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Providing Research and Testing of Products Utilized in Hydraulic Fracturing & Cementing Operations

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Providing Research and Testing of Products Utilized in

Hydraulic Fracturing & Cementing Operations

Mining Company

Manufacturer

Transportation

Pumping Services

Consultant

Operator

Company Background

Established in 2004

3rd Party Independent Lab

Headquartered in Cypress, Texas

Providing Research and Testing of Products Utilized in

Hydraulic Fracturing & Cementing Operations

Partners with Companies Throughout Supply Chain

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Applying API Practices, ISO Standards and PropTester® Procedures to Provide Timely and Accurate Reports

Advanced Technology

Professional Workforce

Superior Communication and Customer

Service

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Recent Partners

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Laboratory Testing Field Oversight Equipment Sales

Fluids

Cement

Proppant

Products and Services

Through the use of our highly advanced technical lab and

on-site validation, PropTester professionally and scientifically assures

customers that quality materials including cement, fluid and proppant are

being used every time in an efficient manner.

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Fluids

Cement

Proppant

Provide Accurate Conclusions In The Lab And Validation At The Well-site.

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The Ideal Proppant

High Strength

No Embedment

Low Specific

Gravity

No FlowbackComplete

Compatibility

Readily Available

Cost Effective

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Does Not Exist

Proppant Laboratory Services

Quality Control Protocols

• ISO 13503-2 Properties

• ISO 13503-5 Conductivity

• Shale Formation Studies

Performance Tests

• PS-50®

• Hot/Wet Crush

• PT Crush Profile

• Beta Factor

• Regained Conductivity

Analysis Through ISO Standards And Non-standard Procedures

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Proppant Laboratory Testing

Full Service Testing (ISO 13503-2/API RP-19C Procedures)

• Turbidity

• Microscopic Exam

• Bulk Density

• Specific Gravity

• Sieve Analysis

• Particle Distribution

• Mean Particle Diameter

• Median Particle Diameter

• K-Factor Crush Test

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Proppant Laboratory Testing

• Full Service Testing (ISO 13503-2/API RP-19C Procedures)

• Two Automated Presses

• Sand, Ceramic and Resin Coated Proppants

• Hot/Wet Crush Profile

• Specific To Your Reservoir Conditions

• Particle Analyzer

• Full Particle Size Distribution For Frac And Gravel Pack Applications

Capable of up to 500F and 30,000 psi

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Proppant Conductivity Testing

• Long Term Conductivity Presses(API RP-19D)

• Increased Capacity – Operational March 2015

• 4 two-stack presses

• 7 four-stack presses

• Regained Conductivity Procedures(ISO TC/67 13503-5)

• Measures the impact of fracturing fluid on the proppant pack performance

Past research has shown as little as 5% fines may reduce flow capacity by at least 50%

Capable of up to 500F and 20,000 psi

By creating highly conductive proppant packs to maximize effective permeability

while reducing fines and migration, overall well productivity can be increased.

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Proppant Conductivity Testing

PS-50 ™ Point Specific Test

Provides answers to proppant flow capacity at your specific reservoir

pressure and temperature environment.

Customize Your Results. You Select:

Proppant

Temperature

Pressure Profile Conductivity machines capable of

stress levels to 20,000 psi and 500°F

Customizable, Quick Turnaround Time, Cost Effective

Single Point Conductivity Testing Using

API Set-Up Procedures (API RP 19D)

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Proppant Oversight

A B

Source or

OriginPoint of

Application

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PropTester On-Site Services

www.proptester.com

Blender Hopper with 20-40 Sand20/40 mesh Sintered Bauxite

3% by weight 12-20 mesh raw sand Straw, Feathers, and 1 Dead FrogAs Little As 25% Raw Sand Can Disable The

Curable Resin Coated Sand

• Correct Sizes and Type of Proppant

• Unknown Contaminants

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PropTester On-Site Services

Resin Dust is result of High Discharge Pressure

Manufacturer Recommends < 7 psi Off-Loading Pressure

www.proptester.com

• Clean Field Storage

• Proppant Transport Discharge Monitoring

• Correct Amount of Proppant

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PropTester Field Testing Services

Sample Collection

by PropTester

Technician

Full API Testing on

Location with

Mobile Laboratory

www.proptester.com

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Fluids

Cement

Proppant

Provide Accurate Conclusions In The Lab And Validation At The Well-site.

