microsoft outlook - memo style · overburden using an atv-mounted drilling rig, equipped with...

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Spakes, Rita

From: Fowler, Robert <[email protected]>Sent: Tuesday, April 25, 2017 11:34 AMTo: Sadler, BillCc: Taylor, Jodi; McCullough, DanielSubject: Jefferson County - Installation Report for Replacement Well MW-8SRAttachments: FINAL Jefferson County Installation Report for Replacement Well (8S).pdf

Bill,�

On�behalf�of�Waste�Management�of�Arkansas,�SCS�is�pleased�to�present�you�with�the�Installation�Report�for�Replacement�well�MW�8SR�for�the�Jefferson�County�Landfill.��If�you�have�any�questions�or�concerns,�feel�free�to�contact�me�or�Dan�at�your�convenience.��Sincerely,��Robert Fowler�Project Geologist��

Robert Fowler�Project Geologist��

�11219 Richardson Drive�North Little Rock, Arkansas 72113�501-503-4779�501-672-9320 cell�[email protected]�www.scsengineers.com��This�email�may�contain�confidential�information�and�is�intended�for�use�by�the�addressee�and/or�their�intended�representatives�only.��If�you�are�not�the�intended�recipient,�please�do�not�transmit,�copy,�disclose,�store�or�utilize�this�communication�in�any�manner.��If�you�received�this�message�in�error,�please�notify�the�sender�immediately�and�permanently�delete�this�message�from�your�computer.��SCS�Engineers�accepts�no�liability�for�the�content�of�this�email�or�for�the�consequences�of�any�actions�taken�on�the�basis�of�the�information�provided.�–�SCS�Engineers�

Rec’d Digitally

AFIN:_________________________

PMT#:_________________________ SW

DOC ID#:______________________ MD

TO:___________________________

By spakes at 3:05 pm, Apr 25, 2017

35-00170

0308-S1-R1

71620

BS>FILE <RDS

Environmental Consultants 11219 Richardson Drive 501-812-4551 and Contractors North Little Rock, AR 72113 FAX 501 812-4551 www.scsengineers.com

April 25, 2017 File No. 27216348.00 Mr. Bill Sadler, P.G. Solid Waste Division Arkansas Department of Environmental Quality 5301 Northshore Drive North Little Rock, AR 72118-5317 Subject: Decommissioning of MW-8S,Installation of Replacement Well MW-8SR and

sampling of MW-8D at The Waste Management of Arkansas, Inc. - Jefferson County Landfill AFIN: 35-00170; Permit No. 0308-S1-R1

Dear Mr. Sadler: On behalf of Waste Management of Arkansas, Inc. (WMA), SCS Engineers (SCS) is pleased to present this Report outlining the field activities associated with the decommissioning of monitoring well MW-8S and the installation of replacement monitoring well MW-8SR at the Jefferson County Landfill. As outlined in the Amended Alternative Source Demonstration (ASD) dated September 28, 2016 (Doc. 70349), WMA believes well integrity issues may be causing changes in geochemistry at MW-8S. Therefore, as part of the ASD, WMA proposed to replace MW-8S with a well screened at the same elevations and constructed to the ADEQ standards (Doc. #70568). This report outlines the field portion of the Amended ASD. Conditional approval of the workplan to replace MW-8S with MW-8SR was obtained from Arkansas Department of Environmental Quality (ADEQ) in a letter dated December 2, 2016 (Doc # 70677). ADEQs December 2, 2016 Conditional Approval letter also requested that MW-8D not be decommissioned and that a sample of MW-8D be taken at the same time for the same parameters as the replacement well for MW-8S. A SCS geologist documented the decommissioning of monitoring well MW-8S and the installation of replacement groundwater monitoring well MW-8SR on December 28, 2106. See Attachment A - Figure 1 for the location of the replacement monitoring well MW-8SR.


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D e c o m m i s s i o n i n g a n d I n s t a l l a t i o n o f M o n i t o r i n g W e l l s

Decommissioning was performed in accordance with the “EPA Handbook of Suggested Practices for Design and Installation of Groundwater Monitoring Wells”. The decommissioning was accomplished by pulling protective cover and then the PVC pipe from the borehole. The well was then overdrilled to 20 feet below ground surface (bgs) and backfilled with hydrated bentonite hole plug. The boring for MW-8SR, located approximately 15 ft north of MW-8S, was advanced through overburden using an ATV-mounted drilling rig, equipped with hollow stem augers that have an outside diameter (O.D.) of 8.25-inch and an inside diameter (I.D.) of 4.25-inch. Once groundwater was encountered, the boring was advanced ten additional feet and the well was installed at the same specifications of the original well MW-8S. The replacement monitoring well (MW-8SR) was drilled in order to monitor saturated conditions at the uppermost depth. MW-8S top of screen was at 371.33 fmsl. The replacement well MW-8SR top of screen is approximately 373 fmsl. MW-8SR was advanced to 25 ft below ground surface which was approximately 10 ft below first encountered groundwater. Monitoring well MW-8SR was constructed in accordance with “ASTM D5092 Standard Practice for Design and Installation of Groundwater Monitoring Well in Aquifers”. The monitoring well construction consisted of 2-inch diameter Schedule 40 PVC solid riser and 0.010” slotted screen (10 foot in length). The sand filter pack extended to two (2) feet above the screened interval. A three (3) foot bentonite pellet seal was placed immediately above the filter pack. After placement of the entire bentonite seal, the pellets were allowed to hydrate prior to the placement of the remaining bentonite chip seal to the surface. The depth of sand or bentonite was measured as the material was added to the borehole with a tape to insure that bridging did not occur within any portion of the borehole. Surface completion of the monitoring well consisted of a monument-type protective cover of galvanized steel, concrete pad, and protective bollard poles. The boring log/construction diagram for monitoring well MW-8SR has been included as Attachment B to this report. In an attempt to prevent future sedimentation to the newly installed MW-8SR a protective concrete wall was installed on the east side of the monitoring well. This wall is intended to divert stormwater runoff and to prevent sedimentation from occurring in the vicinity of the monitoring well. These subcontract drilling services were supervised by an experienced Arkansas Licensed monitoring well driller. The replacement well was surveyed by Mason Surveying & Consulting; Inc. The stamped survey information is provided as Attachment C to this report.


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S a m p l i n g o f M o n i t o r i n g W e l l M W - 8 S R a n d M W - 8 D

The new monitoring well was developed with a submersible pump. Field data (pH, conductivity, Temperature, and Turbidity) were recorded, as well as the volume of water removed from the well during well development. Once a minimum of 5 well volumes were removed, field parameters were allowed to stabilize and a groundwater sample was obtained from MW-8SR. The field information form is included as Attachment D to this report. The procedures for obtaining groundwater samples, parameters analyzed, sample preservation, and handling were conducted in accordance with the Facility approved Groundwater Sampling and Analysis Plan. Samples from monitoring wells MW-8SR and MW-8D were collected and containerized in the order of the volatilization sensitivity of the parameter. The analytical results are presented as Attachment D to this report. TABLE 1 presents a summary of the groundwater quality for the inorganic constituents at monitoring points MW-8SR and MW-8D and the equipment blank. The table also presents a comparison of these results to applicable EPA Primary Drinking Water Standard- Maximum Contaminant Levels (MCLs).

Jefferson County Landfill

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TABLE 1 GROUNDWATER QUALITY RESULTS

WELL # As

(ug/L) Ba

(ug/L) Cr

(ug/L) Pb

(ug/L) Mn

(ug/L) K

(ug/L) Na

(ug/L) Mg

(ug/L) Fe

(ug/L) Ni

(ug/L) TDS

(mg/L) Zn

(ug/L) Ammonia

(mg/L) Ag

(ug/L)

MW-8SR 1.2 J 38 J 1.7 J,B 4.2 J 110 3100 27000 24000 2100 36 390 80 0.080 J <10 MW-8D 2.1 J 27 J 1.8 J, B <5.0 390 9100 37000 25000 1900 3.0 J 510 11 J <0.10 <10

EPA Standards 10* 2000* 100* 15* --- --- --- --- --- --- --- --- --- ---

WELL # Alkalinity

(mg/L) TOC

(mg/L) SO4

(mg/L) Ca

(ug/L) Cl

(mg/L) Be

(ug/L) Cd

(ug/L) Cu

(ug/L) Se

(ug/L) Tl

(ug/L) Co

(ug/L) Sb

(ug/L) V

(ug/L)

MW-8SR 3.1 J 1.7 B 200 26000 B 31 4.6 1.2 J <15 <5.0 0.24 J 28 <20 1.1 J MW-8D 52 0.74 J, B 300 82000 B 30 <1.0 <5 4.4 J <5.0 <1.0 <10 <20 <5.0

EPA Standards --- --- --- --- --- 4* 5* 1300* 50* 2* --- --- ---

*Primary Drinking Water Standard – Maximum Contaminant Level (MCL) J = estimated concentration below the Reporting Limit B= compound was found in the lab blank and sample

TABLE 1 (CONT’D) - GROUNDWATER QUALITY RESULTS WELL # CisDCEE VC

Bis(2-ethylhexl) phthalate

MW-8SR 0.42 J 0.31J <5.8 MW-8D <1 <1 15

EPA Standards 70* 2* 6*

*Primary Drinking Water Standard – Maximum Contaminant Level (MCL) J = estimated concentration below the Reporting Limit B= compound was found in the lab blank and sample

ATTACHMENT A – MONITORING WELL LOCATION MAP

EXISTING

CELL 1

(11.3 AC)

EXISTING

CELL 2B

(5.1 AC)

EXISTING

CELL 2A

(5.3 AC)

EXISTING

CELL 3B

(5.1 AC)

EXISTING

CELL 3A

(5.3 AC)

EXISTING

CELL 4B

(5.1 AC)

EXISTING

CELL 4A

(5.3 AC)

FUTURE

CELL 5B

(5.1 AC)

PROPOSED

CELL 5A

(5.3 AC)

FUTURE

CELL 4B

(10.5 AC)

