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Page 1: Metaproteomic characterization of dissolved organic matter in coastal seawater

SHORT CONTRIBUTION

Metaproteomic characterization of dissolved organic matterin coastal seawater

Mitsuhiro Yoshida • Keitaro Yamamoto •

Satoru Suzuki

Received: 13 June 2013 / Revised: 19 November 2013 / Accepted: 10 December 2013 / Published online: 29 December 2013

� The Oceanographic Society of Japan and Springer Japan 2013

Abstract We performed a comprehensive metaproteomic

analysis of the dissolved organic matter (DOM) in Japanese

coastal waters using liquid chromatography–tandem mass

spectrometry and demonstrated that these proteomes were

characterized by proteins with various functions, including

metabolic enzymes, membranes, and photosynthetic pro-

teins. The protein sources included cyanobacteria, hetero-

trophic bacteria, and eukaryotic phytoplankton. Most of the

components were similar among samples and also similar

to pelagic components. We also observed differences in the

compositions of the microbial communities of origin

among the different dissolved protein samples and differ-

ences in the relative abundance of specific dissolved pro-

tein types (e.g., cytoskeletal proteins), possibly indicating

potential dynamics in the coastal DOM pool.

Keywords Dissolved organic matter � Dissolved

proteins � Proteomics � LC–MS/MS � Microbial loop �Coastal area

1 Introduction

Dissolved organic matter (DOM) in seawater is the largest

pool of organic matter in the oceanic carbon and nitrogen

cycles (Siegenthaler and Sarmiento 1993), and it plays

important roles in utilization and production by heterotro-

phic bacteria and the subsequent food-web processes in the

marine microbial loop (e.g., Ducklow 2002). Among the

high-molecular-weight DOM ([1 kDa) in seawater, dis-

solved proteins are essential sources of nitrogen and energy

acquisition for heterotrophic bacterial production through

the microbial loop. These dissolved proteins are derived

from proteins that contain 85 % of the organic nitrogen in

marine organisms (Tanoue 1995). Thus, the proteins from

marine organisms are eventually transferred to the dis-

solved pool via biogeochemical processes; however, the

processes involved in the production and fate of marine

dissolved proteins and the source organisms for these

proteins are not yet well understood.

Regarding the protein species dissolved in seawater,

Tanoue et al. (1995) first reported that specific bacterial

porin proteins are ubiquitously distributed in the ocean. His

coworkers then expanded this research to include other

protein species (Yamada and Tanoue 2003) and to identify

the source bacterial groups for dissolved proteins (Suzuki

et al. 2000). Throughout the 1990s, gel electrophoresis,

western blotting, and N-terminal sequencing were the main

approaches used to study dissolved proteins (Suzuki et al.

1997; Tanoue et al. 1995; Yamada and Tanoue 2003).

Following recent advances in comprehensive ‘omics’

studies, the metaproteomic approach of using the liquid

chromatography–tandem mass spectrometry (LC–MS/MS)

method allows us to detect expressed proteins and thus

verify microbial functions in situ in various environments,

including marine waters (Morris et al. 2010; Sowell et al.

Electronic supplementary material The online version of thisarticle (doi:10.1007/s10872-013-0212-6) contains supplementarymaterial, which is available to authorized users.

M. Yoshida � K. Yamamoto � S. Suzuki

Center for Marine Environmental Studies (CMES), Ehime

University, 3 Bunkyo-cho, Matsuyama, Ehime 790-8577, Japan

Present Address:

M. Yoshida (&)

Japan Agency for Marine-Earth Science and Technology

(JAMSTEC), 2-15 Natsushima-cho, Yokosuka,

Kanagawa 237-0061, Japan

e-mail: [email protected]

123

J Oceanogr (2014) 70:105–113

DOI 10.1007/s10872-013-0212-6

Page 2: Metaproteomic characterization of dissolved organic matter in coastal seawater

2009, 2011). Using this technique, the specific proteomes

of the DOM fractions in seawater were recently charac-

terized in the pelagic environment (Dong et al. 2013;

Powell et al. 2005; Wang et al. 2011). In contrast, little

effort has been devoted to the proteomic content of the

dissolved fraction in coastal areas (Dong et al. 2013).

Coastal marine ecosystems have high biological activity,

abundant biomass, and various DOM sources that are

unlikely to be observed in oceanic pelagic ecosystems.

These considerations suggest that a wide variety of marine

dissolved proteins in the coastal ecosystem may possibly

be derived not only from marine biota but also from ter-

restrial sources.

To investigate the biological origin and chemical char-

acterization of these coastal dissolved proteins, we per-

formed an LC–MS/MS-based metaproteomic analysis of

the dissolved proteins in Japanese coastal waters. To our

knowledge, this study is the first report to describe the

comprehensive characteristics of dissolved proteins in

various coastal environments, including intensive sampling

locations in an inland sea where a red-tide bloom was

observed.

2 Materials and methods

2.1 Sample collection and preparation of dissolved

proteins in coastal DOM

Surface seawater samples (20 L) were collected at stations

(Stns) U1 (32�930N, 132�570E), U2 (32�950N, 132�570E),

and U3 (32�960N, 132�570E) in the Uwa Sea and at Stn H

(33�900N, 132�740E) in Horie Port, Matsuyama, Ehime

Prefecture, Japan (Fig. 1). The sampling at Stns U1-3 and

H was conducted on June 1 and October 6, 2010, respec-

tively. Stns U1 and U2 are located near fish farms. Blooms

of the red-tide dinoflagellate Gymnodinium-like cells were

observed at Stn U3 during the sampling (Fig. S1).

Each seawater sample was filtered with a plankton net

(mesh size 150 lm) immediately after sampling and

poured into a 20-L sampling bag. The concentration and

desalting of dissolved proteins were carried out according

to the procedures of Tanoue (1995). Sodium azide [NaN3

100 lM (w/v)] and sodium dodecyl sulfate [SDS 0.01 %

(w/v)] were added to the filtrates to prevent bacterial

growth and to help solubilize the proteins, respectively.

Then, the filtrates were further filtered through a 0.2-lm

cartridge filter (Advantec Toyo, Tokyo, Japan) to remove

particulates and microorganisms. Dissolved proteins in the

filtrate were concentrated using a Pellicon 2 cassette tan-

gential flow filtration system equipped with two 10-kDa

regenerated cellulose filter cassettes (Millipore, Billerica,

MA, USA). The concentrate was desalted with 0.01 %

(w/v) SDS/35 mM ammonium bicarbonate rinsing solution

(pH 7.8).

Bovine serum albumin (BSA 66.4 kD) was used as a

standard protein to evaluate the recovery of DOM by the

tangential flow filtration system. Seawater that had been

prefiltered through the 0.2-lm cartridge filter was spiked

with the BSA standard. The spiked solution was then run

through the Pellicon 2 cassette tangential flow filtration

system according to the procedure described above.

Quantification of the standard BSA added in the recovery

experiments was performed by densitometric measurement

of the band detected in SDS–PAGE analysis (see details

below). The recovery of the standard protein by the tan-

gential flow filtration system was 19–34 %.

Dissolved proteins in the concentrate from tangential

flow filtration were precipitated with ice-cold 10 % tri-

chloroacetic acid (TCA) for at least 12 h at 4 �C (Suzuki

et al. 1997; Tanoue 1995). The TCA-insoluble fraction was

centrifuged at 14,000g for 30 min at 4 �C, and then the

pellets were washed sequentially with 100 % ethanol and

100 % diethyl ether and were air-dried. Each dried pellet of

dissolved protein samples was redissolved in a sample

buffer solution of 62.5 mM Tris–HCl (pH 6.8), 2 % (w/v)

SDS, 5 % (v/v) 2-mercaptoethanol, and 10 % (w/v) glyc-

erol, heated to 95 �C, and maintained at this temperature

for 3 min. The sample was then analyzed using SDS–

polyacrylamide gel electrophoresis (SDS–PAGE).

