report 122: the crustal evolution of the rudall province ...€¦ · tessalina s 2013, the crustal...

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Government of Western Australia THE CRUSTAL EVOLUTION OF THE RUDALL PROVINCE FROM AN ISOTOPIC PERSPECTIVE Department of Mines and Petroleum by CL Kirkland, SP Johnson, RH Smithies, JA Hollis, MTD Wingate,IM Tyler, AH Hickman, JB Cliff, EA Belousova, RC Murphy, and S Tessalina Geological Survey of Western Australia REPORT 122

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Page 1: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

Government of Western Australia

THE CRUSTAL EVOLUTION OF THE

RUDALL PROVINCE FROM AN

ISOTOPIC PERSPECTIVE

Department of

Mines and Petroleum

by CL Kirkland, SP Johnson, RH Smithies, JA Hollis,

MTD Wingate,IM Tyler, AH Hickman, JB Cliff,

EA Belousova, RC Murphy, and S Tessalina

Geological Survey of Western Australia

REPORT122

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REPORT 122

THE CRUSTAL EVOLUTION OF THE

RUDALL PROVINCE FROM AN

ISOTOPIC PERSPECTIVE

byCL Kirkland, SP Johnson, RH Smithies, JA Hollis, MTD Wingate,

IM Tyler, AH Hickman, JB Cliff, EA Belousova1, RC Murphy1, and S Tessalina2

Perth 2013

Geological Survey of Western Australia

1 GEMOC, Department of Earth & Planetary Sciences, Macquarie University, Sydney NSW 2109

2 John De Laeter Centre for Isotope Research, GPO Box U1987, Perth WA 6845

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MINISTER FOR MINES AND PETROLEUM

Hon. Bill Marmion MLA

DIRECTOR GENERAL, DEPARTMENT OF MINES AND PETROLEUM

Richard Sellers

EXECUTIVE DIRECTOR, GEOLOGICAL SURVEY OF WESTERN AUSTRALIA

Rick Rogerson

REFERENCE

The recommended reference for this publication is:

Kirkland CL, Johnson SP, Smithies RH, Hollis JA, Wingate MTD, Tyler IM, Hickman AH, Cliff JB, Belousova EA, Murphy RC and

Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey of Western Australia,

Report 122, 30p.

National Library of Australia Cataloguing-in-Publication entry

Author: Kirkland, C. L., author.

Title: The crustal evolution of the Rudall province from an isotopic perspective / C. L. Kirkland [and ten others]

ISBN: 9781741684995 (ebook)

Subjects: Soil crusting--Western Australia--Rudall Province.

Earth (Planet)--Crust.

Isotopes.

Other Authors/Contributors: Geological Survey of Western Australia, issuing body

Dewey Number: 551.1409941

ISSN 0508–4741

U–Pb measurements were conducted using the SHRIMP II ion microprobes at the John de Laeter Centre of Isotope Research

at Curtin University in Perth, Australia. Isotope analyses were funded in part by the Western Australian Government

Exploration Incentive Scheme (EIS). Lu–Hf measurements were conducted using LA-ICPMS at the ARC National Key Centre

for Geochemical Evolution and Metallogeny of Continents (GEMOC), via the ARC Centre of Excellence in Core to Crust Fluid

Systems (CCFS), based in the Department of Earth and Planetary Sciences at Macquarie University, Australia.

Copy editor: K Coyle

Cartography: M Prause

Desktop publishing: RL Hitchings

Printed by Images on Paper, Perth, Western Australia

Published 2013 by Geological Survey of Western Australia

This Report is published in digital format (PDF), as part of a digital dataset, and is available online at

<www.dmp.wa.gov.au/GSWApublications>.

Further details of geological publications and maps produced by the Geological Survey of Western Australia

are available from:

Information Centre

Department of Mines and Petroleum

100 Plain Street

EAST PERTH WESTERN AUSTRALIA 6004

Telephone: +61 8 9222 3459 Facsimile: +61 8 9222 3444

www.dmp.wa.gov.au/GSWApublications

Cover photograph: Bouguer gravity anomaly map of central Western Australia. The image highlights the Anketell Regional Gravity

Ridge which approximately outlines the location of the Paterson Orogen. The Rudall Province lies within this gravity feature.

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iii

Contents

Abstract ..................................................................................................................................................................1

Introduction ............................................................................................................................................................1

Geological setting of the Rudall Province .............................................................................................................2

The Talbot Terrane ..........................................................................................................................................2

The Connaughton Terrane ...............................................................................................................................4

The Tabletop Terrane .......................................................................................................................................4

Structural evolution .........................................................................................................................................4

Lu–Hf and oxygen isotopes, and reinterpreted SHRIMP U–Pb geochronology ...................................................5

Analytical methodology ..................................................................................................................................5

Lu–Hf isotopes .........................................................................................................................................5

Oxygen isotopes .....................................................................................................................................14

Talbot Terrane ...............................................................................................................................................14

Kalkan Supersuite ..................................................................................................................................14

GSWA 112379: biotite monzogranite (augen) gneiss, Split Rock ..................................................14

GSWA 104981: biotite–muscovite monzogranite gneiss, southern part of Graphite Valley ..........14

GSWA 111854: biotite–muscovite granodiorite gneiss, Poonemerlarra Creek west......................14

GSWA 112341: micromonzogranite (meta-aplite) dyke, Rudall airstrip .......................................16

GSWA 110056: biotite–hornblende granodiorite gneiss, Rooney Creek .......................................17

GSWA 112101: biotite-epidote monzogranite gneiss, Larry Creek ...............................................17

GSWA 111843: biotite–muscovite monzogranite gneiss, Poynton Creek ......................................17

GSWA 104980: monzogranite gneiss, Graphite Valley ..................................................................17

GSWA 112310: granodiorite gneiss, Dunn Creek west ..................................................................18

GSWA 112397: coarse-grained porphyritic biotite monzogranite (augen) gneiss,

Watrara Inlier ..................................................................................................................................18

Eastern Association ................................................................................................................................18

GSWA 104989: muscovite quartzite, Fingoon Quartzite................................................................18

Mesoproterozoic granites .......................................................................................................................18

GSWA 112102: seriate biotite metamonzogranite, southern part of the Watrara Inlier .................18

Connaughton Terrane ....................................................................................................................................18

Kalkan Supersuite ..................................................................................................................................18

GSWA 113035: orthogneiss, east of South Rudall Dome ..............................................................18

GSWA 113002: granodiorite gneiss, Cotton Creek ........................................................................18

Unassigned gneissic rocks .....................................................................................................................19

GSWA 112160: garnet microgneiss, Harbutt Range ......................................................................19

Tabletop Terrane .....................................................................................................................................19

GSWA 118914: foliated granite, north of Harbutt Range ...............................................................19

Discussion ............................................................................................................................................................19

Hf isotope signatures of Paleoproterozoic Australia .....................................................................................19

Capricorn Orogen ...................................................................................................................................19

Pilbara Craton ........................................................................................................................................21

Arunta Orogen........................................................................................................................................21

Musgrave Province .................................................................................................................................21

Inherited and detrital zircons of the Rudall Province ....................................................................................22

Hf isotopic signature of the Rudall Province ...............................................................................................23

Crust formation and underplating at 1900 Ma .......................................................................................23

Constraints on the tectonic evolution of the Rudall Province ......................................................................25

Implications for terrane boundaries .............................................................................................................26

Conclusions ...................................................................................................................................................26

References ............................................................................................................................................................27

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iv

Figures

1. Simplified geological map indicating the location of the Rudall Province relative to other

Proterozoic orogens and Archean cratons in Western Australia ...................................................................3

2. Simplified geological map of the Rudall Province, indicating the main geological features

and the distribution of terranes .....................................................................................................................3

3. a) and b): Stacked concordia diagrams showing U–Pb zircon analytical data for zircons from

Rudall Province samples analysed by SHRIMP ion microprobe ...............................................................15

4. Hf evolution diagrams for Rudall Province samples compared to potential source regions ....................17

5. Initial 176Hf/177Hf evolution diagram for samples from the Rudall Province compared to

potential source regions ..............................................................................................................................20

6. Hf evolution diagram for inherited zircons from Rudall Province intrusive rocks compared to

potential West Australian Craton source regions ........................................................................................22

7. Magmatic crystallization ages and two-stage Hf model ages for zircons from Rudall Province

magmatic rocks ............................................................................................................................................. 24

8. Oxygen isotope analyses of zircons from Mesoproterozoic metamonzogranite sample

GSWA 112102 ............................................................................................................................................24

9. Comparison of 176Yb/177Hf ratios for zircons from two Mesoproterozoic magmatic rocks with

those from other Rudall Province magmatic rocks of Paleoproterozoic age ............................................24

10. Time-space diagrams showing magmatic and metamorphic U–Pb ages for the Gascoyne

Province, Rudall Province, and Arunta Orogen .........................................................................................25

Tables

1. Lu–Hf isotopic measurement of zircons from the Rudall Province .............................................................6

2. Oxygen isotope analyses from zircons of sample GSWA 112102 .............................................................12

3. Summary of U-Pb SIMS dates for Rudall Province ..................................................................................13

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1

The crustal evolution of the Rudall Province

from an isotopic perspective

by

CL Kirkland, SP Johnson, RH Smithies, JA Hollis, MTD Wingate, IM Tyler, AH Hickman, JB Cliff, EA Belousova1, RC Murphy1, and S Tessalina2

AbstractThe Rudall Province, in the Paterson Orogen, is part of the West Australian Craton (WAC) and now lies to the east of the Archean

East Pilbara Terrane. Components within the Rudall Province have previously been linked to the Arunta Orogen of the North

Australian Craton based on similarities in timing of magmatism, deformation, and metamorphism and hence have been regarded

as exotic terranes on the margin of the WAC. The Rudall Province is divided into three lithotectonic elements known as the Talbot,

Connaughton, and Tabletop Terranes. The southern two terranes (Talbot and Connaughton) were affected by magmatism related

to collision between the West and North Australian Cratons during the 1800–1765 Ma Yapungku Orogeny. Zircons within the

Talbot Terrane and Connaughton Terrane indicate crustal residence ages of 3.4 – 2.4 Ga, with strong isotopic and, in the case of

inheritance, temporal affinity to detritus that originated from Capricorn Orogen basement sources (e.g. 2005–1970 Ma Dalgaringa

Supersuite of the Glenburgh Terrane). Furthermore, the range of Hf isotopic compositions in c. 1800 Ma magmatic zircons in the

Rudall Province has similarity to that in the c. 1800 Ma Bridget Suite, which has an undisputed association to the Pilbara Craton.

Hence, sources for all isotopic compositions preserved within the Rudall Province are present within the proximal West Australian

Craton. There is no necessity to invoke transfer of exotic North Australian Craton lithotectonic units to the West Australian Craton

margin and to suggest an accretionary style of orogenesis for the Rudall Province.

The Tabletop Terrane has been regarded as a different far-travelled block with crust unique to the other components of the Rudall

Province. This inference was based on the resemblance of magmatism in this terrane to that in the northern Gawler and Musgrave

regions. However, the similarity of source compositions throughout all three terranes of the Rudall Province implies that the

Tabletop Terrane was derived from crust of similar composition to the Connaughton and Talbot terranes. A phase of crust formation

at 1.9 Ga is indicated by zircons within a Talbot Terrane c. 1450 Ma monzogranite, which have mantle-like oxygen isotope ratios.

This timing of crust formation is distinctive and implies an affinity to a major deep lithospheric source of similar age documented

in the Musgrave Province and could indicate a regional underplate of this age. These data indicate that the major suture between

the North and West Australian Cratons lies to the east of the Rudall Province (present-day coordinates).

KEYWORDS: continental accretion, crustal evolution, earth crust, hafnium isotopes, lutetium isotopes, oxygen isotopes,

radiometric dating, structural evolution, zircon, zircon dating

1 GEMOC, Department of Earth & Planetary Sciences, Macquarie

University, Sydney NSW 2109

2 John De Laeter Centre for Isotope Research, GPO Box U1987, Perth

WA 6845

IntroductionPrecambrian Australia comprises three main cratonic entities — the North, South, and West Australian Cratons — each of which was assembled and stabilized during the Paleoproterozoic. The West Australian Craton, which includes the Pilbara and Yilgarn Cratons and a wedge of exotic Archean to Paleoproterozoic continental crust known as the Glenburgh Terrane (Johnson et al., 2011a, 2012), was assembled along the Capricorn Orogen during two separate and distinct tectonic events. First, the Pilbara Craton and Glenburgh Terrane were sutured during the

2.2 – 2.1 Ga Ophthalmian Orogeny, and second, this combined cratonic block collided with the Yilgarn Craton during the c. 1.9 Ga Glenburgh Orogeny (Johnson et al., 2012). Subsequent tectono-magmatic events include the 1820–1770 Ma Capricorn Orogeny and the 1800–1765 Ma Yapungku Orogeny; the latter recorded within the Rudall Province of the Paterson Orogen along the eastern margin of the West Australian Craton (all directions refer to present-day coordinates). In the Rudall Province, deformation, metamorphism, and magmatism during the Yapungku Orogeny have been interpreted as a response to either accretional events that sutured exotic terranes to the craton margin (Bagas, 2004), or to the collision and amalgamation of the North and West Australian Cratons (Bagas and Smithies, 1997; Tyler, 2000; Li et al., 2008). Deformation and magmatism associated with the Capricorn Orogeny is interpreted as an intraplate response to these far-field plate-margin events (Sheppard et al.,

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2010a; Johnson et al., 2012). Understanding the tectonic setting of the Rudall Province is important because this province may record the collision between the North and West Australian Cratons and preserve a major crustal suture related to the Proterozoic assembly of Australia. Furthermore, within the region, a range of Neoproterozoic mineral systems exist, including Zn–Pb (Warrabarty; Smith, 1996), Cu (Nifty; Huston et al., 2007), U (Kintyre; Cross et al., 2011) and Au–Cu (Telfer; Maidment et al., 2008; 2010). The isotopic signature of units characterized in this report may be of significance for constraining the influence and role of crystalline basement on these younger mineralizing systems.

This report uses time-constrained Lu–Hf isotope analyses to evaluate the tectonic and crustal evolution of the Rudall Province, including:

1. whether the 1800–1765 Ma Yapungku Orogeny records the collision between the North and West Australian Cratons, or the assembly of exotic lithotectonic units to the West Australian Craton margin during accretionary orogenesis

2. whether terranes within the Rudall Province are (para)autochthonous and related to the thickening of a Proterozoic margin of the Pilbara Craton

or, alternatively,

3. whether terranes within the Rudall Province are exotic entities that:

a. formed part of the opposing North Australian Craton margin, being juxtaposed with the West Australian Craton during collisional orogenesis

or

b. have an entirely exotic source (e.g. part of the northern Gawler and Musgrave regions; (Cassidy et al., 2006), having been accreted to the West Australian Craton margin during accretionary or collisional orogenesis.

Geological setting of the

Rudall Province The ~2000 km long Paterson/Petermann Orogens of Western Australia extend along the eastern margin of the Archean Pilbara Craton, beneath younger sedimentary rocks, and into Central Australia (Fig. 1). The orogen includes Paleoproterozoic to Mesoproterozoic metasedimentary and igneous rocks of the Rudall and Musgrave Provinces, and Neoproterozoic to Paleozoic sedimentary rocks of the Centralian Superbasin (Myers and Hocking, 1988; Williams and Myers, 1990; Clarke, 1991; Bagas and Lubieniecki, 2000; Bagas et al., 2001; Haines et al., 2001; Bagas, 2004; Cawood and Korsch, 2008; Smithies et al., 2011; Reading et al., 2012). The Rudall and Musgrave Provinces are separated by younger sedimentary rocks of the Yeneena, northwest Officer, and Canning Basins, but appear to be connected via a

pronounced gravity high, known as the Anketell Regional Gravity Ridge (GSWA, 2012). Metasedimentary and igneous rocks within the two provinces were deformed and metamorphosed at medium to high metamorphic grades during the Proterozoic. However, the timing of tectono-magmatic events in the two regions is distinctly different, with events in the Rudall Province dominated by the 1800–1765 Ma Yapungku Orogeny (Bagas, 2004), and those in the Musgrave Province by the 1345–1293 Ma Mount West Orogeny, the 1220–1150 Ma Musgrave Orogeny, and the 1085–1040 Ma Giles Event (Smithies et al., 2011). However, both provinces (including parts of the Centralian Superbasin), were reworked at low to medium metamorphic grades during the c. 550 Ma Paterson/Petermann Orogeny, implying that juxtaposition of the Musgrave and the Rudall regions may have occurred during latest Neoproterozoic to Cambrian time (Williams and Myers, 1990).