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Chemicals and Additives

Goals Successfully transport the propping agent into the fracture

Be compatible with the formation rock and fluid

Generate enough pressure drop along the fracture to create a wide fracture

Minimize friction pressure losses during injection

Be formulated using chemical additives that are approved by the local

environmental regulations.

Exhibit controlled-break to a low-viscosity fluid for cleanup after the treatment

Be cost-effective.

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Fluid Services

Field QC

• Water Quality

• Gel Hydration

• Cross-Link Time

• Breaker Test

• Chemical Inventory

• Material Balance

• Bucket Tests

• HT/HP Rheometer

Laboratory QC

• Water Analysis

• Guar Analysis

• Rheology – Base Fluid & Gelled Fluid

• HP/HT Viscometer – XL Fluids & Break Tests

• Flow Loop – Fluid Shear History & FR Evaluation Available mid 2014 www.proptester.com

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Fluids Laboratory Testing Services

High Pressure / High Temperature Rheometer

Capable of up to 400F and 2000 psi

• Fracture Fluids Testing

• Regain Conductivity Fluid Testing

• Water Analysis

• Guar Testing

• Barite Testing

• Rheology - Base Fluid & Gelled Fluid

• HP/HT Viscometer - Fluids & Breaker

Which fluid is best suited for your specific field application

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Fluids Oversight Services

Acid Mixing Oversight

Polymer Injection

Fracture Fluids Oversight

• Physical Inventory (Final / Initial)

• Bucket Testing or Checking Accuracy of LAS Pumps

• Pre-frac Water Analysis

• Hydration Rate / Viscosity Yield With Rotational

Viscometer

• Measurement of Cross-link Time (where applicable)

• Confirmation of Breaker Types, Loadings & Scheduling

• Evaluation of Clean & Dirty Samples During Frac Job

• Mass Balance Calculation

• Correlation of Actual Execution with Job Design

• HCl Acid Titration (when applicable)

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Fluids Laboratory Testing Services

Quality Analysis Recommended Formulations

Expert Technicians Customized Systems

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Fluids

Cement

Proppant

Provide Accurate Conclusions In The Lab And Validation At The Well-site.

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The life of your well depends on successful cementing operations.

With intricate well designs and completion practices, cement failures have become an increasing threat.

PropTester Cement Lab Services

• Create Zonal Isolation

• Protect Useable Water

• Provide Structural Support for Casing

• Protect from Corrosion

• Isolate Casing Seat for Subsequent Drilling

• Create Hydraulic Seal

Protect the environment and community &

Obtain maximum value from your wells

Goals of Cementing:

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• Loss of structural integrity

• Loss of wellbore integrity

• Loss of zonal isolation

• Barrier failure

• Gas migration (GM)

What problems have you encountered during your cement jobs?

PropTester Cement Lab Services

Cement failure will cost your company lost production time, costly repairs and increased liability.

Primary Cementing Cost ~15% of Total Well Cost

About 15% of Primary Jobs Require Remedial Cementing

Assume 10% of Wells Will Leak Within 5 Years

Typical Number of Squeezes to Solve a Problem = 3

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PropTester Cement Lab Services

• Rheology

• Density

• Fluid Loss

• Thickening Time

• Compressive Strength

Lab Equipment Includes:

Model 2040 HTHP

Consistometer

Volumetric Cement

Expansion Device

Cement Permeameter

High Pressure Dual Cell

UCA

Volumetric Cement

Expansion Device

Pressurized Fluid Density

Scale

Lab Testing Capabilities Include:

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Field Cementing Services

Field Cementing Worksheet Catarina Briscoe Springman Unit B-3H

South Texas

4/4/2013

PRE-Job Checks

Witness Loading Plugs into Plug Container

Mud Properties prior to Cementing (Density, Viscosity, Gas Free)

Casing Type - Liner, Production Casing, Surface Casing, Int. Casing

Total Depth of Pipe in Hole and Pipe Size and Weight

Confirm Bulk Tank Order of Mixing

Pre-Job Safety Meeting Y/N

Water Temperature Checked Y/N (See Attached Analysis)

Water Analysis Run? Y/N (See Attached Analysis)

Y N 5 1/2" Baker Latch Down

Density 11.2 lb./gal.