2.2 One-dimensional SDS–PAGE of dissolved proteins

The rehydrated dissolved protein concentrate was loaded

onto a 14 % Bis–Tris gel according to the method of

Laemmli (1970). Electrophoresis was run at 20 mA in a

Tris–glycine-SDS buffer electrode solution. Low-molecu-

lar-weight markers were used for reference. After electro-

phoresis, the proteins in the gel were stained with colloidal

Coomassie Brilliant Blue-R250 (CBB-R; Bio-Rad, Hercu-

les, CA, USA).

2.3 N-terminal amino acid sequence analysis

Proteins in the bands detected by SDS–PAGE were sub-

jected to N-terminal amino acid sequencing. After the

SDS–PAGE separation, the proteins in the gel were

transferred onto a polyvinylidene difluoride (PVDF)

membrane (Immobilon-PSQ transfer membrane; Millipore)

at 40 mA for 45 min with a blotting device. Protein spots

on the membrane were visualized by the CBB-R250 (Bio-

Rad) staining method. The stained spots were cut out, and

the N-terminal amino acid sequence was determined using

an automated protein sequencer (ABI Procise 491HT;

Applied Biosystems, Foster City, CA, USA). The sequence

obtained from each protein spot was subjected to a

106 M. Yoshida et al.

123

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BLASTp homology search against the NCBI GenBank

nonredundant (nr) protein database (Altschul et al. 1997).

2.4 Enzymatic digestion of dissolved proteins

For the ‘‘shotgun’’ proteomics experiments (Dong et al.

2009, 2013; Wang et al. 2011), the SDS–PAGE gel was cut

into seven pieces based on molecular weight marker size

([97.2, 97.2–66.4, 66.4–45.0, 45.0–29.0, 29.0–20.1,

20.1–14.3, and \14.3 kDa) to isolate molecular weight

fractions, and the pieces were subjected to enzymatic

digestion with the endoproteinase trypsin (in-gel digestion;

Wilm et al. 1996). Briefly, the gel pieces were destained

and dehydrated. After dithiothreitol reduction and iodoa-

cetamide alkylation, the trypsin solution (modified

sequencing grade; Promega, Madison, WI, USA; 10 lg/

mL) was added, and the pieces were incubated at 37 �C

overnight. In-gel digests were extracted with 50 % (v/v)

acetonitrile/5 % (v/v) trifluoroacetic acid rinses to recover

peptides, and the extracts were dried in a SpeedVac and

stored in a freezer (-20 �C) until LC–MS/MS analysis.

2.5 Mass spectrometry analysis

A tandem mass spectrometry (MS/MS) measurement was

performed using an in-line high-performance liquid chro-

matography (LC) system composed of a Paradigm MS4

microflow LC pump (Michrom BioResources, Auburn,

CA, USA) and an HTC PAL auto-sampler (CTC Analytics,

Zwingen, Switzerland) connected to an ion trap mass

spectrometer (LCQ Advantage; Thermo Finnigan, San

Jose, CA, USA). Briefly, the peptide extracts from the gel

Fig. 1 Sampling stations in the

Uwa Sea (Stns U1–3) and Horie

Port (Stn H), Japan

Metaproteomics of dissolved organic matter in coastal water 107

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Page 4: Metaproteomic characterization of dissolved organic matter in coastal seawater

sample were injected onto a peptide CapTrap column

(0.5 9 2 mm, Michrom BioResources). The peptides were

eluted from the trap and subsequently separated on a C18

reverse-phase column (0.2 9 50 mm, packed with 3-lm

Magic C18 AQ particles; Michrom BioResources) with a

100-min linear gradient of 3–65 % mobile phase B [90 %

(v/v) acetonitrile/0.1 % (v/v) formic acid] in mobile phase

A [2 % (v/v) acetonitrile/0.1 % (v/v) formic acid] over

120 min at a flow rate of 2 lL/min. The separated sample

was introduced into the mass spectrometer via a fused-

silica Fortis Tip emitter (AMR, Tokyo, Japan). The LTQ

mass spectrometer operated with the following parameters:

spray voltage, 2.5 kV; spray temperature, 200 �C; and full

scan m/z range 450–2,000. The LC–MS system was fully

automated and under the direct control of the Xcalibur

software system (v.1.3; Thermo Finnigan).