SOUTH

STORMWATER

BASIN

NORTH STORMWATER BASIN

WE

ST

S

TO

RM

WA

TE

R B

AS

IN

EXISTING

COMPOST

AREA

WETLAND

MITIGATION AREA

MW-7D

MW-15R

MW-14

MW-13

MW-12R

MW-11

MW-8S

MW-16

MW-09 MW-10

MW-8SRMW-8D

(DECOMISSIONED)

GROUNDWATER MONITORING WELL INSTALLATION

WASTE MANAGEMENT

SCS ENGINEERS

FIGURE

JEFFERSON COUNTY LANDFILL FACILITY

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11219 RICHARDSON DRIVENORTH LITTLE ROCK, AR. 72113

PH. (501) 812-4551 WEB. www.scsengineers.com

NEWLY INSTALLED MONITORING WELL LOCATION

MW-8SR 1923166.94 1254235.31 34°20'42.5410" 390.82 388.23

MW IDNUMBER

NORTHING(STATE PLANECOORDINATES)

EASTING(STATE PLANECOORDINATES)

LATITUDE LONGITUDE

TOP OF PVCPIPE

ELEVATION(FEET)

TOP OFADJACENTGROUND

ELEVATION(FEET)

92°11'32.9095"

0150300 300

SCALE: 1" = 300'

MW-8SR

MW-09

NEWLY INSTALLED GROUNDWATERMONITORING WELL

EXISTING GROUNDWATERMONITORING WELL

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4/11/17

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ATTACHMENT B – MW-8SR BORING LOG/CONSTRUCTION DIAGRAM

379.2

392

387

382

377

372

367

25

20

15

10

5

0

Stick Up (2.59ft)

Concrete Pad(Approximately 6")

Bentonite pellet seal fromground surface to 12.5 ft

bgs

2 in dia. Sch. 40 PVC soildriser from 0-14.67 ft bgs

Sand filter pack from 12.5ft to 25 ft bgs

10 ft of 2 in dia, 0.010slot, Sch. 40 PVC sreen

End CapTD - 25 ft bgs

Topsoil; dark brown withrootlets

Sandy Clay; reddish brownwith light gray mottling

Sandy Clay; gray sandyclay with some gravels

Sandy Clay; dark gray withfine grained sand

12/28/201612/28/2016Robert FowlerJefferson County Lanfill, AR27216348.00Jefferson County Well ReplacementWaste Management

REC

OV

ERY

(%)

LITHOLOGY LITHOLOGY DESCRIPTION MONITORING WELL CONSTRUCTION MONITORING WELL DESCRIPTION

390.82 fmsl25 fbgs

11.6 fbgs

MW-8SR

388.23 fmsl

379.22 fmsl1/23/2017

1254235.311923166.94

THE STRATIFICATION LINES REPRESENT APPROXIMATEBOUNDARY LINES BETWEEN SOIL AND ROCK TYPES: ACTUALTRANSITIONS MAY BE GRADUAL

ATTACHMENT C – SURVEY OF MONITORING WELL MW-8SR

Table 1. Surveyed Locations of Monitoring Wells (MW)

MW IDNumber

Northing (StatePlane

Coordinates) (1,4)

Easting(StatePlane

Coordinates) (1,4) Latitude (5) Longitude (5)

Top of PVC PipeElevation (feet) (2)

Top of AdjacentGround

Elevation (feet)(3)

MW - 8SR 1923166.94 1254235.31 34°20'42.5410" 92°11'32.9095" 390.82 388.23

Notes:

1. Northing and Easting Locations are at top of MW PVC casing.

Table 2. Jefferson County Landfill Control InformationPoint Northing Easting Elevation

6 1922593.78 1255648.97 414.138 1923813.42 1254340.25 396.41

12 1922833.98 1255534.36 413.45

Survey of Monitoring Well Installed by SCS AQUATERRAWaste Management - Jefferson County LandfillPermit No. 0308-S1-R1; AFIN 35-00170MSCI Project No.: 16026

3. Top of adjacent ground elevation was measured at the north side of well just beyond the concrete pad.

2. Top of PVC pipe elevation was measured on north side of pipe and marked at surveyed location.

4. Field measurements were surveyed by MSCI on January 02, 2017 and are based on site specific control data as provided by WM to MSCI. Site specific control datumis scaled and rotated on State Plane Projection NAD83, Arkansas South and NAVD88 as provided to MSCI. No independent survey has been performed by MSCI to verifythe correctness of the site control datum to NAD83 and NAVD88. Table 2 below shows site benchmarks used to control the survey.5. Geodetic coordinates were converted from the Northing and Easting in Table 1 using Carlson Survey Software and are based on the site specific control datum

ATTACHMENT D – LABORATORY ANALYTICAL REPORT/FIELD INFORMATION FORM

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Denver4955 Yarrow StreetArvada, CO 80002Tel: (303)736-0100

TestAmerica Job ID: 280-93303-1Client Project/Site: 667|Jefferson County LF

For:Waste Management100 Two Pine DriveNorth Little Rock, Arkansas 72117-1583

Attn: Jodi Reynolds-Coffelt

Authorized for release by:2/7/2017 3:49:17 PM

Danielle Harrington, Project Manager II(303)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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mailto:[email protected]

Table of Contents

Client: Waste ManagementProject/Site: 667|Jefferson County LF

TestAmerica Job ID: 280-93303-1

Page 2 of 39TestAmerica Denver

2/7/2017

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

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Definitions/GlossaryTestAmerica Job ID: 280-93303-1Client: Waste Management

Project/Site: 667|Jefferson County LF

Qualifiers

GC/MS VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

F2 MS/MSD RPD exceeds control limits

Metals



Qualifier

B Compound was found in the blank and sample.

F1 MS and/or MSD Recovery is outside acceptance limits.

General Chemistry


B Compound was found in the blank and sample.

Qualifier


Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Denver

Page 3 of 39 2/7/2017

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Case NarrativeClient: Waste Management TestAmerica Job ID: 280-93303-1Project/Site: 667|Jefferson County LF

Job ID: 280-93303-1

Laboratory: TestAmerica Denver

Narrative

CASE NARRATIVE

Client: Waste Management

Project: 667|Jefferson County

Permit #308-S1-R1

AFIN# 35-00170

Report Number: 280-93303-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

This report may include reporting limits (RLs) less than TestAmerica’s standard reporting limit. The reported sample results and associated reporting limits are being used specifically to meet the needs of this project. Note that data are not normally reported to these levels without qualification because they are inherently less reliable and potentially less defensible than required by the latest industry standards.

This submission may contain field data obtained by the sampler. The methods referenced in this submission for the field data results may not be the methods used to obtain the field data by the sampler.

RECEIPT

These samples were received on 1/24/2017 with cooler temperatures of 1.0º C.

Please note, four hydrochloric preserved VOA vials for a TRIP BLANK were received but not listed on the chain of custody. The laboratory

proceeded with the 8260B analysis. The client was notified on 1/24/2017.

All sample bottles were received in acceptable condition.

HOLDING TIMES

All Holding Times were met.

METHOD BLANKSLow levels of Calcium and Chromium are present in the method blank associated with QC batch 280-360084. Because the concentration

in the method blank is not present at a level greater than the reporting limit, corrective action is deemed unnecessary.

Low levels of Total Organic Carbon are present in the method blank associated with QC batch 280-360090. Because the concentration in

the method blank is not present at a level greater than the reporting limit, corrective action is deemed unnecessary.

All other Method Blanks were within the acceptance limits.

LABORATORY CONTROL SAMPLES (LCS)

All Laboratory Control Samples were within the acceptance limits.

TestAmerica DenverPage 4 of 39 2/7/2017

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Case NarrativeClient: Waste Management TestAmerica Job ID: 280-93303-1Project/Site: 667|Jefferson County LF

Job ID: 280-93303-1 (Continued)

Laboratory: TestAmerica Denver (Continued)

MATRIX SPIKE (MS) and MATRIX SPIKE DUPLICATES (MSD)

Laboratory generated MS/MSD analysis data have been provided. The MS/MSD for method 8260B exhibited spike compound recoveries outside the QC limits for 1,2-Dibromo-3-Chloropropane. The acceptable LCS analysis data indicated that the analytical system was

operating within control; therefore, corrective action is deemed unnecessary.

The method 8270C could not be performed for this batch, due to insufficient sample volume. Method precision and accuracy have been

verified by the acceptable LCS/LCSD analysis data.

Laboratory generated MS/MSD analysis data have been provided. The MS/MSD for method 6010B exhibited spike compound recoveries

outside the QC limits for Iron. The acceptable LCS analysis data indicated that the analytical system was operating within control; therefore, corrective action is deemed unnecessary.

All other Matrix Spike and Matrix Spike Duplicates were within the acceptance limits.

GENERAL CHEMISTRYThe samples were analyzed at dilutions due to high analyte concentrations for Sulfate. The reporting limits have been adjusted relative to the dilution required.


