lso/lyso crystals for future high energy physics...
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May 22, 2007 1Informal HEP Seminar, Ren-yuan Zhu, Caltech
LSO/LYSO Crystals for FutureHigh Energy Physics Experiments
Ren-yuan Zhu
California Institute of Technology
May 22, 2007 2Ren-yuan Zhu, Informal HEP Seminar at Caltech
Why Crystal Calorimeter Enhance physics discovery potential since photons and electrons are fundamental particles for the standard model physics and new physics.
Performance of a crystal calorimeter is well understood:
The best possible energy resolution, good position and photon angular resolution;Good e/photon identification and reconstruction efficiency;Good missing energy resolutions;Good jet energy resolution.
May 22, 2007 3Ren-yuan Zhu, Informal HEP Seminar at Caltech
Physics with Precision Crystal Calorimeters
Charmonium system observedby CB through Inclusive photons
CB NaI(Tl) L3 BGO
Charmed Meson in Z Decay
May 22, 2007 4Ren-yuan Zhu, Informal HEP Seminar at Caltech
H→γγ Search Needs Precision ECAL
Narrow width and large background
LEP
H→ γγ
H → ZZ → 4 leptons*
H →ZZ → 4 leptons
H →WW or ZZjj
LHC
Natural width (GeV)
Higgs Mass (GeV)0 50 100 200 400 800
0.001 0.004 1.4 30 250
σm / m = 0.5 [σE1 /E1 ⊕ σE2 /E2 ⊕ σθ /tan(θ/2)],where σE / E = a /√ E ⊕ b ⊕ c/E and E in GeV
γ1
γ2
H
CMS PWO
H→γγ at LHC
May 22, 2007 5Ren-yuan Zhu, Informal HEP Seminar at Caltech
KTeV CsI Position Resolution
σx = 3 /√ E ⊕ 0.3 mm for L3 BGO & CMS PWO
3256 CsI
May 22, 2007 6Ren-yuan Zhu, Informal HEP Seminar at Caltech
BaBar CsI(Tl) Energy Resolution
BaBar CsI(Tl)
Good light yield of CsI(Tl) provides excellent energy resolution at low energies
M. Kocian, SLAC, CALOR2002M. Kocian, SLAC, CALOR2002
33--9 GeV, 12h9 GeV, 12h
0.030.03--3 GeV3 GeV
0.00613 GeV, 1/2h0.00613 GeV, 1/2h
6580 CsI(Tl)
May 22, 2007 7Ren-yuan Zhu, Informal HEP Seminar at Caltech
L3 BGO Energy ResolutionContribution “Radiative”+Intrinsic Temperature Calibration Overall
Barrel 0.8% 0.5% 0.5% 1.07%Endcaps 0.6% 0.5% 0.4% 0.88%
L3 BGO
May 22, 2007 8Ren-yuan Zhu, Informal HEP Seminar at Caltech
CMS PWO Energy Resolution
Designed Resolution
Measured Resolutionσ(E)/E < 1% if E > 25 GeV
σ(E)/E ~ 0.5% at 120 GeV
CMS PWO
May 22, 2007 9Ren-yuan Zhu, Informal HEP Seminar at Caltech
Mass Produced CrystalsCrystal NaI(Tl) CsI(Tl) CsI BaF2 BGO PWO(Y) LSO(Ce) GSO(Ce)
Density (g/cm3) 3.67 4.51 4.51 4.89 7.13 8.3 7.40 6.71Melting Point (ºC) 651 621 621 1280 1050 1123 2050 1950Radiation Length (cm) 2.59 1.86 1.86 2.03 1.12 0.89 1.14 1.38Molière Radius (cm) 4.13 3.57 3.57 3.10 2.23 2.00 2.07 2.23Interaction Length (cm) 42.9 39.3 39.3 30.7 22.8 20.7 20.9 22.2Refractive Index a 1.85 1.79 1.95 1.50 2.15 2.20 1.82 1.85Hygroscopicity Yes Slight Slight No No No No NoLuminescence b (nm)(at peak)
410 550 420310
300220
480 425420
402 440
Decay Time b (ns) 230 1250 306
6300.9
300 3010
40 60
Light Yield b,c (%) 100 165 3.61.1
363.4
21 0.29.083
83 30
d(LY)/dT b (%/ ºC) -0.2 0.3 -1.3 -1.3 -0.9 -2.7 -0.2 -0.1
Experiment Crystal Ball
CLEO BaBar BELLEBES III
KTeV TAPS(L*)
(GEM)
L3BELLE
PANDA?
CMSALICEPrimEx
PANDA?
Super B? -
a. at peak of emission; b. up/low row: slow/fast component; c. PMT QE taken out.
May 22, 2007 10Ren-yuan Zhu, Informal HEP Seminar at Caltech
Crystal Density: Radiation Length1.5 X0 Cubic Samples:
Hygroscopic Halides
Non-hygroscopic
Full Size Crystals:
BaBar CsI(Tl): 16 X0
L3 BGO: 22 X0
CMS PWO(Y): 25 X0
BaBar CsI(Tl)
L3 BGO
CMS PWO
PWO LSO LYSO BGO CeF3 BaF2
CsI CsI(Na) CsI(Tl) NaI(Tl)
May 22, 2007 11Ren-yuan Zhu, Informal HEP Seminar at Caltech
Excitation, Photo-Luminescence, Transmission
Black Dots: Theoretical limit of transmittance: NIM A333 (1993) 422
LSO
LYSO
May 22, 2007 12Ren-yuan Zhu, Informal HEP Seminar at Caltech
Scintillation Light Decay TimeRecorded with an Agilent 6052A digital scope
Fast Scintillators Slow Scintillators
LSO
LYSO
May 22, 2007 13Ren-yuan Zhu, Informal HEP Seminar at Caltech
Light Output & Decay KineticsMeasured with Philips XP2254B PMT (multi-alkali cathode)
p.e./MeV: LSO/LYSO is 6 & 230 times of BGO & PWO respectively
Fast Scintillators Slow Scintillators
LYSO
LSO
May 22, 2007 14Ren-yuan Zhu, Informal HEP Seminar at Caltech
Temperature Dependent Light Output
LSO/LYSO light output has a small temperature coefficient
LYSOLSO
May 22, 2007 15Ren-yuan Zhu, Informal HEP Seminar at Caltech
Photo-Luminescence Weighted Q.E.
Taking out QE, L.O. of LSO/LYSO is 4/200 times BGO/PWO Hamamatsu S8664-55 APD has QE 75% for LSO/LYSO
LSO / LYSO
LSO / LYSO
May 22, 2007 16Ren-yuan Zhu, Informal HEP Seminar at Caltech
LSO/LYSO Mass Production
CTI: LSO CPI: LYSO Saint-GobainLYSO
Additional Capability: SIPAT @ Sichuan, China
May 22, 2007 17Ren-yuan Zhu, Informal HEP Seminar at Caltech
Total area(占地面积):52,258m2
Construction area(建筑面积):38,331m2
For R&D (研发用建筑面积):27,765m2
Sichuan Institute of Piezoelectric and Acousto-optic Technology (SIPAT)
May 22, 2007 18Ren-yuan Zhu, Informal HEP Seminar at Caltech
SIPAT Ø 60 x 250 mm LYSO Boles
May 22, 2007 19Ren-yuan Zhu, Informal HEP Seminar at Caltech
BGO, LSO & LYSO Samples2.5 x 2.5 x 20 cm (18 X0) Bar
CPI LYSO
Saint-Gobain LYSO
SIC BGO
CTI LSO
May 22, 2007 20Ren-yuan Zhu, Informal HEP Seminar at Caltech
Excitation, Photo-Luminescence, TransmissionIdentical transmittance, emission & excitation spectra
Part of emitted light may be self-absorbed in long samples
1.7 cm Cube 2.5 x 2.5 x 20 cm Bar
May 22, 2007 21Ren-yuan Zhu, Informal HEP Seminar at Caltech
CTI LSO: longitudinal optical uniformity No longitudinal variation in optical properties
Transverse transmittance approaches theoretical limit
May 22, 2007 22Ren-yuan Zhu, Informal HEP Seminar at Caltech
