olar. - harold weisbergjfk.hood.edu/collection/weisberg subject index files/g disk/guinn... · mr....

40
r 488 HS C VOL 7 -F fc I Commission? expert opinion, did the FBI do an adequate job in their ballistics test after the death of President Kennedy and for the Warren explanation of? today that you would like to comment on or make any extra revolvers relating to any of the testimony that has been given members: Is there anything related to the rifle or either of the two olar. EDGAR. Thank you. Let me just ask each of you as panel Mr. EDGAR. Let me ask you one final question, then. In your Mr. CHAMPAGNE. No, sir. Mr. CHAMPAGNE. I would say, considering the pressures at the time, the FBI did a very good job. Mr. EDGAR. Are there any tests that you would have done at the time that were not done? Mr. CHAMPAGNE. No, sir. . Mr. EDGAR. Thank you. Mr. Chairman, I have no further ques- tions. Chairman STOKES. The time of the gentleman has expired. The Chair recognizes the gentleman from Indiana, Mr. Fithian. Mr. FITHIAN. Thank you, Mr. Chairman. I wonder if the panel, any one of all of you, would comment on what has been one of the widely written about and discussed features of the actual shooting. As I understand it, the distance from the window where Oswald was supposed to have been located to the President was 165 feet. With that weapon which you now have inspected and test fired, how difficult a shot is it with the scope or without the scope, sort of from left to right? Mr. LUTZ. The answer I would give, I believe, would be that it would not appear to be a difficult shot with either device with reasonable training or a reasonable capability of a firer that was familiar with that firearm. I personally feel that the iron sights would have provided a better capability because of the problems of sighting through the other device, through-the telescopic sight, but I feel that it could have very easily been accomplished from that distancae with that rifle. Mr. FITHIAN. And with the car moving at the estimated speed? Mr. LUTZ. From the data I have about the movement of the vehicle and the speeds involved, I still feel that it would not have been a difficult target at that distance. Mr. FITHIAN. Is there any other member of tlit panel who be- lieves that it would be somehow an exceptional feat to have hit the target from that range? Mr. BATES. I don't believe so, no. Mr. CHAMPAGNE. No, sir. Mr. FITHIAN. Mr. Newquist stated, I believe, that the panel could not match their own test•fired bullets with either the FBI's tests from 1963—maybe I rnisnderstood this—or the so-called pristine bullet that has been so much talked about and the bullet frag- ments removed from the limousine? One of the reasons theorized that a match could not be made was that the rifle had been fired too often, somehow destroying or altering the land-and-groove markings. Does anyone on the panel know how many times the weapon was fired by the FBI? 489 Mr. BATES. No; I do not. Mr. CHAMPAGNE. Are you referring just to the FBI firing it or the number of times it was actually fired? Mr. FImLAN. I was just going in the order I though: it was fired once it was acquired by the FBI and then by the committee panel and by anybody else. I was trying to get at how much actual wear and alteration there has been. Let me rephrase the question. I am informed by our counsel that the weapon has been fired over 100 times. Is that sufficient wear that it would significantly alter the markings and :he identifica- tions? Mr. CHAMPAGNE. Yes; I think with this type of weapon and the type of bullets involved, that it is. I think that probably the weapon has been fired more than 100 times. Mr. FITHIAN. Mr. Chairman, I have no other questions of this panel. Chairman STOKES. The time of the gentleman has expired. Gentlemen, any witnesses appearing before this committee are entitled, after they have concluded their testimony, to 5 additional minutes in which to explain, amplify, or in any manner expand upon their testimony. On behalf of the committee I at this time extend to you 5 minutes in which any of you may make any comments you so desire. Mr. Luzz. I don't believe there is any further expanding on the examinations that we have conducted. I think we feel that they have been as thorough as could have possibly been done. We have been given the opportunity to examine every piece of evidence that we asked for. We didn't have any restrictions. We weren't bound to come up with a particular finding. So I think in that respect we have been very fortunate to conduct an objective examination. I also would like to express on behalf of the entire panel the thanks to our own employers, the State of Wisconsin, the State of Florida, the State of Iowa, the State of New York, and the Metro- politan Police Department of the District of Columbia for allowing us to participate in this panel. I would like further to extend on behalf of the entire panel our appreciation to the staff of the committee, for the assistance they have given us and especially to thank the committee itself for the privilege and the honor of ap- pearing before it. Chairman STOKES. We certainly deem ourselves fortunate to have had such a distinguished panel of experts lend their services to this cause. We appreciate all the time that you have expended on behalf of the report that you have brought to the committee and the testimony you have given us here today. We express at this time our very deep appreciation to each of you for the services that you have rendered. Thank you. The Chair recognizes Professor Blakey. NARRATION BY G. ROBERT BLAKEY. CHIEF COUNSEL AND _ - STAFF DIRECTOR Mr. BLAKEY. Thank you, Mr. Chairman. Mr. Chairman. there have been several prior attempts to analyze missiles and fragments recovered from the assassination from the standpoint of their m c-

Upload: others

Post on 21-Jul-2020

0 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

r 488

HS C

VO

L

7-F

fc—I

Com

mission?

expert o

pin

ion, d

id th

e FB

I do an

adeq

uate jo

b in

their b

allistics test after th

e death

of P

residen

t Ken

ned

y an

d fo

r the W

arren

explanation of? to

day

that y

ou w

ould

like to

com

men

t on o

r mak

e any ex

tra rev

olv

ers relating to

any o

f the testim

ony th

at has b

een g

iven

m

embers: Is there anything related to the rifle or either of the tw

o

olar. E

DG

AR

. Than

k y

ou. L

et me ju

st ask each

of y

ou as p

anel

Mr.

ED

GA

R.

Let m

e ask y

ou o

ne fin

al questio

n, th

en. In

your

Mr. C

HA

MP

AG

NE

. No, sir.

Mr.

CH

AM

PA

GN

E. I w

ould

say, co

nsid

ering th

e pressu

res at the

time, the F

BI did a very good job.

Mr. E

DG

AR

. Are th

ere any tests th

at you w

ould

hav

e done at th

e tim

e that were not done?

Mr. C

HA

MP

AG

NE

. No, sir.

. M

r. E

DG

AR

. Than

k y

ou. M

r. Chairm

an, I h

ave n

o fu

rther q

ues-

tions. C

hairman

STO

KE

S. The tim

e of th

e gen

tleman

has ex

pired

. The

Chair recognizes the gentlem

an from Indiana, M

r. Fithian.

Mr.

FIT

HIA

N. T

han

k y

ou, M

r. Chairm

an. I w

onder if th

e pan

el, any one of all of you, w

ould comm

ent on what has been one of the

widely w

ritten about and discussed features of the actual shooting. A

s I understan

d it, th

e distan

ce from

the w

indow

where O

swald

w

as supposed

to h

ave b

een lo

cated to

the P

residen

t was 1

65 feet.

With

that w

eapon w

hich

you n

ow

hav

e insp

ected an

d test fired

, how

difficult a shot is it with the scope or w

ithout the scope, sort of from

left to right? M

r. L

UT

Z. T

he an

swer I w

ould

giv

e, I believ

e, would

be th

at it w

ould

not ap

pear to

be a d

ifficult sh

ot w

ith eith

er dev

ice with

reaso

nab

le trainin

g o

r a reasonab

le capab

ility o

f a firer that w

as fam

iliar with that firearm

. I

perso

nally

feel that th

e iron sig

hts w

ould

hav

e pro

vid

ed a

better cap

ability

becau

se of th

e pro

blem

s of sig

htin

g th

rough th

e oth

er dev

ice, thro

ugh-th

e telescopic sig

ht, b

ut I feel th

at it could

have very easily been accom

plished from that distancae w

ith that rifle.

Mr. F

ITH

IAN

. And w

ith th

e car movin

g at th

e estimated

speed

? M

r. L

UT

Z.

Fro

m th

e data I h

ave ab

out th

e movem

ent o

f the

veh

icle and th

e speed

s involv

ed, I still feel th

at it would

not h

ave

been a difficult target at that distance. M

r. F

ITH

IAN

. Is there an

y o

ther m

ember o

f tlit pan

el who b

e-lieves that it w

ould be somehow

an exceptional feat to have hit the target from

that range? M

r. BA

TE

S. I don't believe so, no.

Mr. C

HA

MP

AG

NE

. No, sir.

Mr. F

ITH

IAN

. Mr. N

ewquist stated, I believe, that the panel could

not m

atch th

eir ow

n test•fired

bullets w

ith eith

er the F

BI's tests

from 1963—

maybe I rnisnderstood this—

or the so-called pristine bullet th

at has b

een so

much

talked

about an

d th

e bullet frag

-m

ents removed from

the limousine?

One of the reasons theorized that a m

atch could not be made w

as th

at the rifle h

ad b

een fired

too o

ften, so

meh

ow

destro

yin

g

or

altering the land-and-groove markings. D

oes anyone on the panel know

how m

any times the w

eapon was fired by the F

BI?

489

Mr. B

AT

ES

. No; I do not.

Mr.

CH

AM

PA

GN

E. A

re you referrin

g ju

st to th

e FB

I firing it o

r the num

ber of times it w

as actually fired? M

r. FIm

LA

N. I w

as just going in the order I though: it was fired

once it w

as acquired by the FB

I and then by the comm

ittee panel and by anybody else. I w

as trying to get at how m

uch actual wear

and alteration there has been. L

et me rephrase the question. I am

informed by our counsel that

the w

eapon h

as been

fired o

ver 1

00 tim

es. Is that su

fficient w

ear th

at it would

significan

tly alter th

e mark

ings an

d :h

e iden

tifica-tions?

Mr. C

HA

MP

AG

NE

. Yes; I th

ink w

ith th

is type o

f weap

on an

d th

e ty

pe o

f bullets in

volv

ed, th

at it is. I thin

k th

at pro

bab

ly th

e w

eapon has been fired more than 100 tim

es. M

r. FIT

HIA

N. M

r. Chairm

an, I have no other questions of this panel.

Chairm

an STO

KE

S. The tim

e of the gentleman has expired.

Gen

tlemen

, any w

itnesses ap

pearin

g b

efore th

is com

mittee are

entitled, after they have concluded their testimony, to 5 additional

min

utes in

which

to ex

plain

, amplify

, or in

any m

anner ex

pan

d

upon th

eir testimony. O

n b

ehalf o

f the co

mm

ittee I at this tim

e ex

tend to

you 5

min

utes in

which

any o

f you m

ay m

ake an

y

comm

ents you so desire. M

r. Luzz. I d

on't b

elieve th

ere is any fu

rther ex

pan

din

g o

n th

e ex

amin

ations th

at we h

ave co

nducted

. I thin

k w

e feel that th

ey

have been as thorough as could have possibly been done. We have

been given the opportunity to examine every piece of evidence that

we asked for. W

e didn't have any restrictions. We w

eren't bound to co

me u

p w

ith a p

articular fin

din

g. S

o I th

ink in

that resp

ect we

hav

e been

very

fortu

nate to

conduct an

objectiv

e exam

inatio

n.

I also w

ould

like to

express o

n b

ehalf o

f the en

tire pan

el the

thanks to our own em

ployers, the State of W

isconsin, the State of

Florida, the S

tate of Iowa, the S

tate of New

York, and the M

etro-politan P

olice Departm

ent of the District of C

olumbia for allow

ing us to

particip

ate in th

is pan

el. I would

like fu

rther to

exten

d o

n

beh

alf of th

e entire p

anel o

ur ap

preciatio

n to

the staff o

f the

comm

ittee, for the assistance they have given us and especially to th

ank th

e com

mittee itself fo

r the p

rivileg

e and th

e honor o

f ap-

pearing before it. C

hairman ST

OK

ES. W

e certainly deem ourselves fortunate to have

had such a distinguished panel of experts lend their services to this cau

se. We ap

preciate all th

e time th

at you h

ave ex

pen

ded

on

beh

alf of th

e report th

at you h

ave b

rought to

the co

mm

ittee and

the testim

ony y

ou h

ave g

iven

us h

ere today

. We ex

press at th

is tim

e our very deep appreciation to each of you for the services that you have rendered. T

hank you. T

he Chair recognizes P

rofessor Blakey.

NA

RR

AT

ION

BY

G. R

OB

ER

T B

LA

KE

Y. C

HIE

F C

OU

NS

EL

AN

D

_ - S

TA

FF

DIR

EC

TO

R

Mr.

BL

AK

EY

. Than

k y

ou, M

r. Chairm

an. M

r. Chairm

an. th

ere have been several prior attem

pts to analyze missiles and fragm

ents recovered from

the assassination from the standpoint of their m

c-

Page 2: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

491 -I tallic m

akeu

p to

determ

ine, fo

r one p

ossib

ility, if th

ey h

ave a

comm

on origin. In N

ovember and D

ecember 1963 the F

BI applied to the evidence

samples a technique called em

ission spectography. It is a process in w

hich

the sam

ples are su

bjected

to in

tense h

eat and th

eir metallic

com

positio

n is d

etermin

ed b

y th

e colo

r of th

e gas th

at is then

em

itted. E

missio

n sp

ectograp

hy, h

ow

ever, is n

ot h

ighly

sensitiv

e and the tests w

ere deemed by the F

BI inconclusive.

In May 1964 the F

BI also perform

ed neutron activation analysis on som

e of the samples. T

hat is a nuclear method to determ

ine the elem

ents p

resent. A

n an

alysis o

f trace elemen

ts found in

the

sample o

f similar m

aterials—fo

r exam

ple, b

ullet lead

—en

ables a

highly trained scientist to come to a conclusion as to the probabil-

ity of thesamples having a com

mon origin.

Nev

ertheless, "in

conclu

sive" w

as also th

e term u

sed b

y th

e FB

I to describe its neutron activation analysis. T

he report it submitted

to th

e Warren

Com

missio

n stated

that th

e tests would

not, q

uote,

,*perm

it positiv

ely d

ifferentiatin

g am

ong th

e larger b

ullet frag

-m

ents an

d th

us p

ositiv

ely d

etermin

ing fro

m w

hich

of th

e larger

bullet frag

men

ts any g

iven

small lead

fragm

ent m

ay h

ave co

me,"

unquote. T

he Warren C

omm

ission did not divulge that the neutron activa-tion analysis had taken place in its final report. Indeed the fact did not becom

e public until the early 1970's. H

opefu

l that n

ew tests m

ight su

cceed w

here o

ld effo

rts had

failed

, the co

mm

ittee engag

ed as a co

nsu

ltant D

r. Vin

cent P

. G

uin

n, p

rofesso

r of ch

emistry

at the U

niv

ersity o

f Califo

rnia at

Irvin

e. Dr. G

uin

n h

ad n

o relatio

n to

the W

arren C

om

missio

n. D

r. G

uinn analyzed the assassination evidence samples as w

ell as the bullet allegedly fired at G

eneral Walker.

In h

is experim

ents, D

r. Guin

n u

sed a h

igh reso

lutio

n lith

ium

-drifted germ

anium detector, a device that is far m

ore sensitive, and hopefu

lly accu

rate, than

the o

ne u

sed fo

r the F

BI test in

1964.

Dr. G

uin

n receiv

ed an

A.B

. and an

M.S

. deg

ree in ch

emistry

from

the University of S

outhern California in 1939 and 1941 and a

Ph. D

. in physical chemistry from

Harvard U

niversity in 1949. Dr.

Guinn studied radioisotopes at the O

ak Ridge Institute of N

uclear S

tudies, Oak R

idge, Tenn., in 1952. H

e is a fellow of the A

merican

Nuclear S

ociety, the Am

erican Academ

y of Forensic S

cientists, and he is a m

ember of the A

merican C

hemical S

ociety. D

r. Guinn has published num

erous scientific articles in the area of activation analysis and forensic chem

istry. He hat' served as an

adviser to such agencies as the Atom

ic Energy C

omm

ission and he has m

ade a training film on neutron activation analysis w

hich is in w

ide use today. It w

ould

be ap

pro

priate, M

r. Chairm

an, at th

is time to

call Dr.

Guinn. C

hairman ST

OK

ES. T

he comm

ittee calls Dr. G

uinn. S

ir, would

you p

lease stand an

d raise y

our rig

ht h

and an

d b

e sw

orn. D

o you solemnly sw

eari the testimony you w

ill give before this. co

mm

ittee is the tru

th, th

e whole tru

th an

d n

oth

ing b

ut th

e truth

, so help you G

od'? D

r. GIA

NN

. Yes. I do.

Chairm

an STO

KE

S. Thank you. Y

ou may be seated.

The C

hair recognizes comm

ittee counsel Jim W

olf. T

EST

IMO

NY

OF D

R. V

INC

EN

T P. G

UIN

N

Mr. W

OL

F. F

or the record, could you please state your full name?

Dr. G

UIN

N. V

incent P. G

uinn. M

r. Wocr. W

here are you currently employed?

Dr. G

UIN

N. A

s a professor of chemistry, U

niversity of California,

Irvine campus.

Mr. W

OL

F.

Are y

ou fam

iliar with

the tech

niq

ue o

f analy

sis of

evidence samples know

n as neutron activation analysis? D

r. QU

INN

. Yes; I have been involved in such w

ork for over 20 years.

Mr. W

OL

F. W

hen did you first personally perform this technique?

Dr. G

UIN

N. A

bout 1956. M

r. WO

LF

. Have you testified in legal proceedings before on the

applicab

ility o

f neu

tron activ

ation an

alysis to

evid

ence sam

ples?

Dr. G

UIN

N. Y

es, on many occasions.

Mr. W

ota. D

id y

ou testify

in th

e capacity

as an ex

pert w

itness?

Dr. G

UIN

N. Y

es. M

r. W

OL

F. In

your cap

acity as an

expert w

itness d

id y

ou b

oth

testify as to sam

ples you had analyzed and performed the analysis

on as well as an evaluation of analyses that other people had done?

Dr. G

UIN

N. Y

es, both of them.

Mr. W

ord. Approxim

ately how m

any times have you testified in

your capacity as an expert witness?

Dr. G

UIN

N. I w

ould say approximately 50 tim

es. M

n W

OL

F. G

enerally, Dr. G

uinn, why w

ould one subject an evi-dence sam

ple to neutron activation analysis? D

r. GU

INN

. It dep

ends o

n th

e kin

d o

f evid

ence sam

ple, b

ut fo

r m

any k

inds th

e purp

ose is to

detect v

arious elem

ents in

the sam

- ples and com

pare specimens to see if they are sufficiently sim

ilar in

com

positio

n th

at it indicates a h

igh p

robab

ility o

f com

mon

origin or, if they differ widely, a definite probability of noncom

mon

origin. M

r. WO

LF

. So it may be possible, by neutron activation analysis,

to determine if tw

o or more unknow

n evidence specimens are from

the sam

e batch or item, is that correct?

Dr. Q

UIN

N. T

hat is correct. M

r. WO

LF

. To u

se an ex

ample, if a crim

e had

been

com

mitted

an

d th

e victim

hit o

ver th

e head

with

an ax

, and m

etal fragm

ents

were found in the skull of the victim

, might you be able to analyze

the m

etal fragm

ents fo

und in

the sk

ull to

see if they

match

ed th

e ty

pe o

f ax th

at was fo

und in

a particu

lar perso

n's h

ouse w

ho is

accused of that crime?

Dr. G

UIN

N. Y

es; if one found the same elem

ents at approximate-

ly th

e same co

ncen

trations in

both

, you co

uld

establish

that th

ere w

as a good p

robab

ility th

at it came fro

m th

e same ty

pe o

f ax. It

wouldn t identify that particular ax because there m

ight have been a h

undred

or so

mad

e of th

e same b

atch o

f metal b

ut it w

ould

establish that particular brand and production lot perhaps.

Mr. W

OL

F. Is it easier F

or you to state your conclusion that two

objects are alik

e or is it easier to

establish

the co

nclu

sion th

e two

items are not alike?

Page 3: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

4V2

Dr. G

UIN

N. It is m

uch easier to exclude; if you find two sam

ples that differ m

arkedly, it is easy to say definitively they did not have a co

mm

on o

rigin

. If they

look sim

ilar in co

mpositio

n, th

en y

our

first statemen

t is: "They

may

hav

e a com

mon o

rigin

," and y

ou

have to look more carefully and look at background data that you

have obtained on such materials to try to even estim

ate a probabil-ity that they really do have a com

mon origin.

Mr.

WO

LF

. B

riefly, D

r. Guin

n, I w

ould

like to

ask y

ou a few

general questions about procedures one w

ould employ to do a neu-

tron activation analysis. If, for example, you had a m

etal specimen

to test, what w

ould you do to that metal specim

en to prepare it for testing?

Dr. G

utstx. On m

any kinds of samples it is necessary to rem

ove, as best you can, any external contam

ination, dust, moisture, or salt

from handling and perspiration. Y

ou may have to w

ash them, then

dry

them

, and so

on, ju

st to g

et rid o

f extern

al, extran

eous co

n-

tamination that w

ould otherwise change the m

easured composition

from w

hat the real material w

as. That is quite com

mon.

Mr.

WO

LF

. After p

reparin

g th

e sample, y

ou w

ould

then

insert

that sample in a nuclear reactor, is that correct?

Dr. G

UIN

N. Y

ou normally place the individual sam

ples in small

plastic (polyethylene) vials as a container and, of course, you put that into the nuclear reactor.

Mr.

WO

LF

. And th

e sample w

ould

be m

ade rad

ioactiv

e after it w

as placed in the nuclear reactor, is that correct? D

r. G

UIN

N. Y

es; in th

e reactor th

e purp

ose is to

bom

bard

the

sample w

ith n

eutro

ns. T

he n

eutro

ns—

som

e of th

em g

et captu

red

by th

e nuclei o

f the d

ifferent k

inds o

f atom

s in th

e sample, an

d

that makes som

e of these radioactive. So w

hen the sample com

es out—

particularly metal sam

ples—there is no change in w

eight that you can m

easure, there is no change in appearance, but the sample

is now

radio

active an

d y

ou can

then

test it with

suitab

le countin

g

equipment.

Mr.

WO

LF

. N

ow

, radio

active m

aterials decay

, is that co

rrect? D

r. Guirese Y

es. Differen

t radio

isoto

pes h

ave d

ifferent rates o

f decay.

Mr. W

OL

F. C

an you explain in layman's term

s what "radioactive

decay" means?

Dr. G

m-sm

. "Rad

ioactiv

e decay

" mean

s that an

even

t occu

rs in

the n

ucleu

s of an

atom

resultin

g in

it releasing en

ergy an

d p

ene-

trating rad

iation an

d/o

r a particle su

ch as a b

eta pactbicle, w

hich is a h

igh-en

ergy electro

n. In

the p

rocess, it ch

anges n

orm

ally to

a stable isotope, of the next elem

ent in the case of beta-minus em

is-sion. T

he process of that decay is called "radioactivity" or "radioac-tive decay.

Som

e elemen

ts hav

e a num

ber o

f differen

t radio

isoto

pes th

at hav

e been

mad

e in th

e reactor w

ith n

eutro

ns. S

om

e of th

em w

ill only

form

one rad

ioiso

tope; so

me w

ill form

two o

r three. T

he

radioisotopes of different .elements are characterized by the ener-

gies of the radiations that', they emit in the process of decaying and

also b

y th

eir half-liv

es, vith

ich is a m

easure o

f how

- rapid

ly th

ey

decay away.

Mr. S

limy. Y

ou are tellin

g u

s differen

t elemen

ts hav

e differen

t radioactive half-lives and, by detecting the radioactive decay of the

493

unknown sam

ple, you would be able to identify the elem

ents pres-ent in that sam

ple, is that correct? D

r. GU

INN

. Yes, particularly, in practice, by looking at the ener-

gies o

f the g

amm

a rays th

at are emitted

by th

e sample, rath

er th

an actu

ally m

easurin

g th

e halflife. W

e mak

e use o

f the h

alflife but w

e don't usually actually measure it.