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Detection SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


Client Sample ID: MW-08D Lab Sample ID: 280-93303-1

Field Conductivity

NONE

umhos/cm

NONEAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1666 Field Sampling

Field Dissolved Oxygen mg/L Total/NA12.84 Field Sampling

Field Temperature Degrees C Total/NA117.4 Field Sampling

Field pH SU Total/NA15.38 Field Sampling

Depth to water ft Total/NA128.31 Field Sampling

Field Turbidity NTU Total/NA18.66 Field Sampling

Field EH/ORP millivolts Total/NA182.7 Field Sampling

Bis(2-ethylhexyl) phthalate

RL

5.8 ug/L

MDL

0.54

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA115 8270C

Barium 100 ug/L0.82 Total/NA127 J 6010B

Calcium 200 ug/L35 Total/NA182000 B 6010B

Chromium 10 ug/L0.66 Total/NA11.8 J B 6010B

Copper 15 ug/L4.2 Total/NA14.4 J 6010B

Iron 100 ug/L22 Total/NA11900 6010B

Magnesium 200 ug/L11 Total/NA125000 6010B

Manganese 15 ug/L0.26 Total/NA1390 6010B

Nickel 12 ug/L2.6 Total/NA13.0 J 6010B

Potassium 3000 ug/L240 Total/NA19100 6010B

Sodium 5000 ug/L120 Total/NA137000 6010B

Zinc 20 ug/L4.5 Total/NA111 J 6010B

Arsenic 10 ug/L0.33 Total/NA12.1 J 6020

Chloride 0.60 mg/L0.25 Total/NA130 300.0

Sulfate 10 mg/L0.46 Total/NA2300 300.0

Total Alkalinity 5.0 mg/L1.1 Total/NA152 SM 2320B

Bicarbonate Alkalinity 5.0 mg/L1.1 Total/NA152 SM 2320B

Total Dissolved Solids 5.4 mg/L4.7 Total/NA1540 SM 2540C

Total Organic Carbon - Average 1.0 mg/L0.16 Total/NA10.74 J B SM 5310B

Client Sample ID: MW-08SR Lab Sample ID: 280-93303-2

Field Conductivity

NONE

umhos/cm

NONEAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1473 Field Sampling

Field Dissolved Oxygen mg/L Total/NA10.32 Field Sampling

Field Temperature Degrees C Total/NA117.8 Field Sampling

Field pH SU Total/NA13.95 Field Sampling

Depth to water ft Total/NA111.60 Field Sampling

Field Turbidity NTU Total/NA19.61 Field Sampling

Field EH/ORP millivolts Total/NA189.2 Field Sampling

cis-1,2-Dichloroethene

RL

1.0 ug/L

MDL

0.15


Total/NA1J0.42 8260B

Vinyl chloride 1.0 ug/L0.10 Total/NA10.31 J 8260B

Barium 100 ug/L0.82 Total/NA138 J 6010B

Beryllium 1.0 ug/L0.47 Total/NA14.6 6010B

Cadmium 5.0 ug/L0.45 Total/NA11.2 J 6010B

Calcium 200 ug/L35 Total/NA126000 B 6010B

Chromium 10 ug/L0.66 Total/NA11.7 J B 6010B

Cobalt 10 ug/L1.2 Total/NA128 6010B

Iron 100 ug/L22 Total/NA12100 F1 6010B

Lead 5.0 ug/L2.7 Total/NA14.2 J 6010B

Magnesium 200 ug/L11 Total/NA124000 6010B

TestAmerica Denver

This Detection Summary does not include radiochemical test results.

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Detection SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


Client Sample ID: MW-08SR (Continued) Lab Sample ID: 280-93303-2

Manganese

RL

15 ug/L

MDL

0.26


Total/NA1110 6010B

Nickel 12 ug/L2.6 Total/NA136 6010B

Potassium 3000 ug/L240 Total/NA13100 6010B

Sodium 5000 ug/L120 Total/NA127000 6010B

Zinc 20 ug/L4.5 Total/NA180 6010B

Arsenic 10 ug/L0.33 Total/NA11.2 J 6020

Thallium 1.0 ug/L0.050 Total/NA10.24 J 6020

Vanadium 5.0 ug/L0.50 Total/NA11.1 J 6020

Chloride 0.60 mg/L0.25 Total/NA131 300.0

Sulfate 10 mg/L0.46 Total/NA2200 300.0

Ammonia as N 0.10 mg/L0.022 Total/NA10.080 J 350.1

Total Alkalinity 5.0 mg/L1.1 Total/NA13.1 J SM 2320B

Bicarbonate Alkalinity 5.0 mg/L1.1 Total/NA13.1 J SM 2320B

Total Dissolved Solids 5.4 mg/L4.7 Total/NA1390 SM 2540C

Total Organic Carbon - Average 1.0 mg/L0.16 Total/NA11.7 B SM 5310B

Client Sample ID: TRIP BLANK Lab Sample ID: 280-93303-3

No Detections.

TestAmerica Denver

This Detection Summary does not include radiochemical test results.

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Sample SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

280-93303-1 MW-08D Water 01/23/17 13:12 01/24/17 10:15

280-93303-2 MW-08SR Water 01/23/17 14:38 01/24/17 10:15

280-93303-3 TRIP BLANK Water 01/23/17 00:00 01/24/17 10:15

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Method SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL DEN

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL DEN

SW8466010B Metals (ICP) TAL DEN

SW8466020 Metals (ICP/MS) TAL DEN

MCAWW300.0 Anions, Ion Chromatography TAL DEN

MCAWW350.1 Nitrogen, Ammonia TAL DEN

SMSM 2320B Alkalinity TAL DEN

SMSM 2540C Solids, Total Dissolved (TDS) TAL DEN

SMSM 5310B Organic Carbon, Total (TOC) TAL DEN

EPAField Sampling Field Sampling TAL DEN

Protocol References:

EPA = US Environmental Protection Agency

MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100

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Client Sample ResultsTestAmerica Job ID: 280-93303-1Client: Waste Management


Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: 280-93303-1Client Sample ID: MW-08DMatrix: WaterDate Collected: 01/23/17 13:12

Date Received: 01/24/17 10:15RL MDL

1,1,1,2-Tetrachloroethane ND 1.0 0.21 ug/L 01/26/17 16:00 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 0.16 ug/L 01/26/17 16:00 11,1,1-Trichloroethane ND

1.0 0.21 ug/L 01/26/17 16:00 11,1,2,2-Tetrachloroethane ND


1.0 0.22 ug/L 01/26/17 16:00 11,1-Dichloroethane ND

1.0 0.23 ug/L 01/26/17 16:00 11,1-Dichloroethene ND

1.0 0.33 ug/L 01/26/17 16:00 11,2,3-Trichloropropane ND

2.0 0.47 ug/L 01/26/17 16:00 11,2-Dibromo-3-Chloropropane ND

1.0 0.18 ug/L 01/26/17 16:00 11,2-Dibromoethane ND

1.0 0.15 ug/L 01/26/17 16:00 11,2-Dichlorobenzene ND


1.0 0.18 ug/L 01/26/17 16:00 11,2-Dichloropropane ND


5.0 2.0 ug/L 01/26/17 16:00 12-Butanone (MEK) ND

5.0 1.7 ug/L 01/26/17 16:00 12-Hexanone ND

5.0 0.98 ug/L 01/26/17 16:00 14-Methyl-2-pentanone (MIBK) ND

10 1.9 ug/L 01/26/17 16:00 1Acetone ND

20 1.4 ug/L 01/26/17 16:00 1Acrylonitrile ND

1.0 0.16 ug/L 01/26/17 16:00 1Benzene ND

1.0 0.10 ug/L 01/26/17 16:00 1Bromochloromethane ND

1.0 0.17 ug/L 01/26/17 16:00 1Bromodichloromethane ND

1.0 0.19 ug/L 01/26/17 16:00 1Bromoform ND

2.0 0.21 ug/L 01/26/17 16:00 1Bromomethane ND

1.0 0.45 ug/L 01/26/17 16:00 1Carbon disulfide ND

1.0 0.19 ug/L 01/26/17 16:00 1Carbon tetrachloride ND

1.0 0.17 ug/L 01/26/17 16:00 1Chlorobenzene ND

2.0 0.41 ug/L 01/26/17 16:00 1Chloroethane ND

1.0 0.16 ug/L 01/26/17 16:00 1Chloroform ND

2.0 0.30 ug/L 01/26/17 16:00 1Chloromethane ND

1.0 0.15 ug/L 01/26/17 16:00 1cis-1,2-Dichloroethene ND

1.0 0.16 ug/L 01/26/17 16:00 1cis-1,3-Dichloropropene ND

1.0 0.17 ug/L 01/26/17 16:00 1Dibromochloromethane ND

1.0 0.17 ug/L 01/26/17 16:00 1Dibromomethane ND

1.0 0.16 ug/L 01/26/17 16:00 1Ethylbenzene ND

1.0 0.23 ug/L 01/26/17 16:00 1Iodomethane ND

5.0 0.32 ug/L 01/26/17 16:00 1Methylene Chloride ND

1.0 0.17 ug/L 01/26/17 16:00 1Styrene ND

1.0 0.20 ug/L 01/26/17 16:00 1Tetrachloroethene ND

1.0 0.17 ug/L 01/26/17 16:00 1Toluene ND

1.0 0.15 ug/L 01/26/17 16:00 1trans-1,2-Dichloroethene ND

1.0 0.19 ug/L 01/26/17 16:00 1trans-1,3-Dichloropropene ND

1.0 0.80 ug/L 01/26/17 16:00 1trans-1,4-Dichloro-2-butene ND

1.0 0.16 ug/L 01/26/17 16:00 1Trichloroethene ND

2.0 0.29 ug/L 01/26/17 16:00 1Trichlorofluoromethane ND

2.0 0.94 ug/L 01/26/17 16:00 1Vinyl acetate ND

1.0 0.10 ug/L 01/26/17 16:00 1Vinyl chloride ND

2.0 0.19 ug/L 01/26/17 16:00 1Xylenes (total) ND

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

1,2-Dichloroethane-d4 (Surr) 119 70 - 127 01/26/17 16:00 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 103 01/26/17 16:00 178 - 120

Dibromofluoromethane (Surr) 115 01/26/17 16:00 177 - 120

Toluene-d8 (Surr) 100 01/26/17 16:00 180 - 125

Lab Sample ID: 280-93303-2Client Sample ID: MW-08SRMatrix: WaterDate Collected: 01/23/17 14:38

















5.0 1.7 ug/L 01/26/17 16:19 12-Hexanone ND


10 1.9 ug/L 01/26/17 16:19 1Acetone ND


1.0 0.16 ug/L 01/26/17 16:19 1Benzene ND



1.0 0.19 ug/L 01/26/17 16:19 1Bromoform ND








1.0 0.15 ug/L 01/26/17 16:19 1cis-1,2-Dichloroethene 0.42 J






5.0 0.32 ug/L 01/26/17 16:19 1Methylene Chloride ND

1.0 0.17 ug/L 01/26/17 16:19 1Styrene ND


1.0 0.17 ug/L 01/26/17 16:19 1Toluene ND





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Trichlorofluoromethane ND 2.0 0.29 ug/L 01/26/17 16:19 1



1.0 0.10 ug/L 01/26/17 16:19 1Vinyl chloride 0.31 J






Toluene-d8 (Surr) 101 01/26/17 16:19 180 - 125

Lab Sample ID: 280-93303-3Client Sample ID: TRIP BLANKMatrix: WaterDate Collected: 01/23/17 00:00

