PMT Based Readout with CoincidenceSystematic error with repeated mounts & measurements: < 1%
May 22, 2007 23Ren-yuan Zhu, Informal HEP Seminar at Caltech
LSO/LYSO Resolution with PMT Readout
~10% FWHM resolution for 22Na source (0.51 MeV)
2.5 x 2.5 x 20 cm Bar1.7 cm Cube
May 22, 2007 24Ren-yuan Zhu, Informal HEP Seminar at Caltech
LSO/LYSO LO with PMT Readout1,200 p.e./MeV, 5/230 times of BGO/PWO
1.7 cm Cube 2.5 x 2.5 x 20 cm Bar
May 22, 2007 25Ren-yuan Zhu, Informal HEP Seminar at Caltech
APD Based Readout with Coincidence Two Hamamatsu S6664-55 APD, Canberra 2003 BT preamplifier
and ORTEC 673 shaping amplifier with shaping time 250 ns
Hamamatsu S6664-55 APD
May 22, 2007 26Ren-yuan Zhu, Informal HEP Seminar at Caltech
Calibration of the APD ReadoutPedestal: 34 ADC, corresponding to 57 electrons Corrections for 5.9 keV X-ray: 78%; Good linearity
May 22, 2007 27Ren-yuan Zhu, Informal HEP Seminar at Caltech
LSO/LYSO with APD ReadoutL.O.: 1,500 p.e./MeV, 4/200 times of BGO/PWO
Readout Noise: < 40 keV
May 22, 2007 28Ren-yuan Zhu, Informal HEP Seminar at Caltech
γ-ray Induced Damage in LSO/LYSO
No damage in Photo-Luminescence LT recovery very slow
May 22, 2007 29Ren-yuan Zhu, Informal HEP Seminar at Caltech
Transmittance Damage
300oC thermal annealing effective LT damage: 8% @ 1 Mrad
May 22, 2007 30Ren-yuan Zhu, Informal HEP Seminar at Caltech
Light Output Damage with PMT Readout
Light output loss: about 12% to 14% @ 1 Mrad
May 22, 2007 31Ren-yuan Zhu, Informal HEP Seminar at Caltech
Light Output Damage with APD Readout
Light output loss: about 10% to 12% @ 1 Mrad
May 22, 2007 32Ren-yuan Zhu, Informal HEP Seminar at Caltech
LRU with PMT Readout Uniformity depends on end coupled to the PMT
No damage in the light response uniformity
A end Coupling B end Coupling
May 22, 2007 33Ren-yuan Zhu, Informal HEP Seminar at Caltech
LRU with APD Readout Uniformity depends on end coupled to the APDSome change in the light response uniformity
A end Coupling B end Coupling
May 22, 2007 34Ren-yuan Zhu, Informal HEP Seminar at Caltech
Possible Origin of Non UniformityC. Melcher: LO in LSO is a function of Ce concentration
B. Chai: LO in LYSO is a function of Yttrium fraction
May 22, 2007 35Ren-yuan Zhu, Informal HEP Seminar at Caltech
Radiation Induced Phosphorescence Phosphorescence peaked at 430 nm
with decay time constant of 2.5 h observed
May 22, 2007 36Ren-yuan Zhu, Informal HEP Seminar at Caltech
γ–ray Induced Readout Noise
γ–ray induced PMT anode current can be converted to the photoelectron numbers (Q) integrated in 100 ns gate. Its statistical fluctuation contributes to the readout noise (σ).
Sample L.Y. F Q15 rad/h Q500 rad/h σ15 rad/h σ500 rad/h
ID p.e./MeV μA/rad/h p.e. p.e. MeV MeV
CPI 1,480 41 6.98x104 2.33x106 0.18 1.03SG 1,580 42 7.15x104 2.38x106 0.17 0.97
May 22, 2007 37Ren-yuan Zhu, Informal HEP Seminar at Caltech
LSO/LYSO ECAL Performance
Less demanding to the environment because of small temperature coefficient.Radiation damage is less an issue as compared to other crystals.A better energy resolution, σ(E)/E, at low energies than L3 BGO and CMS PWO because of its high light output and low readout noise:
EE /2.0%55.0/%5.2 ⊕⊕2.0 0.5 .001/E
May 22, 2007 38Ren-yuan Zhu, Informal HEP Seminar at Caltech
BaBar Upgrade for Super B Factory
LSO/LYSO
Aiming at 1036/cm2/s luminosity for rare B decays
Need fast detector with low noise at endcap
Super B Conceptual Design Report, INFN/AE-07/2, SLAC-R-856, LAL 07-15, March 2007
May 22, 2007 39Ren-yuan Zhu, Informal HEP Seminar at Caltech
Six LSO & LYSO Samples
Saint-Gobain LYSO
Saint-Gobain LYSO
Saint-Gobain LYSO
CTI LSO
CTI LSO
CTI LSO
2.5 x 2.5 x 20 cm (18 X0) Bar
Three LSO/LYSO crystals are obtained from CTI/Saint-Gobain.
A statistical comparison is under way.
May 22, 2007 40Ren-yuan Zhu, Informal HEP Seminar at Caltech
Statistical ComparisonRecent LYSO crystals seems better than LSO
May 22, 2007 41Ren-yuan Zhu, Informal HEP Seminar at Caltech
First SIPAT LYSO Bole for HEP
Ø 60 x 250 mm
R&D aiming at producing crystals for HEP experiments
Broken after 1st attempt cutting two 2.5 x 2.5 x 20 cm samples
May 22, 2007 42Ren-yuan Zhu, Informal HEP Seminar at Caltech
11 Samples from the 1st SIPAT Bole
May 22, 2007 43Ren-yuan Zhu, Informal HEP Seminar at Caltech
Excitation & Photo LuminescenceNo variation in excitation and emission
May 22, 2007 44Ren-yuan Zhu, Informal HEP Seminar at Caltech
Transmittance
Transmittance degrades after 5 cm from the seed
May 22, 2007 45Ren-yuan Zhu, Informal HEP Seminar at Caltech
Light Output
Light output degrades after 10 cm from the seed
May 22, 2007 46Ren-yuan Zhu, Informal HEP Seminar at Caltech
Energy Resolution
Resolution degrades after 10 cm from the seed
May 22, 2007 47Ren-yuan Zhu, Informal HEP Seminar at Caltech
Excellent Correlations
Between light output and resolution/transmittance
May 22, 2007 48Ren-yuan Zhu, Informal HEP Seminar at Caltech
Summary
LSO/LYSO crystals are a good candidate for future precision crystal calorimeters.R&D is under way to further understand LSO and LYSO crystals and to develop cost effective LYSO crystals for future HEP experiments.Thanks to the DOE ADR program for supporting this work.
May 22, 2007 49Ren-yuan Zhu, Informal HEP Seminar at Caltech
Transmittance MeasurementHITACHI U-3210 UV/VIS Spectrophotometer
with a Large Sample Compartment
Beam 1
Beam 2
A simple way for looking absorption bands. No controversy.
Precision of 0.3% can be reached.
Issue for PWO:birefringence.
Theoretical limit: D.A. Ma et al., NIM A333 (1993) 422
May 22, 2007 50Ren-yuan Zhu, Informal HEP Seminar at Caltech
Radio-Luminescence MeasurementIssue: Absorption affects emission blue edge
Corrections: Grating efficiency & PMT (Hamamatsu R758) QE R.Y. Zhu et al., NIM A376 (1996) 376
May 22, 2007 51Ren-yuan Zhu, Informal HEP Seminar at Caltech
Photo Luminescence MeasurementHITACHI F4500 Fluorescence Spectrophotometer
Light Source (1), Gratings Efficiencies (2 & 3) & PMT QE (4)Red-Extended Hamamatsu R928 PMT(4): 185 to 900 nm
3
4
2
1
May 22, 2007 52Ren-yuan Zhu, Informal HEP Seminar at Caltech
Photo Luminescence and ExcitationMeasured by using HITACHI F4500
Photo luminescence depends on the excitation wavelength
May 22, 2007 53Ren-yuan Zhu, Informal HEP Seminar at Caltech
Absorption and Photo Luminescence
With internal absorption Without internal absorption
θ = 0o θ = 10o