precision data working product wise for various modes of transport
TRANSCRIPT
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8/7/2019 Precision Data working product wise for various modes of transport
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Characteristic
770 7100.5
Distillation:(E-70), % v 45 10 1
Distillation:(E-100), % v 70 40 1
Distillation:(E-180), % v 90 1
215 1
88 0
88 0.2
4011.87
0.05
0.01
60 350.02
1 0.04
3 0.03
0.01
0
Application of Precision D
Test
MethodRequirements
LimitsRepetabilit
yUpper
Lower
Density @ 15oC, Kg/m3
P:16
P:18/ D:86
RON
Existent Gum, g/m3 P:29
Sulphur, Total % mass P:34
(RVP) at 38oC kPa P:39Benzene, % by Vol. D:3606
Lead, g/lit IP:352
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1.2 769.29 710.71 770.71 709.29 769.29 710.71
3 43.23 11.77 46.77 8.23 43.23 11.77
3 68.23 41.77 71.77 38.23 68.23 41.77
3 91.77 88.23 #VALUE! 91.77
4 212.64 217.36 212.64 #VALUE!
1 88.59 87.41 #VALUE! 88.59
0.7 88.41 87.59 #VALUE! 88.41
23.33 26.24 53.76 26.24#VALUE!
0.01 0.04 0.06 0.0434#VALUE!
0.04 59.98 35.02 60.02 34.98 59.98 35.02
0.18 0.89 1.11 0.89#VALUE!
0.84 2.5 3.5 2.50#VALUE!
0.01 0.01 0.02 0.008#VALUE!
ata MS BSII IS 2796
Reproduci
bilityA1-A2>4R;
A1,A2>2R
Acceptable Margins,Supplier ,
Not OK Margins,Recipient ,
RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R
60>4.8 OK35>12 OK30>12 OK90>6 OK
215>8 OK88>2 OK
88>1.4 OK
40>46.66 NOT OK
0.5>0.224 OK
25>0.16 OK1>0.36 OK3>1.68 OK. .
5 OK
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770.71 709.29
46.77 8.23
71.77 38.23
#VALUE! 88.23
217.36 #VALUE!
#VALUE! 87.41
#VALUE! 87.59
53.76#VALUE!
0.0566#VALUE!
60.02 34.98
1.11#VALUE!
3.50#VALUE!
0.018#VALUE!
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Characteristic
775 720 0.5 1.2
Distill:(E-70), % v 45 10 1 3
Distill:(E-100), % v 70 40 1 3Distill:(E-150), % v 75 1 3
210 1 8
91 0.2 0.7
5 2.1 4.04
0.02
0.01 0.01
60 0.02 0.04
1 0.04 0.18
42 1.6 3.5
21 1.6 6.80.01
0 0.01
Application of Precision Data
Test
MethodRequirements
Repetability
Reproduci
bilityUpper
Lower
Den @ 15oC, Kg/m3
P:18/ D:86
Sulphur, Total % m D:4294
o
Lead, g/lit IP:352
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774.29 720.71 775.71 719.29
43.23 11.77 46.77 8.23
68.23 41.77 71.77 38.2376.77 73.23
205.28 214.72
91.41 90.59
2.62 7.38
0.01 0.02
59.98 60.02
0.89 1.11
39.94 44.07
16.99 25.01
0 0.01
S BSIII IS 2796
A1-A2>4R;
A1,A2>2R
Acceptable Margins,Supplier
Not OK Margins,Recipient
RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R55>4.8 OK35>12 OK
30>12 OK75>6 OK210>16 OK91>1.4 OK5>8.08 NOT OK. .