Production Casing15,021' 5 1/2" 20#

Y N

Y N

Y N 70 DEGREES F

Y N

Cement Spacer

Was Mud/Spacer/Cmt Compatibilities tested (OBM/SBM)

Density of Spacer confirmed with press scale Y/N

Spacer Additives Correct Volume Y/N

Spacer mixed on the fly or batch mixed

Correct Volume of Spacer Pumped Y/N

Y N

Y N 12.8 ppg

Y N

Batch Mixed

Y N 40 bbls

Lead Slurry

Cement Blend Confirmed

Confirm Compressive Strength (12,24 hrs) from Lab Test

Confirm Thickening Time compared to job time from Lab Test

Planned BBLs of Slurry Pumped? Actual BBLs Pumped

Wet and Dry Slurry Samples Collected? (Lead) Y/N

Y N

10 SEC 29.89 lbf/100ft2 10 MIN 33.09 lbf/100ft2

Y N 6:19 hr:mm

P 197 bbls A 197 bbls

Y N

Tail Slurry

Cement Blend Confirmed

Confirm Compressive Strength (12-24 hrs) from Lab Test

Confirm Thickening Time compared to job time from Lab Test

Planned BBLs of Slurry Pumped? Actual BBLs Pumped

Wet and Dry Slurry Samples Collected? (Tail) Y/N

Y N

10 SEC 28.82 lbf/100ft2 10 MIN 48.03 lbf/100ft2

Y N 5:50 hr:mm

P 447 bbls A 447 bbls

Y N

Operations

Witness Dropping Plug(s)

Time of Shutdown between rig pump circulation and cement job

Recorded PSI at Plug Bump

Floats Held on bleed off? Y/N

Full Returns during Job?

Was Pump Rate Schedule followed for the job (Rate Recorded)

Total Displacement (BBLS) Planned

Total Displacement (BBLS) Actual

Slurry Dry and Wet Storage (Lead & Tail) Date

Y N

30 MIN

2800 psi increased to 3800 psi to latch plug

Y N 3.5 bbls Flow Back

Y N

Y N 8 BPM

P 330 bbls

A 330 bbls

4/4/2013

• Pre-Job Checks

• Cement Spacer

• Lead & Tail Slurry Confirmations

• Operations Oversight

• Fresh Water Tank Volumes

Example Report

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Cement Field Services

• Material Balances – Water, Cement,

Chemical Additives, Float Equipment

• Field Blend Analysis

• Water Analysis

• Cement Calculations

• Displacement Calculations

• Cement Density Down-Hole

• Pump Rates Down-Hole

Example Report

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Field Sample Program

Eliminate Fear, Uncertainty and Doubt By Utilizing the Final Step of Cement Quality Assurance

Field Sample Collection and Testing

Field Sample Quality Assurance Program

Procedures: Collect samples of the dry blended cement and mix water as mixing progresses. Samples

must be taken in clean, well marked containers, and stored securely at proper temperatures should they be required for post job evaluation.

Thickening Time Test

UCA 24-Hour Compressive Strength Test

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Competitive Advantages

www.proptester.com

Limited Time:

FREE

1. Collect a dry sample and water sample

from location

2. Mail to PropTester facility

Thickening Time Test

UCA 24-Hour Compressive Strength Test

Field sample test results will give you peace of mind that quality materials were pumped.

Need Sample Containers? Contact PropTester for dry material and water sample containers.

Limited Time Cement Quality Assurance Discount

For new customers

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Resources

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PropTester Personal Lab Space Capabilities

Build-to-Suit Laboratories

Companies in need of lab space for specialized research and development are welcome to rent space from PropTester’s facility.

Full-time lab technicians and a personal security system can be utilized.

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Capable of Housing All Forms of Oil Field Testing:

• Proppant Analysis – API RP 19C

• Long-Term Conductivity Machine Rentals

• Full Fluids Set Up

• API Cementing Testing

PropTester Resources for Customers

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Competitive Advantages

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Conclusions

Strategically Located Customer Oriented

Long-Lasting

Partnerships

Value-Added Company

Throughout

Supply Chain

Partnering Throughout The Supply Chain To Provide Accurate Conclusions In The Lab And Validation At The Well-site.

Michelle Stribling

Sales & Marketing

713-826-5971

[email protected]

For questions or more information, please contact: