O lin 3855 NORTH OCOEE STREET SUITE 200 CLEVELAND TN 37312

OFFICE (423) 336-4000 FAX (423) 336-4166

February 10 2010

Wilmington MA 01887

Re Residential Well Sampling Program

Dear

Please find enclosed the data validation summary and laboratory analytical data from the independent laboratory that analyzed the water sample collected in November 2009 from your home In the attached information references to samples that were not collected from your property have been blacked out to avoid confusion Also enclosed is a review by the consultant that has been retained to review all data that is related to human health that might be associated with the Olin facilities located at 51 Eames Street

As you can see from the report there are two analytes detected outside of their regulatory standard or guideline

NDMA was detected at a concentration of 0000017 milligrams per liter (mgL) which is slightly above the Massachusetts Depaltment of Environmental Protections (MassDEP) Office of Research and Standards guideline limit of 00000 1 mgL in drinking water supplies MassDEP recommends that a well exceeding a guideline limit be re-sampled

Sodium was detected in your well at a maximum concenhation of 28 mgL compared to the MassDEP Office of Research and Standards guideline limit of 20 mgL in drinking water

Should there be any questions after you review this information you can call the facility at (978) 658shy6121 Inform them that you would like for me to call you and I will retuITI your call

Sincerely

Steve Morrow Principal Environmental Specialist

cc Jim DiLorenzo USEPA

POLfNWilmingtonPrivate November 2009 Letter to ResidenlNOV2009doc o L - I NCO R P 0 RAT ION

REDACTED

~MACTEC engineering and constructing a better tomorrow

February 8 20 I 0

Mr Steve Morrow Olin Corporation 3855 orth Ocoee lreet Suite 200 Cleveland TN 37312

Subject Residential Well Sampling 51 Eames Street Facility

Dear Mr Morrow

Pcr your requcst MACTEC Engincering and Consulting Inc has evaluated the ~hcmical data for

the water samp le collected in November 2009 fr 111 the residence in Wilm ington undcr

Olins rcsidcntial wcll sampling program This evaluntion wa performed to confirm tile suitability

of drinking water at the residential propel1y Chemical concentrations in the well water were

compared to Mas achusetts and federal drinking water tandards and guidelines

Attached is a table summarizing well monitoring data for the residence The ample was

analyzed for volatiles semi-volatiles inorganics the mctals calcium chromium and sodium

formaldehyde and acctaldchyde hydraLines n-nitrosodimclh laminc (NDIIA) and n-nitrosodi-nshy

propyl-amine (NDPA) The table lists all detected analytes and their associated concentrations

The appropriate standard andor guidclinc for each parameter is provided for com pari on

Two analtes were detected at a concentration above their respective sta ndard andlor guideline

Sodilllll was detected in the Stanley residential well at a concentration of 28 III ill igrallls pcr liter

(lllgiL) (27 mglL in the dupli~ate sample) compared to the OrJicc of Research and Standards

guideline limit or20 mglL

NDMA was detccted at a concentration of 0000017 mgL which is slightly greater than the

Massachusetts Department of Environmental Protections (lvlassDEP) i sLlcd guideline limit or

00000 I mgL in drinking ater supplies

MassDEP recommend that a ell exceeding a guidelinc limit be rc-sampled so thi is sugge led

forNDIvlA

MACTEC Engineering and Consulting Inc 107 Audul)11 R(Jnd Bldq 1 )l ilt 30 I bull W(J~f leld 1M 01880 bull Phone 812456606 bull fox 1812465060 wwwmocteccom

REDACTED

~MACTEC engineering and constructing a better tomorrow

February 8 20 I 0

Mr Steve Morrow Olin Corporation 3855 orth Ocoee lreet Suite 200 Cleveland TN 37312

Subject Residential Well Sampling 51 Eames Street Facility

Dear Mr Morrow

Pcr your requcst MACTEC Engincering and Consulting Inc has evaluated the ~hcmical data for

the water samp le collected in November 2009 fr 111 the residence in Wilm ington undcr

