n/a matrix : derivative certificate of analysis sample size
TRANSCRIPT
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
David GreeneLab Director
State License # 19-05-02PISO Accreditation #
17025:2017___________________Signature
12/31/2019
___________________Signed On
673 N. Bardstown Rd
Kaycha Labs1500mg/30ml Full Spectrum CBD Tincture Oil
N/AMatrix : Derivative
Certificateof Analysis
SAMPLE:MO91223002-001Harvest/Lot ID: BB12181902-01
Seed to Sale #N/ABatch#: BB12181902-01
Sample Size: 30 mlOrdered : 12/20/19Sampled : 12/20/19
Completed: 12/31/19 Expires: 12/31/20Sampling Method: SOP Client Method
Dec 31, 2019 | BluegrassBest CBD15410 Beckley Crossing LouisvilleKY, USA 40205
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.188%Total CBD
4.332%Total Cannabinoids
0.000%0.188 % ND 4.332 % ND ND ND 0.028 % 0.022 % 0.144 % ND ND
1.880mg/g ND
43.320mg/g ND ND ND
0.280mg/g
0.220mg/g
1.440mg/g ND ND
D9-THC THCA CBD CBDA D8-THC THCV CBN CBDV CBC CBG CBGA
Cannabinoid Profile TestAnalyst Weight Sample Prep : Extracted By :19 2.9885g NA NA
Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -MO000046POT
Reagent Dilution Consums. ID
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method:SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1mg/L).
Filth PASSED
Analyte Weight Sample Prep : Extracted By :9 1g NA NA
Analysis Method -SOP.T.40.013Analytical Batch -MO000047FIL
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
David GreeneLab Director
State License # 19-05-02PISO Accreditation #
17025:2017___________________Signature
12/31/2019
___________________Signed On
673 N. Bardstown Rd
Kaycha Labs1500mg/30ml Full Spectrum CBD Tincture Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Bluegrass Best CBD
15410 Beckley Crossing LouisvilleKY, USA 40205Telephone: 502-418-1821Email: [email protected]
Sample : MO91223002-001Harvest/LOT ID: BB12181902-01
Batch# :BB12181902-01Sample Size : 30mlOrdered : 12/20/19
Sampled : 12/20/19Completed : 12/31/19 Expires : 12/31/20Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSED
Pesticides LOQ Action Level Units ResultDAMINOZIDE 0.020 ppm NDACEPHATE 0.010 ppm NDFLONICAMID 0.010 ppm NDOXAMYL 0.010 ppm NDMETHOMYL 0.010 ppm NDTHIAMETHOXAM 0.010 ppm NDIMIDACLOPRID 0.010 ppm NDDIMETHOATE 0.010 ppm NDACETAMIPRID 0.010 ppm NDTHIACLOPRID 0.010 ppm NDALDICARB 0.020 ppm NDDICHLORVOS 0.050 ppm NDPROPOXUR 0.010 ppm NDCARBOFURAN 0.010 ppm NDCARBARYL 0.010 ppm NDIMAZALIL 0.010 ppm NDMETALAXYL 0.010 ppm NDCHLORANTRANILIPROLE 0.010 ppm NDPHOSMET 0.010 ppm NDSPIROXAMINE 0.010 ppm NDMETHIOCARB 0.010 ppm NDAZOXYSTROBIN 0.010 ppm NDPACLOBUTRAZOL 0.010 ppm NDMALATHION 0.010 ppm NDMYCLOBUTANIL 0.010 ppm NDBIFENAZATE 0.010 ppm NDSPIROTETRAMAT 0.020 ppm NDETHOPROPHOS 0.010 ppm NDFENOXYCARB 0.010 ppm NDKRESOXIM-METHYL 0.010 ppm NDTEBUCONAZOLE 0.010 ppm NDDIAZANON 0.010 ppm NDPROPICONAZOLE 0.010 ppm NDCLOFENTEZINE 0.010 ppm NDSPINOSAD (SPINOSYN A) 0.010 ppm NDPRALLETHRIN 0.050 ppm NDTRIFLOXYSTROBIN 0.010 ppm NDPIPERONYL BUTOXIDE 0.010 ppm NDCHLORPYRIFOS 0.010 ppm ND
Pesticides LOQ Action Level Units ResultHEXYTHIAZOX 0.010 ppm NDETOXAZOLE 0.010 ppm NDSPIROMESIFEN 0.010 ppm NDFENPYROXIMATE 0.010 ppm NDPYRIDABEN 0.010 ppm NDABAMECTIN B1A 0.020 ppm NDETOFENPROX 0.010 ppm NDBIFENTHRIN 0.010 ppm NDFLUDIOXONIL 0.010 ppm NDFIPRONIL 0.020 ppm NDCYPERMETHRIN 0.020 ppm NDMEVINPHOS 0.010 ppm NDDIMETHOMORPH 0.005 ppm NDFENHEXAMID 0.005 ppm NDCOUMAPHOS 0.005 ppm NDSPINOSAD (SPINOSYN D) 0.010 ppm ND