8 NOT OK60>0.08 OK1>0.36 OK42>7.0 OK
21>13.6 OK. .5 NOT OK
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Characteristic
1 860 820 0.5 1.2
2 0.01
0 0.01
3 0.3
0.04 0.06
4 0.25 0.04 0.05
5 0.05
0.01 0.05
6 Pour Point,oC,winter 3 3 6
7 Pour,oC,summer 15 3 6
8 48 0 2
9 35 1 1.5
10 5 2 0.02 0.04
5 2 0.01 0.01
11 Distill(E-350), % v 85 2 5
Distill:(E-370), % v 95 2 5
12 0.2 0.1 0.2
13 0.05 0.1 0.2
14 0.05
0.03 0.05
Application of Precision Data HSD
Sl. TestMethod
Requirements
Repetability
Reproduci
bilityUpper
Lower
Density @ 15oC, Kg/m3 Ash, % by Mass P:4
RCR, %by mass P:8
Sulphur, Total % m IP:336
K V, cSt at 40
o
C P:25P:18/ D:86
-
Sediment P:30
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859.29 820.71 860.71 819.29
0.01 0.01
0.26 0.34
0.22 0.28
0.02 0.08
0 6.54
11.46 18.54
49.18 46.82
35.89 34.12
4.98 2.02 5.02 1.98
4.99 2.01 5.01 1.99
87.95 82.05
97.95 92.05
0.08 0.32
-0.07 0.17
0.02 0.08
IS 1460 BSII
A1-A2>4R;
A1,A2>2R
Acceptable Margins,Supplier
Not OK Margins,Recipient
RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59R40>4.8 OK
0.01=0.01 BORDER
0.3>0.124 OK0.25>0.1 OK
0.05>0.094 NOT OK15>12 OK3>12 NOT OK48>4 OK35>3 OK
3>0.14 OK3>0.06 OK85>10 OK95>10 OK
0.2>0.4 NOT OK0.05>0.4 NOT OK
0.05=0.05 BORDER
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Characteristic
845 820 0.5 1.2
0.01 0
0 0.01
0.3 0
0.04 0.06
0.04 0
0.01 0.01
0 51 0 2
0 35 1 1.5
4.5 2 0.02 0.03
4.5 2 0.01 0.01
Distillation(E-360), % v 0 95 2 5
Water Content, %(v/v) 0.02 0
0 0.01CFPP,oC,winter 6 0 1 2
CFPP,oC,summer 18 0 0.5 1
0 25 6.7 13.1
11 0 1.77 3.83
0 460 63 120
Application of Precision Data HSD IS 1460 Test
MethodRequirements
Repetability
Reproduci
bilityA1-A2>4R;
A1,A2>2RUpper
Lower
Density @ 15oC, Kg/m3 25>4.8
Ash, % by Mass P:4 0.01=0.01
RCR, %by mass P:8 0.3>0.124
Sulphur, Total % mass D:4294. .
2
51>4
35>3
K V, cSt at 40 oC P:25 3>0.143>0.06
95>10
P:40 0.02=0.02 6>4
18>2
25>26.2
11>7.66
460>204
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844.29 820.71 845.71 819.29
0.01 0.01 0.01 0.01
0.26 0.34 0.34 0.26
0.03 0.04 0.04 0.03
49.82 52.18 1.18 49.82
34.12 35.89 35.89 34.12
4.48 2.02 4.52 1.98
4.49 2.01 4.51 1.99
92.05 97.95 97.95 92.05
0.01 0.01 0.03 -0.01
4.82 7.18 7.18 4.82
17.41 18.59 18.59 17.41
17.27 32.73 32.73 17.27
8.74 13.26 13.26 8.74
389.2 530.8 530.8 389.2
SIIIAcceptable Margins,
SupplierNot OK Margins,
Recipient
RemarksA1-0.59RA2+0.59RA1+0.59RA2-0.59ROK
BORDER
OK
OKOKOKOKOKOK
BORDEROKOK
NOT OKOKOK
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Characteristic
Nov-38 Nov-38
75 76 76
90 91.8 91 92
215 210 212 200 200 200
88 91 88.42 88.2 91.2 91.2
500 150 225 480 145 125
60 58 58
Benz, % v. Max. 1 1 0.89 0.9 0.9 0.9
3 0.03/.84 2.5 2.8
Cu Corr, Max.
Seven Critical Parameters for MS BSII- Rail/Road and PipelineBIS BSII
SpecsBIS BSIII
SpecsPrecision
Limits(Repet./Repro)
TestMarginsas per
ISO 4259based on
singletest
result
Rail/RoadMfg
Specs
BSII
Rail/RoadMfg
Specs
BSIII
P/L MfgSpecsBSIII
{2000ppm SKOinterface
}
Density @ 15oC,Kg/m3
710 770720-7750.5/0.12710.72-711-768*721-773721-773
Distill-Rec, 70oC , % v10 4510 45 - 11.8-43.211-38*
100oC , % v40 7040 70 - 41.8-68.241-70 41-70 41-70
150oC , % v-
180o
C , % v Min - FBP, oC, Max.
-
Sul % m, Max. 145/467
RVP at 38oC kPa 35 60 3.2/5.237.1-57.638-58*
0.04/0.18
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To take care of test margin
To take care of Testing Margin
Justification/Remarks
ethanolo a e care o s orage an
handling impact and upper limitto take care of addition of
ethanol
handling impact.
handling impact.
margin. UL to facilitate
absorption of ethanol
To take care of Testing Margin
and production constraints
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Characteristic
1 46 47.98 47
2 95 96.2 96
3 35 36.8 37
4 0.05 0.7 225 450
5 460 388 420
7 1
Seven Critical Parameters for HSD- Rail/Road and Pipeline
Sl. BISSpecs
PrecisionLimits
(Repetability/
Reproducibility)
Test Margins asper ISO 4259
based on single
test result
Rail/RoadMfg
Specs
Distillation :Recovery up to
370oC (E-370), % by Vol. Min-
Flash Point, Deg C, Min 1/1.5Sulphur, Total Percent by
Copper Strip Corrosion, for3hrs at 50oC, Max.
