropyltoluene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
4-Methyl-2-pentanone (MIBK) 349 ug/Kg 1U 349 109 06/03/13 18:08
Benzene 17.4 ug/Kg 1U 17.4 5.44 06/03/13 18:08
Bromobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Bromochloromethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Bromodichloromethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Bromoform 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Bromomethane 279 ug/Kg 1U 279 86.5 06/03/13 18:08
Carbon disulfide 140 ug/Kg 1U 140 43.3 06/03/13 18:08
Carbon tetrachloride 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Chlorobenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Chloroethane 279 ug/Kg 1U 279 86.5 06/03/13 18:08
Chloroform 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Chloromethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
cis-1,2-Dichloroethene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
cis-1,3-Dichloropropene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Dibromochloromethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Dibromomethane 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Dichlorodifluoromethane 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C252
Client Sample ID: SMIC-O (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110012
Lab Project ID: 1132110
Collection Date: 05/31/13 09:06
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.7
Results by Volatile GC/MS
Results of SMIC-O (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Hexachlorobutadiene 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
Isopropylbenzene (Cumene) 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Methyl-t-butyl ether 140 ug/Kg 1U 140 43.3 06/03/13 18:08
Methylene chloride 140 ug/Kg 1U 140 43.3 06/03/13 18:08
n-Butylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
n-Propylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Naphthalene 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
o-Xylene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
P & M -Xylene 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
sec-Butylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Styrene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
tert-Butylbenzene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Tetrachloroethene 17.4 ug/Kg 1U 17.4 5.44 06/03/13 18:08
Toluene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
trans-1,2-Dichloroethene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
trans-1,3-Dichloropropene 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Trichloroethene 17.4 ug/Kg 1U 17.4 5.44 06/03/13 18:08
Trichlorofluoromethane 69.8 ug/Kg 1U 69.8 20.9 06/03/13 18:08
Vinyl chloride 34.9 ug/Kg 1U 34.9 10.9 06/03/13 18:08
Xylenes (total) 140 ug/Kg 1U 140 43.3 06/03/13 18:08
Surrogates
1,2-Dichloroethane-D4 114 % 179-118 06/03/13 18:08
4-Bromofluorobenzene 97.5 % 167-138 06/03/13 18:08
Toluene-d8 104 % 185-115 06/03/13 18:08
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 09:06
Prep Initial Wt./Vol.: 38.921 g
Prep Extract Vol: 26.2675 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 18:08
Container ID: 1132110012-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C253
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Metals by ICP/MS
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.64 mg/Kg 101.10 0.341 06/04/13 18:10
Barium 32.5 mg/Kg 100.330 0.103 06/04/13 18:10
Cadmium 0.220 mg/Kg 10U 0.220 0.0682 06/04/13 18:10
Chromium 32.9 mg/Kg 100.440 0.132 06/04/13 18:10
Lead 5.30 mg/Kg 100.220 0.0682 06/04/13 18:10
Mercury 0.0440 mg/Kg 10U 0.0440 0.0132 06/04/13 18:10
Selenium 0.550 mg/Kg 10U 0.550 0.165 06/04/13 18:10
Silver 0.110 mg/Kg 10U 0.110 0.0341 06/04/13 18:10
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.06 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:10
Container ID: 1132110013-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C254
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Semivolatile Organic Fuels
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 23.0 mg/Kg 1U 23.0 7.12 06/08/13 21:45
Surrogates
5a Androstane 91.2 % 150-150 06/08/13 21:45
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.47 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:45
Container ID: 1132110013-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 23.0 mg/Kg 1U 23.0 7.12 06/08/13 21:45
Surrogates
n-Triacontane-d62 103 % 150-150 06/08/13 21:45
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.47 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:45
Container ID: 1132110013-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C255
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Semivolatile Organic GC/MS
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
1,2-Dichlorobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
1,3-Dichlorobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
1,4-Dichlorobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
1-Chloronaphthalene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,4,5-Trichlorophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,4,6-Trichlorophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,4-Dichlorophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,4-Dimethylphenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,4-Dinitrophenol 3.49 mg/Kg 1U 3.49 1.09 06/11/13 23:56
2,4-Dinitrotoluene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,6-Dichlorophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2,6-Dinitrotoluene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Chloronaphthalene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Chlorophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Methyl-4,6-dinitrophenol 2.32 mg/Kg 1U 2.32 0.720 06/11/13 23:56
2-Methylnaphthalene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Methylphenol (o-Cresol) 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Nitroaniline 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
2-Nitrophenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
3&4-Methylphenol (p&m-Cresol) 1.16 mg/Kg 1U 1.16 0.360 06/11/13 23:56
3,3-Dichlorobenzidine 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
3-Nitroaniline 0.581 mg/Kg 1U 0.581 0.174 06/11/13 23:56
4-Bromophenyl-phenylether 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
4-Chloro-3-methylphenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
4-Chloroaniline 0.581 mg/Kg 1U 0.581 0.174 06/11/13 23:56
4-Chlorophenyl-phenylether 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
4-Nitroaniline 3.49 mg/Kg 1U 3.49 1.09 06/11/13 23:56
4-Nitrophenol 1.16 mg/Kg 1U 1.16 0.360 06/11/13 23:56
Acenaphthene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Acenaphthylene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Aniline 2.32 mg/Kg 1U 2.32 0.720 06/11/13 23:56
Anthracene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Azobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzo(a)Anthracene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzo[a]pyrene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzo[b]Fluoranthene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzo[g,h,i]perylene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzo[k]fluoranthene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Benzoic acid 1.74 mg/Kg 1U 1.74 0.871 06/11/13 23:56
Benzyl alcohol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Bis(2-Chloroethoxy)methane 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Bis(2-Chloroethyl)ether 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
bis(2-Ethylhexyl)phthalate 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C256
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Semivolatile Organic GC/MS
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Butylbenzylphthalate 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Carbazole 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Chrysene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Di-n-butylphthalate 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
di-n-Octylphthalate 0.581 mg/Kg 1U 0.581 0.174 06/11/13 23:56
Dibenzo[a,h]anthracene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Dibenzofuran 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Diethylphthalate 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Dimethylphthalate 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Fluoranthene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Fluorene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Hexachlorobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Hexachlorobutadiene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Hexachlorocyclopentadiene 0.813 mg/Kg 1U 0.813 0.232 06/11/13 23:56
Hexachloroethane 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Indeno[1,2,3-c,d] pyrene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Isophorone 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
N-Nitroso-di-n-propylamine 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
N-Nitrosodimethylamine 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
N-Nitrosodiphenylamine 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Naphthalene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Nitrobenzene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Pentachlorophenol 2.32 mg/Kg 1U 2.32 0.720 06/11/13 23:56
Phenanthrene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Phenol 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Pyrene 0.290 mg/Kg 1U 0.290 0.0906 06/11/13 23:56
Surrogates
2,4,6-Tribromophenol 94.9 % 135-125 06/11/13 23:56
2-Fluorobiphenyl 92.2 % 145-105 06/11/13 23:56
2-Fluorophenol 63.2 % 135-105 06/11/13 23:56
Nitrobenzene-d5 67.2 % 135-100 06/11/13 23:56
Phenol-d6 72.1 % 140-100 06/11/13 23:56
Terphenyl-d14 98.2 % 130-125 06/11/13 23:56
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.579 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 23:56
Container ID: 1132110013-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C257
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Volatile Fuels
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 3.01 mg/Kg 1U 3.01 0.903 06/06/13 22:39
Surrogates
4-Bromofluorobenzene 101 % 150-150 06/06/13 22:39
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 09:32
Prep Initial Wt./Vol.: 66.856 g
Prep Extract Vol: 34.5157 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 22:39
Container ID: 1132110013-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C258
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Volatile GC/MS
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,1,1-Trichloroethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,1,2,2-Tetrachloroethane 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
1,1,2-Trichloroethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,1-Dichloroethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,1-Dichloroethene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,1-Dichloropropene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2,3-Trichlorobenzene 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
1,2,3-Trichloropropane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2,4-Trichlorobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2,4-Trimethylbenzene 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
1,2-Dibromo-3-chloropropane 120 ug/Kg 1U 120 37.3 06/03/13 18:25
1,2-Dibromoethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2-Dichlorobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2-Dichloroethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,2-Dichloropropane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,3,5-Trimethylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,3-Dichlorobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,3-Dichloropropane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
1,4-Dichlorobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
2,2-Dichloropropane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
2-Butanone (MEK) 301 ug/Kg 1U 301 93.9 06/03/13 18:25
2-Chlorotoluene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
2-Hexanone 301 ug/Kg 1U 301 93.9 06/03/13 18:25
4-Chlorotoluene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
4-Isopropyltoluene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
4-Methyl-2-pentanone (MIBK) 301 ug/Kg 1U 301 93.9 06/03/13 18:25
Benzene 15.0 ug/Kg 1U 15.0 4.70 06/03/13 18:25
Bromobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Bromochloromethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Bromodichloromethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Bromoform 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Bromomethane 241 ug/Kg 1U 241 74.6 06/03/13 18:25
Carbon disulfide 120 ug/Kg 1U 120 37.3 06/03/13 18:25
Carbon tetrachloride 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Chlorobenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Chloroethane 241 ug/Kg 1U 241 74.6 06/03/13 18:25
Chloroform 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Chloromethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
cis-1,2-Dichloroethene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
cis-1,3-Dichloropropene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Dibromochloromethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Dibromomethane 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Dichlorodifluoromethane 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C259
Client Sample ID: SMIC-O (25)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110013
Lab Project ID: 1132110
Collection Date: 05/31/13 09:32
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 85.8
Results by Volatile GC/MS
Results of SMIC-O (25)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Hexachlorobutadiene 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
Isopropylbenzene (Cumene) 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Methyl-t-butyl ether 120 ug/Kg 1U 120 37.3 06/03/13 18:25
Methylene chloride 120 ug/Kg 1U 120 37.3 06/03/13 18:25
n-Butylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
n-Propylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Naphthalene 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
o-Xylene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
P & M -Xylene 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
sec-Butylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Styrene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
tert-Butylbenzene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Tetrachloroethene 15.0 ug/Kg 1U 15.0 4.70 06/03/13 18:25
Toluene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
trans-1,2-Dichloroethene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
trans-1,3-Dichloropropene 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Trichloroethene 15.0 ug/Kg 1U 15.0 4.70 06/03/13 18:25
Trichlorofluoromethane 60.2 ug/Kg 1U 60.2 18.1 06/03/13 18:25
Vinyl chloride 30.1 ug/Kg 1U 30.1 9.39 06/03/13 18:25
Xylenes (total) 120 ug/Kg 1U 120 37.3 06/03/13 18:25
Surrogates
1,2-Dichloroethane-D4 108 % 179-118 06/03/13 18:25
4-Bromofluorobenzene 98 % 167-138 06/03/13 18:25
Toluene-d8 98.7 % 185-115 06/03/13 18:25
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 09:32
Prep Initial Wt./Vol.: 66.856 g
Prep Extract Vol: 34.5157 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 18:25
Container ID: 1132110013-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C260
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Metals by ICP/MS
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.19 mg/Kg 100.964 0.299 06/04/13 18:16
Barium 33.9 mg/Kg 100.289 0.0906 06/04/13 18:16
Cadmium 0.193 mg/Kg 10U 0.193 0.0598 06/04/13 18:16
Chromium 32.0 mg/Kg 100.386 0.116 06/04/13 18:16
Lead 5.05 mg/Kg 100.193 0.0598 06/04/13 18:16
Mercury 0.0386 mg/Kg 10U 0.0386 0.0116 06/04/13 18:16
Selenium 0.482 mg/Kg 10U 0.482 0.145 06/04/13 18:16
Silver 0.0964 mg/Kg 10U 0.0964 0.0299 06/04/13 18:16
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.064 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:16
Container ID: 1132110014-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C261
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic Fuels
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 24.3 mg/Kg 120.2 6.27 06/08/13 21:54
Surrogates
5a Androstane 119 % 150-150 06/08/13 21:54
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.426 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 21:54
Container ID: 1132110014-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 146 mg/Kg 120.2 6.27 06/08/13 21:54
Surrogates
n-Triacontane-d62 140 % 150-150 06/08/13 21:54
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.426 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 21:54
Container ID: 1132110014-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C262
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic GC/MS
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
1,2-Dichlorobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
1,3-Dichlorobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
1,4-Dichlorobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
1-Chloronaphthalene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,4,5-Trichlorophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,4,6-Trichlorophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,4-Dichlorophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,4-Dimethylphenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,4-Dinitrophenol 3.03 mg/Kg 1U 3.03 0.949 06/12/13 00:13
2,4-Dinitrotoluene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,6-Dichlorophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2,6-Dinitrotoluene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Chloronaphthalene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Chlorophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Methyl-4,6-dinitrophenol 2.02 mg/Kg 1U 2.02 0.626 06/12/13 00:13
2-Methylnaphthalene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Methylphenol (o-Cresol) 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Nitroaniline 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
2-Nitrophenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
3&4-Methylphenol (p&m-Cresol) 1.01 mg/Kg 1U 1.01 0.313 06/12/13 00:13
3,3-Dichlorobenzidine 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
3-Nitroaniline 0.505 mg/Kg 1U 0.505 0.151 06/12/13 00:13
4-Bromophenyl-phenylether 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
4-Chloro-3-methylphenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
4-Chloroaniline 0.505 mg/Kg 1U 0.505 0.151 06/12/13 00:13
4-Chlorophenyl-phenylether 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
4-Nitroaniline 3.03 mg/Kg 1U 3.03 0.949 06/12/13 00:13
4-Nitrophenol 1.01 mg/Kg 1U 1.01 0.313 06/12/13 00:13
Acenaphthene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Acenaphthylene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Aniline 2.02 mg/Kg 1U 2.02 0.626 06/12/13 00:13
Anthracene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Azobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzo(a)Anthracene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzo[a]pyrene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzo[b]Fluoranthene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzo[g,h,i]perylene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzo[k]fluoranthene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Benzoic acid 1.51 mg/Kg 1U 1.51 0.757 06/12/13 00:13
Benzyl alcohol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Bis(2-Chloroethoxy)methane 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Bis(2-Chloroethyl)ether 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
bis(2-Ethylhexyl)phthalate 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C263
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Semivolatile Organic GC/MS
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Butylbenzylphthalate 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Carbazole 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Chrysene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Di-n-butylphthalate 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
di-n-Octylphthalate 0.505 mg/Kg 1U 0.505 0.151 06/12/13 00:13
Dibenzo[a,h]anthracene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Dibenzofuran 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Diethylphthalate 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Dimethylphthalate 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Fluoranthene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Fluorene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Hexachlorobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Hexachlorobutadiene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Hexachlorocyclopentadiene 0.707 mg/Kg 1U 0.707 0.202 06/12/13 00:13
Hexachloroethane 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Indeno[1,2,3-c,d] pyrene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Isophorone 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
N-Nitroso-di-n-propylamine 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
N-Nitrosodimethylamine 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
N-Nitrosodiphenylamine 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Naphthalene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Nitrobenzene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Pentachlorophenol 2.02 mg/Kg 1U 2.02 0.626 06/12/13 00:13
Phenanthrene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Phenol 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Pyrene 0.252 mg/Kg 1U 0.252 0.0788 06/12/13 00:13
Surrogates
2,4,6-Tribromophenol 95.5 % 135-125 06/12/13 00:13
2-Fluorobiphenyl 96.4 % 145-105 06/12/13 00:13
2-Fluorophenol 70 % 135-105 06/12/13 00:13
Nitrobenzene-d5 73.1 % 135-100 06/12/13 00:13
Phenol-d6 78.9 % 140-100 06/12/13 00:13
Terphenyl-d14 102 % 130-125 06/12/13 00:13
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.846 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 00:13
Container ID: 1132110014-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C264
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile Fuels
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 1.99 mg/Kg 1U 1.99 0.597 06/06/13 22:58
Surrogates
4-Bromofluorobenzene 99.9 % 150-150 06/06/13 22:58
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:23
Prep Initial Wt./Vol.: 68.799 g
Prep Extract Vol: 26.7071 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 22:58
Container ID: 1132110014-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C265
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile GC/MS
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,1,1-Trichloroethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,1,2,2-Tetrachloroethane 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
1,1,2-Trichloroethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,1-Dichloroethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,1-Dichloroethene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,1-Dichloropropene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2,3-Trichlorobenzene 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
1,2,3-Trichloropropane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2,4-Trichlorobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2,4-Trimethylbenzene 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
1,2-Dibromo-3-chloropropane 79.6 ug/Kg 1U 79.6 24.7 06/03/13 18:42
1,2-Dibromoethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2-Dichlorobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2-Dichloroethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,2-Dichloropropane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,3,5-Trimethylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,3-Dichlorobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,3-Dichloropropane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
1,4-Dichlorobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
2,2-Dichloropropane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
2-Butanone (MEK) 199 ug/Kg 1U 199 62.1 06/03/13 18:42
2-Chlorotoluene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
2-Hexanone 199 ug/Kg 1U 199 62.1 06/03/13 18:42
4-Chlorotoluene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
4-Isopropyltoluene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
4-Methyl-2-pentanone (MIBK) 199 ug/Kg 1U 199 62.1 06/03/13 18:42
Benzene 9.95 ug/Kg 1U 9.95 3.10 06/03/13 18:42
Bromobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Bromochloromethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Bromodichloromethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Bromoform 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Bromomethane 159 ug/Kg 1U 159 49.4 06/03/13 18:42
Carbon disulfide 79.6 ug/Kg 1U 79.6 24.7 06/03/13 18:42
Carbon tetrachloride 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Chlorobenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Chloroethane 159 ug/Kg 1U 159 49.4 06/03/13 18:42
Chloroform 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Chloromethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
cis-1,2-Dichloroethene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
cis-1,3-Dichloropropene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Dibromochloromethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Dibromomethane 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Dichlorodifluoromethane 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C266
Client Sample ID: SMIC-M (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110014
Lab Project ID: 1132110
Collection Date: 05/31/13 13:23
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.5
Results by Volatile GC/MS
Results of SMIC-M (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Hexachlorobutadiene 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
Isopropylbenzene (Cumene) 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Methyl-t-butyl ether 79.6 ug/Kg 1U 79.6 24.7 06/03/13 18:42
Methylene chloride 79.6 ug/Kg 1U 79.6 24.7 06/03/13 18:42
n-Butylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
n-Propylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Naphthalene 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
o-Xylene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
P & M -Xylene 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
sec-Butylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Styrene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
tert-Butylbenzene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Tetrachloroethene 9.95 ug/Kg 1U 9.95 3.10 06/03/13 18:42
Toluene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
trans-1,2-Dichloroethene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
trans-1,3-Dichloropropene 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Trichloroethene 9.95 ug/Kg 1U 9.95 3.10 06/03/13 18:42
Trichlorofluoromethane 39.8 ug/Kg 1U 39.8 11.9 06/03/13 18:42
Vinyl chloride 19.9 ug/Kg 1U 19.9 6.21 06/03/13 18:42
Xylenes (total) 79.6 ug/Kg 1U 79.6 24.7 06/03/13 18:42
Surrogates
1,2-Dichloroethane-D4 114 % 179-118 06/03/13 18:42
4-Bromofluorobenzene 99.4 % 167-138 06/03/13 18:42
Toluene-d8 102 % 185-115 06/03/13 18:42
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:23
Prep Initial Wt./Vol.: 68.799 g
Prep Extract Vol: 26.7071 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 18:42
Container ID: 1132110014-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C267
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Metals by ICP/MS
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.44 mg/Kg 100.962 0.298 06/04/13 18:19
Barium 37.0 mg/Kg 100.289 0.0904 06/04/13 18:19
Cadmium 0.192 mg/Kg 10U 0.192 0.0597 06/04/13 18:19
Chromium 32.7 mg/Kg 100.385 0.115 06/04/13 18:19
Lead 5.56 mg/Kg 100.192 0.0597 06/04/13 18:19
Mercury 0.0385 mg/Kg 10U 0.0385 0.0115 06/04/13 18:19
Selenium 0.481 mg/Kg 10U 0.481 0.144 06/04/13 18:19
Silver 0.0962 mg/Kg 10U 0.0962 0.0298 06/04/13 18:19
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.067 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:19
Container ID: 1132110015-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C268
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic Fuels
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 32.6 mg/Kg 120.0 6.20 06/08/13 22:04
Surrogates
5a Androstane 122 % 150-150 06/08/13 22:04
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.794 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:04
Container ID: 1132110015-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 184 mg/Kg 120.0 6.20 06/08/13 22:04
Surrogates
n-Triacontane-d62 141 % 150-150 06/08/13 22:04
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.794 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:04
Container ID: 1132110015-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C269
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,4-Dinitrophenol 3.05 mg/Kg 1U 3.05 0.956 06/12/13 00:30
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.631 06/12/13 00:30
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.315 06/12/13 00:30
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
3-Nitroaniline 0.509 mg/Kg 1U 0.509 0.153 06/12/13 00:30
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
4-Chloroaniline 0.509 mg/Kg 1U 0.509 0.153 06/12/13 00:30
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
4-Nitroaniline 3.05 mg/Kg 1U 3.05 0.956 06/12/13 00:30
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.315 06/12/13 00:30
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Aniline 2.03 mg/Kg 1U 2.03 0.631 06/12/13 00:30
Anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Azobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Benzoic acid 1.53 mg/Kg 1U 1.53 0.763 06/12/13 00:30
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C270
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Semivolatile Organic GC/MS
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Carbazole 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Chrysene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
di-n-Octylphthalate 0.509 mg/Kg 1U 0.509 0.153 06/12/13 00:30
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Fluorene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Hexachlorocyclopentadiene 0.712 mg/Kg 1U 0.712 0.203 06/12/13 00:30
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Isophorone 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Naphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.631 06/12/13 00:30
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Phenol 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/12/13 00:30
Surrogates
2,4,6-Tribromophenol 95.9 % 135-125 06/12/13 00:30
2-Fluorobiphenyl 90.7 % 145-105 06/12/13 00:30
2-Fluorophenol 65.3 % 135-105 06/12/13 00:30
Nitrobenzene-d5 67.5 % 135-100 06/12/13 00:30
Phenol-d6 75.9 % 140-100 06/12/13 00:30
Terphenyl-d14 106 % 130-125 06/12/13 00:30
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.713 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 00:30
Container ID: 1132110015-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C271
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile Fuels
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.00 mg/Kg 1U 2.00 0.599 06/06/13 23:17
Surrogates
4-Bromofluorobenzene 104 % 150-150 06/06/13 23:17
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:29
Prep Initial Wt./Vol.: 68.812 g
Prep Extract Vol: 26.7848 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 23:17
Container ID: 1132110015-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C272