Pesticides PASSED
Analyst Weight Sample Prep : Extracted By :1 1.0050g NA NA
Analysis Method -SOP.T.30.060, SOP.T.40.060Analytical Batch - MO000050PES
Reagent Dilution Consums. ID
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 57 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.060 Procedure for Pesticide Quantification Using LCMS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
David GreeneLab Director
State License # 19-05-02PISO Accreditation #
17025:2017___________________Signature
12/31/2019
___________________Signed On
673 N. Bardstown Rd
Kaycha Labs1500mg/30ml Full Spectrum CBD Tincture Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Bluegrass Best CBD
15410 Beckley Crossing LouisvilleKY, USA 40205Telephone: 502-418-1821Email: [email protected]
Sample : MO91223002-001Harvest/LOT ID: BB12181902-01
Batch# :BB12181902-01Sample Size : 30mlOrdered : 12/20/19
Sampled : 12/20/19Completed : 12/31/19 Expires : 12/31/20Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
SOLVENT ACTION LEVEL(PPM)
PASS/FAIL RESULT
TRICHLOROETHENE PASS ND
CHLOROFORM PASS ND
1,2-DICHLOROETHENE PASS ND
1,1-DICHLOROETHENE PASS ND
PENTANES PASS ND
BUTANES (N-BUTANE) PASS ND
ACETONITRILE PASS ND
BENZENE PASS ND
ACETONE PASS ND
2-PROPANOL PASS ND
HEXANES PASS ND
XYLENES PASS ND
TOLUENE PASS ND
PROPANE PASS ND
METHANOL PASS ND
XYLENES-P (1,4-DIMETHYLBENZENE) PASS ND
HEPTANE PASS ND
XYLENES-M (1,3-DIMETHYLBENZENE) PASS ND
ETHYLENE OXIDE PASS ND
XYLENES-O (1,2-DIMETHYLBENZENE) PASS ND
ETHYL ETHER PASS ND
ETHYL ACETATE PASS ND
DICHLOROMETHANE PASS ND
ETHANOL PASS ND
Residual Solvents PASSED
Analyst Weight Sample Prep : Extracted By :NA NA NA NA
Analysis Method -SOP.T.40.032Analytical Batch -
Reagent Dilution Consums. ID
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 33 Residual solvents.(Method: SOP.T.30.042 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
David GreeneLab Director
State License # 19-05-02PISO Accreditation #
17025:2017___________________Signature
12/31/2019
___________________Signed On
673 N. Bardstown Rd
Kaycha Labs1500mg/30ml Full Spectrum CBD Tincture Oil
N/AMatrix : Derivative
Certificate of Analysis PASSED
Bluegrass Best CBD
15410 Beckley Crossing LouisvilleKY, USA 40205Telephone: 502-418-1821Email: [email protected]
Sample : MO91223002-001Harvest/LOT ID: BB12181902-01
Batch# :BB12181902-01Sample Size : 30mlOrdered : 12/20/19
Sampled : 12/20/19Completed : 12/31/19 Expires : 12/31/20Sample Method : SOP Client Method
Page 4 of 4
Mycotoxins PASSED
Analyte Result Action Level (PPM)AFLATOXIN G2 NDAFLATOXIN G1 NDAFLATOXIN B2 NDAFLATOXIN B1 NDOCHRATOXIN A+ ND
Analysis Method -SOP.T.30.060, SOP.T.40.060Analytical Batch -MO000045
Analyst Weight Sample Prep : Extracted By :1 1.0050g NA NA
Microbials PASSED
Analyte ResultASPERGILLUS_TERREUS_1J2 not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.TOTAL_YEAST_AND_MOLD not present in 1 gram.
Analysis Method -SOP.T.40.043Analytical Batch -MO000048MIC
Analyst Weight Sample Prep : Extracted By :10 1.0401g NA NA
Heavy Metals PASSED
Reagent Dilution Consums. ID
Metal Result Action Level (PPM)
ARSENIC NDCADMIUM NDLEAD NDMERCURY ND
Analyst Weight Sample Prep : Extracted By :19 0.501g NA NA
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -MO000043HEA
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.