Mr. W

OL

F. W

hat are some of the different types of m

aterials you have tested by neutron activation analysis for the purpose of com

-parison?

Dr. G

UIN

N. W

ell, almost all the kinds of m

aterials you can think of that m

ay get involved in some kind of crim

inal case—gunshot

residues, bullet lead, glass, paint, paper, cloth, oil, greases, and so on and on and on.

Mr. W

OL

F. H

ow m

any different types of bullets have you exam-

ined by neutron activation analysis? D

r. G

UIN

N. A

pproximately 165 different actual, know

n brands and know

n production lots of bullets. M

r. WO

LF

. Were these of different calibers as w

ell as manufac-

turers? D

r. GU

INN

. Yes; they covered the full range of calibers as w

ell. M

r. WO

LF

. What elem

ents have you found were the m

ost distinct to distinguish am

ong different brands of bullets? D

r. Gum

w. L

ooking over all of the data that we have obtained

and also other people have obtained who have been using the sam

e general approach, w

e find there are three elements that com

monly

show

up in

bullet lead

s but at w

idely

differen

t concen

trations,

dep

endin

g u

pon w

hich

bullet lead

it is. These th

ree elemen

ts ate antim

ony, silver, and copper. A

nd I would

say th

at that is ab

out th

e appro

xim

ate ord

er of

importance—

that is, antimony being perhaps the m

ost informative

or th

e most critical elem

ent to

measu

re; silver, v

ery clo

se to it;

copper, somew

hat less, though, mainly because copper w

ouldn't be so

bad

in an

d o

f itself but, in

crimin

al cases, you v

ery freq

uen

tly

are lookin

g at little b

its and p

ieces of b

ullets, an

d th

e orig

inal

bullets were copper-jacketed and that m

eans some of the fragm

ents you get m

ay have a little bit of copper imbedded in them

physically that you can't see and yet it w

ill show up m

arkedly in the analysis. S

o the copper numbers can often bounce around.

Mr.

WO

LF

. A

re oth

er elemen

ts found to

be p

resent in

bullets

when you analyze them

, apart from antim

ony, silver, and copper? D

r. G

UIN

N. W

ell, man

y tim

es in b

ullets, u

nder th

e conditio

ns

that w

e norm

ally u

se, you w

ill just see those th

ree. Very

often

, unless y

ou v

ery carefu

lly clean

them

, you w

ill find a little b

it of

sodium and a little bit of chlorine, com

ing from salt, w

hich may be

from

persp

iration if an

ybody h

as han

dled

the sp

ecimen

s, or salt

spray

in th

e air if it is anyw

here n

ear the o

cean, fo

r exam

ple.

Often you w

ill find a little trace of manganese, not so m

uch that it is com

mon but w

e happen to be extremely sensitive for m

anganese. T

he main reason for using the activation analysis m

ethod is that it is an extrem

ely sensitive method. it w

ill detect very small con-

centratio

ns, b

ut- it d

oesn

t hav

e the sam

e sensitiv

ity fo

r all ele-m

ents. Som

e are far more sensitive than others. S

o we som

etimes

see a little man

gan

ese : occasio

nally

a little alum

inum

, once in

a w

hile some arsenic or tin.

Page 4: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

494

Th

at abo

ut co

vers all o

f the elem

ents th

at we h

ave ev

er seen in

all bullet leads.

Mr.

WO

LF

. Have you analyzed M

annlicher-Carcano bullets pro-

duced by the Western C

artridge Co. (W

CC

)? D

r. GU

INN

. Yes, I have.

Mr. W

OL

F. W

hen did you do these analyses? D

r. GU

INN

. A num

ber of years ago. I believe I started doing the first an

alyses ab

ou

t 19

73

. A co

lleagu

e, no

t at Irvin

e bu

t at the

University of K

ansas, Dr. John N

ichols, had been interested in the P

residen

t Ken

ned

y case fo

r quite so

me tim

e and h

e contacted

me

and said he had been able to acquire boxes of Mannlicher-C

arcano am

munition from

the four production lots that had been produced by th

e WC

C, an

d h

e was w

onderin

g if I w

ould

be in

terested in

doin

g an

alyses o

n th

em sin

ce I had

earlier analy

zed a lo

t of o

ther

kinds of bullets. I said yes, and I did, and we found som

e unusual features about W

CC

Mannlicher-C

arcano amm

unition that showed

it was different from

most kinds of bullets.

Mr. W

ei's. Prio

r to g

etting

into

tho

se features, d

id y

ou

exam

ine

bu

llets from

every

lot p

rod

uced

by

the W

estern C

artridg

e Co

.? D

r. GU

INN

. Yes. T

he W

estern C

artridg

e Co

. repo

rtedly

mad

e 1

million rounds of each of 4 production runs, lots 6,000, 6,001, 6,002,

and 6,003. They w

ere made at different tim

es in 1954, and report-edly those are the only lots they ever produced, and w

e had boxes from

each of those lots. M

r. WO

LF

. Addressing your analyses, did you find W

CC

Mann-

licher-C

arcano

bu

llets differed

from

mo

st oth

er bu

llets yo

u h

ad

analyzed? D

r. GU

INN

. Yes; they did.

Mr. W

OL

F. H

ow did they differ?

Dr. G

UIN

N. W

ell, as of th

e time th

at I first measu

red th

em, th

ey

had a lower antim

ony content than I had encountered prior to that in

most o

ther b

ullets, b

ecause a v

ery larg

e percen

tage o

f bullets

you d

o lo

ok at, co

mm

ercial ones, are h

arden

ed lead

, where they

deliberatedly add anywhere from

half a percent up to perhaps 4 or 5

percen

t antim

on

y to

mak

e the lead

mu

ch h

arder. A

very

large

percen

tage o

f com

mercial b

ullets d

o h

ave h

arden

ed lead

. So

we

have usually found much higher antim

ony levels than in the WC

C

Mannlicher-C

arcano bullets. M

r. WO

LF

. And W

CC

Mannlicher-C

arcano bullets are considered unhardened bullets. Is that correct?

Dr. G

UIN

N. T

hey

are defin

itely u

nhard

ened

bultits. T

hat p

uts

them dow

n much low

er in antimony than m

ost bullets. S

ubseq

uen

tly w

e—in

lookin

g at a lo

t more b

rands in

the in

ter-im

—did find som

e others that were also low

, some of them

lower

yet in antimony, but that w

as one unusual feature. T

he o

ther u

nu

sual featu

re of th

e WC

C M

ann

licher-C

arcano

is that there seem

s to be no uniformity w

ithin a production lot. That

is, even

wh

en w

e wo

uld

take a b

ox

of cartrid

ges all fro

m a g

iven

pro

ductio

n lo

t, take 1

cartridge o

ut an

d th

en an

oth

er and th

en

anoth

er and th

en an

oth

er. all out o

f the sam

e box—

boxes o

f 20,_

th

ese were—

and an

alyie th

em, th

ey all in

gen

eral look d

ifferent

and widely different. particularly in their antim

ony content. T

his is n

ot tru

e of most bullet leads that w

e have ever looked at before, w

hich are very uniform. In general, if you take m

ost boxes

495

of amm

unition—and w

e published on this; it is in the literature—tak

e a bu

nch

of th

em o

ut, y

ou

can't tell o

ne fro

m th

e oth

er. Th

ey

all look like little carbon copies even to activation analysis, but not so w

ith the Mannlicher-C

arcano. M

r. WO

LF

. Did any of the 165 know

n brands and lots of bullets y

ou

hav

e prev

iou

sly ex

amin

ed h

ave co

nstitu

ent ran

ges th

at were

the same as the W

CC

Mannlicher-C

arcano bullets _a their antimo-

ny and silver characteristics? D

r. G

UIN

N.

Yes; th

e rang

e of th

e WC

C M

ann

lieher-C

arcano

s, esp

ecially in

the an

timony co

nten

t, is so w

ide th

s: it does encom-

pass some of the others w

hich are down at that low

end; and out of 165, there w

ere 4 different groups, .1 U.S

. made and 3 foreign m

ade, that fell som

ewhere in that range.

Mr. W

OL

F. A

ddressing the work you did for this com

mittee, D

r. G

uinn, where did you obtain the evidence sam

ples that you exam-

ined for this comm

ittee? D

r. GU

INN

. Well, it w

as durin

g last y

ear. First o

f all, we m

ade

the arran

gem

ents in

advan

ce, and th

en in

Sep

tember o

f last year

Mr. Jam

es L. G

ear of th

e Natio

nal A

rchiv

es bro

ug

ht th

e samp

les out. H

e flew out w

ith them and brought them

down w

ith a couple of F

ederal guards, down to the laboratory, m

y laboratory at Irvine. M

r. WO

LF

. All th

e samp

les yo

u ex

amin

ed fo

r this co

mm

ittee w

ere obtained from the N

ational Archives, is that correct?

Dr. G

UIN

N. Y

es. M

r. WO

LF

. How

man

y item

s were b

rought to

you fro

m th

e Na-

tional Archives for you to first exam

ine? D

r. GU

INN

. There w

ere 10 different specimens that had C

E auin-

bers an

d/o

r FB

I Q n

um

bers attach

ed to

them

-10 d

ifferent o

nes.

Mr. W

OL

F. D

id y

ou

test all these 1

0 d

ifferent item

s by

neu

tron

activiation analysis?

Dr. G

UIN

N. N

o. T

he first th

ing w

e did

was fo

r me to

look o

ver

the samples to see if they w

ere suitable for analysis—if there w

as an

yth

ing left th

ere to an

alyze fo

r one th

ing, if an

analy

zable

sample could be obtained. T

hree of them w

ere not suitable. M

r. WO

LF

. Wh

ich th

ree items w

ere no

t suitab

le for an

alysis?

Dr. G

UIN

N. L

et me ju

st check

so I can

get th

e pro

per n

um

bers

for them. O

ne was the so-called D

allas curbing sample.

Mr. W

OL

F. Is that F

BI N

o. Q-609?

Dr. G

UIN

N. Y

es; the FB

I number w

as Q-609. T

hat was a piece of

curb

ing th

at was cu

t away

in D

ealey P

laza becau

se it appeared

th

ere was a sm

ear that m

igh

t be fro

m a g

razing

bu

llet, and

that

was b

rou

gh

t ou

t to th

e labo

ratory

. Bu

t after loo

kin

g at it, it w

as q

uite ap

paren

t that th

ere wo

uld

be n

o w

ay—

it was ju

st hard

ly a

visible smudge. T

o get a sample rem

oved from it, you w

ould have to

scrape it an

d y

ou w

ould

end u

p w

ith a sample that w

as mostly

cement.

You m

ight b

e able to

detect a little an

timony o

r som

ethin

g lik

e th

at, bu

t yo

u co

uld

nev

er relate it to a p

articular k

ind

of b

ullet

lead. This had beettscraped before by F

BI to take th

eir samp

les for em

ission sp

ectograp

hy. an

d th

at is why p

ractically n

oth

ing w

as left.

Mr. W

OL

F. W

hat are the other samples that w

ere not suitable for analysis?

Page 5: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

496

Dr. G

uth

rie. Anoth

er one w

as FB

I Q-3

, which

has a C

om

missio

n

num

ber, C

E-5

69. T

hat w

as reported

ly a frag

men

t recovered

from

th

e fron

t seat of th

e Dallas lim

ou

sine.

Mr. W

OL

F. W

hy w

as that n

ot su

itable fo

r analy

sis? D

r. GU

INN

. That

was a sizab

le fragm

ent, b

ut it w

as on

ly th

e jack

et material. T

he lead

that h

ad b

een in

side o

f it was all g

on

e an

d, sin

ce I was try

ing to

analy

ze bullet lead

, not jack

et material,

there w

as noth

ing left in

that o

ne to

analy

ze. M

r. WO

LF

. Th

e third

item th

at was u

nsu

itable fo

r analy

sis was

what?

Dr. G

om

a. FB

I Q-1

5, w

hich

' also h

as CE

No. 8

41. T

hat w

as rep

orted

ly so

me v

ery tin

y p

articles scraped

from

the in

side su

rface o

f the w

ind

shield

of th

e Dallas lim

ou

sine. A

pp

arently

in th

e prev

i-ous F

BI em

ission sp

ectrograp

hic ex

amin

ations th

at little bit o

f m

aterial had

been

com

pletely

used

up

. We o

pen

ed th

e con

tainer

but w

e could

find n

oth

ing in

there, n

otin

g in

there at all, ev

en w

ith

magnification. M

r. WO

LF

. Ad

dressin

g th

e items y

ou

did

analy

ze for th

e Co

mm

it-tee, co

uld

you d

escribe w

here th

e two item

s in w

hat y

ou h

ave

characterized

as gro

up

2 w

ere fou

nd

, Co

mm

ission

exh

ibit 5

73

and

C

omm

ission exhibit 141? D

r. GU

INN

. Yes; just for convenience of discussion I have grouped

the sev

en sp

ecimen

s that w

ere analy

zed—

that I d

id an

alyze—

into

these tw

o groups. Group 2 consisted of just tw

o specimens: F

BI Q

-8, w

hich

also h

as the C

om

missio

n N

o. C

E-1

41

. Th

at is wh

at has b

een

referred to

recently

here, to

o, as th

e com

plete, u

nfired

Western

C

artridge C

o. 6

lie-millim

eter cartridge rep

orted

ly fo

und in

the

cham

ber o

f the M

ann

licher-C

arcano

rifle fou

nd

in th

e Tex

as Sch

oo

l D

epository Building on N

ovember 22, 1963.

Mr. W

OL

F. A

nd Com

mission exhibit 573?

Dr. G

imes,. Y

es; Com

misio

n ex

hib

it 573 is th

e oth

er one, w

hich

has an

FB

I num

ber o

f Q-1

88 also

. It is a mash

ed b

ullet still in

tae jack

et, and

it is the en

e that w

as repo

rtedly

fired at G

en. E

dw

in

Walk

er in A

pril o

f 1963. I to

ok sam

ples o

f both

of th

ose, o

f the

bullet lead

, and an

alyzed

them

. M

r. W

OL

F.

Addressin

g th

e five ev

iden

ce fragm

ents w

hich

you

exam

ined

in w

hich

you called

gro

up 1

, all of w

hich

were alleg

edly

fo

un

d in

or n

ear the o

ccup

ants o

f the P

residen

t's limo

usin

e, cou

ld

yo

u g

ive th

eir Co

mm

ission

exh

ibit n

um

bers an

d state w

here th

ey

were found, please?

D

r. GU

INN

. Yes; th

e first one w

ould

be C

om

missio

n ex

hib

it 399.

That is th

e specim

en o

ften referred

to as th

e pristin

e bullet, rep

ort-

ed

ly fo

un

d o

n th

e stre

tch

er a

t Park

lan

d M

em

oria

l Ho

spita

l in

Dallas that afternoon of N

ovember 22, 1963,

[Interru

ptio

n fro

m th

e floo

r.] C

hairm

an

STO

KE

S. T

he g

entle

man in

the re

ar o

f the ro

om

is req

uested

to rem

ov

e him

self from

the ro

om

. C

ounsel, you may proceed.

Mr. W

OL

F. D

r. Gut*

. if we co

uld

again

start with

the item

s that

we h

ave p

laced in

gro

up 1

of th

e items, all fo

und in

or n

ear the

eccucan

ts of th

e Presid

ent's lim

ousin

e, and if y

ou co

uld

giv

e their

Co

rrun

ission

exh

ibit n

um

bers an

d th

e locatio

n w

here th

ey

were

allegedly found.

491

Dr. Q

UIN

N. T

he first of the five was C

E-399. T

hat is the so-called pristin

e bullet rep

orted

ly fo

und o

n a stretch

er at Park

land M

emo-

rial Hosp

ital in D

allas. The seco

nd w

as Com

missio

n ex

hib

it 567.

Th

at was a m

ashed

large b

ullet frag

men

t still in its jack

et repo

rt-ed

ly reco

vered

from

the fro

nt seat o

f the D

allas limousin

e. T

he th

ird o

ne, C

E-8

43

, con

sisted o

f on

e larger frag

men

t and

on

e sm

aller fragm

ent rep

orted

ly reco

vered

from

Presid

ent K

enn

edy

's b

rain at au

top

sy. T

he fo

urth

on

e was C

E-8

42

, on

e larger frag

men

t an

d tw

o sm

aller ones rep

orted

ly reco

vered

from

Govern

or C

onnal-

ly's w

rist durin

g su

rgery

. And th

e fun one w

as CE

-840, frag

men

ts rep

orted

ly reco

vered

from

the rear flo

or o

f the D

allas limo

usin

e. M

r. WO

LF

. Was th

ere any

lead o

n an

y o

f the ev

iden

ce samp

les in

the N

ational A

rchiv

es on th

e cloth

ing o

f Govern

or C

onnally

or

Presid

ent K

enn

edy

that y

ou

cou

ld su

bject to

neu

tron

activatio

n

analy

sis? D

r. GU

INN

. No

t so far as I am

- aware, an

d I d

id n

ot an

alyze an

y

materials fro

m clo

thin

g at all, ju

st these b

ullets o

r bu

llet frag-

men

ts. M

r. Worse. In

additio

n to

the ev

iden

ce samples, y

ou also

mad

e rad

ioactiv

e kn

ow

n stan

dard

s of th

ree elemen

ts, is that co

rrect? D

r. GuIN

N. Y

es, the n

orm

al pro

cedure is to

not o

nly

detect

elemen

ts in sam

ple; b

ut to

measu

re their co

ncen

tration

s qu

anita-

tively

. To

do

this, y

ou

need

to k

no

w, fo

r on

e thin

g, th

e weig

ht o

f th

e sample an

d, seco

nd, y

ou h

ave to

com

pare th

e radio

activities

that y

ou o

bserv

e in th

e activated

samples w

ith th

ose fro

m stan

dard

sam

ples o

f kn

ow

n w

eigh

ts of th

e elemen

ts that y

ou

are detectin

g.

Mr.

WO

LF

. A

nd th

e three stan

dard

s you u

sed w

ere onE

" .:, co

pp

er, antim

on

y, an

d silv

er, is that co

rrect? D

r. GU

INN

. Th

at is correct.

Mr. W

OL

F. M

r. Ch

airman

, I wo

uld

ask at th

is time to

sho

w th

e w

itness w

hat h

as been

mark

ed as "JF

K ex

hib

it No

. F-3

29

," wh

ich

is a grap

h o

f the d

ecay p

attern o

f an an

itimony stan

dard

. and th

e decay

pattern

of C

om

missio

n ex

hib

it 843, rep

orted

ly a frag

men

t reco

vered

from

Presid

ent K

enn

edy

's brain

du

ring

the au

top

sy.

after each h

ad b

een activ

ated in

the n

uclear reacto

r. D

r. Guin

n, d

id y

ou p

repare th

ese grap

hs?

Dr. G

unest. Yes; I did.

Mr.

WO

LF

. A

nd

add

ressing

yo

urself to

the lo

wer o

f the tw

o

grap

hs, w

hat d

oes th

at grap

h illu

strate? D

r. GU

INN

. Wh

at it sho

ws is th

e peak

in th

e gam

ma-ray

spec-

trum

, the m

easured

gam

ma-ray

spectru

m, fro

m rad

ioactiv

e antim

o-

ny, th

e radio

isoto

pe an

timony 1

22. It h

as one p

rincip

al gam

ma ray

w

ith a certain

energ

y, 5

64,0

00 electro

n v

olts; an

d th

at mean

s as we

measu

re it, it sho

uld

fall in a certain

po

sition

, ho

rizon

tally, o

n th

e sp

ectrum

. W

hat w

e se

e is ju

st an e

nla

rged sm

all p

ortio

n o

f the w

hole

sp

ectrum

. You m

ay n

ote w

e hav

e a chan

nel n

um

ber th

ere and th

is enlarged portion only ranges from

roughly channel Nos. G

OO

to 700. T

he en

tire spectru

m g

oes all th

e way

from

chan

nel 1

to ch

annel

4,0

96. Y

ou can

see this is ju

st a small p

art, but an

y sam

ple L

iles has b

een activ

ated an

d co

unted

under th

ese conditio

ns an

timony in

m

easurab

le qu

antity

sho

uld

sho

w a p

eak at ex

actly th

at locat:o

n.

Page 6: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

213 mg A

NT

IMO

NY

A

NT

IMO

NY

ST

D. S

b - 1 1, =

60 min . td =

55 min

tc=

5 min. L

IVE

TIM

E

TA

GW

OR

D 0050

Om

= 1.0 x 1017 N

/CM

2- SE

C

SE

PT

. 14. 1977

564 keV

122 Sb

12,000

10,000 z

.' 8000

z

0

2000

70,000

60.000

t.0 Z

50,000

40.000

a. 30.000

,n 20,000

10.000

41.9 MIL

LIG

RA

MS

SA

MP

LE

HC

- 4 - 1 564 keV

t = 6

0 m

in.. td = 102

122 Sb

= 5 m

in. LIV

ET

IME

T

AG

WO

RD

0056 O

m=

1.0 x 10' 7 N/C

M2- S

EC

S

EP

T. 14, 1977

670 680

690 C

HA

NN

EL

NU

MB

ER

6000

4000

V.P

. Guinn

700 710

V.P

.Guin

n

496

Mr. W

OL

F. A

nd th

e low

er grap

h, D

r. Guinn, is th

e grap

h o

f the

know

n stan

dard

of an

timony th

at was m

ade rad

ioactiv

e, is that

correct? D

r. GU

INN

. That is correct.

Mr. W

OL

F. A

nd w

hat d

oes th

e upper g

raph illu

strate, which

is th

e decay

pattern

of a frag

men

t reported

ly reco

vered

from

Presi-

den

t Ken

ned

y's b

rain d

urin

g th

e auto

psy

? D

r. GU

INN

. That sh

ow

s the larg

er brain

sample, w

hich

weig

hed

, as it sh

ow

s there-4

1.9

millig

rams is th

e sample w

eight. It w

as irrad

iated in

the reacto

r at the sam

e time th

e standard

was, fo

r th

e same len

gth

of tim

e; and th

en after so

me tim

e of d

ecay after-

ward

, it was th

en co

unted

under th

e same co

nditio

ns, an

d y

ou d

o

see you g

et a peak

at the sam

e locatio

n—

the size o

f the p

eak is

differen

t becau

se the sam

ple an

d stan

dard

don't h

ave th

e same

amount o

f antim

ony, b

ut th

e locatio

n o

f the p

eak is th

e same. T

hat

tells us th

at that sam

ple co

ntain

s antim

ony.

Of co

urse, in

that sp

ectrum

, if you w

ere to lo

ok at th

e entire

spectru

m, y

ou w

ould

see oth

er peak

s due to

copper an

d so

on as

well. B

ut w

e are just lo

okin

g at th

e antim

ony p

art of th

e spectru

m

here. M

r. Wats. W

hat is th

e significan

ce of th

e fact that th

e peak

of

the g

raph ab

ove is d

irectly ab

ove th

e peak

of th

e grap

h b

elow

? D

r. GU

INN

. Well, fallin

g in

the sam

e chan

nel n

um

ber m

eans th

e gam

ma ray

s you are m

easurin

g h

ave th

e same en

ergy, w

ithin

plu

s or m

inus ab

out 1

,000 electro

n v

olts, an

d th

at is what h

elps y

ou

iden

tify it.

Mr. W

OL

F. M

r. Chairm

an, I w

ould

like JF

K ex

hib

it No. F

-328

adm

itted in

to ev

iden

ce at this p

oin

t. C

hairm

an S

TO

KE

S. W

ithout o

bjectio

n, it m

ay b

e entered

into

the

record

at this p

oin

t. [JF

K ex

hib

it No. F

-328 w

as entered

into

the reco

rd.]