5.0 1.7 ug/L 01/26/17 12:47 12-Hexanone ND


10 1.9 ug/L 01/26/17 12:47 1Acetone ND


1.0 0.16 ug/L 01/26/17 12:47 1Benzene ND



1.0 0.19 ug/L 01/26/17 12:47 1Bromoform ND








1.0 0.15 ug/L 01/26/17 12:47 1cis-1,2-Dichloroethene ND






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Lab Sample ID: 280-93303-3Client Sample ID: TRIP BLANKMatrix: WaterDate Collected: 01/23/17 00:00


Methylene Chloride ND 5.0 0.32 ug/L 01/26/17 12:47 1


1.0 0.17 ug/L 01/26/17 12:47 1Styrene ND


1.0 0.17 ug/L 01/26/17 12:47 1Toluene ND





2.0 0.29 ug/L 01/26/17 12:47 1Trichlorofluoromethane ND


1.0 0.10 ug/L 01/26/17 12:47 1Vinyl chloride ND






Toluene-d8 (Surr) 106 01/26/17 12:47 180 - 125

Method: 8270C - Semivolatile Organic Compounds (GC/MS)



Bis(2-ethylhexyl) phthalate 15 5.8 0.54 ug/L 01/25/17 10:11 02/01/17 05:27 1


2-Fluorophenol 86 41 - 135 01/25/17 10:11 02/01/17 05:27 1


2-Fluorobiphenyl 87 01/25/17 10:11 02/01/17 05:27 148 - 135

Nitrobenzene-d5 90 01/25/17 10:11 02/01/17 05:27 142 - 135

Phenol-d5 90 01/25/17 10:11 02/01/17 05:27 146 - 135

Terphenyl-d14 97 01/25/17 10:11 02/01/17 05:27 120 - 135

2,4,6-Tribromophenol 92 01/25/17 10:11 02/01/17 05:27 148 - 135



Bis(2-ethylhexyl) phthalate ND 5.8 0.54 ug/L 01/25/17 10:11 02/02/17 19:40 1


2-Fluorophenol 82 41 - 135 01/25/17 10:11 02/02/17 19:40 1


2-Fluorobiphenyl 82 01/25/17 10:11 02/02/17 19:40 148 - 135

Nitrobenzene-d5 78 01/25/17 10:11 02/02/17 19:40 142 - 135

Phenol-d5 81 01/25/17 10:11 02/02/17 19:40 146 - 135

Terphenyl-d14 91 01/25/17 10:11 02/02/17 19:40 120 - 135

2,4,6-Tribromophenol 91 01/25/17 10:11 02/02/17 19:40 148 - 135

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Method: 6010B - Metals (ICP)



Antimony ND 20 5.2 ug/L 01/25/17 14:30 01/26/17 01:16 1


100 0.82 ug/L 01/25/17 14:30 01/26/17 01:16 1Barium 27 J

1.0 0.47 ug/L 01/25/17 14:30 01/26/17 01:16 1Beryllium ND

5.0 0.45 ug/L 01/25/17 14:30 01/26/17 01:16 1Cadmium ND

200 35 ug/L 01/25/17 14:30 01/26/17 01:16 1Calcium 82000 B

10 0.66 ug/L 01/25/17 14:30 01/26/17 01:16 1Chromium 1.8 J B

10 1.2 ug/L 01/25/17 14:30 01/26/17 01:16 1Cobalt ND

15 4.2 ug/L 01/25/17 14:30 01/26/17 01:16 1Copper 4.4 J

100 22 ug/L 01/25/17 14:30 01/26/17 01:16 1Iron 1900

5.0 2.7 ug/L 01/25/17 14:30 01/26/17 01:16 1Lead ND

200 11 ug/L 01/25/17 14:30 01/26/17 01:16 1Magnesium 25000

15 0.26 ug/L 01/25/17 14:30 01/26/17 01:16 1Manganese 390

12 2.6 ug/L 01/25/17 14:30 01/26/17 01:16 1Nickel 3.0 J

3000 240 ug/L 01/25/17 14:30 01/26/17 01:16 1Potassium 9100

10 0.93 ug/L 01/25/17 14:30 01/26/17 01:16 1Silver ND

5000 120 ug/L 01/25/17 14:30 01/26/17 01:16 1Sodium 37000

20 4.5 ug/L 01/25/17 14:30 01/26/17 01:16 1Zinc 11 J



Antimony ND 20 5.2 ug/L 01/25/17 14:30 01/26/17 01:19 1


100 0.82 ug/L 01/25/17 14:30 01/26/17 01:19 1Barium 38 J

1.0 0.47 ug/L 01/25/17 14:30 01/26/17 01:19 1Beryllium 4.6

5.0 0.45 ug/L 01/25/17 14:30 01/26/17 01:19 1Cadmium 1.2 J

200 35 ug/L 01/25/17 14:30 01/26/17 01:19 1Calcium 26000 B

10 0.66 ug/L 01/25/17 14:30 01/26/17 01:19 1Chromium 1.7 J B

10 1.2 ug/L 01/25/17 14:30 01/26/17 01:19 1Cobalt 28

15 4.2 ug/L 01/25/17 14:30 01/26/17 01:19 1Copper ND

100 22 ug/L 01/25/17 14:30 01/26/17 01:19 1Iron 2100 F1

5.0 2.7 ug/L 01/25/17 14:30 01/26/17 01:19 1Lead 4.2 J

200 11 ug/L 01/25/17 14:30 01/26/17 01:19 1Magnesium 24000

15 0.26 ug/L 01/25/17 14:30 01/26/17 01:19 1Manganese 110

12 2.6 ug/L 01/25/17 14:30 01/26/17 01:19 1Nickel 36

3000 240 ug/L 01/25/17 14:30 01/26/17 01:19 1Potassium 3100

10 0.93 ug/L 01/25/17 14:30 01/26/17 01:19 1Silver ND

5000 120 ug/L 01/25/17 14:30 01/26/17 01:19 1Sodium 27000

20 4.5 ug/L 01/25/17 14:30 01/26/17 01:19 1Zinc 80

Method: 6020 - Metals (ICP/MS)



Arsenic 2.1 J 10 0.33 ug/L 01/25/17 14:30 01/25/17 22:11 1


5.0 0.70 ug/L 01/25/17 14:30 01/25/17 22:11 1Selenium ND

1.0 0.050 ug/L 01/25/17 14:30 01/25/17 22:11 1Thallium ND

5.0 0.50 ug/L 01/25/17 14:30 01/25/17 22:11 1Vanadium ND

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Arsenic 1.2 J 10 0.33 ug/L 01/25/17 14:30 01/25/17 22:30 1


5.0 0.70 ug/L 01/25/17 14:30 01/25/17 22:30 1Selenium ND

1.0 0.050 ug/L 01/25/17 14:30 01/25/17 22:30 1Thallium 0.24 J

5.0 0.50 ug/L 01/25/17 14:30 01/25/17 22:30 1Vanadium 1.1 J

General Chemistry



Chloride 30 0.60 0.25 mg/L 01/25/17 12:00 1


10 0.46 mg/L 01/25/17 20:41 2Sulfate 300

0.10 0.022 mg/L 01/26/17 14:38 1Ammonia as N ND

5.0 1.1 mg/L 01/25/17 09:53 1Total Alkalinity 52

5.0 1.1 mg/L 01/25/17 09:53 1Bicarbonate Alkalinity 52

5.0 1.1 mg/L 01/25/17 09:53 1Carbonate Alkalinity ND

5.4 4.7 mg/L 01/26/17 09:24 1Total Dissolved Solids 540

1.0 0.16 mg/L 01/25/17 15:53 1Total Organic Carbon - Average 0.74 J B



Chloride 31 0.60 0.25 mg/L 01/25/17 12:17 1


10 0.46 mg/L 01/25/17 20:58 2Sulfate 200

0.10 0.022 mg/L 01/26/17 14:40 1Ammonia as N 0.080 J

5.0 1.1 mg/L 01/25/17 09:57 1Total Alkalinity 3.1 J

5.0 1.1 mg/L 01/25/17 09:57 1Bicarbonate Alkalinity 3.1 J

5.0 1.1 mg/L 01/25/17 09:57 1Carbonate Alkalinity ND

5.4 4.7 mg/L 01/26/17 09:24 1Total Dissolved Solids 390

1.0 0.16 mg/L 01/25/17 16:09 1Total Organic Carbon - Average 1.7 B

Method: Field Sampling - Field Sampling


Date Received: 01/24/17 10:15NONE NONE

Field Conductivity 666 umhos/cm 01/23/17 12:12 1


mg/L 01/23/17 12:12 1Field Dissolved Oxygen 2.84

Degrees C 01/23/17 12:12 1Field Temperature 17.4

SU 01/23/17 12:12 1Field pH 5.38

ft 01/23/17 12:12 1Depth to water 28.31

NTU 01/23/17 12:12 1Field Turbidity 8.66

millivolts 01/23/17 12:12 1Field EH/ORP 82.7



Field Conductivity 473 umhos/cm 01/23/17 13:38 1


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Method: Field Sampling - Field Sampling (Continued)



Field Dissolved Oxygen 0.32 mg/L 01/23/17 13:38 1


Degrees C 01/23/17 13:38 1Field Temperature 17.8

SU 01/23/17 13:38 1Field pH 3.95

ft 01/23/17 13:38 1Depth to water 11.60

NTU 01/23/17 13:38 1Field Turbidity 9.61

millivolts 01/23/17 13:38 1Field EH/ORP 89.2

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Surrogate SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (70-127) (78-120) (77-120) (80-125)

12DCE BFB DBFM TOL

119 103 115 100280-93303-1

Percent Surrogate Recovery (Acceptance Limits)

MW-08D

119 102 113 101280-93303-2 MW-08SR

111 108 109 106280-93303-3 TRIP BLANK

109 99 105 100280-93329-G-1 MS Matrix Spike

110 103 108 101280-93329-G-1 MSD Matrix Spike Duplicate

114 102 106 102LCS 280-360061/4 Lab Control Sample

103 88 97 91MB 280-360061/6 Method Blank

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (41-135) (48-135) (42-135) (46-135) (20-135) (48-135)