The Rudall Province is divided into three major lithotectonic elements: the Talbot, Connaughton, and Tabletop Terranes (Hickman et al., 1994; Hickman and Bagas, 1995, 1999a; Bagas and Smithies, 1997; Fig. 2). The Talbot and Connaughton Terranes contain Paleoproterozoic intrusive rocks that formed during the Yapungku Orogeny, whereas the Tabletop Terrane consists of younger Mesoproterozoic granites. The three terranes are bounded by major faults that have been considered a response to terrane juxtaposition during the Yapungku Orogeny, or the c. 650 Ma Miles Orogeny, or both (Bagas and Smithies, 1997; Bagas, 2004).

The Talbot Terrane

The Talbot Terrane occupies the western parts of the Rudall Province (Fig. 2), and consists of multiply deformed and metamorphosed supracrustal and felsic intrusive rocks (Bagas and Smithies, 1997; Hickman and Bagas, 1999b, 1999a). The depositional setting of the siliciclastic rocks has been interpreted as a deltaic to moderately deep-water marine basin on the southeastern margin of the Pilbara Craton (Hickman et al., 1994).

Basement to the supracrustal rocks is not exposed, although a syenogranite gneiss from the Sundowner drillhole was interpreted to have crystallized at c. 2015 Ma (GSWA 104932; Nelson, 1995a). However, it is possible that the granitic protolith to the gneiss is much younger, and contains only inherited zircons. Major zircon age components, at 2715–2577, 2010, and 1960 Ma, are also present in this gneiss (Nelson, 1995a).

The metasedimentary rocks of the Talbot Terrane are divided into a western association of quartzite, amphibolite, serpentinite, and banded iron-formation, and an extensive eastern association containing nearly 5 km of siliciclastic sedimentary rocks. The eastern association consists of quartz-feldspar-mica paragneisses of the Larry Formation, conformably overlain by a succession of quartzite and minor mica schist known as the Fingoon Quartzite (Hickman et al., 1994; Bagas and Smithies, 1998). Quartz-muscovite schist, iron-rich graphitic pelitic schist, banded iron-formation, and chert of the

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GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

3

CLK88 27.03.13

OfficerBasin

0

1000

2000

3000

4000

Phanerozoic

Neoproterozoic

Mesoproterozoic

Palaeoproterozoic

Archean

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Age

(Ma)

115° 120°

20°

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YILGARN CRATON

Edmund Basin

Collier

Basin

Ashburton

Basin

Fortescue, Hamersley, and

TureeCreek Basins

Canning

Basin

Carnarvon

Basin

Rudall

Province

Southern

Cross

Narryer Terrane

Murchison Domain

Domain

East PilbaraTerrane

200 km

PATERSON O

ROGEN

CAPRIC

ORN

OROGEN

Eastern GoldfieldsSuperterane

PILBARA CRATON

AruntaMusgraves

Gascoyne

Province

LRF

CG

GT

Tarcunyah Group

Throssell Group &Lamil Group undivided

Tabletop Terrane

Tabletop Terrane

Talbot Terrane

Talbot Terrane

Connaughton Terrane

Pate

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rogen

Rudall P

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CLK80 27.03.13

23°

Fault Zone

Camel–Tabletop

McKay

Fault

123°122°

Late graniticrocks

Fault

Thrust

Normal fault

CANNINGBASIN

20 km

Southwest Thrust

Permian

Connaughton

Terrane

Figure 1. Simplified geological map indicating the location of the Rudall Province relative to other Proterozoic

orogens and Archean cratons in Western Australia (modified after Sheppard et al., 2010a). Red dashed

line indicates the approximate coverage of an extensive basin system during the 1820–1770 Ma Capricorn

Orogeny. Inset map (top right) shows the location of the main map as a red rectangle and the WAC (West

Australian Craton) in the context of other tectonic entities. Abbreviations used in figure: CG — Capricorn

Group, GC — Gawler Craton, GT — Glenburgh Terrane, KC — Kimberley Craton, LRF — Lyons River Fault,

NAC — North Australian Craton, PC — Pilbara Craton, SAC — South Australian Craton, YC — Yilgarn Craton,

WAC — West Australian Craton.

Figure 2. Simplified geological map of the Rudall Province,

indicating the main geological features and the

distribution of terranes (modified after Bagas and

Smithies, 1997; Smithies and Bagas, 1997).

Yandagooge Formation rest conformably on the Fingoon Quartzite. The Yandagooge Formation is overlain by banded paragneiss and minor amphibole-chlorite schist of the Butler Creek Formation, and quartzite and quartz-feldspar-mica gneiss of the Poynton Formation. Detrital zircon age data for the Fingoon Quartzite indicate a unimodal zircon age component at 1791 ± 10 Ma (Nelson, 1995e), which also provides a maximum depositional age for the sedimentary protolith to the quartzite and for the lowermost part of the eastern association.

Based on the presence of western association xenoliths within strongly deformed orthogneisses with c. 2015 and c. 1972 Ma zircon age components, the western association has generally been regarded as considerably older than the eastern association (Bagas, 2004). However, it is possible that the protoliths to the orthogneisses are much younger, containing only inherited zircons, and thus the two sequences may be of comparable age (Neumann and Fraser, 2007).

Metasedimentary rocks in both the eastern and western associations of the Talbot Terrane have been intruded by voluminous granites of the 1800–1765 Ma Kalkan Supersuite (Budd et al., 2002). These granitic rocks are characterized by high-K, metaluminous, calc-alkaline chemistry, with large K-feldspar phenocrysts and

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Sr depleted, Y-undepleted trace-element patterns typical of many Australian Proterozoic granite suites (Wyborn, 2001). These granites have crystallization ages between c. 1800 and c. 1760 Ma (Nelson, 1995i, 1995k), which provide a younger limit for deposition of the protoliths to both metasedimentary associations in the Rudall Province. Compressional shear zones within the Talbot Terrane contain enclaves of deformed ultramafic and mafic rocks, interpreted to represent slivers of dismembered ophiolite (Carr, 1989).

The Talbot Terrane also records minor magmatic episodes during the Mesoproterozoic, including a 1453 ± 10 Ma monzogranite that crosscuts fabrics associated with the Yapungku Orogeny (Nelson, 1996b) and a 1291 ± 10 Ma pegmatite close to the Camel–Tabletop Fault (Nelson, 1995b).

The Connaughton Terrane

The Connaughton Terrane (Fig. 2), within the southeastern part of the province, comprises a series of poorly dated metavolcanic and metasedimentary rocks. This terrane contains a significantly higher proportion of amphibolite than the Talbot Terrane (Bagas and Smithies, 1998). The amphibolite is interlayered with banded iron-formation, quartzite, pelitic metasedimentary rocks, chert, and ultramafic rocks (Hickman et al., 1994). In a situation similar to the Talbot Terrane, basement rocks are not exposed. Importantly, all rocks within the Connaughton Terrane were metamorphosed at upper amphibolite to granulite facies conditions (peak 800°C, 12 kbar) during the Yapungku Orogeny (Smithies and Bagas, 1997).

Preliminary U–Pb geochronology of detrital zircons in quartzite provides a maximum depositional age of c. 2300 Ma, and a provenance signature (age spectrum) significantly different from that of the Fingoon Quartzite of the Talbot Terrane (Maidment et al., in prep. reported in Neumann and Fraser, 2007). Insufficient geochronological data from metasedimentary rocks from both the Talbot and Connaughton Terranes makes it difficult to determine if they had different sedimentary source regions or depositional ages, or both.

Granitic rocks of the 1800–1765 Ma Kalkan Supersuite (Nelson, 1995m; 1996d) form a major component of the Connaughton Terrane. This terrane may also have been subject to minor Mesoproterozoic magmatic activity. A garnet-bearing gneiss, south of Harbutt Range in the Connaughton Terrane, yielded zircon age components at c. 1800, 1672, and 1222 Ma (Nelson, 1996c), with the youngest group interpreted to date crystallization of the felsic intrusive protolith. However, the c. 1222 Ma date was obtained from zircon rims that have elevated thorium and common Pb contents and may have grown during metamorphism.

The Tabletop Terrane

The Tabletop Terrane (Fig. 2) is dominated by weakly deformed and metamorphosed felsic and mafic igneous

rocks of the Krackatinny Suite, with minor quartzite, mafic and ultramafic schists, amphibolite, and banded iron-formation (Bagas et al., 1999). Unpublished geochronology reported in Neumann and Fraser (2007) indicates that most of the felsic and mafic intrusive rocks of the Krackatinny Suite away from the Camel–Tabletop Fault were emplaced between c. 1590 and c. 1550 Ma. Other felsic intrusive rocks in this terrane have been dated at 1476 ± 10 Ma (unpublished result referred to in Bagas, 2004) and 1310 ± 4 Ma (Nelson, 1996e).

Available geochronology suggests that the magmatic history of the Tabletop Terrane is distinctly different from that in the Talbot and Connaughton Terranes, which share a common structural, magmatic, and deformational history (Bagas, 2004). The Tabletop Terrane does not appear to contain evidence for 1800–1760 Ma magmatism, whereas the Talbot and Connaughton Terranes lack 1590–1550 Ma magmatism, possibly implying that the Camel–Tabletop Fault (Fig. 2), which separates these terranes, is a major crustal boundary (Hickman et al., 1994; Bagas and Lubieniecki, 2000).

Structural evolution

The Talbot and Connaughton Terranes share a similar structural history, including two high-grade tectono-magmatic events during the Paleoproterozoic Yapungku Orogeny (Clarke, 1991; Hickman et al., 1994; Bagas and Smithies, 1997; Hickman and Bagas, 1999b; Bagas, 2004). The timing and duration of the Yapungku Orogeny is defined by the age of the oldest and youngest granitic components at c. 1800 and c. 1760 Ma, respectively (Smithies and Bagas, 1997; Bagas, 2004). In the Talbot Terrane, both tectonothermal events occurred prior to c. 1778 Ma, as constrained by the age of undeformed aplite dykes (Nelson, 1995j) that crosscut the major tectonic fabrics. The main phase of deformation and metamorphism in the Connaughton Terrane is not well established, but has been interpreted to be coeval with lower-pressure metamorphism (M2) in the Talbot Terrane (Bagas and Smithies, 1997; Bagas, 2004).

The first deformation event (D1) is preserved as bedding-parallel fabrics in the Talbot Terrane (Clarke, 1991; Bagas and Smithies, 1998). Associated metamorphic features indicate low-pressure metamorphism at amphibolite facies. The timing of D1 in the Talbot Terrane is constrained to be older than 1802 ± 14 Ma, the age of a K-feldspar porphyritic granite that crosscuts D1 fabrics (Nelson, 1995i). Evidence for D1 and M1 in the Connaughton Terrane is preserved only as inclusion trails of epidote, titanite, and amphibole within garnet porphyroblasts (Smithies and Bagas, 1997).

The D2 event produced north–south isoclinal folding, faulting, and crustal thickening in the Talbot and Connaughton Terranes, and was coeval with thrusting and the emplacement of granitic, mafic, and ultramafic (peridotite–dunite) rocks in the Talbot Terrane (Hickman and Bagas, 1995, 1999b). Geochronology of syn-D2 granitic rocks in the Talbot Terrane indicates that the D2 event occurred between c. 1801 and c. 1765 Ma

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GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

5

(Nelson, 1995i, 1995k, 1995c; Bagas, 2004). In the Connaughton Terrane, peak regional M2 metamorphism was synchronous with, but outlasted, D2 deformation in the Talbot Terrane (Hickman et al., 1994). Pelitic schists within the Talbot Terrane contain peak M2 mineral assemblages of kyanite + garnet + staurolite, which are indicative of metamorphism in the mid-amphibolite facies (Smithies and Bagas, 1997; Bagas, 2004). In the Connaughton Terrane, peak M2 metamorphism is characterized by the presence of amphibolites and mafic granulites that were metamorphosed at high pressures (≤ 1200 MPa) close to the amphibolite–granulite facies transition, indicating that crust from depths of up to 40 km is now exposed at the surface (Smithies and Bagas, 1997). These conditions also imply that the deformation and metamorphism assigned to D2/M2 were in response to crustal thickening in which the Connaughton Terrane was thrust westwards over the Talbot Terrane (Bagas, 2004).

The Rudall Province has also been subject to several Neoproterozoic deformation events (Bagas, 2004). Northwesterly trending folds and north-northeasterly trending faults ascribed to D3/4 were developed during the c. 650 Ma Miles Orogeny (Bagas and Smithies, 1998; Hickman and Bagas, 1999b). Lower-greenschist facies metamorphism prevailed during northeasterly to southwesterly oriented shortening associated with the D4 event. An enigmatic D5 event is believed to be a response to northwest-directed shortening against the Pilbara Craton. The late Neoproterozoic (550 Ma) Paterson Orogeny, ascribed to D6, was responsible for easterly trending transpressional folds (Bagas, 2004).

Lu–Hf and oxygen isotopes,

and reinterpreted SHRIMP

U–Pb geochronologyThis section presents new Lu–Hf (Table 1) and oxygen isotope data (Table 2) for previously dated samples from the Rudall Province. The geochemical characteristics of many of these samples have previously been discussed in Wyborn (2001). We calculate concordia ages from the previously published SHRIMP U–Pb geochronology data for these rocks. Where the location of the mean U–Pb composition can be assumed to fall on the concordia curve (i.e. the zircons have not undergone modern or ancient radiogenic-Pb loss), the ‘concordia age’ makes the optimum use of both 207Pb*/206Pb* and 238U/206Pb* ratios (Ludwig, 1998)1. This approach generally yields a more precise mean age than can be obtained using either ratio alone, and also yields an objective and quantitative measure of concordance. In cases where the U–Pb data do not fall on concordia, it is likely that the zircons have undergone modern or ancient radiogenic-Pb loss. Where the distribution of U–Pb data are consistent with mainly geologically-recent loss of radiogenic Pb, we calculate the weighted mean 207Pb*/206Pb* date. Weighted mean and concordia ages are reported below with 95% confidence intervals. A summary of the U–Pb geochronology is presented in Table 3.

Analytical methodology

Lu–Hf isotopes

Hafnium isotope analyses were conducted on previously dated zircons using a New Wave/Merchantek LUV213 laser-ablation microprobe attached to a Nu Plasma multi-collector inductively coupled plasma mass spectrometer (LA-MC-ICPMS). The analyses employed a beam diameter of c. 40 μm and a 5 Hz repetition rate, and energies of 0.6 – 1.3 mJ per pulse, which resulted in ablation pits typically 40–60 μm deep during a 30–120 second analysis. Total Hf signals were between 1 x 10-11 and 6 x 10-11 amperes. The ablated sample material was transported from the laser cell to the ICPMS torch by a helium carrier gas. Interference of 176Lu on 176Hf was corrected by measurement of interference-free 175Lu, and using the invariant 176Lu/175Lu correction factor of 0.02669 (Debievre and Taylor, 1993). The measurement of accurate 176Hf/177Hf ratios in zircon requires correction of the isobaric interferences of 176Lu and 176Yb on 176Hf. The interference of 176Yb on 176Hf was corrected by measuring the interference-free 172Yb isotope and using the 176Yb/172Yb ratio to calculate the intensity of 176Yb. The appropriate value of 176Yb/172Yb (0.5865) was determined by successively doping a JMC475 Hf standard (100 ppb solution) with various amounts of Yb, and determining the value of 176Yb/172Yb required to yield the value of 176Hf/177Hf in the undoped solution.

Twenty-three zircons from the Mud Tank carbonatite locality were analysed, together with the samples, as a measure of the accuracy of the results. Most of the data and the mean 176Hf/177Hf value (0.282530 ± 0.000022; n = 23) are within two standard deviations (SD) of the recommended value (0.282522 ± 0.000042 (2 ; Griffin, 2007). Temora-2 zircon was run as an independent check on the accuracy of the Yb correction. Temora zircon has an average 176Yb/177Hf ratio of 0.037, which is similar to the average 176Yb/177Hf ratio of Rudall zircon of 0.039. The average 176Hf/177Hf ratio for Temora-2 is 0.282683 ± 0.000022 (1 ), which is consistent with the published value for the Temora-2 standard (0.282686 ± 8, solution ICPMS, Woodhead and Hergt, 2005; 0.282687 ± 24, LA-ICPMS, Hawkesworth and Kemp, 2006).

Calculation of initial 176Hf/177Hf (e.g. 176Hf/177Hfi) is based on the 176Lu decay constant of Scherer et al. (2001; 1.867 x 10-11 yr-1). Since 176Hf/177Hf departures from the CHUR evolution line are very small, the epsilon notation is used whereby one epsilon unit represents a one part per 10 000 deviation from the CHUR composition. Hf values employ the present-day chondritic measurement of Blichert-Toft and Albarède (1997; 0.282772). Calculation of model ages (TDM) is based on a depleted-mantle source with 176Hf/177Hfi = 0.279718 at 4.56 Ga and 176Lu/177Hf = 0.0384 (Griffin et al., 2004).

Measured isotope compositions are referred to model bulk-Earth Hf reservoirs, including Depleted Mantle (DM; Griffin et al., 2000, 2004) and Chondritic Uniform Reservoir (CHUR; Blichert-Toft and Albarède 1997).

1 Pb* refers to radiogenic Pb produced by the in-situ decay of uranium.

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Kirkland et al.