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,1,1-Trichloroethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,1,2,2-Tetrachloroethane 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
1,1,2-Trichloroethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,1-Dichloroethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,1-Dichloroethene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,1-Dichloropropene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2,3-Trichlorobenzene 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
1,2,3-Trichloropropane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2,4-Trichlorobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2,4-Trimethylbenzene 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
1,2-Dibromo-3-chloropropane 79.9 ug/Kg 1U 79.9 24.8 06/03/13 18:58
1,2-Dibromoethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2-Dichlorobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2-Dichloroethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,2-Dichloropropane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,3,5-Trimethylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,3-Dichlorobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,3-Dichloropropane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
1,4-Dichlorobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
2,2-Dichloropropane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
2-Butanone (MEK) 200 ug/Kg 1U 200 62.3 06/03/13 18:58
2-Chlorotoluene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
2-Hexanone 200 ug/Kg 1U 200 62.3 06/03/13 18:58
4-Chlorotoluene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
4-Isopropyltoluene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
4-Methyl-2-pentanone (MIBK) 200 ug/Kg 1U 200 62.3 06/03/13 18:58
Benzene 9.99 ug/Kg 1U 9.99 3.12 06/03/13 18:58
Bromobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Bromochloromethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Bromodichloromethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Bromoform 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Bromomethane 160 ug/Kg 1U 160 49.6 06/03/13 18:58
Carbon disulfide 79.9 ug/Kg 1U 79.9 24.8 06/03/13 18:58
Carbon tetrachloride 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Chlorobenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Chloroethane 160 ug/Kg 1U 160 49.6 06/03/13 18:58
Chloroform 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Chloromethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
cis-1,2-Dichloroethene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
cis-1,3-Dichloropropene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Dibromochloromethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Dibromomethane 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Dichlorodifluoromethane 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C273
Client Sample ID: SMIC-M (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110015
Lab Project ID: 1132110
Collection Date: 05/31/13 13:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.4
Results by Volatile GC/MS
Results of SMIC-M (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Hexachlorobutadiene 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
Isopropylbenzene (Cumene) 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Methyl-t-butyl ether 79.9 ug/Kg 1U 79.9 24.8 06/03/13 18:58
Methylene chloride 79.9 ug/Kg 1U 79.9 24.8 06/03/13 18:58
n-Butylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
n-Propylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Naphthalene 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
o-Xylene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
P & M -Xylene 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
sec-Butylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Styrene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
tert-Butylbenzene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Tetrachloroethene 9.99 ug/Kg 1U 9.99 3.12 06/03/13 18:58
Toluene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
trans-1,2-Dichloroethene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
trans-1,3-Dichloropropene 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Trichloroethene 9.99 ug/Kg 1U 9.99 3.12 06/03/13 18:58
Trichlorofluoromethane 40.0 ug/Kg 1U 40.0 12.0 06/03/13 18:58
Vinyl chloride 20.0 ug/Kg 1U 20.0 6.23 06/03/13 18:58
Xylenes (total) 79.9 ug/Kg 1U 79.9 24.8 06/03/13 18:58
Surrogates
1,2-Dichloroethane-D4 110 % 179-118 06/03/13 18:58
4-Bromofluorobenzene 101 % 167-138 06/03/13 18:58
Toluene-d8 103 % 185-115 06/03/13 18:58
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:29
Prep Initial Wt./Vol.: 68.812 g
Prep Extract Vol: 26.7848 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 18:58
Container ID: 1132110015-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C274
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Metals by ICP/MS
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.06 mg/Kg 100.985 0.305 06/04/13 18:21
Barium 31.5 mg/Kg 100.295 0.0926 06/04/13 18:21
Cadmium 0.197 mg/Kg 10U 0.197 0.0611 06/04/13 18:21
Chromium 27.3 mg/Kg 100.394 0.118 06/04/13 18:21
Lead 5.55 mg/Kg 100.197 0.0611 06/04/13 18:21
Mercury 0.0394 mg/Kg 10U 0.0394 0.0118 06/04/13 18:21
Selenium 0.492 mg/Kg 10U 0.492 0.148 06/04/13 18:21
Silver 0.0985 mg/Kg 10U 0.0985 0.0305 06/04/13 18:21
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.043 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:21
Container ID: 1132110016-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C275
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Semivolatile Organic Fuels
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.1 mg/Kg 1U 20.1 6.23 06/08/13 22:13
Surrogates
5a Androstane 100 % 150-150 06/08/13 22:13
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.665 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:13
Container ID: 1132110016-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 20.1 mg/Kg 1U 20.1 6.23 06/08/13 22:13
Surrogates
n-Triacontane-d62 114 % 150-150 06/08/13 22:13
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.665 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:13
Container ID: 1132110016-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C276
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Semivolatile Organic GC/MS
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
1,2-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
1,3-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
1,4-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
1-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,4,5-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,4,6-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,4-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,4-Dimethylphenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,4-Dinitrophenol 3.06 mg/Kg 1U 3.06 0.959 06/12/13 00:47
2,4-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,6-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2,6-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Chlorophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Methyl-4,6-dinitrophenol 2.04 mg/Kg 1U 2.04 0.633 06/12/13 00:47
2-Methylnaphthalene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Methylphenol (o-Cresol) 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Nitroaniline 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
2-Nitrophenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.316 06/12/13 00:47
3,3-Dichlorobenzidine 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
3-Nitroaniline 0.510 mg/Kg 1U 0.510 0.153 06/12/13 00:47
4-Bromophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
4-Chloro-3-methylphenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
4-Chloroaniline 0.510 mg/Kg 1U 0.510 0.153 06/12/13 00:47
4-Chlorophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
4-Nitroaniline 3.06 mg/Kg 1U 3.06 0.959 06/12/13 00:47
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.316 06/12/13 00:47
Acenaphthene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Acenaphthylene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Aniline 2.04 mg/Kg 1U 2.04 0.633 06/12/13 00:47
Anthracene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Azobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzo(a)Anthracene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzo[a]pyrene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzo[b]Fluoranthene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzo[g,h,i]perylene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzo[k]fluoranthene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Benzoic acid 1.53 mg/Kg 1U 1.53 0.765 06/12/13 00:47
Benzyl alcohol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Bis(2-Chloroethoxy)methane 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Bis(2-Chloroethyl)ether 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
bis(2-Ethylhexyl)phthalate 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C277
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Semivolatile Organic GC/MS
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Butylbenzylphthalate 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Carbazole 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Chrysene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Di-n-butylphthalate 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
di-n-Octylphthalate 0.510 mg/Kg 1U 0.510 0.153 06/12/13 00:47
Dibenzo[a,h]anthracene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Dibenzofuran 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Diethylphthalate 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Dimethylphthalate 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Fluoranthene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Fluorene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Hexachlorobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Hexachlorobutadiene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Hexachlorocyclopentadiene 0.714 mg/Kg 1U 0.714 0.204 06/12/13 00:47
Hexachloroethane 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Indeno[1,2,3-c,d] pyrene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Isophorone 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
N-Nitroso-di-n-propylamine 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
N-Nitrosodimethylamine 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
N-Nitrosodiphenylamine 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Naphthalene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Nitrobenzene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Pentachlorophenol 2.04 mg/Kg 1U 2.04 0.633 06/12/13 00:47
Phenanthrene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Phenol 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Pyrene 0.255 mg/Kg 1U 0.255 0.0796 06/12/13 00:47
Surrogates
2,4,6-Tribromophenol 96.9 % 135-125 06/12/13 00:47
2-Fluorobiphenyl 92.4 % 145-105 06/12/13 00:47
2-Fluorophenol 65.5 % 135-105 06/12/13 00:47
Nitrobenzene-d5 65.1 % 135-100 06/12/13 00:47
Phenol-d6 76.3 % 140-100 06/12/13 00:47
Terphenyl-d14 99 % 130-125 06/12/13 00:47
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.658 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 00:47
Container ID: 1132110016-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C278
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Volatile Fuels
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.80 mg/Kg 1U 2.80 0.841 06/06/13 23:35
Surrogates
4-Bromofluorobenzene 97.8 % 150-150 06/06/13 23:35
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:37
Prep Initial Wt./Vol.: 48.143 g
Prep Extract Vol: 26.2816 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 23:35
Container ID: 1132110016-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C279
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Volatile GC/MS
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,1,1-Trichloroethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,1,2,2-Tetrachloroethane 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
1,1,2-Trichloroethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,1-Dichloroethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,1-Dichloroethene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,1-Dichloropropene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2,3-Trichlorobenzene 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
1,2,3-Trichloropropane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2,4-Trichlorobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2,4-Trimethylbenzene 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
1,2-Dibromo-3-chloropropane 112 ug/Kg 1U 112 34.8 06/03/13 19:15
1,2-Dibromoethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2-Dichloroethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,2-Dichloropropane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,3,5-Trimethylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,3-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,3-Dichloropropane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
1,4-Dichlorobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
2,2-Dichloropropane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
2-Butanone (MEK) 280 ug/Kg 1U 280 87.5 06/03/13 19:15
2-Chlorotoluene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
2-Hexanone 280 ug/Kg 1U 280 87.5 06/03/13 19:15
4-Chlorotoluene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
4-Isopropyltoluene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
4-Methyl-2-pentanone (MIBK) 280 ug/Kg 1U 280 87.5 06/03/13 19:15
Benzene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 19:15
Bromobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Bromochloromethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Bromodichloromethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Bromoform 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Bromomethane 224 ug/Kg 1U 224 69.5 06/03/13 19:15
Carbon disulfide 112 ug/Kg 1U 112 34.8 06/03/13 19:15
Carbon tetrachloride 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Chlorobenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Chloroethane 224 ug/Kg 1U 224 69.5 06/03/13 19:15
Chloroform 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Chloromethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
cis-1,2-Dichloroethene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
cis-1,3-Dichloropropene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Dibromochloromethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Dibromomethane 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Dichlorodifluoromethane 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C280
Client Sample ID: SMIC-M (5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110016
Lab Project ID: 1132110
Collection Date: 05/31/13 13:37
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.3
Results by Volatile GC/MS
Results of SMIC-M (5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Hexachlorobutadiene 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
Isopropylbenzene (Cumene) 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Methyl-t-butyl ether 112 ug/Kg 1U 112 34.8 06/03/13 19:15
Methylene chloride 112 ug/Kg 1U 112 34.8 06/03/13 19:15
n-Butylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
n-Propylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Naphthalene 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
o-Xylene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
P & M -Xylene 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
sec-Butylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Styrene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
tert-Butylbenzene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Tetrachloroethene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 19:15
Toluene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
trans-1,2-Dichloroethene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
trans-1,3-Dichloropropene 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Trichloroethene 14.0 ug/Kg 1U 14.0 4.37 06/03/13 19:15
Trichlorofluoromethane 56.1 ug/Kg 1U 56.1 16.8 06/03/13 19:15
Vinyl chloride 28.0 ug/Kg 1U 28.0 8.75 06/03/13 19:15
Xylenes (total) 112 ug/Kg 1U 112 34.8 06/03/13 19:15
Surrogates
1,2-Dichloroethane-D4 108 % 179-118 06/03/13 19:15
4-Bromofluorobenzene 96.4 % 167-138 06/03/13 19:15
Toluene-d8 102 % 185-115 06/03/13 19:15
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:37
Prep Initial Wt./Vol.: 48.143 g
Prep Extract Vol: 26.2816 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 19:15
Container ID: 1132110016-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C281
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Metals by ICP/MS
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.66 mg/Kg 100.986 0.306 06/04/13 18:23
Barium 43.0 mg/Kg 100.296 0.0927 06/04/13 18:23
Cadmium 0.197 mg/Kg 10U 0.197 0.0611 06/04/13 18:23
Chromium 34.2 mg/Kg 100.394 0.118 06/04/13 18:23
Lead 5.59 mg/Kg 100.197 0.0611 06/04/13 18:23
Mercury 0.0394 mg/Kg 10U 0.0394 0.0118 06/04/13 18:23
Selenium 0.493 mg/Kg 10U 0.493 0.148 06/04/13 18:23
Silver 0.0986 mg/Kg 10U 0.0986 0.0306 06/04/13 18:23
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.171 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:23
Container ID: 1132110017-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C282
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Semivolatile Organic Fuels
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.9 mg/Kg 1U 22.9 7.08 06/08/13 22:22
Surrogates
5a Androstane 96.1 % 150-150 06/08/13 22:22
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.321 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:22
Container ID: 1132110017-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.9 mg/Kg 1U 22.9 7.08 06/08/13 22:22
Surrogates
n-Triacontane-d62 112 % 150-150 06/08/13 22:22
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.321 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:22
Container ID: 1132110017-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C283
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Semivolatile Organic GC/MS
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
1,2-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
1,3-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
1,4-Dichlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
1-Chloronaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,4,5-Trichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,4,6-Trichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,4-Dichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,4-Dimethylphenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,4-Dinitrophenol 3.39 mg/Kg 1U 3.39 1.06 06/12/13 01:04
2,4-Dinitrotoluene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,6-Dichlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2,6-Dinitrotoluene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Chloronaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Chlorophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Methyl-4,6-dinitrophenol 2.26 mg/Kg 1U 2.26 0.701 06/12/13 01:04
2-Methylnaphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Methylphenol (o-Cresol) 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Nitroaniline 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
2-Nitrophenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
3&4-Methylphenol (p&m-Cresol) 1.13 mg/Kg 1U 1.13 0.351 06/12/13 01:04
3,3-Dichlorobenzidine 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
3-Nitroaniline 0.566 mg/Kg 1U 0.566 0.170 06/12/13 01:04
4-Bromophenyl-phenylether 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
4-Chloro-3-methylphenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
4-Chloroaniline 0.566 mg/Kg 1U 0.566 0.170 06/12/13 01:04
4-Chlorophenyl-phenylether 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
4-Nitroaniline 3.39 mg/Kg 1U 3.39 1.06 06/12/13 01:04
4-Nitrophenol 1.13 mg/Kg 1U 1.13 0.351 06/12/13 01:04
Acenaphthene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Acenaphthylene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Aniline 2.26 mg/Kg 1U 2.26 0.701 06/12/13 01:04
Anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Azobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzo(a)Anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzo[a]pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzo[b]Fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzo[g,h,i]perylene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzo[k]fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Benzoic acid 1.70 mg/Kg 1U 1.70 0.848 06/12/13 01:04
Benzyl alcohol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Bis(2-Chloroethoxy)methane 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Bis(2-Chloroethyl)ether 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
bis(2-Ethylhexyl)phthalate 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C284
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Semivolatile Organic GC/MS
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Butylbenzylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Carbazole 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Chrysene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Di-n-butylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
di-n-Octylphthalate 0.566 mg/Kg 1U 0.566 0.170 06/12/13 01:04
Dibenzo[a,h]anthracene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Dibenzofuran 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Diethylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Dimethylphthalate 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Fluoranthene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Fluorene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Hexachlorobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Hexachlorobutadiene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Hexachlorocyclopentadiene 0.792 mg/Kg 1U 0.792 0.226 06/12/13 01:04
Hexachloroethane 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Indeno[1,2,3-c,d] pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Isophorone 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
N-Nitroso-di-n-propylamine 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
N-Nitrosodimethylamine 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
N-Nitrosodiphenylamine 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Naphthalene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Nitrobenzene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Pentachlorophenol 2.26 mg/Kg 1U 2.26 0.701 06/12/13 01:04
Phenanthrene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Phenol 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Pyrene 0.283 mg/Kg 1U 0.283 0.0882 06/12/13 01:04
Surrogates
2,4,6-Tribromophenol 88.5 % 135-125 06/12/13 01:04
2-Fluorobiphenyl 86 % 145-105 06/12/13 01:04
2-Fluorophenol 58.7 % 135-105 06/12/13 01:04
Nitrobenzene-d5 60.4 % 135-100 06/12/13 01:04
Phenol-d6 68.4 % 140-100 06/12/13 01:04
Terphenyl-d14 96.1 % 130-125 06/12/13 01:04
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.971 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 01:04
Container ID: 1132110017-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C285
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Volatile Fuels
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.45 mg/Kg 1U 2.45 0.735 06/06/13 23:54
Surrogates
4-Bromofluorobenzene 112 % 150-150 06/06/13 23:54
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 14:02
Prep Initial Wt./Vol.: 86.107 g
Prep Extract Vol: 36.542 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 23:54
Container ID: 1132110017-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C286
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Volatile GC/MS
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,1,1-Trichloroethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,1,2,2-Tetrachloroethane 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
1,1,2-Trichloroethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,1-Dichloroethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,1-Dichloroethene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,1-Dichloropropene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2,3-Trichlorobenzene 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
1,2,3-Trichloropropane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2,4-Trichlorobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2,4-Trimethylbenzene 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
1,2-Dibromo-3-chloropropane 98.0 ug/Kg 1U 98.0 30.4 06/03/13 19:32
1,2-Dibromoethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2-Dichlorobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2-Dichloroethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,2-Dichloropropane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,3,5-Trimethylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,3-Dichlorobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,3-Dichloropropane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
1,4-Dichlorobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
2,2-Dichloropropane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
2-Butanone (MEK) 245 ug/Kg 1U 245 76.5 06/03/13 19:32
2-Chlorotoluene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
2-Hexanone 245 ug/Kg 1U 245 76.5 06/03/13 19:32
4-Chlorotoluene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
4-Isopropyltoluene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
4-Methyl-2-pentanone (MIBK) 245 ug/Kg 1U 245 76.5 06/03/13 19:32
Benzene 12.3 ug/Kg 1U 12.3 3.82 06/03/13 19:32
Bromobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Bromochloromethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Bromodichloromethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Bromoform 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Bromomethane 196 ug/Kg 1U 196 60.8 06/03/13 19:32
Carbon disulfide 98.0 ug/Kg 1U 98.0 30.4 06/03/13 19:32
Carbon tetrachloride 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Chlorobenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Chloroethane 196 ug/Kg 1U 196 60.8 06/03/13 19:32
Chloroform 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Chloromethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
cis-1,2-Dichloroethene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
cis-1,3-Dichloropropene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Dibromochloromethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Dibromomethane 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Dichlorodifluoromethane 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C287
Client Sample ID: SMIC-M (20)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110017
Lab Project ID: 1132110
Collection Date: 05/31/13 14:02
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 86.6
Results by Volatile GC/MS
Results of SMIC-M (20)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Hexachlorobutadiene 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
Isopropylbenzene (Cumene) 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Methyl-t-butyl ether 98.0 ug/Kg 1U 98.0 30.4 06/03/13 19:32
Methylene chloride 98.0 ug/Kg 1U 98.0 30.4 06/03/13 19:32
n-Butylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
n-Propylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Naphthalene 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
o-Xylene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
P & M -Xylene 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
sec-Butylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Styrene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
tert-Butylbenzene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Tetrachloroethene 12.3 ug/Kg 1U 12.3 3.82 06/03/13 19:32
Toluene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
trans-1,2-Dichloroethene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
trans-1,3-Dichloropropene 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Trichloroethene 12.3 ug/Kg 1U 12.3 3.82 06/03/13 19:32
Trichlorofluoromethane 49.0 ug/Kg 1U 49.0 14.7 06/03/13 19:32
Vinyl chloride 24.5 ug/Kg 1U 24.5 7.65 06/03/13 19:32
Xylenes (total) 98.0 ug/Kg 1U 98.0 30.4 06/03/13 19:32
Surrogates
1,2-Dichloroethane-D4 110 % 179-118 06/03/13 19:32
4-Bromofluorobenzene 101 % 167-138 06/03/13 19:32
Toluene-d8 101 % 185-115 06/03/13 19:32
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 14:02
Prep Initial Wt./Vol.: 86.107 g
Prep Extract Vol: 36.542 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 19:32
Container ID: 1132110017-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C288
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Metals by ICP/MS
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 4.34 mg/Kg 100.990 0.307 06/04/13 18:25
Barium 44.3 mg/Kg 100.297 0.0931 06/04/13 18:25
Cadmium 0.198 mg/Kg 10U 0.198 0.0614 06/04/13 18:25
Chromium 34.2 mg/Kg 100.396 0.119 06/04/13 18:25
Lead 5.05 mg/Kg 100.198 0.0614 06/04/13 18:25
Mercury 0.0396 mg/Kg 10U 0.0396 0.0119 06/04/13 18:25
Selenium 0.495 mg/Kg 10U 0.495 0.149 06/04/13 18:25
Silver 0.0990 mg/Kg 10U 0.0990 0.0307 06/04/13 18:25
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.031 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:25
Container ID: 1132110018-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C289
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Semivolatile Organic Fuels
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.2 mg/Kg 1U 20.2 6.26 06/08/13 22:32
Surrogates
5a Androstane 103 % 150-150 06/08/13 22:32
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.338 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:32
Container ID: 1132110018-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 36.3 mg/Kg 120.2 6.26 06/08/13 22:32
Surrogates
n-Triacontane-d62 114 % 150-150 06/08/13 22:32
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.338 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:32
Container ID: 1132110018-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C290
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Semivolatile Organic GC/MS
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,4-Dinitrophenol 3.05 mg/Kg 1U 3.05 0.955 06/12/13 01:21
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.630 06/12/13 01:21
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.315 06/12/13 01:21
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
3-Nitroaniline 0.508 mg/Kg 1U 0.508 0.152 06/12/13 01:21
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
4-Chloroaniline 0.508 mg/Kg 1U 0.508 0.152 06/12/13 01:21
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
4-Nitroaniline 3.05 mg/Kg 1U 3.05 0.955 06/12/13 01:21
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.315 06/12/13 01:21
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Aniline 2.03 mg/Kg 1U 2.03 0.630 06/12/13 01:21
Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Azobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Benzoic acid 1.52 mg/Kg 1U 1.52 0.762 06/12/13 01:21
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C291
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Semivolatile Organic GC/MS
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Carbazole 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Chrysene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
di-n-Octylphthalate 0.508 mg/Kg 1U 0.508 0.152 06/12/13 01:21
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Fluorene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Hexachlorocyclopentadiene 0.711 mg/Kg 1U 0.711 0.203 06/12/13 01:21