Olins rcsidcntial wcll sampling program This evaluntion wa performed to confirm tile suitability

of drinking water at the residential propel1y Chemical concentrations in the well water were

compared to Mas achusetts and federal drinking water tandards and guidelines

Attached is a table summarizing well monitoring data for the residence The ample was

analyzed for volatiles semi-volatiles inorganics the mctals calcium chromium and sodium

formaldehyde and acctaldchyde hydraLines n-nitrosodimclh laminc (NDIIA) and n-nitrosodi-nshy

propyl-amine (NDPA) The table lists all detected analytes and their associated concentrations

The appropriate standard andor guidclinc for each parameter is provided for com pari on

Two analtes were detected at a concentration above their respective sta ndard andlor guideline

Sodilllll was detected in the Stanley residential well at a concentration of 28 III ill igrallls pcr liter

(lllgiL) (27 mglL in the dupli~ate sample) compared to the OrJicc of Research and Standards

guideline limit or20 mglL

NDMA was detccted at a concentration of 0000017 mgL which is slightly greater than the

Massachusetts Department of Environmental Protections (lvlassDEP) i sLlcd guideline limit or

00000 I mgL in drinking ater supplies

MassDEP recommend that a ell exceeding a guidelinc limit be rc-sampled so thi is sugge led

forNDIvlA

MACTEC Engineering and Consulting Inc 107 Audul)11 R(Jnd Bldq 1 )l ilt 30 I bull W(J~f leld 1M 01880 bull Phone 812456606 bull fox 1812465060 wwwmocteccom

REDACTED

Olin 5 I Eames Street Wilmington AlA - ResidentiallVefl Sampling Fehruw) 82010 IvACTEe Engineering and Consulting Inc Project Number 607- 10-0016 Page 2

If you have any questions about the evaluation or if you require additional information please feel

free to contact Michael Murphy at (781) 245-6606

Sincerely MACTEC Engineering and Consulting Inc

I ~ itlff Maim

for ~r rhomps~ Michael J Murphy Project Manager with permission Sr Principal Environmental Scientist

Attachment

cc MACTEC Project File lP hI07 ItI(I0 16middot 0 Ltn WilmJnSlO CSS24I1l ojlaquot MlttaampmKSJ Adtllinlslr tioln 1 ~COt1iSflodulcI l ~ 1 1 (tleu FcI)

~IACTEC Engineering and Consulting Inc 107 AuuuooJl Road Suile 30 1

Wal-elicld MA 01880 Tel (78 I ) 245-6606 bull Fa~ (78 1) 246-5060

REDACTED

SUMMARY OF PRIVATE RESIDENCE WELL MONITORING DATA1 AND COMPARISON TO FEDERAL AND MASSACHUSETIS DRINKING WATER STANDARDSGUIDELINES

RESIDENCE

Sample Drinking Water Type of Parameter Results2 Units StandardlGuideline StandardGuideline Volatiles Methyl tert-butyl ether 0002 mgL 007 ORSG Semi-Volatiles None Detected -- -- -- --Inorganics Calcium 47 mgL NS -shySodium 28 mglL 20 ORSG Chloride 72 mgL 250 SMCL Sulfate 27 mgL 250 SMCL N-Nitrosodimethylamine 0000017 mgL 000001 ORSG N-Nitrosodi-n-propyl-amine Not Detected - -- - --FormaldehydeAcetaldehyde None Detected - -- -- --Hydrazines None Detected -- -- -- -shy

Prepared bylDate KASK 1212309 Notes Checked byDate BJR 11310 - Results are non-detect NS - No standard or guideline available SMCL - Federal and Massachusetts Secondary Maximum Contaminant Level - USEPA 2009 MassDEP 2009 mgL - milligrams per liter ORSG - Massachusetts Drinking Water Guideline - MassDEP 2009