NA Qualitative test. NoPrecision limit
1a
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Justification/Remarks
To take care of Test marginrecovery higher than 95% to
To take care of test margin
To take care of TestingMargin
To take care of TestingTo improve product quality
further
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Characteristic
1 Smoke Point, mm, Min. 18 2-Jan 19.8 19
2 300 297 290
4 2500 2160 2400
Four Critical Parameters for SKO- Rail/Road and Pipe
Sl. BISSpecs
PrecisionLimits
(Repetability/
Reproducibility)
TestMarginsas per
ISO 4259based on
singletest
result
Rail/RoadMfg
Specs
Distillation : FBP, Deg C,
-
Sulphur, Total % mass,
175/580
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To take care of Testing Margin
line
Justification/Remarks
To take care of test margin. 20
for Rlys and 22 for Defence
owing to production difficulty.
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Eight Critical parameters for ATF- RaiCharacteristic
1
25 23.2 20
2
0 0
3
3000 2700 2500
4 300 297 290
5 38 38.9 40
6 -47 -48.38 -49
8
Lubricity: WSD, mm, Max 0.78 0.65
Sl. BISS ecs
PrecisionLimits
TestMargins
Rail/Road
Mf S ecsAromatics, percent byvolume, Max 1.4/3.0Sulphur mercaptan, percent
by mass, Max
0.003/0.0
NA
Sulphur Total, ppm by mass,Max 50/175Final Boiling Point, oC, Max
-Flash point ( Abel ), oC, Min Freezing point, oC, Max
0.85/ 0.65 -
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l/Road
Justification/Remarks
Def Reqmt 20. Since product cannot be segregated
Def Reqmt 0.002
Def Reqmt 2500To take care of Test MarginTo take care of Test MarginTo take care of Test Margin
Def reqmnt-0.65
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S Prod Characteristic Road/Rail Movement Coastal
1 MS Density
RON 0.5 unit > BS-II -88 0.5 unit > BS-II -88
BS-III-91 BS-III-91
Distillation 1% above of Min Range 1% above of Min Range
FBP
Benzene
RVP BS-I:38 Min; 58 Max BS-I:38 Min; 58 Max
BS-II: 58 Max BS-II: 58 Max
Sulfur 20 ppm < BS-II:500 ppm; 20 ppm < BS-II:500 ppm;
5 ppmBS-II: 95% Vol
Cetane Index -
Cetane No - 0.4>BS-II:48;BS-III:51
Flash Point
Lubricity 40< BS-II/BS-III: 460 mu 40< BS-II/BS-III: 460 mu
Oxidation stabili ty 3 35 oC
+/-0.002 @ 15 oC +/-0.002 @ 15 oParticulate Visual inspection- free from Visual inspection- free
mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015 -
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Water
Silver Strip Corr.
Copper Strip Corro
Lubricity Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85
Conductivity 250-450 PS/M
Using conductivity meter
S Test E:
1 Appearance
2
3 Flash Point
4 Existent Gum
5 Copper Strip Corrosion Test
6 Distillation
7 Doctor Test
8 Water Reaction
9 Freezing Point
30 ppm through Aquadischeck
Free from dissolved waterusing aquadis check
Test H after loading TT /Tank Wagon
Test E after loading
Test H after loading TT /Tank Wagon
Def-1; Civil-1 as perTestE after loading
250-450 PS/M usingconductivity meter
Density @ 15 oC
Note: The Customer may take product Coastally and push into cross country pipelinto take care of the Max/Min limits of the most stringent requirement. In ATF conductiTanks it has to be in the range of 350 + as per our experience factor.
