number of cleavage steps

Upload: priyavrat-sathe

Post on 30-May-2018

227 views

Category:

Documents


0 download

TRANSCRIPT

  • 8/9/2019 Number of Cleavage Steps

    1/26

    2 Mechanisms of fracture and crackgrowth

    number of cleavage steps, which may join and form a river pattern. The

    convergence of r iver patterns is a lways downstream; this gives a

    possibility to determine the direction of local crack propagation in a

    micrograph. Examples of cleavage steps and river patterns, as observed by

    electron fractography. arc presented in figure 2.10. They arc places where

    small scale plastic deformation is likely to occur. Plastic deformation

    requires energy, and therefore river patterns and steps are observed more

    abundantly on cleavage fractures produced at temperatures close to the

    transition temperature.

    A cleavage tongue is another typical feature of a cleavage fracture. It is

    called a tongue because of its apparent shape. Cleavage longues of various

    sizes are shown in figure 2.11. They are believed [23, 27] to be formed by

    local fracture along a twin-matrix interface, (Twins are formed as a result

    of the high rates of deformation in front of the advancing crack). Tongues

    in iron are thought to be generated when a cleavage crack, growing along a

    (100) plane, intersects a (112) twin interface and propagates along the

    interface for some distance, while (100) cleavage continues around (he

    twin Final separation occurs when the twin fractures in an unidentified

    manner.

    Lvidence for this formation process can be obtained from slcreograpliie

    measurements It turns out that different ways of interaction with twins are

    possible [51. One of these possibilities will now be illustrated. A section

    along a (110) matrix plane through a twin in a bee lattice is shown in figure

    2,12. The composition plane of a twin in this lattice is the (112) plane.

    This plane is perpendicular to (llO), i.e. perpendicular to the plain: of the paper, and it intersects (M0) along the [111] direction. The crack is

    assumed to propagate along (001)[ 110] from A to B. where it impinges on

    the twin. Then it continues along (he matrix-twin interface (112)| 111 ]

    from B to C. Simultaneously, (he main crack may circumvent the (win

    1

    K

    36

    2.2 Cleava e fracture

    Figure 2.11. ("lea \ agelongues (arrows)

    * [no]Figure 2.12. Formation of cleavage tongue (BCD) due to

    passage of twin. Cul along (110) plane through a coherent twinin bec lattice

  • 8/9/2019 Number of Cleavage Steps

    2/26

    ^Mechanisms of fracture and crack growth

    a,t ^rie bones seem lo support this point of view.

    1Jnder normal circumstances face-centcred-cubic (fee) crystal structures cJo not

    exhibit cleavage fractures: extensive plastic deformation will always cid^ v i r in

    these materials before the cleavage stress is reached. Cleavage does occur in body-

    centered-cubic (bec) and many hexagonal-close-packed hc=p>) structures. It occurs

    particularly in iron and low carbon steel (bec). I i i ngstcn, molybdenum, chromium

    (all bec) and zinc, beryllium and magnesium (all hep) are materials capable of

    cleaving.

    2.3 Ductile fracture

    Fracture occurring under the single application of a continuously in-creasing load

    can either be brit t le c leavage fracture or fracture associated wi t-H plastic

    deformation, wich is essentially ductile. For the latter the amount of plastic

    deformation required to produce fracture may be so lirrited in certain cases, that

    relatively l i tt le energy is consumed. Then the fructure is s t il l brit t le in an

    engineering sense and can be initiated at a shiirp notch or crack at a comparatively

    low nominal s tress, particularly w lien a state of plane strain reduces the

    possibilities for plastic deformation.

    The most familiar type of ductile fracture is by overload in tension, w l- ich produces

    the classic cup and cone fracture. After the maximum load hiis been reached the

    plastic elongation of a prismatic-tensile coupon becomes inhomogeneousand

    concentrates in a small portion of the specimen such that necking occurs. In extremely

    pure metals, which are virtually fre e of second phase particles, it is possible for plastic

    deformation on c "jugate slip planes to continue until the specimen has necked down

    to an arrow point by 100 per cent reduction of area (figure 2.14). Such a fiiilure is a

    geometric consequence of the slip deformations. As an example, figure 2.15 shows a

    single crystal that has almost failed by shear on a single slip plane.