1 Data were collected in November 2009 Shading indicates a concentration greater than the standardlguideline for that parameter

2Data reported are the maximum detected concentration between the original and duplicate samples

Massachusetts Department of Environmental Protection (MassDEP) 2009 2009 Standards and Guidelines for Contaminants in Massachusetts Drinking Water

USEPA 2009 2009 Edition of the Drinking Water Standards and Health Advisories EPA 822-R-09-011

POllNWilmingtonPrivatel lNovember 2009 _November -09 _ TABSheet1 Page 1 of 1

REDACTED

REDACTED

To From Chris Ricardi

Site

Data Validation Test America Data Slts 360-25526-1 and 360-25526-2 Lancaster Date Set OLN25A (i 170551)

10 Introduction

set contains results fi)f residential well Test America Laboratories Method 831 alld West

Method 260B USEPA Mcth~l(l 8270C

15A

USEPA Method

modified

mcluded i1 this nvitw arc sUlHlmlrized on results an the methods listed above

the Olin final

20 NUMANHPA

REDACTED

Validation checks met and method

21 Validation Observations and Actions

There were no data and arc the

30 Volatile

that criteria wen mel

31 Validation Observations ilfld Actions

REDACTED

40 Semiyoiatiilts

and Technical Times GClMS Instrument Perfonmmcc Check Initial Calibration

Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

and OC-M24L54~DUP were

1) a not

REDACTED

TICs

ill and method blank as discussed above under

acid for

50

1--17 were reviewed criteria described in tJSEPA data validation

data validation

Initial Calibration Verification Verification

all

Validation Observations and Actions

laent fied data validation and results bt usable

60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

no data validation and results usable the

70 Metals

Times

that all met

71 Validation Observations and ctions

daw validatioH an

REDACTED

811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

P Prcgt(~tsdtn lmmiddot~ YIOlifcJM CSS 2~ O_Sot9 OataJ _lcllJ_03IdlRM JPOI-t leN Pogram ton~mber 2t)(9 ttfllO-2S516 h)ampgt 1 xl~ Tett I~ Page I of J

REDACTED

SUMMARY OF PRIVATE RESIDENCE WELL MONITORING DATA1 AND COMPARISON TO FEDERAL AND MASSACHUSETIS DRINKING WATER STANDARDSGUIDELINES

RESIDENCE

Sample Drinking Water Type of Parameter Results2 Units StandardlGuideline StandardGuideline Volatiles Methyl tert-butyl ether 0002 mgL 007 ORSG Semi-Volatiles None Detected -- -- -- --Inorganics Calcium 47 mgL NS -shySodium 28 mglL 20 ORSG Chloride 72 mgL 250 SMCL Sulfate 27 mgL 250 SMCL N-Nitrosodimethylamine 0000017 mgL 000001 ORSG N-Nitrosodi-n-propyl-amine Not Detected - -- - --FormaldehydeAcetaldehyde None Detected - -- -- --Hydrazines None Detected -- -- -- -shy

Prepared bylDate KASK 1212309 Notes Checked byDate BJR 11310 - Results are non-detect NS - No standard or guideline available SMCL - Federal and Massachusetts Secondary Maximum Contaminant Level - USEPA 2009 MassDEP 2009 mgL - milligrams per liter ORSG - Massachusetts Drinking Water Guideline - MassDEP 2009

1 Data were collected in November 2009 Shading indicates a concentration greater than the standardlguideline for that parameter

2Data reported are the maximum detected concentration between the original and duplicate samples

Massachusetts Department of Environmental Protection (MassDEP) 2009 2009 Standards and Guidelines for Contaminants in Massachusetts Drinking Water

USEPA 2009 2009 Edition of the Drinking Water Standards and Health Advisories EPA 822-R-09-011