670 680

690 C

HA

NN

EL

NU

MB

ER

JFK

Eximirr

F-32S

700 710

Page 7: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

14

00

65

8 ke

V

11

0 A

g

600

41.9

MIL

LIG

RA

MS

S

AM

PL

E H

C -4

. 1

ti = td =

= 4

0 S

EC

ON

DS

A

VG

. % D

EA

DT

IME

= 2

.5%

T

AG

WO

RD

00

07

O

TH

2.5

x 1

012 N

/CM

2 . SE

C

SE

PT

. 13, 1

977

646 keV

124m

1 S

h

_1 600

4C • 4

00

E 300

Z

- 200

0

• 100

658 ke

V

11

0 A

g

V.P

. Guin

n

790

803

810

CH

AN

NE

L N

UM

BE

R

325 m

g S

ILV

ER

1200 S

ILV

ER

ST

D. A

O

I.= t d

= l e

= 4

0 S

EC

ON

DS

A

VG

. °/0 D

EA

DT

IME

=8.5

%

TA

GW

OR

D 0

00

1

OTH

= 2

.5 x 1

0tz

N/C

M2- S

EC

SE

PT

. 13, 1

977

V.P

. Guin

n

200

790

800

810

CH

AN

NE

L N

UM

BE

R

JF

K E

x14181T

F-3

29

501

2 ▪ 1000

z

• 800

rz

1—

D 0

600

400

500

Mr.

WO

LF

. M

r. Chairm

an, I w

ould

like to

hav

e show

n to

the

witn

ess what h

as been

mark

ed

for identification as JFK

exhib

it 329, w

hich is a photograph depicting the decay pattern of a silver stan

dard

and a p

hoto

grap

h d

epictin

g th

e decay

pattern

of a frag

-m

ent removed from

President K

ennedy's brain during the autopsy, after each had been activated in the nuclear reactor.

Dr. G

uin

n, th

e photo

grap

h at th

e botto

m in

dicates th

e decay

pattern of the know

n sample of silver, is that correct?

Dr. G

uiNN

. That is correct.

Mr. W

OL

F. A

nd what does the top graph depict?

Dr.

GU

INN

. It is the sam

e sample th

at you saw

on th

e prev

ious

photograph, the 41.9 milligram

sample of m

aterial removed from

P

residen

t Ken

ned

y's b

rain, b

ut activ

ated th

is time u

nder v

ery

differen

t conditio

ns, v

ery rap

idly

, becau

se we w

ere lookin

g fo

r a very

short liv

ed iso

tope h

ere, nam

ely, th

e radio

active silv

er 110,

which has a half life of only 24.4 seconds. T

hat means it is rapidly

disappearing by decay, dropping in half roughly every 24 seconds. S

o you must look at it very quickly to see it at all.

Mr.

WO

LF

. How

does th

e antim

ony o

n th

e photo

peak

on th

e rig

ht, JF

K ex

hib

it F-3

29, d

iffer from

the an

timony o

n th

e photo

-peak on the upper left?

Dr. G

UIN

N. I p

icked

this o

ne p

articularly

to illu

strate this p

oin

t, th

at even

with

the h

igh reso

lutio

n g

erman

ium

detecto

r you w

ill notice th

at close to

the silv

er peak

of th

e sample, b

ut n

ot o

f the

silver stan

dard

, there is a little p

eak o

ver to

the left, an

d th

at is also

from

radio

active an

timony, b

ut it is fro

m a d

ifferent iso

tope

with

a differen

t half life. T

hat is an

timony —

124 m

,, which

has a

gamm

a-ray energy of 646,000 electronvolts, which brings it close to

the 658,000 electron-volt peak of silver —110. R

ather than use this sm

aller antim

on

y —

12

4 m

, peak

, from

the sh

ort irrad

iation

, to

measu

re the an

timony co

nten

ts quan

titatively

, I used

the m

uch

larg

er peak

of an

timony —

122, fro

m th

e longer irrad

iation, to

obtain

a more p

recise _m

easurem

ent. W

ith silv

er there is really

only one choice, the short-lived silver —

110. M

r. W

OL

F. I w

ould

move th

at JFK

exhib

it F-3

29 b

e adm

itted

into evidence. C

hairman S

TO

KE

S. W

ithout objection, it may be entered into the

record. [T

he above referred to JFK

exhibit F-329 follow

s:] M

r. Wou.. D

r. Guin

n, I w

ould

now

like to

turn

to so

me o

f the

results of the analyses you performed for the com

mittee and som

e of the conclusions you m

ay have obtained. T

urning to the items in w

hat you characterized as group 2, first, this consisted of the alleged bullet fired at G

eneral Walker and the

unfired WC

C M

annlicher-Carcano cartridge. W

as the unfired WC

C

Mannlicher-C

arcano cartridge similar to the previous W

CC

Mann-

licher-Carcano cartridges you had tested?

Dr. G

UIN

N. F

irst of all, I am looking for the table here.

Would you repeat the question, please?

Mr.

WO

LF

. Was the unfired W

CC

Mannlicher-C

arcano cartridge th

at you tested

similar to

the p

revio

us o

nes y

ou h

ad tested

inde-

pendent of the work you did for this com

mittee?

Page 8: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

502

Dr. G

UIN

N. Y

es, sir; the k

ey 'elemen

ts, the an

timon

y and

the

silver, w

ere in th

e sam

e ran

ge a

s the o

ther W

CC

Man

nlich

er-C

arcano sam

ples. T

he an

timon

y was d

efinitely d

own

at the low

er en

d an

d th

e silver was u

p at th

e up

per en

d, b

ut it w

as in th

e same

general ran

ge. M

r. WO

LF

. An

d w

hat w

as the com

position

you fou

nd

in you

r an

alysis of the W

alker b

ullet fragm

ent?

Dr. G

UIN

N. A

bout 1.7 parts p

er million

antim

ony. E

ach valu

e has

a little un

certainty to it, b

ut ju

st stating th

e nu

mb

ers, 17 parts p

er m

illion an

timon

y, and

20.6 parts p

er million

silver, in th

e Walk

er b

ullet. M

r. WO

LF

. Was th

is similar to th

e comp

osition of th

e un

fired

WC

C M

annlicher-Carcano cartridge?

Dr. G

UIN

N. Y

es, sir; the u

nfired

WC

C M

ann

licher-C

arcano car-

tridge w

hich

we took

apart, took

a little samp

le out of th

e lead;

and

pu

t back

together again

, instead

of 17 parts p

er million

anti-

mon

y it was 15, in

stead of 20.6 p

arts per m

illion silver, it w

as 22.4. T

hese are w

ell with

in th

e ranges of sligh

t variation th

at you get

from w

ithin

such

materials.

Mr. W

OL

F. In

your p

rofessional op

inion

, Dr. G

uin

n, is th

e frag-m

ent rem

oved from

Gen

eral Walk

er's hou

se a fragmen

t from a

WC

C M

annlicher-Carcano bullet?

Dr. G

UIN

N. I w

ou

ld sa

y th

at it is ex

tremely

likely

that it is,

beca

use th

ere are v

ery few

, very

few o

ther a

mm

un

ition

s that

wou

ld b

e in th

is range. I d

on't k

now

of any th

at are specifically

this close

as these n

um

bers in

dicate, b

ut som

ewh

ere near th

em

there are a few

others, b

ut essen

tially this is in

the ran

ge that is

rather ch

aracteristic of WC

C M

ann

licher-C

arcano b

ullet lead

. M

r. WO

LF

. Tu

rnin

g to

wh

at h

as a

lread

y b

een p

laced

on

the

exhib

it board

and

labeled

at table 1 an

d m

arked

for iden

tification

as JFK

exhib

it F-330, D

r. Gu

inn

, was th

is chart p

repared

by you

? D

r. GU

INN

. Yes, it w

as. M

r. WO

LF

. Does th

is chart rep

resent th

e results you

obtain

ed

du

ring you

r tests of the evid

ence sp

ecimen

s? D

r. GU

INN

. Yes, for th

ese five eviden

ce specim

ens, th

is chart lists

all of the in

formation

obtain

ed, even

for a few traces of elem

ents

for wh

ich w

e find

no real sign

ificance. B

ut, for th

e sake of com

-p

leteness th

ey are all listed. T

here are som

e eight elem

ents listed

for each

samp

le. M

r. WO

LF

. I move th

at JFK

exhib

it No. F

-330' be-ad

mitted

into

eviden

ce. C

hairman ST

OK

ES. W

ithout objection, it may be received.

[Th

e above referred

JFK

exhib

it No. F

-330 follows:]

503

Tab

le I R

ES

ULTS

FRO

M S

EP

TEM

BE

R 1977 IN

AA

O

F E

VID

EN

CE

SP

EC

IME

NS

AT

U.C

. IRV

INE

S

amp

le Nu

mb

er

PP

. PIPP1

po

. P

P.

PP

. P

an, ppm

C

E-

F131 0- 1.1

C-

% L

eal A

jam

ny

624....14.

c_opper A

lumm

um4 M

an

pee

0_!L__,rn.

h

e In

ane.,

798. 1

1

101.4

b

83

3. 9

39

- 14

58 3

N

O4

0.09 0.02 5

.1 19

-12 587

2

2

953

902 4

I I 0

.6

45 1

1.1 .0 4 901 0

.01

9.1

22 5

843

4,5

4.1

553

621

-4 7.9

-0.3

40

2 5,5

-07

0.1

0001

134 3

59 1

0

842 9

9.1

104

.2

797 7

9

.8 0

.5

994 7

8.1 14

0.07-9

02

1204

257-14 840

14 1

4 1

94

-2

638 4

8.6

- 0 3

44

2

2.7.0 6

098 0

01

13. 1

38 7

14-2

163

-2 647 4

730.5

42 2

2.4

0.5

0.0

5 0

01

19 1

40 8

The ebtolutt ve1hel. Oahe. for 41

• .1 C I e.,

nu

n to

1,14. 41elin,•

• r nth n.hl. but Iihle valve...nest ■ner.ei N

ehevery 111.142.4 .131 M

ee

Tn. L wen. 041.11o. P

b, 35, Cu

owl C

l ewer...eh ae•

.me. ,71 ,•■•

ereentinerrehhl•el• Thov.1.1 ,f .A

.Th • •-.• h ■•■••■•■• 1,..hhergir eh.r,

and Mee:ow

ns eL

evenh

en F

ee a• eh.,

ge 3.1 O

bh

heo

ll In relax,.

"Mai

As1/013 TO. ...no, pl. Tn..

- lc,. A

, en. A

• w

oe Frueeterod

,n •

fahre ePhr.vn 17

evne. /*am 1

.

el:101111M SIA14741111. h11/1h M

eal:Iowa. ' rN Iw

o eehere WTI 17.0 1chehe11 rn 104 larger erv.110e1

4 NO

mains norm

detected

JF

K E

am

on - F

-330

Mr. W

OL

F. D

r. Gu

inn

, add

ressing you

r attention

to the colu

mn

lab

eled "

percen

tage lead,"

wh

at does th

is ind

icate? D

r. GU

INN

. Lead

is one of th

e elemen

ts that w

e can d

etect with

activation

analysis, b

ut n

ot with

great sensitivity. H

owever, if you

h

ave dealin

gs with

samp

les that are m

ostly lead, you

don

't m

esa great sen

sitivity to at least detect it, et cetera, b

ut even

here th

e p

recision

of m

easu

remen

t is not g

reat, a

nd

if you

look

at th

e n

um

bers you

will see p

ercent of lead

is show

n as p

lus or m

inu

s 2, p

lus or m

inu

s 3, or even p

lus or m

inu

s 4 percen

t. You

will n

ote th

at they all com

e out ab

out in

the ran

ge of 100. A

ll this really sh

ows is th

at these m

etal fragmen

ts that w

e were

look

ing a

t ind

eed w

ere lead

fragm

ents, th

ey w

eren't steel

frag-m

ents, for exam

ple, or som

ethin

g else; they w

ere lead.

Mr. W

ou. W

hat d

oes the P

PM

prior to th

e listing for each

of the

other elem

ents in

dicate?

Dr. G

UIN

N. P

PM

is just th

e abb

reviation for p

arts per m

illion b

y w

eight. O

ne p

art per m

illion is on

ly one ten

-thou

sand

th of a p

er-cen

t. M

r. WO

LF

. Dr. G

uin

n, b

ased on

these resu

lts, do you

have an

op

inio

n a

s to w

hat ty

pe o

f bu

llets these fra

gm

ents w

ere from

?

Dr. G

UIN

N. O

nce again

, every one of th

ese samp

les is in th

e same

range, w

hich

is an u

nu

sual ran

ge, as the b

ackgrou

nd

WC

C M

ann

-lich

er-Carcan

o samp

les that w

e have look

ed at from

all four p

ro-d

uction

lots. Th

ese five fall right in

the m

idran

ge, in fact. T

hey are

not th

e high

est; they are n

ot the low

est of the an

timon

y range, an

d

the sam

e is true of th

e silver. M

r. Wats._ Is it you

r opin

ion th

en th

at these all are fragm

ents

from W

CC

Mannlicher-C

arcano bullets? • D

r. GU

INN

. I thin

k th

at is their m

ost lik

ely o

rigin

, yes.

Mr.

WO

LF

. L

ook

ing a

t these resu

lts, can

you

determ

ine h

ow

m

any b

ullets th

ese eviden

ce specim

ens cam

e from?

Page 9: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

504

Dr. G

uINN

. Yes, that is the really interesting part of this. I don't

sup

po

se peo

ple in

back

can see, o

r yo

u u

p th

ere can see, th

e num

bers on the chart very well, but you have the report to look at.

If you look at these five that are listed up here, and you first of all lo

ok

at the p

rime o

r key

elemen

t, wh

ich is an

timo

ny

, yo

u fin

d o

f th

e five sam

ples, th

at there are tw

o o

f them

that are u

p so

me-

where around 800 parts per m

illion, and you find three others that are dow

n just a shade over 600 parts per million.

Now

, after each n

um

ber th

ere is show

n a p

lus o

r min

us. T

his is

only the uncertainty of that particular measurem

ent from w

hat we

call the counting statistics. That uncertainty w

e can measure.

Mr. W

OL

F. D

r. Guinn. B

efore we go into a m

ore technical expla-natio

n, can

you ju

st from

lookin

g at th

e results, state w

hat is th

e num

ber of bullets that these evidence specimens cam

e from?

Dr. G

UIN

N. Y

es, sir, I can. M

r. W

OL

F.

What is th

e num

ber o

f bullets, in

your o

pin

ion?

Dr. G

uiNN

. These num

bers correspond to two bullets. T

wo of the

samples have indistinguishable com

positions, indicating that they cam

e from

the sam

e bu

llet, and

the o

ther th

ree particles are ev

i-dently sam

ples from another bullet.

Mr.

WO

LF

. So

it is y

our o

pin

ion

that th

e evid

ence sp

ecimen

s represent only evidence of tw

o bullets, is that correct? D

r. GU

INN

. Yes, sir, th

ere is no ev

iden

ce for th

ree bullets, fo

ur

bullets, or anything more than tw

o, but there is clear evidence that there are tw

o. M

r. WO

LF

. And w

hich specimens that correspond, respectively, of

the two bullets?

Dr. G

uINN

. Using the C

E num

bers, the 399 specimen, w

hich is th

e so-called

stretcher o

r pristin

e bullet—

it has v

arious n

ames—

agrees in

com

po

sition

bo

th in

its antim

on

y an

d its silv

er with

C

E-842, w

hich are the fragments reportedly recovered from

Gover-

nor Cannally's w

rist. M

r. WO

LF

. Is it your' testimony that C

E-399 and C

E-842, the so-

called p

ristine b

ullet, an

d th

e fragm

ents rem

oved

from

Govern

or

Co

nn

ally's w

rist du

ring

surg

ery, b

oth

came fro

m th

e same b

ullet?

Dr. G

uINN

. Yes. O

ne, of course, is almost a com

plete bullet so it m

eans th

at the 8

42

fragm

ents cam

e from

, in th

is case, the b

ase of

the bullet. M

r. WO

LF

. Dr. G

uin

n, am

I correct th

at technically

you can

not

today

testify to

the co

mplete v

alidity

of th

e so-caned single bullet th

eory

becau

se there w

as no lead

left in th

e back

wound o

f the

President or around the P

resident's throat that would allow

you to ex

amin

e it and, th

erefore p

ossib

ly d

etermin

e that C

E-3

99 p

assed

through the President?

Dr. G

UIN

N. Y

es, reportedly there were no lead fragm

ents found in

the b

ack-to

-thro

at wound o

f the P

residen

t, and h

ence n

o sp

eci-m

ens to

be an

alyzed

,' so

I k

no

w n

oth

ing

abo

ut th

at particu

lar w

ound. M

r. WO

LF

. You can, how

ever, today state for the first time scien-

tifically that CE

-399 did cause the injuries to Governor C

onnally's w

rist? D

r. Gurzfrt. Y

es sir. those two m

atch so closely that I would say

that such was the case.

505

Mr. W

OL

F. W

hat is th

e deg

ree of co

nfid

ence an

d certain

ty w

ith

which you can state this conclusion? D

r. GU

INN

. I wish that I could put a num

ber on it, as we often

can do, that is, calculate a probability, but we really don't have the

back

gro

un

d in

form

ation

to m

ake a n

um

erical calculatio

n in

this

case. One can only show

what inform

ation we do have, and that is

that you simply do not find a w

ide variation in composition w

ithin individual W

CC

Mannlicher-C

arcano bullets, but you do find wide

composition differences from

bullet to bullet for this kind of bullet lead. T

hus, when you find .tw

o specimens that agree this closely,

you can

say it lo

oks in

deed

like th

ey are p

ieces from

the sam

e bullet.

Mr. W

OL

F. W

ou

ld y

ou

state that y

ou

r con

clusio

n is m

ore p

rob

-able than not, highly probable, or w

hat is the degree of certainty of your conclusion?

Dr. G

UIN

N. I w

ould say highly probable, yes. I would not w

ant to say

how

hig

h, w

heth

er it was 9

9 p

ercent o

r 90 p

ercent o

r 99.9

percent. I can't m

ake a calculation like that. M

r. WO

LF

. You w

ould state it is highly probable that the injuries to

Govern

or C

onnally

's wrist cam

e from

the so

-called p

ristine

bullet? D

r. GutN

N. T

hat is correct. M

r. WO

LF

. Were y

ou p

resent y

esterday

durin

g th

e testimony o

f D

r. Wecht?

Dr. G

UIN

N. Y

es, sir; I was.

Mr. W

OL

F. D

id you hear Dr. W

echt testify, in response to ques-tions from

counsel, that in his opinion it was im

possible for CE

-7:. to have caused the injury to G

overnor Connally's w

rist, even• if it h

it no

thin

g else, b

ecause C

E-3

99

wo

uld

hav

e had

to sh

ow

mo

re deform

ity? D

r. GuiN

N. Y

es: I heard him m

ake that statement.

Mr. W

OL

F. D

r. Guinn. on the basis of your scientific analysis, do

you believe Dr. W

echt to have been correct? D

r. GU

INN

. W

ell, I th

ink th

at is his o

pin

ion, b

ut lik

e man

y

op

inio

ns an

d m

any

theo

ries, som

etimes th

ey d

on

't agree w

ith th

e facts.

Mr. W

ats. Dr. G

uin

n, h

ave y

ou

prep

ared a rep

ort fo

r the co

m-

mittee w

hich

com

pletely

describ

es your w

ork

for th

e com

mittee

and your conclusions? D

r. GU

INN

. Yes, sir.

Mr. W

OL

F. D

o you have that report with you?

Dr. G

UIN

N. Y

es, sir. It is right here. M

r. W

OL

F.

Mr. C

hairm

an, I m

ov

e that D

r. Gu

inn

's repo

rt be

mark

ed as JF

K ex

hib

it No. F

-331 an

d in

troduced

into

evid

ence.

Chairm

an Srroias. W

ithout objection it may b

e introd

uced

at this

point. [T

he above referred to JFK

exhibit F-331 follow

s:]

Page 10: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

506

JFK

Extuerr F-331

A R

EP

OR

T T

O :H

Z R

OU

SE

OF

RE

PR

ES

En:A

TIV

ES

SEL

EC

T C

OM

MI7T

EE

ON

ASSA

SSINA

T:';N

S

on the subject of

1977 NE

UT

RO

N A

CT

: -:,1710N A

NA

LY

SIS

'-i-EASU

REZIEN

TS

ON BULLET-LEAD SPECIME:i3 7NvOLVED IN TRE 19,S

3 ASSASSINATION

OF PRES:LENT JOHN F. KENNEZ7

by

Dr. Vincent P. Guinn (Ph.D.)

Prcfessor of Chemistry

University of California

Irvine, California

, 147

Se7ber, 1973

se.

5UT

I. INTRODUCTION

This report is a presentation of the results obtained

and their interpretation, in a September 12-14, 1977 instru-

mental neutron activation analysis (INAA) study of bullet-

lead specimens involved in the November 22, 1961 assassina-

tion of President John F. Kennedy in Dallas, and of a

specimen

from a bullet allegedly fired at General Edwin Walker

in April

of 1963. The author has been engaged in neutron activation

analysis !NAA) research and applications for the past 20

years -- first, as Read of the Radiochemistry Section of the

-

Shell Development Conpany, next (1962-1979) as Technical Direc-

tor of the Activation Analysis Program at General Atomic, and

(since early 1979) as Professor of Chemistry at the Univer-

sity of California at Irvine (UCT). The author's first

studies of the applicatiOn of the highly sensitive NAA method

to problems in the field of scientific crime-investigation

commenced in early 1352, have continued steadily sin

ce that

time, and his forensic activation analysis publications consti-

tute 93 of his 181 publications, to date, In the field of

radiochemistry/activation analysis. During the period. 1362-

197i, his forensic NA research was supoerted first by the

U. S. Atom'-:

.Energ

y Commission and later jointly by the AEC

and the Law Enforcement Assistance Administration (LE2A1 of the

U. 3. Cepartmeht of Zustita. From this research cane the 7:AA

method for detection of gunshot resid...es that is now used

by the F31 and many other law enforcement agencies around the

Page 11: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

508

world, and extensive reports on the use of INAA for the trace-'

element characterization (as to probability of common origin)

of such evidence-type materials as bullet lead, paint, paper,.

and oil.

NAA is a nuclear method of elemental analysis. It is

a nuclear method of analyzing samples of all kinds of materials

to determine the elements present in them.

The sa

mp

les to

be

analy

zed are placed in small plastic vials, lowered into or

near ti:te cars of a research-type nuclear reactor, and. then

bombarded with a very large number of slow neutrons (typically,

about 10 trillion per second) for a selected period of time.

When the samples are removed from the reactor, they are essen-

tially unchanged in composition (and in most cases, in appear-

anrel, but they are now radioactive, since capture of a

neutron by many of th

e a

tom

ic n

ucle

i of

many of th

e ele

men

ts

prusent in the samples has formed radioactive (unstable) nuclei

of _mesa elements. :Cith or without (as needed) some chemical

prores5og of the activeted samples before counting, the

serp_ies are then counted on a gamma-ray spect;ommter -- a

-

sopnisticated detector and electronic apparatus that measures

the energies and numbers of the gamma rays emitted by each

railoactive sample. The gamma-ray energies, observed as peaks

in earn epectrtim, ilentify the various elements that have been

made ierectably

-ra

dio

activ

e, and the ressured sizes of the peaks

the =Run=s of the elements present.