6

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

112160-1

.11872

0.2

81396

0.0

00

00

90

.00

04

92

0.0

14

04

20

.28

13

79

-7.6

0.3

22.5

63.0

2C

onnaughto

n

112160-2

.11831

0.2

81358

0.0

00

015

0.0

00

69

90

.02

05

83

0.2

813

34

-10.1

0.5

32.6

33.1

5C

onnaughto

n

112160-3

.11873

0.2

81438

0.0

00

018

0.0

012

86

0.0

36

35

00

.28

13

92

-7.1

0.6

32.5

62.9

9C

onnaughto

n

112160-4

.11764

0.2

81370

0.0

00

017

0.0

00

95

50

.02

874

90

.28

13

38

-11.

50.6

02.6

33.1

9C

onnaughto

n

112160-5

.11684

0.2

81406

0.0

00

04

90

.0016

72

0.0

50

07

70

.28

13

53

-12.8

1.72

2.6

33.2

0C

onnaughto

n

112160-6

.11771

0.2

81369

0.0

00

014

0.0

02

75

90

.09

88

71

0.2

812

76

-13.5

0.4

92.7

63.3

2C

onnaughto

n

112160-7

.11772

0.2

81338

0.0

00

011

0.0

012

55

0.0

36

49

40

.28

12

96

-12.8

0.3

92.6

93.2

7C

onnaughto

n

112160-8

.11629

0.2

81436

0.0

00

015

0.0

00

80

20

.02

35

92

0.2

814

11-1

1.9

0.5

32.5

33.1

1C

onnaughto

n

112160-9

.11274

0.2

81369

0.0

00

013

0.0

014

63

0.0

55

740

0.2

813

34

-22.7

0.4

62.6

63.5

0C

onnaughto

n

112160-9

.211

44

0.2

81410

0.0

00

011

0.0

00

747

0.0

29

04

10

.28

13

94

-23.5

0.3

92.5

63.4

5C

onnaughto

n

112160-1

0.1

1820

0.2

81504

0.0

00

02

00

.00

36

59

0.1

48

09

20

.28

13

78

-8.8

0.7

02.6

33.0

6C

onnaughto

n

112160-1

1.1

1677

0.2

81287

0.0

00

017

0.0

012

20

0.0

36

13

90

.28

12

48

-16.6

0.6

02.7

63.4

4C

onnaughto

n

113002-0

1.1

1769

0.2

81531

0.0

00

00

90

.00

09

01

0.0

26

66

10

.28

15

01

-5.6

0.3

12.4

02.8

2C

onnaughto

n

113002-0

2.1

1787

0.2

81531

0.0

00

010

0.0

00

85

90

.02

49

97

0.2

815

02

-5.1

0.3

52.4

02.8

0C

onnaughto

n

113002-0

3.1

1770

0.2

81519

0.0

00

00

80

.00

06

60

0.0

19

63

60

.28

14

97

-5.7

0.2

92.4

02.8

3C

onnaughto

n

113002-0

5.1

1762

0.2

81539

0.0

00

00

90

.00

08

27

0.0

25

36

10

.28

15

11-5

.40.3

02.3

92.8

0C

onnaughto

n

113002-0

6.1

1780

0.2

81536

0.0

00

00

70

.00

04

36

0.0

12

56

80

.28

15

21

-4.6

0.2

52.3

72.7

6C

onnaughto

n

113002-0

8.1

174

20.2

81553

0.0

00

00

90

.00

07

08

0.0

22

819

0.2

815

30

-5.2

0.3

22.3

62.7

7C

onnaughto

n

113002-0

9.1

1773

0.2

81546

0.0

00

00

90

.00

05

59

0.0

17

819

0.2

815

27

-4.6

0.3

02.3

62.7

6C

onnaughto

n

113002-1

0.1

1772

0.2

81572

0.0

00

00

80

.00

08

72

0.0

26

52

00

.28

15

43

-4.0

0.2

72.3

52.7

2C

onnaughto

n

113002-1

2.1

1777

0.2

81583

0.0

00

00

70

.00

06

67

0.0

20

67

00

.28

15

61

-3.3

0.2

62.3

22.6

8C

onnaughto

n

113002-1

4.1

1760

0.2

81541

0.0

00

00

90

.00

076

30

.02

44

64

0.2

815

16

-5.3

0.3

32.3

82.7

9C

onnaughto

n

113035-0

6.1

1765

0.2

81580

0.0

00

011

0.0

00

47

80

.015

54

70

.28

15

64

-3.4

0.3

92.3

12.6

8C

onnaughto

n

113035-0

7.1

1763

0.2

81696

0.0

00

013

0.0

00

78

00

.02

28

21

0.2

816

70

0.3

0.4

62.1

72.4

4C

onnaughto

n

113035-0

8.1

1765

0.2

81642

0.0

00

014

0.0

00

79

20

.02

43

60

0.2

816

16

-1.6

0.4

92.2

42.5

6C

onnaughto

n

113035-0

9.1

1788

0.2

81618

0.0

00

015

0.0

00

58

80

.019

98

20

.28

15

98

-1.7

0.5

32.2

72.5

9C

onnaughto

n

113035-1

0.1

1785

0.2

81631

0.0

00

017

0.0

00

78

70

.02

83

04

0.2

816

04

-1.6

0.6

02.2

62.5

7C

onnaughto

n

113035-1

1.1

1756

0.2

81623

0.0

00

00

90

.00

06

50

0.0

19

90

50

.28

16

01

-2.3

0.3

22.2

62.6

0C

onnaughto

n

113035-1

2.1

1791

0.2

81608

0.0

00

00

90

.00

08

02

0.0

24

70

60

.28

15

81

-2.3

0.3

22.2

92.6

2C

onnaughto

n

113035-1

3.1

1771

0.2

81648

0.0

00

011

0.0

00

99

30

.03

49

88

0.2

816

15

-1.5

0.3

92.2

52.5

6C

onnaughto

n

118914-0

1.1

1265

0.2

81903

0.0

00

014

0.0

03

001

0.0

976

56

0.2

818

31

-5.3

0.4

92.0

02.4

1Table

top

118914-0

2.1

1495

0.2

81729

0.0

00

013

0.0

03

62

30

.14

10

91

0.2

816

27

-7.3

0.4

62.3

02.7

2Table

top

Tabl

e 1.

L

u–H

f iso

topi

c m

easu

rem

ent o

f zir

cons

from

the

Rud

all P

rovi

nce

Page 12: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

7

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

118914-0

3.1

1320

0.2

81803

0.0

00

011

0.0

02

519

0.0

85

45

80

.28

174

0-7

.20.3

92.1

22.5

7Table

top

118914-0

4.1

1315

0.2

81802

0.0

00

011

0.0

02

42

70

.08

82

81

0.2

8174

2-7

.30.3

92.1

22.5

7Table

top

118914-0

5.1

1312

0.2

81791

0.0

00

02

10

.00

218

40

.07

37

25

0.2

817

37

-7.5

0.7

42.1

22.5

9Table

top

118914-0

6.1

1324

0.2

81771

0.0

00

017

0.0

02

29

50

.076

76

40

.28

17

14

-8.1

0.6

02.1

52.6

3Table

top

118914-0

7.1

1312

0.2

81826

0.0

00

014

0.0

03

05

70

.1016

81

0.2

817

50

-7.1

0.4

92.1

22.5

6Table

top

118914-0

8.1

1194

0.2

81766

0.0

00

013

0.0

03

03

40

.1018

63

0.2

816

98

-11.

60.4

62.2

02.7

5Table

top

118914-0

9.1

1241

0.2

81798

0.0

00

016

0.0

03

22

90

.09

30

79

0.2

817

22

-9.7

0.5

62.1

72.6

6Table

top

118914-1

0.1

1298

0.2

81780

0.0

00

011

0.0

02

83

50

.10

08

51

0.2

817

11-8

.80.3

92.1

72.6

5Table

top

118914-1

1.1

1297

0.2

8174

20

.00

0018

0.0

04

09

70

.15

78

83

0.2

816

42

-11.

30.6

32.3

12.8

1Table

top

118914-1

2.1

1287

0.2

81776

0.0

00

03

20

.00

22

47

0.0

815

15

0.2

817

21

-8.7

1.12

2.1

42.6

4Table

top

118914-1

5.1

1308

0.2

81765

0.0

00

00

80

.00

27

26

0.1

00

72

00

.28

16

98

-9.0

0.2

82.1

92.6

8Table

top

118914-1

6.1

1311

0.2

81798

0.0

00

02

00

.00

29

38

0.1

13

40

90

.28

17

25

-8.0

0.7

02.1

52.6

1Table

top

118914-1

7.1

1311

0.2

81764

0.0

00

010

0.0

02

95

80

.1019

49

0.2

816

91

-9.2

0.3

42.2

02.6

9Table

top

118914-1

9.1

1311

0.2

81764

0.0

00

00

50

.00

24

45

0.0

82

73

30

.28

17

03

-8.8

0.1

92.1

72.6

6Table

top

112102-4

.11475

0.2

82035

0.0

00

014

0.0

02

52

00

.09

04

35

0.2

819

65

4.2

0.4

91.

79

1.97

Talb

ot

112102-5

.11453

0.2

82033

0.0

00

013

0.0

02

00

90

.06

58

85

0.2

819

78

4.2

0.4

61.

76

1.95

Talb

ot

112102-6

.11452

0.2

82040

0.0

00

013

0.0

02

47

50

.09

33

36

0.2

819

72

4.0

0.4

61.

78

1.96

Talb

ot

112102-7

.11435

0.2

82031

0.0

00

02

80

.00

22

43

0.0

79

45

00

.28

19

70

3.5

0.9

81.

78

1.98

Talb

ot

112102-8

.11414

0.2

82013

0.0

00

011

0.0

02

15

70

.07

18

07

0.2

819

55

2.5

0.3

91.

80

2.0

3Talb

ot

112102-9

.11426

0.2

82054

0.0

00

014

0.0

02

92

20

.09

50

44

0.2

819

75

3.5

0.4

91.

78

1.97

Talb

ot

112102-1

0.1

1460

0.2

82068

0.0

00

02

50

.00

22

70

0.0

84

06

20

.28

20

05

5.3

0.8

81.

73

1.88

Talb

ot

112102-1

1.1

1453

0.2

82094

0.0

00

012

0.0

02

73

00

.10

05

53

0.2

82

019

5.6

0.4

21.

71

1.86

Talb

ot

112101-

01.

21755

0.2

81442

0.0

00

00

80

.00

09

68

0.0

37

09

40

.28

14

10

-9.1

0.2

72.5

33.0

3Talb

ot

112101-

03.1

1810

0.2

81463

0.0

00

00

50

.00

06

98

0.0

25

32

20

.28

14

39

-6.9

0.1

92.4

82.9

3Talb

ot

112101-

04.1

1814

0.2

81472

0.0

00

00

80

.00

08

18

0.0

312

65

0.2

814

44

-6.6

0.2

72.4

82.9

2Talb

ot

112101-

05.1

1796

0.2

81575

0.0

00

013

0.0

013

41

0.0

513

04

0.2

815

29

-4.0

0.4

62.3

72.7

4Talb

ot

112101-

06.1

1784

0.2

81513

0.0

00

012

0.0

017

88

0.0

75

70

60

.28

14

53

-7.0

0.4

22.4

92.9

2Talb

ot

112101-

07.

11790

0.2

81572

0.0

00

013

0.0

00

76

60

.02

65

06

0.2

815

46

-3.5

0.4

62.3

42.7

0Talb

ot

112101-

08.1

1799

0.2

81598

0.0

00

015

0.0

010

44

0.0

42

03

70

.28

15

62

-2.7

0.5

32.3

22.6

6Talb

ot

112101-

16.1

1781

0.2

81591

0.0

00

012

0.0

010

56

0.0

43

86

40

.28

15

55

-3.4

0.4

22.3

32.6

9Talb

ot

112101-

17.

11777

0.2

81597

0.0

00

010

0.0

00

89

10

.03

33

06

0.2

815

67

-3.1

0.3

42.3

12.6

6Talb

ot

Tabl

e 1.

co

ntin

ued

Page 13: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

Kirkland et al.

8

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

104980-0

2.1

1717

0.2

81569

0.0

00

02

30

.0018

25

0.0

919

36

0.2

815

10

-6.5

0.8

12.4

12.8

3Talb

ot

104980-0

3.1

1804

0.2

81466

0.0

00

015

0.0

014

07

0.0

65

62

20

.28

14

18

-7.7

0.5

32.5

32.9

8Talb

ot

104980-0

5.1

1800

0.2

81467

0.0

00

02

10

.0010

61

0.0

49

39

90

.28

14

31

-7.4

0.7

42.5

02.9

5Talb

ot

104980-0

6.1

1801

0.2

81451

0.0

00

00

80

.0011

96

0.0

516

47

0.2

814

10

-8.1

0.2

62.5

33.0

0Talb

ot

104980-0

7.1

1795

0.2

81448

0.0

00

00

60

.0013

12

0.0

58

22

40

.28

14

03

-8.5

0.2

12.5

43.0

2Talb

ot

104980-0

8.1

1809

0.2

81453

0.0

00

018

0.0

012

01

0.0

56

86

00

.28

14

12

-7.8

0.6

32.5

32.9

9Talb

ot

104980-0

9.1

1799

0.2

81457

0.0

00

010

0.0

013

02

0.0

618

24

0.2

814

13

-8.0

0.3

42.5

33.0

0Talb

ot

104980-1

2.1

1794

0.2

81442

0.0

00

00

90

.0012

71

0.0

64

20

70

.28

13

99

-8.7

0.3

32.5

53.0

3Talb

ot

104980-1

3.1

1786

0.2

81444

0.0

00

00

80

.0010

45

0.0

49

18

00

.28

14

09

-8.5

0.2

62.5

33.0

1Talb

ot

112341-

02.1

1772

0.2

81564

0.0

00

02

70

.00

67

93

0.2

576

77

0.2

813

36

-11.

40.9

52.7

93.1

9Talb

ot

112341-

03.1

1806

0.2

81572

0.0

00

00

60

.0011

41

0.0

45

45

50

.28

15

33

-3.6

0.2

22.3

62.7

2Talb

ot

112341-

04.1

1797

0.2

81536

0.0

00

012

0.0

011

43

0.0

56

48

30

.28

14

97

-5.1

0.4

22.4

12.8

1Talb

ot

112341-

05.1

1788

0.2

81518

0.0

00

011

0.0

015

34

0.0

75

16

80

.28

14

66

-6.4

0.3

92.4

62.8

8Talb

ot

112341-

06.1

1760

0.2

81502

0.0

00

00

90

.00

07

88

0.0

376

69

0.2

814

76

-6.7

0.3

32.4

42.8

8Talb

ot

112341-

07.