    Engineering materials a lways contain large amounts of second phase

    particles. Three types of particles can be distinguished:

    a. Large particles, visible under the optical microscope. Their size may vary

    from 120 um. They usually consist of complicated compounds of trie various

    alloying elements. The alloying elements may be added to mprove castability or

    some other property. The particles are not essential to the strength of the

    material and generally serve no purpose at all

    2

    7

  • 8/9/2019 Number of Cleavage Steps

    3/26

    2 Mechanisms of fracture and crackgrowth

    Somelimcs. however, particles of this size may be produced on purpose, as

    in the case of carbides in certain steels.

    b. Intermediate particles, only visible by means of the electron micro-

    scope. Their size is in the order of 500-5000 Angstrom units. These

    particles may also consist of complex compounds of the various alloying

    i

    n

    el

    em

    ent

    s.S

    o

    m

    et

    i

    m

    es

    p

    ar

    ti

    clesof

    this

    siz

    e

    ar

    e

    es

    se

    nt

    ia

    l

    fo

    r

    the

    pro

    per

    I

    ie

    i

    of

    th

    e

    m

    at

    er

    ia

    l,as

    in the case o f d ispe rs ionmetals (such -is AI-AI2Oj or N

    the case of steels were carbi

    are intentionally developed.

    c

    4

    2.3 Ductile /nature

    figure 2.14. Failure by pure sliciir deformation

    (slip) in pure mclal

    Figure 2.16. Cracking of large particles in AI-Cu-Mg-alloy. A. 3per cent strain: B. (> pel I oil slrain; C. 14 per cent strain: I). 25

    per cent strain. Note development of crack between NOP.Straining direction vertical

    Figure 2 I 5. Sheared single crystals of pure

    copper (courtesy Weiner)

  • 8/9/2019 Number of Cleavage Steps

    4/26

    2 Mechanisms of fracture and crackgrowth

    The large particles are often very brittle and therefore they cannot

    accommodate the plastic deformation of the surrounding matrix. As a result

    they fail early on. when the matrix has undergone only a small amount of

    plastic deformation. This means that voids are formed. The initiation of

    voids at large particles can be observed with an optical microscope [16.

    29], Various stages in this process are shown in f igure 2 .16. When

    comparing the distance between two particular inclusions in the various

    stages, one obtains an impression of the increasing strain.

    The figure indicates that voids are already initiated by large particles at

    small strains in the order of a few per cent, whereas final fracture look

    place al s trains in the order of 25 per cent. This being so. the large

    inclusions visible in the optical microscope cannot be essential to the

    fracture process, although the) will decrease the ductility of the material.When fractured they cause a stress concentration giving a local increase of

    the strain, which could ill the absence of the particles be obtained as an

    overall strain throughout the material. This implies that the large inclusions

    can determine the instant and location of ductile fracture, but they do not

    play a role m the process of ductile fracture itself

    fracture is finally induced by the much smaller intermediate particles of

    the sub-micron size [4. 16. 29]. Since these particles cannot deform as

    easily as the matrix, they lose coherence with the matrix when extensive

    plastic How takes place in their vicinity. In this way tiny voids arc formed,

    which grow by slip: the material between the voids necks down to the lull

    100 per cent in the same way as in figure 2.14. This necking takes place al

    a micro-scale and the resulting tolal elongation remains small.

    The mechanism of initiation, growth and coalescence of micro-voids

    gives rise to characteristic fraclographic features. When observed in the

    electron microscope the fracture surface consists of small dimples which

    represent the coalesced voids (fig. 2.17). In most of the dimples the smallparticle that initiated the void can easily be recognized.

    Dimples always have an irregular shape, due to the random occurrence of

    voids. However, dimples can be roughly divided into two categories

    according to their apparent shape, namely equiaxed and parabolic. The

    shape m which they appear in the microscope depends upon the stress

    systems that were active during their formation [9. 10], and upon the angle

    of observation in the microscope [4, 30]. Equiaxed dimples may be formed

    if the stresses arc predominantly tensile (figure 2.18a). and elongated

    dimples occur in the shear or tear mode (figure 2.18b, c). Both dimj types

    arc present in figure 2.19.