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Pipeline Transfers Guarantee to Customer
BS-II -88
BS-III-91
1% above of Min Range
BS-I:38 Min; 58 Max
BS-II: 58 Max
50 ppm < BS-II:500 ppm;
25 ppm 2 Cst for BS-II, BS-III BS-II: 2-5 Cst;
BS-III: 2-4.5 Cst
0.5>BS-II: 95% Vol
0.5 unit > BS-II: 46; BS-III 51 BS-II: 46;
BS-III 51
0.4>BS-II:48;BS-III:51 BS-II: 48;
BS-III 51
40< BS-II/BS-III: 460 mu BS-II: 460;
BS-III 460
3 BSII -88(93); BSIII-91 {whenSKO is intermediate Product}
BS-II Rec@70:10-45%;@100:40-70%@180: 90% Min
BS-III Rec@70:10-45%;@100:40-70%@150: 75% Min
Min 20 oC < BS-II:215 oC; BS-III:210 oC{when SKO is intermediate Product}
BS-II:215 oC;
BS-III:210 oC
0.2 35 oC BS-II/BS-III: 35o
C Min
BS-III: 25 g/m3, Max
+/-0.002 @ 15 oC
mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015 -
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(Qtly Millipore gravimetric test)
15 ppm using aquadis check
Def-1; Civil-2
Def-1; Civil-1
Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85
250-450 PS/M 50-450 PS/M
Using conductivity meter
Sr Test H:
1
2 Temperature
3 Appearance
4 Water / Sediments
Free from dissolved water using aquadischeck
Test H after commencement of PLT
Test H after commencement of PLT
Density @ 15 oC
We are producing only one Grade of ATF. Since the Defence Grade is morestringent, the Defence specs needs to be met so that we can supply to both civil aswell as defence requirements.
s at the destination. In such a eventuality, the manufacturing specs will haveity insisted ex Mktg Company is 250 PSM Min by OMCs. Therefore at ref
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S Prod Characteristic Refinery to Mkt Coastal
1 MS Density
RON(AKI) - 0.5 unit > B
BS-III-91 BS-III-91FBP - -
Sulfur - 20 ppm B
Sulfur - -
4 ATF Density
1.0 mg/lit
Water
Silver Strip Corr. Def-0; Civil-1
Def-1; Civil-1
Road/RailMovement
BS-II-88(93)
Min 10oC <
III:210 oC
20 ppm < BS-II:500 ppm;
5 ppm
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Lubricity Def- 0.65; Civil-0.85 Def- 0.65;
Conductivity 250-450 P
Using cond
s Test E:
1 Appearance
2
3 Flash Point
4 Existent Gum
5 Copper Strip Corrosion Test
6 Distillation
7 Doctor Test
8 Water Reaction
9 Freezing Point
Def- 0.65; Civil-0.85
300-450 PS/M usingconductivity meter
250-450 PS/Musing conductivity
Density @ 15 oC
Note: The Customer may take product Coastally and push into cross countryspecs will have to take care of the Max/Min limits of the most stringent requirMin by OMCs. Therefore at ref Tanks it has to be in the range of 350 + as per
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Pipeline Transfers
S-II -88(93) BS-II -88(93)
BS-III-91(95)
S-II:500 ppm; 50 ppm < BS-II:500 ppm;
III:150 ppm 25 ppm 2 Cst for BS-II, BS-IIIBS-III: 2-4.5 Cst
S-II: 48; BS-III 51 0.5 unit > BS-II: 48; BS-III 51
BS-III 51
BS-III:350 ppm
775-840
0.22 mg/lit
Def-1; Civil-2
Def-1; Civil-1
Guarantee toCustomer
15 oC +/-0.0025 @ 15 oC BS-II :710-770;BS-III: 720-
1 unit > BSII -88(93); BSIII-91{when SKO is intermediate
Product}
BS-II:215 oC; BS-
Min 15 oC < BS-II:215 oC; BS-III:210 oC {when SKO isintermediate Product}
BS-II:215 oC;
BS-III:210 oC
BS-II:500 ppm;BS-III:150
ppm
{when SKO is intermediateProduct}
15 oC +/-0.0025 @ 15 oC
42 oC Min {when interfacedwith MS/ Naphtha}
35 oC Min
15 oC +/-0.0025 @ 15 oC BS-II: 820-860;
BS-II: 2-5 Cst;
BS-II: 48;
S-II:500 ppm;BS-
50 ppm < BS-II:500 ppm;BS-III:350 ppm
BS-II:500 ppm;
15 oC +/-0.0025@ 15 oC
ction- free from Visual inspection- free fromsediments (Qtly Millipore
gravimetric test)issolved water usingck
Free from dissolved waterusing aquadis check
15 ppm usingaquadis check
r loading Test H after commencementof PLT
1 as perTest E afterTest H after commencementof PLT
mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.003@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015mailto:+/-0.003@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.002@%2015mailto:+/-0.0025@%2015mailto:+/-0.0025@%2015 -
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ivil-0.85 Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85
/M 250-450 PS/M 50-450 PS/M
uctivity meter Using conductivity meter
sr Test H:
1
2 Temperature
3 Appearance
4 Water / Sediments
Density @ 15 oC
We are producing only one Grade of ATF. Since the Defence Grade ismore stringent, the Defence specs needs to be met so that we can supplyto both civil as well as defence requirements.
pipelines at the destination. In such a eventuality, the manufacturingment. In ATF conductivity insisted ex Mktg Company is 250 PSMur experience factor.