11727

0.2

81515

0.0

00

011

0.0

013

99

0.0

70

912

0.2

814

69

-7.7

0.3

92.4

62.9

2Talb

ot

112341-

09.1

1612

0.2

81572

0.0

00

00

90

.00

08

77

0.0

36

72

40

.28

15

45

-7.6

0.3

02.3

52.8

2Talb

ot

112341-

10.1

1765

0.2

81490

0.0

00

00

90

.0010

27

0.0

43

101

0.2

814

56

-7.3

0.3

02.4

72.9

2Talb

ot

112341-

11.1

1703

0.2

81509

0.0

00

010

0.0

011

97

0.0

65

56

30

.28

14

70

-8.2

0.3

42.4

52.9

3Talb

ot

112341-

12.1

1786

0.2

81535

0.0

00

011

0.0

012

13

0.0

619

97

0.2

814

94

-5.5

0.3

92.4

22.8

2Talb

ot

112341-

13.1

1754

0.2

81524

0.0

00

011

0.0

011

52

0.0

43

213

0.2

814

86

-6.5

0.3

92.4

32.8

6Talb

ot

112341-

14.1

1739

0.2

81518

0.0

00

011

0.0

013

65

0.0

69

14

80

.28

14

73

-7.3

0.3

92.4

52.9

0Talb

ot

112341-

15.1

1717

0.2

81526

0.0

00

014

0.0

012

90

0.0

63

274

0.2

814

84

-7.4

0.4

92.4

32.8

9Talb

ot

111843-0

1.1

1778

0.2

81554

0.0

00

014

0.0

00

90

00

.02

62

60

0.2

815

24

-4.6

0.4

92.3

72.7

6Talb

ot

111843-0

1.2

1877

0.2

81488

0.0

00

010

0.0

00

89

10

.02

57

88

0.2

814

56

-4.7

0.3

52.4

62.8

5Talb

ot

111843-0

2.1

1790

0.2

81483

0.0

00

012

0.0

00

82

20

.02

42

79

0.2

814

55

-6.7

0.4

22.4

62.9

1Talb

ot

111843-0

3.1

2102

0.2

81309

0.0

00

016

0.0

00

58

70

.018

82

00

.28

12

86

-5.7

0.5

62.6

83.0

8Talb

ot

111843-0

4.1

1715

0.2

81477

0.0

00

00

90

.00

07

88

0.0

25

412

0.2

814

51

-8.6

0.3

12.4

72.9

6Talb

ot

111843-0

7.1

1756

0.2

81450

0.0

00

018

0.0

00

93

50

.02

84

99

0.2

814

19

-8.8

0.6

32.5

23.0

1Talb

ot

111843-0

7.2

1807

0.2

81498

0.0

00

015

0.0

010

65

0.0

35

54

60

.28

14

62

-6.1

0.5

32.4

62.8

8Talb

ot

111843-0

8.1

1723

0.2

81430

0.0

00

00

80

.0012

84

0.0

38

48

00

.28

13

88

-10.6

0.2

62.5

73.1

0Talb

ot

111843-0

9.1

1790

0.2

81354

0.0

00

010

0.0

013

73

0.0

46

59

80

.28

13

07

-12.0

0.3

52.6

83.2

4Talb

ot

111843-1

0.1

1809

0.2

81459

0.0

00

016

0.0

011

51

0.0

35

119

0.2

814

20

-7.6

0.5

62.5

22.9

7Talb

ot

Tabl

e 1.

co

ntin

ued

Page 14: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

9

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

111843-1

0.2

1810

0.2

81475

0.0

00

00

90

.00

09

16

0.0

28

39

10

.28

14

44

-6.7

0.3

22.4

82.9

2Talb

ot

111843-1

1.1

1928

0.2

81253

0.0

00

00

80

.00

09

01

0.0

28

78

20

.28

12

20

-12.0

0.2

92.7

83.3

4Talb

ot

104989-0

1.1

1777

0.2

81589

0.0

00

013

0.0

016

18

0.0

52

24

50

.28

15

34

-4.2

0.4

62.3

72.7

4Talb

ot

104989-0

2.1

1791

0.2

81478

0.0

00

012

0.0

011

25

0.0

39

60

90

.28

14

40

-7.3

0.4

22.4

92.9

4Talb

ot

104989-0

3.1

1796

0.2

81495

0.0

00

011

0.0

00

95

70

.03

413

00

.28

14

62

-6.3

0.3

92.4

62.8

9Talb

ot

104989-0

4.1

1816

0.2

81284

0.0

00

013

0.0

00

30

60

.012

54

60

.28

12

73

-12.6

0.4

62.7

03.3

0Talb

ot

104989-0

5.1

1817

0.2

81488

0.0

00

00

90

.00

09

66

0.0

30

22

70

.28

14

55

-6.1

0.3

22.4

72.8

9Talb

ot

104989-0

6.1

1815

0.2

81587

0.0

00

013

0.0

015

50

0.0

49

10

20

.28

15

34

-3.4

0.4

62.3

72.7

1Talb

ot

104989-0

7.1

1791

0.2

81467

0.0

00

010

0.0

02

49

90

.09

89

45

0.2

813

82

-9.3

0.3

52.6

03.0

7Talb

ot

104989-0

8.1

1810

0.2

81504

0.0

00

015

0.0

010

58

0.0

33

601

0.2

814

68

-5.8

0.5

32.4

52.8

6Talb

ot

104989-0

9.1

1804

0.2

81499

0.0

00

013

0.0

016

76

0.0

60

60

60

.28

14

42

-6.9

0.4

62.5

02.9

3Talb

ot

104989-1

0.1

1777

0.2

81589

0.0

00

00

90

.00

08

84

0.0

28

60

60

.28

15

59

-3.3

0.3

12.3

22.6

8Talb

ot

104989-1

1.1

1791

0.2

81490

0.0

00

011

0.0

011

77

0.0

45

774

0.2

814

50

-6.9

0.3

92.4

82.9

2Talb

ot

104989-1

2.1

1786

0.2

81497

0.0

00

013

0.0

00

701

0.0

24

10

70

.28

14

73

-6.2

0.4

62.4

42.8

7Talb

ot

104989-1

3.1

1777

0.2

81489

0.0

00

00

70

.00

06

98

0.0

22

93

80

.28

14

65

-6.7

0.2

52.4

52.8

9Talb

ot

104989-1

4.1

1775

0.2

81469

0.0

00

011

0.0

02

715

0.1

07

96

40

.28

13

78

-9.8

0.3

92.6

13.0

9Talb

ot

104989-1

6.1

1955

0.2

81316

0.0

00

00

90

.00

076

40

.02

55

57

0.2

812

88

-8.9

0.3

02.6

93.1

7Talb

ot

104989-1

7.1

1805

0.2

81573

0.0

00

013

0.0

00

83

20

.02

60

43

0.2

815

45

-3.2

0.4

62.3

42.7

0Talb

ot

104989-1

8.1

1801

0.2

81517

0.0

00

011

0.0

00

72

40

.02

43

56

0.2

814

92

-5.2

0.3

92.4

12.8

2Talb

ot

104989-1

9.1

1761

0.2

81556

0.0

00

011

0.0

00

57

70

.018

48

30

.28

15

37

-4.5

0.3

92.3

52.7

4Talb

ot

111854-0

1.1

1794

0.2

81495

0.0

00

00

70

.0014

83

0.0

59

610

0.2

814

45

-7.0

0.2

62.4

92.9

3Talb

ot

111854-0

2.1

1785

0.2

81533

0.0

00

011

0.0

012

25

0.0

54

23

80

.28

14

92

-5.6

0.3

92.4

22.8

3Talb

ot

111854-0

4.1

1755

0.2

81504

0.0

00

02

70

.00

212

80

.09

12

38

0.2

814

33

-8.3

0.9

52.5

22.9

8Talb

ot

111854-0

5.1

2327

0.2

81402

0.0

00

010

0.0

010

28

0.0

45

93

80

.28

13

56

2.0

0.3

52.5

92.7

6Talb

ot

111854-0

6.1

1784

0.2

81538

0.0

00

00

90

.0014

33

0.0

617

32

0.2

814

90

-5.7

0.3

12.4

32.8

3Talb

ot

111854-0

8.1

174

60.2

81478

0.0

00

00

80

.0012

10

0.0

55

63

00

.28

14

38

-8.3

0.2

82.5

02.9

7Talb

ot

111854-0

9.1

174

90.2

81498

0.0

00

00

80

.001013

0.0

44

43

90

.28

14

64

-7.3

0.2

92.4

62.9

1Talb

ot

111854-1

1.1

1778

0.2

81452

0.0

00

012

0.0

00

65

10

.02

97

02

0.2

814

30

-7.9

0.4

22.4

92.9

7Talb

ot

111854-1

2.1

1792

0.2

81421

0.0

00

00

90

.0013

33

0.0

48

24

00

.28

13

76

-9.5

0.3

32.5

83.0

8Talb

ot

112310-0

1.1

1977

0.2

81544

0.0

00

00

50

.0015

36

0.0

44

43

20

.28

14

86

-1.4

0.1

92.4

32.7

1Talb

ot

112310-0

2.1

1811

0.2

81512

0.0

00

00

80

.00

07

54

0.0

215

41

0.2

814

86

-5.2

0.2

72.4

22.8

2Talb

ot

Tabl

e 1.

co

ntin

ued

Page 15: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

Kirkland et al.

10

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

112310-0

3.1

1963

0.2

81555

0.0

00

015

0.0

011

740

.03

22

89

0.2

815

11-0

.80.5

32.3

92.6

6Talb

ot

112310-0

4.1

1797

0.2

81481

0.0

00

014

0.0

014

73

0.0

43

45

50

.28

14

31

-7.4

0.4

92.5

12.9

6Talb

ot

112310-0

5.1

1816

0.2

81475

0.0

00

02

10

.00

09

77

0.0

27

34

20

.28

14

41

-6.6

0.7

42.4

82.9

2Talb

ot

112310-0

6.1

1972

0.2

81537

0.0

00

013

0.0

016

42

0.0

47

88

20

.28

14

75

-1.9

0.4

62.4

42.7

4Talb

ot

112310-0

7.1

1780

0.2

81419

0.0

00

02

00

.0010

23

0.0

28

09

90

.28

13

84

-9.5

0.7

02.5

63.0

7Talb

ot

112310-0

8.1

1974

0.2

81584

0.0

00

018

0.0

015

98

0.0

47

09

20

.28

15

24

-0.1

0.6

32.3

72.6

3Talb

ot

112310-0

9.1

1975

0.2

81504

0.0

00

018

0.0

018

00

0.0

48

29

10

.28

14

36

-3.2

0.6

32.5

02.8

2Talb

ot

112310-1

0.1

1975

0.2

81601

0.0

00

00

80

.0014

79

0.0

46

07

80

.28

15

45

0.7

0.2

72.3

42.5

8Talb

ot

112310-1

4.1

1932

0.2

81564

0.0

00

00

90

.0014

09

0.0

40

72

50

.28

15

12

-1.5

0.3

32.3

92.6

8Talb

ot

112310-1

6.1

1980

0.2

81569

0.0

00

00

90

.00

07

03

0.0

18

59

70

.28

15

43

0.7

0.3

02.3

42.5

8Talb

ot

112310-1

7.1

1958

0.2

81554

0.0

00

011

0.0

011

44

0.0

32

714

0.2

815

11-0

.90.3

92.3

92.6

7Talb

ot

112310-1

8.1

1937

0.2

81548

0.0

00

011

0.0

00

95

80

.02

36

14

0.2

815

13

-1.3

0.3

92.3

82.6

8Talb

ot

112379-0

1.1

1810

0.2

81499

0.0

00

02

00

.00

07

30

0.0

20

89

60

.28

14

74-5

.60.7

02.4

42.8

5Talb

ot

112379-0

3.1

1760

0.2

81485

0.0

00

016

0.0

00

82

10

.02

54

99

0.2

814

58

-7.3

0.5

62.4

62.9

2Talb

ot

112379-0

4.1

1763

0.2

81527

0.0

00

02

20

.00

05

79

0.0

19

05

20

.28

15

08

-5.5

0.7

72.3

92.8

1Talb

ot

112379-0

5.1

1775

0.2

81455

0.0

00

011

0.0

00

66

80

.02

10

22

0.2

814

33

-7.9

0.3

92.4

92.9

7Talb

ot

112379-0

6.1

1752

0.2

81474

0.0

00

010

0.0

013

69

0.0

45

03

10

.28

14

29

-8.5

0.3

52.5

12.9

9Talb

ot

112379-0

7.1

1788

0.2

81455

0.0

00

00

70

.00

06

42

0.0

215

21

0.2

814

33

-7.6

0.2

62.4

92.9

6Talb

ot

112379-0

8.1

174

10.2

81421

0.0

00

00

90

.00

06

12

0.0

19

913

0.2

814

01

-9.8

0.3

22.5

33.0

6Talb

ot

112379-1

4.1

1802

0.2

81477

0.0

00

011

0.0

00

92

00

.03

03

84

0.2

814

46

-6.8

0.3

92.4

82.9

2Talb

ot

112379-1

5.1

1794

0.2

81445

0.0

00

011

0.0

00

748

0.0

25

45

20

.28

14

20

-7.9

0.3

92.5

12.9

8Talb

ot

112379-1

7.1

174

10.2

81477

0.0

00

013

0.0

00

94

80

.03

18

23

0.2

814

46

-8.2

0.4

62.4

82.9

6Talb

ot

112379-1

8.1

174

60.2

81442

0.0

00

00

90

.00

07

01

0.0

22

22

50

.28

14

19

-9.0

0.3

02.5

13.0

2Talb

ot

112379-1

9.1

1682

0.2

81478

0.0

00

00

90

.00

05

62

0.0

17

87

00

.28

14

60

-9.0

0.3

02.4

52.9

7Talb

ot

112397-

01.

11785

0.2

81469

0.0

00

00

90

.00

05

110

.015

59

90

.28

14

52

-7.0

0.3

02.4

62.9

2Talb

ot

112397-

02.1

1784

0.2

81454

0.0

00

010

0.0

00

50

30

.016

20

70

.28

14

37

-7.5

0.3

42.4

82.9

5Talb

ot

112397-

03.1

1768

0.2

81480

0.0

00

00

90

.00

06

01

0.0

18

63

00

.28

14

60

-7.1

0.3

12.4

52.9

1Talb

ot

112397-

04.1

1771

0.2

81489

0.0

00

010

0.0

00

73

60

.02

34

83

0.2

814

64

-6.8

0.3

52.4

52.9

0Talb

ot

112397-

05.1

1793

0.2

81499

0.0

00

016

0.0

00

54

30

.017

93

20

.28

14

81

-5.8

0.5

62.4

22.8

5Talb

ot

112397-

06.1

1780

0.2

81468

0.0

00

010

0.0

00

614

0.0

19

93

30

.28

14

47

-7.2

0.3

52.4

72.9

3Talb

ot

112397-

07.

11796

0.2

81484

0.0

00

011

0.0

00

69

40

.02

17

57

0.2

814

60

-6.4

0.3

92.4

52.8

9Talb

ot

112397-

08.1

1817

0.2

81448

0.0

00

00

90

.00

07

02

0.0

2174

70

.28

14

24

-7.2

0.3

32.5

02.9

6Talb

ot

Tabl

e 1.

co

ntin

ued

Page 16: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

11

Analy

sis

No

.207P

b*/

206P

b*

(Ma)

176H

f/177H

f1 S

E176Lu/1

77H

f176Y

b/1

77H

f176H

f/177H

f iH

f1 S

E T

DM

T

DM

2Te

rrane

112397-

09.1

1781

0.2

81416

0.0

00

00

90

.00

05

97

0.0

18

80

00

.28

13

96

-9.0

0.3

12.5

43.0

5Talb

ot

112397-

11.1

1792

0.2

81544

0.0

00

010

0.0

00

35

70

.010

88

40

.28

15

32

-4.0

0.3

52.3

52.7

3Talb

ot

112397-

13.1

1786

0.2

81486

0.0

00

011

0.0

00

58

40

.018

97

70

.28

14

66

-6.4

0.3

92.4

42.8

8Talb

ot

112397-

15.1

1785

0.2

81478

0.0

00

010

0.0

00

76

70

.02

66

62

0.2

814

52

-7.0

0.3

52.4

72.9

2Talb

ot

104981-

3.1

1784

0.2

81547

0.0

00

017

0.0

00

86

00

.02

39

49

0.2

815

18

-4.6

0.6

02.3

82.7

7Talb

ot

104981-

5.1

1766

0.2

81538

0.0

00

013

0.0

00

96

60

.02

60

83

0.2

815

06

-5.5

0.4

62.4

02.8

1Talb

ot

104981-

6.1

1799

0.2

81519

0.0

00

02

40

.0011

49

0.0

311

03

0.2

814

80

-5.7

0.8

42.4

42.8

5Talb

ot

104981-

7.1

1761

0.2

81553

0.0

00

018

0.0

00

83

20

.02

03

66

0.2

815

25

-4.9

0.6

32.3

72.7

7Talb

ot

104981-

8.1

174

80.2

81482

0.0

00

02

00

.00

09

34

0.0

23

56

70

.28

14

51

-7.8

0.7

02.4

72.9

4Talb

ot

104981-

9.1

1795

0.2

81460

0.0

00

02

30

.0010

64

0.0

25

92

10

.28

14

24

-7.7

0.8

12.5

12.9

7Talb

ot

104981-

11.1

1764

0.2

81538

0.0

00

019

0.0

01010

0.0

27

16

80

.28

15

04

-5.6

0.6

72.4

02.8

1Talb

ot

104981-

12.1

1770

0.2

81518

0.0

00

02

10

.0016

45

0.0

45

56

20

.28

14

63

-6.9

0.7

42.4

72.9

0Talb

ot

104981-

13.1

1785

0.2

81545

0.0

00

02

10

.0011

39

0.0

316

77

0.2

815

06

-5.0

0.7

42.4

02.7

9Talb

ot

104981-

14.1

1883

0.2

81516

0.0

00

02

30

.00

07

55

0.0

20

55

70

.28

14

89

-3.4

0.8

12.4

12.7

7Talb

ot

104981-

17.

