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No. 28519

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Site; RTF

te q u i s i t i o n N u M b e r ; 6280.0001ase; 7039C1 2780Del iverables ; 21lb31401000

. .Turna round! 26 Days P r i o r i t y ;analysis Codes; 199

CoMpuCheM Number; 28519Account NuMber; 703901

Due: 06/26/84

Lab I n s t r u c t i o n s ;•-'" ̂ *—— •̂* Mf —" •B4F ———— *f B^ •&" •^~ *^ •̂ - -——* ^̂ > '» ̂ * 4^* *&« •4«* M 4— k—— *̂ 4b —4 f 4-J ̂ ——— fk «M k— fa^J fft _M ——J •M* rtM bf w —^ ^^ *—— lu ̂ uf _J ——— te4 «faJ fq k——r If •M| f—— «« K——m -bJ ̂ J h^J.kJ ft— nu •q ——I ——— _^ ._-» ___

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|iC C o u n t e r ; 177 Ac t ion Step; 2Log Page; 352 Origin; 1 0 0 Type; SS

Data Req CoMplete ^0

§-^^--_-.^ „-„„_„„» Acids Ex t rac t i ons /GCMS Uorksheet, CoMpound List, RIC Ac^diSi

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REPEAT REQUEST FORM

3 Product-ion sample ^J>3-Quality Control sampleI: 3BL J>^SS XX£)5 C 3BS C 3&UF'

'ft! IOH; CTR/LOG page /

Igacid

3 TCDDlerbic ide

•t 3 base/neutralE 3 VOPT$>a pesticidet 3 Other;

Samples to choose 4*roiB i_________„"usc^/ftJy ^f^e^Tft^^ €^E_Special Instructions i

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3WEINJECT ONLY E>rf RE-EXTRACT t REINJECT E 3 REPREP & REIHJECT

1LUTE C 3 SECONDARY CLEAMUP C 3 OTHER -EN-

CODES

iC LABORATORY

GC (XCK UST

IStFORHATlOh mrr. (4 pages)

?ASE OF EXTRACTION WORWTlON/CtmKTS

Jst run s^pio ehroBiatOflram & quantUatlon report ceq. code /^?^

,1st run stftnrffifd chroma trogwis 2 ^uantUstlon report seq. cede__„

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COMPOUND LIST

COMPUCHEM NO*^2,gJ79 PATE

IDEMTIFIIR PESTICIDES (IQW IEVEL-S011D)«0.

s*2.3.4.5.6.7.8.9.

10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.

COMPUCHEMCOWOUHDJlimBER

0701070207030704070507060707

07090710071107120713071407150716071707180719072007210722072307240725

Sp/k^ ̂ c. =- / pCOyOUHDN^E______ RESULT DETECTION \W\ ("aAgL^ALDP.1K ——".—————-———. ^ 4.0 X -̂̂ Ty ;̂AlPHA-BHC -———-.*-— 4.0 ' /-8EU-BHC —-——"——- 4,0 / ̂6AWA-8HC ——"——**- 4.0DELTA-BHC ————«—«.— 4»0CMLORDANE -

6C CHECKLIST

YESCOMM SOLIDSEPA SOLIDS NO

PESTICIDES-LOW LEVEL(1 ) 10% present?

If no, schedule for re-extraction (unless Hs QC"send to OA).

(2) d1 butyl chlorendate—advisory >25% >25%

If no, send to QA for evaluation (unless Us being re-extracted),

(3) possible carryover or contamination? {̂ 3

If yes, ffiust relnject for carryover and reextract for contanlnatlon.

(4) other problems for resolution by QA? r~'|

If yes, describe:

If this Is re*extraet/reprep data (due to failed surrogates) the results mustconfirm the original surr. recovery problems to be accepted; the spproprl&te QANotice (#14) wust be -(riserted. FOR £PAs. If original data differs from repeat'sproblem (sim unacceptable), the sample fnust be repeated ag^ln, FORCOWERC1ALS, both sets of data should he sent to QA Department.+EA » re-extract acceptable IF DATA FAILS. INSERT COM01TION CODE

JA • relnject acceptable FROM REPEAT P^UEST FORM IN BOX.OA * repeat conflrwed original muUsOK « original data acceptable (not for REPEATS) FINAL STATUS COOE^ G^//QM •* Insufficient sample for repeat ••'''̂ ^Q7^

IF MULTIPLE PACKAGES EXIST. REPORT THIS DATA:

001478

PESTICIDES—LOW LEVEL SOLIDS (p. 2)

ADDITIONAL CRITERIA FOR QC SAMPLES:

(5) b1anks"-HSL compounds confirmed by relnjectlon?

If yes, send to QA Department for evaluation of associated samples. *•a(6) blanks (cont'd)—serious non-HSL contamination confirmed? | |fc nni I

If yes» send to QA Oept. for evaluation.(7) blank splkes—HSL eompoun

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7-1-836C CHECK LIST

JKF&RWTION INSET. {4 pages)

J*A6E OF EXTRACTION INFORMATION/COMMENTS

Jst run sample chromatogram & qu&ntltaUon report seq. codg_^^^ _

Jst run standard chromatrograffis 6 QuantUation report seq. code.^fL

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EXTRACTION INrORrtATlON

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