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Isophorone 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Naphthalene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.630 06/12/13 01:21
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Phenol 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Pyrene 0.254 mg/Kg 1U 0.254 0.0792 06/12/13 01:21
Surrogates
2,4,6-Tribromophenol 89.6 % 135-125 06/12/13 01:21
2-Fluorobiphenyl 88.2 % 145-105 06/12/13 01:21
2-Fluorophenol 63.5 % 135-105 06/12/13 01:21
Nitrobenzene-d5 64.8 % 135-100 06/12/13 01:21
Phenol-d6 72.9 % 140-100 06/12/13 01:21
Terphenyl-d14 104 % 130-125 06/12/13 01:21
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.621 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 01:21
Container ID: 1132110018-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C292
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Volatile Fuels
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.11 mg/Kg 1U 2.11 0.633 06/07/13 00:13
Surrogates
4-Bromofluorobenzene 99.1 % 150-150 06/07/13 00:13
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:31
Prep Initial Wt./Vol.: 63.587 g
Prep Extract Vol: 26.3032 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/07/13 00:13
Container ID: 1132110018-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C293
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Volatile GC/MS
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,1,1-Trichloroethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,1,2,2-Tetrachloroethane 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
1,1,2-Trichloroethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,1-Dichloroethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,1-Dichloroethene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,1-Dichloropropene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2,3-Trichlorobenzene 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
1,2,3-Trichloropropane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2,4-Trichlorobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2,4-Trimethylbenzene 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
1,2-Dibromo-3-chloropropane 84.5 ug/Kg 1U 84.5 26.2 06/03/13 19:49
1,2-Dibromoethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2-Dichlorobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2-Dichloroethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,2-Dichloropropane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,3,5-Trimethylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,3-Dichlorobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,3-Dichloropropane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
1,4-Dichlorobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
2,2-Dichloropropane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
2-Butanone (MEK) 211 ug/Kg 1U 211 65.9 06/03/13 19:49
2-Chlorotoluene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
2-Hexanone 211 ug/Kg 1U 211 65.9 06/03/13 19:49
4-Chlorotoluene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
4-Isopropyltoluene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
4-Methyl-2-pentanone (MIBK) 211 ug/Kg 1U 211 65.9 06/03/13 19:49
Benzene 10.6 ug/Kg 1U 10.6 3.29 06/03/13 19:49
Bromobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Bromochloromethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Bromodichloromethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Bromoform 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Bromomethane 169 ug/Kg 1U 169 52.4 06/03/13 19:49
Carbon disulfide 84.5 ug/Kg 1U 84.5 26.2 06/03/13 19:49
Carbon tetrachloride 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Chlorobenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Chloroethane 169 ug/Kg 1U 169 52.4 06/03/13 19:49
Chloroform 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Chloromethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
cis-1,2-Dichloroethene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
cis-1,3-Dichloropropene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Dibromochloromethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Dibromomethane 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Dichlorodifluoromethane 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C294
Client Sample ID: SMIC-M (1.5) D
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110018
Lab Project ID: 1132110
Collection Date: 05/31/13 13:31
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 98.0
Results by Volatile GC/MS
Results of SMIC-M (1.5) D
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Hexachlorobutadiene 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
Isopropylbenzene (Cumene) 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Methyl-t-butyl ether 84.5 ug/Kg 1U 84.5 26.2 06/03/13 19:49
Methylene chloride 84.5 ug/Kg 1U 84.5 26.2 06/03/13 19:49
n-Butylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
n-Propylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Naphthalene 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
o-Xylene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
P & M -Xylene 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
sec-Butylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Styrene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
tert-Butylbenzene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Tetrachloroethene 10.6 ug/Kg 1U 10.6 3.29 06/03/13 19:49
Toluene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
trans-1,2-Dichloroethene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
trans-1,3-Dichloropropene 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Trichloroethene 10.6 ug/Kg 1U 10.6 3.29 06/03/13 19:49
Trichlorofluoromethane 42.2 ug/Kg 1U 42.2 12.7 06/03/13 19:49
Vinyl chloride 21.1 ug/Kg 1U 21.1 6.59 06/03/13 19:49
Xylenes (total) 84.5 ug/Kg 1U 84.5 26.2 06/03/13 19:49
Surrogates
1,2-Dichloroethane-D4 119 % 179-118 06/03/13 19:49*4-Bromofluorobenzene 101 % 167-138 06/03/13 19:49
Toluene-d8 107 % 185-115 06/03/13 19:49
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 13:31
Prep Initial Wt./Vol.: 63.587 g
Prep Extract Vol: 26.3032 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 19:49
Container ID: 1132110018-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C295
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Metals by ICP/MS
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 14.3 mg/Kg 100.976 0.302 06/04/13 18:28
Barium 32.9 mg/Kg 100.293 0.0917 06/04/13 18:28
Cadmium 0.195 mg/Kg 10U 0.195 0.0605 06/04/13 18:28
Chromium 39.3 mg/Kg 100.390 0.117 06/04/13 18:28
Lead 7.88 mg/Kg 100.195 0.0605 06/04/13 18:28
Mercury 0.0749 mg/Kg 100.0390 0.0117 06/04/13 18:28
Selenium 0.488 mg/Kg 10U 0.488 0.146 06/04/13 18:28
Silver 0.0976 mg/Kg 10U 0.0976 0.0302 06/04/13 18:28
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.054 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:28
Container ID: 1132110019-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C296
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Semivolatile Organic Fuels
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.4 mg/Kg 1U 20.4 6.31 06/08/13 22:41
Surrogates
5a Androstane 114 % 150-150 06/08/13 22:41
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.309 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:41
Container ID: 1132110019-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 23.7 mg/Kg 120.4 6.31 06/08/13 22:41
Surrogates
n-Triacontane-d62 132 % 150-150 06/08/13 22:41
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.309 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:41
Container ID: 1132110019-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C297
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Semivolatile Organic GC/MS
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
1,2-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
1,3-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
1,4-Dichlorobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
1-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,4,5-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,4,6-Trichlorophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,4-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,4-Dimethylphenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,4-Dinitrophenol 3.06 mg/Kg 1U 3.06 0.958 06/12/13 01:38
2,4-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,6-Dichlorophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2,6-Dinitrotoluene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Chloronaphthalene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Chlorophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Methyl-4,6-dinitrophenol 2.04 mg/Kg 1U 2.04 0.632 06/12/13 01:38
2-Methylnaphthalene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Methylphenol (o-Cresol) 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Nitroaniline 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
2-Nitrophenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.316 06/12/13 01:38
3,3-Dichlorobenzidine 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
3-Nitroaniline 0.510 mg/Kg 1U 0.510 0.153 06/12/13 01:38
4-Bromophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
4-Chloro-3-methylphenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
4-Chloroaniline 0.510 mg/Kg 1U 0.510 0.153 06/12/13 01:38
4-Chlorophenyl-phenylether 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
4-Nitroaniline 3.06 mg/Kg 1U 3.06 0.958 06/12/13 01:38
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.316 06/12/13 01:38
Acenaphthene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Acenaphthylene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Aniline 2.04 mg/Kg 1U 2.04 0.632 06/12/13 01:38
Anthracene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Azobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzo(a)Anthracene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzo[a]pyrene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzo[b]Fluoranthene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzo[g,h,i]perylene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzo[k]fluoranthene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Benzoic acid 1.53 mg/Kg 1U 1.53 0.764 06/12/13 01:38
Benzyl alcohol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Bis(2-Chloroethoxy)methane 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Bis(2-Chloroethyl)ether 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
bis(2-Ethylhexyl)phthalate 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C298
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Semivolatile Organic GC/MS
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Butylbenzylphthalate 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Carbazole 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Chrysene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Di-n-butylphthalate 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
di-n-Octylphthalate 0.510 mg/Kg 1U 0.510 0.153 06/12/13 01:38
Dibenzo[a,h]anthracene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Dibenzofuran 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Diethylphthalate 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Dimethylphthalate 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Fluoranthene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Fluorene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Hexachlorobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Hexachlorobutadiene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Hexachlorocyclopentadiene 0.713 mg/Kg 1U 0.713 0.204 06/12/13 01:38
Hexachloroethane 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Indeno[1,2,3-c,d] pyrene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Isophorone 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
N-Nitroso-di-n-propylamine 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
N-Nitrosodimethylamine 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
N-Nitrosodiphenylamine 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Naphthalene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Nitrobenzene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Pentachlorophenol 2.04 mg/Kg 1U 2.04 0.632 06/12/13 01:38
Phenanthrene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Phenol 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Pyrene 0.255 mg/Kg 1U 0.255 0.0795 06/12/13 01:38
Surrogates
2,4,6-Tribromophenol 89.7 % 135-125 06/12/13 01:38
2-Fluorobiphenyl 88.8 % 145-105 06/12/13 01:38
2-Fluorophenol 61.1 % 135-105 06/12/13 01:38
Nitrobenzene-d5 67.1 % 135-100 06/12/13 01:38
Phenol-d6 72.7 % 140-100 06/12/13 01:38
Terphenyl-d14 99.7 % 130-125 06/12/13 01:38
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.702 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 01:38
Container ID: 1132110019-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C299
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Volatile Fuels
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.21 mg/Kg 1U 2.21 0.662 06/07/13 13:11
Surrogates
4-Bromofluorobenzene 85.4 % 150-150 06/07/13 13:11
Batch Information
Prep Batch: VXX24787
Prep Method: SW5035A
Prep Date/Time: 05/31/13 10:49
Prep Initial Wt./Vol.: 62.269 g
Prep Extract Vol: 26.7173 mL
Analytical Batch: VFC11454
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/07/13 13:11
Container ID: 1132110019-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C300
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Volatile GC/MS
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,1,1-Trichloroethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,1,2,2-Tetrachloroethane 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
1,1,2-Trichloroethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,1-Dichloroethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,1-Dichloroethene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,1-Dichloropropene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2,3-Trichlorobenzene 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
1,2,3-Trichloropropane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2,4-Trichlorobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2,4-Trimethylbenzene 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
1,2-Dibromo-3-chloropropane 88.2 ug/Kg 1U 88.2 27.4 06/03/13 20:05
1,2-Dibromoethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2-Dichlorobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2-Dichloroethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,2-Dichloropropane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,3,5-Trimethylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,3-Dichlorobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,3-Dichloropropane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
1,4-Dichlorobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
2,2-Dichloropropane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
2-Butanone (MEK) 221 ug/Kg 1U 221 68.8 06/03/13 20:05
2-Chlorotoluene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
2-Hexanone 221 ug/Kg 1U 221 68.8 06/03/13 20:05
4-Chlorotoluene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
4-Isopropyltoluene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
4-Methyl-2-pentanone (MIBK) 221 ug/Kg 1U 221 68.8 06/03/13 20:05
Benzene 11.0 ug/Kg 1U 11.0 3.44 06/03/13 20:05
Bromobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Bromochloromethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Bromodichloromethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Bromoform 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Bromomethane 176 ug/Kg 1U 176 54.7 06/03/13 20:05
Carbon disulfide 88.2 ug/Kg 1U 88.2 27.4 06/03/13 20:05
Carbon tetrachloride 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Chlorobenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Chloroethane 176 ug/Kg 1U 176 54.7 06/03/13 20:05
Chloroform 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Chloromethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
cis-1,2-Dichloroethene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
cis-1,3-Dichloropropene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Dibromochloromethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Dibromomethane 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Dichlorodifluoromethane 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C301
Client Sample ID: SMIC-N (0)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110019
Lab Project ID: 1132110
Collection Date: 05/31/13 10:49
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 97.2
Results by Volatile GC/MS
Results of SMIC-N (0)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Hexachlorobutadiene 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
Isopropylbenzene (Cumene) 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Methyl-t-butyl ether 88.2 ug/Kg 1U 88.2 27.4 06/03/13 20:05
Methylene chloride 88.2 ug/Kg 1U 88.2 27.4 06/03/13 20:05
n-Butylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
n-Propylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Naphthalene 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
o-Xylene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
P & M -Xylene 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
sec-Butylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Styrene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
tert-Butylbenzene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Tetrachloroethene 11.0 ug/Kg 1U 11.0 3.44 06/03/13 20:05
Toluene 50.5 ug/Kg 122.1 6.88 06/03/13 20:05
trans-1,2-Dichloroethene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
trans-1,3-Dichloropropene 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Trichloroethene 11.0 ug/Kg 1U 11.0 3.44 06/03/13 20:05
Trichlorofluoromethane 44.1 ug/Kg 1U 44.1 13.2 06/03/13 20:05
Vinyl chloride 22.1 ug/Kg 1U 22.1 6.88 06/03/13 20:05
Xylenes (total) 88.2 ug/Kg 1U 88.2 27.4 06/03/13 20:05
Surrogates
1,2-Dichloroethane-D4 103 % 179-118 06/03/13 20:05
4-Bromofluorobenzene 80.8 % 167-138 06/03/13 20:05
Toluene-d8 89.1 % 185-115 06/03/13 20:05
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/31/13 10:49
Prep Initial Wt./Vol.: 62.269 g
Prep Extract Vol: 26.7173 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 20:05
Container ID: 1132110019-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C302
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Metals by ICP/MS
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 17.3 mg/Kg 101.00 0.310 06/04/13 18:30
Barium 30.0 mg/Kg 100.300 0.0940 06/04/13 18:30
Cadmium 0.200 mg/Kg 10U 0.200 0.0620 06/04/13 18:30
Chromium 36.6 mg/Kg 100.400 0.120 06/04/13 18:30
Lead 9.04 mg/Kg 100.200 0.0620 06/04/13 18:30
Mercury 0.0561 mg/Kg 100.0400 0.0120 06/04/13 18:30
Selenium 0.500 mg/Kg 10U 0.500 0.150 06/04/13 18:30
Silver 0.100 mg/Kg 10U 0.100 0.0310 06/04/13 18:30
Batch Information
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.032 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 18:30
Container ID: 1132110020-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C303
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Semivolatile Organic Fuels
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 20.5 mg/Kg 1U 20.5 6.35 06/08/13 22:51
Surrogates
5a Androstane 123 % 150-150 06/08/13 22:51
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.221 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/08/13 22:51
Container ID: 1132110020-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 44.7 mg/Kg 120.5 6.35 06/08/13 22:51
Surrogates
n-Triacontane-d62 149 % 150-150 06/08/13 22:51
Batch Information
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/13 09:10
Prep Initial Wt./Vol.: 30.221 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/08/13 22:51
Container ID: 1132110020-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C304
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Semivolatile Organic GC/MS
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
1,2-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
1,3-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
1,4-Dichlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
1-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,4,5-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,4,6-Trichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,4-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,4-Dimethylphenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,4-Dinitrophenol 3.05 mg/Kg 1U 3.05 0.956 06/11/13 20:47
2,4-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,6-Dichlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2,6-Dinitrotoluene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Chloronaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Chlorophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Methyl-4,6-dinitrophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 20:47
2-Methylnaphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Methylphenol (o-Cresol) 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Nitroaniline 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
2-Nitrophenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
3&4-Methylphenol (p&m-Cresol) 1.02 mg/Kg 1U 1.02 0.315 06/11/13 20:47
3,3-Dichlorobenzidine 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
3-Nitroaniline 0.508 mg/Kg 1U 0.508 0.153 06/11/13 20:47
4-Bromophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
4-Chloro-3-methylphenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
4-Chloroaniline 0.508 mg/Kg 1U 0.508 0.153 06/11/13 20:47
4-Chlorophenyl-phenylether 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
4-Nitroaniline 3.05 mg/Kg 1U 3.05 0.956 06/11/13 20:47
4-Nitrophenol 1.02 mg/Kg 1U 1.02 0.315 06/11/13 20:47
Acenaphthene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Acenaphthylene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Aniline 2.03 mg/Kg 1U 2.03 0.630 06/11/13 20:47
Anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Azobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzo(a)Anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzo[a]pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzo[b]Fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzo[g,h,i]perylene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzo[k]fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Benzoic acid 1.53 mg/Kg 1U 1.53 0.763 06/11/13 20:47
Benzyl alcohol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Bis(2-Chloroethoxy)methane 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Bis(2-Chloroethyl)ether 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
bis(2-Ethylhexyl)phthalate 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C305
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Semivolatile Organic GC/MS
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Butylbenzylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Carbazole 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Chrysene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Di-n-butylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
di-n-Octylphthalate 0.508 mg/Kg 1U 0.508 0.153 06/11/13 20:47
Dibenzo[a,h]anthracene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Dibenzofuran 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Diethylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Dimethylphthalate 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Fluoranthene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Fluorene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Hexachlorobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Hexachlorobutadiene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Hexachlorocyclopentadiene 0.712 mg/Kg 1U 0.712 0.203 06/11/13 20:47
Hexachloroethane 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Indeno[1,2,3-c,d] pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Isophorone 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
N-Nitroso-di-n-propylamine 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
N-Nitrosodimethylamine 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
N-Nitrosodiphenylamine 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Naphthalene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Nitrobenzene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Pentachlorophenol 2.03 mg/Kg 1U 2.03 0.630 06/11/13 20:47
Phenanthrene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Phenol 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Pyrene 0.254 mg/Kg 1U 0.254 0.0793 06/11/13 20:47
Surrogates
2,4,6-Tribromophenol 85 % 135-125 06/11/13 20:47
2-Fluorobiphenyl 78.6 % 145-105 06/11/13 20:47
2-Fluorophenol 58.6 % 135-105 06/11/13 20:47
Nitrobenzene-d5 57.3 % 135-100 06/11/13 20:47
Phenol-d6 66.7 % 140-100 06/11/13 20:47
Terphenyl-d14 91.1 % 130-125 06/11/13 20:47
Batch Information
Prep Batch: XXX29103
Prep Method: SW3550C
Prep Date/Time: 06/05/13 12:00
Prep Initial Wt./Vol.: 22.838 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/11/13 20:47
Container ID: 1132110020-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C306
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Volatile Fuels
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.69 mg/Kg 1U 2.69 0.807 06/05/13 04:27
Surrogates
4-Bromofluorobenzene 87 % 150-150 06/05/13 04:27
Batch Information
Prep Batch: VXX24768
Prep Method: SW5035A
Prep Date/Time: 05/31/13 10:56
Prep Initial Wt./Vol.: 50.99 g
Prep Extract Vol: 26.5902 mL
Analytical Batch: VFC11446
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/05/13 04:27
Container ID: 1132110020-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C307
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Volatile GC/MS
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,1,1-Trichloroethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,1,2,2-Tetrachloroethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
1,1,2-Trichloroethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,1-Dichloroethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,1-Dichloroethene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,1-Dichloropropene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2,3-Trichlorobenzene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
1,2,3-Trichloropropane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2,4-Trichlorobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2,4-Trimethylbenzene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
1,2-Dibromo-3-chloropropane 108 ug/Kg 1U 108 33.4 06/04/13 14:10
1,2-Dibromoethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2-Dichloroethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,2-Dichloropropane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,3,5-Trimethylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,3-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,3-Dichloropropane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
1,4-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
2,2-Dichloropropane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
2-Butanone (MEK) 269 ug/Kg 1U 269 84.0 06/04/13 14:10
2-Chlorotoluene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
2-Hexanone 269 ug/Kg 1U 269 84.0 06/04/13 14:10
4-Chlorotoluene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
4-Isopropyltoluene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
4-Methyl-2-pentanone (MIBK) 269 ug/Kg 1U 269 84.0 06/04/13 14:10
Benzene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:10
Bromobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Bromochloromethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Bromodichloromethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Bromoform 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Bromomethane 215 ug/Kg 1U 215 66.7 06/04/13 14:10
Carbon disulfide 108 ug/Kg 1U 108 33.4 06/04/13 14:10
Carbon tetrachloride 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Chlorobenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Chloroethane 215 ug/Kg 1U 215 66.7 06/04/13 14:10
Chloroform 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Chloromethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
cis-1,2-Dichloroethene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
cis-1,3-Dichloropropene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Dibromochloromethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Dibromomethane 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Dichlorodifluoromethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C308
Client Sample ID: SMIC-N (1.5)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110020
Lab Project ID: 1132110
Collection Date: 05/31/13 10:56
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 96.9
Results by Volatile GC/MS
Results of SMIC-N (1.5)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Hexachlorobutadiene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
Isopropylbenzene (Cumene) 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Methyl-t-butyl ether 108 ug/Kg 1U 108 33.4 06/04/13 14:10
Methylene chloride 108 ug/Kg 1U 108 33.4 06/04/13 14:10
n-Butylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
n-Propylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Naphthalene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
o-Xylene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
P & M -Xylene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
sec-Butylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Styrene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
tert-Butylbenzene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Tetrachloroethene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:10
Toluene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
trans-1,2-Dichloroethene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
trans-1,3-Dichloropropene 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Trichloroethene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:10
Trichlorofluoromethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:10
Vinyl chloride 26.9 ug/Kg 1U 26.9 8.40 06/04/13 14:10
Xylenes (total) 108 ug/Kg 1U 108 33.4 06/04/13 14:10
Surrogates
1,2-Dichloroethane-D4 117 % 179-118 06/04/13 14:10
4-Bromofluorobenzene 85.8 % 167-138 06/04/13 14:10
Toluene-d8 102 % 185-115 06/04/13 14:10
Batch Information
Prep Batch: VXX24769
Prep Method: SW5035A
Prep Date/Time: 05/31/13 10:56
Prep Initial Wt./Vol.: 50.99 g
Prep Extract Vol: 26.5902 mL
Analytical Batch: VMS13532
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/04/13 14:10
Container ID: 1132110020-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C309
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Metals by ICP/MS
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 6.34 mg/Kg 101.05 0.326 06/04/13 14:58
Barium 35.1 mg/Kg 100.315 0.0988 06/04/13 14:58
Cadmium 0.210 mg/Kg 10U 0.210 0.0652 06/04/13 14:58
Chromium 37.9 mg/Kg 100.420 0.126 06/04/13 14:58
Lead 4.39 mg/Kg 100.210 0.0652 06/04/13 14:58
Mercury 0.0420 mg/Kg 10U 0.0420 0.0126 06/04/13 14:58
Selenium 0.526 mg/Kg 10U 0.526 0.158 06/04/13 14:58
Silver 0.105 mg/Kg 10U 0.105 0.0326 06/04/13 14:58
Batch Information
Prep Batch: MXX26524
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.048 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 14:58
Container ID: 1132110021-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C310
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Semivolatile Organic Fuels
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 21.7 mg/Kg 1U 21.7 6.71 06/09/13 01:41
Surrogates
5a Androstane 102 % 150-150 06/09/13 01:41
Batch Information
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/13 11:15
Prep Initial Wt./Vol.: 30.527 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/09/13 01:41
Container ID: 1132110021-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 21.7 mg/Kg 1U 21.7 6.71 06/09/13 01:41
Surrogates
n-Triacontane-d62 119 % 150-150 06/09/13 01:41
Batch Information
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/13 11:15
Prep Initial Wt./Vol.: 30.527 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/09/13 01:41
Container ID: 1132110021-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C311
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Semivolatile Organic GC/MS
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
1,2-Dichlorobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
1,3-Dichlorobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
1,4-Dichlorobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
1-Chloronaphthalene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,4,5-Trichlorophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,4,6-Trichlorophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,4-Dichlorophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,4-Dimethylphenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,4-Dinitrophenol 3.26 mg/Kg 1U 3.26 1.02 06/06/13 02:29
2,4-Dinitrotoluene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,6-Dichlorophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2,6-Dinitrotoluene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Chloronaphthalene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Chlorophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Methyl-4,6-dinitrophenol 2.17 mg/Kg 1U 2.17 0.673 06/06/13 02:29
2-Methylnaphthalene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Methylphenol (o-Cresol) 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Nitroaniline 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
2-Nitrophenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
3&4-Methylphenol (p&m-Cresol) 1.09 mg/Kg 1U 1.09 0.337 06/06/13 02:29
3,3-Dichlorobenzidine 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
3-Nitroaniline 0.543 mg/Kg 1U 0.543 0.163 06/06/13 02:29
4-Bromophenyl-phenylether 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
4-Chloro-3-methylphenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
4-Chloroaniline 0.543 mg/Kg 1U 0.543 0.163 06/06/13 02:29
4-Chlorophenyl-phenylether 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
4-Nitroaniline 3.26 mg/Kg 1U 3.26 1.02 06/06/13 02:29
4-Nitrophenol 1.09 mg/Kg 1U 1.09 0.337 06/06/13 02:29
Acenaphthene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Acenaphthylene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Aniline 2.17 mg/Kg 1U 2.17 0.673 06/06/13 02:29
Anthracene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Azobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzo(a)Anthracene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzo[a]pyrene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzo[b]Fluoranthene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzo[g,h,i]perylene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzo[k]fluoranthene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Benzoic acid 1.63 mg/Kg 1U 1.63 0.814 06/06/13 02:29
Benzyl alcohol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Bis(2-Chloroethoxy)methane 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Bis(2-Chloroethyl)ether 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
bis(2-Ethylhexyl)phthalate 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C312
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Semivolatile Organic GC/MS
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Butylbenzylphthalate 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Carbazole 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Chrysene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Di-n-butylphthalate 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
di-n-Octylphthalate 0.543 mg/Kg 1U 0.543 0.163 06/06/13 02:29
Dibenzo[a,h]anthracene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Dibenzofuran 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Diethylphthalate 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Dimethylphthalate 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Fluoranthene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Fluorene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Hexachlorobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Hexachlorobutadiene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Hexachlorocyclopentadiene 0.760 mg/Kg 1U 0.760 0.217 06/06/13 02:29
Hexachloroethane 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Indeno[1,2,3-c,d] pyrene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Isophorone 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
N-Nitroso-di-n-propylamine 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
N-Nitrosodimethylamine 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
N-Nitrosodiphenylamine 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Naphthalene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Nitrobenzene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Pentachlorophenol 2.17 mg/Kg 1U 2.17 0.673 06/06/13 02:29
Phenanthrene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Phenol 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Pyrene 0.271 mg/Kg 1U 0.271 0.0847 06/06/13 02:29
Surrogates
2,4,6-Tribromophenol 85.3 % 135-125 06/06/13 02:29
2-Fluorobiphenyl 83.4 % 145-105 06/06/13 02:29
2-Fluorophenol 64.7 % 135-105 06/06/13 02:29
Nitrobenzene-d5 71.4 % 135-100 06/06/13 02:29
Phenol-d6 74.9 % 140-100 06/06/13 02:29
Terphenyl-d14 119 % 130-125 06/06/13 02:29
Batch Information
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/13 14:00
Prep Initial Wt./Vol.: 22.83 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Analyst: RTS
Analytical Date/Time: 06/06/13 02:29
Container ID: 1132110021-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C313
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Volatile Fuels
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.69 mg/Kg 1U 2.69 0.807 06/07/13 13:48
Surrogates
4-Bromofluorobenzene 95.9 % 150-150 06/07/13 13:48
Batch Information
Prep Batch: VXX24787
Prep Method: SW5035A
Prep Date/Time: 05/31/13 11:10
Prep Initial Wt./Vol.: 63.114 g
Prep Extract Vol: 30.8239 mL
Analytical Batch: VFC11454
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/07/13 13:48
Container ID: 1132110021-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C314
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Volatile GC/MS
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,1,1-Trichloroethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,1,2,2-Tetrachloroethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
1,1,2-Trichloroethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,1-Dichloroethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,1-Dichloroethene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,1-Dichloropropene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2,3-Trichlorobenzene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
1,2,3-Trichloropropane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2,4-Trichlorobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2,4-Trimethylbenzene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
1,2-Dibromo-3-chloropropane 108 ug/Kg 1U 108 33.4 06/04/13 14:26
1,2-Dibromoethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2-Dichloroethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,2-Dichloropropane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,3,5-Trimethylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,3-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,3-Dichloropropane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
1,4-Dichlorobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
2,2-Dichloropropane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
2-Butanone (MEK) 269 ug/Kg 1U 269 83.9 06/04/13 14:26
2-Chlorotoluene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
2-Hexanone 269 ug/Kg 1U 269 83.9 06/04/13 14:26
4-Chlorotoluene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
4-Isopropyltoluene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
4-Methyl-2-pentanone (MIBK) 269 ug/Kg 1U 269 83.9 06/04/13 14:26
Benzene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:26
Bromobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Bromochloromethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Bromodichloromethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Bromoform 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Bromomethane 215 ug/Kg 1U 215 66.7 06/04/13 14:26
Carbon disulfide 108 ug/Kg 1U 108 33.4 06/04/13 14:26
Carbon tetrachloride 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Chlorobenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Chloroethane 215 ug/Kg 1U 215 66.7 06/04/13 14:26
Chloroform 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Chloromethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
cis-1,2-Dichloroethene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
cis-1,3-Dichloropropene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Dibromochloromethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Dibromomethane 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Dichlorodifluoromethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C315
Client Sample ID: SMIC-N (10)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110021
Lab Project ID: 1132110
Collection Date: 05/31/13 11:10
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.8
Results by Volatile GC/MS
Results of SMIC-N (10)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Hexachlorobutadiene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
Isopropylbenzene (Cumene) 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Methyl-t-butyl ether 108 ug/Kg 1U 108 33.4 06/04/13 14:26
Methylene chloride 108 ug/Kg 1U 108 33.4 06/04/13 14:26
n-Butylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
n-Propylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Naphthalene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
o-Xylene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
P & M -Xylene 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
sec-Butylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Styrene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
tert-Butylbenzene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Tetrachloroethene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:26
Toluene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
trans-1,2-Dichloroethene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
trans-1,3-Dichloropropene 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Trichloroethene 13.5 ug/Kg 1U 13.5 4.20 06/04/13 14:26
Trichlorofluoromethane 53.8 ug/Kg 1U 53.8 16.1 06/04/13 14:26
Vinyl chloride 26.9 ug/Kg 1U 26.9 8.39 06/04/13 14:26
Xylenes (total) 108 ug/Kg 1U 108 33.4 06/04/13 14:26
Surrogates
1,2-Dichloroethane-D4 117 % 179-118 06/04/13 14:26
4-Bromofluorobenzene 92.7 % 167-138 06/04/13 14:26
Toluene-d8 101 % 185-115 06/04/13 14:26
Batch Information
Prep Batch: VXX24769
Prep Method: SW5035A
Prep Date/Time: 05/31/13 11:10
Prep Initial Wt./Vol.: 63.114 g
Prep Extract Vol: 30.8239 mL
Analytical Batch: VMS13532
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/04/13 14:26
Container ID: 1132110021-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C316
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Metals by ICP/MS
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Arsenic 8.08 mg/Kg 101.08 0.336 06/04/13 15:00
Barium 50.3 mg/Kg 100.325 0.102 06/04/13 15:00
Cadmium 0.217 mg/Kg 10U 0.217 0.0672 06/04/13 15:00
Chromium 29.2 mg/Kg 100.434 0.130 06/04/13 15:00
Lead 7.48 mg/Kg 100.217 0.0672 06/04/13 15:00
Mercury 0.0434 mg/Kg 10U 0.0434 0.0130 06/04/13 15:00
Selenium 0.542 mg/Kg 10U 0.542 0.163 06/04/13 15:00
Silver 0.108 mg/Kg 10U 0.108 0.0336 06/04/13 15:00
Batch Information
Prep Batch: MXX26524
Prep Method: SW3050B
Prep Date/Time: 06/04/13 09:35
Prep Initial Wt./Vol.: 1.02 g
Prep Extract Vol: 50 mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Analyst: HKS
Analytical Date/Time: 06/04/13 15:00
Container ID: 1132110022-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C317
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Semivolatile Organic Fuels
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Diesel Range Organics 22.0 mg/Kg 1U 22.0 6.81 06/09/13 01:51
Surrogates
5a Androstane 99.5 % 150-150 06/09/13 01:51
Batch Information
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/13 11:15
Prep Initial Wt./Vol.: 30.222 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK102
Analyst: MCM
Analytical Date/Time: 06/09/13 01:51
Container ID: 1132110022-A
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Residual Range Organics 22.0 mg/Kg 1U 22.0 6.81 06/09/13 01:51
Surrogates
n-Triacontane-d62 115 % 150-150 06/09/13 01:51
Batch Information
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/13 11:15
Prep Initial Wt./Vol.: 30.222 g
Prep Extract Vol: 1 mL
Analytical Batch: XFC10918
Analytical Method: AK103
Analyst: MCM
Analytical Date/Time: 06/09/13 01:51
Container ID: 1132110022-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C318
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Semivolatile Organic GC/MS
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,2,4-Trichlorobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
1,2-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
1,3-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
1,4-Dichlorobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
1-Chloronaphthalene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,4,5-Trichlorophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,4,6-Trichlorophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,4-Dichlorophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,4-Dimethylphenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,4-Dinitrophenol 3.26 mg/Kg 1U 3.26 1.02 06/12/13 01:55
2,4-Dinitrotoluene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,6-Dichlorophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2,6-Dinitrotoluene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Chloronaphthalene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Chlorophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Methyl-4,6-dinitrophenol 2.17 mg/Kg 1U 2.17 0.674 06/12/13 01:55
2-Methylnaphthalene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Methylphenol (o-Cresol) 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Nitroaniline 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
2-Nitrophenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
3&4-Methylphenol (p&m-Cresol) 1.09 mg/Kg 1U 1.09 0.337 06/12/13 01:55
3,3-Dichlorobenzidine 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
3-Nitroaniline 0.543 mg/Kg 1U 0.543 0.163 06/12/13 01:55
4-Bromophenyl-phenylether 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
4-Chloro-3-methylphenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
4-Chloroaniline 0.543 mg/Kg 1U 0.543 0.163 06/12/13 01:55
4-Chlorophenyl-phenylether 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
4-Nitroaniline 3.26 mg/Kg 1U 3.26 1.02 06/12/13 01:55
4-Nitrophenol 1.09 mg/Kg 1U 1.09 0.337 06/12/13 01:55
Acenaphthene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Acenaphthylene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Aniline 2.17 mg/Kg 1U 2.17 0.674 06/12/13 01:55
Anthracene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Azobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzo(a)Anthracene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzo[a]pyrene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzo[b]Fluoranthene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzo[g,h,i]perylene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzo[k]fluoranthene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Benzoic acid 1.63 mg/Kg 1U 1.63 0.815 06/12/13 01:55
Benzyl alcohol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Bis(2-Chloroethoxy)methane 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Bis(2-Chloroethyl)ether 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
bis(2-Ethylhexyl)phthalate 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C319
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Semivolatile Organic GC/MS
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Bis(2chloro1methylethyl)Ether 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Butylbenzylphthalate 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Carbazole 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Chrysene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Di-n-butylphthalate 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
di-n-Octylphthalate 0.543 mg/Kg 1U 0.543 0.163 06/12/13 01:55
Dibenzo[a,h]anthracene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Dibenzofuran 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Diethylphthalate 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Dimethylphthalate 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Fluoranthene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Fluorene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Hexachlorobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Hexachlorobutadiene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Hexachlorocyclopentadiene 0.761 mg/Kg 1U 0.761 0.217 06/12/13 01:55
Hexachloroethane 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Indeno[1,2,3-c,d] pyrene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Isophorone 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
N-Nitroso-di-n-propylamine 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
N-Nitrosodimethylamine 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
N-Nitrosodiphenylamine 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Naphthalene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Nitrobenzene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Pentachlorophenol 2.17 mg/Kg 1U 2.17 0.674 06/12/13 01:55
Phenanthrene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Phenol 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Pyrene 0.272 mg/Kg 1U 0.272 0.0847 06/12/13 01:55
Surrogates
2,4,6-Tribromophenol 91.1 % 135-125 06/12/13 01:55
2-Fluorobiphenyl 85.1 % 145-105 06/12/13 01:55
2-Fluorophenol 63.6 % 135-105 06/12/13 01:55
Nitrobenzene-d5 65.1 % 135-100 06/12/13 01:55
Phenol-d6 71.6 % 140-100 06/12/13 01:55
Terphenyl-d14 99.7 % 130-125 06/12/13 01:55
Batch Information
Prep Batch: XXX29103
Prep Method: SW3550C
Prep Date/Time: 06/05/13 12:00
Prep Initial Wt./Vol.: 22.907 g
Prep Extract Vol: 1 mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Analyst: DSH
Analytical Date/Time: 06/12/13 01:55
Container ID: 1132110022-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C320
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Volatile Fuels
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.35 mg/Kg 1U 2.35 0.704 06/07/13 14:06
Surrogates
4-Bromofluorobenzene 98.5 % 150-150 06/07/13 14:06
Batch Information
Prep Batch: VXX24787
Prep Method: SW5035A
Prep Date/Time: 05/31/13 11:45
Prep Initial Wt./Vol.: 76.179 g
Prep Extract Vol: 32.3084 mL
Analytical Batch: VFC11454
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/07/13 14:06
Container ID: 1132110022-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C321
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Volatile GC/MS
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,1,1-Trichloroethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,1,2,2-Tetrachloroethane 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
1,1,2-Trichloroethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,1-Dichloroethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,1-Dichloroethene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,1-Dichloropropene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2,3-Trichlorobenzene 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
1,2,3-Trichloropropane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2,4-Trichlorobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2,4-Trimethylbenzene 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
1,2-Dibromo-3-chloropropane 93.8 ug/Kg 1U 93.8 29.1 06/04/13 14:43
1,2-Dibromoethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2-Dichlorobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2-Dichloroethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,2-Dichloropropane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,3,5-Trimethylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,3-Dichlorobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,3-Dichloropropane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
1,4-Dichlorobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
2,2-Dichloropropane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
2-Butanone (MEK) 235 ug/Kg 1U 235 73.2 06/04/13 14:43
2-Chlorotoluene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
2-Hexanone 235 ug/Kg 1U 235 73.2 06/04/13 14:43
4-Chlorotoluene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
4-Isopropyltoluene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
4-Methyl-2-pentanone (MIBK) 235 ug/Kg 1U 235 73.2 06/04/13 14:43
Benzene 11.7 ug/Kg 1U 11.7 3.66 06/04/13 14:43
Bromobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Bromochloromethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Bromodichloromethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Bromoform 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Bromomethane 188 ug/Kg 1U 188 58.2 06/04/13 14:43
Carbon disulfide 93.8 ug/Kg 1U 93.8 29.1 06/04/13 14:43
Carbon tetrachloride 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Chlorobenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Chloroethane 188 ug/Kg 1U 188 58.2 06/04/13 14:43
Chloroform 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Chloromethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
cis-1,2-Dichloroethene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
cis-1,3-Dichloropropene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Dibromochloromethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Dibromomethane 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Dichlorodifluoromethane 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C322
Client Sample ID: SMIC-N (30)
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110022
Lab Project ID: 1132110
Collection Date: 05/31/13 11:45
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%): 90.4
Results by Volatile GC/MS
Results of SMIC-N (30)
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Hexachlorobutadiene 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
Isopropylbenzene (Cumene) 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Methyl-t-butyl ether 93.8 ug/Kg 1U 93.8 29.1 06/04/13 14:43
Methylene chloride 93.8 ug/Kg 1U 93.8 29.1 06/04/13 14:43
n-Butylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
n-Propylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Naphthalene 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
o-Xylene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
P & M -Xylene 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
sec-Butylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Styrene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
tert-Butylbenzene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Tetrachloroethene 11.7 ug/Kg 1U 11.7 3.66 06/04/13 14:43
Toluene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
trans-1,2-Dichloroethene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
trans-1,3-Dichloropropene 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Trichloroethene 11.7 ug/Kg 1U 11.7 3.66 06/04/13 14:43
Trichlorofluoromethane 46.9 ug/Kg 1U 46.9 14.1 06/04/13 14:43
Vinyl chloride 23.5 ug/Kg 1U 23.5 7.32 06/04/13 14:43
Xylenes (total) 93.8 ug/Kg 1U 93.8 29.1 06/04/13 14:43
Surrogates
1,2-Dichloroethane-D4 119 % 179-118 06/04/13 14:43*4-Bromofluorobenzene 103 % 167-138 06/04/13 14:43
Toluene-d8 101 % 185-115 06/04/13 14:43
Batch Information
Prep Batch: VXX24769
Prep Method: SW5035A
Prep Date/Time: 05/31/13 11:45
Prep Initial Wt./Vol.: 76.179 g
Prep Extract Vol: 32.3084 mL
Analytical Batch: VMS13532
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/04/13 14:43
Container ID: 1132110022-B
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C323
Client Sample ID: Trip Blank
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110023
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile Fuels
Results of Trip Blank
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Gasoline Range Organics 2.54 mg/Kg 1U 2.54 0.762 06/06/13 20:47
Surrogates
4-Bromofluorobenzene 101 % 150-150 06/06/13 20:47
Batch Information
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:29
Prep Initial Wt./Vol.: 49.225 g
Prep Extract Vol: 25 mL
Analytical Batch: VFC11451
Analytical Method: AK101
Analyst: ST
Analytical Date/Time: 06/06/13 20:47
Container ID: 1132110023-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C324
Client Sample ID: Trip Blank
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110023
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile GC/MS
Results of Trip Blank
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
1,1,1,2-Tetrachloroethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,1,1-Trichloroethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,1,2,2-Tetrachloroethane 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
1,1,2-Trichloroethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,1-Dichloroethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,1-Dichloroethene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,1-Dichloropropene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2,3-Trichlorobenzene 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
1,2,3-Trichloropropane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2,4-Trichlorobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2,4-Trimethylbenzene 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
1,2-Dibromo-3-chloropropane 102 ug/Kg 1U 102 31.5 06/03/13 14:47
1,2-Dibromoethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2-Dichlorobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2-Dichloroethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,2-Dichloropropane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,3,5-Trimethylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,3-Dichlorobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,3-Dichloropropane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
1,4-Dichlorobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
2,2-Dichloropropane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
2-Butanone (MEK) 254 ug/Kg 1U 254 79.2 06/03/13 14:47
2-Chlorotoluene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
2-Hexanone 254 ug/Kg 1U 254 79.2 06/03/13 14:47
4-Chlorotoluene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
4-Isopropyltoluene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
4-Methyl-2-pentanone (MIBK) 254 ug/Kg 1U 254 79.2 06/03/13 14:47
Benzene 12.7 ug/Kg 1U 12.7 3.96 06/03/13 14:47
Bromobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Bromochloromethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Bromodichloromethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Bromoform 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Bromomethane 203 ug/Kg 1U 203 63.0 06/03/13 14:47
Carbon disulfide 102 ug/Kg 1U 102 31.5 06/03/13 14:47
Carbon tetrachloride 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Chlorobenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Chloroethane 203 ug/Kg 1U 203 63.0 06/03/13 14:47
Chloroform 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Chloromethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
cis-1,2-Dichloroethene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
cis-1,3-Dichloropropene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Dibromochloromethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Dibromomethane 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Dichlorodifluoromethane 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C325
Client Sample ID: Trip Blank
Client Project ID: SMIC Improvements 1770.01
Lab Sample ID: 1132110023
Lab Project ID: 1132110
Collection Date: 05/30/13 10:29
Received Date: 06/03/13 09:25
Matrix: Soil/Solid (dry weight)
Solids (%):
Results by Volatile GC/MS
Results of Trip Blank
Date AnalyzedParameter DFUnitsQualResult LOQ/CL DL
Ethylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Hexachlorobutadiene 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
Isopropylbenzene (Cumene) 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Methyl-t-butyl ether 102 ug/Kg 1U 102 31.5 06/03/13 14:47
Methylene chloride 102 ug/Kg 1U 102 31.5 06/03/13 14:47
n-Butylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
n-Propylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Naphthalene 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
o-Xylene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
P & M -Xylene 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
sec-Butylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Styrene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
tert-Butylbenzene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Tetrachloroethene 12.7 ug/Kg 1U 12.7 3.96 06/03/13 14:47
Toluene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
trans-1,2-Dichloroethene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
trans-1,3-Dichloropropene 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Trichloroethene 12.7 ug/Kg 1U 12.7 3.96 06/03/13 14:47
Trichlorofluoromethane 50.8 ug/Kg 1U 50.8 15.2 06/03/13 14:47
Vinyl chloride 25.4 ug/Kg 1U 25.4 7.92 06/03/13 14:47
Xylenes (total) 102 ug/Kg 1U 102 31.5 06/03/13 14:47
Surrogates
1,2-Dichloroethane-D4 108 % 179-118 06/03/13 14:47
4-Bromofluorobenzene 93.9 % 167-138 06/03/13 14:47
Toluene-d8 99.3 % 185-115 06/03/13 14:47
Batch Information
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 05/30/13 10:29
Prep Initial Wt./Vol.: 49.225 g
Prep Extract Vol: 25 mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Analyst: HM
Analytical Date/Time: 06/03/13 14:47
Container ID: 1132110023-A
Print Date: 06/27/2013 5:39:07PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C326
Blank ID: MB for HBN 1453096 [MXX/26523]
Blank Lab ID: 1150929
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110020
Matrix: Soil/Solid (dry weight)
Results by SW6020
DL UnitsLOQ/CLResultsParameter
Method Blank
Arsenic 1.00 mg/Kg0.3100.620U
Barium 0.300 mg/Kg0.09400.188U
Cadmium 0.200 mg/Kg0.06200.124U
Chromium 0.400 mg/Kg0.1200.240U
Lead 0.200 mg/Kg0.06200.124U
Mercury 0.0400 mg/Kg0.01200.0240U
Selenium 0.500 mg/Kg0.1500.300U
Silver 0.100 mg/Kg0.03100.0620U
Batch Information
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Analytical Date/Time: 6/4/2013 5:23:08PM
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 6/4/2013 9:35:00AM
Prep Initial Wt./Vol.: 1 g
Prep Extract Vol: 50 mL
Print Date: 06/27/2013 5:39:22PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
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C327
Blank Spike ID: LCS for HBN 1132110 [MXX26523]
Blank Spike Lab ID: 1150930
Date Analyzed: 06/04/2013 17:25
Results by SW6020
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110020
Result
Arsenic 50 106 ( 80-120 )52.9
Barium 50 109 ( 80-120 )54.6
Cadmium 5 106 ( 80-120 )5.32
Chromium 20 111 ( 80-120 )22.2
Lead 50 116 ( 80-120 )57.9
Mercury 0.5 102 ( 80-120 )0.510