POllNWilmingtonPrivatel lNovember 2009 _November -09 _ TABSheet1 Page 1 of 1

REDACTED

REDACTED

To From Chris Ricardi

Site

Data Validation Test America Data Slts 360-25526-1 and 360-25526-2 Lancaster Date Set OLN25A (i 170551)

10 Introduction

set contains results fi)f residential well Test America Laboratories Method 831 alld West

Method 260B USEPA Mcth~l(l 8270C

15A

USEPA Method

modified

mcluded i1 this nvitw arc sUlHlmlrized on results an the methods listed above

the Olin final

20 NUMANHPA

REDACTED

Validation checks met and method

21 Validation Observations and Actions

There were no data and arc the

30 Volatile

that criteria wen mel

31 Validation Observations ilfld Actions

REDACTED

40 Semiyoiatiilts

and Technical Times GClMS Instrument Perfonmmcc Check Initial Calibration

Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

and OC-M24L54~DUP were

1) a not

REDACTED

TICs

ill and method blank as discussed above under

acid for

50

1--17 were reviewed criteria described in tJSEPA data validation

data validation

Initial Calibration Verification Verification

all

Validation Observations and Actions

laent fied data validation and results bt usable

60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

no data validation and results usable the

70 Metals

Times

that all met

71 Validation Observations and ctions

daw validatioH an

REDACTED

811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

P Prcgt(~tsdtn lmmiddot~ YIOlifcJM CSS 2~ O_Sot9 OataJ _lcllJ_03IdlRM JPOI-t leN Pogram ton~mber 2t)(9 ttfllO-2S516 h)ampgt 1 xl~ Tett I~ Page I of J

REDACTED

REDACTED

To From Chris Ricardi

Site

Data Validation Test America Data Slts 360-25526-1 and 360-25526-2 Lancaster Date Set OLN25A (i 170551)

10 Introduction

set contains results fi)f residential well Test America Laboratories Method 831 alld West

Method 260B USEPA Mcth~l(l 8270C

15A

USEPA Method

modified

mcluded i1 this nvitw arc sUlHlmlrized on results an the methods listed above

the Olin final

20 NUMANHPA

REDACTED

Validation checks met and method

21 Validation Observations and Actions

There were no data and arc the

30 Volatile

that criteria wen mel

31 Validation Observations ilfld Actions

REDACTED

40 Semiyoiatiilts

and Technical Times GClMS Instrument Perfonmmcc Check Initial Calibration

Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

and OC-M24L54~DUP were

1) a not

REDACTED

TICs

ill and method blank as discussed above under

acid for

50

1--17 were reviewed criteria described in tJSEPA data validation

data validation

Initial Calibration Verification Verification

all

Validation Observations and Actions

laent fied data validation and results bt usable

60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

no data validation and results usable the

70 Metals

Times

that all met

71 Validation Observations and ctions

daw validatioH an

REDACTED

811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

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Data Validation Test America Data Slts 360-25526-1 and 360-25526-2 Lancaster Date Set OLN25A (i 170551)

10 Introduction

set contains results fi)f residential well Test America Laboratories Method 831 alld West

Method 260B USEPA Mcth~l(l 8270C

15A

USEPA Method

modified

mcluded i1 this nvitw arc sUlHlmlrized on results an the methods listed above

the Olin final

20 NUMANHPA

REDACTED

Validation checks met and method

21 Validation Observations and Actions

There were no data and arc the

30 Volatile

that criteria wen mel

31 Validation Observations ilfld Actions

REDACTED

40 Semiyoiatiilts

and Technical Times GClMS Instrument Perfonmmcc Check Initial Calibration

Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

and OC-M24L54~DUP were

1) a not

REDACTED

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50

1--17 were reviewed criteria described in tJSEPA data validation

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laent fied data validation and results bt usable

60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

no data validation and results usable the

70 Metals

Times

that all met

71 Validation Observations and ctions

daw validatioH an

REDACTED

811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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Validation checks met and method

21 Validation Observations and Actions

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31 Validation Observations ilfld Actions

REDACTED

40 Semiyoiatiilts

and Technical Times GClMS Instrument Perfonmmcc Check Initial Calibration

Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

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60

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m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

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61 Validation Observations and Actions

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that all met

71 Validation Observations and ctions

daw validatioH an

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811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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40 Semiyoiatiilts

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Results

Recoveries

Internal Standard Area and Retention Time Results

Caleulation Verification Electronic Database Review

that all criteria were met for control

41 Validation Observations lind Actions

The response validation value

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1--17 were reviewed criteria described in tJSEPA data validation

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60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

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71 Validation Observations and ctions

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811 Anions nitrate and and Ammonia

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that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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60

REDACTED

m

Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

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70 Metals

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71 Validation Observations and ctions

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811 Anions nitrate and and Ammonia

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for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

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Raw data review and calculation checks Detection Limi[ Review Electronic Oaw Verification

Validation checks met and

61 Validation Observations and Actions

no data validation and results usable the

70 Metals

Times

that all met

71 Validation Observations and ctions

daw validatioH an

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811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

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811 Anions nitrate and and Ammonia

m

that all criteria

There were no data and results arc to he usable as the

for the validation actions noted the results are to be usable TestAmerica

REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

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Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

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REDACTED

References

EPA-NF )((1lt- Data Validation Assurance

REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

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REDACTED

Table 1 Sample Summary - 36025526

Data Validation Report November 2009 Residential Sampling

Oln Chemical Superfund Site Wilmington Massachusetts

RED

ACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

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Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

P Prcgt(~tsdtn lmmiddot~ YIOlifcJM CSS 2~ O_Sot9 OataJ _lcllJ_03IdlRM JPOI-t leN Pogram ton~mber 2t)(9 ttfllO-2S516 h)ampgt 1 xl~ Tett I~ Page I of J

REDACTED

-

II IIO O

Table 2 Final Res ul ts Summ ary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massach usetts

