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Getting started with Applying fluoropolymer coatings is not unreasonably complicated. Yet, there are many opportunities for error — pitfalls that can lead to what is perceived as “coating failure” but in fact is due to common mistakes in processing. This document helps avoid these mistakes. Where good ideas come to the surface Mixing... Mixing... Spraying... Spraying... Curing... Curing... Testing... Testing...

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Page 1: Mixing Spraying - Whitford Worldwide started with... · All Xylan coatings must be cured at a specific temperature to provide maximum ... parators (to check grit-blast and phosphate

Getting started with

Applying fluoropolymer coatings is notunreasonably complicated. Yet, there are many opportunities

for error — pitfalls that can lead to what is perceived as “coating failure” but in fact is due to common mistakes in processing.

This document helps avoid these mistakes.

Where good ideas come to the surface

Mixing...Mixing... Spraying...Spraying...

Curing...Curing... Testing...Testing...

Page 2: Mixing Spraying - Whitford Worldwide started with... · All Xylan coatings must be cured at a specific temperature to provide maximum ... parators (to check grit-blast and phosphate

1. Choose the proper solvent If Xylan is “paint” and the paint store sells “paint thinner”, then shouldn’t that work

just fine? The answer is No.There are many different chemicals used to reduce coatings and to clean up after

their application. Most of these are not available at your local paint store.Every Xylan coating has been chemically crafted to achieve specific performance

characteristics. And Whitford has a special solvent designed for maximum efficiencywith each coating. Whitford publishes Product Data Sheets that specify the correctsolvent as well as the ideal reduction ratio. Paying attention to this at the outset avoidsserious problems later.

2. Don’t get mixed up about mixingAll Xylan coatings must be properly mixed to provide maximum performance. But

not all Xylan coatings can be mixed the same way. Some must be mixed vigorouslywith a high-shear blade, which actually “cuts”the coating into smaller and smaller bits, ulti-mately dispersing it to fine particles. Other Xylancoatings (such as PTFE-heavy topcoats) must berolled slowly (or they will coagulate and be ren-dered useless). Roll for 1 hour at 30-40 rpm.Check the bottom to ensure that no sedimentremains after mixing.

Whitford recommends using an air mixer witha high-speed dispersion blade for most Xylancoatings. This equipment can be purchasedthrough INDCO (indco.com), (800) 851-1049, orFawcett Company (fawcettco.com), (330) 659-

4187. INDCO also sells rolling machines that are suitable for shear-sensitive coatings.Avoid mixing too fast, which can entrap air. Note: Paddle-type mixing blades are use-ful for keeping a coating mixed once it has been dispersed with a high-shear blade,as are five-gallon paint shakers (also available from INDCO). But use these only withnon-shear-sensitive coatings. Check Whitford’s Product Data Sheets for proper mixinginstructions.

3. Think before you spray

Protect yourself with the proper safety equipment. Wear a respirator with a carbonfilter. Use a full face shield. Put on safety gloves. All these items are available throughAir Gas Safety Division, (855) 625-5285 X4626

Select the right spray booth and gunMost regular and HVLP (High Volume, Low Pressure) spray guns work well. But

make sure you have the proper fluid nozzle and air cap that correspond to the idealspraying viscosity of the coating (found in the Product Data Sheet).

Improper mixing is probably the mostcommon mistake made in the applicationof Xylan coatings.

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The booth must comply with the proper permits to meet local fire and safety regu-lations. Two reliable suppliers of spray guns and booths are A.O.M. America, LLC(800) 533-6254 and Finishing Brands (800) 237-5000).

5. Look before you leap

Whitford recommends that you test the viscosity, the nozzle and the spray patternbefore you actually spray the part. Spray a thin aluminum test panel, which curesquickly, letting you check for smoothness and film thickness. If there are any prob-lems, it’s better to discover them on a throwaway panel rather than on a part. If youhave any questions regarding the test results, you can always send the panel toWhitford so that our technicians can check it for you (whitfordww.com). Panels areavailable through Q Panel Lab Products(q-lab.com) at (440) 835-8700.

6. Prepare the part properly

All Xylan industrial coatings requirethat the surface be properly prepared.First, any oils and contaminates must beremoved by degreasing the part with agood degreaser (such as an alkalinecleaner), or the coating will not adhere.Alkaline washing cleans parts with mod-erate or high pH cleaners. This is pre-ferred for high volumes of parts. Partswhich should not be washed by thismethod are those which may beadversely affected by the chemistryinvolved. If the part can withstand elevated temperatures (800˚F/425˚C),burn off any contaminants.