2FP FBP NBZ PHL TPH TBP

86 87 90 90 97 92280-93303-1

Percent Surrogate Recovery (Acceptance Limits)

MW-08D

82 82 78 9181 91280-93303-2 MW-08SR

80 85 86 9482 88LCS 280-359912/2-A Lab Control Sample

89 92 94 9790 88LCSD 280-359912/3-A Lab Control Sample Dup

86 79 87 10088 76MB 280-359912/1-A Method Blank

Surrogate Legend

2FP = 2-Fluorophenol

FBP = 2-Fluorobiphenyl

NBZ = Nitrobenzene-d5

PHL = Phenol-d5

TPH = Terphenyl-d14

TBP = 2,4,6-Tribromophenol

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QC Sample ResultsTestAmerica Job ID: 280-93303-1Client: Waste Management


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 280-360061/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 360061

RL MDL


MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.161.0 ug/L 01/26/17 08:35 11,1,1-Trichloroethane

ND 0.211.0 ug/L 01/26/17 08:35 11,1,2,2-Tetrachloroethane

ND 0.271.0 ug/L 01/26/17 08:35 11,1,2-Trichloroethane

ND 0.221.0 ug/L 01/26/17 08:35 11,1-Dichloroethane

ND 0.231.0 ug/L 01/26/17 08:35 11,1-Dichloroethene

ND 0.331.0 ug/L 01/26/17 08:35 11,2,3-Trichloropropane

ND 0.472.0 ug/L 01/26/17 08:35 11,2-Dibromo-3-Chloropropane

ND 0.181.0 ug/L 01/26/17 08:35 11,2-Dibromoethane

ND 0.151.0 ug/L 01/26/17 08:35 11,2-Dichlorobenzene

ND 0.131.0 ug/L 01/26/17 08:35 11,2-Dichloroethane

ND 0.181.0 ug/L 01/26/17 08:35 11,2-Dichloropropane

ND 0.161.0 ug/L 01/26/17 08:35 11,4-Dichlorobenzene

ND 2.05.0 ug/L 01/26/17 08:35 12-Butanone (MEK)

ND 1.75.0 ug/L 01/26/17 08:35 12-Hexanone

ND 0.985.0 ug/L 01/26/17 08:35 14-Methyl-2-pentanone (MIBK)

ND 1.910 ug/L 01/26/17 08:35 1Acetone

ND 1.420 ug/L 01/26/17 08:35 1Acrylonitrile

ND 0.161.0 ug/L 01/26/17 08:35 1Benzene

ND 0.101.0 ug/L 01/26/17 08:35 1Bromochloromethane

ND 0.171.0 ug/L 01/26/17 08:35 1Bromodichloromethane

ND 0.191.0 ug/L 01/26/17 08:35 1Bromoform

ND 0.212.0 ug/L 01/26/17 08:35 1Bromomethane

ND 0.451.0 ug/L 01/26/17 08:35 1Carbon disulfide

ND 0.191.0 ug/L 01/26/17 08:35 1Carbon tetrachloride

ND 0.171.0 ug/L 01/26/17 08:35 1Chlorobenzene

ND 0.412.0 ug/L 01/26/17 08:35 1Chloroethane

ND 0.161.0 ug/L 01/26/17 08:35 1Chloroform

ND 0.302.0 ug/L 01/26/17 08:35 1Chloromethane

ND 0.151.0 ug/L 01/26/17 08:35 1cis-1,2-Dichloroethene

ND 0.161.0 ug/L 01/26/17 08:35 1cis-1,3-Dichloropropene

ND 0.171.0 ug/L 01/26/17 08:35 1Dibromochloromethane

ND 0.171.0 ug/L 01/26/17 08:35 1Dibromomethane

ND 0.161.0 ug/L 01/26/17 08:35 1Ethylbenzene

ND 0.231.0 ug/L 01/26/17 08:35 1Iodomethane

ND 0.325.0 ug/L 01/26/17 08:35 1Methylene Chloride

ND 0.171.0 ug/L 01/26/17 08:35 1Styrene

ND 0.201.0 ug/L 01/26/17 08:35 1Tetrachloroethene

ND 0.171.0 ug/L 01/26/17 08:35 1Toluene

ND 0.151.0 ug/L 01/26/17 08:35 1trans-1,2-Dichloroethene

ND 0.191.0 ug/L 01/26/17 08:35 1trans-1,3-Dichloropropene

ND 0.801.0 ug/L 01/26/17 08:35 1trans-1,4-Dichloro-2-butene

ND 0.161.0 ug/L 01/26/17 08:35 1Trichloroethene

ND 0.292.0 ug/L 01/26/17 08:35 1Trichlorofluoromethane

ND 0.942.0 ug/L 01/26/17 08:35 1Vinyl acetate

ND 0.101.0 ug/L 01/26/17 08:35 1Vinyl chloride

ND 0.192.0 ug/L 01/26/17 08:35 1Xylenes (total)

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MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

88 01/26/17 08:35 14-Bromofluorobenzene (Surr) 78 - 120

97 01/26/17 08:35 1Dibromofluoromethane (Surr) 77 - 120

91 01/26/17 08:35 1Toluene-d8 (Surr) 80 - 125

Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-360061/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 360061

1,1,1,2-Tetrachloroethane 5.00 5.04 ug/L 101 65 - 135

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,1-Trichloroethane 5.00 5.75 ug/L 115 65 - 135

1,1,2,2-Tetrachloroethane 5.00 4.37 ug/L 87 58 - 135

1,1,2-Trichloroethane 5.00 5.02 ug/L 100 64 - 135

1,1-Dichloroethane 5.00 4.94 ug/L 99 65 - 135

1,1-Dichloroethene 5.00 5.05 ug/L 101 65 - 136

1,2,3-Trichloropropane 5.00 5.28 ug/L 106 65 - 135

1,2-Dibromo-3-Chloropropane 5.00 3.59 ug/L 72 57 - 135

1,2-Dibromoethane 5.00 4.52 ug/L 90 65 - 135

1,2-Dichlorobenzene 5.00 5.00 ug/L 100 65 - 135

1,2-Dichloroethane 5.00 5.37 ug/L 107 65 - 135

1,2-Dichloropropane 5.00 4.86 ug/L 97 64 - 135

1,4-Dichlorobenzene 5.00 5.16 ug/L 103 65 - 135

2-Butanone (MEK) 20.0 19.8 ug/L 99 44 - 177

2-Hexanone 20.0 16.4 ug/L 82 57 - 139

4-Methyl-2-pentanone (MIBK) 20.0 17.4 ug/L 87 60 - 150

Acetone 20.0 21.3 ug/L 106 39 - 156

Acrylonitrile 50.0 48.2 ug/L 96 56 - 135

Benzene 5.00 4.97 ug/L 99 65 - 135

Bromochloromethane 5.00 5.13 ug/L 103 65 - 135

Bromodichloromethane 5.00 5.18 ug/L 104 65 - 135

Bromoform 5.00 4.99 ug/L 100 62 - 135

Bromomethane 5.00 5.01 ug/L 100 45 - 135

Carbon disulfide 5.00 5.16 ug/L 103 55 - 143

Carbon tetrachloride 5.00 5.93 ug/L 119 65 - 135

Chlorobenzene 5.00 4.77 ug/L 95 65 - 135

Chloroethane 5.00 4.83 ug/L 97 46 - 136

Chloroform 5.00 5.36 ug/L 107 65 - 135

Chloromethane 5.00 4.51 ug/L 90 34 - 145

cis-1,2-Dichloroethene 5.00 5.17 ug/L 103 65 - 135

cis-1,3-Dichloropropene 5.00 4.68 ug/L 94 65 - 135

Dibromochloromethane 5.00 4.75 ug/L 95 65 - 135

Dibromomethane 5.00 5.07 ug/L 101 65 - 135

Ethylbenzene 5.00 4.82 ug/L 96 65 - 135

Iodomethane 5.00 5.25 ug/L 105 65 - 142

Methylene Chloride 5.00 5.51 ug/L 110 54 - 141

Styrene 5.00 4.82 ug/L 96 65 - 135

Tetrachloroethene 5.00 5.24 ug/L 105 65 - 135

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Toluene 5.00 5.15 ug/L 103 65 - 135

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

trans-1,2-Dichloroethene 5.00 5.37 ug/L 107 65 - 135

trans-1,3-Dichloropropene 5.00 5.07 ug/L 101 65 - 135

trans-1,4-Dichloro-2-butene 5.00 4.39 ug/L 88 53 - 135

Trichloroethene 5.00 5.23 ug/L 105 65 - 135

Trichlorofluoromethane 5.00 5.30 ug/L 106 53 - 137

Vinyl acetate 10.0 9.19 ug/L 92 11 - 187

Vinyl chloride 5.00 4.68 ug/L 94 40 - 137

Xylenes (total) 10.0 9.67 ug/L 97 65 - 135

1,2-Dichloroethane-d4 (Surr) 70 - 127

Surrogate

114

LCS LCS

Qualifier Limits%Recovery

1024-Bromofluorobenzene (Surr) 78 - 120

106Dibromofluoromethane (Surr) 77 - 120

102Toluene-d8 (Surr) 80 - 125

Client Sample ID: Matrix SpikeLab Sample ID: 280-93329-G-1 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360061

1,1,1,2-Tetrachloroethane ND 5.00 4.73 ug/L 95 65 - 135

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,1,1-Trichloroethane ND 5.00 5.10 ug/L 102 65 - 135