Selenium 50 110 ( 80-120 )55.0
Silver 5 104 ( 80-120 )5.19
Batch Information
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Prep Batch: MXX26523
Prep Method: SW3050B
Prep Date/Time: 06/04/2013 09:35
Spike Init Wt./Vol.: 50 mg/Kg Extract Vol: 50 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:23PM
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C328
Original Sample ID: 1132110006
MS Sample ID: 1150931 MS
MSD Sample ID: 1150932 MSD
Analysis Date: 06/04/2013 17:27
Analysis Date: 06/04/2013 17:32
Analysis Date: 06/04/2013 17:34
Matrix: Soil/Solid (dry weight)
Results by SW6020
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110020
Matrix Spike Summary
RPD CL
Arsenic 48.94.73 54.8 102 49.6 56.1 103 80-120 2.39 (< 20 )
Barium 48.933.0 94.1 125 49.6 99.1 133 80-120 5.20 (< 20 )* *
Cadmium 4.890.192U 5.21 107 4.96 5.26 106 80-120 0.95 (< 20 )
Chromium 19.647.1 58.6 58 19.9 54.9 39 80-120 6.35 (< 20 )* *
Lead 48.94.78 59.5 112 49.6 60.0 111 80-120 0.86 (< 20 )
Mercury 0.4890.0384U 0.509 104 0.496 0.515 104 80-120 1.30 (< 20 )
Selenium 48.90.480U 52.0 106 49.6 53.5 108 80-120 2.61 (< 20 )
Silver 4.890.0959U 5.04 103 4.96 5.20 105 80-120 3.18 (< 20 )
Batch Information
Prep Batch: MXX26523
Prep Method: Soils/Solids Digest for Metals by ICP-MS
Prep Date/Time: 6/4/2013 9:35:00AM
Prep Initial Wt./Vol.: 1.04g
Prep Extract Vol: 50.00mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Analytical Date/Time: 6/4/2013 5:32:15PM
Print Date: 06/27/2013 5:39:23PM
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C329
Original Sample ID: 1132110006
MS Sample ID: 1150933 BND
MSD Sample ID:
Analysis Date: 06/04/2013 17:27
Analysis Date: 06/04/2013 17:36
Analysis Date:
Matrix: Soil/Solid (dry weight)
Results by SW6020
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110020
Bench Spike Summary
RPD CL
Barium 23933.0 280 103 75-125
Chromium 12047.1 167 100 75-125
Batch Information
Prep Batch: MXX26523
Prep Method: Soils/Solids Digest for Metals by ICP-MS
Prep Date/Time: 6/4/2013 9:35:00AM
Prep Initial Wt./Vol.: 1.06g
Prep Extract Vol: 50.00mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Analytical Date/Time: 6/4/2013 5:36:46PM
Print Date: 06/27/2013 5:39:23PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C330
Blank ID: MB for HBN 1453097 [MXX/26524]
Blank Lab ID: 1150935
QC for Samples:
1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW6020
DL UnitsLOQ/CLResultsParameter
Method Blank
Arsenic 1.00 mg/Kg0.3100.620U
Barium 0.300 mg/Kg0.09400.188U
Cadmium 0.200 mg/Kg0.06200.124U
Chromium 0.400 mg/Kg0.1200.240U
Lead 0.200 mg/Kg0.06200.124U
Mercury 0.0400 mg/Kg0.01200.0240U
Selenium 0.500 mg/Kg0.1500.300U
Silver 0.100 mg/Kg0.03100.0620U
Batch Information
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Analytical Date/Time: 6/4/2013 2:33:57PM
Prep Batch: MXX26524
Prep Method: SW3050B
Prep Date/Time: 6/4/2013 9:35:00AM
Prep Initial Wt./Vol.: 1 g
Prep Extract Vol: 50 mL
Print Date: 06/27/2013 5:39:24PM
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C331
Blank Spike ID: LCS for HBN 1132110 [MXX26524]
Blank Spike Lab ID: 1150936
Date Analyzed: 06/04/2013 14:36
Results by SW6020
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110021, 1132110022
Result
Arsenic 50 109 ( 80-120 )54.4
Barium 50 112 ( 80-120 )56.1
Cadmium 5 108 ( 80-120 )5.38
Chromium 20 113 ( 80-120 )22.7
Lead 50 116 ( 80-120 )58.1
Mercury 0.5 101 ( 80-120 )0.505
Selenium 50 114 ( 80-120 )57.0
Silver 5 109 ( 80-120 )5.43
Batch Information
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Prep Batch: MXX26524
Prep Method: SW3050B
Prep Date/Time: 06/04/2013 09:35
Spike Init Wt./Vol.: 50 mg/Kg Extract Vol: 50 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:25PM
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C332
Original Sample ID: 1131859001
MS Sample ID: 1150937 MS
MSD Sample ID: 1150938 MSD
Analysis Date: 06/04/2013 14:38
Analysis Date: 06/04/2013 14:40
Analysis Date: 06/04/2013 14:42
Matrix: Soil/Solid (dry weight)
Results by SW6020
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110021, 1132110022
Matrix Spike Summary
RPD CL
Lead 55.34.43 68.6 116 52.8 65.0 115 80-120 5.25 (< 20 )
Batch Information
Prep Batch: MXX26524
Prep Method: Soils/Solids Digest for Metals by ICP-MS
Prep Date/Time: 6/4/2013 9:35:00AM
Prep Initial Wt./Vol.: 1.05g
Prep Extract Vol: 50.00mL
Analytical Batch: MMS7983
Analytical Method: SW6020
Instrument: Perkin Elmer Sciex ICP-MS P3
Analyst: HKS
Analytical Date/Time: 6/4/2013 2:40:36PM
Print Date: 06/27/2013 5:39:25PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C333
Blank ID: MB for HBN 1453073 [SPT/9033]
Blank Lab ID: 1150850
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110020, 1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SM21 2540G
DL UnitsLOQ/CLResultsParameter
Method Blank
Total Solids %100
Batch Information
Analytical Batch: SPT9033
Analytical Method: SM21 2540G
Instrument:
Analyst: KRL
Analytical Date/Time: 6/4/2013 5:02:00PM
Print Date: 06/27/2013 5:39:26PM
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C334
Original Sample ID: 1132130002
Duplicate Sample ID: 1151077
Analysis Date: 06/04/2013 17:02
Matrix: Soil/Solid (dry weight)
Results by SM21 2540G
Duplicate Sample Summary
NAME Original (15.00) Duplicate (15.00)
QC for Samples:
RPD CL
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110020, 1132110021, 1132110022
RPD (%)
Total Solids 95.4 95.2 15.000.22
Analytical Batch: SPT9033
Analytical Method: SM21 2540G
Instrument:
Analyst: KRL
Batch Information
Print Date: 06/27/2013 5:39:26PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C335
Blank ID: MB for HBN 1453074 [VXX/24765]
Blank Lab ID: 1150852
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110023
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
1,1,1,2-Tetrachloroethane 25.0 ug/Kg7.8015.6U
1,1,1-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1,2,2-Tetrachloroethane 50.0 ug/Kg15.030.0U
1,1,2-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethene 25.0 ug/Kg7.8015.6U
1,1-Dichloropropene 25.0 ug/Kg7.8015.6U
1,2,3-Trichlorobenzene 50.0 ug/Kg15.030.0U
1,2,3-Trichloropropane 25.0 ug/Kg7.8015.6U
1,2,4-Trichlorobenzene 25.0 ug/Kg7.8015.6U
1,2,4-Trimethylbenzene 50.0 ug/Kg15.030.0U
1,2-Dibromo-3-chloropropane 100 ug/Kg31.062.0U
1,2-Dibromoethane 25.0 ug/Kg7.8015.6U
1,2-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,2-Dichloroethane 25.0 ug/Kg7.8015.6U
1,2-Dichloropropane 25.0 ug/Kg7.8015.6U
1,3,5-Trimethylbenzene 25.0 ug/Kg7.8015.6U
1,3-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,3-Dichloropropane 25.0 ug/Kg7.8015.6U
1,4-Dichlorobenzene 25.0 ug/Kg7.8015.6U
2,2-Dichloropropane 25.0 ug/Kg7.8015.6U
2-Butanone (MEK) 250 ug/Kg78.0156U
2-Chlorotoluene 25.0 ug/Kg7.8015.6U
2-Hexanone 250 ug/Kg78.0156U
4-Chlorotoluene 25.0 ug/Kg7.8015.6U
4-Isopropyltoluene 25.0 ug/Kg7.8015.6U
4-Methyl-2-pentanone (MIBK) 250 ug/Kg78.0156U
Benzene 12.5 ug/Kg3.907.80U
Bromobenzene 25.0 ug/Kg7.8015.6U
Bromochloromethane 25.0 ug/Kg7.8015.6U
Bromodichloromethane 25.0 ug/Kg7.8015.6U
Bromoform 25.0 ug/Kg7.8015.6U
Bromomethane 200 ug/Kg62.0124U
Carbon disulfide 100 ug/Kg31.062.0U
Carbon tetrachloride 25.0 ug/Kg7.8015.6U
Chlorobenzene 25.0 ug/Kg7.8015.6U
Chloroethane 200 ug/Kg62.0124U
Chloroform 25.0 ug/Kg7.8015.6U
Print Date: 06/27/2013 5:39:28PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C336
Blank ID: MB for HBN 1453074 [VXX/24765]
Blank Lab ID: 1150852
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110023
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Chloromethane 25.0 ug/Kg7.8015.6U
cis-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
cis-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Dibromochloromethane 25.0 ug/Kg7.8015.6U
Dibromomethane 25.0 ug/Kg7.8015.6U
Dichlorodifluoromethane 50.0 ug/Kg15.030.0U
Ethylbenzene 25.0 ug/Kg7.8015.6U
Hexachlorobutadiene 50.0 ug/Kg15.030.0U
Isopropylbenzene (Cumene) 25.0 ug/Kg7.8015.6U
Methylene chloride 100 ug/Kg31.062.0U
Methyl-t-butyl ether 100 ug/Kg31.062.0U
Naphthalene 50.0 ug/Kg15.030.0U
n-Butylbenzene 25.0 ug/Kg7.8015.6U
n-Propylbenzene 25.0 ug/Kg7.8015.6U
o-Xylene 25.0 ug/Kg7.8015.6U
P & M -Xylene 50.0 ug/Kg15.030.0U
sec-Butylbenzene 25.0 ug/Kg7.8015.6U
Styrene 25.0 ug/Kg7.8015.6U
tert-Butylbenzene 25.0 ug/Kg7.8015.6U
Tetrachloroethene 12.5 ug/Kg3.907.80U
Toluene 25.0 ug/Kg7.8015.6U
trans-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
trans-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Trichloroethene 12.5 ug/Kg3.907.80U
Trichlorofluoromethane 50.0 ug/Kg15.030.0U
Vinyl chloride 25.0 ug/Kg7.8015.6U
Xylenes (total) 100 ug/Kg31.062.0U
Surrogates
1,2-Dichloroethane-D4 79-118 %113
4-Bromofluorobenzene 67-138 %97.7
Toluene-d8 85-115 %105
Print Date: 06/27/2013 5:39:28PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C337
Blank ID: MB for HBN 1453074 [VXX/24765]
Blank Lab ID: 1150852
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110023
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Batch Information
Analytical Batch: VMS13531
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 6/3/2013 12:58:01PM
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 6/3/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:28PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C338
Blank Spike ID: LCS for HBN 1132110 [VXX24765]
Blank Spike Lab ID: 1150853
Date Analyzed: 06/03/2013 13:19
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Result
1,1,1,2-Tetrachloroethane 750 106 ( 75-125 )796
1,1,1-Trichloroethane 750 112 ( 70-135 )836
1,1,2,2-Tetrachloroethane 750 112 ( 55-130 )837
1,1,2-Trichloroethane 750 111 ( 60-125 )833
1,1-Dichloroethane 750 110 ( 75-125 )828
1,1-Dichloroethene 750 109 ( 65-135 )816
1,1-Dichloropropene 750 111 ( 70-135 )829
1,2,3-Trichlorobenzene 750 103 ( 60-135 )771
1,2,3-Trichloropropane 750 110 ( 65-130 )827
1,2,4-Trichlorobenzene 750 102 ( 65-130 )766
1,2,4-Trimethylbenzene 750 104 ( 65-135 )782
1,2-Dibromo-3-chloropropane 750 119 ( 40-135 )891
1,2-Dibromoethane 750 105 ( 70-125 )790
1,2-Dichlorobenzene 750 102 ( 75-120 )768
1,2-Dichloroethane 750 109 ( 70-135 )814
1,2-Dichloropropane 750 110 ( 70-120 )823
1,3,5-Trimethylbenzene 750 105 ( 65-135 )786
1,3-Dichlorobenzene 750 103 ( 70-125 )775
1,3-Dichloropropane 750 107 ( 75-125 )802
1,4-Dichlorobenzene 750 103 ( 70-125 )775
2,2-Dichloropropane 750 115 ( 65-135 )866
2-Butanone (MEK) 2250 122 ( 30-160 )2760
2-Chlorotoluene 750 106 ( 70-130 )797
2-Hexanone 2250 124 ( 45-145 )2790
4-Chlorotoluene 750 102 ( 75-125 )766
4-Isopropyltoluene 750 105 ( 75-135 )789
4-Methyl-2-pentanone (MIBK) 2250 120 ( 45-145 )2710
Benzene 750 102 ( 75-125 )763
Bromobenzene 750 104 ( 65-120 )781
Bromochloromethane 750 106 ( 70-125 )792
Bromodichloromethane 750 110 ( 70-130 )822
Bromoform 750 109 ( 55-135 )817
Bromomethane 750 119 ( 30-160 )892
Carbon disulfide 1130 104 ( 45-160 )1180
Print Date: 06/27/2013 5:39:28PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
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C339
Blank Spike ID: LCS for HBN 1132110 [VXX24765]
Blank Spike Lab ID: 1150853
Date Analyzed: 06/03/2013 13:19
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Result
Carbon tetrachloride 750 102 ( 65-135 )768
Chlorobenzene 750 105 ( 75-125 )791
Chloroethane 750 130 ( 40-155 )979
Chloroform 750 109 ( 70-125 )816
Chloromethane 750 122 ( 50-130 )919
cis-1,2-Dichloroethene 750 108 ( 65-125 )811
cis-1,3-Dichloropropene 750 110 ( 70-125 )825
Dibromochloromethane 750 109 ( 65-130 )816
Dibromomethane 750 108 ( 75-130 )808
Dichlorodifluoromethane 750 116 ( 35-135 )868
Ethylbenzene 750 106 ( 75-125 )795
Hexachlorobutadiene 750 107 ( 55-140 )799
Isopropylbenzene (Cumene) 750 105 ( 75-130 )788
Methyl-t-butyl ether 1130 108 ( 63-149 )1220
Methylene chloride 750 101 ( 55-140 )756
n-Butylbenzene 750 105 ( 65-140 )785
n-Propylbenzene 750 106 ( 65-135 )796
Naphthalene 750 108 ( 40-125 )806
o-Xylene 750 105 ( 75-125 )786
P & M -Xylene 1500 105 ( 80-125 )1580
sec-Butylbenzene 750 105 ( 65-130 )787
Styrene 750 104 ( 75-125 )778
tert-Butylbenzene 750 104 ( 65-130 )782
Tetrachloroethene 750 108 ( 65-140 )813
Toluene 750 106 ( 70-125 )793
trans-1,2-Dichloroethene 750 108 ( 65-135 )808
trans-1,3-Dichloropropene 750 109 ( 65-125 )817
Trichloroethene 750 102 ( 75-125 )766
Trichlorofluoromethane 750 113 ( 25-185 )846
Vinyl chloride 750 125 ( 60-125 )935
Xylenes (total) 2250 105 ( 80-125 )2370
Surrogates
1,2-Dichloroethane-D4 750 109 ( 79-118 )109
Print Date: 06/27/2013 5:39:28PM
Member of SGS Group
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C340
Blank Spike ID: LCS for HBN 1132110 [VXX24765]
Blank Spike Lab ID: 1150853
Date Analyzed: 06/03/2013 13:19
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (%)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Result
4-Bromofluorobenzene 750 98 ( 67-138 )98.2
Toluene-d8 750 103 ( 85-115 )103
Batch Information
Analytical Batch: VMS13531
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Prep Batch: VXX24765
Prep Method: SW5035A
Prep Date/Time: 06/03/2013 08:00
Spike Init Wt./Vol.: 750 ug/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:28PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C341
Original Sample ID: 1132110001
MS Sample ID: 1150854 MS
MSD Sample ID: 1150855 MSD
Analysis Date: 06/03/2013 15:04
Analysis Date: 06/03/2013 13:40
Analysis Date: 06/03/2013 13:57
Matrix: Soil/Solid (dry weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Matrix Spike Summary
RPD CL
1,1,1,2-Tetrachloroethane 77127.6U 798 103 771 826 107 75-125 3.50 (< 20 )
1,1,1-Trichloroethane 77127.6U 836 108 771 862 112 70-135 3.10 (< 20 )
1,1,2,2-Tetrachloroethane 77155.3U 843 109 771 844 110 55-130 0.18 (< 20 )
1,1,2-Trichloroethane 77127.6U 819 106 771 852 110 60-125 3.80 (< 20 )
1,1-Dichloroethane 77127.6U 820 106 771 846 110 75-125 3.20 (< 20 )
1,1-Dichloroethene 77127.6U 823 107 771 838 109 65-135 1.80 (< 20 )
1,1-Dichloropropene 77127.6U 846 110 771 864 112 70-135 2.20 (< 20 )
1,2,3-Trichlorobenzene 77155.3U 870 113 771 849 110 60-135 2.40 (< 20 )
1,2,3-Trichloropropane 77127.6U 842 109 771 842 109 65-130 0.09 (< 20 )
1,2,4-Trichlorobenzene 77127.6U 836 108 771 837 109 65-130 0.06 (< 20 )
1,2,4-Trimethylbenzene 77155.3U 803 104 771 821 107 65-135 2.30 (< 20 )
1,2-Dibromo-3-chloropropane 771111U 944 122 771 910 118 40-135 3.70 (< 20 )
1,2-Dibromoethane 77127.6U 793 103 771 814 106 70-125 2.50 (< 20 )
1,2-Dichlorobenzene 77127.6U 773 100 771 802 104 75-120 3.70 (< 20 )
1,2-Dichloroethane 77127.6U 810 105 771 841 109 70-135 3.80 (< 20 )
1,2-Dichloropropane 77127.6U 818 106 771 850 110 70-120 3.90 (< 20 )
1,3,5-Trimethylbenzene 77127.6U 800 104 771 823 107 65-135 2.90 (< 20 )
1,3-Dichlorobenzene 77127.6U 790 103 771 795 103 70-125 0.62 (< 20 )
1,3-Dichloropropane 77127.6U 795 103 771 820 106 75-125 3.10 (< 20 )
1,4-Dichlorobenzene 77127.6U 786 102 771 805 104 70-125 2.40 (< 20 )
2,2-Dichloropropane 77127.6U 874 113 771 897 116 65-135 2.50 (< 20 )
2-Butanone (MEK) 2316276U 2980 129 2316 2949 128 30-160 0.98 (< 20 )
2-Chlorotoluene 77127.6U 813 105 771 817 106 70-130 0.57 (< 20 )
2-Hexanone 2316276U 2908 126 2316 2887 125 45-145 0.76 (< 20 )
4-Chlorotoluene 77127.6U 803 104 771 852 111 75-125 6.00 (< 20 )
4-Isopropyltoluene 77127.6U 821 107 771 836 108 75-135 1.80 (< 20 )
4-Methyl-2-pentanone (MIBK) 2316276U 2773 120 2316 2793 121 45-145 0.92 (< 20 )
Benzene 77113.8U 766 99 771 791 103 75-125 3.10 (< 20 )
Bromobenzene 77127.6U 784 102 771 807 105 65-120 2.80 (< 20 )
Bromochloromethane 77127.6U 791 103 771 820 106 70-125 3.60 (< 20 )
Bromodichloromethane 77127.6U 813 106 771 848 110 70-130 4.20 (< 20 )
Bromoform 77127.6U 822 107 771 846 110 55-135 2.80 (< 20 )
Bromomethane 771221U 820 106 771 819 106 30-160 0.13 (< 20 )
Carbon disulfide 1153111U 1288 111 1153 1298 112 45-160 0.66 (< 20 )
Carbon tetrachloride 77127.6U 772 100 771 787 102 65-135 2.00 (< 20 )
Chlorobenzene 77127.6U 793 103 771 814 106 75-125 2.60 (< 20 )
Chloroethane 771221U 934 121 771 865 112 40-155 7.60 (< 20 )
Print Date: 06/27/2013 5:39:29PM
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C342
Original Sample ID: 1132110001
MS Sample ID: 1150854 MS
MSD Sample ID: 1150855 MSD
Analysis Date: 06/03/2013 15:04
Analysis Date: 06/03/2013 13:40
Analysis Date: 06/03/2013 13:57
Matrix: Soil/Solid (dry weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Matrix Spike Summary
RPD CL
Chloroform 77127.6U 820 106 771 846 110 70-125 3.10 (< 20 )
Chloromethane 77127.6U 910 118 771 919 119 50-130 0.98 (< 20 )
cis-1,2-Dichloroethene 77127.6U 812 105 771 838 109 65-125 3.10 (< 20 )
cis-1,3-Dichloropropene 77127.6U 823 107 771 860 112 70-125 4.20 (< 20 )
Dibromochloromethane 77127.6U 810 105 771 833 108 65-130 2.80 (< 20 )
Dibromomethane 77127.6U 808 105 771 835 108 75-130 3.30 (< 20 )
Dichlorodifluoromethane 77155.3U 850 110 771 859 111 35-135 1.10 (< 20 )
Ethylbenzene 77127.6U 809 105 771 830 108 75-125 2.50 (< 20 )
Hexachlorobutadiene 77155.3U 936 121 771 931 121 55-140 0.44 (< 20 )
Isopropylbenzene (Cumene) 77127.6U 823 107 771 843 109 75-130 2.30 (< 20 )
Methyl-t-butyl ether 1153111U 1194 103 1153 1246 108 63-149 4.60 (< 20 )
Methylene chloride 771111U 757 98 771 790 103 55-140 4.30 (< 20 )
n-Butylbenzene 77127.6U 849 110 771 856 111 65-140 0.72 (< 20 )
n-Propylbenzene 77127.6U 819 106 771 828 107 65-135 1.10 (< 20 )
Naphthalene 77155.3U 892 116 771 856 111 40-125 4.20 (< 20 )
o-Xylene 77127.6U 794 103 771 818 106 75-125 3.00 (< 20 )
P & M -Xylene 153755.3U 1599 104 1537 1661 108 80-125 3.40 (< 20 )
sec-Butylbenzene 77127.6U 822 107 771 841 109 65-130 2.30 (< 20 )
Styrene 77127.6U 789 102 771 832 108 75-125 5.20 (< 20 )
tert-Butylbenzene 77127.6U 801 104 771 830 108 65-130 3.50 (< 20 )
Tetrachloroethene 77113.8U 842 109 771 860 112 65-140 2.10 (< 20 )
Toluene 77127.6U 810 105 771 830 108 70-125 2.40 (< 20 )
trans-1,2-Dichloroethene 77127.6U 840 109 771 856 111 65-135 1.80 (< 20 )
trans-1,3-Dichloropropene 77127.6U 826 107 771 847 110 65-125 2.60 (< 20 )
Trichloroethene 77113.8U 772 100 771 798 103 75-125 3.20 (< 20 )
Trichlorofluoromethane 77155.3U 834 108 771 839 109 25-185 0.71 (< 20 )
Vinyl chloride 77127.6U 947 123 771 961 125 60-125 1.40 (< 20 )
Xylenes (total) 2316111U 2399 104 2316 2471 107 80-125 3.30 (< 20 )
Surrogates
1,2-Dichloroethane-D4 771 832 108 771 832 108 79-118 0.09
4-Bromofluorobenzene 2056 1952 95 2056 1952 95 67-138 0.12
Toluene-d8 771 803 104 771 796 103 85-115 0.74
Print Date: 06/27/2013 5:39:29PM
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C343
Original Sample ID: 1132110001
MS Sample ID: 1150854 MS
MSD Sample ID: 1150855 MSD
Analysis Date:
Analysis Date: 06/03/2013 13:40
Analysis Date: 06/03/2013 13:57
Matrix: Soil/Solid (dry weight)
Results by SW8260B
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110023
Matrix Spike Summary
RPD CL
Batch Information
Prep Batch: VXX24765
Prep Method: Vol. Extraction SW8260 Field Extracted L
Prep Date/Time: 6/3/2013 8:00:00AM
Prep Initial Wt./Vol.: 50.51g
Prep Extract Vol: 25.00mL
Analytical Batch: VMS13531
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 6/3/2013 1:40:00PM
Print Date: 06/27/2013 5:39:29PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C344
Blank ID: MB for HBN 1453161 [VXX/24768]
Blank Lab ID: 1151052
QC for Samples:
1132110020
Matrix: Soil/Solid (dry weight)
Results by AK101
DL UnitsLOQ/CLResultsParameter
Method Blank
Gasoline Range Organics 2.50 mg/Kg0.7500.946J
Surrogates
4-Bromofluorobenzene 50-150 %82.3
Batch Information
Analytical Batch: VFC11446
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Analytical Date/Time: 6/4/2013 8:00:00PM
Prep Batch: VXX24768
Prep Method: SW5035A
Prep Date/Time: 6/4/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:30PM
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C345
Blank Spike ID: LCS for HBN 1132110 [VXX24768]
Blank Spike Lab ID: 1151062
Date Analyzed: 06/04/2013 20:56
Spike Duplicate ID: LCSD for HBN 1132110
[VXX24768]
Spike Duplicate Lab ID: 1151063
Results by AK101
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110020
Result
Gasoline Range Organics 10.0 97 10.0 8.79 88 ( 60-120 ) (< 20 ) 9.409.65
Surrogates
4-Bromofluorobenzene 1.25 82 1.25 74.4 74 ( 50-150 ) 10.2082.3
Batch Information
Analytical Batch: VFC11446
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Prep Batch: VXX24768
Prep Method: SW5035A
Prep Date/Time: 06/04/2013 08:00
Spike Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:30PM
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C346
Blank ID: MB for HBN 1453193 [VXX/24769]
Blank Lab ID: 1151212
QC for Samples:
1132110020, 1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
1,1,1,2-Tetrachloroethane 25.0 ug/Kg7.8015.6U
1,1,1-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1,2,2-Tetrachloroethane 50.0 ug/Kg15.030.0U
1,1,2-Trichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethane 25.0 ug/Kg7.8015.6U
1,1-Dichloroethene 25.0 ug/Kg7.8015.6U
1,1-Dichloropropene 25.0 ug/Kg7.8015.6U
1,2,3-Trichlorobenzene 50.0 ug/Kg15.030.0U
1,2,3-Trichloropropane 25.0 ug/Kg7.8015.6U
1,2,4-Trichlorobenzene 25.0 ug/Kg7.8015.6U
1,2,4-Trimethylbenzene 50.0 ug/Kg15.030.0U
1,2-Dibromo-3-chloropropane 100 ug/Kg31.062.0U
1,2-Dibromoethane 25.0 ug/Kg7.8015.6U
1,2-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,2-Dichloroethane 25.0 ug/Kg7.8015.6U
1,2-Dichloropropane 25.0 ug/Kg7.8015.6U
1,3,5-Trimethylbenzene 25.0 ug/Kg7.8015.6U
1,3-Dichlorobenzene 25.0 ug/Kg7.8015.6U
1,3-Dichloropropane 25.0 ug/Kg7.8015.6U
1,4-Dichlorobenzene 25.0 ug/Kg7.8015.6U
2,2-Dichloropropane 25.0 ug/Kg7.8015.6U
2-Butanone (MEK) 250 ug/Kg78.0156U
2-Chlorotoluene 25.0 ug/Kg7.8015.6U
2-Hexanone 250 ug/Kg78.0156U
4-Chlorotoluene 25.0 ug/Kg7.8015.6U
4-Isopropyltoluene 25.0 ug/Kg7.8015.6U
4-Methyl-2-pentanone (MIBK) 250 ug/Kg78.0156U
Benzene 12.5 ug/Kg3.907.80U
Bromobenzene 25.0 ug/Kg7.8015.6U
Bromochloromethane 25.0 ug/Kg7.8015.6U
Bromodichloromethane 25.0 ug/Kg7.8015.6U
Bromoform 25.0 ug/Kg7.8015.6U
Bromomethane 200 ug/Kg62.0124U
Carbon disulfide 100 ug/Kg31.062.0U
Carbon tetrachloride 25.0 ug/Kg7.8015.6U
Chlorobenzene 25.0 ug/Kg7.8015.6U
Chloroethane 200 ug/Kg62.0124U
Chloroform 25.0 ug/Kg7.8015.6U
Print Date: 06/27/2013 5:39:31PM
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C347
Blank ID: MB for HBN 1453193 [VXX/24769]
Blank Lab ID: 1151212
QC for Samples:
1132110020, 1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Chloromethane 25.0 ug/Kg7.8015.6U
cis-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
cis-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Dibromochloromethane 25.0 ug/Kg7.8015.6U
Dibromomethane 25.0 ug/Kg7.8015.6U
Dichlorodifluoromethane 50.0 ug/Kg15.030.0U
Ethylbenzene 25.0 ug/Kg7.8015.6U
Hexachlorobutadiene 50.0 ug/Kg15.030.0U
Isopropylbenzene (Cumene) 25.0 ug/Kg7.8015.6U
Methylene chloride 100 ug/Kg31.062.0U
Methyl-t-butyl ether 100 ug/Kg31.062.0U
Naphthalene 50.0 ug/Kg15.030.0U
n-Butylbenzene 25.0 ug/Kg7.8015.6U
n-Propylbenzene 25.0 ug/Kg7.8015.6U
o-Xylene 25.0 ug/Kg7.8015.6U
P & M -Xylene 50.0 ug/Kg15.030.0U
sec-Butylbenzene 25.0 ug/Kg7.8015.6U
Styrene 25.0 ug/Kg7.8015.6U
tert-Butylbenzene 25.0 ug/Kg7.8015.6U
Tetrachloroethene 12.5 ug/Kg3.907.80U
Toluene 25.0 ug/Kg7.8015.6U
trans-1,2-Dichloroethene 25.0 ug/Kg7.8015.6U
trans-1,3-Dichloropropene 25.0 ug/Kg7.8015.6U
Trichloroethene 12.5 ug/Kg3.907.80U
Trichlorofluoromethane 50.0 ug/Kg15.030.0U
Vinyl chloride 25.0 ug/Kg7.8015.6U
Xylenes (total) 100 ug/Kg31.062.0U
Surrogates
1,2-Dichloroethane-D4 79-118 %111
4-Bromofluorobenzene 67-138 %90.7
Toluene-d8 85-115 %98.5
Print Date: 06/27/2013 5:39:31PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C348
Blank ID: MB for HBN 1453193 [VXX/24769]
Blank Lab ID: 1151212
QC for Samples:
1132110020, 1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8260B
DL UnitsLOQ/CLResultsParameter
Method Blank
Batch Information
Analytical Batch: VMS13532
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 6/4/2013 11:48:01AM
Prep Batch: VXX24769
Prep Method: SW5035A
Prep Date/Time: 6/4/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:31PM
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C349
Blank Spike ID: LCS for HBN 1132110 [VXX24769]
Blank Spike Lab ID: 1151213
Date Analyzed: 06/04/2013 12:22
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132110020, 1132110021, 1132110022
Result
1,1,1,2-Tetrachloroethane 750 99 ( 75-125 )744
1,1,1-Trichloroethane 750 108 ( 70-135 )808
1,1,2,2-Tetrachloroethane 750 100 ( 55-130 )747
1,1,2-Trichloroethane 750 102 ( 60-125 )762
1,1-Dichloroethane 750 106 ( 75-125 )794
1,1-Dichloroethene 750 109 ( 65-135 )815
1,1-Dichloropropene 750 109 ( 70-135 )816
1,2,3-Trichlorobenzene 750 98 ( 60-135 )736
1,2,3-Trichloropropane 750 99 ( 65-130 )740
1,2,4-Trichlorobenzene 750 97 ( 65-130 )727
1,2,4-Trimethylbenzene 750 97 ( 65-135 )725
1,2-Dibromo-3-chloropropane 750 108 ( 40-135 )811
1,2-Dibromoethane 750 98 ( 70-125 )737
1,2-Dichlorobenzene 750 95 ( 75-120 )714
1,2-Dichloroethane 750 105 ( 70-135 )789
1,2-Dichloropropane 750 104 ( 70-120 )781
1,3,5-Trimethylbenzene 750 97 ( 65-135 )726
1,3-Dichlorobenzene 750 95 ( 70-125 )715
1,3-Dichloropropane 750 99 ( 75-125 )740
1,4-Dichlorobenzene 750 93 ( 70-125 )699
2,2-Dichloropropane 750 110 ( 65-135 )825
2-Butanone (MEK) 2250 122 ( 30-160 )2750
2-Chlorotoluene 750 98 ( 70-130 )736
2-Hexanone 2250 117 ( 45-145 )2620
4-Chlorotoluene 750 97 ( 75-125 )726
4-Isopropyltoluene 750 98 ( 75-135 )733
4-Methyl-2-pentanone (MIBK) 2250 114 ( 45-145 )2570
Benzene 750 96 ( 75-125 )718
Bromobenzene 750 95 ( 65-120 )711
Bromochloromethane 750 100 ( 70-125 )752
Bromodichloromethane 750 103 ( 70-130 )776
Bromoform 750 100 ( 55-135 )748
Bromomethane 750 110 ( 30-160 )828
Carbon disulfide 1130 105 ( 45-160 )1180
Print Date: 06/27/2013 5:39:32PM
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C350
Blank Spike ID: LCS for HBN 1132110 [VXX24769]
Blank Spike Lab ID: 1151213
Date Analyzed: 06/04/2013 12:22
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (ug/Kg)
QC for Samples: 1132110020, 1132110021, 1132110022
Result
Carbon tetrachloride 750 99 ( 65-135 )746
Chlorobenzene 750 98 ( 75-125 )736
Chloroethane 750 119 ( 40-155 )894
Chloroform 750 106 ( 70-125 )792
Chloromethane 750 107 ( 50-130 )801
cis-1,2-Dichloroethene 750 102 ( 65-125 )765
cis-1,3-Dichloropropene 750 104 ( 70-125 )777
Dibromochloromethane 750 99 ( 65-130 )743
Dibromomethane 750 103 ( 75-130 )769
Dichlorodifluoromethane 750 100 ( 35-135 )751
Ethylbenzene 750 101 ( 75-125 )759
Hexachlorobutadiene 750 105 ( 55-140 )786
Isopropylbenzene (Cumene) 750 102 ( 75-130 )767
Methyl-t-butyl ether 1130 102 ( 63-149 )1150
Methylene chloride 750 98 ( 55-140 )732
n-Butylbenzene 750 101 ( 65-140 )756
n-Propylbenzene 750 100 ( 65-135 )748
Naphthalene 750 98 ( 40-125 )735
o-Xylene 750 99 ( 75-125 )745
P & M -Xylene 1500 100 ( 80-125 )1500
sec-Butylbenzene 750 99 ( 65-130 )744
Styrene 750 99 ( 75-125 )740
tert-Butylbenzene 750 97 ( 65-130 )729
Tetrachloroethene 750 104 ( 65-140 )783
Toluene 750 99 ( 70-125 )742
trans-1,2-Dichloroethene 750 104 ( 65-135 )779
trans-1,3-Dichloropropene 750 100 ( 65-125 )750
Trichloroethene 750 97 ( 75-125 )731
Trichlorofluoromethane 750 105 ( 25-185 )791
Vinyl chloride 750 111 ( 60-125 )835
Xylenes (total) 2250 100 ( 80-125 )2250
Surrogates
1,2-Dichloroethane-D4 750 106 ( 79-118 )106
Print Date: 06/27/2013 5:39:32PM
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C351
Blank Spike ID: LCS for HBN 1132110 [VXX24769]
Blank Spike Lab ID: 1151213
Date Analyzed: 06/04/2013 12:22
Results by SW8260B
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (%)
QC for Samples: 1132110020, 1132110021, 1132110022
Result
4-Bromofluorobenzene 750 91 ( 67-138 )90.7
Toluene-d8 750 97 ( 85-115 )97.2
Batch Information
Analytical Batch: VMS13532
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Prep Batch: VXX24769
Prep Method: SW5035A
Prep Date/Time: 06/04/2013 08:00
Spike Init Wt./Vol.: 750 ug/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:32PM
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C352
Original Sample ID: 1151214
MS Sample ID: 1151215 MS
MSD Sample ID: 1151216 MSD
Analysis Date: 06/04/2013 14:10
Analysis Date: 06/04/2013 12:46
Analysis Date: 06/04/2013 13:03
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110021, 1132110022
Matrix Spike Summary
RPD CL
1,1,1,2-Tetrachloroethane 73515.3U 678 92 735 824 112 75-125 19.40 (< 20 )
1,1,1-Trichloroethane 73515.3U 699 95 735 856 116 70-135 20.20 (< 20 )*
1,1,2,2-Tetrachloroethane 73529.4U 683 93 735 840 114 55-130 20.60 (< 20 )*
1,1,2-Trichloroethane 73515.3U 708 96 735 861 117 60-125 19.60 (< 20 )
1,1-Dichloroethane 73515.3U 714 97 735 864 117 75-125 19.00 (< 20 )
1,1-Dichloroethene 73515.3U 692 94 735 837 114 65-135 19.00 (< 20 )
1,1-Dichloropropene 73515.3U 699 95 735 858 117 70-135 20.40 (< 20 )*
1,2,3-Trichlorobenzene 73529.4U 660 90 735 848 115 60-135 24.80 (< 20 )*
1,2,3-Trichloropropane 73515.3U 682 93 735 823 112 65-130 18.80 (< 20 )
1,2,4-Trichlorobenzene 73515.3U 654 89 735 828 113 65-130 23.50 (< 20 )*
1,2,4-Trimethylbenzene 73529.4U 642 87 735 792 108 65-135 20.90 (< 20 )*
1,2-Dibromo-3-chloropropane 73560.8U 726 99 735 906 123 40-135 22.00 (< 20 )*
1,2-Dibromoethane 73515.3U 686 93 735 834 113 70-125 19.60 (< 20 )
1,2-Dichlorobenzene 73515.3U 642 87 735 792 108 75-120 20.80 (< 20 )*
1,2-Dichloroethane 73515.3U 740 101 735 895 122 70-135 18.90 (< 20 )
1,2-Dichloropropane 73515.3U 726 99 735 879 120 70-120 19.00 (< 20 )
1,3,5-Trimethylbenzene 73515.3U 633 86 735 786 107 65-135 21.60 (< 20 )*
1,3-Dichlorobenzene 73515.3U 639 87 735 785 107 70-125 20.50 (< 20 )*
1,3-Dichloropropane 73515.3U 690 94 735 833 113 75-125 18.70 (< 20 )
1,4-Dichlorobenzene 73515.3U 636 87 735 792 108 70-125 21.70 (< 20 )*
2,2-Dichloropropane 73515.3U 715 97 735 872 119 65-135 19.70 (< 20 )
2-Butanone (MEK) 2210153U 2480 112 2210 3090 140 30-160 22.10 (< 20 )*
2-Chlorotoluene 73515.3U 575 78 735 713 97 70-130 21.40 (< 20 )*
2-Hexanone 2210153U 2390 109 2210 2930 133 45-145 20.10 (< 20 )*
4-Chlorotoluene 73515.3U 666 91 735 790 107 75-125 17.00 (< 20 )
4-Isopropyltoluene 73515.3U 635 86 735 795 108 75-135 22.50 (< 20 )*
4-Methyl-2-pentanone (MIBK) 2210153U 2420 110 2210 2930 133 45-145 19.20 (< 20 )
Benzene 7357.64U 664 90 735 814 111 75-125 20.30 (< 20 )*
Bromobenzene 73515.3U 640 87 735 787 107 65-120 20.60 (< 20 )*
Bromochloromethane 73515.3U 713 97 735 861 117 70-125 18.70 (< 20 )
Bromodichloromethane 73515.3U 728 99 735 877 119 70-130 18.50 (< 20 )
Bromoform 73515.3U 698 95 735 832 113 55-135 17.60 (< 20 )
Bromomethane 735122U 758 103 735 894 122 30-160 16.40 (< 20 )
Carbon disulfide 110060.8U 1090 99 1100 1280 116 45-160 15.70 (< 20 )
Carbon tetrachloride 73515.3U 637 87 735 770 105 65-135 18.90 (< 20 )
Chlorobenzene 73515.3U 663 90 735 829 113 75-125 22.30 (< 20 )*
Chloroethane 735122U 828 113 735 935 127 40-155 12.20 (< 20 )
Print Date: 06/27/2013 5:39:33PM
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C353
Original Sample ID: 1151214
MS Sample ID: 1151215 MS
MSD Sample ID: 1151216 MSD
Analysis Date: 06/04/2013 14:10
Analysis Date: 06/04/2013 12:46
Analysis Date: 06/04/2013 13:03
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (ug/Kg) Spike Duplicate (ug/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110021, 1132110022
Matrix Spike Summary
RPD CL
Chloroform 73515.3U 721 98 735 876 119 70-125 19.40 (< 20 )
Chloromethane 73515.3U 785 107 735 951 129 50-130 19.10 (< 20 )
cis-1,2-Dichloroethene 73515.3U 715 97 735 869 118 65-125 19.40 (< 20 )
cis-1,3-Dichloropropene 73515.3U 722 98 735 880 120 70-125 19.70 (< 20 )
Dibromochloromethane 73515.3U 685 93 735 838 114 65-130 20.20 (< 20 )*
Dibromomethane 73515.3U 732 100 735 875 119 75-130 17.90 (< 20 )
Dichlorodifluoromethane 73529.4U 687 93 735 834 113 35-135 19.30 (< 20 )
Ethylbenzene 73515.3U 668 91 735 826 112 75-125 21.20 (< 20 )*
Hexachlorobutadiene 73529.4U 667 91 735 822 112 55-140 20.80 (< 20 )*
Isopropylbenzene (Cumene) 73515.3U 667 91 735 810 110 75-130 19.50 (< 20 )