2.6 Bioinformatic analysis

To identify the coastal dissolved proteins and their bio-

logical origins by the MS/MS analysis, the datasets of

protein sequences from the microbial taxa that possibly

contribute to the marine DOM pool were selected from the

GenBank nr protein database, and an original protein

database for the analysis was constructed. The proteins

from bacteria were classified broadly into five subgroups:

Cyanobacteria, a-Proteobacteria, b-Proteobacteria, c-Pro-

teobacteria, and a Bacteroidetes/Chlorobi group, and the

proteins from eukaryotic algae were classified into five

subgroups: Dinophyta, Cryptophyta, Haptophyta, Bacilla-

riophyta, and Chlorophyta. Proteins from other taxonomic

groups, including Archaea, Crustacea, and Stramenopiles,

were also used in this study.

The proteins related to the MS/MS spectra data obtained

by the mass spectrometry were identified by a similarity

search against the NCBI nr protein database from the

selected biological taxa mentioned above, using the SE-

QUEST algorithm (Thermo Finnigan). All SEQUEST

searches were performed using Bioworks software (v.3.1;

Thermo Finnigan), with the following parameters: fully

tryptic peptide, parent mass tolerance = 1.4, and peptide

mass tolerance = 1.5. The protein identification criteria

were applied based on a Delta CN ([0.1) and Xcorr (one

charge [1.9; two charges [2.2; three charges [3.75).

The integration of identified peptide hits into a related

protein was conducted with the in-house software Build-

Summary. Redundant proteins having the same peptide

hit(s) in a biological taxon were removed. The functional

assignments of the proteins identified were determined

according to the Kyoto encyclopedia of genes and genomes

(KEGG) classification system (http://www.genome.jp/

kegg/) (Kanehisa et al. 2008).

3 Results

3.1 SDS–PAGE

The profiles of the SDS–PAGE results for the dissolved

proteins from the four sampling sites (Stns U1, U2, U3, and

H) are shown in Fig. 2. The lanes of the U1, U2, and H

samples displayed a smeared staining pattern, and some

bands were observed with a smeared background. In con-

trast, the U3 sample displayed three distinct bands (namely

X, Y, and Z) within the 45.0–66.4 kDa molecular weight

range.

The protein sample from band X was subjected to

N-terminal amino acid sequencing, which indicated a

sequence of N-KHVAGEFTTG-C. This sequence did not

match reference sequences in the NCBI GenBank nr pro-

tein database. The samples from the other two bands (Y and

Z) did not yield enough protein for N-terminal amino acid

sequence analysis.

3.2 LC–MS/MS analysis

We used LC–MS/MS to identify proteins extracted from

the SDS–PAGE gel. For the above-mentioned bands, the

MS/MS spectra data matched the peptide sequences of

multiple proteins in the public database. Using the MS-

based ‘‘shotgun’’ method for gel slice sampling (Dong et al.

2009, 2013; Wang et al. 2011), the data of the MS/MS

Fig. 2 The SDS–PAGE electrophoretogram of the dissolved

proteins of the four coastal DOM samples. The left lane is a

molecular weight standard

108 M. Yoshida et al.

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spectra obtained were processed, and the peptide sequences

in each fraction were identified. A total of 1,175 proteins,

each identified by one or more peptides in the samples,

were found in the four samples. The maximum number of

proteins (346 proteins) was observed in sample U3,

whereas the minimum number (192 proteins) was observed

in sample U1, which was located at an offshore site.

3.3 Biological sources of dissolved proteins

The taxonomic composition of the biological groups

derived from the identified dissolved proteins is shown in

Fig. 3. A wide variety of microbial taxa were identified,

including a-, b-, and c-Proteobacteria, Cyanobacteria,

Chlorophyta, the Bacteroidetes/Chlorobi group, Archaea,

viruses, and Stramenopiles. These taxa were abundantly

distributed among the four coastal water sites, accounting

for 85–95 % of the total number of identified proteins. In

contrast, the dissolved proteins associated with the

eukaryotic plankton from Bacillariophyta, Cryptophyta,

Dinophyceae, Crustacea, and Haptophyta were minor

constituents. The red-tide bloom sample U3 displayed a

relatively high abundance of Cyanobacteria, Chlorophyta,

and viruses, while proteobacterial proteins dominated at the

other three sites: U1, U2, and H (e.g., the a- and c-prote-

obacterial proteins in U2 and H).