1,1,2,2-Tetrachloroethane ND 5.00 4.34 ug/L 87 58 - 135

1,1,2-Trichloroethane ND 5.00 5.01 ug/L 100 64 - 135

1,1-Dichloroethane 0.31 J 5.00 4.99 ug/L 94 65 - 135

1,1-Dichloroethene 2.6 5.00 7.31 ug/L 95 65 - 136

1,2,3-Trichloropropane ND 5.00 5.10 ug/L 102 65 - 135

1,2-Dibromo-3-Chloropropane ND F2 5.00 3.69 ug/L 74 57 - 135

1,2-Dibromoethane ND 5.00 4.62 ug/L 92 65 - 135

1,2-Dichlorobenzene ND 5.00 4.51 ug/L 90 65 - 135

1,2-Dichloroethane 6.3 5.00 11.2 ug/L 97 65 - 135

1,2-Dichloropropane ND 5.00 4.55 ug/L 91 64 - 135

1,4-Dichlorobenzene ND 5.00 4.58 ug/L 92 65 - 135

2-Butanone (MEK) ND 20.0 21.4 ug/L 107 44 - 177

2-Hexanone ND 20.0 19.6 ug/L 98 57 - 139

4-Methyl-2-pentanone (MIBK) ND 20.0 20.6 ug/L 103 60 - 150

Acetone ND 20.0 22.6 ug/L 113 39 - 156

Acrylonitrile ND 50.0 48.5 ug/L 97 56 - 135

Benzene ND 5.00 4.66 ug/L 93 65 - 135

Bromochloromethane ND 5.00 4.92 ug/L 98 65 - 135

Bromodichloromethane ND 5.00 4.94 ug/L 99 65 - 135

Bromoform ND 5.00 4.57 ug/L 91 62 - 135

Bromomethane ND 5.00 5.25 ug/L 105 45 - 135

Carbon disulfide ND 5.00 4.70 ug/L 94 55 - 143

Carbon tetrachloride ND 5.00 5.04 ug/L 101 65 - 135

Chlorobenzene ND 5.00 4.38 ug/L 88 65 - 135

Chloroethane ND 5.00 4.84 ug/L 97 46 - 136

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Client Sample ID: Matrix SpikeLab Sample ID: 280-93329-G-1 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360061

Chloroform ND 5.00 4.96 ug/L 99 65 - 135

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Chloromethane ND 5.00 4.71 ug/L 94 34 - 145

cis-1,2-Dichloroethene 4.6 5.00 9.42 ug/L 95 65 - 135

cis-1,3-Dichloropropene ND 5.00 4.49 ug/L 90 65 - 135

Dibromochloromethane ND 5.00 4.42 ug/L 88 65 - 135

Dibromomethane ND 5.00 5.00 ug/L 100 65 - 135

Ethylbenzene ND 5.00 4.37 ug/L 87 65 - 135

Iodomethane ND 5.00 5.02 ug/L 100 65 - 142

Methylene Chloride ND 5.00 4.78 J ug/L 96 54 - 141

Styrene ND 5.00 4.29 ug/L 86 65 - 135

Tetrachloroethene ND 5.00 4.48 ug/L 90 65 - 135

Toluene ND 5.00 4.76 ug/L 95 65 - 135

trans-1,2-Dichloroethene ND 5.00 5.04 ug/L 101 65 - 135

trans-1,3-Dichloropropene ND 5.00 4.84 ug/L 97 65 - 135

trans-1,4-Dichloro-2-butene ND 5.00 4.61 ug/L 92 53 - 135

Trichloroethene 0.45 J 5.00 5.21 ug/L 95 65 - 135

Trichlorofluoromethane ND 5.00 5.05 ug/L 101 53 - 137

Vinyl acetate ND 10.0 9.38 ug/L 94 11 - 187

Vinyl chloride 1.6 5.00 6.46 ug/L 97 40 - 137

Xylenes (total) ND 10.0 8.62 ug/L 86 65 - 135


Surrogate

109

MS MS





Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-93329-G-1 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360061

1,1,1,2-Tetrachloroethane ND 5.00 5.44 ug/L 109 65 - 135 14 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

1,1,1-Trichloroethane ND 5.00 5.81 ug/L 116 65 - 135 13 20

1,1,2,2-Tetrachloroethane ND 5.00 4.82 ug/L 96 58 - 135 10 20

1,1,2-Trichloroethane ND 5.00 5.55 ug/L 111 64 - 135 10 27

1,1-Dichloroethane 0.31 J 5.00 5.28 ug/L 99 65 - 135 6 21

1,1-Dichloroethene 2.6 5.00 7.72 ug/L 103 65 - 136 5 20

1,2,3-Trichloropropane ND 5.00 5.26 ug/L 105 65 - 135 3 23

1,2-Dibromo-3-Chloropropane ND F2 5.00 4.68 F2 ug/L 94 57 - 135 24 22

1,2-Dibromoethane ND 5.00 4.98 ug/L 100 65 - 135 8 27

1,2-Dichlorobenzene ND 5.00 5.23 ug/L 105 65 - 135 15 20

1,2-Dichloroethane 6.3 5.00 11.8 ug/L 110 65 - 135 5 20

1,2-Dichloropropane ND 5.00 5.07 ug/L 101 64 - 135 11 20

1,4-Dichlorobenzene ND 5.00 5.40 ug/L 108 65 - 135 17 23

2-Butanone (MEK) ND 20.0 23.0 ug/L 115 44 - 177 7 32

2-Hexanone ND 20.0 20.1 ug/L 100 57 - 139 2 25

4-Methyl-2-pentanone (MIBK) ND 20.0 21.5 ug/L 108 60 - 150 4 22

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Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-93329-G-1 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360061

Acetone ND 20.0 21.5 ug/L 107 39 - 156 5 23

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Acrylonitrile ND 50.0 52.7 ug/L 105 56 - 135 8 30

Benzene ND 5.00 5.22 ug/L 104 65 - 135 11 20

Bromochloromethane ND 5.00 5.37 ug/L 107 65 - 135 9 29

Bromodichloromethane ND 5.00 5.51 ug/L 110 65 - 135 11 20

Bromoform ND 5.00 5.20 ug/L 104 62 - 135 13 27

Bromomethane ND 5.00 5.50 ug/L 110 45 - 135 5 33

Carbon disulfide ND 5.00 5.29 ug/L 106 55 - 143 12 20

Carbon tetrachloride ND 5.00 5.88 ug/L 118 65 - 135 15 21

Chlorobenzene ND 5.00 4.96 ug/L 99 65 - 135 12 20

Chloroethane ND 5.00 5.21 ug/L 104 46 - 136 7 25

Chloroform ND 5.00 5.55 ug/L 111 65 - 135 11 20

Chloromethane ND 5.00 5.08 ug/L 102 34 - 145 7 24

cis-1,2-Dichloroethene 4.6 5.00 9.98 ug/L 107 65 - 135 6 20

cis-1,3-Dichloropropene ND 5.00 4.84 ug/L 97 65 - 135 7 26

Dibromochloromethane ND 5.00 5.07 ug/L 101 65 - 135 14 20

Dibromomethane ND 5.00 5.60 ug/L 112 65 - 135 11 26

Ethylbenzene ND 5.00 4.87 ug/L 97 65 - 135 11 20

Iodomethane ND 5.00 5.60 ug/L 112 65 - 142 11 25

Methylene Chloride ND 5.00 5.28 ug/L 106 54 - 141 10 26

Styrene ND 5.00 4.96 ug/L 99 65 - 135 15 26

Tetrachloroethene ND 5.00 5.16 ug/L 103 65 - 135 14 20

Toluene ND 5.00 5.38 ug/L 108 65 - 135 12 20

trans-1,2-Dichloroethene ND 5.00 5.45 ug/L 109 65 - 135 8 24

trans-1,3-Dichloropropene ND 5.00 5.50 ug/L 110 65 - 135 13 26

trans-1,4-Dichloro-2-butene ND 5.00 4.87 ug/L 97 53 - 135 5 25

Trichloroethene 0.45 J 5.00 5.67 ug/L 104 65 - 135 8 20

Trichlorofluoromethane ND 5.00 5.43 ug/L 109 53 - 137 7 27

Vinyl acetate ND 10.0 10.0 ug/L 100 11 - 187 6 24

Vinyl chloride 1.6 5.00 6.71 ug/L 102 40 - 137 4 24

Xylenes (total) ND 10.0 9.85 ug/L 99 65 - 135 13 20


Surrogate

110

MSD MSD





Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 280-359912/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360611 Prep Batch: 359912

RL MDL

Bis(2-ethylhexyl) phthalate ND 6.0 0.56 ug/L 01/25/17 10:11 01/31/17 22:22 1

MB MB


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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)


2-Fluorophenol 86 41 - 135 01/31/17 22:22 1

MB MB

Surrogate

01/25/17 10:11

Dil FacPrepared AnalyzedQualifier Limits%Recovery

79 01/25/17 10:11 01/31/17 22:22 12-Fluorobiphenyl 48 - 135

87 01/25/17 10:11 01/31/17 22:22 1Nitrobenzene-d5 42 - 135

88 01/25/17 10:11 01/31/17 22:22 1Phenol-d5 46 - 135

100 01/25/17 10:11 01/31/17 22:22 1Terphenyl-d14 20 - 135

76 01/25/17 10:11 01/31/17 22:22 12,4,6-Tribromophenol 48 - 135

Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-359912/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360611 Prep Batch: 359912

Bis(2-ethylhexyl) phthalate 80.0 74.0 ug/L 93 65 - 135

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

2-Fluorophenol 41 - 135

Surrogate

80

LCS LCS


852-Fluorobiphenyl 48 - 135

86Nitrobenzene-d5 42 - 135

82Phenol-d5 46 - 135

94Terphenyl-d14 20 - 135

882,4,6-Tribromophenol 48 - 135

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-359912/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360611 Prep Batch: 359912

Bis(2-ethylhexyl) phthalate 80.0 77.8 ug/L 97 65 - 135 5 30

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

2-Fluorophenol 41 - 135

Surrogate

89

LCSD LCSD


922-Fluorobiphenyl 48 - 135

94Nitrobenzene-d5 42 - 135

90Phenol-d5 46 - 135

97Terphenyl-d14 20 - 135

882,4,6-Tribromophenol 48 - 135

Method: 6010B - Metals (ICP)


RL MDL

Antimony ND 20 5.2 ug/L 01/25/17 14:30 01/26/17 01:12 1

MB MB


ND 0.82100 ug/L 01/25/17 14:30 01/26/17 01:12 1Barium

ND 0.471.0 ug/L 01/25/17 14:30 01/26/17 01:12 1Beryllium

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Method: 6010B - Metals (ICP) (Continued)