11805

0.2

81485

0.0

00

017

0.0

00

48

00

.012

87

90

.28

14

69

-5.9

0.6

02.4

42.8

7Talb

ot

104981-

18.1

1761

0.2

81514

0.0

00

019

0.0

00

89

30

.02

13

38

0.2

814

84

-6.4

0.6

72.4

32.8

6Talb

ot

104981-

19.1

174

50.2

81473

0.0

00

018

0.0

010

73

0.0

316

55

0.2

814

37

-8.4

0.6

32.4

92.9

8Talb

ot

110056-1

.11915

0.2

81535

0.0

00

018

0.0

02

26

70

.07

89

92

0.2

814

53

-4.0

0.6

32.4

92.8

3Talb

ot

110056-2

.12422

0.2

81424

0.0

00

02

30

.0016

07

0.0

53

79

00

.28

13

50

4.0

0.8

12.6

02.7

1Talb

ot

110056-4

.11806

0.2

81461

0.0

00

012

0.0

00

63

90

.02

09

33

0.2

814

39

-6.9

0.4

22.4

82.9

3Talb

ot

110056-7

.11994

0.2

81479

0.0

00

013

0.0

00

54

80

.017

72

40

.28

14

58

-2.0

0.4

62.4

52.7

6Talb

ot

110056-1

0.1

1767

0.2

81586

0.0

00

02

20

.0019

62

0.0

67

55

10

.28

15

20

-4.9

0.7

72.3

92.7

8Talb

ot

110056-1

2.1

2078

0.2

81495

0.0

00

02

50

.0011

42

0.0

34

86

20

.28

14

50

-0.4

0.8

82.4

72.7

2Talb

ot

110056-1

4.1

1856

0.2

81449

0.0

00

02

10

.0012

62

0.0

43

53

90

.28

14

05

-7.0

0.7

42.5

42.9

8Talb

ot

110056-1

5.1

2192

0.2

81402

0.0

00

018

0.0

010

62

0.0

33

70

70

.28

13

58

-1.0

0.6

32.5

92.8

5Talb

ot

110056-1

6.1

1759

0.2

81468

0.0

00

012

0.0

00

26

20

.00

84

67

0.2

814

59

-7.3

0.4

22.4

52.9

2Talb

ot

110056-1

7.1

2433

0.2

81237

0.0

00

02

30

.00

05

05

0.0

15

52

00

.28

12

14

-0.6

0.8

12.7

83.0

1Talb

ot

110056-1

8.1

1774

0.2

81548

0.0

00

018

0.0

00

44

40

.013

95

90

.28

15

33

-4.3

0.6

32.3

52.7

4Talb

ot

110056-1

9.1

2005

0.2

81447

0.0

00

019

0.0

00

52

30

.016

70

60

.28

14

27

-2.8

0.6

72.4

92.8

3Talb

ot

NO

TE

:

The A

naly

sis

No. is

the s

am

ple

num

ber

'-' gra

in n

um

be

r '.'

spot

num

ber. 1

76H

f/177H

f i,

Hf

and T

DM o

f zircons a

re c

alc

ula

ted u

sin

g t

he 2

07P

b*/

206P

b*

age o

f gra

in. T

DM

2 is c

alc

ula

ted u

sin

g a

tw

o-s

tage e

volu

tion a

ssum

ing a

mean 1

76Lu/1

77H

f ra

tio o

f cru

st

= 0

.015.

TD

M a

nd T

DM

2 a

re in G

a.

Tabl

e 1.

co

ntin

ued

Page 17: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

Kirkland et al.

12

Sample id Background corrected 18O/16O(a) 18O(b) 1 Excluded

Penglai@1 0.0020144 0.006 5.24 0.12 std

Penglai@2 0.0020145 0.020 5.27 0.40 std

Penglai@3 0.0020148 0.007 5.40 0.13 std

Penglai@4 0.0020145 0.007 5.28 0.14 std

Penglai@5 0.0020145 0.006 5.25 0.11 std

Penglai@6 0.0020144 0.006 5.24 0.12 std

112102@1 0.0020146 0.006 5.31 0.11

112102@02 0.0020146 0.008 5.32 0.16

112102@03 0.0020188 0.007 7.42 0.14 yes

112102@04 0.0020147 0.008 5.39 0.15

112102@05 0.0020246 0.014 10.30 0.28 yes

112102@06 0.0020186 0.017 7.28 0.34 yes

112102@07 0.0020138 0.005 4.94 0.10

112102@08 0.0020182 0.009 7.09 0.18 yes

112102@09 0.0020148 0.008 5.40 0.15

112102@10 0.0020149 0.007 5.48 0.14

112102@11 0.0020144 0.007 5.25 0.13

112102@12 0.0020208 0.009 8.40 0.18 yes

112102@13 0.0020138 0.010 4.94 0.19

112102@14 0.0020147 0.011 5.35 0.21

112102@15 0.0020217 0.006 8.86 0.12 yes

112102@16 0.0020151 0.007 5.57 0.14

112102@17 0.0020142 0.006 5.11 0.12

112102@18 0.0020144 0.008 5.21 0.15

112102@19 0.0020172 0.007 6.62 0.14 yes

112102@20 0.0020138 0.008 4.94 0.16

112102@21 0.0020146 0.013 5.33 0.26

Penglai@7 0.0020144 0.008 5.20 0.16 std

Penglai@8 0.0020145 0.006 5.29 0.12 std

Penglai@9 0.0020147 0.006 5.37 0.12 std

Penglai@10 0.0020144 0.012 5.24 0.23 std

Penglai@11 0.0020148 0.010 5.44 0.19 std

NOTES: Each 18O uncertainty (1 ) represents the sum of counting statistics errors for each individual spot and the

external error based on all standards analysed during the session, which were added in quadrature. Table is

in sequential order of analyses.

(a) Raw ratios corrected for measured Faraday offsets and yields.

(b) Normalized to a Penglai value of 5.3 per mil.

Excluded analyses were located on fractures or overlapped inclusions. Accepted analyses are from grains

interpreted to preserve magmatic values. Std denotes standard analysis

Table 2. Oxygen isotope analyses from zircons of sample GSWA 112102

Page 18: Report 122: The crustal evolution of the Rudall Province ...€¦ · Tessalina S 2013, The crustal evolution of the Rudall Province from an isotopic perspective: Geological Survey

GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

13

Mag

mat

icIn

herit

ance

Ag

e(s)

Det

rital

Ag

e(s)

Sam

ple

idU

nit

Lith

olog

yLa

titud

eLo

ngitu

de

Ag

e2σ

Talb

ot T

erra

ne

1123

79K

alka

n S

uper

suite

Bio

tite

mon

zogr

anite

(au

gen)

gne

iss

-22.

5375

212

2.18

105

1762

13

1049

81K

alka

n S

uper

suite

Bio

tite–

mus

covi

te m

onzo

gran

ite g

neis

s-2

2.77

444

122.

2591

717

6413

1118

54K

alka

n S

uper

suite

Bio

tite–

mus

covi

te g

rano

dior

ite g

neis

s-2

2.59

918

122.

2863

317

8212

>23

27

1123

41K

alka

n S

uper

suite

Mic

rom

onzo

gran

ite (

met

a-ap

lite)

dyk

e-2

2.55

919

122.

1741

117

7315

1100

56K

alka

n S

uper

suite

Bio

tite–

horn

blen

de g

rano

dior

ite g

neis

s-2

2.56

808

122.

3580

017

9512

2433

–191

5

1121

01K

alka

n S

uper

suite

Bio

tite-

epid

ote

mon

zogr

anite

gne

iss

-22.

6170

212

2.29

166

1793

831

23

1118

43K

alka

n S

uper

suite

Bio

tite–

mus

covi

te m

onzo

gran

ite g

neis

s-2

2.57

140

122.

3171

717

8916

1049

80K

alka

n S

uper

suite

Mon

zogr

anite

gne

iss

-22.

7323

312

2.30

067

1800

3

1123

10K

alka

n S

uper

suite

Gra

nodi

orite

gne

iss

-22.

5611

312

2.28

161

1801

12

1123

97K

alka

n S

uper

suite

Bio

tite

mon

zogr

anite

(au

gen)

gne

iss

-22.

4694

612

2.06

106

1783

6

1049

89E

aste

rn A

ssoc

iatio

nM

usco

vite

qua

rtzi

te-2

2.67

750

122.

3138

917

91, 1

955

1121

02M

esop

rote

rozo

ic g

rani

tes

Ser

iate

bio

tite

met

amon

zogr

anite

-22.

6209

112

2.12

083

1453

10

Co

nn

aug

hto

n T

erra

ne

1130

35K

alka

n S

uper

suite

Ort

hogn

eiss

-22.

8950

812

2.61

305

1777

6

1130

02K

alka

n S

uper

suite

Gra

nodi

orite

gne

iss

-22.

8014

712

2.57

583

1768

7

1121

60U

nass

igne

d gr

aniti

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Kirkland et al.

14

Model ages2, (TDM), which are calculated using the measured 176Lu/177Hf of the zircon, provide only a minimum age for the source material of the magma from which the zircon crystallized, because the 176Lu/177Hf ratio of zircon is much lower than the 176Lu/177Hf ratio of all reasonable reservoirs for Hf. Therefore, we have calculated two-stage model ages (TDM

2), which assumes that the parental magma was produced from an average continental crust (176Lu/177Hf = 0.015) that originally was derived from the depleted mantle (Griffin et al., 2004).

In the following text, the term ‘array’ is used to indicate variable 176Hf/177Hfi values at a single point in time, as could be due to mixing of isotopically distinct sources. The term ‘evolution’ refers to the variation of 176Hf/177Hfi values through time, consistent with the increase in daughter isotopes by decay of 176Lu within crust having a specific 176Lu/177Hf ratio.

Oxygen isotopes

Oxygen isotope ratios (18O/16O) were determined using a Cameca IMS 1280 multi-collector ion microprobe located at the Centre for Microscopy, Characterisation and Analysis (CMCA) at the University of Western Australia. Analytical conditions were similar to those outlined in detail by Kita et al. (2009). A static ~3 nA Cs+ beam with an impact energy of 20 keV was focused to a 15 μm spot on the sample surface. Instrument parameters included a magnification of 130x between the sample and field aperture, 400 μm contrast aperture, 4000 μm field aperture, 120 μm entrance slit, 500 μm exit slits, and a 40 eV band pass for the energy slit with a 5 eV gap. Secondary O- ions were accelerated to 10 keV and analysed with a mass resolving power of approximately 2400 using dual Faraday Cup detectors. A normal-incidence electron gun was used to provide charge compensation.

Each analysis spot was pre-sputtered for 10 seconds prior to automated peak-centering using secondary deflectors DTFA-X, DTFA-Y, and DTCA-X. Each analysis consisted of 20 four-second cycles through the mass stations, which gave an average internal precision of 0.17 ‰ (1 SDmean). Bracketing of standards permits instrumental mass fractionation (IMF) and drift to be assessed and corrected. IMF was corrected using the Penglai zircon standard (5.31  ± 0.10‰ 2 , (Li et al., 2010). A single block of 21 sample analyses of GSWA 112102 was bracketed by 11 standard analyses and IMF was calculated using a correction scheme similar to that described by Kita et al. (2009) with propagation of uncertainty as outlined in Appendix A1 of Kirkland et al. (2012). The spot-to-spot reproducibility (external precision) for standard spots on Penglai zircons was 0.08‰ (1 SDext, n=11). Corrected 18O/16O ratios are reported in 18O notation, in per mil variations relative to Vienna Standard Mean Ocean Water (VSMOW).

2 A model age, in its simplest form, is the time at which a sample

was separated from its source in the mantle, assuming the source is

not a mixture. More specifically, it is the time at which the isotopic

signature of the sample was the same as that of a model reservoir

Talbot Terrane

Kalkan Supersuite

GSWA 112379: biotite monzogranite (augen) gneiss, Split Rock

This sample was dated by Nelson (1995k). Zircons isolated from this sample are colourless to yellow, euhedral, and have aspect ratios up to 5:1. Both transmitted and reflected-light images imply that there are no inherited cores within this zircon sample. Excluding one U–Pb analysis that is 14% discordant and has lost radiogenic Pb, the remaining 20 analyses yield a concordia age of 1762 ± 13 Ma (MSWD = 1.8; Fig. 3a), interpreted as the igneous crystallization age of the granite protolith. This result is slightly younger than the 1765 ± 15 Ma date proposed by Nelson (1995k). Hf isotope measurements of 12 zircons yield Hf(t) values that range from –5.5 to –9.8 and are more unradiogenic than CHUR (Fig. 4). The Hf isotope data are well grouped and indicate a TDM

2 of c. 2.8 Ga.

GSWA 104981: biotite–muscovite monzogranite gneiss, southern part of Graphite Valley

The geochronology of this sample was reported by Nelson (1995d). Zircons from this sample are colourless to dark brown, euhedral to subhedral, typically fractured, and have aspect ratios up to 5:1. Transmitted-light images indicate potentially older cores within several zircons, although most crystals are apparently homogeneous. The U–Pb analyses are concordant to strongly discordant. Five analyses >10% discordant are not considered further. Thirteen analyses yield a concordia age of 1764  ±  13  Ma (MSWD = 2.0; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith to the gneiss. This date is younger than the 1775 ± 10 Ma date reported by Nelson (1995d). One analysis yields a 207Pb*/206Pb* date (1 ) of 1883 ± 47 Ma, interpreted as the age of an inherited component (Nelson, 1995d). Hf isotope measurements of 13 zircons yield Hf(t) values of –3.4 to –8.4, and are more unradiogenic than CHUR (Fig. 4). The Hf isotope data define an array indicating a maximum TDM

2 of c. 3.0 Ga.

GSWA 111854: biotite–muscovite granodiorite gneiss, Poonemerlarra Creek west

This sample was dated by Nelson (1995h). Zircons from this sample are colourless to yellow, euhedral, and equant to elongate, with aspect ratios up to 6:1. Transmitted-light images suggest that most crystals are homogeneous with no inherited cores. Four analyses greater than 5% discordant have probably lost radiogenic Pb and are not considered further. One of these discordant analyses is of an inherited core that indicated a minimum age of 2327  Ma. The remaining eight analyses yield a concordia age of 1782 ± 12 Ma (MSWD = 1.6; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith to the gneiss. This date is slightly older than the 1778 ± 17 Ma date reported by Nelson (1995h). Hf isotope

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GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

15

2200

2000

1800

1600

1400

12000.08

0.10

0.12

0.14

0.16

2.0 2.4 2.8 3.2 3.6 4.0 4.4 4.8

20

72

06

Pb

*/

P

b*

238 206

U/ Pb*

GSWA 112379: biotite monzogranite (augen) gneiss, Split Rock

GSWA 104981: biotite-muscovite monzogranite gneiss,

southern part of Graphite Valley

GSWA 111854: biotite-muscovite granodiorite gneiss,

Poonemerlarra Creek west

GSWA 112341: micromonzogranite

(meta-aplite) dyke, Rudall airstrip

GSWA 110056: biotite-hornblende

granodiorite gneiss, Rooney Creek

GSWA 112101: biotite-epidote

monzogranite gneiss, Larry Creek

GSWA 112397:

coarse-grained

porphyritic biotite

monzogranite

(augen) gneiss,

Watrara Inlier

GSWA 112310:

granodiorite

gneiss, Dunn

Creek west

GSWA 104980:

monzogranite

gneiss, Graphite Valley

GSWA 111843: biotite-

muscovite monzogranite gneiss,

Poynton Creek

CLK83_1 27.03.13

Talb

otTerr

ane

Figure 3a. Stacked concordia diagrams showing U–Pb zircon analytical data for zircons from Rudall Province samples analysed

by SHRIMP ion microprobe. Error crosses are shown at the 2-sigma level. All data (see Nelson et al. in the reference

list) are available online (www.dmp.wa.gov.au/geochron). Yellow squares indicate magmatic zircon; red squares

indicate inherited / detrital zircon; blue squares indicate youngest detrital zircon; green squares indicate metamorphic

zircon; grey squares indicate discordant analyses; black squares indicate concordant analyses interpreted to have

undergone radiogenic-Pb loss.

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Kirkland et al.

16

1400

1600

1800

2000

2200

1200

4.84.40.08

0.10

0.12

0.14

0.16

2.0

CLK83_2 27.03.13

Connaughto

n

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ot

Table

top

207

206

Pb

*/

Pb

*

238 206

U/ Pb*

2.4 2.8 3.2 3.6 4.0

GSWA 118914:

foliated granite,

north of Harbutt Range

GSWA 104989: muscovite

quartzite, Fingoon Quartzite

GSWA 112102: seriate biotite metamonzogranite,

southern part of the Watrara Inlier

GSWA 113035: orthogneiss,

east of South Rudall Dome

GSWA 113002: granodiorite gneiss,

Cotton Creek

GSWA 112160:

garnet microgneiss,

Harbutt Range

Figure 3b. Stacked concordia diagrams showing U–Pb zircon analytical data for zircons from Rudall Province

samples analysed by SHRIMP ion microprobe. Error crosses are shown at the 2-sigma level. All data (see

Nelson et al. in the reference list) are available online <www.dmp.wa.gov.au/geochron>. Yellow squares

indicate magmatic zircon; red squares indicate inherited / detrital zircon; blue squares indicate youngest

detrital zircon; green squares indicate metamorphic zircon; grey squares indicate discordant analyses;

black squares indicate concordant analyses interpreted to have undergone radiogenic-Pb loss.

measurements of 11 zircons yield Hf(t) values ranging from –5.6 to –9.5, and form an array that is slightly to strongly more unradiogenic than CHUR (Fig. 4), and define a maximum TDM

2 of c. 3.4 Ga. The single discordant core yields an Hf(t) value of +2.

GSWA 112341: micromonzogranite (meta-aplite) dyke, Rudall airstrip

This sample, dated by Nelson (1995j), yielded zircons that are yellow to brown, subhedral to anhedral, and have aspect ratios up to 4:1. Transmitted-light images do not indicate any obvious cores. Excluding one

younger analysis, 15 analyses yield a concordia age of 1773 ± 15 Ma (MSWD = 1.0; Fig. 3a), interpreted as the age of magmatic crystallization of the dyke. This date is slightly younger than the 1778 ± 16 Ma date reported by Nelson (1995j). The single excluded analysis yields a 207Pb*/206Pb* date of 1612 ± 44 Ma (1 ), interpreted by Nelson (1995j) to reflect disturbance by younger metamorphic events. Hf isotope measurements of 13 zircons yield Hf(t) values ranging from –3.6 to –11.4, plot as an array that is slightly to strongly more unradiogenic than CHUR (Fig. 4), and indicate a maximum TDM

2 of c. 3.1 Ga.

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GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

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GSWA 110056: biotite–hornblende granodiorite gneiss, Rooney Creek

This sample was dated by Nelson (1995f), and yielded zircons that are brown to black, euhedral to subhedral, and have aspect ratios up to 5:1. Transmitted-light images reveal that many crystals contain apparently older cores. Excluding seven analyses of inherited zircon cores, five analyses >5% discordant, and one analysis with high common Pb (>10% common 206Pb), six analyses yield a concordia age of 1795 ± 12 Ma (MSWD = 1.04; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith to the gneiss. This date is slightly older than the 1790 ± 17 Ma date reported by Nelson (1995f). Inherited cores yield 207Pb*/206Pb* dates of 2433–1915 Ma. Hf isotope measurements of five zircons from the magmatic component in this sample yield Hf(t) values of –0.6 to –7.3, and seven analyses of inherited zircon cores yield Hf(t) values ranging from –0.4 to –4.0 (Fig. 4). The Hf isotope data define an evolution trend from a source with a maximum TDM

2 of 3.0 Ga.

GSWA 112101: biotite-epidote monzogranite gneiss, Larry Creek

The geochronology of this sample was reported by Nelson (1996a). Zircons from this sample are yellow to dark brown, euhedral, and have aspect ratios up to 5:1. Transmitted-light images reveal concentric zoning made visible by variable degrees of radiation damage. Several crystals contain apparently older cores. Seventeen analyses yield a weighted mean 207Pb*/206Pb* date of 1793 ± 8 Ma (MSWD = 1.02; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith. This date is similar to the 1792 ± 9 Ma result reported by Nelson (1996a). A single analysis located on a xenocrystic core yields a 207Pb*/206Pb* date of 3123 ± 16 Ma (1 ) (Fig. 3a). Hf isotope measurements on 10 magmatic zircons yield Hf(t) values of –2.7 to –9.1 (Fig. 4) and define an array

with a maximum TDM2 of 3.0 Ga.

GSWA 111843: biotite–muscovite monzogranite gneiss, Poynton Creek

This sample was dated by Nelson (1995g), and yielded zircons that are colourless to black, euhedral, and have aspect ratios up to 5:1. Many crystals contain apparently older cores. Excluding two analyses >10% discordant, 10 analyses yield a concordia age of 1789 ±  16 Ma (MSWD  =  0.81; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith. This date is slightly younger that the 1795 ± 17 Ma date reported by Nelson (1995g). Four other analyses yield dates of 2102– 1877 Ma, interpreted as xenocrystic components (Fig. 3a). Hf isotope measurements of 12 zircons yield Hf(t) values of –4.6 to –12.0 (Fig. 4), and define an array with a maximum TDM

2 of 3.3 Ga. The older inherited zircons yield Hf isotope signatures consistent with evolution from the same source as the c. 1789 Ma magmatism (Fig. 4).

-30

-30

-30

-20

-20

-20

-10

-10

-10

0

0

0

10

10

10

1000 1200 1400 1600 1800 2000 2200 2400

Age (Ma)

Ep

sil

on

Hf

Tabletop Terrane

Connaughton Terrane

Talbot Terrane

CLK82a 1 . .14 01 3

D

GT EPT

D

GT EPT

D

GT EPT

M

Figure 4. Hf evolution diagrams for Rudall Province samples

(circles, this study) compared to potential source

regions. Shaded fields illustrate normal crustal

evolution of Hf along a 176Lu/177Hf slope of 0.015.

Abbreviations used in figure: EPT — East Pilbara

Terrane, GT — Glenburgh Terrane (Capricorn

Orogen basement), D — Dalgaringa Supersuite

intrusive rocks. Red line is the depleted mantle

model of Griffin et al. (2000) and the blue line is

CHUR.

GSWA 104980: monzogranite gneiss, Graphite Valley

This sample was dated by Nelson (1995c). Zircons from this sample are colourless to brown, euhedral, elongate to equant, and have aspect ratios up to 5:1. No cores are apparent in transmitted-light images. Fourteen analyses yield a concordia age of 1800 ± 3 Ma (MSWD = 0.84; Fig. 3a), interpreted as the age of magmatic crystallization of the protolith, and identical to the result reported by Nelson (1995c). Hf isotope measurements of 10 zircons yield Hf(t) values ranging from –6.5 to –8.7 (Fig. 4), and indicate a maximum TDM

2 of 3.0 Ga.

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Kirkland et al.

18

GSWA 112310: granodiorite gneiss, Dunn Creek west

This sample was dated by Nelson (1995i). Zircons from this sample are colourless to dark brown, euhedral, elongate and have aspect ratios up to 6:1. Idiomorphic zoning is ubiquitous and apparently older cores are visible in transmitted light. Excluding one analysis >10% discordant, four analyses yield a concordia age of 1801 ± 12 Ma (MSWD = 1.8; Fig. 3a), interpreted as the age of magmatic crystallization of the granite protolith. This date is identical to that reported by Nelson (1995i). A further 13 analyses from this sample yield 207Pb*/206Pb* dates of 1980–1932 Ma, interpreted as the ages of inherited components. A significant age component at 1967 ± 10 Ma (MSWD = 2.2; Fig. 3a), was interpreted by Nelson (1995i) as the age of an older granitic component within the orthogneiss. Hf isotope measurements of 14 zircons yield Hf(t) values ranging from +0.7 to –9.5 (Fig. 4). The Hf data from the c. 1800 Ma component define an array with a maximum TDM

2 of 3.0 Ga, whereas the older c. 1970 Ma component defines a more radiogenic array with a maximum TDM

2 of 2.8 Ga (Fig. 4).

GSWA 112397: coarse-grained porphyritic biotite monzogranite (augen) gneiss, Watrara Inlier

This sample was dated by Nelson (1995l). Zircons from this sample are colourless, euhedral, and elongate, with aspect ratios up to 6:1. No older cores are apparent in transmitted light. Fifteen analyses yield a concordia age of 1783 ± 6 Ma (MSWD = 1.3; Fig. 3a), interpreted as the age of magmatic crystallization of the granite protolith. This date is slightly younger than the 1787 ± 5 Ma date reported by Nelson (1995l). Hf isotope measurements of 14 zircons yield Hf(t) values of –3.4 to –9.0 (Fig. 4), and define an array with a maximum TDM

2 of 3.0 Ga.

Eastern Association

GSWA 104989: muscovite quartzite, Fingoon Quartzite

This sample, dated by Nelson (1995e), yielded zircons that are colourless, anhedral to subhedral, and have aspect ratios up to 5:1. Most crystals have strongly rounded terminations, consistent with sedimentary transport. Transmitted-light images reveal mainly homogeneous zircons, including a few that contain apparently older cores. The detrital zircon age spectrum is dominated by 18 analyses that yield a weighted mean 207Pb*/206Pb* date of 1791 ± 10 Ma (MSWD = 0.68; Fig. 3b), representing the age of a significant detrital component within the precursor sediment and a conservative maximum depositional age. One older detrital grain yields a 207Pb*/206Pb* date of 1955 ± 15 Ma (1 ). Hf isotope measurements of 17 zircons from the main detrital age component yield Hf(t) values ranging from –3.2 to –12.6 (Fig. 4). A single analysis of the older detrital zircon yields a Hf(t) value of –8.9. The Hf isotope data define an array with a maximum TDM

2 of 3.2 Ga. The older detrital grain has a similar Hf source to that of the c. 1790 Ma component.

Mesoproterozoic granites

GSWA 112102: seriate biotite metamonzogranite, southern part of the Watrara Inlier

Geochronology of this sample was reported by Nelson (1996b). The zircons are colourless to yellow or brown, euhedral, and predominantly equant with aspect ratios up to 4:1. Transmitted and reflected light images do not indicate the presence of older cores. Eleven analyses indicate variable recent radiogenic-Pb loss and yield a weighted mean 207Pb*/206Pb* date of 1453 ± 10 Ma (MSWD = 0.68; Fig. 3b), interpreted as the igneous crystallization age of the granite (Nelson, 1996b). Hf isotope measurements of eight zircons yield Hf(t) values of +2.5 to +5.6, and plot between CHUR and DM (Fig. 4). The Hf isotope data are well grouped and indicate a TDM

2 of c. 1.9 Ga. Oxygen isotopes were measured in 21 zircons, and include six analyses that ablated through cracks and one analysis that incorporated limonite adhered to the grain margin. These seven analyses yield heavy

18O values of >6.6 ‰ and are considered to represent modified 18O values. The remaining 14 analyses yield

18O values from 4.9 to 5.6 ‰, with a weighted mean of 5.23 ± 0.12 ‰ (MSWD = 2.1; Table 2).

Connaughton Terrane

Kalkan Supersuite

GSWA 113035: orthogneiss, east of South Rudall Dome

This sample was dated by Nelson (1996d). Zircons from this sample are yellow to brown, euhedral, and have aspect ratios up to 5:1. No older cores are apparent in transmitted light. The analyses are slightly reversely discordant. The zircons have relatively low uranium (<300 ppm 238U) and thorium contents; hence, the reverse discordance is unlikely to reflect matrix effects associated with radiation damage (metamictization), commonly observed in analyses of high-U zircons. Thirteen analyses yield a weighted mean 207Pb*/206Pb* date of 1777 ± 6 Ma (MSWD  = 1.0; Fig. 3b), interpreted as the age of magmatic crystallization of the granite protolith (Nelson, 1996d). Hf isotope measurements of eight zircons yield Hf(t) values ranging from +0.3 to –3.4 (Fig. 4). The

Hf isotopic data define an array that clusters towards the evolved end (further from CHUR) and indicates a maximum TDM

2 of 2.6 Ga.

GSWA 113002: granodiorite gneiss, Cotton Creek

This sample was dated by Nelson (1995m). Zircons from this sample are yellow to black, euhedral, inclusion-rich, and have aspect ratios up to 5:1. One xenocrystic core is visible in transmitted light, but was not analysed. Excluding one strongly discordant analysis, 13 analyses yield a concordia age of 1768 ± 7 Ma (MSWD = 0.50; Fig. 3b), interpreted as the age of magmatic crystallization of the granite protolith. Nelson (1995m) reports an age of

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1769 ± 7 Ma for this sample. Hf isotope measurements of 10 zircons yield well-grouped Hf(t) values between –3.3 and –5.7 (Fig. 4), and indicate an average TDM

2 of 2.7 Ga.

Unassigned gneissic rocks

GSWA 112160: garnet microgneiss, Harbutt Range

Geochronology of this sample was reported by Nelson (1996c). Zircons from this sample are yellow to brown, subhedral, elongate with rounded terminations, and have aspect ratios up to 5:1. Xenocrystic cores are visible in transmitted light images. It is currently unclear whether the protolith of this rock was igneous or sedimentary in origin. Twelve analyses were conducted of 11 zircons. Seven analyses of zircon cores yield 207Pb*/206Pb* dates of 1873–1764 Ma. Three imprecise and slightly dispersed analyses yield a weighted mean 207Pb*/206Pb* date of 1672 ± 65 Ma (MSWD = 1.2; Fig. 3b). Two analyses of a low-U zircon rim yield very imprecise dates around 1200 Ma (Fig. 3b). The seven analyses of zircon cores are dispersed beyond analytical uncertainty and the dates are interpreted as the ages of inherited components within the gneiss. The date of 1672 ± 65 Ma for three analyses could approximate the age of migmatization of the rock or, if the protolith was of sedimentary origin, could represent a maximum age of deposition, as suggested by Nelson (1996c). The dates of c. 1200 Ma for two analyses of a zircon rim have high Th/U ratios that Nelson (1996c) interpreted as an indication of igneous rather than metamorphic growth. Ten Hf isotope measurements of 10 Paleoproterozoic zircons yield Hf(t) values ranging from –7.1 to –16.6 (Fig. 4), and define a dispersed array with a maximum TDM

2 of 3.4 Ga, consistent with a heterogeneous source. Two analyses sited on the Mesoproterozoic zircon rim yield similar 176Hf/177Hf and 176Lu/177Hf ratios to the rest of the population, which suggests this rim did not grow in the presence of a HREE sequestering phase (e.g. garnet).

Tabletop Terrane

GSWA 118914: foliated granite, north of Harbutt Range

This sample was dated by Nelson (1996e). Zircons from this sample are colourless to yellow, euhedral, and mainly equant, with aspect ratios up to 4:1. Most crystals appear homogeneous in transmitted-light images. Excluding two analyses with high common Pb (>1% common 206Pb), and four analyses interpreted to have undergone minor ancient radiogenic-Pb loss, the remaining 13 analyses yield a weighted mean 207Pb*/206Pb* date of 1310 ± 5 Ma (MSWD = 1.4; Fig. 3b), essentially identical to that reported by Nelson (1996e), and interpreted as the age of magmatic crystallization. Hf isotope measurements of 16 zircons yield Hf(t) values ranging from –5.3 to –11.6 (Fig. 4). The Hf isotope data are well grouped and yield an average TDM

2 of 2.6 Ga, although one analysis indicates a value of 2.8 Ga.

Discussion

Hf isotope signatures of

Paleoproterozoic Australia

During the Proterozoic, Archean crustal fragments were progressively amalgamated into larger cratons that now form the North, West, and South Australian Cratons (Tyler, 2005). Some Proterozoic orogenic belts were produced by continental collision or arc collision, and thus contain oceanic or exotic microcontinental components. The West Australian Craton comprises the Archean Pilbara and Yilgarn Cratons, the Archean to Paleoproterozoic Glenburgh Terrane (Johnson et al., 2012), and other potentially exotic elements such as the Rudall Province. Major additions of crust to the margins of the West Australian Craton in the form of the Albany–Fraser and Pinjarra Orogens occurred during several pulses in the Proterozoic (Kirkland et al., 2012; Spaggiari et al., 2012). Hf isotopes can be used to characterize the influence of new additions from the mantle, and the reworking of pre-existing crust, through time. Thus, the isotopic signatures of well-dated magmatic rocks can be used to examine possible genetic connections between crustal fragments and to diagnose the presence or absence of exotic terranes. The various rifted pieces of a once-united crustal block should share a comparable isotopic signature to their ancestral home, because they would likely share a common time of crust formation. The similar ages of deformation and metamorphism in the Rudall Province, Capricorn Orogen, and Arunta Orogen suggest that the relationships between these lithological blocks and other Proterozoic orogenic belts should be evaluated (Bagas, 2004; Johnson et al., 2012; Fig. 5).

Capricorn Orogen

The Capricorn Orogen is situated to the west of the Rudall Province and is a region of Proterozoic tectono-metamorphism and magmatism that separates the Archean Pilbara and Yilgarn Cratons (Johnson et al., 2011a, 2012). The Capricorn Orogen records the Paleoproterozoic collision of these cratons to form the West Australian Craton, as well as several intracratonic reworking events between Paleoproterozoic and latest Neoproterozoic time (Tyler and Thorne, 1990; Cawood and Tyler, 2004; Johnson et al., 2012). The Gascoyne Province, at the western end of the orogen, contains several Proterozoic granite suites, including the voluminous 1820–1775 Ma Moorarie Supersuite, which is similar in age to magmatic rocks in the Rudall Province.

The Glenburgh Terrane, which forms the basement to the Gascoyne Province, comprises 2555–2430 Ma granitic gneisses of the Halfway Gneiss, mid-Paleoproterozoic metasedimentary rocks, and an arc-related granitic batholith of the 2005–1970 Ma Dalgaringa Supersuite (Johnson et al., 2012). The Hf isotope compositions of zircons within the Glenburgh Terrane indicate a major period of crustal growth between c. 2730 and c. 2600 Ma, although much of this material was reworked during

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Kirkland et al.

20

tectono-magmatic events between c. 2555 and c. 2430 Ma (Johnson et al., 2011a). Both the crystallization history and crustal source of the Halfway Gneiss is somewhat dissimilar to the Pilbara and Yilgarn Cratons, which led Johnson et al. (2012) to infer that the Glenburgh Terrane was an element exotic to both these cratons. The Glenburgh Terrane is envisaged to have collided with the Pilbara Craton during the 2215–2145 Ma Ophthalmian Orogeny, and the combined Pilbara Craton–Glenburgh Terrane (‘Pilboyne Craton’) collided with the Yilgarn Craton during the 2005–1950 Ma Glenburgh Orogeny (Johnson et al., 2012).