3.4 Functional assignment

The dissolved proteins identified in this study were func-

tionally classified based on the KEGG taxonomic system

(Fig. 4). Consequently, 71, 139, 119, and 161 proteins in

the U1, U2, U3, and H samples, respectively, were related

to at least one functional assignment in a KEGG classifi-

cation category, representing 34–50 % of the total proteins

identified. Enzymes and enzyme-related proteins associ-

ated with metabolism, including carbohydrate, amino acid,

and energy metabolism, comprised a relatively high pro-

portion of the total identified proteins. Amino acid meta-

bolic enzymes were derived only from prokaryotes,

whereas other metabolic enzymes were derived from both

prokaryotes and eukaryotes. Cytoskeletal proteins, includ-

ing the tubulins (a- and b-tubulins) and actins, were

identified from the eukaryotic algae (Chlorophyta, Bacil-

lariophyta, Cryptophyta, Dinophyceae, and Haptophyta),

Crustacea, and Stramenopiles. These proteins were pre-

dominantly detected in the U2 and H site samples (11 and

13 % of the total identified proteins, respectively) and were

not detected in the samples from the other sites. Mem-

brane-associated and photosynthetic proteins were also

detected in the coastal DOM in this study. A large pro-

portion (50–66 %) of the proteins could not be identified.

4 Discussion

Prior to the development of MS-based comprehensive

proteomics, several pioneering works on marine dissolved

proteins involved analysis by N-terminal sequencing (Ta-

noue et al. 1995) and western blotting (Suzuki et al. 1997,

2000). The shotgun proteomic approach by LC–MS/MS,

presented here, illustrated that the dissolved protein frac-

tions from the four coastal water samples were composed

of proteins with varying functions that originated from

various microbial taxa. The results confirmed that a few

bacterial membrane proteins were sources of coastal dis-

solved protein constituents (Yamada and Tanoue 2009;

Yamada et al. 2000). In addition to previously known

heterotrophic bacteria, such as Pseudomonas and Vibrio

(Suzuki et al. 1997; Tanoue et al. 1995; Yamada and Ta-

noue 2006, 2009; Yamada et al. 2000), photosynthetic

organisms (including cyanobacteria and some eukaryotic

algae), Archaea, and Stramenopiles also appear to play

important roles as potential contributors to the costal DOM

pool. In addition, we observed that virus-associated pro-

teins detected in the coastal DOM fractions represented

5–13 % of the total dissolved proteins in each DOM

sample (Fig. 3).

In this study, proteins from most eukaryotic planktons

(Bacillariophyta, Cryptophyta, Dinophyceae, Crustacea,

and Haptophyta) displayed a relatively low abundance of

the total proteins identified, compared with those of

prokaryotes, for example; and as mentioned above, the

relatively abundant enzymes involved in amino acid

Fig. 3 Distribution of the biological origin associated with the

dissolved proteins detected in the four coastal DOM samples

Metaproteomics of dissolved organic matter in coastal water 109

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metabolism were derived only from prokaryotes. Given

that protists can represent as much as half of the biomass

in surface seawater (Caron et al. 1995), it should be

noted that there is a large set of proteins still unidentified

due to the lack of a proteomic database for these marine

eukaryotes, especially Dinophyceae, Haptophyta, and

Cryptophyta (Table 1). Accordingly, the observations for

these eukaryotic planktons must be interpreted carefully.

When examining the dissolved protein at Stn 3, where

red-tide blooms by a Dinophyceae species were observed

(Fig. S1), Dinophyceae proteins were minor components,

whereas those from Cyanobacteria, Chlorophyta, and

viruses were predominant. These findings might be due

to an insufficient eukaryotic phytoplankton database or

to the lability of proteins from this type of phytoplank-

ton bloom.