RL MDL

Cadmium ND 5.0 0.45 ug/L 01/25/17 14:30 01/26/17 01:12 1

MB MB


36.5 J 35200 ug/L 01/25/17 14:30 01/26/17 01:12 1Calcium

1.47 J 0.6610 ug/L 01/25/17 14:30 01/26/17 01:12 1Chromium

ND 1.210 ug/L 01/25/17 14:30 01/26/17 01:12 1Cobalt

ND 4.215 ug/L 01/25/17 14:30 01/26/17 01:12 1Copper

ND 22100 ug/L 01/25/17 14:30 01/26/17 01:12 1Iron

ND 2.75.0 ug/L 01/25/17 14:30 01/26/17 01:12 1Lead

ND 11200 ug/L 01/25/17 14:30 01/26/17 01:12 1Magnesium

ND 0.2615 ug/L 01/25/17 14:30 01/26/17 01:12 1Manganese

ND 2.612 ug/L 01/25/17 14:30 01/26/17 01:12 1Nickel

ND 2403000 ug/L 01/25/17 14:30 01/26/17 01:12 1Potassium

ND 0.9310 ug/L 01/25/17 14:30 01/26/17 01:12 1Silver

ND 1205000 ug/L 01/25/17 14:30 01/26/17 01:12 1Sodium

ND 4.520 ug/L 01/25/17 14:30 01/26/17 01:12 1Zinc


Antimony 500 479 ug/L 96 88 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 2000 1930 ug/L 96 90 - 112

Beryllium 50.0 47.0 ug/L 94 89 - 113

Cadmium 100 95.1 ug/L 95 88 - 111

Calcium 50000 47400 ug/L 95 90 - 111

Chromium 200 192 ug/L 96 90 - 113

Cobalt 500 465 ug/L 93 89 - 111

Copper 250 251 ug/L 101 86 - 112

Iron 1000 949 ug/L 95 89 - 115

Lead 500 469 ug/L 94 89 - 110

Magnesium 50000 45800 ug/L 92 90 - 113

Manganese 500 452 ug/L 90 90 - 110

Nickel 500 460 ug/L 92 89 - 111

Potassium 50000 49200 ug/L 98 89 - 114

Silver 50.0 48.1 ug/L 96 86 - 115

Sodium 50000 49000 ug/L 98 90 - 115

Zinc 500 435 ug/L 87 85 - 111

Client Sample ID: MW-08SRLab Sample ID: 280-93303-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360084 Prep Batch: 359900

Antimony ND 500 476 ug/L 95 81 - 124

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 38 J 2000 1980 ug/L 97 85 - 120

Beryllium 4.6 50.0 52.4 ug/L 96 79 - 121

Cadmium 1.2 J 100 96.1 ug/L 95 82 - 119

Calcium 26000 B 50000 73800 ug/L 96 48 - 153

Chromium 1.7 J B 200 192 ug/L 95 73 - 135

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Method: 6010B - Metals (ICP) (Continued)

Client Sample ID: MW-08SRLab Sample ID: 280-93303-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360084 Prep Batch: 359900

Cobalt 28 500 490 ug/L 92 82 - 119

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Copper ND 250 254 ug/L 101 82 - 129

Iron 2100 F1 1000 3560 ug/L 149 52 - 155

Lead 4.2 J 500 468 ug/L 93 89 - 121

Magnesium 24000 50000 70500 ug/L 92 62 - 146

Manganese 110 500 562 ug/L 90 79 - 121

Nickel 36 500 493 ug/L 91 84 - 120

Potassium 3100 50000 52500 ug/L 99 76 - 132

Silver ND 50.0 47.7 ug/L 95 75 - 141

Sodium 27000 50000 75700 ug/L 97 70 - 203

Zinc 80 500 518 ug/L 88 60 - 137

Client Sample ID: MW-08SRLab Sample ID: 280-93303-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360084 Prep Batch: 359900

Antimony ND 500 475 ug/L 95 81 - 124 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 38 J 2000 1970 ug/L 97 85 - 120 0 20

Beryllium 4.6 50.0 52.3 ug/L 96 79 - 121 0 20

Cadmium 1.2 J 100 96.2 ug/L 95 82 - 119 0 20

Calcium 26000 B 50000 74700 ug/L 97 48 - 153 1 20

Chromium 1.7 J B 200 191 ug/L 95 73 - 135 0 20

Cobalt 28 500 490 ug/L 92 82 - 119 0 20

Copper ND 250 252 ug/L 101 82 - 129 1 20

Iron 2100 F1 1000 3640 F1 ug/L 157 52 - 155 2 20

Lead 4.2 J 500 466 ug/L 92 89 - 121 0 20

Magnesium 24000 50000 71300 ug/L 94 62 - 146 1 20

Manganese 110 500 564 ug/L 91 79 - 121 0 20

Nickel 36 500 494 ug/L 92 84 - 120 0 20

Potassium 3100 50000 52700 ug/L 99 76 - 132 0 20

Silver ND 50.0 48.4 ug/L 97 75 - 141 2 20

Sodium 27000 50000 76500 ug/L 98 70 - 203 1 20

Zinc 80 500 518 ug/L 88 60 - 137 0 20

Method: 6020 - Metals (ICP/MS)


RL MDL

Arsenic ND 10 0.33 ug/L 01/25/17 14:30 01/25/17 21:56 1

MB MB


ND 0.705.0 ug/L 01/25/17 14:30 01/25/17 21:56 1Selenium

ND 0.0501.0 ug/L 01/25/17 14:30 01/25/17 21:56 1Thallium

ND 0.505.0 ug/L 01/25/17 14:30 01/25/17 21:56 1Vanadium

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Method: 6020 - Metals (ICP/MS) (Continued)


Arsenic 40.0 41.3 ug/L 103 85 - 117

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Selenium 40.0 41.1 ug/L 103 77 - 122

Thallium 40.0 40.3 ug/L 101 85 - 118

Vanadium 40.0 42.3 ug/L 106 85 - 120

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-359902/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 360085 Prep Batch: 359902

Arsenic 40.0 42.9 ug/L 107 85 - 117 4 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Selenium 40.0 41.3 ug/L 103 77 - 122 0 20

Thallium 40.0 40.8 ug/L 102 85 - 118 1 20

Vanadium 40.0 42.2 ug/L 105 85 - 120 0 20

Client Sample ID: MW-08DLab Sample ID: 280-93303-1 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360085 Prep Batch: 359902

Arsenic 2.1 J 40.0 45.1 ug/L 107 85 - 117

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Selenium ND 40.0 41.3 ug/L 103 77 - 122

Thallium ND 40.0 40.3 ug/L 101 85 - 118

Vanadium ND 40.0 43.6 ug/L 109 85 - 120

Client Sample ID: MW-08DLab Sample ID: 280-93303-1 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360085 Prep Batch: 359902

Arsenic 2.1 J 40.0 45.8 ug/L 109 85 - 117 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Selenium ND 40.0 41.1 ug/L 103 77 - 122 1 20

Thallium ND 40.0 40.7 ug/L 102 85 - 118 1 20

Vanadium ND 40.0 42.4 ug/L 106 85 - 120 3 20

Method: 300.0 - Anions, Ion Chromatography


RL MDL

Chloride ND 0.60 0.25 mg/L 01/25/17 10:31 1

MB MB


ND 0.235.0 mg/L 01/25/17 10:31 1Sulfate

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Method: 300.0 - Anions, Ion Chromatography (Continued)


Chloride 100 103 mg/L 103 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Sulfate 100 103 mg/L 103 90 - 110

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-359944/5Matrix: Water Prep Type: Total/NAAnalysis Batch: 359944

Chloride 100 103 mg/L 103 90 - 110 0 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Sulfate 100 103 mg/L 103 90 - 110 0 10

Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-359944/3Matrix: Water Prep Type: Total/NAAnalysis Batch: 359944

Chloride 2.50 2.57 J mg/L 103 50 - 150

Analyte

MRL MRL


Spike

Added

%Rec.

Limits

Sulfate 2.50 2.37 J mg/L 95 50 - 150

Client Sample ID: Matrix SpikeLab Sample ID: 280-93306-A-6 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 359944

Chloride 11 25.0 37.4 mg/L 105 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Sulfate 8.0 25.0 34.5 mg/L 106 80 - 120

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-93306-A-6 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 359944

Chloride 11 25.0 37.5 mg/L 105 80 - 120 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Sulfate 8.0 25.0 34.7 mg/L 106 80 - 120 0 20

Client Sample ID: DuplicateLab Sample ID: 280-93306-A-6 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 359944

Chloride 11 11.3 mg/L 0 15

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Sulfate 8.0 8.04 mg/L 0.08 15

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Method: 350.1 - Nitrogen, Ammonia


RL MDL

Ammonia as N ND 0.10 0.022 mg/L 01/26/17 13:31 1

MB MB



Ammonia as N 2.50 2.52 mg/L 101 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-360179/19Matrix: Water Prep Type: Total/NAAnalysis Batch: 360179

Ammonia as N 2.50 2.30 mg/L 92 90 - 110 9 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Matrix SpikeLab Sample ID: 280-93321-J-16 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360179

Ammonia as N 0.035 J 1.00 1.13 mg/L 110 90 - 110

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-93321-J-16 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360179

Ammonia as N 0.035 J 1.00 1.13 mg/L 110 90 - 110 0 10

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: SM 2320B - Alkalinity


RL MDL

Total Alkalinity ND 5.0 1.1 mg/L 01/25/17 09:15 1

MB MB


ND 1.15.0 mg/L 01/25/17 09:15 1Bicarbonate Alkalinity

ND 1.15.0 mg/L 01/25/17 09:15 1Carbonate Alkalinity


Total Alkalinity 200 201 mg/L 100 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: SM 2320B - Alkalinity (Continued)

Client Sample ID: DuplicateLab Sample ID: 280-93135-A-5 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 359982

Total Alkalinity 47 46.9 mg/L 0.8 10

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: SM 2540C - Solids, Total Dissolved (TDS)


RL MDL

Total Dissolved Solids ND 5.4 4.7 mg/L 01/26/17 09:24 1

MB MB



Total Dissolved Solids 500 489 mg/L 98 86 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: MW-08SRLab Sample ID: 280-93303-2 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 360103

Total Dissolved Solids 390 381 mg/L 3 10

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: SM 5310B - Organic Carbon, Total (TOC)