    Putlick [31], Roberts [32] and Crussard et al. [33] were among the ft to

    consider inclusions or intermelallic particles as the initiation sites the

    voids. Various models have been established for void growth a coalescence,

    but so far none is fully compatible with the observations tl can be made

    from ductile fracture surfaces, although some models m apply in certain

    cases [4, 16, 29, 34].

    An impression of the process of void growth and coalescence can

    obtained from the study of dimple profiles. Cross sections of replicas g a

    good idea of the topography of the fracture surfaces [4, 16, 29]. This

    il lustrated in f igure 2 .20 which gives an example obtained al hi

    magnification. The cut will not always be through the center of a dimj but

    the apparent average depth-to-width ratio in the cross sections v be

    approximately the same as the actual depth-to-width ratio of the dimp

    441

    2.3 Ductile fracture

    Figure 2.17. Dimples initialed at intermediate size

    particles (arrows). Al-alloy

  • 8/9/2019 Number of Cleavage Steps

    5/26

    2 Mechanisms oj fracture and crack growth!I M1111........................................................................................ F11! i n i ' 11 ip 11'i F11111 ir 11 Mr 11 r 11' 1! 11 n fpi r 11 p > i ' i r' i r i i r I r' r l r r r ' r r i r iT ' i r i r i r ' i r r i r 11 r i r 11 n I r ir: i nr r l r! I r 11 Mr 11 pi r Mr i; Mi [; r 11 [ 111 i r 11 r 11 M111 r i' 11 [ 11........IIIMIIIIIIIIIIIMIMIIIMIIIIIIMIIIIIIII...............................................................

    2.J Ductile fracturespecimen and stresscondition

    t t t t

    M i l

    UUUt

    .

    i t i__________________

    fracture surfaces

    eguiaxed dimples

    ___ - ^

    ^opposite direction

    shear dimples

    l same direction

    tear dimples

    1 I *

    igurc 2. IK. Occurrence of different types of dimples

    [16]. Thus it can be asserted from figure 2.20 that the depth-to-width ratio

    is low and that dimples are relatively shallow holes. The latter is confirmed

    by stereoscopic measurements of dimple topography. Apparently, voids

    grow mainly in lateral directions, causing them to remain shallow. In oxide-

    dispersion strengthened materials the initiation and growth of voids at the

    dispersed particles can be made visible when a thin foil is subjected to a

    tensile deformation while under observation in the electron microscope [35.

    36, 37]. In normal structural materials voids at the intermediate particles

    can seldom be observed. In a study of 13 different aluminium alloys Broek

    5 44

    figure 2.19. Equia\cd dimples at A. parabolic dimples al 1! 1urge cleaned panicle (ol l\po sliov.il in figure 2.16) al I). 2024-

    T.1 Al-alloy

    http://sliov.il/http://sliov.il/
  • 8/9/2019 Number of Cleavage Steps

    6/26

    2 Mechanisms oj fracture and crack growth

    [4, 16. 29] showed the occurrence of voids at the intermediate particles:

    slender particles have a tendency to fracture (figure 2.21) while particles of

    other shapes lose coherence with the matrix (figure 2.22). However, in

    general only very few voids were found.

    Apparently, the cohesive forces between the matrix and particles are

    extremely large in conventional materials. They are so large that void

    6 44

  • 8/9/2019 Number of Cleavage Steps

    7/26

    I-mure 2.21). Cross section throughreplica of dimples

    2 Mechanisms of fracture and crack growth

    |

    |

    7

    5

    2.3 Ductile fracture

    Figure 2.21. Crackedparticles in AI-allo\

  • 8/9/2019 Number of Cleavage Steps

    8/26

    2 Mechanisms of fracture and crack growth

    Initiatio

    n does

    not take

    place

    until

    very late

    in the

    fracture

    process.

    The luck

    of many observable voids leads to the assumption that immediate

    coalescence must take place at the moment that voids are formed in some

    quantity. This implies that voids can only be initiated at such high stresses HI

    strains that the conditions for coalescence are already fulfilled. This requires

    a model for void initiation which predicts immediate and spontaneous

    void.growth. (Where void growth in oxide-dispersion strength-i tud

    materials was reported, it occurred in the direction of the tensile stress.