In addition, in the U3 sample, we found three intense

bands that were possible proteins associated with the red-

tide bloom phenomenon, but we could not identify the

Fig. 4 KEGG-based functional

assignments of the dissolved

proteins detected in the coastal

DOM samples. The KEGG

categories including more than

1 % of the total identified

proteins are presented

Table 1 The protein databases used in this study

Protein database No. of protein

entries

c-Proteobacteria 4,848,684

a-Proteobacteria 1,806,838

b-Proteobacteria 1,645,045

Viruses 1,204,312

Archaea 934,592

Bacteroidetes/Chlorobi group 875,673

Cyanobacteria 480,588

Chlorophyta 112,201

Stramenopiles 55,536

Crustacea 52,218

Bacillariophyta 49,322

Cryptophyta 3,587

Dinophyceae 3,530

Haptophyceae 1,074

110 M. Yoshida et al.

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potential origin of the major band using N-terminal amino

acid sequencing. Instead, based on the LC–MS/MS data,

the peptide sequences suspected for each of the distinct

three bands matched with various proteins that have not yet

been reported in marine DOM, a result similar to the study

by Powell et al. (2005). Thus, these bands may have con-

sisted of mixed bands with similar molecular sizes. The

possible sources of these bands may have not been iden-

tified due to the lack of a protein database for marine

organisms, together with the data of N-terminal amino acid

sequencing as described above.

In all the sampling sites, enzymes involved in the

metabolism of carbohydrates, amino acids, and energy,

along with cytoskeletal proteins, membrane proteins,

transporters, and photosynthetic proteins, were commonly

detected. These categories were found in previous studies

that examined oceanic surface waters (Powell et al. 2005;

Suzuki et al. 1997; Wang et al. 2011; Yamada and Tanoue

2006, 2009). To date, alkaline phosphatase, ATP synthase,

ribulose-1,5-bisphosphate carboxylase/oxygenase (RuBi-

sCo), and pyruvate carboxylase have been detected in

oceanic DOM samples (Powell et al. 2005; Wang et al.

2011; Yamada and Tanoue 2006, 2009). In this study, we

also detected alkaline phosphatase, ATP synthase, and

RuBisCo, indicating that the DOM fractions harbored

many more types of bacterial enzymes than previously

reported in other coastal areas (Yamada and Tanoue 2009).

Most of the enzymes identified in the present study were

associated with nutrient (such as carbohydrates and amino

acids) and energy metabolism, and their numbers accoun-

ted for 41–64 % of the total dissolved proteins. Bacterial

enzymes were also major constituents of the coastal DOM

pool, indicating high bacterial activity in the coastal zone

that may be linked to the high frequency of the enzymes.

This bacterial activity may be a relevant factor modulating

the DOM components in coastal environments, rather than

the accumulation of refractory bacterial membrane proteins

(e.g., OprP and OmpA-like proteins) found in pelagic

waters. Some of the detected enzymes were exo- and

periplasmic enzymes, including esterases, peptidases, pro-

teases, lipases, phosphatases, and ATP synthases. These

enzymes are potentially exposed to the outside of the cell,

and some of these enzymes are associated with the outer

and inner membrane, which may act as refractory protein

mechanisms and thus protect the proteins from degradation

due to the association with lipid bilayers, as reported by

Nagata et al. (1998), as well as association with peptido-

glycan (Miyoshi and Suzuki 2004).

Residues of refractory dissolved proteins, such as porin

P and OmpA-like membranes, have been reported in

pelagic waters (Suzuki et al. 1997; Tanoue et al. 1995;

Yamada and Tanoue 2006), whereas this study did not

detect these membrane proteins in our coastal samples.

Instead, other membrane-associated proteins, e.g., proteins

from prokaryotic outer membranes, such as lipoproteins

and inner membrane-associated proteins, transporters

(including largely ABC transporters and TonB-dependent

transporters), and ATP synthases, were observed. The

subcellular localization of these proteins is also likely to be

associated with refractory characteristics and a subsequent

accumulation in seawater (Wang et al. 2011).