509

The principal advantages of the reactor neutron

activation analysis method are (1) it can detect and accurate-

ly measure even very tiny amounts (typically, one billionth

of a gram) and very low concentrations (e.g., one part per

billion( of many elements in a sample, (2) it can utilize

sample sizes ranging all the way from a tiny speck . u

p to

several grams, (3) it can simultaneously detect a number of

elements in a sample, and (4) it can in many instances be

carried out nondestructively. The main induced radioactivities

are those that have rather short half lives (l.e., they decay

away in a matter of seconds, minutes, or hours), and hence

the analyzed samples soon become negligibly radioactive and

hence can be handled with complete safety.

in previous extensive INAA studies of bullet-lead

specimens (of many different calibers, manufacturers, and pro-

duction lots), it was found that three key elements were al-

most always detectably present, but at widely different con-

centretions, depending coon the source of the bullet lead:

antimony (Sb), silver (Ag), and copper I Cu). Antimony con-

centrations in the range of about 1 to 10 parts per million

by weight (Ipom = 0.0001%) are usually found in unhardened

bullet lead, made with virgin lead, whereas levels in the

range of about 0.4% to 4i Sb are found in commercial bullet

leads that have been hardened by alloying Sb with the lead.

Intermediate Sb levels (i.e., between about 10 ppm and perhaps

Page 12: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

51

0

/500 ppm) are encountered in unhardened bullet lead Ln which

some recycled lead is used, along with virgin teed, but in

which no

Sb has b

een d

elib

era

tely

added for hardening. Silver

concentrations are usually found to lie in the range from

shout 0.5 ppm to 100 ppm, and the Ag appears to come in mainly

as a natural impurity in the lead supply. Copper concentra-

tions are usually found to 142 in the range of about S ppm

to 400 ppm, and the Cu also appears to come in vainly as a

natural impurity in the lead supply. Of these three key

elements, Cu is the one of least usefulness for comparisons,

due to a-eat:ant occlusion of tiny bits of copper in the bullet

lea

d co

min

g fro

m th

e copper jacket of jacketed bullets in

the

sampling, and from the brass cartridge or brass primer cap in

the firing of the cartridge-- producing occasional spuriously

hiph Cu values.

Occasionally, the :NAA at bullet-lead specimens also

shows the presence of traces of certain other elements, such as

aluminum, arsenic, manganese, tin, sodium, and chlorine.

Thete elements, where detected. have generally not proved to

he tonsistent enough to be useful for the characterization of

bullet lead as to its origin. Sodium and cnlorine, the con-

stituents of common salt, appear to occur primarily as the

result of external contamination.

In earlier INAA studies of bullet leads from many

different manufacturers (See, references 4 and 5 in Appendix

20, it was found that bullets from a given manufacturer and

51

1

production lot were generally quite uniform in their Sb and

Ag concentrations, both within a given bullet and amongst

bullets from the same box or p

roductio

n lot. Thus, for such

typical ammunition it is generally not possible to distin-

guish amongst bullets, or bullet fragments, from the same

box of cartridges.

However, when the author analyzed (See, Appendix C)

quite a number of Western Cartridge Company Mannlicher-

Carcano 6.5 ra

m b

ulle

ts, from

their production lots 6000, 6001,

6002, and 6001 Ith

e only four lots they produced of this

type), this ammunition was found

to differ sharply from

typical bullet leads- Although in

div

idual b

ulle

ts w

ere

found

to be fairly homogeneous in their Sb and Ag concentrations,

they d

iffere

d greatly from bullet to bullet amongst samples

taken from the same box. For example, the Ag levels in

bullets from lot 6003 ranged from 7.5 ppm to 15.9 ppm, the Sb

levels from 80 to 730 Pam (and the Cu levels from 17 to 62

ppm

). This

gre

at variation from bullet to bullet from the

same box thus indicated that for this unusual kind of am-

munition, it would be possible to distinguish one bullet (or

bialet fragment) from another, even though they both came

from the same box of Mannlicher-Caroano cartridges.

Page 13: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

512 513

PREPARATION OF THE SAMPLES FOR ANALYSIS

The analyses that are the subject of this report

were conducted at the University of California at Irvine

(UCI) during the period of September 12-14, 077. In these

measurements, eight elements were determined quantitatively,

by the method of instrumental neutron activation analysis

(INAA), using the thermal-neutron flux of the UCI research-

type nuclear reactor for the activation of the samples, and

the 38 cm3 G

e(Li)/4096-channel gamma-ray spectrometer at UCI

for the counting of the activated samples. The eight ele-

ments measured in the samples were the following:

lead

aluminum

'silver

manganese

antimony

sodium

copper

chlorine

The evidence specimens to be tested were removed

from the U. S. National Archives, in Washington, D. C. by

Mr. James L. Gear of the Archives staff.-

1/ The evidence

1. The specimens were brought to California in secure con-

tainers by commercial airline. Except during the day-

time periods of September 12, 13, and 14, 1977, when they

were in the process of being sampled and analyzed, they

were kept locked up at the Laguna Niguel, California,

branch of the National Archives.

During all of the opera-

tions on the evidence specimens carried out at UCI during

the September 12-14, 1977 period, the specimens were ac-

companied by Mr. James Gear, of the National Archives,

and by two Federal guards from Los Angeles. At the end

of the day on September 14, 1977 all of the activated

samples were returned to Mr. Gear.

specimens which are the subject of this report may he put in

two groups. The first group are those reportedly found

located in or near the occupants of the President's limousine,

the limousine, or the area immediately surrounding it. The

second group consists of a sample taken from the unfired cart-

ridge reportedly found in the Texas School Book Depository

Building on November 22. 1963, and a sample taken from the

mashed bullet reportedly found in the home of General Edwin

Walker, after he was reportedly fired upon in April of 1963.

The evidence specimens consisted of the following, l/

Groom i;

(1)

FBI no. Q609. Reportedly piece of curb from

Dealey Plaza.

(2) FBI no. 03 (CE-569). Reportedly a fragment re-

covered from the front seat of the Dallas limousine.

(3) FBI no. 015 tcE-541). Reportedly particles

scraped from the inside surface of the wind-

shield of the Dallas limousine.

(4) FBI no. Ql ICE-399). Whole bullet, still in

its jacket, reportedly found on a stretcher

at the Parkland Memorial Hospital in Dallas,

on the afternoon of November 22, 1963.

(5) FBI no. Q2 (CE-567). Mashed large bullet

2.

The CE-number is the number assigned by the Warren

Commission as its exhibit numbers; the FBI 0 number

is the identification number assignee by the FBI

Laboratory.

Page 14: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

514 515

fragment, still

in its jacket, reportedly

Dallas curbing sample (FBI no. 0609) was not suitable for

recovered from the front seat of the Dallas

INAA analysts. The slight gray smear on it had previously

limousine.

been scraped by the FBI Laboratory, and the scrapings

161 FBI nos. 04. 5 tcz-6411.

One larger fragment,

analyzed by emission spectography, in 1964. The amount of

and one smaller fragment, reportedly recovered

remaining metal (?) in the smear was too small for proper

from President Xennedy's brain at autopsy.

INAA measurements,. and, further, any material scraped from

171 FBI no. Q9 !CE-8421. One larger fragment, and

the curbing would be too contaminated by cement material to

two smaller ones, reportedly recovered from

yield any meaningful INAA results.

Governor Connally's wrist during surgery.

On September 13, 1977, the remaining evidence speci-

(91 FBI no. Q14 (CE-840). Fragments reportedly

mans were examined, one at a time, more closely, under mag-

recovered from the rear floor of the Dallas

nification, to decide which ones were suitable for bullet-

limousine.

lead analysis by INAA. Two additional specimens were found

to be unsuitable for analysis:

FBI no. Q3 (CE-569)• Fragment reportedly recovered

from the front seat of the Dallas limou-

sine. This specimen consisted of only

the copper bullet jacket, with no lead

inside.

FBI no. 015 (CE-841). Particles reportedly scraped

from the inside surface of the windshield

of the Dallas limousine. No particles

were left in the specimen container re-

ceived from the Archives. The particles

probably were entirely consumed in the

emission spectrographic analyses per-

formed by the FBI Laboratory in 1963/1964.

G-our. II:

(9) FBI no. 0 10E-1411. Complete unfired

Western Cartridge Company 6.5 mm cartridge,

reportedly found in the chamber of a Mannlicher-

Careen° rifle found in the Texas School Book

Depository Building (TSBD) on November 22, 1963.

(101

FBI no. 186 (CE-573). Mashed bullet, still

in jacket, reportedly fired at General Walker

in April, 1963.

The evidence specimens from the National Archives

were inspected on September 12, 1977. Each specimen was

examined to determine if it was suitable for INAA analysis.

For a specimen to be suitable for analysis, it must contain

in excess of one milligram of uncontaminated bullet lead.

During the first inspection, it was determined that the

A.

Page 15: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

516

The remaining evidence specimens were deemed suit-

able for INAA measurements, and were prepared for analysis

on September 13. 1977, except for the CE-141, 08 sample,

which was prepared on September 14, 1977.

Samples of the suitable evidence specimens were then

taken and prepared for analysis. Each sample was placed in

a cleaned, labeled, weighed half-dram polyethylene vial,

then weie.hed again to obtain the sample weight. For security

reasons, each vial was labeled 'HC-1', 'HC-9', etc. the PC standing

for "House Committee" and the number being the FBI Q number

(except for the Walker bullet sample, which was labeled ac-

cording to its CE number). Each sample, taken in its entirety,

or a portion of a larger specimen cut off or drilled out, when

necessary to obtain only bullet lead, was washed three times,

alternately, with distilled/deianized water and Reagent Grade

acetone, then air-dried before analysis. Deionized water was

used to remove water-

soluble salts: acetone was used to remove

oil. Once the sample was placed in its polyethylene vial,

the hinged vial cap was snapped tightly shut. Cutting, where

necessary, was performed with a cleaned surgical scalpel.

Drilling, weere necessary, was performed from the center of the

bullet base with a tiny (approximately 0.5 mat diameter)

cleaned carbon-steel drill in a pin vise holier. Care was

taken to avoid contamination of the bullet-lead sample by

jacket material, and each sample was examined under magnifi-

cation, to be sure that no visible jacket material was ad-

ae

517

herieg to the lead sample. In some instances, when more

than one suitable sample could be obtained from the same

specimen, two samples were taken for analysis from a given

specimen (HC-4, 5: HC-3: HC-9 and HC-14). The two separate

samples of a given specimen were then given an additional

number, to distinguish them from one another (e.g., HC-9-1

and HC-9-2).

The samples taken for analysis are summarized below:

CE no.

FBI No.

UC/ No.

Sample

Remarks

HLL1Til 399

QI

HC-1

10.7

Drillings from bullet.

567

Q2

HC-2

50.5

Piece cat from large

fragment.

843

Q4, 5

HC-4-1

41.9

Single larger specimen.

BC-4-2

5.4

Single smaller spec hen.

042

Q9

HC-9-1

16.4

Single larger specimen.

HC-9-2

1.1

Two tiny specimens.

840

014

HC-14-1

33.4

One single specimen.

HC-14-2

13.8

Second single specimen.

573

01BS

HC-573

16.3

Drillings frcm specimen.

1412/

Q8

HC-8-1

24.3

Drillings from bullet.

HC-a-2

6.3

Drillings from bullet.

3.

Regarding the CE-14/ (FBI O8) sampling, a special die for

6.5 mm cartridges was purchased and then used on September

14, 1977. along with the UCI reloading equipment, to dis-

assemble and later reassemble the CE-141 cartridge. The

cartridge was first examined visually, with the following

observations made: (1) the cartridge base was stamped

"WCC 6.5 me', (2) tee entire cartridge case, and the bullet

10

Page 16: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

518

As well as preparing the evidence samples, tour

sample standards, each, of silver, antimony, and copper were

prepared on September 8 and 9, 1977 to be used in this test.

Standard samples of the elements to be measured are necessary

in order to convert the measured gaga-ray peaks quantita-

tively to micrograms of element present In a sample -- this

is the usual comparator method. Samples and standards are

activated and counted exactly the same way. Each silver

standard contained 3.25 micrograms (fig) of silver, each anti-

mony standard contained 2I3 micrograms of antimony, and each

cooper standard contained 192 micrograms of copper. Each

standard consisted of 0.100 cm3 of a freshly prepared aqueous

solution, gently dried in the bottom of a half-dram polyethyl-

ene vial, and cemented down with a few drops of a 101 paraffin

soletion in carbon disulfide (allowed to dry at room

temperature).

packet, were rather dark in color -- indicating external

exidatien/sulfiding, (3) there was no firing-pin impres-

sion at the base, where the primer. cup is located, in-

diceting that the cartridge had never undergone even an

attempted (abortive) firing. Upon disassembly, the

bullet (pro/ectilel part was found to be the same in

shape, dimensions, weight, and single canneiure as other

Western Cartridge Company 6.1 mm Manniicher-Carcano bul-

lets from their production Lots 5000, 5001, 6002, and

6003. The pristine jacketed bullet, before sampling,

was found to weigh 10.4082 grams (160.62 grains). This

compares closely with the nominal bullet weight of 161

grains quoted by the Western Cartridge Company. The gun-

powder from the cartridge was also weighed, and found to

be 2.8294 grams (43.66. grains), which agrees closely with

the manufacturer's nominal value of 44 grains. After the

two. drilling samples were taken from the bullet (24.3 mg

and 6.3 mg), the bullet was reweighed, and found to now

weigh 10.3774 grams (160.15 grains). The cartridge wax

then reassembled, with the gunpowder and sampled bullet

back in place.

519

THE ANALYSES OF THR SAMPLES AT Uti

On September 13, 19771( each sample (except for

samples EC-8-1 and HC-8-2) was activated twice and counted

twice, under conditions optimized for the generation and

detection of short-lived induced radioactive species. 1/ With

the 0CI TRIGA Mark I nuclear reactor running steadily at

full power (250 kilowatts). each sample, in its closed 1.3

cm3 polyethylene vial, was irradiated for 46 seconds in the

pneumatic-tube reactor core position (where the thermal-

neutron flux is 2.5 x 10 12 n/cm2 - sec), allowed to decay

for 40 seconds (during which the activated sample was trans-

ferred to a fresh, labeled vial), and then counted for 40

seconds ciocktime on top of a one-centimeter thick plastic

beta-particle absorber on toy of a 38 cubic-centimeter high-

resalutien coaxial lithium -drifted germanium (Ge(Li)) semi-

conductor games -ray detector, coupled to a 4496-channel

pulse-height analyzer. During the counting of a sample.

4. ?resent during these tests were Dr. Guinn; Michael

Purcell, a laboratory assistant; Archivist James Gear;

and two Federal guards.

5.

Optimized conditions vary for each element. For element

radioisotopes with a short half life, a short irradiation

time, a short decay time, and a short counting time pro-

vide optimized /NAA detection conditions. For element

radioisotopes with a long halflife, optimal conditions

are a long irradiation time, a long decay time, and a

long counting time.

Page 17: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

520 521

the analyzer percentage deadtime was read from the deadtime

meter at the beginning and at the end of the counting

period.g As scan as the counting of the sample was com-

pleted, its complete pulse-height spectrum was transferred

twice to a fresh magnetic tape, identified by its tagword.

The samples, and the standards of antimony, silver, and

copper. were processed identically in this fashion, in suc-

cession, one at a time. Each sample and standard was then

activated and counted a second time, under the same condi-

tions.

On the following day (September L4, 1977) the samples

and the standards of antimony and copper, and sample HC-8-1,

were activated in the reactor again -- this time for one

hour and all at the same time, each sample, in its 1.3 cm3

2olyntevelene vial, in a separate tube of the 40-tube rotary

specimen rack. of the reactor. At full power (250 kilowatts).

6.

.ihele the pulse-height analyzer is measuring the size

of one electrical pulse from the Ge(Li) detector, to

determine in which of the 4096 channels it should be

stored•as a count, the analyzer cannot accept another

input pulse. This period is called "deadtime". In the

analyzer circuiting, the eercentage of the total clock-

time that is deadline is continuously monitored and

displayed on a percent deadtime meter. The counts

obtained during egiven clocktime period are then cor-

rected for this deadtime loss of counts by dividing

the observed counts by (1 minus the average fractional

deadtime) during the counting period. In order to

avoid spectrum distortion, it is not advisable to use

the counting data for really quantitative calculations

if the deadtime during the counting period is greater

than about 103.

each sample en the rotary specimen rack is exposed to an

average thermal-neutron flux of 1.0 x 1012 n/cm2 - sec.

During the first part of this one-hour irradiation, sample

HC-a-2 and one each of the antimony, silver, and copper

standards were activated in the pneumatic-tube reactor posi-

tion (at a thermal-neutron flue of 2.5 x 10 12 n/cm2 - sec)

and counted as in the measurements on the previous day: at

irradiation, decay and counting times of 40 seconds each.

The HC-5-2 sample was activated and counted twice. After

the end of the one-hour Irradiation, each sample and standard

was removed from the rotary specimen rack, each sample

transferred to a fresh labeled polyethylene vial, and then

each counted for 300 seconds livetime on the Ge(ti)/4096-

channel gamma-ray spectrometer as before. As before, also,

each pulse-height spectrum was recorded twice on the magnetic

tape, along with its identifying tagword. The time of day

at which each count was started was noted -- for use in sub-

sequent decay corrections.

At the beginning of the counting on each day, the

energy scale was calibrated by means of the 661.6 keV gamma

ray of cesium - 137 and the 1112.4 key gamma ray of cobalt -

60. The energy calibration pulse-height spectra were also

stored an the magnetic tape. The energy range covered was

from 15 keV (channel 2) to 3277 keV (channel 4096).

On subsequent days, each recorded pulse-height

spectrum was read back off the magnetic tape. Each spectrum

Page 18: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

522

was scanned carefully on the expanded oscilloscope display,

and the energy of each significant photopeak observed was

calculated and printed out on the Teletypewriter, using the

built-in PCP-8 computer. Each selected photopeak of quanti-

tative interest!! was printed out channel by channel, in-

cluding the regions on each side of the peak. In the spectra

from the pneumatic-tube measurements, the principal photo-

peaks obsereed were the following,

1. the 638 keV peak of 24.4-second silver - 110.

2. the 498, 603, and 646 key peaks of 91-second

antimony - 124m1.

3. the 1039 keV peak of 5.10-minute copper - 66.

3matler peaks due to 2.31-minute aluminum - 28 (at 1779 keV)

and due to 66.9-minute lead - 204m (at 175, 899, and 912 keV)

were also observed and printed out. The 564 keV peak of 2.90-

day antimony - 122 and the 511 keV peak of 12.80-hour cooper -

54 were observed, but not printed out.

In the spectra from the rotary-rack.measurements,

7.

An oscilloscope is employed t6 :•isually display the pulse-

height spectrum. Generally, the specteum has tha "shape

of a descending curve, upon which peaks are superimposed.

Each element radioisotope shows characteristic peaks of

certain energies and of different sizes. A peak size

measurement is made by measuring its area. A peak of the

tested sample is rater compared with the area of the cor-

responding peak of one of the known standard samples. The

relative area of the peak from the tasted sample compared

to the area of the peak from the known standard indicates

the total weight of the element within the tested sample.

In some cases, there are overlaes of peaks of similae

energies. Accordingly, the photopeak measured for any

given element is chosen considering two factors -- a large

peak, and one which does not overlap with a peak of another

element. Such a peak is a selected photopeak oeequantita-

tive interest.

523

the principal photopeaks observed were the following:

1. the 511 key peak of 12.80-hour copper - 64.

2. the 564 keV peak of 2.80-day antimony - 122.

Smaller peaks due to 2.576-hour manganese - 56 (primarily

at 847 keV), to 60.4-day antimony - 124 (primarily at 603

keV), to 14.96-hour sodium - 24 (at 1368 keV and 2754 keV),

to 37.29-minute chlorine - 38 (at 1643 keV and 2168 keV),

and to 66.9-minute lead - 204m (at 375, 999, and 912 keV)

were also observed and printed out.

For all spectra, the counts in each channel of each

selected photopeak, and the counts in several channels on

each side of each peak, were printed out. From these read-

outs, and those of the antimony, silver, and copper standards

and the sample •weights, the concentration of each of these

three elements of particular interest (and the standard

deviation of each, calculated from the counting statistics)

was calculated from the pneumatic-tube data for 24.4-second

silver - 110, 93-second antimony - 124m1 (via its 458 key

peak), and 5.10-minute copper - 66. From previous activa-

tions of lead standards, the concentration of lead in each

sample was calculated from the sum of the photopeak areas of

the 375, 899, and 912 keV peaks of 66.9-minute lead - 204m.

Using standard table values, the concentration of aluminum

in each sample was calculated from the 1779 keV peak of 2.31-

Page 19: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

524

minute aluminum - 28. In the calculations, small corrections

were made for the average analyzer fractional deadtime during

each counting.

Similarly, from the rotary-rack data, the concentra-

tion of antimony in each sample was calculated from the site

of the 564 keV peak of 2.30-day antimony - 122, and the con-

centration of copper in each sample was calculated from the

size of the 511 keV oositron annihilation peak of 12.80-

hour copper - 64. From the previous activation of lead

standards, the concentration of lead in each sample was

again calculated from the sum of the photopeak areas of the

375, 899, and 912 keV peaks of 66.9-minute lead - 204m (note:

lead - 204m is a fast-neutron product of lead, rather than a

thermal-neutron (n,le) product, formed by the lead - 204

(n. n') lead - 204m reaction). rising standard table values,

the concentration of manganese in each sample was calculated

from the 847 keV peak of 2.576-hour manganese - 56, of sodium

from the 1368 keV peak of 14.96-hour sodium -.24, and of

chlorine from the 2168 kev peak of 37.29-minute chlorine - 38.

All observed peak areas were, of course, corrected to the same

decay time, by means of the radioisotope halflife and the

time between the end ofothe rotary-rack irradiation and the

start of the counting period of the sample.

525

IV.

THE RESULTS OBTAINED IN THIS STUDY (1977)

The results obtained on the tasted specimens for

Group I are presented in Table I, Appendix B. and those for

Group El in Table III, Appendix G. The Tables list the con-

centration found in weight percent for lead, and in parts-

per-million by w

eight (ppm) for the elements antimony,

silver, copper, aluminum. manganese, sodium, and chlorine --

eight elements in all.

The values shown for silver and aluminum were cal-

culated from peak areas of 24.4-second silver - 110 (at 658

keV) and of 2.31-minute aluminum - 28 (at 1779 keV), re-

spectiv

ely

, in the pulse-height spectra from the 40-second

oneumatic-tube activations. As noted earlier, these spectra

also showed peaks due to antimony - 124m1, comer - 66, and

lead - 204m, but these three elements were determinable sore

exactly from the spectra obtained in the one-hour rotary-

rack irradiation, and, hence the Table values far antimony

(via the 564 keV peak of 2.80-day antimony - 122), copper

(via the 511 keV peak of 12.80-hour copper - 641, and lead

(via the three peaks of 66.9-minute lead - 204m) are those

obtain

ed from the rotary-rack irradiation. The results

shown in the. Tables for manganese, sodium, and chlorine are

also from the rotary-rack irradiation.

Page 20: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

••■

526

Two of the very small samples analyzed (the 5.4

milligram HC-4-2 sample, and the 1.3 milligram HC-9-2

sample) had results within expected standard deviations to

those obtained from the respective larger samples (the 41.9

milligram HC-4-1 sample, and the 16.4 milligram HC-9-1

sample), but the such more exact values obtained from the

larger samples, only, are shown in the Tables.