RL MDL

Total Organic Carbon - Average 0.185 J 1.0 0.16 mg/L 01/25/17 14:20 1

MB MB



Total Organic Carbon - Average 25.0 23.2 mg/L 93 88 - 112

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 280-93250-D-1 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 360090

Total Organic Carbon - Average 1.3 B 25.0 24.4 mg/L 92 88 - 112

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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Method: SM 5310B - Organic Carbon, Total (TOC) (Continued)

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-93250-D-1 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 360090

Total Organic Carbon - Average 1.3 B 25.0 24.5 mg/L 93 88 - 112 0 15

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

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QC Association SummaryTestAmerica Job ID: 280-93303-1Client: Waste Management


GC/MS VOA

Analysis Batch: 360061

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B280-93303-1 MW-08D Total/NA

Water 8260B280-93303-2 MW-08SR Total/NA

Water 8260B280-93303-3 TRIP BLANK Total/NA

Water 8260BMB 280-360061/6 Method Blank Total/NA

Water 8260BLCS 280-360061/4 Lab Control Sample Total/NA

Water 8260B280-93329-G-1 MS Matrix Spike Total/NA

Water 8260B280-93329-G-1 MSD Matrix Spike Duplicate Total/NA

GC/MS Semi VOA

Prep Batch: 359912


Water 3520C280-93303-1 MW-08D Total/NA

Water 3520C280-93303-2 MW-08SR Total/NA

Water 3520CMB 280-359912/1-A Method Blank Total/NA

Water 3520CLCS 280-359912/2-A Lab Control Sample Total/NA

Water 3520CLCSD 280-359912/3-A Lab Control Sample Dup Total/NA



Water 8270C 359912280-93303-1 MW-08D Total/NA

Water 8270C 359912MB 280-359912/1-A Method Blank Total/NA

Water 8270C 359912LCS 280-359912/2-A Lab Control Sample Total/NA

Water 8270C 359912LCSD 280-359912/3-A Lab Control Sample Dup Total/NA



Water 8270C 359912280-93303-2 MW-08SR Total/NA

Metals

Prep Batch: 359900


Water 3010A280-93303-1 MW-08D Total/NA

Water 3010A280-93303-2 MW-08SR Total/NA

Water 3010AMB 280-359900/1-A Method Blank Total/NA

Water 3010ALCS 280-359900/2-A Lab Control Sample Total/NA

Water 3010A280-93303-2 MS MW-08SR Total/NA

Water 3010A280-93303-2 MSD MW-08SR Total/NA

Prep Batch: 359902


Water 3020A280-93303-1 MW-08D Total/NA

Water 3020A280-93303-2 MW-08SR Total/NA

Water 3020AMB 280-359902/1-A Method Blank Total/NA

Water 3020ALCS 280-359902/2-A Lab Control Sample Total/NA

Water 3020ALCSD 280-359902/3-A Lab Control Sample Dup Total/NA

Water 3020A280-93303-1 MS MW-08D Total/NA

Water 3020A280-93303-1 MSD MW-08D Total/NA

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Metals (Continued)



Water 6010B 359900280-93303-1 MW-08D Total/NA

Water 6010B 359900280-93303-2 MW-08SR Total/NA

Water 6010B 359900MB 280-359900/1-A Method Blank Total/NA

Water 6010B 359900LCS 280-359900/2-A Lab Control Sample Total/NA

Water 6010B 359900280-93303-2 MS MW-08SR Total/NA

Water 6010B 359900280-93303-2 MSD MW-08SR Total/NA



Water 6020 359902280-93303-1 MW-08D Total/NA

Water 6020 359902280-93303-2 MW-08SR Total/NA

Water 6020 359902MB 280-359902/1-A Method Blank Total/NA

Water 6020 359902LCS 280-359902/2-A Lab Control Sample Total/NA

Water 6020 359902LCSD 280-359902/3-A Lab Control Sample Dup Total/NA

Water 6020 359902280-93303-1 MS MW-08D Total/NA

Water 6020 359902280-93303-1 MSD MW-08D Total/NA

General Chemistry



Water 300.0280-93303-1 MW-08D Total/NA


Water 300.0280-93303-2 MW-08SR Total/NA


Water 300.0MB 280-359944/6 Method Blank Total/NA

Water 300.0LCS 280-359944/4 Lab Control Sample Total/NA

Water 300.0LCSD 280-359944/5 Lab Control Sample Dup Total/NA

Water 300.0MRL 280-359944/3 Lab Control Sample Total/NA

Water 300.0280-93306-A-6 MS Matrix Spike Total/NA

Water 300.0280-93306-A-6 MSD Matrix Spike Duplicate Total/NA

Water 300.0280-93306-A-6 DU Duplicate Total/NA



Water SM 2320B280-93303-1 MW-08D Total/NA

Water SM 2320B280-93303-2 MW-08SR Total/NA

Water SM 2320BMB 280-359982/5 Method Blank Total/NA

Water SM 2320BLCS 280-359982/4 Lab Control Sample Total/NA

Water SM 2320B280-93135-A-5 DU Duplicate Total/NA



Water SM 5310B280-93303-1 MW-08D Total/NA

Water SM 5310B280-93303-2 MW-08SR Total/NA

Water SM 5310BMB 280-360090/13 Method Blank Total/NA

Water SM 5310BLCS 280-360090/12 Lab Control Sample Total/NA

Water SM 5310B280-93250-D-1 MS Matrix Spike Total/NA

Water SM 5310B280-93250-D-1 MSD Matrix Spike Duplicate Total/NA

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General Chemistry (Continued)



Water SM 2540C280-93303-1 MW-08D Total/NA

Water SM 2540C280-93303-2 MW-08SR Total/NA

Water SM 2540CMB 280-360103/1 Method Blank Total/NA

Water SM 2540CLCS 280-360103/2 Lab Control Sample Total/NA

Water SM 2540C280-93303-2 DU MW-08SR Total/NA





Water 350.1MB 280-360179/20 Method Blank Total/NA

Water 350.1LCS 280-360179/18 Lab Control Sample Total/NA

Water 350.1LCSD 280-360179/19 Lab Control Sample Dup Total/NA

Water 350.1280-93321-J-16 MS Matrix Spike Total/NA

Water 350.1280-93321-J-16 MSD Matrix Spike Duplicate Total/NA

Field Service / Mobile Lab



Water Field Sampling280-93303-1 MW-08D Total/NA

Water Field Sampling280-93303-2 MW-08SR Total/NA

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Lab ChronicleClient: Waste Management TestAmerica Job ID: 280-93303-1Project/Site: 667|Jefferson County LF

Client Sample ID: MW-08D Lab Sample ID: 280-93303-1Matrix: WaterDate Collected: 01/23/17 13:12

Date Received: 01/24/17 10:15

Analysis 8260B DPI01/26/17 16:001 TAL DEN360061

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 20 mL 20 mL

Prep 3520C 359912 01/25/17 10:11 ACW TAL DENTotal/NA 1039.8 mL 1 mL

Analysis 8270C 1 360611 02/01/17 05:27 AFH TAL DENTotal/NA

Prep 3010A 359900 01/25/17 14:30 SEJ TAL DENTotal/NA 50 mL 50 mL

Analysis 6010B 1 360084 01/26/17 01:16 CDH TAL DENTotal/NA


Analysis 6020 1 360085 01/25/17 22:11 LMT TAL DENTotal/NA

Analysis 300.0 1 359944 01/25/17 12:00 AFB TAL DENTotal/NA 5 mL 5 mL


Analysis 350.1 1 360179 01/26/17 14:38 MAS TAL DENTotal/NA

Analysis SM 2320B 1 359982 01/25/17 09:53 MMC TAL DENTotal/NA

Analysis SM 2540C 1 360103 01/26/17 09:24 JAP TAL DENTotal/NA 100 mL 100 mL

Analysis SM 5310B 1 360090 01/25/17 15:53 CCJ TAL DENTotal/NA

Analysis Field Sampling 1 359911 01/23/17 12:12 PS1 TAL DENTotal/NA

Client Sample ID: MW-08SR Lab Sample ID: 280-93303-2Matrix: WaterDate Collected: 01/23/17 14:38



Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil


Prep 3520C 359912 01/25/17 10:11 ACW TAL DENTotal/NA 1040.9 mL 1 mL

Analysis 8270C 1 360894 02/02/17 19:40 DCK TAL DENTotal/NA


Analysis 6010B 1 360084 01/26/17 01:19 CDH TAL DENTotal/NA


Analysis 6020 1 360085 01/25/17 22:30 LMT TAL DENTotal/NA



Analysis 350.1 1 360179 01/26/17 14:40 MAS TAL DENTotal/NA

Analysis SM 2320B 1 359982 01/25/17 09:57 MMC TAL DENTotal/NA

Analysis SM 2540C 1 360103 01/26/17 09:24 JAP TAL DENTotal/NA 100 mL 100 mL

Analysis SM 5310B 1 360090 01/25/17 16:09 CCJ TAL DENTotal/NA

Analysis Field Sampling 1 359911 01/23/17 13:38 PS1 TAL DENTotal/NA

Client Sample ID: TRIP BLANK Lab Sample ID: 280-93303-3Matrix: WaterDate Collected: 01/23/17 00:00



Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil


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Lab ChronicleClient: Waste Management TestAmerica Job ID: 280-93303-1Project/Site: 667|Jefferson County LF

Laboratory References:

TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100

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Login Sample Receipt Checklist

Client: Waste Management Job Number: 280-93303-1

Login Number: 93303

Question Answer Comment

Creator: White, Denise E

List Source: TestAmerica Denver

List Number: 1

N/ARadioactivity either was not measured or, if measured, is at or below background

TrueThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

FalseThere are no discrepancies between the sample IDs on the containers and the COC.

No: Received Trip Blank(s) not listed on COC.

TrueSamples are received within Holding Time (Excluding tests with immediate HTs)..

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

TrueIf necessary, staff have been informed of any short hold time or quick TAT needs

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

TrueSampling Company provided.

TrueSamples received within 48 hours of sampling.

TrueSamples requiring field filtration have been filtered in the field.

TrueChlorine Residual checked.


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