Methyl-t-butyl ether 110060.8U 1080 98 1100 1300 118 63-149 18.70 (< 20 )
Methylene chloride 73560.8U 694 94 735 831 113 55-140 18.00 (< 20 )
n-Butylbenzene 73515.3U 647 88 735 783 107 65-140 19.10 (< 20 )
n-Propylbenzene 73515.3U 626 85 735 790 107 65-135 23.20 (< 20 )*
Naphthalene 73529.4U 678 92 735 869 118 40-125 24.70 (< 20 )*
o-Xylene 73515.3U 672 91 735 824 112 75-125 20.30 (< 20 )*
P & M -Xylene 147029.4U 1320 90 1470 1620 110 80-125 20.50 (< 20 )*
sec-Butylbenzene 73515.3U 636 87 735 793 108 65-130 22.00 (< 20 )*
Styrene 73515.3U 673 92 735 831 113 75-125 20.90 (< 20 )*
tert-Butylbenzene 73515.3U 628 85 735 776 106 65-130 21.00 (< 20 )*
Tetrachloroethene 7357.64U 658 89 735 815 111 65-140 21.40 (< 20 )*
Toluene 73515.3U 666 91 735 818 111 70-125 20.40 (< 20 )*
trans-1,2-Dichloroethene 73515.3U 711 97 735 865 118 65-135 19.50 (< 20 )
trans-1,3-Dichloropropene 73515.3U 699 95 735 843 115 65-125 18.70 (< 20 )
Trichloroethene 7357.64U 659 90 735 805 109 75-125 19.90 (< 20 )
Trichlorofluoromethane 73529.4U 695 95 735 841 114 25-185 19.00 (< 20 )
Vinyl chloride 73515.3U 789 107 735 953 130 60-125 18.80 (< 20 )*
Xylenes (total) 221060.8U 1990 90 2210 2450 111 80-125 20.40 (< 20 )*
Surrogates
1,2-Dichloroethane-D4 735 752 102 735 911 124 79-118 19.10*
4-Bromofluorobenzene 1960 1540 79 1960 1930 98 67-138 22.00
Toluene-d8 735 663 90 735 812 110 85-115 20.20
Print Date: 06/27/2013 5:39:33PM
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C354
Original Sample ID: 1151214
MS Sample ID: 1151215 MS
MSD Sample ID: 1151216 MSD
Analysis Date:
Analysis Date: 06/04/2013 12:46
Analysis Date: 06/04/2013 13:03
Matrix: Solid/Soil (Wet Weight)
Results by SW8260B
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110021, 1132110022
Matrix Spike Summary
RPD CL
Batch Information
Prep Batch: VXX24769
Prep Method: Vol. Extraction SW8260 Field Extracted L
Prep Date/Time: 6/4/2013 8:00:00AM
Prep Initial Wt./Vol.: 50.99g
Prep Extract Vol: 25.00mL
Analytical Batch: VMS13532
Analytical Method: SW8260B
Instrument: Agilent 7890-75MS
Analyst: HM
Analytical Date/Time: 6/4/2013 12:46:00PM
Print Date: 06/27/2013 5:39:33PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C355
Blank ID: MB for HBN 1453288 [VXX/24775]
Blank Lab ID: 1151394
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007
Matrix: Soil/Solid (dry weight)
Results by AK101
DL UnitsLOQ/CLResultsParameter
Method Blank
Gasoline Range Organics 2.50 mg/Kg0.7500.936J
Surrogates
4-Bromofluorobenzene 50-150 %82.3
Batch Information
Analytical Batch: VFC11449
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Analytical Date/Time: 6/5/2013 10:40:00AM
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 6/5/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:33PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
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C356
Blank Spike ID: LCS for HBN 1132110 [VXX24775]
Blank Spike Lab ID: 1151395
Date Analyzed: 06/05/2013 11:36
Spike Duplicate ID: LCSD for HBN 1132110
[VXX24775]
Spike Duplicate Lab ID: 1151396
Results by AK101
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007
Result
Gasoline Range Organics 10.0 98 10.0 9.50 95 ( 60-120 ) (< 20 ) 3.009.80
Surrogates
4-Bromofluorobenzene 1.25 83 1.25 82.9 83 ( 50-150 ) 0.4683.3
Batch Information
Analytical Batch: VFC11449
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Prep Batch: VXX24775
Prep Method: SW5035A
Prep Date/Time: 06/05/2013 08:00
Spike Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:34PM
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C357
Blank ID: MB for HBN 1453364 [VXX/24779]
Blank Lab ID: 1151507
QC for Samples:
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016,
1132110017, 1132110018, 1132110023
Matrix: Soil/Solid (dry weight)
Results by AK101
DL UnitsLOQ/CLResultsParameter
Method Blank
Gasoline Range Organics 2.50 mg/Kg0.7501.30J
Surrogates
4-Bromofluorobenzene 50-150 %97.7
Batch Information
Analytical Batch: VFC11451
Analytical Method: AK101
Instrument: Agilent 7890A PID/FID
Analyst: ST
Analytical Date/Time: 6/6/2013 7:33:00PM
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 6/6/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:35PM
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C358
Blank Spike ID: LCS for HBN 1132110 [VXX24779]
Blank Spike Lab ID: 1151508
Date Analyzed: 06/06/2013 19:52
Spike Duplicate ID: LCSD for HBN 1132110
[VXX24779]
Spike Duplicate Lab ID: 1151509
Results by AK101
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110023
Result
Gasoline Range Organics 10.0 102 10.0 9.96 100 ( 60-120 ) (< 20 ) 2.5010.2
Surrogates
4-Bromofluorobenzene 1.25 100 1.25 98.6 99 ( 50-150 ) 1.40100
Batch Information
Analytical Batch: VFC11451
Analytical Method: AK101
Instrument: Agilent 7890A PID/FID
Analyst: ST
Prep Batch: VXX24779
Prep Method: SW5035A
Prep Date/Time: 06/06/2013 08:00
Spike Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:36PM
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SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C359
Blank ID: MB for HBN 1453763 [VXX/24787]
Blank Lab ID: 1151734
QC for Samples:
1132110019, 1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by AK101
DL UnitsLOQ/CLResultsParameter
Method Blank
Gasoline Range Organics 2.50 mg/Kg0.7500.906J
Surrogates
4-Bromofluorobenzene 50-150 %83.7
Batch Information
Analytical Batch: VFC11454
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Analytical Date/Time: 6/7/2013 10:09:00AM
Prep Batch: VXX24787
Prep Method: SW5035A
Prep Date/Time: 6/7/2013 8:00:00AM
Prep Initial Wt./Vol.: 50 g
Prep Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:37PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C360
Blank Spike ID: LCS for HBN 1132110 [VXX24787]
Blank Spike Lab ID: 1151737
Date Analyzed: 06/07/2013 11:05
Spike Duplicate ID: LCSD for HBN 1132110
[VXX24787]
Spike Duplicate Lab ID: 1151738
Results by AK101
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110019, 1132110021, 1132110022
Result
Gasoline Range Organics 10.0 94 10.0 9.14 91 ( 60-120 ) (< 20 ) 3.109.43
Surrogates
4-Bromofluorobenzene 1.25 83 1.25 79.6 80 ( 50-150 ) 3.8082.6
Batch Information
Analytical Batch: VFC11454
Analytical Method: AK101
Instrument: Agilent 7890 PID/FID
Analyst: ST
Prep Batch: VXX24787
Prep Method: SW5035A
Prep Date/Time: 06/07/2013 08:00
Spike Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Dupe Init Wt./Vol.: 10.0 mg/Kg Extract Vol: 25 mL
Print Date: 06/27/2013 5:39:37PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C361
Blank ID: MB for HBN 1453077 [XXX/29091]
Blank Lab ID: 1150863
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110020
Matrix: Soil/Solid (dry weight)
Results by AK102
DL UnitsLOQ/CLResultsParameter
Method Blank
Diesel Range Organics 20.0 mg/Kg6.2012.4U
Surrogates
5a Androstane 60-120 %97.3
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/8/2013 7:23:00PM
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 6/4/2013 9:10:00AM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:38PM
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C362
Blank Spike ID: LCS for HBN 1132110 [XXX29091]
Blank Spike Lab ID: 1150864
Date Analyzed: 06/08/2013 19:32
Spike Duplicate ID: LCSD for HBN 1132110
[XXX29091]
Spike Duplicate Lab ID: 1150865
Results by AK102
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110020
Result
Diesel Range Organics 167 106 167 159 95 ( 75-125 ) (< 20 ) 10.40177
Surrogates
5a Androstane 3.33 116 3.33 119 119 ( 60-120 ) 2.70116
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/2013 09:10
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:39PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C363
Blank ID: MB for HBN 1453077 [XXX/29091]
Blank Lab ID: 1150863
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110020
Matrix: Soil/Solid (dry weight)
Results by AK103
DL UnitsLOQ/CLResultsParameter
Method Blank
Residual Range Organics 20.0 mg/Kg6.207.22J
Surrogates
n-Triacontane-d62 60-120 %129*
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/8/2013 7:23:00PM
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 6/4/2013 9:10:00AM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:40PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C364
Blank Spike ID: LCS for HBN 1132110 [XXX29091]
Blank Spike Lab ID: 1150864
Date Analyzed: 06/08/2013 19:32
Spike Duplicate ID: LCSD for HBN 1132110
[XXX29091]
Spike Duplicate Lab ID: 1150865
Results by AK103
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110020
Result
Residual Range Organics 167 110 167 164 98 ( 60-120 ) (< 20 ) 11.40184
Surrogates
n-Triacontane-d62 3.33 123 3.33 114 114 ( 60-120 ) 7.60123 *
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29091
Prep Method: SW3550C
Prep Date/Time: 06/04/2013 09:10
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:41PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C365
Blank ID: MB for HBN 1453090 [XXX/29093]
Blank Lab ID: 1150899
QC for Samples:
1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by AK102
DL UnitsLOQ/CLResultsParameter
Method Blank
Diesel Range Organics 20.0 mg/Kg6.2012.4U
Surrogates
5a Androstane 60-120 %99.8
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/8/2013 11:19:00PM
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 6/4/2013 11:15:00AM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:41PM
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t 907.562.2343 f 907.561.5301 www.us.sgs.com
C366
Blank Spike ID: LCS for HBN 1132110 [XXX29093]
Blank Spike Lab ID: 1150900
Date Analyzed: 06/08/2013 23:29
Spike Duplicate ID: LCSD for HBN 1132110
[XXX29093]
Spike Duplicate Lab ID: 1150901
Results by AK102
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110021, 1132110022
Result
Diesel Range Organics 167 101 167 156 94 ( 75-125 ) (< 20 ) 7.20168
Surrogates
5a Androstane 3.33 110 3.33 109 109 ( 60-120 ) 1.30110
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK102
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/2013 11:15
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:42PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C367
Blank ID: MB for HBN 1453090 [XXX/29093]
Blank Lab ID: 1150899
QC for Samples:
1132110021, 1132110022
Matrix: Soil/Solid (dry weight)
Results by AK103
DL UnitsLOQ/CLResultsParameter
Method Blank
Residual Range Organics 20.0 mg/Kg6.2012.4U
Surrogates
n-Triacontane-d62 60-120 %114
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Analytical Date/Time: 6/8/2013 11:19:00PM
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 6/4/2013 11:15:00AM
Prep Initial Wt./Vol.: 30 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:43PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C368
Blank Spike ID: LCS for HBN 1132110 [XXX29093]
Blank Spike Lab ID: 1150900
Date Analyzed: 06/08/2013 23:29
Spike Duplicate ID: LCSD for HBN 1132110
[XXX29093]
Spike Duplicate Lab ID: 1150901
Results by AK103
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) Spike Result Rec (%) RPD (%)CL
Blank Spike (mg/Kg)
RPD CL
Spike Duplicate (mg/Kg)
QC for Samples: 1132110021, 1132110022
Result
Residual Range Organics 167 103 167 164 98 ( 60-120 ) (< 20 ) 4.40171
Surrogates
n-Triacontane-d62 3.33 119 3.33 110 110 ( 60-120 ) 7.50119
Batch Information
Analytical Batch: XFC10918
Analytical Method: AK103
Instrument: HP 6890 Series II FID SV D R
Analyst: MCM
Prep Batch: XXX29093
Prep Method: SW3550C
Prep Date/Time: 06/04/2013 11:15
Spike Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: 167 mg/Kg Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:44PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C369
Blank ID: MB for HBN 1453106 [XXX/29094]
Blank Lab ID: 1150980
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110021
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
1,2,4-Trichlorobenzene 0.250 mg/Kg0.07800.156U
1,2-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,3-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,4-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2,4,5-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4,6-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dimethylphenol 0.250 mg/Kg0.07800.156U
2,4-Dinitrophenol 3.00 mg/Kg0.9401.88U
2,4-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2,6-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,6-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2-Chlorophenol 0.250 mg/Kg0.07800.156U
2-Methyl-4,6-dinitrophenol 2.00 mg/Kg0.6201.24U
2-Methylnaphthalene 0.250 mg/Kg0.07800.156U
2-Methylphenol (o-Cresol) 0.250 mg/Kg0.07800.156U
2-Nitroaniline 0.250 mg/Kg0.07800.156U
2-Nitrophenol 0.250 mg/Kg0.07800.156U
3&4-Methylphenol (p&m-Cresol) 1.00 mg/Kg0.3100.620U
3,3-Dichlorobenzidine 0.250 mg/Kg0.07800.156U
3-Nitroaniline 0.500 mg/Kg0.1500.300U
4-Bromophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Chloro-3-methylphenol 0.250 mg/Kg0.07800.156U
4-Chloroaniline 0.500 mg/Kg0.1500.300U
4-Chlorophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Nitroaniline 3.00 mg/Kg0.9401.88U
4-Nitrophenol 1.00 mg/Kg0.3100.620U
Acenaphthene 0.250 mg/Kg0.07800.156U
Acenaphthylene 0.250 mg/Kg0.07800.156U
Aniline 2.00 mg/Kg0.6201.24U
Anthracene 0.250 mg/Kg0.07800.156U
Azobenzene 0.250 mg/Kg0.07800.156U
Benzo(a)Anthracene 0.250 mg/Kg0.07800.156U
Benzo[a]pyrene 0.250 mg/Kg0.07800.156U
Benzo[b]Fluoranthene 0.250 mg/Kg0.07800.156U
Benzo[g,h,i]perylene 0.250 mg/Kg0.07800.156U
Print Date: 06/27/2013 5:39:45PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C370
Blank ID: MB for HBN 1453106 [XXX/29094]
Blank Lab ID: 1150980
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110021
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Benzo[k]fluoranthene 0.250 mg/Kg0.07800.156U
Benzoic acid 1.50 mg/Kg0.7501.50U
Benzyl alcohol 0.250 mg/Kg0.07800.156U
Bis(2chloro1methylethyl)Ether 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethoxy)methane 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethyl)ether 0.250 mg/Kg0.07800.156U
bis(2-Ethylhexyl)phthalate 0.250 mg/Kg0.07800.156U
Butylbenzylphthalate 0.250 mg/Kg0.07800.156U
Carbazole 0.250 mg/Kg0.07800.156U
Chrysene 0.250 mg/Kg0.07800.156U
Dibenzo[a,h]anthracene 0.250 mg/Kg0.07800.156U
Dibenzofuran 0.250 mg/Kg0.07800.156U
Diethylphthalate 0.250 mg/Kg0.07800.156U
Dimethylphthalate 0.250 mg/Kg0.07800.156U
Di-n-butylphthalate 0.250 mg/Kg0.07800.156U
di-n-Octylphthalate 0.500 mg/Kg0.1500.300U
Fluoranthene 0.250 mg/Kg0.07800.156U
Fluorene 0.250 mg/Kg0.07800.156U
Hexachlorobenzene 0.250 mg/Kg0.07800.156U
Hexachlorobutadiene 0.250 mg/Kg0.07800.156U
Hexachlorocyclopentadiene 0.700 mg/Kg0.2000.400U
Hexachloroethane 0.250 mg/Kg0.07800.156U
Indeno[1,2,3-c,d] pyrene 0.250 mg/Kg0.07800.156U
Isophorone 0.250 mg/Kg0.07800.156U
Naphthalene 0.250 mg/Kg0.07800.156U
Nitrobenzene 0.250 mg/Kg0.07800.156U
N-Nitrosodimethylamine 0.250 mg/Kg0.07800.156U
N-Nitroso-di-n-propylamine 0.250 mg/Kg0.07800.156U
N-Nitrosodiphenylamine 0.250 mg/Kg0.07800.156U
Pentachlorophenol 2.00 mg/Kg0.6201.24U
Phenanthrene 0.250 mg/Kg0.07800.156U
Phenol 0.250 mg/Kg0.07800.156U
Pyrene 0.250 mg/Kg0.07800.156U
Surrogates
2,4,6-Tribromophenol 35-125 %71.9
2-Fluorobiphenyl 45-105 %86.6
2-Fluorophenol 35-105 %69.5
Nitrobenzene-d5 35-100 %77.3
Print Date: 06/27/2013 5:39:45PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C371
Blank ID: MB for HBN 1453106 [XXX/29094]
Blank Lab ID: 1150980
QC for Samples:
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007, 1132110008, 1132110009,
1132110010, 1132110011, 1132110012, 1132110013, 1132110014, 1132110015, 1132110016, 1132110017, 1132110018,
1132110019, 1132110021
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Phenol-d6 40-100 %77.7
Terphenyl-d14 30-125 %103
Batch Information
Analytical Batch: XMS7354
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: RTS
Analytical Date/Time: 6/5/2013 7:43:00PM
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 6/4/2013 2:00:00PM
Prep Initial Wt./Vol.: 22.5 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:45PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C372
Blank Spike ID: LCS for HBN 1132110 [XXX29094]
Blank Spike Lab ID: 1150982
Date Analyzed: 06/05/2013 20:17
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Result
1,2,4-Trichlorobenzene 4.44 76 ( 45-110 )3.37
1,2-Dichlorobenzene 4.44 70 ( 45-100 )3.11
1,3-Dichlorobenzene 4.44 68 ( 40-100 )3.03
1,4-Dichlorobenzene 4.44 70 ( 35-105 )3.10
1-Chloronaphthalene 1.78 94 ( 44-105 )1.67
2,4,5-Trichlorophenol 4.44 93 ( 50-110 )4.12
2,4,6-Trichlorophenol 4.44 88 ( 45-110 )3.89
2,4-Dichlorophenol 4.44 86 ( 45-110 )3.82
2,4-Dimethylphenol 4.44 82 ( 30-105 )3.66
2,4-Dinitrophenol 8 76 ( 15-130 )6.05
2,4-Dinitrotoluene 4.44 100 ( 50-115 )4.45
2,6-Dichlorophenol 1.78 85 ( 52-102 )1.51
2,6-Dinitrotoluene 4.44 91 ( 50-110 )4.03
2-Chloronaphthalene 4.44 85 ( 45-105 )3.79
2-Chlorophenol 4.44 75 ( 45-105 )3.31
2-Methyl-4,6-dinitrophenol 8 99 ( 30-135 )7.91
2-Methylnaphthalene 4.44 84 ( 45-105 )3.74
2-Methylphenol (o-Cresol) 4.44 79 ( 40-105 )3.51
2-Nitroaniline 4.44 100 ( 45-120 )4.44
2-Nitrophenol 4.44 84 ( 40-110 )3.71
3&4-Methylphenol (p&m-Cresol) 6.22 94 ( 40-105 )5.87
3,3-Dichlorobenzidine 4.44 87 ( 10-130 )3.87
3-Nitroaniline 4.44 96 ( 25-110 )4.26
4-Bromophenyl-phenylether 4.44 99 ( 45-115 )4.41
4-Chloro-3-methylphenol 4.44 96 ( 45-115 )4.25
4-Chloroaniline 4.44 86 ( 10-100 )3.82
4-Chlorophenyl-phenylether 4.44 98 ( 45-110 )4.37
4-Nitroaniline 4.44 104 ( 35-115 )4.62
4-Nitrophenol 6.22 92 ( 15-140 )5.72
Acenaphthene 4.44 88 ( 45-110 )3.91
Acenaphthylene 4.44 93 ( 45-105 )4.11
Aniline 4.44 73 ( 20-84 )3.24
Anthracene 4.44 94 ( 55-105 )4.15
Azobenzene 4.44 95 ( 63-117 )4.23
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C373
Blank Spike ID: LCS for HBN 1132110 [XXX29094]
Blank Spike Lab ID: 1150982
Date Analyzed: 06/05/2013 20:17
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Result
Benzo(a)Anthracene 4.44 95 ( 50-110 )4.21
Benzo[a]pyrene 4.44 97 ( 50-110 )4.30
Benzo[b]Fluoranthene 4.44 105 ( 45-115 )4.65
Benzo[g,h,i]perylene 4.44 95 ( 40-125 )4.21
Benzo[k]fluoranthene 4.44 103 ( 45-125 )4.58
Benzoic acid 6.22 76 ( 10-110 )4.75
Benzyl alcohol 4.44 83 ( 20-125 )3.70
Bis(2-Chloroethoxy)methane 4.44 92 ( 45-110 )4.07
Bis(2-Chloroethyl)ether 4.44 92 ( 40-105 )4.09
bis(2-Ethylhexyl)phthalate 4.44 107 ( 45-125 )4.78
Bis(2chloro1methylethyl)Ether 4.44 79 ( 20-115 )3.50
Butylbenzylphthalate 4.44 111 ( 50-125 )4.94
Carbazole 4.44 102 ( 45-115 )4.55
Chrysene 4.44 98 ( 55-110 )4.35
Di-n-butylphthalate 4.44 102 ( 55-110 )4.52
di-n-Octylphthalate 4.44 100 ( 40-130 )4.45
Dibenzo[a,h]anthracene 4.44 94 ( 40-125 )4.18
Dibenzofuran 4.44 94 ( 50-105 )4.17
Diethylphthalate 4.44 104 ( 50-115 )4.62
Dimethylphthalate 4.44 102 ( 50-110 )4.53
Fluoranthene 4.44 98 ( 55-115 )4.33
Fluorene 4.44 95 ( 50-110 )4.22
Hexachlorobenzene 4.44 98 ( 45-120 )4.35
Hexachlorobutadiene 4.44 82 ( 40-115 )3.65
Hexachlorocyclopentadiene 4.44 87 ( 48-108 )3.87
Hexachloroethane 4.44 69 ( 35-110 )3.09
Indeno[1,2,3-c,d] pyrene 4.44 91 ( 40-120 )4.06
Isophorone 4.44 93 ( 45-110 )4.11
N-Nitroso-di-n-propylamine 4.44 90 ( 40-115 )3.99
N-Nitrosodimethylamine 4.44 75 ( 20-115 )3.31
N-Nitrosodiphenylamine 4.44 82 ( 50-115 )3.63
Naphthalene 4.44 78 ( 40-105 )3.47
Nitrobenzene 4.44 83 ( 40-115 )3.67
Pentachlorophenol 6.22 91 ( 25-120 )5.67
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C374
Blank Spike ID: LCS for HBN 1132110 [XXX29094]
Blank Spike Lab ID: 1150982
Date Analyzed: 06/05/2013 20:17
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Result
Phenanthrene 4.44 95 ( 50-110 )4.24
Phenol 4.44 78 ( 40-100 )3.45
Pyrene 4.44 109 ( 45-125 )4.84
Surrogates
2,4,6-Tribromophenol 8.89 93 ( 35-125 )93
2-Fluorobiphenyl 4.44 85 ( 45-105 )84.9
2-Fluorophenol 8.89 70 ( 35-105 )69.5
Nitrobenzene-d5 4.44 78 ( 35-100 )78.2
Phenol-d6 8.89 78 ( 40-100 )78.2
Terphenyl-d14 4.44 113 ( 30-125 )113
Batch Information
Analytical Batch: XMS7354
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: RTS
Prep Batch: XXX29094
Prep Method: SW3550C
Prep Date/Time: 06/04/2013 14:00
Spike Init Wt./Vol.: 4.44 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C375
Original Sample ID: 1132110021
MS Sample ID: 1150984 MS
MSD Sample ID: 1150985 MSD
Analysis Date: 06/06/2013 2:29
Analysis Date: 06/06/2013 2:46
Analysis Date: 06/06/2013 3:03
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Matrix Spike Summary
RPD CL
1,2,4-Trichlorobenzene 4.850.271U 3.47 72 4.97 3.69 74 45-110 6.40 (< 30 )
1,2-Dichlorobenzene 4.850.271U 3.18 66 4.97 3.48 70 45-100 9.00 (< 30 )
1,3-Dichlorobenzene 4.850.271U 3.14 65 4.97 3.37 68 40-100 7.00 (< 30 )
1,4-Dichlorobenzene 4.850.271U 3.15 65 4.97 3.33 67 35-105 5.50 (< 30 )
1-Chloronaphthalene 1.940.271U 1.65 85 1.99 1.88 95 44-105 13.30 (< 30 )
2,4,5-Trichlorophenol 4.850.271U 4.24 88 4.97 4.42 89 50-110 3.90 (< 30 )
2,4,6-Trichlorophenol 4.850.271U 4.07 84 4.97 4.43 89 45-110 8.40 (< 30 )
2,4-Dichlorophenol 4.850.271U 4.04 83 4.97 4.12 83 45-110 2.00 (< 30 )
2,4-Dimethylphenol 4.850.271U 3.85 80 4.97 3.95 80 30-105 2.70 (< 30 )
2,4-Dinitrophenol 8.713.26U 5.97 69 8.95 6.09 68 15-130 2.00 (< 30 )
2,4-Dinitrotoluene 4.850.271U 4.66 96 4.97 4.65 94 50-115 0.26 (< 30 )
2,6-Dichlorophenol 1.940.271U 1.63 84 1.99 1.66 84 52-102 1.90 (< 30 )
2,6-Dinitrotoluene 4.850.271U 4.33 90 4.97 4.67 94 50-110 7.50 (< 30 )
2-Chloronaphthalene 4.850.271U 4.02 83 4.97 4.25 86 45-105 5.60 (< 30 )
2-Chlorophenol 4.850.271U 3.38 70 4.97 3.63 73 45-105 7.30 (< 30 )
2-Methyl-4,6-dinitrophenol 8.712.17U 8.40 96 8.95 9.02 101 30-135 7.10 (< 30 )
2-Methylnaphthalene 4.850.271U 4.02 83 4.97 4.15 84 45-105 3.40 (< 30 )
2-Methylphenol (o-Cresol) 4.850.271U 3.66 76 4.97 3.83 77 40-105 4.80 (< 30 )
2-Nitroaniline 4.850.271U 4.59 95 4.97 4.74 95 45-120 2.90 (< 30 )
2-Nitrophenol 4.850.271U 4.10 85 4.97 4.36 88 40-110 6.10 (< 30 )
3&4-Methylphenol (p&m-Cresol) 6.771.09U 6.28 93 6.96 6.55 94 40-105 4.30 (< 30 )
3,3-Dichlorobenzidine 4.850.271U 3.85 80 4.97 4.35 88 10-130 12.20 (< 30 )
3-Nitroaniline 4.850.543U 4.25 88 4.97 4.24 85 25-110 0.42 (< 30 )
4-Bromophenyl-phenylether 4.850.271U 4.77 99 4.97 5.45 110 45-115 13.20 (< 30 )
4-Chloro-3-methylphenol 4.850.271U 4.44 92 4.97 4.36 88 45-115 1.90 (< 30 )
4-Chloroaniline 4.850.543U 3.98 82 4.97 4.03 81 10-100 1.40 (< 30 )
4-Chlorophenyl-phenylether 4.850.271U 4.49 93 4.97 4.77 96 45-110 6.00 (< 30 )
4-Nitroaniline 4.853.26U 4.02 83 4.97 3.99 80 35-115 0.91 (< 30 )
4-Nitrophenol 6.771.09U 4.78 71 6.96 4.80 69 15-140 0.28 (< 30 )
Acenaphthene 4.850.271U 4.03 83 4.97 4.31 87 45-110 6.70 (< 30 )
Acenaphthylene 4.850.271U 4.20 87 4.97 4.53 91 45-105 7.70 (< 30 )
Aniline 4.852.17U 3.41 71 4.97 3.68 74 20-84 7.40 (< 30 )
Anthracene 4.850.271U 4.26 88 4.97 4.61 93 55-105 8.00 (< 30 )
Azobenzene 4.850.271U 4.61 95 4.97 5.26 106 63-117 13.20 (< 30 )
Benzo(a)Anthracene 4.850.271U 4.24 88 4.97 4.83 97 50-110 13.20 (< 30 )
Benzo[a]pyrene 4.850.271U 4.26 88 4.97 4.74 95 50-110 10.50 (< 30 )
Benzo[b]Fluoranthene 4.850.271U 4.37 90 4.97 4.65 93 45-115 6.00 (< 30 )
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C376
Original Sample ID: 1132110021
MS Sample ID: 1150984 MS
MSD Sample ID: 1150985 MSD
Analysis Date: 06/06/2013 2:29
Analysis Date: 06/06/2013 2:46
Analysis Date: 06/06/2013 3:03
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Matrix Spike Summary
RPD CL
Benzo[g,h,i]perylene 4.850.271U 4.61 95 4.97 5.25 106 40-125 13.00 (< 30 )
Benzo[k]fluoranthene 4.850.271U 4.42 91 4.97 4.68 94 45-125 5.90 (< 30 )
Benzoic acid 6.771.63U 6.35 94 6.96 6.06 87 10-110 4.70 (< 30 )
Benzyl alcohol 4.850.271U 4.00 83 4.97 4.22 85 20-125 5.50 (< 30 )
Bis(2-Chloroethoxy)methane 4.850.271U 4.25 88 4.97 4.53 91 45-110 6.20 (< 30 )
Bis(2-Chloroethyl)ether 4.850.271U 4.34 90 4.97 4.75 96 40-105 8.90 (< 30 )
bis(2-Ethylhexyl)phthalate 4.850.271U 4.87 101 4.97 4.91 99 45-125 0.79 (< 30 )
Bis(2chloro1methylethyl)Ether 4.850.271U 3.81 79 4.97 4.02 81 20-115 5.40 (< 30 )
Butylbenzylphthalate 4.850.271U 4.97 103 4.97 5.25 106 50-125 5.70 (< 30 )
Carbazole 4.850.271U 3.89 80 4.97 4.13 83 45-115 6.00 (< 30 )
Chrysene 4.850.271U 4.36 90 4.97 5.03 101 55-110 14.40 (< 30 )
Di-n-butylphthalate 4.850.271U 4.44 92 4.97 4.57 92 55-110 2.90 (< 30 )
di-n-Octylphthalate 4.850.543U 4.52 93 4.97 4.69 95 40-130 3.90 (< 30 )
Dibenzo[a,h]anthracene 4.850.271U 4.64 96 4.97 5.17 104 40-125 10.70 (< 30 )
Dibenzofuran 4.850.271U 4.19 87 4.97 4.52 91 50-105 7.60 (< 30 )
Diethylphthalate 4.850.271U 4.74 98 4.97 4.99 100 50-115 5.10 (< 30 )
Dimethylphthalate 4.850.271U 4.72 98 4.97 5.14 103 50-110 8.50 (< 30 )
Fluoranthene 4.850.271U 3.50 72 4.97 3.74 75 55-115 6.70 (< 30 )
Fluorene 4.850.271U 4.11 85 4.97 4.27 86 50-110 3.90 (< 30 )
Hexachlorobenzene 4.850.271U 4.60 95 4.97 5.23 105 45-120 12.60 (< 30 )
Hexachlorobutadiene 4.850.271U 3.73 77 4.97 4.04 81 40-115 7.80 (< 30 )
Hexachlorocyclopentadiene 4.850.760U 3.05 63 4.97 3.90 78 48-108 24.20 (< 30 )
Hexachloroethane 4.850.271U 3.16 65 4.97 3.40 69 35-110 7.30 (< 30 )
Indeno[1,2,3-c,d] pyrene 4.850.271U 4.46 92 4.97 5.09 102 40-120 13.30 (< 30 )
Isophorone 4.850.271U 4.37 90 4.97 4.74 95 45-110 8.00 (< 30 )
N-Nitroso-di-n-propylamine 4.850.271U 4.36 90 4.97 4.85 97 40-115 10.40 (< 30 )
N-Nitrosodimethylamine 4.850.271U 3.44 71 4.97 3.56 71 20-115 3.40 (< 30 )
N-Nitrosodiphenylamine 4.850.271U 4.01 83 4.97 4.58 92 50-115 13.50 (< 30 )
Naphthalene 4.850.271U 3.58 74 4.97 3.78 76 40-105 5.30 (< 30 )
Nitrobenzene 4.850.271U 3.85 80 4.97 4.01 81 40-115 4.10 (< 30 )
Pentachlorophenol 6.772.17U 5.26 78 6.96 5.41 78 25-120 2.60 (< 30 )
Phenanthrene 4.850.271U 4.15 86 4.97 4.63 93 50-110 10.90 (< 30 )
Phenol 4.850.271U 3.60 75 4.97 3.79 76 40-100 4.90 (< 30 )
Pyrene 4.850.271U 5.30 109 4.97 5.74 115 45-125 8.00 (< 30 )
Surrogates
2,4,6-Tribromophenol 9.68 8.55 88 9.94 9.47 95 35-125 10.20
2-Fluorobiphenyl 4.85 4.09 85 4.97 4.54 91 45-105 10.30
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C377
Original Sample ID: 1132110021
MS Sample ID: 1150984 MS
MSD Sample ID: 1150985 MSD
Analysis Date:
Analysis Date: 06/06/2013 2:46
Analysis Date: 06/06/2013 3:03
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110001, 1132110002, 1132110003, 1132110004, 1132110005, 1132110006, 1132110007,
1132110008, 1132110009, 1132110010, 1132110011, 1132110012, 1132110013, 1132110014,
1132110015, 1132110016, 1132110017, 1132110018, 1132110019, 1132110021
Matrix Spike Summary
RPD CL
2-Fluorophenol 9.68 6.33 65 9.94 6.60 66 35-105 4.10
Nitrobenzene-d5 4.85 3.74 77 4.97 3.94 79 35-100 5.20
Phenol-d6 9.68 7.24 75 9.94 7.59 76 40-100 4.70
Terphenyl-d14 4.85 5.52 114 4.97 6.00 121 30-125 8.40
Batch Information
Prep Batch: XXX29094
Prep Method: Sonication Extraction Soil SW8270
Prep Date/Time: 6/4/2013 2:00:00PM
Prep Initial Wt./Vol.: 22.75g
Prep Extract Vol: 1.00mL
Analytical Batch: XMS7354
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: RTS
Analytical Date/Time: 6/6/2013 2:46:00AM
Print Date: 06/27/2013 5:39:46PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C378
Blank ID: MB for HBN 1453190 [XXX/29103]
Blank Lab ID: 1151196
QC for Samples:
1132110020, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
1,2,4-Trichlorobenzene 0.250 mg/Kg0.07800.156U
1,2-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,3-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1,4-Dichlorobenzene 0.250 mg/Kg0.07800.156U
1-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2,4,5-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4,6-Trichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,4-Dimethylphenol 0.250 mg/Kg0.07800.156U
2,4-Dinitrophenol 3.00 mg/Kg0.9401.88U
2,4-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2,6-Dichlorophenol 0.250 mg/Kg0.07800.156U
2,6-Dinitrotoluene 0.250 mg/Kg0.07800.156U
2-Chloronaphthalene 0.250 mg/Kg0.07800.156U
2-Chlorophenol 0.250 mg/Kg0.07800.156U
2-Methyl-4,6-dinitrophenol 2.00 mg/Kg0.6201.24U
2-Methylnaphthalene 0.250 mg/Kg0.07800.156U
2-Methylphenol (o-Cresol) 0.250 mg/Kg0.07800.156U
2-Nitroaniline 0.250 mg/Kg0.07800.156U
2-Nitrophenol 0.250 mg/Kg0.07800.156U
3&4-Methylphenol (p&m-Cresol) 1.00 mg/Kg0.3100.620U
3,3-Dichlorobenzidine 0.250 mg/Kg0.07800.156U
3-Nitroaniline 0.500 mg/Kg0.1500.300U
4-Bromophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Chloro-3-methylphenol 0.250 mg/Kg0.07800.156U
4-Chloroaniline 0.500 mg/Kg0.1500.300U
4-Chlorophenyl-phenylether 0.250 mg/Kg0.07800.156U
4-Nitroaniline 3.00 mg/Kg0.9401.88U
4-Nitrophenol 1.00 mg/Kg0.3100.620U
Acenaphthene 0.250 mg/Kg0.07800.156U
Acenaphthylene 0.250 mg/Kg0.07800.156U
Aniline 2.00 mg/Kg0.6201.24U
Anthracene 0.250 mg/Kg0.07800.156U
Azobenzene 0.250 mg/Kg0.07800.156U
Benzo(a)Anthracene 0.250 mg/Kg0.07800.156U
Benzo[a]pyrene 0.250 mg/Kg0.07800.156U
Benzo[b]Fluoranthene 0.250 mg/Kg0.07800.156U
Benzo[g,h,i]perylene 0.250 mg/Kg0.07800.156U
Print Date: 06/27/2013 5:39:47PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C379
Blank ID: MB for HBN 1453190 [XXX/29103]
Blank Lab ID: 1151196
QC for Samples:
1132110020, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Benzo[k]fluoranthene 0.250 mg/Kg0.07800.156U
Benzoic acid 1.50 mg/Kg0.7501.50U
Benzyl alcohol 0.250 mg/Kg0.07800.156U
Bis(2chloro1methylethyl)Ether 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethoxy)methane 0.250 mg/Kg0.07800.156U
Bis(2-Chloroethyl)ether 0.250 mg/Kg0.07800.156U
bis(2-Ethylhexyl)phthalate 0.250 mg/Kg0.07800.156U
Butylbenzylphthalate 0.250 mg/Kg0.07800.156U
Carbazole 0.250 mg/Kg0.07800.156U
Chrysene 0.250 mg/Kg0.07800.156U
Dibenzo[a,h]anthracene 0.250 mg/Kg0.07800.156U
Dibenzofuran 0.250 mg/Kg0.07800.156U
Diethylphthalate 0.250 mg/Kg0.07800.156U
Dimethylphthalate 0.250 mg/Kg0.07800.156U
Di-n-butylphthalate 0.250 mg/Kg0.07800.156U
di-n-Octylphthalate 0.500 mg/Kg0.1500.300U
Fluoranthene 0.250 mg/Kg0.07800.156U
Fluorene 0.250 mg/Kg0.07800.156U
Hexachlorobenzene 0.250 mg/Kg0.07800.156U
Hexachlorobutadiene 0.250 mg/Kg0.07800.156U
Hexachlorocyclopentadiene 0.700 mg/Kg0.2000.400U
Hexachloroethane 0.250 mg/Kg0.07800.156U
Indeno[1,2,3-c,d] pyrene 0.250 mg/Kg0.07800.156U
Isophorone 0.250 mg/Kg0.07800.156U
Naphthalene 0.250 mg/Kg0.07800.156U
Nitrobenzene 0.250 mg/Kg0.07800.156U
N-Nitrosodimethylamine 0.250 mg/Kg0.07800.156U
N-Nitroso-di-n-propylamine 0.250 mg/Kg0.07800.156U
N-Nitrosodiphenylamine 0.250 mg/Kg0.07800.156U
Pentachlorophenol 2.00 mg/Kg0.6201.24U
Phenanthrene 0.250 mg/Kg0.07800.156U
Phenol 0.250 mg/Kg0.07800.156U
Pyrene 0.250 mg/Kg0.07800.156U
Surrogates
2,4,6-Tribromophenol 35-125 %88.9
2-Fluorobiphenyl 45-105 %84.3
2-Fluorophenol 35-105 %60.4
Nitrobenzene-d5 35-100 %62.4
Print Date: 06/27/2013 5:39:47PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C380
Blank ID: MB for HBN 1453190 [XXX/29103]
Blank Lab ID: 1151196
QC for Samples:
1132110020, 1132110022
Matrix: Soil/Solid (dry weight)
Results by SW8270D
DL UnitsLOQ/CLResultsParameter
Method Blank
Phenol-d6 40-100 %69.9
Terphenyl-d14 30-125 %100
Batch Information
Analytical Batch: XMS7361
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Analytical Date/Time: 6/11/2013 8:12:00PM
Prep Batch: XXX29103
Prep Method: SW3550C
Prep Date/Time: 6/5/2013 12:00:00PM
Prep Initial Wt./Vol.: 22.5 g
Prep Extract Vol: 1 mL
Print Date: 06/27/2013 5:39:47PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C381
Blank Spike ID: LCS for HBN 1132110 [XXX29103]
Blank Spike Lab ID: 1151198
Date Analyzed: 06/11/2013 20:29
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110020, 1132110022
Result
1,2,4-Trichlorobenzene 4.44 69 ( 45-110 )3.07
1,2-Dichlorobenzene 4.44 61 ( 45-100 )2.73
1,3-Dichlorobenzene 4.44 61 ( 40-100 )2.70
1,4-Dichlorobenzene 4.44 62 ( 35-105 )2.77
1-Chloronaphthalene 1.78 94 ( 44-105 )1.67
2,4,5-Trichlorophenol 4.44 94 ( 50-110 )4.16
2,4,6-Trichlorophenol 4.44 83 ( 45-110 )3.71
2,4-Dichlorophenol 4.44 77 ( 45-110 )3.40
2,4-Dimethylphenol 4.44 78 ( 30-105 )3.49
2,4-Dinitrophenol 8 83 ( 15-130 )6.67
2,4-Dinitrotoluene 4.44 92 ( 50-115 )4.07
2,6-Dichlorophenol 1.78 79 ( 52-102 )1.41
2,6-Dinitrotoluene 4.44 92 ( 50-110 )4.11
2-Chloronaphthalene 4.44 82 ( 45-105 )3.66