In most cases, the

value shown after each value

in the Tables represents the uncertainty of the value (ex-

pressed as one standard deviation) computed only from the

counting statistics. In general, the overall uncertainty of

a given value may be in some cases as much as two or three

times the standard deviation calculated just from the count-

ing statistics. For silver and aluminum, which were measured

twice on each sample, the + values shown represent one

standard deviation calculated from either the counting

statistics or the spread of the two values -- whichever was

larger.

The ppm values shown in the Tables for antimony,

silver, and copper were obtained, as mentioned earlier, by

comparison with standard samples of these elements activated

and counted along with the various evidence samples, and hence

these values should be quite accurate. Similarly, the results

for lead should be very reliable since they were based on

527

previously tested lead standards. Far the remaining elements

(aluminum, manganese, sodium, and chlorine). whose presence

was not known in advance, as mentioned earlier, standards of

these elements were thus not prepared at the time Of these

experiments. Instead, standard table values were used in the

calculations for these elements. As a result, the reported

ppm values for these four elements present in the evidence

sample could be in error by a factor of perhaps two on an

absolute scale. However, the use of tabulated standard

values does not affect the relative values -- only the absolute

values of a given element in the various samples.S/

17--- For example, if the estimated values for aluminum, based

on standard tables, In two samples were 5.0+0.5 or and

2.5+0.3 ppm, the ratio of their aluminum concentrations

would be 2.01+0.31 to 1. tf the standard table value

for aluminum vera 203 high, for example, the true sample

aluminum values would be 6.2+0.6 ppm and 3.1, -0.3 ppm,

respectively, but their ratio would still be 2.01+0.3)

to 1.

Page 21: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

529 528

v.

CONCLystoNs

A. It is highly probable that the evidence specimens

from Group I are all fragments from Mannlicher-Carcarm bullets.

As discussed in Appendix C., Mannlicher-Carcano am-

:ai^itian displays very distinct characteristics when analyzed

by neutron activation analysis. The ammunition displays an

unusual range of concentrations for the antimony in bullet

lead. The concentrations for silver are unusual as well,

although not as distinct as those of antimony. Based upon

these characteristics, and the results obtained from an analysis

OE the evidence specimens, it is highly probable that all the

evidence soecimens are fracments from Manniicher-Carcano bullets.

The antimony content of the ev

iden

ce fragments is such that

it is significantly h

igher

than that found in most unhardened

bullet lead

examined

by the author, and significantly lower

than

chat found in bultat

elead of hardened lead bullets

examined by the author. Such an intermediate range of antimony

concentrations is particularly characteristic-of MannIicher-

Carcano ammunition. The values of silver found in

the

fragments

also support the conclusion that the fragments are from

Mannlicher-Carcano ammunition, as these values also are within the

range characteristic of̂mannligher-Caroano ammunition.

8- it is hichly probable that the Walker bullet is a

Banclicher-Carcano bullet.

The bullet fragment recovered from the home of

General Walker Is apparently also from mannlicher-Carcano

ammunition. This sample (CE-573, FBI (11881 of a bullet

fragment recovered from the home of General Walker in April

of 1963 was analyzed by the Pt/ in late 1963, but only by

the rather qualitative method of emission spectography.

They did not analyze it by neutron activation analysis.

This sample was analyzed by INAA during the UCI analysis.

It was determined that the bullet lead consisted of almost 100%

lead, with only 17 ppm antimony and 20.6 ppm silver. (See

Appendix G.1 Its composition, therefore, is considerably

different from any of the Dallas specimens -- which are also

almost 100% lead, but contain much more antimony (602 to 833

ppm) end much less silver (7.9 to 9.8 ppm). However, the

antimony content of the Walker bullet is close to the range

of Sb values found earlier at OCT for Mannlicher-Carcano

bullets from the four Western Cartridge Compaoy production

lots (24 to 1218 ppmi, and also close to the range of Ag

values found in such ammunition (6.0 to 15.9 ppml. Further-

more, the composition of the Walker bullet is very close to

that of the unfired Mannlicher-Carcano cartridge reportedly

recovered from the rifle found in the TSBD.

The unfired MC cartridge (CE-141, PSI 08) was never

before taken apart cr analyzed. At MCI it was examined,

taken apart, its several components weighed, the bullet lead

sampled, the cartridge reassembled, and the two small bullet-

lead samples taken from it analyzed byINAA. (See Apendix G.1

Page 22: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

530

631

Its composition (almost 100% lead, 15 poe antimony, and 22.4

pen silver) is extremely close to that of the Walker bullet

and, consequently, supports the conclusion that the Walker

fragment is from WC ammunition.

C. The results indicate the cresence of only two

bullets in Group I.

When the recent DC/ results were analyzed statistic-

ally, taking into account both the overall reproducibility

of the measurements on a single sample and the variability

due :e counting statistics of the individual measurements,

evidence for the presence of only two bullets is found. Where-

as, for most brands of ammunition it is not possible to dis-

tinguish between two bullets from cartridges from the same

box/production lot, earlier studies by the author on western

Cartridge Company Nannlichet-Carcano 5.5 mm bullets have

shown that t:Iis

brand (lots 6000, 6001, 6002, 6003) exhibits

widely different antimony values, even amongst bullets

from a given lot, so that individual bullets of this brand can

usually be distinguished from one another. (See Appendix C.)

The presence of only two bullets is indicated as

follows:

Ol

(Stretcher bullet) and Q9 (fragments from

Connally's wrist) match one another within one

standard deviation in both antimony and silver.

04, 5

(Fragments from President Kennedy's brain),

02 (large fragment found in car), and 014

(smaller fragments found in car) match one

another within one standard deviation in

both antimony and silver.

Di,

although similar in silver content, is

markedly different in antimony content from

02, 04, 5, and 014.

09

differs considerably from 02, Q4, 5, and

014 in bath antimony and silver..

These results therefore indicate the presence of

only two bullets: (01 and 09 one bullet) and (02, 04, 5, and

014 a second bullet). There is no evidence of a third

bullet.2/ The analyses not only resulted in values for silver

and antimony in the various samples, but also in values for

six additional elements: lead, copper, aluminum, manganese,

sodium and chlorine. The values for these additional six

elements do n

ot appear to contribute much useful information

except to confirm, quantitatively, that all the samples are

approximately 100% lead. With the exception of 09, all the

9.

Independent research conducted by the author (See, Refer-

ence Number 10 in Appendix H.) indicates that a careful

analysis of the data obtained by the FBI during the INAA

tests con

du

cted by the FBI in 1954 (using a scintillation

detector rather than the higher-resolution modern Ge(L1)

detector) would reach this same co

nclu

sion.

The Far re-

ported the results of its tests as Inconclusive due to

the wide variety of absolute values obtained each time a

sample was tested. These results, however, were under

differing test conditions. It is necessary to compare

the results obtained under a given set of conditions.

rather than a compariaon of all the values under all

conditinns, to reach

the co

nclu

sion

that only two bullets

were present.

Page 23: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

532

copper values were approximately the same -- in the range of

40 to 58 ppm. The very high copper value of the 09 sample

1994 ppel) is most likely due to contamination from the cooper

jacket of the bullet. The copper values for samples Q4, 5,

Q2, and Q14 average 42 + 2 ppm -- appreciably different from

the 01 (stretcher bullet) copper value of 58 + 3 ppm. The

aluminum values range from 1.1 to 3.1 ppm and show no

systematic trends between the two groups of samples. Similar-

ly, the manganese values range from 0.01 to 0.10 ppm and

show no systenatic behavior. The sodium values show a wide

range. from 5 to 134 ppm, and the chlorine values also show

a wide range, from 19 to 257 ppm -- in both cases with no

evidence of any trends. Even though all the samples were

washed three times with pere water and pure acetone, to free

them of any salt (sodium chloride) possibly accumulated on

the exteriors of tne samples from previous exposures to the

air and/or Possible handling by fingers (perspiration), it

cannot be ruled out that some slight and variable amounts of

salt contamination were still present in some of the

samples. It might be significant that the two samples that

show the highest levels of sodium and chlorine are samples

Q4, 5 (President Kennedy's brain) and Q9 (Governor Connally's

wrist) -- the only two samples that were recovered from

biological tissue. It is barely possible that these samples,

in spite of the washing, still contained a small but signifi-

cant amount of dried body fluid (e.g., blood), which would

111.

533

increase the levels of sodium and chlorine in the samples.

The other samples exhibited much lower levels of sodium

only 5 to 19 ppm) and of chlorine only L9 to 40 ppm).

Accordingly, neutron activation analysis of the

evidence specimens tested indicates the presence of only two

bullets in Group I. It is highly probable that the specimen

tested from Ql (the stretcher bullet) ana the specimen tested

from Q9 (the fragments from Governor Connally's wrist) are

from the same bullet. It is highly probable that G2 (large

fragment found in the limousine), Q4 and S (fragments from

President Kennedy's brain) and 014 (smaller fragments found In

limousine) are all from a second bullet. There is no evidence

of a third bullet from any of the evidence specimens tested.

10.

More recent very detailed INAA studies made at UCI (See

reference 11 in Appendix 9) on 10 samples from each of 16

Mannlicher-Carcano bullets -- 4 from each of the 4 produc-

tion lots -- give a more complete picture of the generally

high degree of homogeneity of individual bullets and the

wide variation from bullet to bullet, regardless of lot

number, of the antimony concentration in particular, the

appreciable variation of the silver concentration, and

the lesser variation of the copper concentration. However,

the earlier data and these more recent data do show some

Mannlicher-Carcano bullets that cannot be distinguished

from one another via only their antimony and silver

concentrations. From these data, it appears that if 2

cartridges are removed at random from a box of Mannlicher-

Careen° cartridges, although it is highly probable that

they would differ significantly in their antimony and

silver concentrations, it is at least possible that they

might not.

Page 24: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

534 635

APPENDIX A

LIST OF ABBAEVIATIONS AND SYMBOLS

0CI

University of California at Irvine, or 0.C. Irvine.

FBI

(U.S.) Federal Bureau of Investigation.

MC

Mannlicher-Carcano.

Sh

Chemical symbol for the element, antimony.

Acs

Chemical symbol for the element, silver.

Cu

Chemical symbol fox the element, copper.

Pb

Chemical symbol for the element, lead.

Al

Chemical symbol for the element, aluminum.

Mn

Chemical symbol for the element, manganese.

Na

Chemical symbol for the element, sodium

Cl

Chemical symbol for the element, chlorine.

122st Symbol for the antimony radioisotope of mass number 122.

(half life of 2.80 days), antimony - 122.

124m15h Symbol for the metastable antimony radioisotope of mass

member 124 (half life

of

93

seconds), antimony

124mi.

1245h Symbol for the antimony radioisotope of mass

number 124 (half Life of 60.4 days}, antimony - 124.

110Ag

Symbol for the silver radioisotope of mass number 110

(half life of 24.4 seconds), silver - 110.

64cu

Symbol for the copper radioisotope of-mass

number 64 (half life of 12.80 h

ou

rs). cop

per -

64.

66Cu

symbol for the copper radioisotope of mass

number 66 (half life of 5.10 minutes), cop

per -

66.

204mph Symbol for the metastable lead radioisotope of

mass number 204 (half' life o

f 66.9

minutes),

lead - 204m.

Symbol fo

r the aluminum radioisotope of mass

28Al

number 28 (half Life of 2.31 minutes), aluminum -

28.

$6

Symbol for the manganese radioisotope of mass

Mn

number 56 (half life

of

2.576 hours), manganese

56.

24ua

Symbol for the sodium radioisotope of mass number

24 (half life of 14.96 hours), sodium - 24.

Symbol for the chlorine radioisotope of mass

3801

number 38 (h

alf life

of 3

7.2

9 minutes),

chlorine - 38.

NAA

Neutron activation analysis.

fNAA

Instrumental nntiti-p

n activation analysis.

CE

Abbreviation for (Warren) "Commission Exhibit".

Page 25: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

537

Abbreviation for standard deviation, a statistical

measure of precision (also abbreviated as r or s).

Abbreviation far centimeter, a metric unit of

length (one inch equals 2.54 cm; one cm equals

10 mm).

Std.

dev.

cm

536

4C

Sample designation abbreviation used at UCI,

referring to "House Committee".

Abbreviation for cubic centimeter, a metric unit

of volume (one cubic inch equals 16.4 cm3).

Ge(1,1) Abbreviation for a lithium-drifted germanium

semiconductor gamma-rav detector.

rim

Aboreviation for millimeter, a metric unit of

length (one inch equals 25.4 mm).

mg

Abbreviation for milligram, a metric unit of mass

or weight (one gram equals 1000 mg.(.

Abbreviation for gram, a metric unit of mass or

weight (one ounce equals 29.3 c).

pg

Abbreviation for microgram. a metric unit of

mass

or weight (one gram equals one million pg).

Abbreviation for neutron, a fundamental particle

that is a constituent of atomic nuclei.

ca 2

Abbreviation for square centimeter, a metric unit

of area (one square inch equals 6.41 cm2).

key

Abbreviation for one thousand electron volts of

energy.

Abbreviation for gamma, as in gamma ray (e'ray).

Abbreviation for parts-per-million by weight (one

ppm

ppm equals one pg of constituent per gram of material).

3 qa

Page 26: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

APPENDIX C

BACKGROUND DATA ON MANNLICHER-CARCANO

AMMUNITION

During 1964, Dr. John Nichols obtained boxes of

Western Cartridge Company Mannlicher-Carcano 6.5 mm

cartridges from the four different production lots

of this ammunition that they produced: Lots 6000, 6001,

6002, and 6003. According to the Western Cartridge

Company, these production lots of this ammunition were of

one million rounds each, all produced in 1954 for the

U. S. Army. Each cartridge contained an average of 44

grains (2.85 grams) of a special blend of Western Ball.

Powder. The lead cores of the bullets weighed 110 grains

(7.13 grams), had a diameter of 5.33 mm and

a length of

26.2 mm, and consisted of 10 soft lead (99.851 pure).

The bullet jacket weighed 51 grains (3.3 grams), had a

side wall thickness of 0.66 mm, and consisted o! CDA No.

220 Commercial Bronze (90% copper, 101 zinc). The primer

cup was made of CDA alloy no. 260 cartridge brass (701

copper, 109 zinc), and its main components were 371 lead

styphnate, 32% barium nitrate, 151 antimony sulfide,

7% aluminum powder, 51 PETS, and 4% tetracene. Dr. Nichols

used some of this ammunition

in various test firings

0 Nn means none detected.

538 539

0 44 V

4

G > 0

V

• -11 91 • 4

44

C LIS C

.14 .I-1 H

I 0.I .-4

‘1. ea

04

H

4

y 0

IN

0 H

L0 mLc.0 L4

DIV

" 00 ,0

. 0

VI .-I-I 7

. C 0

4

44 0

-,-4 >

, 0 . 0 RI

0 H

>

4E

4

924

C n

a 3. 0

in 0 4.4

..1 J.} 93

t..1 C .0 ‘r >

In . . 40

.

ti 10

01

4 H

..0

..4

42CV020

44

44MME.Um

0>

V 0

>.

.0

2 a

c miq 4 3

.4 3

a 0 4

11 • 0

1

4 . . 1

-4 .

> =I t ir 1 .5 4 11 4 4 0;

S 0

a a a a a

C 1

3 H

NI 0

w

in c a

i

c a a a a a 4.• -

c ,-I

04 -1

rrr •-t -4.1

+4 +

1' +

1

-440

a 0

-•r a

a

•Y

a N

43

2 ' 2 VG30 >

0. Cl m a

a 0

. 0

va.1

4.2

c

XL

CL 4.-1,30

0000 0 o O C

M

O

0 m V

a >

VI 0

3

4

M

>L4.1

0.m. 02 04

4.

N v

ut1

I.1

1 a

. 4

00

=0

0

.

• V

'10

vi 4)

0

Cl 0

...1 0

a

0

0.I V

C 4

-I 0 7

0 .c

-,.. 1 2

+ I #

11 +

I +1

0 0

•4

VI H

N V

. LI 3

4

0 2

.,.. 0

0

VI .4-1 a

. 0 u u > o

. 1[.a m. N

0

Qui ....c

..

a

a0041.v

U 2

V

3.G0

E.... m

c

J.. M 0 a

r. .

N

+4

N N

V a

E

NV

>

1 4

0 .0

4

4.• +

1

+1

e- +

I +i

0 V 44

13 q.

Cl C

l 1

3 IS

V

N

0

• =

0 0

0)

01 10 V

v V

•o• v

0

OE

. 0.7

. .

HI Z

M

-100

V

10 H

WI

n 0

2.0

4 Em=

•a a a 0 o

-44 .1

M

CMCcE

4- +1 +4 M M M C

£020

a 5

Cl . aaam

EL

..-10

-,.. 41.00

'2

-LJ CI .1., .C.

14 ✓

at

N a

1 C

7 N

7

01

7

. •"' I.

H m U.

-wa Ii

< .91 . 4.4 C 414

G2

. KS

0 I ....-I 0

0

V

V N

V v

L. 3

H .0

. 0. +

I .0

+

I + 1

4-1

+4 +

4 +

1

0 4

14 rn

a 0

a m 0 a '9 0

1 •

-• N

Ca N

I.L

.

In

0

0

1 a H

v

14

• 01 0

-1

Cl

412 '4

, C

... '4

, W

I =

01

1

4C

4'

1,

1., )0>

c..2

....-lu

a

0

..Ial

40 e-1 00. L

IC

0E

1$3.1

.1

04

/0

0

70

4.1-

1.0

0

-r N

N

4

4.1

4. 0

0 0

433

+4 N

ess +

1 N

+1 1

12.0

LCV04m

m

+ 1

+1 e

r +1 n

cll

14 CU 01

. 1

9

4

a u

, tn

. o c

0

70

34

4

411214:>>

-I

a

a .. a

H •

-I 3.1

4 0

.04

1

0 7

0

MCM ..CL.Cr4=4m.

>O

a

a 414 rs .4

-• NI,

. . . ml

E .0

C W

0 C 1.,

.I

(V I ,

eh i

1 anii mo,.. 4E20

4 4

sr.

0 c a

0 0

.4 H

3 444.1

77.7

• 0

41.1) I•4 .

0 . • ,..

,

0441

gm

.u5S

ou.

.n a a

44 > 0

0 0

0 3

Z.

HP

N

Cl V

J0 V

v0 0

C 0 . 0

•er H

0 .0

44 +

1 V +

I 7

.0 .0

4.1 0 0

. 0 0

Et 0

0

0

OarJaa.0

G.10

gaC

OC

rCu

p

a N

. o

r 0

F

OC

El2

.(JE

84

. a '0

, , e

-

rn

WIC

E.C

7C

0

V

A

APPENDIX B

RE:in/TS EBOM SEPTExBEt: 1977 fNAA 61a EVIDENCE SPECIMENS AT U.C. 1RVINB

4 4

E M4

44 =

X

a 5

.0

E0.1

s ii U

6 >

1

E g

40

3

0

v.

61

a

L., 1

m 0

+1

N 0

+1 +1

+1 r--

+4 41

6-1 .0

N

N

V

I 10

In N

=a "1

a

n'

.

+1 ,

+1 H

H

H

+

t ...4 -1-

1

W

r1

0 M M

Nencl

m 0 m

m

m

Page 27: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

540

that he conducted with a Mannlicher-Carcano rifle of

the sane make as that reportedly used by Lee Harvey

Oswald. Lace in 1972, Or. Nichols contacted the

author, offering to supply bullet-lead samples from

the four production lots, for NAA examination by the

author. The author accepted the offer, and Or. Nichols

shortly sent him two bullets from Lot 6000 and four

each from Lots 6001, 6002, and 6003. The author

commenced analysis of these in late 1973 with most of the

work carried out during 1974 and a few final measurements

early in 1975.

Samples ranging in weight from 44 to 58 milligrams

(each weighed to within

0.1 milligram) were drilled out

from the open base end of each bullet with a cleaned small

steel drill, after first scraping the surface of the

bullet face free of oxidized layer with a clean stainless-

steel scalpel. Each drilled sample was washed with high-

purity toluene, to remove any oil or grease possibly

present. In the first analyses, all 14 samples, along with a

standard of antimony, were activated for 2 hours in the

rotary-specimen rack of the UCI TRIGA Mark I reactor, at

a thermal-neutron flux of 1.0 x 1012 n/cm2-sec. After

541

a decay period of approximately 24 hours, each activated

sample was counted for 200 seconds livetime on top of

a 38 cm3 Ge(1,41 detector (with a 1 cm beta-particle

absorber), coupled to a 4096-channel pulse-height analyzer.

The only photopeaks observed were those of 12.80-hour

64cu, 2.80-day I22Sb, 60.4-day 1246b, and 14.96-hour 24,a.

The counts in the 511 keV peak of "

Cu, in the 564 kev

peak of 1225b, and in the 1368 cell

peak of 24Na were

printed out. After correcting all of the data to the

same decay time, the number of micrograms of copper (Cu),

antimony (Sb), and sodium (Na) in each sample was calculated,

along with its standard deviation -- calculated from the

counting statistics. Dividing each pg value by the sample

weight, in grams, then gave the ppm concentrations. The

Cu and Na values were calculated from tabulated standard

values. These are tabulated in Table II-A.

Later, after the previously-induced activities had

decayed down to negligible levels, the 14 samples were

activated and counted again, under different conditions.

This time, the samples were activated and counted in sequence,

one at a time. Each sample was activated for 40 seconds

in the pneumatic-tube position of the reactor, at a

thermal-neutron flux of 2.5 x 1012 n/cm2 -sec. After a

Page 28: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

543

The new antimony results (from 124mlsb) and the new

copper results (from "Cu) in all cases compared well

with the results for these two elements obtained in the

previous longer irradiation (with measurement, instead,

of 1225b and "

Cu). However, the counting statistics

(precisions) of the 1225b and "

Cu results from the

longer irradiation were much better than those of the

1242'15b and "Cu results from the 40-second irradiations,

so only the 1225b and "

Cu results are given in Table II-A.

The antimony results obtained, shown in Table I1.711,

were surprising. In all earlier studies of commercial bullet

leads, individual bullets were found to be quite homogeneous

in their antimony concentrations, and bullets from the same

box of cartridges were found to be closely similar to one

a thermal-neutron flux only 1/110 as large. Microgram

and ppm values for As, Sb, and Cu wets then calculated

for each sample (along with its standard deviation, based

upon the counting statistics) from the sizes of the 653

another in their antimony concentrations. In sharp con-

trast, the bullet-to-bullet variation in antimony content

amongst bullets from the same box of Mannlicher-Carcano

cartridges is seen to be tremendous:

the four samples

keV peak of 24.4-second 110As, the 498 key peak of 93-

of lot 6001 bullet lead ranged all the way from 158 ppm

second 124711

5b, and the 1039 keV

peak of 5.10-minute

to 1218 ppm Sb; those of lot 6002 bullet lead all the

way from 24 to 949 ppm Sb; and those of lot 6003 all the

66Cu. The silver results are also included in Table II=A

way from 80 to 730 ppm Sb.

In general, such antimony

values indicate that (1) the bullets were indeed a soft

decay period of 40 seconds (during which the a

ctiv

ate

d

sample was transferred

to a fresh v

ial),

each

sample

was counted.

for 40 seconds clocktime under the same

counting conditions used in the previous measurements.

In the subsequent calculations, a small correction was

made for the average analyzer deadtime during each

cou

ntin

g.

The principal induced activities observed

in the pulse-height spectra were those of 24.4-second

110Ag(658 keVa,), 5.10-minute "Cu (1039 keVI), and 93-

second 12

-

4mlab (499, 603, and 646 keVy's), although the

12.80 hour "Cu (511 keV,)') and 2.00-dav 122Sb (564 keV,?-)

activities were also observed, as well as very small peaks

due to 66.9-minute 2134'

''Pb (373„ 899, and 912 keV's).