Lue Ntmt ~ 1 middot~lILmiddotimiddot1 Mmiddot241middotj4

FielJ Samp le ID OC-Ml~L51 OC-~I~~1s4middotDlJr ~

Fie ld Sample DlIe II IOmiddot) 1III0 Oq

QC CoO FS FD FS

Lab Sl1Ip l Deli very C rou l 360middot15526middot1 360-25j~6- 1 360-1556-1 Frnc ~ l rth oJ II ~ I~ te- UnU s Result Q1ilier Rtsult Ouirr Result Quahfier N $W816O 11 I 2-Tctnchlocoltdane ugll I U IU IU N 5W8160 11 I-Trichloroethane ugll I V IV IU N 5W8160 1122-TwochlorOltIhe ugll 05 V 05 U 05 V N $W8260 1 12-Tnchloro-l12middotfnnuoroelhane ugll IV I U I U N SWR2GO 11-Tnd orocthJnlt ugll IU I U I U N 5W8260 I I -Dichloroelhane ugll r V I V IlJ N SWSl60 1 ImiddotDichlorOClhene ugll l U I lJ lU N $W826O 1IDlChloropropene ugll I V I U I U N 5W8260 12J-Tndlorobtn7cnlt ugll I U I U I U N SIV8260 123-TricltloroprOp1I1C ugll I U I V I U N S8260 124-Trichlorobrnzenlt ugll I U I U I U N SW~260 124-Trimetll)lbenzenc ugll I U I U I U N $W8160 12-DibroIllO-]-chl0nllgtO plne uWl 5 U 5 U 5 U N 5W8260 12 Dlbrollloelhane ugll I U I U I U N 5W8260 12DithIOrobcruen ugll I U I U I U N 5W8260 12middotDichl oroethanc ugll I U I U I U N 5W8260 l lmiddotDichloropropanc ugll I U I U I U N SW8260 135-Trimelhylbcnzenr ugfl I U I U I U N 5W8260 13middotDichlorobenzene 1I g1 I U I U I U N SW8260 1]middotDithloropropJIIC uYi I U I U I U N 5W8260 14middotDichlorobcnzellC ugfl I U IU I U N SW8l6O 14middotDioane ugI 50 U 50 U 50 U N SW8260 11middotDichloropropane ugll I UJ I UJ I UJ N 5W8260 2044-Trimchyl- l-penccnc ugl IU I U I U 1 $118260 2I4-Trimethyl--Perltne ugll I U I U IU N 5118260 2-Butanonc ugll 10 U 10 U 10 U N 5118260 2-Ch lorotoluenc ugll I U I U IU N SW8160 2~Hc(anonc ugll 10 U 10 U 10 U N SW8260 4-Chlorololuene ugI I U IU I U N 5W8260 4-wmiddotPropyholuene 110 IU IU I U N 5W8260 ~-Mcthy l 2-pcllt3l1l11lt ugll 10 U 10 U 10 U N SW8260 Acetic acid methy l ester Itgll 10 U 10 U 10 U N 5W8260 Ace lone ugI 50 U SO U 50 U N $W8260 BCIl7enc ugfl I U I U I U N 5W826O Bromobcnlcl1o UWI I U I U I U N 5W826O OronlOChlorolJlcthanc ugll I U I U I U N 5118260 Ilfl)OlodichloTOI1lC h~1C UWI I U I V I U N 5118260 Bromofoml uyl I U IU I U N SW3260 Orolllornetl13ne ugll 2 U UJ 2UJ N SWSl60 Butane 2-llIelhoxy-lmiddotmeth) Ishy ugll 5 UJ S U 5 UJ N W826O CUbon disulfide ugl 10 U 10 U 10 U N 58260 Cbon ItlrachloriJc lid I U IU I U N 5118260 n lorobcll7clle ugI I U I U I U N SW8260 CIlorodibroIllOntcth~ ugll 05 U 05 U 05 U N SWS260 ctlortlltthane ug I 2 U 2 U 1 U N 5W8260 (liorofonn ugll 1 U IU IU N SW8260 CIlorollltlhlltC ugll 2 U 2 U 2 U N 5118260 Ci- I 2-Dichlorcethcre Itgl I U I U IU N 5118260 Ct- I 3-Di Ir l oropro~Qe ugll 04 U OA V 04 U N SW826C Cleiohenc ugll 10 U 10 U 10 U N SWS26C DilromomClllJllc UI IU I U I U N SWS260 DlChlorodinuoronet~lIc uyl IU IU I U N $8260 Dilh) I ether Itgll 10 U 10 U 10 U N 513260 Diisopropylethe r ugll 10 U 10 V 10 U N $W8260 Ethyl benzene ugll I U ILl I U N SW826( Ethyl t-Sul)1 Ether uW I UJ 5 UJ 5 UJ N SW8260 Il c~Jch l orobuJicnc ugll 0 1 U 0 1 U 001 U N SW8260 Isopropylbenzcnc ugll I U I V IU N SIVS160 Meuyl cydohane ugl 10 U 10 U 10 U N SW8260 Melhgt1 Tertgtut 1Ltl-tr ugll 2 19 IU N SWR260 Methylene chloride 1Iyen1 2 U 2 U 1 U I 58160 n Butyllxnzcnc ugl I II II) IU

P Prcgt(~tsdtn lmmiddot~ YIOlifcJM CSS 2~ O_Sot9 OataJ _lcllJ_03IdlRM JPOI-t leN Pogram ton~mber 2t)(9 ttfllO-2S516 h)ampgt 1 xl~ Tett I~ Page I of J

REDACTED

gil ugl

45 U 45 U 45 U -4 )

U 45 U

45

45 U

45 U U

Table 2 Final Results Summary

360middot25526 November 2009 Residentia Groundwater Olin Chemical Superfund Site tJilrrington Massachusetts

ugJj

ugr1

REDACTED

Table 2 Final Results Summary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massachusetts