2-Chlorophenol 4.44 66 ( 45-105 )2.91
2-Methyl-4,6-dinitrophenol 8 100 ( 30-135 )8.00
2-Methylnaphthalene 4.44 77 ( 45-105 )3.42
2-Methylphenol (o-Cresol) 4.44 69 ( 40-105 )3.08
2-Nitroaniline 4.44 94 ( 45-120 )4.17
2-Nitrophenol 4.44 73 ( 40-110 )3.25
3&4-Methylphenol (p&m-Cresol) 6.22 83 ( 40-105 )5.19
3,3-Dichlorobenzidine 4.44 88 ( 10-130 )3.90
3-Nitroaniline 4.44 94 ( 25-110 )4.16
4-Bromophenyl-phenylether 4.44 95 ( 45-115 )4.21
4-Chloro-3-methylphenol 4.44 89 ( 45-115 )3.93
4-Chloroaniline 4.44 78 ( 10-100 )3.46
4-Chlorophenyl-phenylether 4.44 93 ( 45-110 )4.14
4-Nitroaniline 4.44 94 ( 35-115 )4.16
4-Nitrophenol 6.22 97 ( 15-140 )6.05
Acenaphthene 4.44 87 ( 45-110 )3.87
Acenaphthylene 4.44 88 ( 45-105 )3.90
Aniline 4.44 62 ( 20-84 )2.74
Anthracene 4.44 91 ( 55-105 )4.02
Azobenzene 4.44 94 ( 63-117 )4.16
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C382
Blank Spike ID: LCS for HBN 1132110 [XXX29103]
Blank Spike Lab ID: 1151198
Date Analyzed: 06/11/2013 20:29
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110020, 1132110022
Result
Benzo(a)Anthracene 4.44 94 ( 50-110 )4.19
Benzo[a]pyrene 4.44 90 ( 50-110 )3.99
Benzo[b]Fluoranthene 4.44 92 ( 45-115 )4.10
Benzo[g,h,i]perylene 4.44 97 ( 40-125 )4.33
Benzo[k]fluoranthene 4.44 90 ( 45-125 )4.02
Benzoic acid 6.22 85 ( 10-110 )5.31
Benzyl alcohol 4.44 76 ( 20-125 )3.36
Bis(2-Chloroethoxy)methane 4.44 83 ( 45-110 )3.69
Bis(2-Chloroethyl)ether 4.44 81 ( 40-105 )3.58
bis(2-Ethylhexyl)phthalate 4.44 99 ( 45-125 )4.41
Bis(2chloro1methylethyl)Ether 4.44 66 ( 20-115 )2.95
Butylbenzylphthalate 4.44 101 ( 50-125 )4.50
Carbazole 4.44 96 ( 45-115 )4.27
Chrysene 4.44 98 ( 55-110 )4.35
Di-n-butylphthalate 4.44 101 ( 55-110 )4.47
di-n-Octylphthalate 4.44 100 ( 40-130 )4.44
Dibenzo[a,h]anthracene 4.44 98 ( 40-125 )4.36
Dibenzofuran 4.44 92 ( 50-105 )4.08
Diethylphthalate 4.44 97 ( 50-115 )4.31
Dimethylphthalate 4.44 97 ( 50-110 )4.33
Fluoranthene 4.44 92 ( 55-115 )4.08
Fluorene 4.44 89 ( 50-110 )3.97
Hexachlorobenzene 4.44 96 ( 45-120 )4.27
Hexachlorobutadiene 4.44 74 ( 40-115 )3.28
Hexachlorocyclopentadiene 4.44 85 ( 48-108 )3.76
Hexachloroethane 4.44 60 ( 35-110 )2.65
Indeno[1,2,3-c,d] pyrene 4.44 97 ( 40-120 )4.30
Isophorone 4.44 86 ( 45-110 )3.81
N-Nitroso-di-n-propylamine 4.44 83 ( 40-115 )3.67
N-Nitrosodimethylamine 4.44 71 ( 20-115 )3.16
N-Nitrosodiphenylamine 4.44 80 ( 50-115 )3.55
Naphthalene 4.44 71 ( 40-105 )3.16
Nitrobenzene 4.44 73 ( 40-115 )3.25
Pentachlorophenol 6.22 92 ( 25-120 )5.72
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C383
Blank Spike ID: LCS for HBN 1132110 [XXX29103]
Blank Spike Lab ID: 1151198
Date Analyzed: 06/11/2013 20:29
Results by SW8270D
Blank Spike Summary
Matrix: Soil/Solid (dry weight)
Parameter Spike Rec (%) CL
Blank Spike (mg/Kg)
QC for Samples: 1132110020, 1132110022
Result
Phenanthrene 4.44 94 ( 50-110 )4.17
Phenol 4.44 72 ( 40-100 )3.21
Pyrene 4.44 96 ( 45-125 )4.25
Surrogates
2,4,6-Tribromophenol 8.89 91 ( 35-125 )91.3
2-Fluorobiphenyl 4.44 82 ( 45-105 )81.7
2-Fluorophenol 8.89 60 ( 35-105 )59.6
Nitrobenzene-d5 4.44 70 ( 35-100 )69.6
Phenol-d6 8.89 70 ( 40-100 )69.6
Terphenyl-d14 4.44 95 ( 30-125 )95.1
Batch Information
Analytical Batch: XMS7361
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Prep Batch: XXX29103
Prep Method: SW3550C
Prep Date/Time: 06/05/2013 12:00
Spike Init Wt./Vol.: 4.44 mg/Kg Extract Vol: 1 mL
Dupe Init Wt./Vol.: Extract Vol:
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C384
Original Sample ID: 1132110020
MS Sample ID: 1151201 MS
MSD Sample ID: 1151202 MSD
Analysis Date: 06/11/2013 20:47
Analysis Date: 06/11/2013 21:04
Analysis Date: 06/11/2013 21:22
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110022
Matrix Spike Summary
RPD CL
1,2,4-Trichlorobenzene 4.550.254U 3.29 72 4.57 3.44 75 45-110 4.50 (< 30 )
1,2-Dichlorobenzene 4.550.254U 2.85 63 4.57 3.10 68 45-100 8.40 (< 30 )
1,3-Dichlorobenzene 4.550.254U 2.87 63 4.57 3.02 66 40-100 5.40 (< 30 )
1,4-Dichlorobenzene 4.550.254U 2.89 63 4.57 3.07 67 35-105 6.00 (< 30 )
1-Chloronaphthalene 1.830.254U 1.70 94 1.83 1.79 98 44-105 4.70 (< 30 )
2,4,5-Trichlorophenol 4.550.254U 4.34 95 4.57 4.37 96 50-110 0.50 (< 30 )
2,4,6-Trichlorophenol 4.550.254U 3.98 87 4.57 4.02 88 45-110 1.00 (< 30 )
2,4-Dichlorophenol 4.550.254U 3.45 76 4.57 3.81 83 45-110 9.80 (< 30 )
2,4-Dimethylphenol 4.550.254U 3.17 70 4.57 3.29 72 30-105 3.90 (< 30 )
2,4-Dinitrophenol 8.193.05U 5.67 69 8.22 6.01 73 15-130 5.70 (< 30 )
2,4-Dinitrotoluene 4.550.254U 4.17 92 4.57 4.30 94 50-115 3.10 (< 30 )
2,6-Dichlorophenol 1.830.254U 1.46 80 1.83 1.53 84 52-102 5.00 (< 30 )
2,6-Dinitrotoluene 4.550.254U 4.13 91 4.57 4.48 98 50-110 8.20 (< 30 )
2-Chloronaphthalene 4.550.254U 3.87 85 4.57 3.97 87 45-105 2.70 (< 30 )
2-Chlorophenol 4.550.254U 2.96 65 4.57 3.18 70 45-105 7.00 (< 30 )
2-Methyl-4,6-dinitrophenol 8.192.03U 7.81 95 8.22 8.44 103 30-135 7.70 (< 30 )
2-Methylnaphthalene 4.550.254U 3.43 75 4.57 3.64 80 45-105 5.90 (< 30 )
2-Methylphenol (o-Cresol) 4.550.254U 3.10 68 4.57 3.33 73 40-105 7.40 (< 30 )
2-Nitroaniline 4.550.254U 4.38 96 4.57 4.59 100 45-120 4.70 (< 30 )
2-Nitrophenol 4.550.254U 3.40 75 4.57 3.58 78 40-110 5.20 (< 30 )
3&4-Methylphenol (p&m-Cresol) 6.381.02U 5.16 81 6.40 5.44 85 40-105 5.20 (< 30 )
3,3-Dichlorobenzidine 4.550.254U 3.94 87 4.57 4.09 89 10-130 3.50 (< 30 )
3-Nitroaniline 4.550.508U 4.31 95 4.57 4.42 97 25-110 2.40 (< 30 )
4-Bromophenyl-phenylether 4.550.254U 4.29 94 4.57 4.61 101 45-115 7.10 (< 30 )
4-Chloro-3-methylphenol 4.550.254U 3.94 87 4.57 4.07 89 45-115 3.20 (< 30 )
4-Chloroaniline 4.550.508U 3.62 80 4.57 3.74 82 10-100 2.90 (< 30 )
4-Chlorophenyl-phenylether 4.550.254U 4.23 93 4.57 4.36 95 45-110 2.90 (< 30 )
4-Nitroaniline 4.553.05U 4.33 95 4.57 4.42 97 35-115 1.90 (< 30 )
4-Nitrophenol 6.381.02U 6.02 94 6.40 5.96 93 15-140 0.83 (< 30 )
Acenaphthene 4.550.254U 3.99 88 4.57 4.05 89 45-110 1.50 (< 30 )
Acenaphthylene 4.550.254U 4.11 90 4.57 4.21 92 45-105 2.50 (< 30 )
Aniline 4.552.03U 2.98 66 4.57 3.08 67 20-84 2.80 (< 30 )
Anthracene 4.550.254U 4.11 90 4.57 4.33 95 55-105 5.50 (< 30 )
Azobenzene 4.550.254U 4.30 95 4.57 4.38 96 63-117 1.50 (< 30 )
Benzo(a)Anthracene 4.550.254U 4.14 91 4.57 4.28 94 50-110 3.30 (< 30 )
Benzo[a]pyrene 4.550.254U 3.99 88 4.57 4.13 90 50-110 3.30 (< 30 )
Benzo[b]Fluoranthene 4.550.254U 4.19 92 4.57 4.30 94 45-115 2.50 (< 30 )
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C385
Original Sample ID: 1132110020
MS Sample ID: 1151201 MS
MSD Sample ID: 1151202 MSD
Analysis Date: 06/11/2013 20:47
Analysis Date: 06/11/2013 21:04
Analysis Date: 06/11/2013 21:22
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (mg/Kg) Spike Duplicate (mg/Kg)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110022
Matrix Spike Summary
RPD CL
Benzo[g,h,i]perylene 4.550.254U 3.92 86 4.57 3.77 82 40-125 4.20 (< 30 )
Benzo[k]fluoranthene 4.550.254U 3.94 87 4.57 4.19 92 45-125 6.10 (< 30 )
Benzoic acid 6.381.53U 2.09 33 6.40 2.40 38 10-110 13.50 (< 30 )
Benzyl alcohol 4.550.254U 3.38 74 4.57 3.50 77 20-125 3.40 (< 30 )
Bis(2-Chloroethoxy)methane 4.550.254U 3.82 84 4.57 3.99 87 45-110 4.50 (< 30 )
Bis(2-Chloroethyl)ether 4.550.254U 3.70 81 4.57 3.93 86 40-105 6.00 (< 30 )
bis(2-Ethylhexyl)phthalate 4.550.254U 4.50 99 4.57 4.64 102 45-125 3.10 (< 30 )
Bis(2chloro1methylethyl)Ether 4.550.254U 3.03 67 4.57 3.17 69 20-115 4.30 (< 30 )
Butylbenzylphthalate 4.550.254U 4.53 100 4.57 4.77 104 50-125 5.00 (< 30 )
Carbazole 4.550.254U 4.27 94 4.57 4.48 98 45-115 4.60 (< 30 )
Chrysene 4.550.254U 4.29 94 4.57 4.45 97 55-110 3.70 (< 30 )
Di-n-butylphthalate 4.550.254U 4.54 100 4.57 4.73 103 55-110 4.10 (< 30 )
di-n-Octylphthalate 4.550.508U 4.53 99 4.57 4.65 102 40-130 2.70 (< 30 )
Dibenzo[a,h]anthracene 4.550.254U 4.08 90 4.57 3.93 86 40-125 3.60 (< 30 )
Dibenzofuran 4.550.254U 4.08 90 4.57 4.26 93 50-105 4.40 (< 30 )
Diethylphthalate 4.550.254U 4.50 99 4.57 4.66 102 50-115 3.50 (< 30 )
Dimethylphthalate 4.550.254U 4.47 98 4.57 4.57 100 50-110 2.30 (< 30 )
Fluoranthene 4.550.254U 3.97 87 4.57 4.16 91 55-115 4.60 (< 30 )
Fluorene 4.550.254U 4.04 89 4.57 4.14 90 50-110 2.50 (< 30 )
Hexachlorobenzene 4.550.254U 4.15 91 4.57 4.47 98 45-120 7.40 (< 30 )
Hexachlorobutadiene 4.550.254U 3.41 75 4.57 3.64 80 40-115 6.80 (< 30 )
Hexachlorocyclopentadiene 4.550.712U 3.97 87 4.57 4.18 91 48-108 5.00 (< 30 )
Hexachloroethane 4.550.254U 2.76 61 4.57 2.99 66 35-110 8.30 (< 30 )
Indeno[1,2,3-c,d] pyrene 4.550.254U 3.97 87 4.57 3.89 85 40-120 2.00 (< 30 )
Isophorone 4.550.254U 3.83 84 4.57 3.99 87 45-110 4.30 (< 30 )
N-Nitroso-di-n-propylamine 4.550.254U 3.67 81 4.57 3.78 83 40-115 2.90 (< 30 )
N-Nitrosodimethylamine 4.550.254U 3.10 68 4.57 3.20 70 20-115 3.20 (< 30 )
N-Nitrosodiphenylamine 4.550.254U 3.58 79 4.57 3.83 84 50-115 6.80 (< 30 )
Naphthalene 4.550.254U 3.24 71 4.57 3.40 74 40-105 4.70 (< 30 )
Nitrobenzene 4.550.254U 3.24 71 4.57 3.32 73 40-115 2.30 (< 30 )
Pentachlorophenol 6.382.03U 5.25 82 6.40 5.55 87 25-120 5.50 (< 30 )
Phenanthrene 4.550.254U 4.13 91 4.57 4.42 97 50-110 6.80 (< 30 )
Phenol 4.550.254U 3.18 70 4.57 3.33 73 40-100 4.70 (< 30 )
Pyrene 4.550.254U 4.15 91 4.57 4.45 97 45-125 7.00 (< 30 )
Surrogates
2,4,6-Tribromophenol 9.11 8.34 92 9.14 8.85 97 35-125 5.90
2-Fluorobiphenyl 4.55 3.80 83 4.57 3.99 87 45-105 5.00
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C386
Original Sample ID: 1132110020
MS Sample ID: 1151201 MS
MSD Sample ID: 1151202 MSD
Analysis Date:
Analysis Date: 06/11/2013 21:04
Analysis Date: 06/11/2013 21:22
Matrix: Soil/Solid (dry weight)
Results by SW8270D
Matrix Spike (%) Spike Duplicate (%)
QC for Samples:
Parameter SpikeSample Result Rec (%) Spike Result Rec (%) CL RPD (%)
1132110020, 1132110022
Matrix Spike Summary
RPD CL
2-Fluorophenol 9.11 5.47 60 9.14 5.89 65 35-105 7.50
Nitrobenzene-d5 4.55 3.09 68 4.57 3.24 71 35-100 4.90
Phenol-d6 9.11 6.23 68 9.14 6.60 72 40-100 5.80
Terphenyl-d14 4.55 4.22 93 4.57 4.48 98 30-125 6.00
Batch Information
Prep Batch: XXX29103
Prep Method: Sonication Extraction Soil SW8270
Prep Date/Time: 6/5/2013 12:00:00PM
Prep Initial Wt./Vol.: 22.66g
Prep Extract Vol: 1.00mL
Analytical Batch: XMS7361
Analytical Method: SW8270D
Instrument: HP 6890/5973 SSA
Analyst: DSH
Analytical Date/Time: 6/11/2013 9:04:00PM
Print Date: 06/27/2013 5:39:48PM
Member of SGS Group
SGS North America Inc.200 West Potter Drive Anchorage, AK 95518
t 907.562.2343 f 907.561.5301 www.us.sgs.com
C387
C388
C389
C390
C391
ADDRESS 1317 S. 13th Avenue, Kelso, WA 98626 USA PHONE +1 360 577 7222 FAX +1 360 636 1068 ALS Group USA, Corp. Part of the ALS Group An ALS Limited Company
June 20, 2013 Analytical Report for Service Request No: K1305397 Julie Shumway SGS Environmental Services, Inc. 200 West Potter Drive Anchorage, AK 99518 RE: 1132110 Dear Julie: Enclosed are the results of the samples submitted to our laboratory on June 06, 2013. For your reference, these analyses have been assigned our service request number K1305397. Analyses were performed according to our laboratory’s NELAP-approved quality assurance program. The test results meet requirements of the current NELAP standards, where applicable, and except as noted in the laboratory case narrative provided. For a specific list of NELAP-accredited analytes, refer to the certifications section at www.alsglobal.com. All results are intended to be considered in their entirety, and ALS Group USA Corp. dba ALS Environmental (ALS) is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report. Please call if you have any questions. My extension is 3364. You may also contact me via Email at [email protected].
Respectfully submitted, ALS Group USA Corp. dba ALS Environmental Howard Holmes Project Manager HH/mj Page 1 of _______
C392
Acronyms ASTM American Society for Testing and Materials A2LA American Association for Laboratory Accreditation CARB California Air Resources Board CAS Number Chemical Abstract Service registry Number CFC Chlorofluorocarbon CFU Colony-Forming Unit DEC Department of Environmental Conservation DEQ Department of Environmental Quality DHS Department of Health Services DOE Department of Ecology DOH Department of Health EPA U. S. Environmental Protection Agency ELAP Environmental Laboratory Accreditation Program GC Gas Chromatography GC/MS Gas Chromatography/Mass Spectrometry LOD Limit of Detection LOQ Limit of Quantitation LUFT Leaking Underground Fuel Tank M Modified MCL Maximum Contaminant Level is the highest permissible concentration of a substance
allowed in drinking water as established by the USEPA. MDL Method Detection Limit MPN Most Probable Number MRL Method Reporting Limit NA Not Applicable NC Not Calculated NCASI National Council of the Paper Industry for Air and Stream Improvement ND Not Detected NIOSH National Institute for Occupational Safety and Health PQL Practical Quantitation Limit RCRA Resource Conservation and Recovery Act SIM Selected Ion Monitoring TPH Total Petroleum Hydrocarbons tr Trace level is the concentration of an analyte that is less than the PQL but greater
than or equal to the MDL.
C393
Inorganic Data Qualifiers* The result is an outlier. See case narrative.
# The control limit criteria is not applicable. See case narrative.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
E The result is an estimate amount because the value exceeded the instrument calibration range.
J The result is an estimated value.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
H The holding time for this test is immediately following sample collection. The samples were analyzed as soon as possible afterreceipt by the laboratory.
Metals Data Qualifiers# The control limit criteria is not applicable. See case narrative.
J The result is an estimated value.
E The percent difference for the serial dilution was greater than 10%, indicating a possible matrix interference in the sample.
M The duplicate injection precision was not met.
N The Matrix Spike sample recovery is not within control limits. See case narrative.
S The reported value was determined by the Method of Standard Additions (MSA).
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
W The post-digestion spike for furnace AA analysis is out of control limits, while sample absorbance is less than 50% of spike absorbance.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
+ The correlation coefficient for the MSA is less than 0.995.
Q See case narrative. One or more quality control criteria was outside the limits.
Organic Data Qualifiers* The result is an outlier. See case narrative.
# The control limit criteria is not applicable. See case narrative.
A A tentatively identified compound, a suspected aldol-condensation product.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
C The analyte was qualitatively confirmed using GC/MS techniques, pattern recognition, or by comparing to historical data.
D The reported result is from a dilution.
E The result is an estimated value.
J The result is an estimated value.
N The result is presumptive. The analyte was tentatively identified, but a confirmation analysis was not performed.
P The GC or HPLC confirmation criteria was exceeded. The relative percent difference is greater than 40% between the two analytical results.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL. DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a chromatographic interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
Additional Petroleum Hydrocarbon Specific QualifiersF The chromatographic fingerprint of the sample matches the elution pattern of the calibration standard.
L The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of lighter molecular weight constituents than the calibration standard.
H The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of heavier molecular weight constituents than the calibration standard.
O The chromatographic fingerprint of the sample resembles an oil, but does not match the calibration standard.Y The chromatographic fingerprint of the sample resembles a petroleum product eluting in approximately the correct carbon range,
but the elution pattern does not match the calibration standard.
Z The chromatographic fingerprint does not resemble a petroleum product.
C394
Agency Web Site Number
Alaska DEC UST http://dec.alaska.gov/applications/eh/ehllabreports/USTLabs.aspx UST-040
Arizona DHS http://www.azdhs.gov/lab/license/env.htm AZ0339
Arkansas - DEQ http://www.adeq.state.ar.us/techsvs/labcert.htm 88-0637
California DHS (ELAP) http://www.cdph.ca.gov/certlic/labs/Pages/ELAP.aspx 2286
DOD ELAP http://www.denix.osd.mil/edqw/Accreditation/AccreditedLabs.cfm L12-28
Florida DOH http://www.doh.state.fl.us/lab/EnvLabCert/WaterCert.htm E87412
Georgia DNR http://www.gaepd.org/Documents/techguide_pcb.html#cel 881
Hawaii DOH Not available -
Idaho DHWhttp://www.healthandwelfare.idaho.gov/Health/Labs/CertificationDrinkingWaterLabs/tabid/1833/Default.aspx -
Indiana DOH http://www.in.gov/isdh/24859.htm C-WA-01
ISO 17025 http://www.pjlabs.com/ L12-27
Louisiana DEQhttp://www.deq.louisiana.gov/portal/DIVISIONS/PublicParticipationandPermitSupport/LouisianaLaboratoryAccreditationProgram.aspx 3016
Louisiana DHH Not available LA110003
Maine DHS Not available WA0035
Michigan DEQ http://www.michigan.gov/deq/0,1607,7-135-3307_4131_4156---,00.html 9949
Minnesota DOH http://www.health.state.mn.us/accreditation 053-999-368
Montana DPHHS http://www.dphhs.mt.gov/publichealth/ CERT0047
Nevada DEP http://ndep.nv.gov/bsdw/labservice.htm WA35
New Jersey DEP http://www.nj.gov/dep/oqa/ WA005
New Mexico ED http://www.nmenv.state.nm.us/dwb/Index.htm -
North Carolina DWQ http://www.dwqlab.org/ 605
Oklahoma DEQ http://www.deq.state.ok.us/CSDnew/labcert.htm 9801
Oregon – DEQ (NELAP)http://public.health.oregon.gov/LaboratoryServices/EnvironmentalLaboratoryAccreditation/Pages/index.aspx WA200001
South Carolina DHEC http://www.scdhec.gov/environment/envserv/ 61002
Texas CEQ http://www.tceq.texas.gov/field/qa/env_lab_accreditation.html 4704427-08-TX
Washington DOE http://www.ecy.wa.gov/programs/eap/labs/lab-accreditation.html C1203
Wisconsin DNR http://dnr.wi.gov/ 998386840
Wyoming (EPA Region 8) http://www.epa.gov/region8/water/dwhome/wyomingdi.html -
Kelso Laboratory Website www.caslab.com NA
Columbia Analytical Services, Inc. dba ALS Environmental (ALS) - KelsoState Certifications, Accreditations, and Licenses
Analyses were performed according to our laboratory’s NELAP-approved quality assurance program. A complete listing of specific NELAP-certified analytes, can be found in the certification section at www.caslab.com or at the accreditation bodies web sitePlease refer to the certification and/or accreditation body's web site if samples are submitted for compliance purposes. The states highlighted above, require the analysis be listed on the state certification if used for compliance purposes and if the method/anlayte is offered by that state.
C395
Approved by______________________________________________
ALS ENVIRONMENTAL Client: SGS Environmental, Inc. Service Request No.: K1305397 Project: 1132110 Date Received: 06/06/13 Sample Matrix: Soil
Case Narrative All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples designated for Tier II data deliverables. When appropriate to the method, method blank results have been reported with each analytical test. Surrogate recoveries have been reported for all applicable organic analyses. Additional quality control analyses reported herein include: Matrix/Duplicate Matrix Spike (MS/DMS), and Laboratory Control Sample (LCS). Sample Receipt Twelve soil samples were received for analysis at ALS Environmental on 06/06/13. The samples were received in good condition and consistent with the accompanying chain of custody form. The samples were stored in a refrigerator at 4ºC upon receipt at the laboratory. Organotin Compounds Matrix Spike Recovery Exceptions: The matrix spike recovery of Tri-n-butyltin for sample batch QC was outside control criteria. Recovery in the Laboratory Control Sample (LCS) was acceptable, which indicated the analytical batch was in control. No further corrective action was appropriate. No other anomalies associated with the analysis of these samples were observed.
C396
1~lIENT: SGS - AK
PHONE NO: CONTACT: Julie Shumway
~U"""_" PROJECT 1132110 PWSIDI
NAME: PERMIT#:
North America inc.
CHAIN OF CUSTODY RECORD
SGS Reference: ALS Kelso
Additional Comments:
(907) 562-2343 # Preserv :3 / // ative C Used: ~o'><
locations Nationwide
Alaska
New Jersey
North Carolina
West Virgina
Maryland
New York
Indiana
Kentucky www us sos com
Page
I I REPORTS TO: Julie Shumway E-MAil: [email protected] 0 TYPE
I I I
N
I I c=
T m COMP 00
A G= '" I ~
INVOICE TO: QUOTE#: i GRAB I '" I I I N Multi
c I ') P.O.#: 1132110 e
2-RESERVED E Incre- :.::
SAMPLE IDENTIFICATION DATE TIME MATRIX! R mental I-
III MSD SGS lab# lociD REMARK8 for lab use mm/dd/vv HH:MM MATRIX s Soils I- MS
8MIC-K(0) 05/30/13 1029 8 1 GRAB x 1132110001
8MIC-K (1.5) 05/30/13 1037 8 1 GRAB x 1132110002
SMIC-l (0) 05/30/13 1544 S 1 GRAB )( 1132110005 , SMIC-l (1.5) 05/30/13 1552 S 1 GRAB x 1132110006
SMIC-O (0) 05/31/13 844 8 1 GRAB x 1132110009
8MIC-0 (0) D 05/31/13 847 5 1 GRAB x 1132110010
8MIC-0 (1.5) 05/31/13 855 8 1 GRAB x 1132110011
8MIC-M (0) 05/31/13 1323 5 1 GRAB x 1132110014
SMIC-M (1.5) 05/31113 1329 5 1 GRAB x 1132110015
SMIC-M (1.5) DIl 05/31/13 1331 8 1 GRAB x J·432110018
5~U"q,... B7: 1 Da~~ Time Roc,N.d By, vi U:!j)([kl,}"OD Projoot? YES~ Data Deliverable Requirements:
o ;~) 3 160'1- S1~, j/) (ALbiJLI, . Cooler ID: . ;t~1fel II report + csv Excel EDD
~~iShed By: (~) tJ Date Time Received By: i Requested Turnaround Time and-or Special instructions:
Relinquished By: (3) Date Time Received By:
Temp Blank ·C: Chain of Custody Seal: (Circle)
Relinquished By: (4) Date Time Received for Lpwv'Q""', By: or Ambient [ J INTACT BROKEN ABSENT
(See attached Sample Receipt Form) (See attached Sample Receipt form)
1 200 W. Potter Drive Anchorage, AK 99518 Tel: (9071562-2343 Fax: (SO?) 561-5301 http://www.sgs.comltermsandconditions.htm 1 5500 Business Drive Wilmington, NC 28405 Tel: (9101350-1903 Fax: (910) 350-1557
.
I
11321.10 TST
C397
1rdUENT: SGS-AK
PHONE 1110: COIIITACT: Julie Shumway
r<v.J"" PROJECT 1132110 PWSIDI NAME: PERMIT#:
SGS North America Inc.
CHAIN OF CUSTODY RECORD
SGS Reference: ALS Kelso
Additional Comments:
(907) 562-2343 # Preserv :3 // ative C Used:
~c~e,
Locations Nationwide
Alaska
New Jersey
North Carolina
West Virgina
Maryland
New York
Indiana
Kentucky WWW us SQS com
Page
REPORTS TO: Julie Shumway E-MAIL: [email protected] 0 N
I TYPE
I I c=
T '" COMP 00 A G= 0>
~
INVOICE TO: QUOTE#: I GRAB I '" I I I
I I c:
'j 1".0.#: 1132110 N Multi 2 I 2--RESERVED
E Incre~ x: SAMPLE IDENTIFICATION
DATE TIME MATRIX! R mental I-III MSD SGS lab# LoclD for lab use mm/dd/vv HH:MM MATRIX s Soils I- MS REMARKS
SMIC-N {OJ 05131/13 1049 S 1 GRAB x 1132110019
SMIC-N (1.5) 05/31/13 1056 S 1 GRAB x 1132110020
, I I I
//
~o;"~:;'~i Dat~ Time Roc.lv.' By, ~ \.,»00 Pro].", YES~ Data Deliverable Requirements: o 3
{0tI9 IS~';c~.L/~l){A(50 Cooler 10: ~~¥~llIrel>0rt ... csv I;:xcel EDD •.
/VtL~ ~ OS I~uished By: (2) 0 Date Time Received By: I
Relinquished By: (3) Date Time Received By:
Relinquished By: (4) Date Time Received for Laboratory By:
I 200 W. Potter Drive Anchorage, AK 99518 Tel: (907)562-2343 Fax: (907) 561·5301
I 5500 Business Drive Wilmington, NC 28405 Tel: (9101350-1903 Fax: (9101350-1557
Requested Turnaround Time and-or speciai instructions:
Temp Blank ·C: Chain of Custody Seal: (Circle)
or Ambient r ] INTACT BROKEN ABSENT
(See attached Sample Receipt Form) (See attached Sample Receipt form)
http://www.sgs.comftermsalldcol1oitions.htm
.
1132110 TBT2
C398
Cooler Receipt and Preservation Form pc~
Client/rrQj~ FxA,.,c2 .
Received;. i tAlli t.{f, Wt30pened:'IZhLLt:U13 By: tF.
1. Samples were received via? Mail Fed Ex c!iiii:) DHL PDX Courier Hand Delivered ,~
2. Samples were received in: (circle) ('....£.aa~) Envelope Other _____________ _
3. W ere custody seals on coolers? NA N If yes, how many and -- -
If present, were custody seals intact?
. ' r ...... · ~.-;."~:---.~--"
4 .. Paclcing material: Inserts Baggies fQ~ Wet Ice DIY Ice Sleeves
5. Were custody papers properly filled out (ink, signed, etc.)?
6. Did all bottles arrivein good condition (nnbroken)? . Indicat~ in the table below.
7. Were all sample labels complete (i.e aIlillysis; preservation, etcJ?' . . .
8 .. Did all sample hl.beis and t~gs agre~ with custody papers? Indicate major discrepandies in the table on page 2.
9. Were appropriate bottles!Gontaine~s and volumes received for the tests indicated?
IO.Were the pH-preserved bottles (see SMO ciEN SOP) received at the appropriate pH? Indicate in the table below.'
11: Were VOA vials received without headspace? Indicate in the table below.
Votes, Discrepancies, & Reso[utiolts0i.-,lj;"g-\ y VI.." \'- . ..e" vv"'"_v ...... 1 v'"!. Jl.. L. c ...... ,,~ ,
N
N
NA' N
NA N
NA N
NA. N
Y N
Y N
N
Page 01 ___ _ C399
ALS Group USA, Corp. dba ALS Environmental
Sample Name
Date
Collected
Date
Received
Date
AnalyzedLab Code Result
Result Notes
Test Notes:
Analysis Method: Basis: 160.3M Wet
Prep Method: Units: NONE PERCENT
Total Solids
Sample Matrix: Soil
Project: 1132110
Service Request: Client: SGS Environmental Services, Inc. K1305397
Analytical Results
K1305397-001 96.106/13/201305/30/2013 06/06/2013SMIC-K (0)
K1305397-002 97.506/13/201305/30/2013 06/06/2013SMIC-K (1.5)
K1305397-003 95.406/13/201305/30/2013 06/06/2013SMIC-L (0)
K1305397-004 97.706/13/201305/30/2013 06/06/2013SMIC-L (1.5)
K1305397-005 96.806/13/201305/31/2013 06/06/2013SMIC-O (0)
K1305397-006 97.306/13/201305/31/2013 06/06/2013SMIC-O (0) D
K1305397-007 97.206/13/201305/31/2013 06/06/2013SMIC-O (1.5)
K1305397-008 97.606/13/201305/31/2013 06/06/2013SMIC-M (0)
K1305397-009 98.206/13/201305/31/2013 06/06/2013SMIC-M (1.5)
K1305397-010 98.206/13/201305/31/2013 06/06/2013SMIC-M (1.5) D
K1305397-011 97.206/13/201305/31/2013 06/06/2013SMIC-N (0)
K1305397-012 97.106/13/201305/31/2013 06/06/2013SMIC-N (1.5)
SuperSet Reference: W1305749
Printed: 06/18/2013 15:53 1of1Page
u:\Stealth\Crystal.rpt\Solids.rpt
C400
ALS Group USA, Corp. dba ALS Environmental
QA/QC Report
Service Request:
Date Collected:
Date Received:
Date Analyzed:
05/30/2013
06/06/2013
06/13/2013
Client:
Project:
Sample Matrix:
1132110
Soil
Total Solids
Duplicate Sample Summary
Prep Method:
Analysis Method:
Test Notes:
NONE
160.3M
PERCENT
Wet
Units:
Basis:
Sample Name Lab Code
Result NotesSample
Result
Duplicate
Sample
Result Average
Relative
Percent
Difference
SGS Environmental Services, Inc. K1305397
96.496.1 96.3 <1SMIC-K (0) K1305397-001
SuperSet Reference: W1305749
Printed: 06/18/2013 15:53 2of1Page
u:\Stealth\Crystal.rpt\Solids.rpt
C401
ALS Group USA, Corp. dba ALS Environmental
QA/QC Report
Service Request:
Date Collected:
Date Received:
Date Analyzed:
05/31/2013
06/06/2013
06/13/2013
Client:
Project:
Sample Matrix:
1132110
Soil
Total Solids
Duplicate Sample Summary
Prep Method:
Analysis Method:
Test Notes:
NONE
160.3M
PERCENT
Wet
Units:
Basis:
Sample Name Lab Code
Result NotesSample
Result
Duplicate
Sample
Result Average
Relative
Percent
Difference
SGS Environmental Services, Inc. K1305397
97.397.2 97.3 <1SMIC-N (0) K1305397-011
SuperSet Reference: W1305749
Printed: 06/18/2013 15:53 2of2Page
u:\Stealth\Crystal.rpt\Solids.rpt
C402
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-001
ug/Kg
Dry
SMIC-K (0)
05/30/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1386
Comments:
1of1Page18:01:1006/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C403
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-002
ug/Kg
Dry
SMIC-K (1.5)
05/30/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1385
Comments:
1of1Page18:01:1306/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C404
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-003
ug/Kg
Dry
SMIC-L (0)
05/30/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/131.4Tri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1385
Comments:
1of1Page18:01:1606/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C405
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-004
ug/Kg
Dry
SMIC-L (1.5)
05/30/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1357
Comments:
1of1Page18:01:1906/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C406
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-005
ug/Kg
Dry
SMIC-O (0)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1369
Comments:
1of1Page18:01:2306/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C407
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-006
ug/Kg
Dry
SMIC-O (0) D
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1375
Comments:
1of1Page18:01:2606/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C408
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-007
ug/Kg
Dry
SMIC-O (1.5)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1360
Comments:
1of1Page18:01:2906/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C409
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-008
ug/Kg
Dry
SMIC-M (0)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/133.3Tri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1378
Comments:
1of1Page18:01:3206/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C410
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-009
ug/Kg
Dry
SMIC-M (1.5)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1372
Comments:
1of1Page18:01:3506/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C411
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-010
ug/Kg
Dry
SMIC-M (1.5) D
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1369
Comments:
1of1Page18:01:3806/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C412
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-011
ug/Kg
Dry
SMIC-N (0)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1366
Comments:
1of1Page18:01:4106/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C413
Analytical Results
SGS Environmental Services, Inc. K1305397
K1305397-012
ug/Kg
Dry
SMIC-N (1.5)
05/31/2013
06/06/2013
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
1.1 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1371
Comments:
1of1Page18:01:4406/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C414
Analytical Results
SGS Environmental Services, Inc. K1305397
KWG1305915-4
ug/Kg
Dry
Method Blank
NA
NA
1132110
Soil
Client:
Project:
Sample Matrix:
Service Request:
Date Collected:
Date Received:
ALS Group USA, Corp. dba ALS Environmental
Units:
Basis:
Sample Name:
Butyltins (as cation)
Lab Code:
Level: LowExtraction Method:
Analysis Method:
Method
Krone
NoteMRLQResultAnalyte Name
Extraction
Lot
Date
Analyzed
Date
Extracted
Dilution
Factor
0.98 06/13/131 KWG130591506/19/13UNDTri-n-butyltin Cation
Surrogate Name %Rec
Control
Limits NoteDate
Analyzed
10-120 AcceptableTri-n-propyltin 06/19/1389
Comments:
1of1Page18:01:4706/19/2013Printed: Form 1A - Organic
Merged SuperSet Reference: RR156187u:\Stealth\Crystal.rpt\Form1mNew.rpt
C415
ALS Group USA, Corp. dba ALS Environmental
Extraction Method:
QA/QC Report
Surrogate Recovery Summary
SGS Environmental Services, Inc. K1305397
Low
Soil
1132110
Client:
Project:
Sample Matrix:
Service Request:
Units:
Level:
Sample Name Lab Code
Butyltins (as cation)
Method
Analysis Method: Krone
Sur1
Percent
K1305397-001SMIC-K (0) 86
K1305397-002SMIC-K (1.5) 85
K1305397-003SMIC-L (0) 85
K1305397-004SMIC-L (1.5) 57
K1305397-005SMIC-O (0) 69
K1305397-006SMIC-O (0) D 75
K1305397-007SMIC-O (1.5) 60
K1305397-008SMIC-M (0) 78
K1305397-009SMIC-M (1.5) 72
K1305397-010SMIC-M (1.5) D 69
K1305397-011SMIC-N (0) 66
K1305397-012SMIC-N (1.5) 71
K1305491-001Batch QC 66
KWG1305915-4Method Blank 89
KWG1305915-1Batch QCMS 69
KWG1305915-2Batch QCDMS 69
KWG1305915-3Lab Control Sample 84
Form 2A - OrganicPrinted: 06/19/2013 18:01:51 1 of 1
Surrogate Recovery Control Limits (%)
10-120Tri-n-propyltin
Results flagged with an asterisk (*) indicate values outside control criteria.