Standards of silver, antimony, and copper were then

activated and counted under the same conditions, but at

Page 29: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

044 545

Le

ad

, sin

ce

bu

llet le

ad

de

libe

rate

ly h

ard

en

ed

by a

lloyin

g

the L

ead w

ith a

ntim

ony re

quire

s th

e a

dditio

n o

f anyw

here

from

ab

ou

t 0.4

i (40

00

pp

m) S

b u

p to

se

ve

ral p

erc

en

t, (2) n

o

effo

rt was m

ade b

y th

e m

anufa

ctu

rer to

contro

l the

antim

ony c

onte

nt o

f the b

ulle

t lead,

so lo

ng a

s it w

as

much le

ss th

an 4

000 p

pm

, and (3

) the h

igh d

egre

e o

f Sb

va

riab

ility d

urin

g a

pro

du

ctio

n ru

n in

dic

ate

s th

at th

e

lea

d s

up

ply

wa

s o

f mix

ed

so

urc

es, a

pp

are

ntly

co

nta

inin

g a

n

appre

cia

ble

am

ount o

f scra

p le

ad (s

om

e o

f whic

h is

antim

ony-

hard

ene

d le

ad

), sin

ce v

irgin

lea

d s

eld

om

conta

ins m

ore

cha

r. 10

-20

pp

m S

b.

Fro

m a

gre

at d

eal o

f earlie

r work

an th

e /N

AA

of

bu

llet-le

ad

sa

mp

les fo

r Ag

, 5b

, an

d C

u, it h

ad

be

en

esta

blis

hed th

at th

e m

eth

od its

elf w

as h

ighly

repro

ducib

le,

ap

pro

xim

ate

ly to

with

in th

e lim

its im

po

se

d b

y th

e c

ountin

g

sta

tistic

s,

for a

ny in

div

idu

al s

am

ple

. T

o p

rove

this

po

int, h

ow

eve

r, tw

o in

div

idu

al s

pe

cim

en

s

(6.0

01 a

and 6

002

B) w

ere

ea

ch

an

aly

ze

d fo

ur tim

es,

for A

g, 5

b, a

nd C

u,

un

de

r the

pn

eu

ma

tic-tu

be

co

nd

ition

s.

As c

an b

e s

ee

n

fou

r pie

ce

s --

one o

f whic

h w

as th

e sp

ecim

en

an

alyze

d

ea

rlier.

These s

am

ple

s w

ere

then a

naly

zed fo

r Ag,

Sb, a

nd

Cu u

nder th

e s

am

e p

neum

atic

-tube c

onditio

ns u

sed b

efo

re.

The re

sults

are

show

n in

Table

II-C. A

s c

an b

e s

een,

of th

e th

ree

bu

llets

sa

mp

led

, on

e (6

00

1 C

) is

fairly

ho

mo

ge

ne

ou

s in

all th

ree

ele

me

nts

; on

e (6

00

2 A

) is

fairly

hom

ogeneous in

Ag a

nd C

u, b

ut ro

t so h

om

ogeneous

in S

b;

from

the re

sults

, show

n in

Ta

ble

II3,th

e re

pro

du

cib

ility

for a

giv

en

sa

mp

le is

ind

ee

d q

uite

sa

tisfa

cto

ry. A

fter

ea

ch

pp

m v

alu

e is

sh

ow

n its

sta

nd

ard

de

via

tion

, ba

se

d u

po

n

its c

ou

ntin

g s

tatis

tics. T

he

-I-

valu

e s

how

n a

fter e

ach

an

d o

ne

(60

03

A) is

fairly

ho

mo

ge

ne

ou

s in

Cu

, bu

t no

t

ho

mo

ge

ne

ou

s in

Sb

or A

g. H

ow

eve

r, co

mp

aris

on

of

Ta

ble

II-Cw

ithT

ab

leIz

,A in

dic

ate

s th

at, in

genera

l, the

mean v

alu

e, h

ow

ever, is

the s

tandard

devia

tion o

f the

set

of

fou

r va

lue

s, c

alc

ula

ted

from

the

de

via

tion

s o

f the

va

lue

s fro

m th

e m

ea

n v

alu

e. It c

an

be seen th

at th

e

sta

nd

ard

de

via

tion

sh

ow

n w

ith

the m

ean v

alu

e is

ge

ne

rally

fairly

clo

se

to th

e c

ou

ntin

g-s

tatis

tics s

tan

da

rd d

evia

tion

of a

n in

div

idual m

easure

ment.

To s

tudy th

e d

egre

e o

f hom

ogeneity

of in

div

idual

Mannlic

her-C

arc

ano b

ulle

ts, fo

ur s

am

ple

s of b

ulle

t lead w

ere

analy

zed fro

m e

ach o

f thre

e in

div

idual b

ulle

ts (b

ulle

ts

60

01

C, 6

00

2 A

, and 6

003 A

). The la

rger d

rillings o

bta

ined

from

ea

ch

of th

ese

thre

e b

ulle

ts (w

hic

h w

ere

ma

de

ap

pro

xim

ate

ly

dow

n th

e lo

ngitu

din

al a

xis

of e

ach

bu

llet) w

ere

cu

t into

Page 30: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

546 547

heterogeneity within an individual Mannlicher-Car ,ano

bullet is much less than the heterogeneity from one

bullet to another. One of the primary conclusions,

therefore, of the results of the UCI background study of

MC bullet lead indicates a wide range of Sb values.

from bullet to bullet, but reasonable homogeneity within

an individual bullet.

APPENDIX D

TABLE II-A

THE TRACE-ELEMENT COMPOSITION OF MANNLICHER-CARCANO 6.3 mm BULLET

LENDS FROM LOTS 6000, 6001, 6002, AND 6003

(INAA results obtained by V.P. Guinn during 1973-1975)

ppm Element Found, and Standard Deviation in ppm'

Lot No.

Bullet Sample

No.

Wt.(ng)

Silver

Antimony

Copper

Sodium

6000

A

51.2

11.8+0.4

173+3

372+6

13+1

B

45.6

13.5+0.5 261+3

167+4

15+1

6001

A

47.8

12.2+0.6

158+3 (2766+16).. 12,1

B

57.9

15.3+0.5 732+5

23+2

13+1

C

58.3

8.30.4

1218+7

48+2

15+1

0

47.2

11.6+0.4

161+3

147+4

17+1

6002

A

51.8

9.1.0.4

385+4

30,

2

12+1

B

52.8

9.7+0.4

949+6

25+2

12+1

C

55.3

6.0+0.3

24+1

120+3 15+1

0

51.3

8.3+0.6 121+2 (4516+21).. 13+1

6003

A

54.3

15.3+0.5 730+5

21+2

12.1

0 44.6

7.9+0.4

80+2

62+2

20+2

C

44.7

8.3+0.4

464+5

36+2

17+1

13 44.0

8.7.0.4

240+3

17.2

15+1

am. •

One standard deviation, based only upon the counting-

statistics standard deviation of a single measurement.

These two copper values are extremely high. It may be

that these two samples were contaminated with jacket

material during the drilling out of the sample.

• •

Page 31: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

• I

548 '1

9

APPENDIX E

APPENDIX '

TABLE LI-B

TABLE II-u

REPRODUCIBILITY MEASUREMENTS ON TWO INDIVIDUAL SPECIMENS OF

MANNLICHER-CARCANO BULLET LEAD (MACE BY V.P. GUINN, PNEUMATIC-

TUBE CONDITIONS).

Measurement

Specimen

No.

ppm Element Found + One Standard Deviatio:

antimony

sliver

coorier

60013(57.3mg)

1

621,

56

15.3+0.5 19+10

2

646+55

16.6+0.4 19+4

3

646+55

13.9+0.4 18+5

4

791+55

15.0+0.4

20+5

mean:

676+78

15.2+1.1 18.5+1.3

60028(52.9mq)

1

990 . 1

60

9.7+0.4

16+10

2

1007+56

10.1+0.4

10+5

3 942+56

9.8+0.4

24.5

4

946+56

10.7+0.4

24,5

mean:

971-32

10.1+0.5 18.5+6.8

Standard deviation of individual measurements based

upon counting statistics only. Standard deviation

shown with mean values based upon the spread of

the four individual measurements.

HOMOGENEITY MEASUREMENTS ON FOUR SPECIMENS FROM EACH OF THREE

INDIVIDUAL MANNLICHER-CARCANO BULLETS (MADE BY V.P. GUINN,

PNEUMATIC-TUBE CONDITIONS)

Production

Lot

ppm Element Found + One Standard Deviation'

Specimen

Antimony

Silver

Copper

6001

6001C

1139+60

8.5+0.4

67+11

600101

1062.60

9.5+0.4 (391+17)"

6001C2

1235+93

10.1+0.6

20+7

6001C3

1156+90

9.2+0.5

23+10

mea n

: 1148+71

9.3+0.7

37+26

6002

6002A

358+47

9.1+0.4

45-11

6002A1

983+51

10.3+0.3

34+5

6002A2

869+47

9.9+0.3

58+6

6002A3

882+81

10.2+0.5

30+8

mean:

773+281

9.9+0.5

42+13

6003

6003A

e6,4-8

15.9+0.3

27+10

6003A1

395+54

9.6+0.4

28+6

6003A2

363+39

8.3+0.3 (257+12)**

6003A3

441+51

9.8+0.4

16+5

mean:

466-137 10.9+3.4

24+7

• Standard deviation of individual measurements based upon

counting statistics only. Standard deviation shown with

mean values based upon the spread of the four (or three)

individual measurements.

These two copper values excluded from the means as

probably due to contamination from the bullet jackets.

• •

Page 32: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

• 1

N

Ci. 0

r-

V N

M

+

I

0

6!

• M

ea

21

to!

Sample Number

550 551

C

,ua E

C

+1 +1 W

I I

at 0

APPENDIX H

REFERENCES ON THE INAA OF BULLET LEAD

+I

of

I 2

N'

2

+I

o

+I

I a 0

0

!i2

a

2.

0 0

3.

7

C

z

ea 4.

+

i C‘e

I

I.

H.R. Lukens and V. P. Guinn, "Neutron Activation

Analysis of Bullet Lead", Trans. Amer. Nucl. Soc.,

10 (1967)66-67.

H. R. Lukens, 'Forensic Activation Analysis, Bullet

Lead', Trans. Amer. Nucl. Soc., 11 (1968) 80-61.

V. P. Guinn, "Forensic Activation Analysis as Applied

to the Work of the Coroner", Proc. Intl. Assocn. of

Coroners And Medical Examiners, 1967-1959, pages

151-164.

H. R. Lukens, H. L. Schlesinger, V. P. Guinn, and R.P.

Hackleman, "Forensic Neutron Activation Analysis of

Bullet -Lead Specimens", U. S. AEC Report GA-10141

(1970), 48 pages.

5.

H. R. Lukens and V. P. Guinn, "Comparison of Bullet-

Lead Specimens by Nondestructive Neutron Activation

Analysis", 3. Forensic Sciences, 16 (19711 301-308.

V. P. Guinn, "Applications of Nuclear Science in

Crime Investigation", chapter in Annual Review of

Nuclear Science (Vol. 24), edited by E. Segre (Annual

Reviews, Inc., Pala Alto, Calif., 1974, pages 561-591.

7.

V. P, Guinn and H. A. Purcell, 'A Very Rapid Instrumental

Neutron Activation Analysis Method for the Forensic

Comparison of Bullet-Lead Specimens', J. Radioanal.

N

0

a •

0

m +

1 E a.c

N

C

. • M

6

• +

>

0.-.

APPENDIX G

H

R ESULT

S

FRO M

SEPTEMBER

19 77

INA A O F

ANALYSIS

OF

WALKER

BULLET

FRAGMEN T AND

UNFIR ED

C. IRVINE MC CARTRIDGE AT

Page 33: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

553

Mr. W

OL

F. M

r. Ch

airman

, I hav

e no

furth

er qu

estion

s of D

r. G

uinn. C

hairman ST

OK

ES. T

he Chair now

recognizes the gentleman from

Indiana, M

r. Fithian, for such tim

e as he may consum

e. M

r. Frrm

AN

. Thank you, M

r. Chairm

an. D

r. Gu

inn

, we are h

app

y to

hav

e yo

ur ex

pertise assistin

g th

e p

anel. I am

ho

ldin

g in

my

han

d a lead

pen

cil, and

I hav

e no

w

bro

ken

the p

oin

t from

this lead

pen

cil. Would

you tell m

e is this

enough for you to analyze by your process? D

r. GU

INN

. Well, that is a different kind of m

aterial. M

r. FIT

HIA

N. I know

. D

r. GuiN

N. It is called pencil lead; but it is actually graphite—

not lead. M

r. FIT

HIA

N. Sizew

ise? D

r. GurN

N. S

izewise, that is plenty. F

or materials such a bullet

lead, to

be sp

ecific, any sam

ple th

at weig

hs an

yw

here b

etween

1

and

50

millig

rams is su

fficient o

r plen

ty. S

uch

an am

ou

nt rep

re-sents a rather tiny sam

ple of lead, but it is all we need.

Mr. F

ITH

IAN

. Now

, if this were not graphite, and if it w

ere bullet lead

, and it co

ntain

ed a v

ariety o

f these elem

ents th

at you h

ave

describ

ed h

ere tod

ay, an

timo

ny

, silver, an

d so

forth

, wo

uld

yo

ur

neutron activation analysis sort out the count sufficiently accurate-ly to tell us w

hich elements are in that particle?

Dr. G

urN

N. It w

on't tell y

ou all th

e elemen

ts that m

ay b

e in

them

, bu

t it will u

sually

giv

e yo

u n

um

erical results fo

r a nu

mb

er of elem

ents th

at will b

ecom

e detectab

ly rad

ioactiv

e and read

ily

identified; yes. M

r. FrrH

ull. A

s I understan

d it, th

is is from

one p

ass thro

ugh

the eq

uip

men

t, simultan

eously

you read

out sev

eral differen

t ele-m

ents? D

r. Gum

- N. T

hat is true. Usually w

hen you activate a sample for

a certain len

gth

of tim

e in th

e reactor, w

ait a while, an

d th

en

cou

nt th

e samp

le, yo

u see p

eaks fro

m a n

um

ber o

f radio

active

elements. T

hen if you take the same sam

ple, if you wish, and do it

over again, but this time irradiate longer and w

ait longer, then all of the isotopes you saw

before you won't see this tim

e because you have w

aited long enough that they are all gone, and now you w

ill see som

e longerlived isotopes that were not there detectably before

but now they are.

So you don't usually just do an activation and a count once, but

you usually do it two or three tim

es, if you are trying to look for a large num

ber of elements.

Mr. F

ITH

IAN

. You used the term

counting equipment. C

ould you explain that for those of us w

ho are laymen in this?

Dr. G

uiN

N. T

here are m

any k

inds o

f radio

active d

etection d

e-vices w

hich are usually loosely called counters. The m

ost comm

on o

ne m

ost p

eop

le kn

ow

abo

ut is a G

eiger co

un

ter. If these sam

e sam

ples, after activ

ating

them

, had

been

held

near a G

eiger

counter, you would hear the G

eiger counter ticking away. U

nfortu-nately, the G

eiger counter is, No. 1, not very sensitive for gam

ma

radiatio

n, an

d. N

o. 2

, it can't tell o

ne g

amm

a ray fro

m an

oth

er. Y

ou have to go to a more elaborate detector. T

he kind, for exam-

ple, that was used by the F

BI in 1964, w

hich was the only useful

kind that was available then, w

as a scintillation detector. That is a

552

Chem., 39 (19771 95-91.

a. T

. Tzak

-Sira

n a

nd V

. P. G

uin

n, "A

naly

sis of

Meta

l

Frag

men

ts for lead

via th

e 20421, (n

,n,)204m

pb

Reaction", Trans. A

mer. N

ucl.. S

oc., 2

8 (1

578) 9

4.

9. N

. R. W

allis, V

. P

. G

uinn, and

M. A

. Purc

ell,

"Neu

tron A

ctivatio

n Analysis of Shotgun P

elle

ts",

Tran

s. Am

er. Nucl. S

ec., 2

8 (1

97

8) 9

3-9

4.

13.

V. P. Guinn an

d J. N

ich

ols, 'N

eu

tron

Activation

An

aly

sis of S

ulle

t-Laad

Sp

ecim

en

s; Th

e P

resid

en

t

Ken

ned

y A

ssassinatio

n", T

rans. A

mer. N

ucl. S

oc.,

28

(19

73

) 92

-93

.

11

. V

. P. G

uin

n. T

. izak-S

iran, a

nd M

. A. P

urc

ell,

"Detailed Measurements of Homogeneity of

Man

nlich

er-Carm

soc au

llets," to be submitted

for p

ublic

atio

n.

Page 34: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

554

solid

detecto

r. it abso

rbs g

amm

a rays b

etter, so it is m

ore efficien

t, an

d also

the size o

f the o

utp

ut p

ulse fro

m th

e detecto

r is pro

por-

tional to

the g

amm

a ray en

ergy it h

as abso

rbed

. S

o w

ith su

ch a d

etector o

ne h

as the p

ossib

ility o

f usin

g w

hat w

e call a

multic

hannel a

naly

zer to

look a

t the o

utp

ut p

ulse

s, sort

them

into

their sizes, an

d g

et a spectru

m w

ith p

eaks.

Mr.

FIT

HIA

N.

The cu

rrent eq

uip

men

t is gen

erations rem

oved

fro

m th

e 19

64

equ

ipm

ent?

Dr. G

UIN

N. Y

es, sir. The old scintillation detectors are still useful

for so

me p

urp

oses, b

ut th

e difficu

lty is th

at in a sp

ectrum

obtain

ed

from

it, each o

f the p

eaks is ty

pically

abo

ut 2

0 tim

es wid

er than

th

e peak

s from

a modern

germ

aniu

m d

etector. W

e say th

at mean

s th

at the o

lder scin

tillation

detecto

r has v

ery p

oo

r energ

y reso

lu-

tion.

In th

e c

hart e

xam

ple

that sh

ow

s the silv

er-1

10

peak

, with

a

little antim

ony-1

24m

, peak

nex

t to it, fo

r exam

ple, w

ith a scin

til-latio

n d

etector all y

ou w

ould

see would

be o

ne b

road

peak

that

inclu

ded

both

of th

em, an

d y

ou w

ould

n't k

now

that y

ou really

were

lookin

g at tw

o g

amm

a rays, o

f two d

ifferent en

ergies.

The g

erman

ium

detecto

r, the m

ore m

odern

type, w

hich

wasn

't av

ailable g

enerally

in 1

96

4, is a h

igh

-resolu

tion

detecto

r. it is of a

new

gen

eration o

f detecto

rs, and th

at was really

one o

f the p

rimary

reaso

ns fo

r wan

ting

to rean

alyze th

ese samp

les, bu

t no

w w

ith

much

more m

odern

equip

men

t. M

r. F

ITH

IAN

. Ju

st for th

e re

co

rd, b

efo

re I a

sk th

e a

dd

ition

al

qu

estion

s, in y

ou

r answ

er to co

un

sel Wo

lfs qu

estion

yo

u u

sed th

e p

hrase th

at the W

CC

Man

nlich

er-Carcan

o b

ullets w

ere mad

e of

un

hard

ened

lead. Y

ou

were referrin

g o

nly

to th

e lead co

re and

no

t to

the h

arden

ed co

pper jack

et? D

r. GulatN

. That is co

rrect. The sp

ecifications fo

r those b

ullets

were th

at they

were to

be m

ade o

f No. 0

soft lead

, unhard

ened

, th

at was at least 9

9.8

5 p

ercent lead

. M

r. FIT

HIA

N. O

ne o

f the m

ost serio

us q

uestio

ns facin

g th

e pan

el is th

e id

en

tificatio

n o

f the "p

ristine" b

ulle

t with

the fra

gm

en

t tak

en fro

m G

ov

erno

r Co

nn

ally, in

the w

rist wo

un

d area. I realize

the im

po

rtance o

f yo

ur co

nclu

sion

that th

e fragm

ents rem

ov

ed

du

ring

the su

rgery

from

Go

vern

or C

on

nally

's wrist w

ere from

the

"pristin

e" b

ulle

t, and I re

aliz

e th

e d

ifficulty

of sa

yin

g y

ou a

re

abso

lutely

certain to

the ex

clusio

n o

f all oth

er possib

ilities, but I

am w

onderin

g if y

ou co

uld

go an

y fu

rther th

an y

ou h

ave, in

terms

of certain

ty o

f the co

mpariso

n o

f those tw

o sp

ecimen

s? D

r. G

UIN

N. I d

on't th

ink th

at I c

an in

the se

nse

of p

uttin

g a

p

ercent p

rob

ability

or so

meth

ing

like th

at. All I can

say is th

at th

ose tw

o sp

ecimen

s. CE

-399 an

d 8

42, ag

ree so clo

sely in

their

antim

ony co

ncen

tration an

d th

eir silver co

ncen

trations th

at I could

n

ot d

isting

uish

on

e from

. the o

ther. H

ow

ever. I can

clearly d

istin-

guish

those tw

o fro

m th

e ether th

ree specim

ens. T

hey

are differen

t. T

hey

are still WC

C M

annlich

er-Carcan

os; b

ut th

ey rep

resent a

differen

t WC

C M

annlich

er-Carcan

o b

ullet.

Mr. F

ITH

IAN

. An

d so

it is yo

ur testim

on

y th

at it is very

un

likely

:h

at these w

ere fragm

ents fro

m tw

o d

ifferent b

ullets?

Dr. G

UIN

N. It w

ou

ld b

e extrem

ely u

nlik

ely. Y

ou

can im

agin

e that

certainly

there are so

me W

CC

Man

niich

er-Carcan

o b

ullets th

at are o

f essentially

the sam

e com

po

sition

. and

hen

ce that th

e pristin

e

555

bullet m

ight b

e one b

ullet th

at just h

appen

ed to

hav

e the sam

e co

mp

ositio

n as a d

ifferent b

ullet th

at fractured

the w

rist, for ex

am-

ple, b

ut it is v

ery, v

ery u

nlik

ely.

Mr. F

ITH

IAN

. But the scientific term

that you used, is it extreme-

ly u

nlik

ely?

Dr. G

uiana. Extrem

ely unlikely, or very improbable, how

ever you p

refer. M

r. FiT

HIA

N. T

o y

our k

now

ledge, h

as any o

ther scien

tist to d

ate lin

ked

the so

-called p

ristine b

ullet to

the in

juries?

Dr. G

UIN

N. N

ot that I am aw

are of; no. M

r. Frrin

AN

. Eq

ually

imp

ortan

t, as yo

ur co

nclu

sion

s con

cernin

g

Go

vern

or C

on

nally

's wrist in

juries an

d th

e "pristin

e" bu

llet, is the

second co

nclu

sion y

ou m

ake, an

d th

at is that th

ere is no ev

iden

ce of a th

ird, fo

urth

, or fifth

bullet rep

resented

in an

y o

f the frag

-m

ents th

at you tested

? D

r. GuIN

N. T

hat is correct. M

r. Frrin

ata. And th

erefore, it is h

ighly

likely

—is th

at the term

y

ou

used

to M

r. Wo

lf—th

at all fragm

ents tested

match

up

with

two

b

ullets an

d tw

o b

ullets o

nly

? D

r. GU

INN

. Yes, sir. T

he o

ther th

ree samp

les that w

e hav

e been

referrin

g to

—o

ne b

eing

the frag

men

ts recov

ered fro

m P

residen

t K

enned

y's b

rain, an

d th

en tw

o d

ifferent g

roups o

f particles fo

und

on th

e floor o

f the lim

ousin

e—th

ose th

ree specim

ens are in

distin

-guish

able fro

m o

ne an

oth

er, but m

arked

ly d

ifferent fro

m C

E-3

99

and

84

2. S

o th

ere is on

ly ev

iden

ce for th

e presen

ce of tw

o d

ifferent

bu

llets. M

r. Frrzn

AN

. I understan

d th

at the W

arren C

om

missio

n d

id

emissio

n sp

ectrograp

hy tests o

n m

any o

f the sam

e items y

ou h

ave

tested w

ith n

eutro

n activ

ation an

alysis. H

ow

does th

e neu

tron

activatio

n an

alysis p

rocess, ju

st in b

rief laym

an's term

s, differ, an

d

wh

at are the ad

van

tages o

r disad

van

tages o

f the tw

o m

etho

ds o

f testin

g?

