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Fluence Analytics ACOMP Monitoring Polymer Reactions in Real-time

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  • Fluence Analytics

    ACOMPMonitoring Polymer Reactions in Real-time

  • Introducing ACOMP

    ACOMP is Automatic Continuous On-line Monitoring of Polymerization reactions. A patented

    solution that continuously extracts, dilutes, and conditions a small stream of reactor contents for

    analysis by a variety of non-chromatographic and chromatographic methods throughout the entire

    reaction process. The system can directly measure macromolecular properties during production.

    This fundamental information is used by the system to determine monomer conversion kinetics,

    evolution of molar mass, comonomer composition and drift, and other polymer properties

    traditionally measured through discrete, off-line analysis. ACOMP can also immediately identify

    undesired polymerization events such as out-of-range quality specification production or micro-

    gelation due to phase separation or cross-linking, so that corrective control actions can be taken.

    Increases Worker Safety

    Increases Product Quality

    Increases Polymer Yield

    Increases Process Consistency

    Reduces Cycle Time

    Reduces VOCs and Pollution

    Reduces Feedstock Usage

    Reduces Energy Consumption

    ACOMP

    3

    Real-time Analysis:• Conversion Kinetics

    • Residual Monomer PPM

    • Time to Completion

    • Molecular Weight

    • Intrinsic Viscosity

    How It Works

    Polymerization Process:• Batch, Semi-batch

    • Continuous

    • Single or Multi-component

    1

    2

    SamplePreparationContinuously:

    • Extracts

    • Quenches

    • Dilutes

    • Conditions

    5

    Control Room:• Operator views data to improve process

    • Integrates with plant control system

    4

    Automatic Report Generation:• Data Analytics

    • Historical Trends

    • Correlation to Process Data

  • Monitored CharacteristicsMolecularWeight

    MonomerConversion

    ResidualMonomer PPM

    Process AnomalyDetection

    IntrinsicViscosity

    Composition

    Features

    Optional integration with existing APCmodels for off-line optimizations

    Automated, ‘self-aware’ system for highreliability

    Customized, proprietary sample handlingand analysis selection

    Integrated real-time analysis softwareplatform

    Tailored business and technical reports viae-mail or existing analytics solution

    Simplified, automated operation requiresno advanced training

    Designed for 24/7 plant operation

    Analytical Methods and Instruments

    Real-time reaction data

    UVAbsorption

    DifferentialRefractiveIndex

    Conductivity Polarimetry

    pHDiscreteSEC/GPC

    IntrinsicViscosity

    Static LightScattering

    IndustrialACOMP Solution

  • Tailored Solutions

    Customized for target application andcustomer requirements

    R&D ACOMP: Smaller, flexible system forlab-scale or pilot plant reactors

    Industrial ACOMP: Robust system forproduction-scale polymer reactors

    On-site installation and training services

    24/7 remote monitoring and field supportpackages available

    Post-installation optimization consultingservices

    Fluence Analytics’ team of experts is readyto evaluate your application.

    If you think your application can benefitfrom ACOMP, contact Fluence Analytics for an assessment today!

    Fluence Analytics’ team of experts is readyto evaluate your application.

    If you think your application can benefitfrom ACOMP, contact Fluence Analytics for an assessment today!

    Polymer Application Examples

    Endpoint determination:Optimizes cycle time

    Real-time direct quality indicator:Improves quality control

    Process anomaly detection:Reduces batch failure

    Post-polymerization modification process:Optimization

    Post-polymerization modification process:Optimization

    Multi-stage crossover indication:Improves quality control and reducesproduction time in multi-stage process

    Batch, Semi-batch

    Monitor grade changeover:Accurate target determination

    Steady-state online quality indicator:Reduces off-spec product

    Continuous

    Emulsion, Solution, Bulk

    Heterogeneous, Multi-phase, Grafting

    Free Radical, Controlled Radical, Living

    Acrylates, Styrenics, Urethanes, etc.

    Natural Products

    Many Water Soluble Processes:Polyacrylamide, PVP, PVA, etc.

    High Temperature, High Viscosity

    Elastomers

    Types

    R&D ACOMP Solution - PolyRMC at Tulane University

  • 1078 S. Gayoso St. • New Orleans, LA 70125

    Fluence Analytics

    Call us:504.777.2805

    Questions about ACOMP?

    Visit our website:www.fluenceanalytics.com

    Send us an e-mail:[email protected]