The 1820–1770 Ma Capricorn Orogeny took place during a similar time interval to the 1800–1765 Ma Yapungku Orogeny in the Rudall Province, the effects of which are recognized throughout most of the Capricorn Orogen (Sheppard et al., 2010b). The orogeny is associated with low- to medium-grade metamorphism and intense structural reworking, the intrusion of voluminous granitic magmas of the 1820–1775 Ma Moorarie Supersuite, and deposition of sedimentary rocks of the upper Wyloo Group (Ashburton Basin), including the c. 1800 Ma Ashburton Formation (Evans et al., 2003; Sircombe, 2003), the c.  1800 Ma Capricorn Group (Blair Basin; Hall et al., 2001), and the 1840–1810 Ma Leake Spring

CLK75a 15.08.12

0.2805

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Age (Ma)

Talbot

Connaughton

Halfway Gneiss

East PilbaraTerrane

West Arunta

Arunta whole-rock Nd

Tabletop

Dalgaringa Supersuite

Capricorn Orogen

basins

Bridget Suite

MP

D

GT

EPT

rim

176

17

7

Hf/

Hf

init

ial

Figure 5. Initial 176Hf/177Hf evolution diagram for samples from the Rudall Province (circles, this study) compared to potential

source regions. Shaded fields illustrate normal crustal evolution of Hf along a 176Lu/177Hf slope of 0.015. Hf data

are from <www.dmp.wa.gov.au/geochron>. Whole-rock Nd data for the Arunta Orogen are converted to Hf values

assuming a terrestrial array relationship. Abbreviation in figure: MP — Musgrave Province basement. Other notes

as in Figure 4.

Metamorphics (Sheppard et al., 2010b) in the Gascoyne Province (Fig. 1). These sedimentary rocks were deposited in response to the onset of the 1820–1770 Ma Capricorn Orogeny, possibly in a foreland basin setting (Thorne and Seymour, 1991; Sircombe, 2002; Evans et al., 2003). The upper Wyloo Group, including the Ashburton Formation, is mostly a turbiditic deep-marine succession (Thorne and Seymour, 1991). These sedimentary rocks were deformed once, and unconformably overlain by terrestrial, lacustrine to shallow-marine sedimentary rocks of the Capricorn Group (Thorne and Seymour, 1991). Paleocurrent directions in both the Ashburton Formation (Thorne and Seymour, 1991) and Capricorn Group (Thorne and Seymour, 1991; Hall et al., 2001) imply that the sediments were supplied from the southeast and southwest, respectively. The U–Pb age spectrum and Lu–Hf isotopic composition of detrital zircons within both sedimentary successions (Sircombe, 2002; GSWA, unpublished data), combined with the paleocurrent data, indicate that the southern part of the Gascoyne Province was a major source for the sedimentary detritus (Nelson, 2004a,b). In particular, the 2555–2430 Ma Halfway Gneiss and 2005–1970 Ma Dalgaringa Supersuite of the Glenburgh Terrane, and the early c. 1820 to c. 1800 Ma Moorarie Supersuite granites, appear to dominate the detrital signatures.

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The 1840–1810 Ma Leake Spring Metamorphics are a package of low- to medium-metamorphic grade siliciclastic metasedimentary rocks that were deposited across much of the Gascoyne Province, including the Glenburgh Terrane (Sheppard et al., 2010). These sedimentary rocks are thought to pass, with decreasing metamorphic grade, into the Ashburton Formation to the north (Williams, 1986). These metasedimentary rocks were also sourced from the southern part of the Gascoyne Province (Sheppard et al., 2010b).

Pilbara Craton

The boundary between the Pilbara Craton (including the East Pilbara Terrane and the overlying Fortescue, Hamersley, and Turee Creek Basins) and the Rudall Province to the east is covered by unconformably overlying Meso- to Neoproterozoic sedimentary rocks (Fig. 1). During the Archean and prior to 2800 Ma, the Pilbara Craton was dominated by the construction of granite–greenstone terranes (Smithies et al., 1999; Hickman, 2004; Van Kranendonk et al., 2004). These rocks are unconformably overlain by the late Archean to Paleoproterozoic volcanic and sedimentary rocks of the Fortescue, Hamersley, and Turee Creek Groups (Thorne and Trendall, 2001) which in turn are unconformably overlain by siliciclastic rocks of the c. 2200 Ma lower Wyloo Group and the c. 1800 Ma upper Wyloo Group (Thorne and Seymour, 1991). A minor suite of east-northeast-trending kimberlite dykes intruded the eastern Pilbara Craton at c. 1870 Ma (Wyatt et al., 2002).

Calc-alkaline, lamprophyric syenite to monzodiorite granitic rocks of the c. 1800 Ma Bridget Suite (Hickman, 1978; Collins et al., 1988; Budd et al., 2002) form a north-northwest-trending belt within the East Pilbara Terrane and younger parts of the Pilbara Craton, adjacent and subparallel to the northwest−southeast trend of the Paterson Orogen. The rocks have Sr-undepleted, Y-depleted, fractionated compositions. Emplacement of the suite has been interpreted to be a far-field response to continent-continent collision during the Yapungku Orogeny. The crystallization age of a monzodiorite from this suite was dated at 1803 ± 19 Ma (GSWA 169030; Nelson, 2002), and a trondhjemitic pegmatite at 1793 ± 17 Ma (GSWA 178232; Bodorkos et al., 2006). Magmatic zircons from the monzodiorite (GSWA 169030) yield a range of Hf values, from –13.65 to –21.22, while those from the pegmatite yielded a range of Hf, from –4.67 to –7.50 (Fig. 5). Xenocrystic zircon cores dated between c. 3520 to c. 2841 Ma in both samples yielded Hf values from +4.10 to –7.47 (Fig. 5). The ages and

Hf isotopic signatures of the inherited zircons in these magmatic rocks are consistent with incorporation of East Pilbara Terrane crust into Bridget Suite magmas.

Arunta Orogen

The Proterozoic Arunta Orogen lies along the southern margin of the North Australian Craton (Fig. 1; Collins and Shaw, 1995; Dunlap and Teyssier, 1995; Sun et al., 1995; Zhao and Bennett, 1995; Zhao and McCulloch, 1995; Claoue-Long and Hoatson, 2005; Scrimgeour et al., 2005)

and has been divided into a southern Warumpi Province, generally inferred to be exotic, and an autochthonous Aileron Province (Scrimgeour et al., 2005). The Aileron Province had on its southern margin a north-dipping subduction zone during the 1810–1790 Ma Stafford Event (Claoue-Long and Hoatson, 2005). After the Stafford Event, an active margin/back-arc setting developed with several tectono-magmatic events including the c. 1780 Ma Yambah, 1760–1740 Ma Inkamulia, and 1690–1670 Ma Strangways Events (Collins and Williams, 1995; Claoue-Long and Hoatson, 2005).

The 1810–1790 Ma Stafford Event (Claoue-Long and Hoatson, 2005) is coeval with intrusion of the 1800–1765 Ma Kalkan Supersuite in the Rudall Province. Only limited deformation was associated with the Stafford Event, and metamorphism during this event was driven by magmatic heat advection (Claoue-Long and Hoatson, 2005). The c. 1780 Ma Yambah Event in the Arunta Orogen (Collins and Shaw, 1995; Scrimgeour, 2003; Claoue-Long et al., 2008) was also near-synchronous with the youngest components of the Kalkan Supersuite in the Rudall Province. The Yambah Event does not appear to correspond to major crustal thickening (Scrimgeour, 2003) but has been associated with northeast–southwest shortening (Hand and Buick, 2001).

The Warumpi Province records two Paleoproterozoic magmatic events: high-K calc-alkaline magmatism during the 1690–1670 Ma Argilke Event, and magmatism associated with a 1640–1635 Ma accretion event known as the Liebig Orogeny (Scrimgeour et al., 2005). The Argilke event is thought not to have affected the North Australian Craton and has been attributed to an outboard magmatic arc that was subsequently accreted onto the Aileron Province during the 1640–1635 Ma Liebig Orogeny (Scrimgeour et al., 2005). In the westernmost extent of the Arunta Orogen, however, Hf isotope data for a 1690 Ma granite suggests both juvenile input and an Archean source component identical to the Aileron Province (Kirkland et al., 2009). This could imply a situation in which the Warumpi Province developed within proximity to the western Aileron Province during the Argilke Event, either as an autochthonous block that was never substantially displaced or as a rifted fragment that was significantly displaced but subsequently re-accreted onto the southern margin of the Aileron Province during north-directed subduction.

The Hf isotope signature of 1810–1670 Ma zircons from the west Arunta region indicates crustal source regions dominated by components that formed between 2.7 and 2.0 Ga (Fig. 5; Kirkland et al., 2013). Whole-rock Nd isotope data from granites in the central and eastern Arunta imply similar crustal sources, dominated by components formed through mantle extraction at 2.5 – 2.2 Ga (Zhao and McCulloch, 1995).

Musgrave Province

The Musgrave Province lies at the junction of the North, South, and West Australian Cratons. Crystalline basement rocks, dated at 1600–1500 Ma and c. 1400 Ma (Edgoose et al., 2004; Wade et al., 2006; Wade et al., 2008; Kirkland

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22

et al., 2013), are subordinate to 1345–1293 Ma magmatic rocks of the Mount West Orogeny (Howard et al., 2011a; Howard et al., 2011b). The 1220–1150 Ma Musgrave Orogeny, and the 1085–1040 Ma Giles Event are younger, possibly intracontinental, tectono-magmatic events (Evins et al., 2010; Smithies et al., 2010; Smithies et al., 2011). Although the nature of Musgrave Province basement is cryptic, the Nd and Hf isotope evolution of nearly all rocks in the Musgrave Province requires the presence of sources derived from Archean, c. 1900 Ma, and c. 1600 Ma crust with subsequent juvenile additions after c. 1220 Ma. Although there are no physical remnants of c. 1900 Ma juvenile material, radiogenic addition into the crust at this time is required to account for the correspondence between mantle extraction ages and reworking of Archean material, and is indicated by mantle-like oxygen isotope ratios in zircons with c. 1900 Ma Hf model ages (Fig. 5; Kirkland et al., 2013).

Inherited and detrital zircons of

the Rudall Province

In order to appropriately interpret the zircon Hf isotope data with respect to the regional evolution of the Rudall Province and the potential exotic (e.g. North Australian Craton) or endemic (West Australian Craton) nature of basement terranes, an important step is to consider the origin of the inherited zircons in the 1800–1765 Ma Kalkan Supersuite granitic rocks. The zircons may be of local provenance, having been entrained within the granites from basement terranes. In this case, the Hf isotopic evolution of the magmatic and inherited zircons will provide critical information on the nature and origin of the Rudall Province basement. If, however, the zircons are distally-derived (as part of a regionally-sourced sedimentary sequence, having been entrained within the granites during the emplacement of the magmas into the sedimentary succession), little information can be gained on the nature of the local basement, as these data reflect the geological development of all the distal sources of detritus in the region (e.g. the eastern Pilbara margin and Gascoyne Province).

In the eastern association, siliciclastic paragneiss contains c. 1790 Ma detrital zircons (Nelson, 1995e), and is intruded by the 1800–1765 Ma Kalkan Supersuite granites (Bagas, 2004). This indicates deposition of the eastern sedimentary association close to c. 1790 Ma, which is in a similar timeframe for the deposition of sedimentary rocks in the Capricorn Orogen to the west, specifically the c. 1800 Ma Ashburton Formation (Evans et al., 2003; Sircombe, 2003), the c. 1800 Ma Capricorn Group (Hall et al., 2001), and the 1840–1810 Ma Leake Spring Metamorphics (Sheppard et al., 2010b) (Fig. 1). The U–Pb age modes and Lu–Hf isotope composition of inherited zircons within the Kalkan Supersuite granitic rocks from both the Talbot and Connaughton Terranes are similar (Fig. 6). The granitic rocks are dominated by isotopically evolved ( Hf between 0 and –20) zircon with discrete age modes at c. 1800 Ma and c. 2000 Ma, similar to the zircon detritus within the Capricorn Orogen basins (Fig. 6). The presence of a c. 2015 Ma granitic rock in

0

1

2

3

4

5

6

-18

-14

-10

-6

-2

2

6

10

1600 2000 2400 2800

DalgaringaSupersuite

Capricorn OrogenBasins

Rudallinheritance

3200

Age (Ma)

His

tog

ram

freq

uen

cy

Ep

silo

n H

f

CLK98 27.03.13

Figure 6. Hf evolution diagram for inherited zircons from

Rudall Province intrusive rocks (green circles)

compared to potential West Australian Craton

source regions (yellow and blue triangles). The

histogram shows 207Pb*/206Pb* ages of inherited

zircons from Rudall Province intrusive rocks.

The isotopic signature of the inherited material is

consistent with generation from crust similar to

that in the Capricorn Orogen. Lines define fields

for evolution of a source with similar composition

to zircons in basins of the Capricorn Orogen (dash)

and Dalgaringa Supersuite (dash-dot). The red line

is model depleted mantle and the blue line is CHUR.

the province, here reinterpreted as a Kalkan Supersuite granite with abundant c. 2015 Ma-aged inherited zircons, led Clark (1991) and Bagas (2004) to suggest that the Glenburgh Terrane of the Gascoyne Province may form basement to the Talbot Terrane, since rocks of this age have not been documented in the Arunta Province. A recent deep crustal seismic reflection survey through the western part of the Capricorn Orogen (Johnson et al., 2011b), however, indicates that the Glenburgh Terrane is sutured to the southern margin of the Pilbara Craton along a southeast-trending, south-dipping suture zone (Fig. 1; the Lyons River – Minga Bar – Minnie Creek Fault System). The orientation of this suture means that the Glenburgh Terrane is progressively truncated toward the east against the northern margin of the Yilgarn Craton, making it highly unlikely that this terrane forms basement to any part of the Rudall Province.

The similarity in isotopic composition and age of inherited zircons within granitic rocks of the Kalkan Supersuite with detrital zircons in sedimentary rocks in the Capricorn Orogen (Fig. 6) suggests that the Kalkan Supersuite granites may have assimilated similar sedimentary material during their emplacement into the upper crust. The sedimentary rocks of the eastern association of the Talbot Terrane were deposited in a similar timeframe to those in the Capricorn Orogen. The similar timing of basin formation during the early stages (c. 1820 to c. 1800 Ma)

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GSWA Report 122 The crustal evolution of the Rudall Province from an isotopic perspective

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of the Capricorn Orogeny imply the development of a single large basin — or a series of smaller linked basins — around the southern and eastern margins of the Pilbara Craton (Fig. 1). Synchronous regional-scale uplift along the southern margin of the Gascoyne Province provided abundant sedimentary detritus that was transported northward into the developing basin(s).

Considering the data presented above, we suggest that:

were derived by the assimilation of sedimentary material during emplacement of the granites into the upper crust

of a wider, regional-scale Capricorn Orogeny-aged basin(s), the detritus for which was derived from upland areas in the southern part of the Gascoyne Province

to the eastern Pilbara Craton margin (e.g. Hickman et al., 1994), consistent with the view presented by Reading et al. (2012) that thinned and extended Pilbara Craton crust occurs as basement beneath the Talbot Terrane

zircons within the Kalkan Supersuite granites are largely influenced by a variety of autochthonous source regions, including the sedimentary successions into which they were intruded.

Hf isotopic signature of the Rudall

Province

The Talbot and Connaughton Terranes are dominated by granitic rocks of the 1800–1765 Ma Kalkan Supersuite. In the Talbot Terrane, magmatic zircon crystals from these rocks show a range of isotopically evolved compositions with model ages (TDM

2) between 3.4 and 2.6 Ga (Fig. 7), whereas in the Connaughton Terrane model ages (TDM

2) range between 3.4 and 2.4 Ga (Fig. 7). The granites contain abundant inherited zircon cores (that were most likely derived from the sedimentary succession into which the magmas were intruded) that have contributed significantly to the isotopic composition of the granitic magmas. The inherited zircons are interpreted to have been derived from the Glenburgh Terrane (specifically the Halfway Gneiss and Dalgaringa Supersuite) of the Gascoyne Province, and the isotopic compositional range of the granites is also comparable to that for the Glenburgh Terrane (Figs. 5 and 6). The most evolved magmatic grains (those with Hf c. –17), however, are also comparable with the isotopic composition of the East Pilbara Terrane, including the granitic rocks of the Bridget Suite (Fig. 5). The lack of East Pilbara Terrane-aged (3500–3200 Ma) inherited zircons within the Kalkan Supersuite indicates that the most evolved isotopic component of the granites may not have been derived as an inherited sedimentary component, but reflect a contribution directly from the underlying Talbot Terrane basement, with an evolved isotopic signature identical to that of the East Pilbara Terrane.