Grit-blasting with aluminum oxide or other abrasives is a common cleaning tech-nique, preferred for parts whose surface contaminants — rust, scale, corrosion, oldcoatings — must be removed physically. Whitford recommends a grit medium from60- to 120-mesh/250- to 125-microns. Blow off part with compressed air to removeany abrasive residue. To purchase grit-blasting equipment, contact Empire AbrasiveEquipment Co. (empire-airblast.com) at (215) 752-8800.

Phosphating is a secondary surface preparation for steel which is generally usedafter degreasing, alkaline washing or grit-blasting. Whitford recommends a modifiedzinc phosphate with a fine crystalline structure such as Aerocote 4. A thin layer (750-1000 mg/ft2 or 7.5-10 gm/m2) of zinc phosphate is deposited on the surface of thepart to promote better adhesion and dramatically increase corrosion and chemicalresistance. Cleaning and phosphating solutions are available from McDermid Inc.(macdermid.com) at (203) 575-5700.

Whitford has developed a series of test methodsto help assure consistent and ideal performancefor Xylan coatings. For a list of test methods, goto: http://www.whitfordww.com/housewares/test-methods-cookware.html

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7. Cure the part correctlyAll Xylan coatings must be cured at a specific temperature to provide maximum

performance. Details of the cure are in the Product Data Sheet. Please note that theproper cure temperature is the temperature of the part itself, not the temperaturereached inside the oven. Whitford recommends using a hand-held thermocouple to

check the temperature (available through OmegaEngineering Co. (omega.com), [888] 826-6342).

Note: Always use an oven rated for the solvent loadof the coating to prevent explosions. Oven suppliers: TheGrieve Corp. (grievecorp.com) at (847) 546-8225; BGKFinishing Systems (bgk.com) at (763) 784-0466; or SPXThermal Product Solutions (thermalproductsolutions.com) at(800) 586-2473.

8. Test to be sureWhitford recommends that any serious coating appli-

cator have the basic testing equipment to assure idealquality. This includes Zahn cups (to measure viscosity),a film-thickness gauge, a cross-hatch cutter and specialtape (to test adhesion), and visual anchor profile com-

parators (to check grit-blast and phosphate profiles). Such equipment is availablethrough Paul N. Gardner Co. Inc. (gardco.com) at (800) 762-2478 and KTA-Tator, Inc.(kta.com) at (412) 788-1300.

9. Help is at handHaving the right equipment, testing and following the proper procedures will help

guarantee that all Xylan coatings you apply perform as expected. Note: Remember touse the specific Product Data Sheet for each coating you apply.

Whitford offers additional literature to help with the process, a few listed here:1. “Engineering Design Guide” (36 pages of technical information on the applica-

tion and use of fluoropolymer coatings).2. “9 Misconceptions about Xylan Coatings” (9 common mistakes).3. “Fastener Brochure” (which Xylan coatings to use for fasteners).4. “Solving Common Coating Problems” (Wall chart with visual and verbal identifi-

cation of common problems and how to solve them).If you have any questions, or would like any of this literature, please contact us at

[email protected] (http://www.whitfordww.com/contact-us.html).

NON-WARRANTY: THE INFORMATION PRESENTED IN THIS PUBLICATION IS BASED UPON THE RESEARCH AND EXPERIENCE OF WHITFORD. NO REPRE-SENTATION OR WARRANTY IS MADE, HOWEVER, CONCERNING THE ACCURACY OR COMPLETENESS OF THE INFORMATION PRE SENTED IN THIS PUBLICATION. WHITFORD MAKES NO WARRANTY OR REPRESENTATION OF ANY KIND, EXPRESS OR IMPLIED, INCLUDING WITHOUTLIMITATION ANY WARRANTY OF MERCHANTABILITY OR FITNESS FOR ANY PARTICULAR PURPOSE, AND NO WARRANTY OR REPRESENTATION SHALL BEIMPLIED BY LAW OR OTHERWISE. ANY PRODUCTS SOLD BY WHITFORD ARE NOT WARRANTED AS SUITABLE FOR ANY PARTICULAR PURPOSE TO THEBUYER. THE SUITABILITY OF ANY PRODUCTS FOR ANY PURPOSE PARTICULAR TO THE BUYER IS FOR THE BUYER TO DETERMINE. WHITFORD ASSUMESNO RESPONSIBILITY FOR THE SELECTION OF PRODUCTS SUITABLE TO THE PARTICULAR PURPOSES OF ANY PARTICULAR BUYER. WHITFORD SHALL INNO EVENT BE LIABLE FOR ANY SPECIAL, INCIDENTAL OR CONSEQUENTIAL DAMAGES. Xylan is a registered trademark of Whitford Whitford/2014-07

A simple, inexpensive Zahn cupand a stopwatch are perfect forchecking the viscosity of Xylan.

Where good ideas come to the surface