REDACTED

REDACTED

1

REDACTED

Data

OC-MUL54

a2EOS VoaW Organic Compounds

NO

20

REDACTED

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Table 2 Final Results Summary

360-25526 November 2009 Residential Groundwater Olin Chemical Superfund Site Wilmington Massachusetts

REDACTED

REDACTED

1

REDACTED

Data

OC-MUL54

a2EOS VoaW Organic Compounds

NO

20

REDACTED

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

REDACTED

1

REDACTED

Data

OC-MUL54

a2EOS VoaW Organic Compounds

NO

20

REDACTED

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

1

REDACTED

Data

OC-MUL54

a2EOS VoaW Organic Compounds

NO

20

REDACTED

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

OC-MUL54

a2EOS VoaW Organic Compounds

NO

20

REDACTED

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Client S~mplB 10

Preparation

REDACTED

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Volalie Organic Compounds

Tentaliv~ly Idenlficd Compounds o

Anatye Est Result Qualifier

~~efllalively Identified

REDACTED

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Oata

lL SlTljvolatile Compounds by

ul

RlResult

ND ND ND

49

049

REDACTED

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Client

LL 5emivoiatUe Organic Compounds

REDACTED

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Sample

Nummiddot Organic Compounds by GeMSmiddot

Tentatively IdenliUed Compounds Iumber TICs found

636middot67middotlt

FitOMI1C3middotmrlhylmiddot

7225-64middot1 Herladecane 630middot24 14139middot72middot1

638middot68middot6 l1middotpenlylmiddot

REDACTED

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Client Sample ID OC-1l24LM

83i5A Carbonyl Compounds

Dale fldr2eo

Oate f-rep3red ul

REDACTED

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Clienl Smple 10

6l10B Metals

Einalyle

59 NO 13

Sodium 25J

REDACTED

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

as

Ammonia L101middotG6middot1B

REDACTED

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

or-M24L54-0UP

SttOB Volatile

Balch

iGCMSj

Dale PrEpar1

RL

NO

ND NO ND

050 01)1

12-Dibromomiddot3-Chloropropane

12-DcllorrJbelllcnc 1 2middot Dichomelhanc

12 -Dichompropane

135-Tril1elhybenzen l3-Dichmobenzene

NO ND

~m

NlJ

042 OJ5

it

068 054

062

067

051

10

1n

10

50

10 10 if)

HI

to

ND ND

NO ND ND

77

8romcblzenc 11)

ND

REDACTED

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

82eurolJB Volatile Organic

HL

Q24 0 1()