The magmatic zircons from c. 1300 Ma granitic rocks of the Tabletop Terrane are dominated by mildly evolved compositions with model ages of 2.6 Ga. The average 176Yb/177Hf value of zircons from Tabletop Terrane granite sample GSWA 118914 are high to extreme (176Yb/177Hf = 0.100 ± 0.022). However, the average stable 178Hf/177Hf ratio is 1.467241 ± 0.000047 (1SD; n=16), which is within the range of values reported by Thirlwall and Anczkiewicz (2004). The elevated 176Yb/177Hf ratio in this sample, as compared to other typical crustal melts, suggests crystallization either from a strongly fractionated magma or by direct melting of a garnet-bearing source. The Hf isotopic range of the magmatic zircon from the Tabletop Terrane granites is similar to that for the Kalkan Supersuite in the Connaughton Terrane, implying derivation from a similar crustal source.

Crust formation and underplating at

1900 Ma

A post-D2 metamonzogranite in the southern part of the Watrara Inlier in the Talbot Terrane is dated at c. 1450 Ma (GSWA 112102; Nelson, 1996b), and contains zircon crystals with the least evolved Hf isotopic signature in the Rudall Province. The Hf isotopic data indicate that either the granitic material was extracted from the mantle at 1.96 Ga or that it represents a homogenized mix of sources with a component younger than 1.96 Ga. However, oxygen isotopes can be used to determine whether the parental magma from which these zircons grew contained a contribution from near-surface rocks (e.g. those with 18OVSMOW >6.3 ‰). This provides a means to screen the corresponding Hf model age for supracrustal contamination into the magma and to identify a model age that represents a mixing of source materials rather than a discrete crust-forming episode. Whereas zircon in equilibrium with mantle-derived melts has a 18OVSMOW value of 5.3 ± 0.6 ‰ (2 SD; Valley, 2003), incorporation of high- 18O material (i.e. rocks or minerals altered by low-temperature near-surface processes) will increase the

18O value of a melt, so that zircons crystallized from such melts will also have elevated 18O values. Oxygen isotope values for all zircons from this sample (Table 2) are within the mantle zircon field (Fig. 8); hence, the 1.96 Ga model age likely reflects a crust-forming fractionation event in the lithosphere.

Further constraint on the location of this fractionation event can be placed by examining the isotopic signature of this sample. The average 176Yb/177Hf values of zircon crystals from GSWA 112102 are high (176Yb/177Hf = 0.085 ± 0.012; Fig. 9). However, during the course of the analysis of this sample, the average 178Hf/177Hf ratio was 1.467168 ± 0.000051 (1SD; n=8), which is in the range of values reported by Thirlwall and Anczkiewicz (2004), indicating that Yb interference has been satisfactorily dealt with. Hence, the elevated 176Yb/177Hf ratio in these zircon crystals could imply anatexis of residual garnet (Fig. 9).

There is only limited additional evidence for crust formation at c. 1.9 Ga in the West Australian Craton and its marginal terranes. Magmatic and metasedimentary rocks of the Musgrave Province are dominated by two major juvenile Proterozoic crust formation events —

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uen

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ram

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uen

cy

CLK78 05 2 3.0 .1

�Hf < 5–

�Hf 0 to 5–

�Hf >0

Figure 7. Magmatic crystallization ages (left) and two-stage Hf model ages (right) for zircons from

Rudall Province magmatic rocks. Crystallization age data are colour-coded according to

Hf value. Although the timing of magmatism in the Tabletop Terrane is different from that

in the Connaughton and Talbot terranes, the Hf isotopic signatures of all three are broadly

similar, implying that each originated from the same, or a similar, crustal source.

4.0

4.2

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4.6

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6.0

Mean = 5.23 ± 0.12δ18

O

MSWD = 2.1

δ18

OZ

irco

nV

SM

OW

CLK99 28.03.13

Figure 8. Oxygen isotope analyses of zircons from

Mesoproterozoic metamonzogranite sample GSWA

112102 (Nelson, 1996b). Error bars are 2 . Analyses

located on fractures or inclusions are excluded. The

line indicates the weighted mean 18O value for

the analysed zircons; the grey field represents the

range of values expected from zircon crystallized

in equilibrium with the mantle (5.3 ± 0.6 ‰ (2 SD),

e.g. Valley, 2003).

0.00

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Age (Ma)

176

177

Yb

/H

f

GSWA118914

GSWA118914

All otherRudallanalysis

CLK76 28.03.13

Figure 9. Comparison of 176Yb/177Hf ratios for zircons from

two Mesoproterozoic magmatic rocks (circles) with

those from other Rudall Province magmatic rocks

of Paleoproterozoic age (squares). The zircons in

Mesoproterozoic rocks have elevated Yb contents

compared to most of those in Paleoproterozoic

rocks.

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one at 1600–1550 Ma and a more significant event at 1950– 1900 Ma (Kirkland et al., 2013). Although no juvenile rocks or minerals are known from c. 1900 Ma in the Musgrave Province, addition of radiogenic material into the crust at this time is required to account for consistent Nd and Hf evolution patterns that show no indication of mixing processes, and mantle-like oxygen isotope signatures in zircons with 1.9 Ga model ages (Kirkland et al., 2013).

The Edmund Basin is an intracratonic sedimentary basin of early Mesoproterozoic age located between the Pilbara and Yilgarn Cratons (Fig. 1). Metasedimentary strata of the Edmund Group are intruded by voluminous mafic sills of the c. 1465 Ma Narimbunna Dolerite (Martin and Thorne, 2004). Hf isotopes in baddeleyite and zircon crystals from this magmatic suite consistently suggest a juvenile source component formed at 1950–1900 Ma (GSWA, unpublished data). Whole-rock Nd isotopes from these rocks also yield model ages (TCHUR) with a mode of 1.9 Ga (Morris and Pirajno, 2005).

Isotope data for c. 1450 Ma magmatic zircons in Talbot Terrane monzogranite sample GSWA 112102 fall directly on a normal-crustal evolution line from a c. 1900 Ma crust-formation event. This is also the case for isotope evolution in rocks of the Musgrave Province and the Edmund Basin. At c. 1.9 Ga, the timing of this crust formation event is unusual within Proterozoic Australia and supports the idea of an extensive 1.9 Ga underplate beneath these regions.

Constraints on the tectonic

evolution of the Rudall Province

Metasedimentary rocks of the eastern association in the Talbot and Connaughton Terranes have a similar structural and metamorphic history to the northern and central Arunta Orogen (Collins and Shaw, 1995; Bagas, 2004; Claoue-Long and Hoatson, 2005), and this has been considered as evidence that the Rudall Province and Arunta Orogen formed part of the North Australian Craton prior to the Yapungku Orogeny (Bagas, 2004; Fig. 10). However, it appears that the Rudall Province has more in common with a Capricorn Orogen source than it does with the Arunta Orogen.

The Arunta Orogen contains 1690–1670 Ma magmatic rocks, whereas those in the Rudall Province are dominated by the 1800–1765 Ma Kalkan Supersuite. With regard to the age of crustal residence within these terranes, only the Connaughton Terrane has somewhat similar model ages to the Aileron Province of the Arunta Orogen (Kirkland et al., 2013), implying that this terrane could have a North Australian Craton heritage. However, the U–Pb age and Hf isotopic signature of inherited

YapungkuOrogeny

YambahEvent

ChewingsEvent

1200 1400 1600 1800 2000

MutherbukinTectonic Event

CapricornOrogeny

StaffordEvent

LiebigOrogeny

MangaroonOrogeny

GlenburghOrogeny

Argilke lgneousEvent

StrangwaysEvent

GascoyneArunta Rudall

Magmatic

Metamorphic

Tectonicdomains

Aru

nta

Oro

ge

n

Age (Ma)

Ga

sc

oy

ne

Pro

vin

ce

Ru

da

ll P

ro

vin

ce

Wa

rum

pi P

rovin

ce

Boora Boora Zone

Margaroon Zone

Lime Juice Zone

Mutherbukin Zone

Mooloo Zone

Paradise Zone

Table Top

Connaughton

Talbot

West

Yaya

Kintore

Haasts Bluff

Camel–Tabletop Fault Zone

Vines–Southwest–Mckay Faults

CLK79 14.06.13

Aile

ron

Pro

vin

ce

Figure 10. Time-space diagrams showing magmatic and

metamorphic U–Pb ages for the Gascoyne Province,

Rudall Province, and Arunta Orogen. Data include

all GSWA U–Pb zircon and baddeleyite ages <www.

dmp.wa.gov.au/geochron> and Arunta Orogen data

compiled in Neumann and Fraser, (2007).

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zircons within all the Kalkan Supersuite granites, from both terranes, are most similar to sources in the West Australian Craton, in particular the Glenburgh Terrane in the southern part of the Gascoyne Province (Fig. 1). The presence of 2.0 and 1.8 Ga inherited zircons are consistent with the magmatic rocks of the Kalkan Supersuite having incorporated material from metasedimentary rocks of the eastern association, which was deposited in a similar timeframe to the Capricorn Orogeny-aged basins. The presence of 2715–2577 Ma-aged inherited zircons in a syenogranitic gneiss of the Talbot Terrane (GSWA 104932, Nelson, 1995a) are consistent with their derivation from the Fortescue and Hamersley Groups of the Pilbara Craton. The Hf isotopic evolution of granitic rocks within the Talbot and Connaughton Terranes also implies the involvement of unradiogenic crust, probably as basement to the sediments of the eastern succession (Fig. 5). This crust likely had a composition similar to that of the East Pilbara Terrane, consistent with the recent results of passive seismic study across the province, which suggests that thinned East Pilbara Terrane crust extends as basement beneath the western part of the Rudall Province (Reading et al., 2012), thus implying an autochthonous setting for the Talbot Terrane.

The Tabletop Terrane has been regarded as geologically distinct from the Connaughton and Talbot Terranes (Bagas, 2004). However, crust within the Tabletop Terrane appears to have been generated at the same time as that in the Connaughton Terrane and also from a similar source to inheritance in the Talbot Terrane (Fig. 7). It has, however, a distinct magmatic and overprinting history.

In addition, the Paleoproterozoic isotope evolution of the Rudall Province is different from that of the Musgrave Province (Fig. 5). The isotopic composition of the Rudall Province lies mainly in the gap between the 3.0 and 1.9 – 1.6 Ga crustal evolution lines that are characteristic of the Musgrave Province, implying that the crust of the two provinces is broadly dissimilar (Fig. 5). The Archean source within the Musgrave Province is unidentified, although it could be the Gawler Craton (Kirkland et al., 2013). This Archean component overlaps the array from the most unradiogenic components of the Talbot and Connaughton Terranes, although such a signature is common to many Archean crustal blocks.

These data imply an autochthonous setting for the Rudall Province on the margin of the East Pilbara Terrane, and do not necessitate any connection to the Arunta Orogen, the North Australian Craton or the Musgrave Province. Therefore, a model of suturing at 1800–1765  Ma of an allochthonous block (Arunta Orogen) of the North Australian Craton to the Pilbara Craton margin is inconsistent with the distinctly different post-1765 Ma tectonic histories of these two regions (Neumann and Fraser, 2007). Such a model predicts a shared history of post-suturing events. Although the Arunta Orogen records late Paleoproterozoic tectonic events such as the 1680– 1650 Ma Argilke tectonic event and the 1620– 1580  Ma Chewings Orogeny (Claoue-Long and Hoatson, 2005), no contemporaneous events are known in the Rudall Province.

Implications for terrane

boundaries

The 1800–1765 Ma Yapungku Orogeny is considered to represent collision of the North Australian Craton with the West Australian Craton. Isotope data demonstrate that the Rudall Province is a (para)autochthonous assemblage that developed on the eastern margin of the Pilbara Craton. Such a finding is consistent with the initial interpretation, based on regional 1:250 000 scale geological mapping, that the >5-km-thick clastic succession of the Talbot Terrane was deposited on the eastern margin of the Pilbara Craton, and immediately thereafter was intruded by the Kalkan Supersuite during southwest-directed thrusting (Hickman et al., 1994; Hickman and Bagas, 1995; Bagas and Smithies, 1997; Hickman and Bagas, 1999a). Therefore, the suture zone between the North and West Australian Cratons should be located to the east (in present-day coordinates) of the province. The Connaughton Terrane was thrust westwards over the Talbot Terrane during the latter stages of the Yapungku Orogeny (Bagas, 2004).

The Camel–Tabletop Fault (Bagas and Lubieniecki, 2000) is a post-Yapungku structure, along which pieces of the same crustal block were reorganized. The timing of reworking in the Tabletop Terrane is similar to that of Mesoproterozoic events in the Musgrave Province. Magmatism at c. 1450 Ma in the Talbot Terrane appears to have tapped a more radiogenic source, in contrast to all other magmas of the Rudall Province. This radiogenic source shares similarities to the isotopic signature of the Musgrave Province, with a dominant isotopic crust formation age of c. 1900 Ma. Narimbunna Dolerites in the Mesoproterozoic Edmund Basin of the Capricorn Orogen (Fig. 1), also indicate a juvenile source formed at 1950–1900 Ma. The potential of a c. 1900 Ma source in the basement of the Rudall Province, Edmund Basin and Musgrave Province could support a regional underplate of this age in the deep geology of the West Australian Craton. Such a structure could indicate a c. 1950–1900 Ma subduction zone dipping and underplating oceanic crust towards the present-day southwest. Nonetheless, the crustal source of the Kalkan Supersuite is vastly different from the crust of the Musgrave Province, which implies at least some dissimilar basement components within these two regions.

Conclusions

The U–Pb age and Hf isotopic composition of inherited zircons within Kalkan Supersuite granitic rocks throughout the Rudall Province are consistent with these magmas incorporating material from sedimentary rocks that were sourced from the Glenburgh Terrane of the Gascoyne Province. The >5-km-thick eastern association of sedimentary rocks in the Talbot Terrane were deposited at c. 1790 Ma, in a similar timeframe to other sedimentary rocks in the Capricorn Orogen, which were also sourced from the Glenburgh Terrane. This suggests that during the 1800–1765 Ma Yapungku Orogeny and 1820–1770 Ma

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Capricorn Orogeny, the southern margin of the Gascoyne Province was uplifted to supply detritus into an extended sedimentary basin, or series of linked basins, that wrapped around the southern and eastern margins of the Pilbara Craton.

The Hf isotopic composition of magmatic zircons in the Kalkan Supersuite has similarity to components within the c. 1800 Ma Bridget Supersuite of the East Pilbara Terrane. This implies that the East Pilbara Terrane extends eastward to form basement to the Talbot and Connaughton Terranes, a view supported by a recent passive seismic study of the area (Reading et al., 2012).

The broad similarity of crustal residence ages for all terranes in the Rudall Province indicates that they share a common heritage, although Mesoproterozoic reworking (infra-crustal magmatism) apparently occurred only in the Tabletop Terrane. These data indicate that the Rudall Province formed in an autochthonous setting and thus all components are endemic to the West Australian Craton. There is no necessity to invoke transfer of North Australian Craton terranes to the West Australian Craton margin or an accretionary style of orogenesis for the Rudall Province. The major suture between the North and West Australian Cratons must lie to the present-day east of the Rudall Province.

A younger phase of crust formation at 1.96 Ga is indicated by Hf isotopes of a c. 1450 Ma monzogranite in the Talbot Terrane. This isotope signature appears to be similar to a dominant basement component in the Musgrave Province.

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This Report outlines the crustal evolution of the Rudall Province,

with particular emphasis on the development of the Talbot and

Connaughton Terranes. Components within the Rudall Province have

been linked to the Arunta Orogen of the North Australian Craton

and hence regarded as exotic terranes on the margin of

the West Australian Craton. This work presents

time constrained Hf isotopes to elucidate

the affinity of the Rudall Province and

refine models for its genesis. The

Rudall Province is divided into three

lithotectonic elements known as the

Talbot, Connaughton, and Tabletop

Terranes. The Talbot and Connaughton

Terranes were affected by magmatism

produced during the collision between

the West and North Australian Cratons at

1800–1765 Ma. Zircons within granitic rocks

related to this event indicate crustal residence

ages of 3.4 – 2.4 Ga, which have similarity

to crustal sources with the basement of the

Capricorn Orogen. Additionally, the Hf

isotopic signature of the Rudall Province has similarity to components

of the c. 1800 Ma Bridget Suite, which has a clear association to

the Pilbara Craton. Hence, sources for most isotopic compositions

preserved within the Rudall Province are present within the proximal

West Australian Craton and an exotic origin for the Rudall Province is

unlikely. A distinctive phase of crust formation at 1.9 Ga in the Talbot

Terrane implies an affinity to a major deep lithospheric source of

similar age in the Musgrave Province and could indicate a regional

underplate of this age.

Further details of geological products and maps produced by the

Geological Survey of Western Australia are available from:

Information Centre

Department of Mines and Petroleum

100 Plain Street

EAST PERTH WA 6004

Phone: (08) 9222 3459 Fax: (08) 9222 3444

www.dmp.wa.gov.au/GSWApublications