    This mode ofvoid growth is a normal consequence of longitudinal Straining,

    which would also occur under elastic conditions). From a physical point of

    view, one would expect a cavity to spread preferentially in a direction

    perpendicular to the tensile stress, as in the ease of a crack This lateral void

    growth is confirmed by the shallowness of the dimples A model that is

    reasonably compatible with the observed facts is the following[16, 29].

    During plastic deformation dislocation pile-ups will form at the particles.

    These piled-up loops are depicted in figure 2.23a, TllC loops arc repelled by

    the particle through the action of their image forces On the other hand, the

    leading loop will be pushed towards the parlicl< by stresses set up by the

    pile-up and the applied shear stress. When one or a couple of loops are

    pushed to the interface a dccohcsion ol ilu

    4S

    8

    5

    2.3 Ductile fracture

  • 8/9/2019 Number of Cleavage Steps

    9/26

    interface will ultimately lake place. If this occurs, a void is formed. The

    consequence is that the repelling forces on subsequent loops are drastically

    reduced "and the greater part of the pile-up can empty itself into the newly

    formed void. The dislocation sources behind the loops, which became

    inactive because of the constraint of the pile-up ahead, can resume action

    and hence the process may lead to unstable lateral void growth and

    coalescence as soon as the voids have been initiated (figure 2.23c, d). In

    figure 2.24 the model is shown in terms of displacements.

    Contrary to cleavage, where the action of a tensile stress is sufficient for

    the separation, ductile fracture cannot occur without plastic deformation.

    The mechanism of final separation is a direct consequence of dislocation

    movements and slip displacements necessary for the growth and

    coalescence of voids. Apart from a stress to induce dislocation movement a

    certain plastic strain is required for ductile separation to occur. This plastic

    deformation may be confined to a small volume of material through which

    the fracture passes. Then failure occurs with relatively little plastic-

    deformation on a macroscale. requiring only little energy. The fracture is

    brittle in an engineering sense. Fractures induced by cracks in high

    strength materials are usually of this type.

    2.4 Fatigue cracking

    Under the action of cyclic loads cracks can be initiated as a result of cyclic

    plastic deformation [38, 39]. Even if the nominal stresses are well below the

    elastic limit, locally the stresses may be above yield due to stress

    concentrations at inclusions or mechanical notches. Consequently, plastic

    deformation occurs locally on a microscale, but it is insufficient to show in

    engineering terms.

    9

    l l l i l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l l i .. .

    I igiire 2 2: IHxvIksion of particles 111 MK>I-\l-llo>. Tophull and lioltom half show live same localion. taken al ilillcrenl

    angles of llic election beam [2')\(courtesy I'ergamim)

    Figure 2.23. Dislocation model for void initiation andgrowth a. Piled up loops; b. Cross section; c. Detail;

    d. Cavity (courtesy Pergamon)

    2 Mechanisms of fracture anil crackgrowth

  • 8/9/2019 Number of Cleavage Steps

    10/26

    2 Mechanisms of fracture and crack growth

    Several equivalent m ode ls have been p roposed [38, 40, 41] to expla in

    the initiation of fatigue cracks by local plastic deformation. The model of

    _ Wood [38] is depic ted in f igure 2 .25 . D ur ing the r ising- load par t of the

    cycle, slip occurs on a favourably oriented slip plane. In the falling-load

    I part, slip takes place in the reverse direction on a parallel slip plane,

    since slip on the first plane is inhibited by strain hardening and by

    * ox ida tion of the newly c rea ted f ree su r face. This f ir s t cyc lic s lip can g ive

    rise to an extrusion or an intrusion in the metal surface. An intrusion can

    grow into a crack by continuing plastic flow during subsequent cycles

    (figure 2.25). If the fatigue loading is cyclic tension-tension this

    mechanism can still work since the plastic deformation occurring at

    increasing load

    'will give rise to residual compressive stresses during load release An

    example of fatigue cracking initiated by cyclic slip [42] is presented in

    figure 2.26.