062

IransmiddotlLmiddotOkhlomethenc NO Irans-l )middotOiG~IO(JpfOPelle ND

NO ND

NO

109

REDACTED

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

CHent

82euroOB

Tontatively Itimtificd Compounds

Cas Number

REDACTED

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

n

S27lC II SlrrivolaWe Organic Compounds by - Lew levels

Dile PI1parel

45 7Hexachioroe11ane

amp 4 Meihylphenoj 2 -Chlorophenol Niirooenzem

0+5

NO

J

REDACTED

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Ocata

llZioe Ll Semvolallb Organic Compounds

Jlalyl MDl

8enzolk~uoranthel1C

Benzoapyrene

Indeno[123dlpyien Dibenz(ah)arlhracene Benzolghijperliene Acetophenone

ND NO NO NO NO ~lD

NO ND NO NO

NO NO

NO NO

015

(115

015

0(172

)085

0lt5

O)~-I

027

15

lmiddotMelhyl1aphthalene 1

NO 0045 45

045 OA5

REDACTED

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

OCmiddotMNL54middotCUP

S2iOC Organic Compounds

Tenlltllively Identified CompflImds Nurnber TiCs Found

1 000221middot98middot0 3D

1928middot30middot9

T N 1754 TJN

630lt35 HL24 TJN 722504middot1

REDACTED

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

OC-I12AL54middotlJP

Bl15A Carboryl

NO

REDACTED

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

Client 10 OC-l124LSimiddotCUP

REDACTED

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Data

NO Analysis Balch 360middot51502

ND 11070610 Amiijsis Batch

Prep Batch

REDACTED

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

CHECKED FOR COMPLETENESS OF PARAMETERS ORDERED

TeslAmerica Laboratories

REDACTED

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

CIient ro OCM-BLS4DUP

Llork Order if Miltrix lJate Received __ Analysis DaLe

Prep Batch Dilution Factor Method

Prep Ikltc_

N~llitrusodimethylamine shy I)

13 225

REDACTED

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

ield

prep Dte Prep Batch [Ii Jut ton Pactor

les

Work OJdcr 11 f1atcix Date Recmved

Method

TIr L 078

REDACTED

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

RED

ACTED

Laboratories I

Rush TAT Reclue~teCl

24 his ReM 48 Mrs _ 5 Day Other

UVV-I iIKII1lt1 waler SW-Surtacewater

Z-Other

53 Southampton Roao Westfield MA 01

(P I 413-572-40CO (F)

Comments

MCP case narrative

I

B

I of I----

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

I 2425 New Holland Pike PO Sex 12425 LanOlster PA 17005middot2425 717-656middot~3()O

I

ion

5

ect 1n 1

ect es

Sit 6 07090016

on 111009

GROUP SAMPLE NUMBERS 1170551 5833860 5833864

PA Cert if 36-00037 NY Cert If 10670 NJ Cert tf PAOlI NC Cert If 52 TX Cert It TI04704194-08A-TX

Reviewed

REDACTED

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

Sa~plE Description Ililmington

24LS4

l~tholAa Rec~ived Dctectiofl FactorNo

~isc Organics sw- 83151 ugl

nodified N103-12

025 51 110342 ttcthlhyh~Zz inc

General Sample Co~~ent8

Laboratory Sample Analysis Record

t~l rrial~ lIach 110

REDACTED

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

63 LLI SampleSample

Project Site6 0709006

Misc Organicpound SW~l46 ugft

modified 0

General Sample comments

Laboratory Sauple P~alygi8 Record

REDACTED

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035

RED

ACTED

For Lancaster Laboratories use only

~1~Lancaster Acct 1 J9amp j 0 Group J 110551 Sample 55 2331oDltcH coc 225534 ~ rLaboratormiddotes Please print Instructions on reverse Side correspond with circled numbers

_-----M--=-A-=CTt EL=_______ ACCt _____

Project Namel OJ (n JV1mJ~gVhJ HA PWSID _____

Project Manager PeJ-ev=no cflt pSav Po ______

Sampler Ck1 vi s tl Zl d iyi Quote _____

Presorvation Codes

H=HCI T=Thiosulfate N=HN03 B=NaOH S=H~O O=Other

Turnaround Time Requested (TAT) (plpase ci ---- Rush

(Rush TAT is subject to Lancaster Laboratories approval and surcharge)

Date results are needed ________________

Rush results requested by (please circle) Phone Fax E-mail Phone ________________ Fax ______ _____

E-mail address

Data Package Options (please circle If required) SDG Complete

Type I (validationNJ Reg) 13 Yes Relinquished by Type II (Tier II)

Type III (Reduced NJ) No

Ty~ IV (CLP SOV) ~OG_n__~J Relinquished by Ty~ VI (Raw Data On y) Internal COC Required Yes I No_ ____

Lancaster Laboratories Inc 2425 New Holland Pike Lancaster PA 17601 (717) 656-2300 Fax (717) 656-6766 Copies White and yellow should accompany samples to Lancaster Laboratories The pink copy should be retained by the client

21 0203

1. barcodetext SDMS DocID 485035
2. barcode 485035