Dr. G

UIN

N. W

ell, they

hav

e som

e similarities an

d th

ey h

ave

som

e differen

ces. Th

ey are b

oth

meth

od

s of elem

ental an

alysis.

Th

ey w

ill bo

th d

etect do

wn

into

wh

at we call th

e trace elemen

t ran

ge, ap

pro

achin

g p

arts per m

illion, let's say

, and th

ey w

ill both

detect a n

um

ber o

f elemen

ts more o

r less simultan

eously

in th

e specim

ens. N

ow

, wh

ere they

differ is th

at for m

ost elem

ents, at least, w

e can

detect m

uch

low

er con

centratio

ns b

y activ

ation

analy

sis. In o

ther

word

s, activatio

n an

alysis is m

ore sen

sitive fo

r most elem

ents.

Wh

at is perh

aps ev

en m

ore im

po

rtant, th

ou

gh

, is that activ

ation

an

alysis, w

hen

it measu

res som

ethin

g, m

easures it v

ery q

uan

tita-tively. E

mission spectrography does not.

I hav

e a cop

y o

f all of th

e FB

I raw d

ata from

tho

se measu

re-m

ents, an

d th

ey list th

ings lik

e mag

nesiu

m, a trace; ch

rom

ium

, a very

slight trace; an

d th

ings lik

e that. N

o n

um

bers. S

o y

ou can

't m

ake an

y k

ind o

f quan

titative co

mpariso

ns b

y lo

okin

g at in

form

a-tio

n o

f that so

rt. And th

e remain

ing d

ifference is th

at the em

ission

spectro

grap

hic m

etho

d is d

estructiv

e. Yo

u n

orm

ally w

ou

ld lik

e to

hav

e abo

ut 1

0 m

illigram

s of sam

pies, w

hich

isn't a g

reat deal. b

ut

that 1

0 m

illigram

s is totally

consu

med

, it is vap

orized

and it is

gone. wh

ereas th

e way

we an

alyze b

ullet-lead

samp

les. at least, and

Page 35: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

• v. a

556

man

y o

ther k

inds. b

y activ

ation an

alysis, th

e meth

od is n

onde-

structive. T

hese sam

e samples I an

alyzed

, if som

ebody d

idn't ag

ree with

the num

bers, they could come back and do them

all over again on the sam

e specimens.

Mr. F

ITH

IAN

. Your results then could be verified by others?

Dr. G

utx

x. Y

es, sir, all the sam

ples I activ

ated an

d an

alyzed

w

ere turn

ed rig

ht b

ack o

ver to

the A

rchiv

es, and

they

are righ

t back there, and they could be reanalyzed.

Mr. F

ITH

IAN

. Dr. G

uin

n. th

is is not m

eant to

be an

embarrassin

g

questio

n, b

ut I th

ink I m

ust ask

it. Mr. C

hairm

an, a recen

t article in

the N

ew T

imes m

agazin

e stated th

at yo

u h

ad w

ork

ed fo

r the

Warren C

omm

ission and, therefore, your conclusions for this com-

mittee w

ould be implicitly biased.

Did

you ev

en w

ork

for th

e Warren

Com

missio

n o

r work

for th

e F

BI in

connectio

n w

ith th

e analy

sis of th

ese evid

ence sam

ples?

Dr. G

UIN

N. N

either one. I think Mr. W

olf called my attention to

the existence of this article, which I haven't seen, and I don't know

w

here th

ey g

ot th

eir misin

form

ation, b

ut I n

ever d

id an

yth

ing fo

r the W

arren Com

mission, and although I know

people in the FB

I, I have never done any w

ork for them.

Mr. F

ITH

IAN

. Bu

t it is correct, isn

't it, that th

e Warren

Co

mm

is-sio

n h

ad th

e FB

I perfo

rm n

eutro

n activ

ation an

alysis m

easure-

ments on the bullet-lead specim

ens in 1964? D

r. GU

INN

. Yes, sir.

Mr. F

rraux. How

did you find this out? D

r. GU

INN

. Well, it w

as rather interesting because both Dr. John

Nich

ols an

d I felt th

at activatio

n an

alysis o

f the b

ullet-lead

speci-

men

s in th

e Presid

ent K

enned

y case sh

ould

be d

one, an

d h

e in

particu

lar was try

ing to

persu

ade J. E

dgar H

oover, first, an

d later

Claren

ce Kelley

, that th

ese thin

gs sh

ou

ld b

e do

ne. H

e mad

e no

progress w

ith them, an

d th

en q

uite accid

entally

there tu

rned

up in

th

e Arch

ives a letter fro

m J. E

dg

ar Ho

ov

er to J. L

ee Ran

kin

, in

July

19

64

, stating

that in

deed

the F

BI h

ad m

ade activ

ation

analy

-sis m

easurements on these sam

ples. Until then, this fact w

as total-ly unknow

n to us, so, therefore, after that we requested the results,

becau

se, the letter d

idn

't giv

e any

nu

merical resu

lts; it just said

th

at the an

alyses h

ad b

een d

one an

d th

e results w

ere gen

erally

inco

nclu

sive. T

his ag

ain to

ok

qu

ite som

e time, an

d it w

as on

ly

finally

, under th

e amen

ded

Freed

om

of In

form

ation A

ct, that D

r. N

ichols w

as able to

obtain

the so

me 7

0 p

ages o

f raw d

ata copied

out o

f the F

BI reco

rds, fro

m th

e FB

I. I then

took all o

f those d

ata and recalculated them

from scratch.

Mr. F

ri-aux

. I wan

t to co

me b

ack to

that d

ata in ju

st a mo

men

t; becau

se I thin

k it is v

ery, v

ery, im

po

rtant fo

r us to

explo

re that

with you, but let m

e ask, i prior to doing that, do you know w

hy the existence of these tests w

as never divulged until recently? D

r. GU

INN

. No; I certainly don't know

why. I can just speculate.

The letter states th

at—if I m

ay ju

st read th

is one last little sh

ort

sentence in it—th

is is from

J. Edgar H

oover to

the W

arren C

om

-m

ission. It states: W

hile

min

or va

riatio

n%

in co

mpositio

n w

en. fo

un

d b

y this m

eth

od. th

ese

were

not

, ansu

rvpiv d

iffere

ntia

ting in

vine,th

e ia

nte

r ou

tlet

557

fragm

ents a

nd th

us p

ositive

ly dete

rmin

ing fro

m w

hich

of th

e la

rger b

ulle

t frag-

ments a

ny g

iven sm

all le

ad fra

gm

ent m

ay h

ave

com

e.

I believe probably that the FB

I and the Warren C

omm

ission both felt th

at this d

idn't p

rove an

yth

ing, in

their o

pin

ion, an

d, th

ere-fore, didn't need to be noted.

Sin

ce we h

ad b

een ask

ing th

em fo

r quite so

metim

e to p

erform

su

ch an

alyses, w

e rather th

ou

gh

t it wo

uld

hav

e been

nice if th

ey

had

told

us, in

stead o

f our ev

entu

ally fin

din

g o

ut accid

entally

. M

r. Frraux. M

r. Chairm

an, I would like the record to show

that th

e witn

ess, Dr. G

uin

n, w

as readin

g th

e last parag

raph o

f a letter from

J. Edgar H

oover to J. Lee R

ankin, the General C

ounsel to the P

resident's Com

mission, the so-called W

arren Com

mission, dated

July 8, 1964, and delivered by courier service. I would ask that the

entire letter b

e mad

e a part o

f this ex

hib

it as JFK

exhib

it No.

F-332. C

hairman S

TO

KE

S. W

ithout objection, it may be entered into the

record. [T

he above referred to JFK

exhibit No. F

-332 follows:]

Page 36: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

a .•

a

558

UN

ITE

:0 ST

AT

ES

DE

PA

RT

ME

NT

OF

JUS

TIC

E ,

r coE

rst suu

mA

u o

r tsrEsT

icAT

[es • s

W•1

11

.1C

TO

M

we

m

By C

ou

rie

r S

ervic

e E

. 2

W •

a =

Ju

ly 8

, 19

64

Ro

no

rab

la J

. Lee R

an

kin

G

enera

l Co

un

sel T

he P

resid

ea

t's Co

mm

ission

2

00

liary

lan

d A

ven

ue, N

orth

east'

Yar."

4ial.co=,

D. C

.

Doer ;Ir. R

an

kin

:

As p

revio

usly

rep

orte

d to

the C

om

missio

n, c

erta

in

small le

ad

meta

l fragm

en

ts un

covered

in c

on

nectio

n w

ith th

is m

atte

r T

erse

an

aly

zed

spectr

og

ra

ph

ica

lly to

dete

rm

ine w

heth

er

they c

ou

ld b

e a

ssocia

ted

with

on

e o

r m

ore o

f the le

ad

bu

llet

fragm

en

ts an

d n

o sig

nific

an

t diffe

ren

ces w

ere fo

un

d w

ithin

th

e se

nsitiv

ity o

f the sp

ectr

ograp

hic

neth

od

.

Beca

use

of th

e h

igh

er se

nsitiv

ity o

f th

e n

eu

tron

activ

atio

n tn

elY

sls, certa

in o

f the sm

all le

ad

fragm

en

ts were

Th

ee su

bje

cte

d to

neu

tron

activ

atio

n a

naly

ses a

nd

com

pariso

ns

vita

the la

rger b

ulle

t fragm

en

ts. Th

e ite

ms a

naly

zed

inclu

ded

th

e fo

llow

ing

: Cl - b

ulle

t Iro

n str

etc

her; C

2 - fr

ag

men

t fro

m

fro

st sea

t cu

shio

n; C

4 an

d C

S - m

eta

l fra

gm

en

ts fro

m P

resid

en

t K

en

ned

y's h

ead

; C9 - n

ata

l fragm

en

t from

the a

rm

of G

overn

or

Co

nn

elly

; C1

6 - n

ata

l fragmen

ts from

rear flo

or b

oard

carp

et

of th

e c

ar.

,a1 -a6 C

a'ra-a. W

hile

min

or v

aria

tion

s in c

ocg

ositio

n w

ere fo

un

d b

y

:his m

eth

od

, these

were n

ot c

on

sidered

suffic

ien

t to p

erm

it 1,a

sittray d

ifferen

tiatin

g a

mon

g th

e la

rger b

ulle

t fragzen

ts A

nd

Th

us p

ositiv

ely

dete

rm

inin

g Ir

on

Th

igh

of th

e la

rger b

ulle

t fra

gm

ents a

ny g

iven

small'Id

ad

fragm

ent m

ay h

av

e Com

e.

.Sin

cerely

nw

s,

JFK

EX

HIB

IT F

-332

559

Dr. G

urm

i. May

I com

men

t—I w

ill giv

e yo

u th

is cop

y o

f the

letter—but it does have stam

ped on it, which of course w

asn't th

ere originally, John N

ichols stamp w

hen he received it, in Novem

ber 1

97

3, an

d h

e also w

rote in

him

self on

e little han

dw

ritten lin

e. T

hose were not in original, but otherw

ise it is a copy of the original letter.

Mr. F

rrinat4

. So, fo

r the reco

rd, th

en, th

e han

dw

ritten n

otatio

n

between paragraphs tw

o and three, which read "H

e did not exam-

ine the copper, zinc jackets and fragments, "

was w

ritten b

y P

rof.

John N

ichols an

d w

ere not a p

art of th

e orig

inal letter w

hen

we

received it? D

r. GU

INN

. I guess that was John N

ichols little note from him

to m

e that h

e put in

there.

Mr. F

ITH

IAN

. With regard to that im

portant paragraph that says. "T

hese are inconclusive," I w

ould like now to ask you, D

r. Guinn, if

you could tell us what your findings w

ere when you looked at the

same 7

0 p

ages o

f raw d

ata, and

prio

r to th

at, are yo

u aw

are or d

o

you know w

ho and how this neutron activation analysis w

ork was

done an

d w

heth

er this w

as a com

mon p

ractice of th

e FB

I or ju

st how

this came about?

Dr. G

inral. Y

es, I hav

e sub

sequ

ently

fou

nd

ou

t mo

st of th

e details of it. T

he FB

I work w

as done in May 1964, at w

hich time

the F

BI lab

orato

ry h

ad n

ot d

one an

y p

rior activ

ation an

alysis

work

, so far as I am

aware. B

ut in

the sam

e elemen

tal analy

sis group, w

here such work w

ould normally fall, they asked M

r Jack G

allagher (John F. G

allagher) of their staff, whom

I know, to take

these bullet lead specimens dow

n to the Oak R

idge National L

abo-ratory.

Mr. F

ITH

IAN

. To w

here? D

r. GU

INN

. To the O

ak Ridge N

ational Laboratory, in O

ak Ridge,

Ten

n., w

here th

ey h

ave all th

e nuclear facilities, an

d so

on, th

ey

are qu

ite go

od

, and

they

do

a lot o

f activatio

n an

alysis w

ork

, alth

ough n

ot u

sually

connected

with

crime in

vestig

ation, b

ut fo

r other purposes. H

e took the samples dow

n there. T

wo o

f the p

eople d

ow

n th

ere, who w

ere hig

hly

conversan

t in

activatio

n an

alysis, b

ut n

ot in

foren

sic wo

rk, an

d M

r. Gallag

her,

who w

as highly conversant in forensic work but not in activation

analysis work, w

orked together. He actually did all of the m

easure-m

ents, but with the tw

o Oak R

idge people showing him

how to do

it and

ho

w to

calculate th

e results, et cetera, sin

ce this really

was

his first experience in this field. M

r. FIT

HIA

N. A

re you saying this was the first neutron activation

analysis work done by the F

BI?

Dr. G

unill. So far as I am

aware, it w

as; yes. M

r. FIT

HIA

N. T

his is the first that they had ever done? D

r. G

UIN

N.

Tw

o y

ears later, in 1

966, th

ey set u

p a reg

ular

activation analysis group in the FB

I laboratory, which it still oper-

ates. Bu

t at that tim

e, it was th

eir first, direct co

ntact w

ith th

e m

ethod, I believe. A

t any rate, Jack Gallagher. in a period of som

e days there. did g

o ah

ead an

d an

alyze th

e samp

les. and

he calcu

lated th

e results.

and he obtained a lot of numerical results.

Page 37: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

• 1. *

560

When

I obtain

ed all o

f these d

ata and w

ent th

rough th

e calcula-

tions, m

y in

itial reaction w

as pretty

much

the sam

e as theirs, o

r his. M

r. FIT

HIA

N. T

hat is, it was inconclusive?

Dr. G

UIN

N. T

he numbers appeared to bounce everyw

here. Any

on

e samp

le just d

idn

't seem to

be co

nsisten

t. To

just p

ick an

ex

amp

le here, fo

r one p

articular sp

ecimen

, one tim

e he m

easured

it, and found it to be 977 parts per m

illion antimony. A

nother time

he m

easured

it, but th

e result w

as only

676. T

he n

um

bers ju

st bounced around.

He m

easured

each sam

ple a n

um

ber o

f times u

nder so

mew

hat

differen

t con

ditio

ns, b

ut th

is sho

uld

n't m

ake an

y d

ifference, y

ou

sh

ould

get essen

tially th

e same n

um

ber ev

ery tim

e, merely

som

e-w

hat d

ifferent w

ith u

ncertain

ties. My in

itial reaction w

as thus,

exactly

the sam

e as his. A

t that tim

e I just w

ent th

rough all o

f the

data quickly and initially could not make any sense of it. I conclud-

ed th

ey h

ad d

one carefu

l work

, in g

eneral, b

ut it so

meh

ow

did

n't

make sense. T

hen

I did

my o

wn an

alyses h

ere and fo

und v

ery d

efinitely

that

the sam

ples fell in

to th

e two g

roups, tw

o b

ullets, so

then

I asked

m

y self, as far as I k

now

, even

though th

ey h

ad m

ore an

tiquated

eq

uip

men

t at that tim

e, these an

alyses w

ere done w

ell, why can

't you get the sam

e results out of their data, and I went back through

a second tim

e, and in

a very

detailed

way

, and I tried

a little bit

differen

t appro

ach, an

d I th

ink I fig

ured

out fin

ally w

hat w

as w

rong with their original w

ork, which they w

ere not aware of and

I wasn

't initially

either.

If you tak

e the n

um

bers th

at they

obtain

ed o

n th

e whole g

roup

of sam

ples an

d y

ou o

nly

look at th

em u

nder o

ne set o

f measu

re-m

ent conditions, that is, you don't look at all the conditions for the m

om

ent, b

ut ju

st loo

k at o

ne set o

f con

ditio

ns, to

and

beh

old

, it is ex

actly th

e same resu

lt. ' M

r. FIT

HIA

N. T

he same result as w

hat? D

r. GU

INN

. As w

hat I found in my ow

n measurem

ents. M

r. FrrH

IAN

. How

do you mean?

Dr. G

UIN

N. C

E-3

99 m

atches C

E-8

42 in

each o

f the fo

ur sets o

f co

nditio

ns th

at he u

sed, an

d th

e oth

er three sp

ecimen

s match

one

another and are different from the other tw

o every time. B

ut if you lo

ok at all th

e num

bers at o

nce, ev

eryth

ing is v

aryin

ek m

uch

you

don't g

et the p

icture at all. B

ut o

nce y

ou so

rt them

out th

is way

then the sam

e result comes out as w

hat I obtained—a little fuzzier

picture of course, because his detector didn't have the sharp resolu-tion of the m

odern germanium

detector. But, of course, hindsight is

much

better th

an fo

resight. I d

idn't g

et this o

ut o

f his d

ata either

until after I had my ow

n data. In a sense it is confirming.

Mr. F

ITH

IAN

. Are you testifying then, D

r. Guinn, that a m

ore in-dep

th read

ing o

f the 1

964 n

eutro

n activ

ation an

alysis d

ata would

hav

e led eq

ually

trained

; scientists to

the co

nclu

sion th

at there

were in

fact fragm

ents fro

m o

nly

two

bu

llets that w

ere tested?

Dr. G

UIN

N. Y

es; the data were there but they w

ere not interpret-ed as far as they could have been taken.

Mr. F

irsnAN

. Using the charts that you provided the com

mittee.

and they have been previously admitted into evidence, w

ould you

561

just briefly summ

arize for me how

the readings of your equipment

mig

ht b

e more accu

rate, more sp

ecific, than

those o

f the F

BI?

Let m

e see if I can understand this as a layman. A

s I understand th

e pro

cess, what y

ou d

o is y

ou tak

e a particle o

f som

ethin

g an

d

you p

ut it in

som

e kin

d o

f little—

Dr. G

UIN

N. C

ontainer. M

r. FIT

HIA

N [continuing]. C

ontainer. And you put that inside the

nuclear reacto

r and y

ou b

om

bard

it with

trillions o

f neu

trons p

er second?

Dr. G

UIN

N. Y

es, sir. M

r. FrrH

IAN

. And th

en y

ou rem

ove it fro

m th

e reactor, an

d in

so

me tim

e frame th

ereafter, the u

nstab

le atom

ic nuclei th

at hav

e been

created, each

by th

e abso

rptio

n o

f a neu

tron, fro

m th

e extra

neutrons that you have bombarded the sam

ple with, undergo radio-

active decay, with the em

ission of gamm

a rays of characteristic, or identifying energies. A

m I roughly correct?

Dr. G

uiNN

. Yes, each radioactive nucleus that undergoes disinte-

gratio

n, w

hich

it decid

es on its o

wn to

do, sp

ontan

eously

, in th

e typical case em

its a beta particle of some energy (w

hich turns out not to

be v

ery u

seful to

measu

re, for d

etailed reaso

ns), b

ut it also

usually em

its one or sometim

es two or three different gam

ma rays,

gam

ma ray

s of d

ifferent en

ergies. T

hose w

e can m

easure m

uch

m

ore easily

and ex

actly, an

d so

those are th

e ones w

e look fo

r. T

he decay of one nucleus may just give one gam

ma-ray photon.

At b

est it would

giv

e one co

unt o

n th

at counter. S

o w

hat w

e are looking at, of course, are thousands or m

illions of these disintegrat-ing nuclei, and w

e accumulate the results. T

he detector is capable of d

istinguish

ing b

etween

gam

ma ray

s of d

ifferent en

ergies, an

d

they show up in our spectra as peaks.

Whether you are looking for it or not, for exam

ple, if somebody

gave me a sam

ple and I didn't know it had any antim

ony in it, if I activ

ated it an

d lo

oked

at it under eith

er of th

ose co

nditio

ns an

d

saw that peak, at 564 keV

, I would know

that the sample contained

antimony.

Mr. F

rrHIA

N. T

he antimony peak w

ill always com

e at the same

part of the spectrum?

Dr. G

ursrsr. That is right, that is the characteristic; yes.

Mr. F

ITH

IAN

. And, therefore, w

ithout any knowledge of w

hat is in

it, if you see a p

eak in

that fram

e of n

um

bers, it h

as to b

e antim

ony? D

r. Gum

s .. That is right.

Mr.

FrrH

IAN

. A

nd th

en th

e heig

ht o

f the p

eak in

dicates th

e quantity?

Dr. G

UIN

N. It is proportional to it. W

e usually measure the area

of th

e peak

instead

of its height, because the p

eaks aren

't quite

symm

etrical, but otherwise you are right.

Mr. F

ITH

IAN

. You h

ave said

this w

hole p

rocess th

at you g

o

through does not destroy the material, is that correct?

Dr. G

UIN

N. T

hat is correct. M

r. FIT

HIA

N. N

ow, then; did you test exactly the sam

e particles that the F

BI tested in 1964?

Dr. G

UIN

N. W

ell, it turns out I did not, for reasons I don't know.

because as they did the analysis, they did not destroy the samples

either.

Page 38: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

562

Mr. F

ITH

IAN

. So? D

r. G

UIN

N.

The p

articular little p

ieces that th

ey an

alyzed

, I co

uld

just as w

ell hav

e analy

zed o

ver ag

ain, b

ut th

e pieces th

at w

ere brought out from the A

rchives—w

hich reportedly, according to

Mr. G

ear, were th

e on

ly b

ullet-lead

fragm

ents fro

m th

is case still p

resent in

the A

rchiv

es—d

id n

ot in

clud

e any

of th

e specific

little pieces that the FB

I had analyzed. P

resumably those are in existence som

ewhere, I am

sure nobody threw

them out, but w

here they are, I have no idea. M

r. FIT

HIA

N. A

nd the 1964 equipment w

ouldn't have consumed

them either?

Dr. G

uam. N

o. M

r. FIT

HIA

N. W

hat w

as the state o

f the k

now

ledge at th

at time

in term

s of sto

ring

radio

active m

aterials? Wo

uld

there h

ave b

een

any p

rosp

ect that so

meo

ne n

ot ad

equately

info

rmed

, such

as per-

hap

s the F

BI at th

at time o

r law in

forcem

ent p

eople, w

ould

hav

e been

a little leery ab

out k

eepin

g rad

ioactiv

e materials in

their

files? D

r. GU

INN

. I wo

uld

n't th

ink

so. I am

sure b

y th

at time th

ey

knew

enough ab

out th

e safety asp

ects that, co

nsid

ering th

e very

sm

all size of samples w

e are dealing with here, and the very sm

all am

oun

t of rad

ioactiv

ity in

them

, they

wo

uld

hav

e righ

tly co

nsid

-ered them

to be perfectly harmless. A

lso, the little activity in them

soon decayed out. M

r. Frrx

isst. So

, finally

, it is yo

ur co

nclu

sion

that d

espite w

hat

Mr. H

oover said to Mr. R

ankin, the FB

I data are not really incon-clusive, though it appeared to be so to you initially?