    49

    10.4 Fati ue

    crackin

    Figure 2.24. Voidcoalescence by slip

    Figure 2.25. Wood's model forfatigue crack initiation

  • 8/9/2019 Number of Cleavage Steps

    11/26

    2 Mechanisms of fracture and crack growth

    A fatigue crack, once started, can also grow by a mechanism of reversed

    49

    11.4 Fati ue

    crackin

  • 8/9/2019 Number of Cleavage Steps

    12/26

    2 Mechanisms of fracture and crack growthI........IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIM

    52 51

    2.4 Fati ue crackin

    Figure 2.27. Possible model for

    Figure 2.28. Striations on fatigue cracksurface of Al-C'u-Mg alloy

    opening

    opening

    closing

  • 8/9/2019 Number of Cleavage Steps

    13/26

    2 Mechanisms of fracture and crack growthslip [43-52], Spveral stages of fatigue crack growth are shown in figure

    2.27. A sharp crack in a tension field causes a large stress concentration at

    its tip where slip can occur fairly easily. The material above the crack

    (stages I and 2 in figure 2.27) may slip along a favourable slip plane in the

    direction of maximum shear stress. Due to that slip the crack opens, but it

    also extends in length. Slip can now occur on another plane (stage 3).

    Work hardening and increasing stress will finally activate other parallel

    slip planes, which leads to a blunt crack tip (stage 4). During the rising

    loadpart of the cycle the crack has propagated by an amount Aa.

    Plastic deformation has occurred in a small region embedded in elastic

    surroundings. During load release the elastic surroundings will contract

    and the plastically deformed region, which has become loo l arge, does noi

    fit any more in its surroundings. In order to make it fit the elastic material

    will exert compressive stresses on the plastic region during the decreasing

    load part of the cycle. These compressive stresses will be above yield

    again, at least at the crack tip. This means that reversed plastic

    deformation occurs, which will close and resharpen the crack lip, as is

    shown in stage 5 of figure 2.27.

    The cyclic opening and closing of the crack (stages 1-5 and 6-7) will

    develop a typical pattern of ripples, every new cycle adding a new ripple

    52 51

    2.4 Fati ue crackin

  • 8/9/2019 Number of Cleavage Steps

    14/26

    2 Mechanisms of fracture and crackgrowth

    These ripples show up on the fracture surface in the electron microscope;

    they arc called fatigue slrialions. Figure 2.28 shows fatigue striations hra

    commercial Al -Cu-Mg alloy. The model of striation formation given in

    figure 2.27 is a general representation of crack blunting and resharpening. It

    is a synthesis of the various models proposed in the literature [46 52]. kind

    it may give an appreciation of the mechanism of fatigue crack growth,

    lufficient as a background for the study of fracture mechanics principles. A

    more detailed model allowing a limited quantitative analysis has been put

    forward recently by Neumann [52]. A mechanism of cleavage ma\

    KOllKlimes be involved in fatigue crack propagation. This gives way to the

    lo'i-iiiation of brittle striations [44. 45] as opposed to the ductile striations

    dim ussed above.

    Striations represent the successive positions of the crack front during

    i i .uk propagation. This can be deduced from figure 2.29, showing an clcFurther, although phenomenologically sound, the

    energy approach has an intangible. Quality that makes it hard to visualize. For these and other

    reasons, the focus of attention in the theory of fracture mechanics in the 1960s was on the stress

    field approach to LEFM. From this viewpoint, the theory of fracture is treated as a subset of the

    engineering discipline of solid mechanics. In particular, fracture mechanics is a study of the

    mechanics of deformable bodies containing crack-like singularities. In order to develop the concept

    of fracture mechanics from this perspective, it is first necessary to master a working knowledge of

    linear elasticity. Accordingly, in the next few chapters, we will first treat those aspects of solid

    mechanics necessary to develop a theory of fracture based on the stress analysis approach and then

    go on to formulate a suitable theory and study its consequences.

    REFERENCES

    ASTM, 1960, "Fracture Testing of High-Strength Sheet Materials (A Report of a Special ASTM

    Committee),"ASTM Bulletin, No. 243, January 1960, pp. 29^0, and No. 244, February 1960,

    pp. 18-28.