Page
Results flagged with a pound (#) indicate the control criteria is not applicable.
RR156187SuperSet Reference:
Sur1 =
u:\Stealth\Crystal.rpt\Form2.rpt
C416
Matrix Spike/Duplicate Matrix Spike Summary
Sample
Result %Rec
Matrix Spike
%Rec
Limits
Duplicate Matrix Spike
%Rec RPD
RPD
Limit
QA/QC Report
SGS Environmental Services, Inc.
Batch QC
K1305491-001
Krone
K1305397
ug/Kg
Dry
Butyltins (as cation)
Soil
Low
1132110
Client:
Project:
Sample Matrix:
Service Request:
Sample Name:
Lab Code:
Extraction Method:
Analysis Method:
Units:
Basis:
Level:
Extraction Lot:
Analyte Name Result Result
ALS Group USA, Corp. dba ALS Environmental
Date Extracted:
Date Analyzed:
06/13/2013
06/19/2013
Method
KWG1305915
KWG1305915-2KWG1305915-1
Batch QCMS Batch QCDMS
Spike
Amount
Spike
Amount
10-115*12 29.6 4Tri-n-butyltin Cation 29.7 6 40413.6 13.1*
Form 3A - OrganicPrinted: 06/19/2013 18:01:54 Page 1 of 1
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
RR156187SuperSet Reference:
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
u:\Stealth\Crystal.rpt\Form3DMS.rpt
C417
Lab Control Spike Summary
%Rec
Lab Control Spike
%Rec
Limits
QA/QC Report
SGS Environmental Services, Inc. K1305397
Krone
ug/Kg
Dry
Lab Control Sample
KWG1305915-3
Butyltins (as cation)
KWG1305915
Soil
Low
1132110
Client:
Project:
Sample Matrix:
Service Request:
Units:
Basis:
Level:
Extraction Lot:
Analyte Name Result
Extraction Method:
Analysis Method:
ALS Group USA, Corp. dba ALS Environmental
Date Extracted:
Date Analyzed: 06/19/2013
06/13/2013
Method
Spike
Amount
10-122Tri-n-butyltin Cation 22.2 5111.4
Form 3C - OrganicPrinted: 06/19/2013 18:01:57 Page 1 of 1
Results flagged with an asterisk (*) indicate values outside control criteria.
RR156187SuperSet Reference:
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
u:\Stealth\Crystal.rpt\Form3LCS.rpt
C418
Page 1 of 7Version 2.7 01/10
Laboratory Data Review Checklist
Completed by: Kristi McLean
Title: Environmental Specialist Date: 24 July 2013
CS Report Name: SMIC Improvements 1770.01 Report Date: 27 June 2013
Consultant Firm: R&M Consultants, Inc.
Laboratory Name: SGS North America, Inc. Laboratory Report Number: 1132110
ADEC File Number: NA ADEC RecKey Number: NA
1. Laboratory
a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample analyses?
Comments:Yes No NA (Please explain.)
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS approved?
Comments:
Columbia Analytical Services, Inc. dba ALS Environmental is certified by the State of Alaska
NA (Please explain)Yes No
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)?
Comments:NA (Please explain)Yes No
b. Correct analyses requested? Comments:NA (Please explain)Yes No
3. Laboratory Sample Receipt Documentation
a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Comments:NA (Please explain)Yes No
C419
Page 2 of 7Version 2.7 01/10
b. Sample preservation acceptable - acidified waters, Methanol preserved VOC soil (GRO, BTEX, Volatile Chlorinated Solvents, etc.)?
Comments:NA (Please explain)Yes No
c. Sample condition documented - broken, leaking (Methanol), zero headspace (VOC vials)?
Comments:
All samples were received in good condition
NA (Please explain)Yes No
d. If there were any discrepancies, were they documented? - For example, incorrect sample containers/preservation, sample temperature outside of acceptance range, insufficient or missing samples, etc.?
Comments:
No discrepancies were documented.
NA (Please explain)Yes No
e. Data quality or usability affected? (Please explain)
Comments:
NA
a. Present and understandable?
4. Case Narrative
Comments:NA (Please explain)Yes No
b. Discrepancies, errors or QC failures identified by the lab?
Comments:NA (Please explain)Yes No
c. Were all corrective actions documented? Comments:
No corrective actions were identified.
NA (Please explain)Yes No
d. What is the effect on data quality/usability according to the case narrative? Comments:
NA
C420
Page 3 of 7Version 2.7 01/10
a. Correct analyses performed/reported as requested on COC?
5. Samples Results
Comments:NA (Please explain)Yes No
b. All applicable holding times met?
Comments:NA (Please explain)Yes No
c. All soils reported on a dry weight basis?
Comments:NA (Please explain)Yes No
Comments:
d. Are the reported PQLs less than the Cleanup Level or the minimum required detection level for the project?
NA (Please explain)Yes No
e. Data quality or usability affected? (Please explain) Comments:
Sample handling and results did not result in an issue that would have affected data quality or usability.
a. Method Blank6. QC Samples
i. One method blank reported per matrix, analysis and 20 samples?
Comments:NA (Please explain)Yes No
ii. All method blank results less than PQL? Comments:NA (Please explain)Yes No
iii. If above PQL, what samples are affected? Comments:
NA
C421
Page 4 of 7Version 2.7 01/10
iv. Do the affected sample(s) have data flags? If so, are the data flags clearly defined? Comments:
No samples were affected
NA (Please explain)Yes No
v. Data quality or usability affected? (Please explain) Comments:
No samples were affected; data quality and usability was not compromised.
i. Organics - One LCS/LCSD reported per matrix, analysis and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846)
Comments:
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
Yes No NA (Please explain)
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples?
Comments:NA (Please explain)Yes No
iii. Accuracy - All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK Petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages)
Comments:
LCS recovery for n-Triacontance is outside of QC criteria in one sample.
NA (Please explain)Yes No
iv. Precision - All relative percent differences (RPD) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/DMSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages)
Comments:NA (Please explain)Yes No
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments:
No samples were affected.
C422
Page 5 of 7Version 2.7 01/10
vi. Do the affected samples(s) have data flags? If so, are the data flags clearly defined?
Comments:
The samples were not affected and therefore not flagged.
NA (Please explain)Yes No
vii. Data quality or usability affected? (Please explain) Comments:
QC criteria was biased high and the identified analytes were not detected in the associated samples.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses - field, QC and laboratory samples?
Comments:NA (Please explain)Yes No
ii. Accuracy - All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages)
Comments:
Percent recoveries fell outside laboratory limits for 7 samples; QC was biased high and the identified analytes were not detected in the associated samples, therefore the data was not flagged.
NA (Please explain)NoYes
iii. Do the sample results with failed surrogate recoveries have data flags? If so, are the data flags clearly defined?
Comments:
No samples with failed surrogate recoveries were flagged.
NA (Please explain)Yes No
iv. Data quality or usability affected? (Use the comment box to explain.). Comments:
QC criteria was biased high and the identified analytes were not detected in the associated samples.
d. Trip Blank - Volatile analyses only (GRO, BTEX, Volatile Chlorinated Solvents, etc.): Water and Soil
i. One trip blank reported per matrix, analysis and for each cooler containing volatile samples? (If not, enter explanation below.)
Comments:Yes No NA (Please explain.)
ii. Is the cooler used to transport the trip blank and VOA samples clearly indicated on the COC? (If not, a comment explaining why must be entered below)
Comments:Yes No NA (Please explain.)
C423
Page 6 of 7Version 2.7 01/10
iii. All results less than PQL?
Comments:Yes No NA (Please explain.)
Comments:
NA
iv. If above PQL, what samples are affected?
v. Data quality or usability affected? (Please explain.)
Comments:
NA
e. Field Duplicatei. One field duplicate submitted per matrix, analysis and 10 project samples?
Comments:NA (Please explain)NoYes
ii. Submitted blind to lab?
Comments:Yes No NA (Please explain.)
iii. Precision - All relative percent differences (RPD) less than specified DQOs? (Recommended: 30% water, 50% soil) RPD (%) = Absolute Value of: (R1- R2) x 100 ((R1+ R2)/2) Where R1 = Sample Concentration R2 = Field Duplicate Concentration
Comments:
The RPD for sample SMIC-M(1.5) was 200% for DRO and 140% for RRO. DRO was detected in the sample but not the duplicate. All other RPDs were well below 20%.
NA (Please explain)Yes No
iv. Data quality or usability affected? (Use the comment box to explain why or why not.) Comments:
There is often variability with grab soil samples.
Yes No NA (Please explain)
C424
Page 7 of 7Version 2.7 01/10
Comments:
No decontamination sample was submitted to the lab.
f. Decontamination or Equipment Blank (if applicable)
i. All results less than PQL?
Comments:NA (Please explain)NoYes
NA (Please explain)Yes No
ii. If above PQL, what samples are affected? Comments:
NA
iii. Data quality or usability affected? (Please explain.) Comments:
NA
a. Defined and appropriate?
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab Specific, etc.)
Comments:
No data flags/qualifiers were associated with the samples.
Yes No NA (Please explain)
Reset Form
C425
APPENDIX D
2013 SAMPLING AND ANALYSIS PLAN Sampling and Analysis Plan For Dredge Sediment Characterization: Seward Marine Industrial Center Improvements, Seward, Alaska; Prepared by R&M Consultants, Inc., May 2013 ................................................................. 11 Pages
SAMPLING AND ANALYSIS PLAN for
DREDGE SEDIMENT CHARACTERIZATION: SEWARD MARINE INDUSTRIAL CENTER IMPROVEMENTS
SEWARD, ALASKA
Prepared for:
City of Seward P.O. Box 167
Seward, Alaska 99664
Prepared by:
R&M Consultants, Inc. 9101 Vanguard Drive
Anchorage, Alaska 99507
May 15, 2013
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 1 Seward, Alaska
SAMPLING AND ANALYSIS PLAN for
DREDGE SEDIMENT CHARACTERIZATION: SEWARD MARINE INDUSTRIAL CENTER IMPROVEMENTS
SEWARD, ALASKA
BACKGROUND AND OBJECTIVES R&M Consultants, Inc. (R&M) has been retained by the City of Seward to design and permit improvements to the existing Seward Marine Industrial Center (SMIC). The existing SMIC is a fairly open industrial harbor on the east side of Resurrection Bay (Figures 1 and 2); it was constructed in the early 1980’s, and has been in operation since. The Seward Ships Drydock Inc. (SSDI) is a lessor at SMIC who offers upland storage and maintenance/repair areas for vessels and a 5,000-ton Syncrolift vessel haul out facility. The SMIC also hosts Polar Seafoods (a seafood processor) and the City’s 250-ton marine TraveLift. The North Dock, which is a sheetpile cargo dock, has a fuel header (owned/operated by Shoreside Petroleum, Inc.) that is connected via subsurface 6-inch diameter pipeline to an aboveground fuel storage tank (AST), located on the north side of Morris Avenue just east of the intersection of Nash Road and Morris Avenue (Figure 2). The header and pipeline were reportedly constructed in the early 1980’s along with the rest of the SMIC. They have been used intermittently since construction. The existing SMIC basin has an approximate depth of -20 feet to -24 feet mean lower low water (MLLW). Proposed SMIC improvements generally include partially enclosing the harbor with a new breakwater on the west side, extending both the existing North Dock and East Dock, significantly enlarging the harbor basin by excavating/dredging inland, and adding moorage floats, gangways, utilities, and associated amenities. The purpose of this sampling and analysis plan is to set forth the dredge sediment characterization efforts that will be performed for this project, to inform both the permitting process and disposal considerations. Two disposal scenarios are being considered for this project, offshore disposal (offshore area to be determined) and upland disposal (location or locations to be determined), or a combination thereof. For offshore disposal, the U.S. Army Corps of Engineers (USACE) will have primary permitting authority, while for upland disposal options the Alaska Department of Environmental Conservation (ADEC) would be chiefly involved. For the actual permitting of the dredging and other SMIC improvements, the USACE will have primary permitting authority, while the ADEC will provide Section 401 water quality certification. SITE CONDITIONS AND “REASON TO BELIEVE ANALYSIS” Geology and Subsurface Conditions The site is located on the fan-delta of Fourth of July Creek. Fan-deltas are complex deposits consisting of sand, gravel and cobbles with minor amounts of fines. The deposits grade to finer sand and silt farther from shore. The density of the material is typically loose to medium dense. Fan-deltas are produced by rapid deposition of material on a steep slope at the angle-of-repose. The angle-of-repose is by definition at the limiting natural angle of gravitational stability. The following references comprise existing subsurface information available for the SMIC site. The boreholes from these references confirm that the deposits at the site generally consist of poorly graded gravel
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 2 Seward, Alaska
with sand interlayered with silty sand and silty gravel. Scattered thin layers of silt containing organic material were noted on some borehole logs. H4M Corporation, “Preliminary Report Soils Exploration, Fourth of July Creek, Seward, Alaska”, August 17, 1981. This investigation included drilling 11 test borings to depths ranging from 22 to 90 feet. The locations of the borings were not included in the available copies of the report. Most of the borings appear to have been drilled onshore, or in shallow water. The maximum water depth on any of the logs was 10 feet. Tetratech Limited, “Report of Geotechnical Investigations, Fourth of July Creek Marine Industrial Park, Seward, Alaska”, October 4, 1985. This investigation was performed to evaluate the stability of the cellular breakwater constructed in 1982. The report includes the logs of six borings by Quadra Engineering, Inc. from 1981, four borings by Golder and Associates from 1983, and five borings by Tetratech LTD from 1984. All of the these borings appear to have been drilled within the existing cellular breakwater, however, no drawing showing the borehole locations was included in the report. Peratrovich, Nottingham & Drage, Inc., “Seward Marine Industrial Center, North Dock Geotechnical Study” November, 1987. This investigation included two test pits on the beach, and five test borings in upland areas, all in the vicinity of the “North Dock”. The drilling method was not described in the report, however the logs indicate that “heaving sand” caused problems with sampling below the water table. Proximity to Potential Pollutant Sources ADEC Contaminated Sites Two sites listed in the ADEC contaminated sites database exist within 0.5-miles of the SMIC, and both are on the 165+ acre SMIC property. They are described below.
• During removal of a 1,000-gallon diesel underground storage tank in 1998, minor amounts of petroleum-based soil contamination were encountered, but at levels far below ADEC cleanup levels. A UST Assessment report was prepared in 2000, and ADEC closed the site without institutional controls in 2002.
• SSDI is an active boat refurbishing facility that has operated at the SMIC since 1985, offering services including sandblasting and painting of commercial ships. In 2007, Ecology and Environment, Incorporated, performed a site inspection at the SSDI facility, under contract to the United States Environmental Protection Agency (EPA). A total of 19 soil samples were collected at the SSDI facility in locations ranging from surface soils across the site to within the transfer pit (Figure 2) and from stockpiles of sandblast media. Diesel range organics (DRO), tributyltin (TBT), arsenic, copper, benzo[a]pyrene, polychlorinated biphenyls (PCB), nickel, benzo[b]fluoranthene, dibenzo[a,h]anthracene, barium, chromium and thallium were detected above the ADEC soil cleanup levels, and were evaluated as contaminants of potential concern. Following the site inspection, soils visibly impacted by spent sandblast media, and stockpiles of spent sandblast media, were removed from the site and disposed of at the Kenai Peninsula Borough landfill near Soldotna, Alaska. In 2009, soil sampling was performed at twelve areas across the SSDI site (at depths of 1.5 to 2.5 feet) to characterize any petroleum hydrocarbon contamination (DRO, gasoline range organics or
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 3 Seward, Alaska
GRO, and residual range organics or RRO, and benzene, toluene, ethylbenzene, and xylenes or BTEX); none was detected. In summary, during the investigations at this site soil samples were analyzed for contaminants of potential concern with the following laboratory analyses; DRO, GRO, RRO, volatile organic compounds (VOC) including BTEX, polycyclic aromatic hydrocarbons (PAH), semivolatile organic compounds (SVOC), metals, PCB, and TBT; these analyses identified the contaminants of potential concern mentioned previously. Based on this data and the subsequent cleanup actions at the site (hauling away affected materials), ADEC issued a Cleanup Complete letter in March of 2013.
Other Environmental Considerations Shoreside Petroleum, Inc. owns and operates an 8-inch diameter fuel header with three risers at the North Dock. The header is connected to the AST via an approximately 1,200-foot long, 6-inch diameter, buried fuel pipeline. Based on a search of the ADEC SPILLS and contaminated sites databases, there are no known leaks or spills associated with either the AST or the pipeline or header. This system is reportedly used only intermittently, as needed to supplement Shoreside Petroleum’s main operation in the City of Seward. Reason to Believe Based on available information, none of the environmental conditions noted above are expected to have directly impacted offshore sediments and upland soils targeted for dredging and excavation as part of the SMIC Improvements project. However, given their proximity and the industrial character of the area, there is sufficient “reason to believe” that contaminants may be present in the discharge material to warrant sampling and chemical testing. PCB were detected only in one general location in 2007, among debris in the bottom of the “transfer pit” (Figure 2). Given the subsurface, contained nature of the pit and the lack of any detected PCB in other 2007 surface soil samples near the transfer pit, there is no reason to believe that PCB are a contaminant of concern for this project, which involves excavation/dredging in areas significantly removed from the transfer pit. Petroleum constituents (DRO, GRO, RRO), VOC’s, and SVOC’s have been detected in prior investigations (E&E, 2007), but at discrete locations in upland work areas of the SSDI facility. The absence of any spill history and lack of sources (except the buried fuel pipeline and North Dock header) indicates a low likelihood that these contaminants are widespread across upland or offshore areas. However, the possibility of their presence cannot be ruled out with available information, so sampling for these constituents is included at a screening level in this sampling plan. TBT and metals have the greatest potential for being carried (e.g. in sandblast grit) by wind and water at the SMIC, and so sampling for these constituents is included throughout the methodology outlined below. The following sampling and analysis methods are proposed.
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 4 Seward, Alaska
SCOPE AND METHODS General Scope of Work Environmental sampling and analysis will be conducted in conjunction with a geotechnical drilling and sampling program. A truck-mounted drill rig will be used to advance borings, both offshore (from a large landing craft) and onshore. In addition, a Petersen grab sampler (clamshell-style) will be used from the landing craft to gather seafloor surface sediments. General locations of proposed drilling and grab-sampling operations are depicted in Figure 2, and summarized below in Table 1. Missing letters in the sequence reflect the fact that other geotechnical-specific boreholes are also being drilled, but are not designated for environmental sampling.
Table 1: Summary of Proposed Boreholes and Grab Samples
PRELIMINARY BOREHOLE/GRAB
ID
TYPE, PURPOSE
PLANNED TOTAL DEPTH (FEET)
ENVIRON- MENTAL SAMPLES
GEOTECH SAMPLES
E Drill, Full Dredge Prism Characterization 100 0-10 feet 15-100 F Drill, Full Dredge Prism Characterization 100 0-10 feet 15-100 K Drill, Full Dredge Prism Characterization 65 0-40 feet 45-65 L Drill, Full Dredge Prism Characterization 65 0-40 feet 45-65 M Drill, Full Dredge Prism Characterization 40 0-40 feet NA N Drill, Full Dredge Prism Characterization 40 0-40 feet NA O Drill, Full Dredge Prism Characterization 40 0-40 feet NA P Grab, Seafloor Surface Characterization 1 0-1 NA Q Grab, Seafloor Surface Characterization 1 0-1 NA R Grab, Seafloor Surface Characterization 1 0-1 NA S Grab, Seafloor Surface Characterization 1 0-1 NA T Grab, Seafloor Surface Characterization 1 0-1 NA
Full-dredge prism boreholes have been located in uplands, where access is straightforward, and offshore in areas where contamination might be most likely (i.e. nearshore in heavily used areas). The combination of borehole and grab sampler methods is being used to control the extremely high cost of drilling from a large landing craft. Boring/grab locations may be adjusted in the field depending on site conditions. The general work plan is as follows:
• The drillers will be prepared to drill with hollow stem augers, driven casing, or rotary wash methods as conditions warrant. Large split-spoon samplers (2.4” ID) will be used for collecting soils for environmental sampling in order to obtain sufficient sample volume for environmental testing. Sampling below the dredge prism will be performed by other geotechnical methods. This will be a 24-hour drilling operation while offshore.
• R&M’s geologist will directly supervise all drilling and associated activities, and will maintain a field log for each boring; recording the drilling progress, soil sampling intervals and recovery, soil sampler penetration rates, soil and descriptions (following ASTM D 2488, and DOT&PF 2003), and interpretation of the geotechnical conditions between sampled intervals. After drilling, R&M’s geologist will document the actual location of
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 5 Seward, Alaska
each test hole, using a recreational GPS unit. • R&M’s on-site environmental specialist (an ADEC-qualified person) will conduct or
oversee all environmental sampling. Sampling and Analysis Methods Seafloor surface sediment samples will be initially collected with a Petersen grab sampler at each offshore drill site. At upland locations, surface soil samples will be collected by hand from approximately 0 to 6 inches below grade, after the surface soil has been broken by the drill auger. For offshore and upland locations, split-spoon soil samples will generally be collected as close as possible (depending on wind/wave/tidal action) to 2.5 feet (1.5 feet in uplands) below the seafloor or ground surface, then at 5 feet below the seafloor or ground surface, then every 5 feet to the bottom of the dredge prism; a detailed sampling scheme is presented in Table 2. Soil samples from each boring will be screened for contaminants. In addition to physical screening methods of visual and olfactory observation to detect the presence/absence of petroleum contaminants, heated headspace field screening (using a photoionization detector, or PID) will be performed, but only on soil samples from upland borings that are not saturated. Field screening with a PID will be conducted by sealing soil within a zip-top bag, agitating it, and warming it to a minimum of five degrees Celsius prior to screening with a PID. Screening with the PID will be conducted at least 10 minutes, but no longer than one hour, after soil collection. Analytical soil sample collection depths and proposed test methods are described below in Table 2. These apply to both offshore and upland boreholes and grab sample locations.
Table 2: Analytical Soil Sample Collection and Testing BOREHOLE/GRAB
LOCATIONS DEPTH (FEET) BELOW GROUND
SURFACE OR SEAFLOOR ANALYSIS TEST METHOD
E
S*,5,10 S*,5,10 S*,5,10 S*,5,10 S*,5,10
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
F
S*,5,10 S*,5,10 S*,5,10 S*,5,10
S*,5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
K
S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40**
S*,1.5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
L
S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40**
S*,1.5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 6 Seward, Alaska
M
S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40**
S*,1.5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
N
S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40**
S*,1.5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
O
S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40** S*,1.5, 5-40**
S*,1.5
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
P
NA NA S* S* S*
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
Q
NA NA S* S* S*
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
R
NA NA S* S* S*
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
S
S* S* S* S* S*
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989
T
NA NA NA S* S*
GRO/DRO/RRO VOC
SVOC RCRA Metals
TBT
AK101/AK102/AK103 EPA 8260B EPA 8270 EPA 6020
Krone 1989 *S denotes surface sediment sample (0-1 feet) **Up to two additional analytical samples will be collected between 5 and 40 feet based on field screening (visual, olfactory, PID). If no indications of contamination are encountered, sample depths will be assigned to ensure a relatively even distribution of sample depths across the site. If groundwater table is encountered, then one of those samples will be collected from saturated soils just above the groundwater table.
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 7 Seward, Alaska
Analytical soil samples will be collected immediately after opening the split-spoon sampler, in order of decreasing volatility, beginning with GRO and VOC, followed by DRO/RRO, SVOC, RCRA Metals, and TBT. Physical and field screening (described above) results will be used to identify which samples are to be submitted for laboratory analysis, in accordance with the scheme set forth in Table 2. A dedicated stainless steel sample spoon and nitrile gloves will be used for each sample. Soil samples will be placed in new laboratory-grade glass jars, and sealed with teflon-lined (as appropriate) screw caps. Each analytical soil sample will be given a unique identifier with the site ID, location, and sample depth, namely SMIC-E (5’). All sample containers will be labeled immediately upon or prior to filling, and placed in a cooler on frozen gel packs along with a Chain-of Custody form, which will identify the sample location, date, time, and collection personnel for all samples. Samples will be maintained at a temperature of two to six degrees Celsius by R&M until delivery to SGS Laboratories in Anchorage. Sample storage may occur as necessary, when sample shipping to the laboratory cannot be accomplished the same day. Samples will be delivered to the laboratory as rapidly as possible in order to comply with holding time requirements. Decontamination Split-spoon samplers and stainless steel tubs (for handling larger Petersen grab samples) will be decontaminated in a 3-step process. First the item will be washed with sea water or fresh potable water to remove soil and residue, then washed with a 1% Alconox solution in seawater or potable water, then the item will be rinsed with seawater (offshore work) or deionized water (uplands work). Investigation Derived Wastes Unused soil will be discarded over the side of the vessel or spread on uplands adjacent to each sampling site. Decontamination water will be discharged onsite. Solid waste will be bagged and placed in an appropriate dumpster or refuse container. QUALITY CONTROL Duplicate samples will be collected at specific locations at the rate of one duplicate per 10 samples collected, and will be submitted for laboratory analysis in a manner identical to regular samples. Results of duplicate samples will be examined for variation in analytical results. The report will comment on the accuracy of the laboratory analyses. A completed ADEC Laboratory Data Review Checklist will accompany final analytical results submission to ADEC. Chain-of-Custody documentation will accompany all laboratory samples throughout the analytical process. A soil trip blank preserved in methanol will accompany each cooler, and will be analyzed in conjunction with all samples being analyzed for GRO and VOC. SCHEDULE At the present time, field work is scheduled to begin the week May 20, 2013. It is anticipated that the total field program will be completed in approximately two weeks or less.
Sampling and Analysis Plan Seward Marine Industrial Center Improvements R&M Consultants, Inc. 8 Seward, Alaska
REPORTING A report will be prepared by an ADEC-qualified person documenting the work performed, photos of the work, laboratory data, and an ADEC laboratory data review checklist. REFERENCES Alaska Department of Environmental Conservation, “18 AAC 75, Oil and Other Hazardous
Substances Pollution Control,” As Amended Through October 9, 2008. Alaska Department of Environmental Conservation, Division of Spill Prevention and Response,
Contaminated Sires Program, “Draft Field Sampling Guidance,” May, 2010. Alaska Department of Environmental Conservation, Division of Spill Prevention and Response,
Contaminated Sires Program, “ADEC Decision Document: Seward Ship’s Drydock Cleanup Complete Determination”, March 11, 2013.
Ecology and Environment, Inc. (E&E), “Seward Ship’s Drydock Site Inspection, Seward, Alaska”
September 2007.
PROJECT
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LEGEND
GEOTECHNICAL/DREDGE SAMPLING BOREHOLE
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DREDGE LIMITS
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