Dr. G

UIN

N. T

hat is rig

ht, th

e data really

were fu

nd

amen

tally

better th

an th

ey th

ought, o

r than

I initially

thought.

Mr. F

ITH

IAN

. The reason I raise that issue, D

r. Guinn, is this. A

s I understand the critical literature, it falls into tw

o categories with

regard to this question. Earlier on, the critics said that the W

arren C

omm

ission was afraid to do the neutron activation analysis m

ea-su

remen

ts becau

se if they

did

it, it would

show

som

eting o

ther

than

the sin

gle b

ullet th

eory

and th

ereby w

ould

underm

ine th

e entire W

arren Com

mission findings. T

his charge was m

ade in sev-eral p

laces in th

e literature, an

d I h

ave sev

eral exam

ples h

ere to

that effect, namely, that the reason for their not doing the neutron

activatio

n an

alysis w

ork

at that tim

e was th

e fear sgi th

e part o

f the B

ureau that it would show

someting other than a single bullet

theo

ry, th

at is, the frag

men

ts from

Co

nn

ally's w

rist and

the "p

ris-tin

e" bu

llet sample w

ould

turn

ou

t to b

e two

differen

t bullets.

Dr. G

UIN

N. Y

es. M

r. FIT

HIA

N. In post-1973 literature, after the F

reedom of Infor-

mation A

ct episode to which you refer, the critics have said that it

was done, but w

ith inconclusive results, and since the results were

inconclusive, it did not pi-ove that they were from

the same bullet,

and, therefore, the publication or the publishing of the results were

suppressed

becau

sed it aid

not su

pport th

e single b

ullet th

eory

. T

hat is th

e reason

I raised th

e questio

n sp

ecifically ab

out th

e F

BI d

ata and

abo

ut y

ou

r analy

sis or in

terpretatio

n o

f their d

ata. D

r. G

uiss.

I d

on

t kn

ow

any

thin

g ab

ou

t any

of th

e peo

ples

involved motives but w

hat I do know is that indeed in 1964 the F

BI

did

do

the an

alyses an

d acco

rdin

g to

this letter th

at we ju

st intro

-

563

duced

into

evid

ence, th

ey d

id n

ot ap

pear -to

be ab

le to d

raw an

y

conclusions from the num

bers. L

ooking at them m

any years later, I can see why that w

ould be po

ssibly

the case, b

ut as I say

, with

the ad

van

tage o

f these n

ew

results to

guid

e me in

the rig

ht d

irection o

f how

to statistically

treat th

e data th

ey h

ad g

otten

earlier, lo an

d b

eho

ld, th

ey v

ery

defin

itely d

id ag

ree, with

my m

ore recen

t findin

gs fro

m m

y o

wn

measurem

ents, using more pow

erful equipment.

Mr. F

rraisis. No

w, is th

ere any

evid

ence, in

either th

e FB

I interpretation of the test results of 1964 or in your ow

n interpreta-tion of the tests for this com

mittee, that w

ould support the specula-tion that the "pristine" bullet and the one that hit C

onnally's wrist

are two sep

arate bullets? Is th

ere any ev

iden

ce in eith

er report?

Dr. G

UIN

N. N

o, th

ere is no ev

iden

ce either in

my w

ork

or th

e previous F

BI w

ork of that. You cannot distinguish one specim

en fro

m th

e oth

er, from

the an

alytical resu

lts. Bo

th m

y fin

din

gs an

d

the earlier FB

I findings give this same result.

Mr.

FTT

ITIA

N. G

oin

g fro

m th

is conclu

sion, co

uld

the F

BI h

ave

been able to draw the conclusion of only tw

o bullets being present if so

meo

ne, an

yone th

ere, did

not h

ave th

e kin

d o

f expertise in

W

CC

Mannlicher-C

arcano amm

unition that you have testified or that w

e understand you possess? Would som

eone not familiar w

ith that kind of am

munition—

could they have drawn the right conclu-

sion? D

r. G

UIN

N. It w

ou

ld h

ave b

een certain

ly m

uch

mo

re difficu

lt becau

se, as I say, m

ost k

inds o

f amm

unitio

n, o

ther k

inds th

at we

hav

e loo

ked

at ov

er years, h

ave b

een so

un

iform

that y

ou

can't

tell—y

ou

literally can

no

t tell on

e bu

llet from

ano

ther o

ut o

f the

same box.

WC

C M

annlicher-Carcano bullet lead, how

ever, is different. The

concentration range from bullet-to-bullet is trem

endous. For exam

-ple, o

ut o

f the sam

e box, o

ne b

ullet m

ay o

nly

hav

e 20 p

arts per

millio

n an

timo

ny

, the n

ext o

ne y

ou

take o

ut o

f the b

ox

mig

ht b

e 1,200 parts per m

illion antimony, and each of these values can be

measured quite precisely. A

ctually, when Jack G

allagher did these measurem

ents, he also analyzed a couple of know

n WC

C M

annlicher-Carcano bullets, just

as background samples: O

ne from lot 6,000, one from

lot 6,003, but th

at is all. Th

at is no

t mu

ch o

f a back

gro

un

d to

loo

k at; b

ut su

re en

ou

gh

, tho

se two

, just th

e two

that h

e loo

ked

at were q

uite

different from one another—

one was about 90—

I have the numbers

somew

here here but not handy—one w

as like 90 parts per million

antim

ony an

d th

e oth

er one w

as som

ethin

g lik

e 700 p

arts per

million. S

o ev

en th

e two

samp

les he h

app

end

ed to

pick

as back

gro

un

d

samples im

mediately show

ed the same thing regarding w

hich we

have much m

ore data. M

r. FIT

HIA

N. S

o is it your testimony, then, or is it your estim

ate that the F

BI's failure to correctly interpret the 1964 data, w

hich is so

distu

rbin

g to

so m

any

peo

ple—

wo

uld

the F

BI h

ave h

ad th

e k

no

wled

ge an

d ex

perien

ce in 1

96

4 to

correctly

interp

ret the re-

sults? D

r. Gu

inn

. Well, it is a little h

ard to

say. I th

ink

they

mig

ht

have been able to, but I think it might have been m

ore difficult for

Page 39: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

564

them

to at th

at time sin

ce they

did

n't h

ave an

exten

sive b

ack-

ground in activation analysis or interpretation of such results, and th

ey d

idn

't hav

e any

exp

erience w

ith W

CC

Man

nlich

er-Carcan

o

amm

unitio

n, eith

er. For th

at matter, in

1964

I did

n't h

ave an

y

experience with this kind of bullet lead either.

Mr. F

rrmata. W

e must, I think, M

r. Chairm

an, clarify one thing for the record.

Dr. G

uin

n, is y

ou

r interp

retation

of th

e FB

I data b

ased o

n th

e inform

ation you obtained through the FB

I, as opposed to any secret or otherw

ise restricted data you obtained through this comm

ittee? D

r. GU

INN

. No. Y

ou are only referring to the FB

I data? M

r. FIT

HIA

N. Y

es. D

r. GU

INN

. No; th

e FB

I data th

at I hav

e, copies o

f all the raw

d

ata that Jack

Gallag

her g

ot, w

ere ob

tained

actually

no

t even

by

m

e; they

were o

btain

ed b

y D

r. John N

ichols fro

m th

e FB

I under

the Freedom

of Information A

ct, and then turned over to me; since

Dr. N

ichols is not an activation analyst. He didn't know

what to do

with

such

secialized d

ata—his ex

pertise is in

the field

of fo

rensic

pathology. M

r. FIT

HIA

N. T

herefore any information that has been published

either by him or by you no w

ay falls under any restrictions, is that correct?

Dr. G

UIN

N. N

o, none of this is restricted information.

Mr. F

ITH

IAN

. One final line of questioning, D

r. Guinn, and I w

ill su

bsid

e. Hav

e we d

one, h

ave y

ou d

one—

as far as your ex

pert

knowledge is concerned, have w

e done all the tests that are possi-ble to

ascertain th

e num

er of b

ullets th

at the frag

men

ts came

from? Is there anything else that w

e should do? D

r. GU

INN

. One can alw

ays think of other analytical methods, et

cetera, that might show

up some elem

ents that were not detectable

by activation analysis, or you can even—using activation analysis

go to the destructive forin of the method, but then you destroy the

samples. I am

sure that is not desirable. I w

ould

not reco

mm

end an

y fu

rther an

alytical stu

dies at th

e presen

t time. I th

ink th

at the fin

din

gs th

at we h

ave are p

retty

defin

itive an

d m

ost o

ther th

ing

s that o

ne can

thin

k o

f that y

ou

co

uld

try o

n th

e samples m

ight o

r mig

ht n

ot ad

d so

me ad

ditio

nal

information. It is questionable. A

nd most of those m

ethods that are really

sensitiv

e wou

ld d

estroy

or eith

er the sam

pler o

r alter their

compositions.

Mr.

FIT

HIA

N. A

nd I clo

se with

this q

uestio

n, th

en: S

ince th

ere are n

o frag

men

ts from

Presid

ent K

enned

y o

ther th

an th

e skull

shot, in actual fact, using your scientific methods, you cannot shed

any lig

ht o

n w

heth

er or n

ot th

e bullet th

at passed

thro

ugh G

over-

no

r Co

nn

ally also

passed

thro

ug

h th

e Presid

ent; is th

at a correct

statement?

Dr. G

uirsat. That is correct. T

hese results only show that the C

E

399 "p

ristine" b

ullet, o

r so-called

stretcher b

ullet, m

atches th

e frag

men

ts in h

is wrist. T

hey

giv

e yo

u n

o in

form

ation

wh

atsoev

er ab

out w

heth

er that b

ullet first w

ent th

rough P

residen

t Ken

ned

y's

bo

dy

, since it left n

o track

of frag

men

t's and

, for th

at matter, it

doesn't even say that it went through G

overnor Connally—

through his b

ack, th

at is—becau

se it left no track

of frag

men

ts there. A

t

565

least I hav

e nev

er see or h

eard o

f any reco

vered

lead frag

men

ts from

either of those wounds.

The resu

lts, merely

say th

at the stretch

er bullet m

atches th

e fragm

ents in the wrist, and that indicates indeed that that particu-

lar bullet d

id fractu

re the w

rist. It unfo

rtunately

can't tell y

ou

anything else because there were no other bits and pieces along the

other wounds.

Mr. F

rrmars. T

hen your conclusions are what you just stated as

far as the b

ack en

trance an

d th

roat ex

it wound o

f Presid

ent K

en-

nedy, and as far as the close match of the fragm

ents from C

onnal-ly

's wrist w

ith th

e "pristin

e" bu

llet, and

the o

ther co

nclu

sion

yo

u

referred to today is that the particles taken from P

resident Kenne-

dy's skull matches other fragm

ents that were in the car?

Dr. G

urraN

. That is rig

ht, th

ey m

atch o

ne an

oth

er, but th

ey d

o

not match the C

onnally samples.

Mr. F

ITH

IAN

. And that m

eans there were tw

o bullets? D

r. G

UIN

N. T

here w

ere defin

itely tw

o b

ullets. T

here is n

o ev

i-dence for the presence of three, or m

ore. M

r. F

ITH

IAN

. R

epeatin

g th

en, th

ere is no ev

iden

ce for th

ree bullets. T

hank you, Dr. G

uinn. I have no further questions, M

r. Chairm

an. C

hairman ST

OK

ES. T

he time of the gentlem

an has expired. D

r. Guin

n, I th

ink I ju

st hav

e perh

aps m

aybe o

ne, m

aybe tw

o

questions. Obviously from

your testimony here it is evident, as an

exp

ert in n

eutro

n activ

ation

analy

sis, that w

e are talkin

g ab

ou

t a field in w

hich there are relatively few experts; aren't w

e? D

r. Guitars. I w

ouldn't say so any more. It m

ight have been true m

any years back, but every time w

e have an international confer-ence w

e have something like 500 people there, all supposedly and

most of them

really experts in some phase or another of activation

analy

sis. It has g

row

n to

be a field

where th

ere are pro

bab

ly

altogeth

er a few th

ousan

d p

eople w

ho are k

now

ledgeab

le in th

e field.

Chairm

an STO

KE

S. And if w

e go back to the period of time w

e are talk

ing ab

out, 1

963-6

4, th

at perio

d o

f time, w

hat ty

pe o

f field

would there have been then of experts? D

r. G

UIN

N. S

maller n

um

bers, alth

ough ev

en in

1964 w

e had

alread

y h

ad o

ne in

ternatio

nal co

nferen

ce in th

e field. W

e had

another one the year after that. S

o it was obviously already getting

to b

e of so

me size, b

ut o

bvio

usly

not as m

any p

eople as th

ere are now

. It was still considered to be a relatively new

method by som

e people, at least in 1964, although the m

ethod itself was first origi-

nated in 1937; way back then.

Bu

t it cou

ldn

't beco

me a really

very

usefu

l meth

od

un

til the

nu

clear reactor cam

e alon

g, an

d th

at was d

urin

g W

orld

War II,

and th

en it w

as som

e years b

efore reacto

rs becam

e very

wid

ely

available to people; and so it was not until about 1950, you m

ight say, that at least a few

places had nuclear reactors and the scintil-latio

n d

etector k

ind

of co

un

ting

equ

ipm

ent, an

d th

en th

e field

began to grow at a pretty good clip.

Chairm

an ST

OK

ES. I h

ave n

o fu

rther q

uestio

ns. A

t this tim

e. under the rules of our com

mittee, any w

itness appearing oefore the co

mm

ittee, at the co

nclu

sion o

f his testim

ony, is en

titled to

:; m

inutes. During that 5-m

inute period he may explain, am

plify. or

Page 40: olar. - Harold Weisbergjfk.hood.edu/Collection/Weisberg Subject Index Files/G Disk/Guinn... · Mr. Luzz. I don't believe there is any further expanding on the examinations that we

566

in an

y w

ay ex

pan

d u

pon th

e testimony h

e has g

iven

to o

ur co

mm

it-tee. I w

ou

ld lik

e to ex

tend

to y

ou

such

time at th

is time if y

ou

so

desire. D

r. G

UIN

N.

Th

an

k y

ou

, Mr. C

hairm

an

. I will ju

st mak

e o

ne

com

men

t that I th

ought w

e mig

ht h

ave b

rought o

ut b

efore, b

ut w

e did

n't q

uite g

et around to

it. If any o

f you start lo

okin

g at th

ese detailed

num

bers, th

ere need

s to b

e a little furth

er interp

retation.

First o

f all, so

me o

f the e

lem

ents liste

d in

my re

port, in

our

exp

erience w

ith all k

ind

s of b

ullet lead

s often

sho

w u

p an

d o

ften

do

n't sh

ow

up

, and

they

do

n't seem

to b

e characteristic o

f any

-th

ing. S

om

e of th

em are p

robab

ly th

e result o

f extern

al contam

ina-

tion

. Fo

r the sa

ke o

f co

mp

lete

ness, I h

av

e in

clu

ded

all o

f the

elemen

ts detected

, but I d

on't th

ink th

at som

e of th

em co

ntrib

ute

on

e w

ay

or th

e o

ther to

the c

hara

cte

rizatio

n o

f sou

rce o

f the

specimens.

Also

, when

you lo

ok at th

e antim

ony an

d th

e silver v

alues to

see if th

ese samples m

atch th

ese and th

ese match

these, it sh

ould

be

no

ted

that th

e p

lus o

r min

us th

at is sh

ow

n a

fter e

ach

of th

ose

num

bers is m

erely th

e uncertain

ty o

f each v

alue calcu

lated fro

m

what w

e call the co

untin

g statistics. W

e can calcu

late that.

The o

verall m

easurem

ent u

ncertain

ty o

f that n

um

ber o

n th

at sp

ecific sample is so

mew

hat b

igger th

an th

at, mean

ing th

at if we

took th

at iden

tical little piece an

d d

id th

e same ex

perim

ent o

ver

and o

ver ag

ain w

e would

get ab

out th

e same v

alue, b

ut th

e vari-

atio

n w

ou

ld b

e so

mew

hat m

ore

than

that c

alc

ula

ted

from

the

countin

g statistics—

perh

aps as m

uch

as twice larg

er. It dep

ends o

n

the v

alue.

And th

en, if y

ou are try

ing to

match

this p

iece and th

is piece—

which

really b

oth

came fro

m th

e same b

ullet b

ut y

ou d

on't k

now

it an

d y

ou

are

tryin

g to

pro

ve it—

yo

u h

av

e to

tak

e in

to a

cco

un

t an

oth

er factor—

ho

w h

om

og

eneo

us is th

at bu

llet? Is every

piece

that y

ou tak

e from

a bullet th

e same? A

nd th

e answ

er is: No; th

ey

are no

t. Th

e ind

ivid

ual b

ullets are fairly

ho

mo

gen

eou

s, bu

t there

are significan

t variatio

ns w

ithin

them

. W

e hav

e a great d

eal of b

ackgro

un

d d

ata, specifically

on

WC

C

Man

nlich

er-Carcan

o b

ullet lead

, that isn

't in th

e report, b

ut w

e use

that as th

e back

up w

hich

show

s that th

e variatio

n w

ithin

a bullet

is sign

ificant.

So

wh

en y

ou

start to co

mp

are nu

mb

ers, it turn

s ou

t, for ex

amp

le, o

n th

e antim

on

y n

um

bers, ro

ug

hly

speak

ing

, if yo

u rak

e the p

lus

or m

inu

s that is sh

ow

n an

d m

ultip

ly it b

y ab

ou

t 6, th

at will tak

e care o

f all of th

ose v

ariabilities w

ithin

the sam

ple, as w

ell as the

small m

easurem

ent u

ncertain

ties. T

he v

ariation w

ithin

that in

div

idual b

ullet is th

en tak

en in

to

account, an

d th

en y

ou fin

d o

ut th

at two sam

ples in

deed

match

one

anoth

er as closely

as could

be ex

pected

. For ex

ample, th

e CE

-399

samp

le gav

e a measu

red v

alue o

f 83

3 p

arts per m

illion

antim

on

y,

whereas th

e CE

-842 sam

ple sh

ow

ed 7

97. W

ell, any g

ramm

ar school

bo

y w

ill tell yo

u 7

97

is no

t the sam

e as 83

3. B

ut w

hen

yo

u co

nsid

er th

at the 8

33

is plu

s or m

inu

s abo

ut 5

0 an

d th

e 79

7 is p

lus o

r min

us

abo

ut 5

0, th

en y

ou

see that y

ou

can't d

isting

uish

on

e from

the

oth

er. T

hey a

re in

distin

guish

able

. but. b

y th

e sa

me to

ken, th

e

oth

er samp

les wh

ich are o

nly

abo

ut ro

ug

hly

62

0 p

lus o

r min

us a

smaller am

ount. in

that case ab

out 2

0 o

r 30—

they

very

clearly n

ot

567

on

ly m

atch o

ne an

oth

er, bu

t they

also w

idely

differ fro

m th

is 80

0

figure.

But so

me o

f that is ex

plain

ed in

the tex

t of th

e report. Y

ou can

't ju

st take th

e nu

mb

ers from

the tab

le and

blin

dly

go

ahead

; yo

u

hav

e to read

the fin

e prin

t as well to

see that ev

eryth

ing is p

roper-

ly tak

en in

to acco

un

t. In

any

even

t, tho

ug

h, I th

ink

the resu

lts hav

e com

e ou

t in a

fairly clean

-cut fash

ion. W

e did

n't p

redict an

y p

articular w

ay th

ey

wo

uld

com

e ou

t; they

just fell o

ut th

is way

. An

d, as I say

it led m

e to

reexam

ine th

e FB

I data m

ore carefu

lly th

an I h

ad d

on

e earlier. I fran

kly

was v

ery su

rprised

to see th

at even

their d

ata, som

ewhat

fuzzier, et cetera, still fell rig

ht in

to th

e same p

icture.

So

I thin

k th

e con

clusio

ns are w

ell establish

ed. A

lso, as I h

ave

stated earlier, fo

rtunately

by u

sing th

is meth

od o

ne d

oes n

ot d

e-stro

y th

e samples. T

he id

entical sam

ples are still th

ere. They

weig

h

the sam

e; they

can b

e analy

zed all o

ver ag

ain. A

ll of th

e radio

activ-

ity th

at we in

duced

in th

em a y

ear ago h

as long d

ecayed

out, so

th

ey co

uld

readily

be an

alyzed

ov

er again

, if desired

. O

ther th

an th

at, I just w

ant to

say it h

as been

a real pleasu

re w

ork

ing

with

the co

mm

ittee and

with

the staff o

f the co

mm

ittee, an

d I th

ank

yo

u v

ery m

uch

for in

vitin

g m

e here.

Chairm

an ST

OK

ES. I g

uess y

ou

raised o

ne ad

ditio

nal q

uestio

n in

m

y m

ind. A

ssum

ing th

at your d

ata were p

resented

to an

oth

er ex

pert in

your field

, can w

e assum

e with

a reasonab

le deg

ree of

certainty

that th

e exp

ert will co

me to

the sam

e con

clusio

ns th

at you h

ave?

Dr. G

uiro

r. I believ

e so; y

es. As I say

, if you ju

st han

ded

him

the

table o

f measu

red v

alues, h

e initially

mig

ht in

terpret th

e plu

s and

min

uses as m

eanin

g th

e total u

ncertain

ty; an

d, o

f cou

rse, then

he

would

say: W

ell, 79, is n

ot th

e same as 8

33. H

ow

ever, in

the tex

t of

the rep

ort, it is p

oin

ted o

ut th

at the tab

le plu

s-min

us v

alues d

o n

ot

represen

t the to

tal uncertain

ty o

f a sample; it is larg

er than

that.

If he to

ok

that in

to acco

un

t, he w

ou

ld reach

the sam

e con

clusio

ns;

yes. C

hairm

an ST

OK

ES. T

he Chair recognizes counsel Jim

Wolf.

Mr.

WO

LF

. M

r. Chairm

an, fo

r the reco

rd, I w

ould

like to

note

that D

r. Gu

inn

's repo

rt has b

een su

bm

itted to

an in

dep

end

ent

con

sultan

t for rev

iew an

d ev

aluatio

n an

d h

e com

pletely

agreed

w

ith th

e results ach

ieved

and

repo

rted b

y D

r. Gu

inn

. C

hairm

an

STO

KE

S. D

r. Guin

n, o

n b

ehalf o

f our co

mm

ittee, we

than

k y

ou

very

mu

ch. Y

ou

hav

e mad

e a very

valu

able co

ntrib

utio

n

here

today a

nd w

e c

erta

inly

appre

cia

te a

ll the tim

e y

ou h

ave

exp

end

ed o

n o

ur b

ehalf. T

han

k y

ou

. D

r. GU

INN

. Thank you.

Ch

airman

ST

OK

ES.

Th

ere bein

g n

o fu

rther b

usin

ess to co

me

befo

re the co

mm

ittee today

, this co

mm

ittee meetin

g is ad

journ

ed

un

til 9 a.m

. Mo

nd

ay m

orn

ing

. [W

hereu

pon, at 5

:10 p

.m. th

e com

mittee,ad

journ

ed, to

reconven

e at 9 a.m

. Monday, S

eptember 11, 1978.]