Among the protein classes, the cytoskeletal proteins

displayed higher proportions in the U2 and H site samples

(11 and 13 %, respectively). Actin is the most abundant

protein in many eukaryotic cells, and it forms actin fila-

ments, the main structural component of the filopodia and

microvilli (Mogilner and Rubinstein 2005). Tubulin is also

a major structural component of microtubules that form the

flagella or cilia of eukaryotes, but the protein is typically

easily degraded in natural waters because of the absence of

a proteolysis-resistant structure (Dong et al. 2010; Wang

et al. 2011). Therefore, the patchy distribution of such

cytoskeleton proteins among the four sites might be the

result of a rapid decomposition to different net products,

due to the differences in the microbial community com-

position at each site and their different activities among

these sites. In fact, the relative abundance of the dissolved

proteins associated with eukaryotes from sites U2 and H

(average 20 %) was higher than that from sites U1 and U3

(average 14 %), suggesting a mosaic pattern of potential

microbial sources of cytoskeletal protein in this inland sea.

Among the photosynthetic proteins, RuBisCo, ATP synthase,

phycoerythrin, chloroplast light harvesting protein, and phyco-

cyanin from cyanobacteria and eukaryotic algae accounted for

2–9 % of the total proteins (Fig. 4). These results imply that the

contribution of autotrophs to the bulk DOM pool is much higher

in the coastal environment than in oceanic water (Wang et al.

2011). The most abundant photosynthetic protein was RuBisCo,

which is involved in carbon fixation and is known as the most

abundant protein on earth (Cooper 2000; Dhingra et al. 2004).

However, recent reports by Nunn et al. (2009, 2010) indicated

that RuBisCo is not the most abundant protein in the proteome of

the marine diatom Thalassiosira pseudonana and was more

rapidly degraded than other proteins (photosynthesis membrane

proteins and a membrane transporter) during a degradation

experiment with T. pseudonana cells after growth. Thus, RuBi-

sCo may have a short half-life, despite being one of the most

abundant proteins produced by cells.

Most of the functional categories and their potential

microbial origins for the coastal dissolved proteins identi-

fied in this study were observed in each proteome of the

four DOM fractions, and they have also been observed in

open oceanic samples (Dong et al. 2013; Wang et al. 2011);

however, there were several differences between the

coastal and oceanic surface proteomes. For the composition

of the potential DOM-producing microbial community, the

Metaproteomics of dissolved organic matter in coastal water 111

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dissolved proteins derived from b-Proteobacteria, known

as the major phylogenetic group in freshwater environ-

ments such as estuaries (Cottrell and Kirchman 2003), were

more abundant in coastal water (here 5–11 %) than oceanic

surface waters (\1 %; Dong et al. 2013), suggesting the

presence of a coastal-specific DOM resulting from a

potential terrestrial input. The eukaryote-associated pro-

teins of the coastal DOM fractions were also detected

abundantly, ranging from 11 to 23 %, but were not

detected in oceanic waters. The origins of these proteins

are most likely linked with eukaryotic phytoplankton

blooms occurring in the coastal environment. In addition,

our data indicate that a larger proportion (50–66 %) of

functionally unidentified proteins, mostly hypothetical

proteins, was observed in this study compared to the open

ocean (32–43 %; Wang et al. 2011). This outcome may

reflect the fact that the sources of dissolved proteins in

coastal areas are more diverse and complex, although dif-

ferent databases were used in both studies. In the com-

parison of the four coastal samples, we also found

differences in the compositions of the microbial origin

communities for the different dissolved protein samples

and in the relative abundance of specific dissolved protein

types (e.g., cytoskeletons), possibly indicating some

potential dynamics in the coastal DOM pool. A more

detailed spatial and temporal analysis of dissolved proteins

in both coastal and pelagic environments is needed to

further understand the dynamics in the marine DOM pool

and to link the regional DOM dynamics to the possible

biological and geographical processes in a coastal area.

Acknowledgments This study was performed under the ‘‘Global

COE Program in Ehime University’’ of the Ministry of Education,

Culture, Sports, Science, and Technology (MEXT) of Japan and was

partially supported by the Sasagawa Scientific Research Grant (no.

23-728) from the Japan Science Society and a Grant-in-Aid for Sci-

entific Research from the Japan Society for the Promotion of Science

(JSPS).

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