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letter re: notice of intent for remediation general permit ......system. jenkins-starr, llc is...

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  • Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is
47
May 22, 2006 Ms. Olga Vergara United States Environmental Protection Agency Region 1 Suite 1100 1 Congress Street Boston, MA 02114 RE: Notice of Intent for Remediation General Permit Common Street Trust Building 102-104 Trapelo Road Belmont, Massachusetts MADEP RTN 3-23300 Dear Ms. Vergara, Coler & Colantonio, Inc. has prepared this Notice of Intent (NOI) for a Remediation General Permit necessary for dewatering of a basement to complete Immediate Response Actions required by the Massachusetts Department of Environmental Protection. Dewatering of chlorinated volatile organic compound impacted groundwater is required to properly prepare the building basement for the installation of a new vapor/water proof floor. Coler & Colantonio, Inc. is the environmental consultant for the site and will be the operator of the system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is provided below: Coler & Colantonio, Inc. Jenkins-Starr, LLC. 55 Bobala Road 70 Industrial Drive Holyoke, MA. 01040 Holden, MA. 01520 Phone: 413/313-0131 Phone: 978/ 263-1086 Contact: Thomas J. Motsko Contact: Chris Starr, Managing Partner Historic groundwater analyses indicate the presence of a perchlorethylene (PCE) plume extending partially under the structure. The contaminants of concern are listed in the NOI. The groundwater treatment system will comprise of an existing sump pump located in the basement pumping groundwater through a totalizing flow meter to liquid phase granular activated carbon vessels. The discharge will tie into the previously utilized stormwater catch basin. A site locus map and an overview of the proposed system layout are attached with the NOI. 101 Accord Park Drive 781.982.5400 Norwell, MA 02061 Fax: 781.982.5490

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Page 1: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

May 22 2006

Ms Olga Vergara United States Environmental Protection Agency

Region 1 Suite 1100

1 Congress Street Boston MA 02114

RE Notice of Intent for Remediation General Permit Common Street Trust Building 102-104 Trapelo Road Belmont Massachusetts MADEP RTN 3-23300

Dear Ms Vergara

Coler amp Colantonio Inc has prepared this Notice of Intent (NOI) for a Remediation General Permit necessary for dewatering of a basement to complete Immediate Response Actions required by the Massachusetts Department of Environmental Protection Dewatering of chlorinated volatile organic compound impacted groundwater is required to properly prepare the building basement for the installation of a new vaporwater proof floor

Coler amp Colantonio Inc is the environmental consultant for the site and will be the operator of the system Jenkins-Starr LLC is considered the owner of the project Contact information for the owner and operator is provided below

Coler amp Colantonio Inc Jenkins-Starr LLC 55 Bobala Road 70 Industrial Drive Holyoke MA 01040 Holden MA 01520 Phone 413313-0131 Phone 978 263-1086 Contact Thomas J Motsko Contact Chris Starr Managing Partner

Historic groundwater analyses indicate the presence of a perchlorethylene (PCE) plume extending partially under the structure The contaminants of concern are listed in the NOI

The groundwater treatment system will comprise of an existing sump pump located in the basement pumping groundwater through a totalizing flow meter to liquid phase granular activated carbon vessels The discharge will tie into the previously utilized stormwater catch basin A site locus map and an overview of the proposed system layout are attached with the NOI

101 Accord Park Drive 7819825400 Norwell MA 02061 Fax 7819825490

If you require any further assistance please feel free to contact us at the numbers listed below

Sincerely COLER amp COLANTONIO INC

Thomas J Motsko

Mark A Germano LSP Thomas J Motsko Division Manager ndash Environmental Services Project Manager 781982-5429 413313-0131

Attachments

1 Notice of Intent 2 Figure 1 - Site Locus 3 Figure 2 ndash Process Flow and Treatment System Location 4 Laboratory Analytical Reports

101 Accord Park Drive 7819825400 Norwell MA 02061 Fax 7819825490

B Suggested Form for Notice of Intent (NOI) for the Remediation General Permit

1 General site information Please provide the following information about the site

a) Name of facilitysite Facilitysite address

Location of facilitysite longitude__________ latitude__________

Facility SIC code(s) Street

b) Name of facilitysite owner Town

Email address of owner State Zip County

Telephone noof facilitysite owner

Fax no of facilitysite owner Owner is (check one) 1 Federal____ 2 StateTribal_____ 3 Private______ 4 other if so describe

Address of owner (if different from site)

Street

Town State Zip County

c) Legal name of operator Operator telephone no

Operator fax no Operator email

Operator contact name and title

Remediation General Permit - Notice of Intent 1

Address of operator (if different from owner) Street

Town State Zip County

d) Check ldquoyesrdquo or ldquonordquo for the following 1 Has a prior NPDES permit exclusion been granted for the discharge Yes___ No___ if ldquoyesrdquo number 2 Has a prior NPDES application (Form 1 amp 2C) ever been filed for the discharge Yes___ No___ if ldquoyesrdquo date and tracking 3 Is the discharge a ldquonew dischargerdquoas defined by 40 CFR 1222 Yes___ No___ 4 For sites in Massachusetts is the discharge covered under the MA Contingency Plan (MCP) and exempt from state permitting Yes__ No__

e) Is sitefacility subject to any State permitting or other action which is causing the generation of discharge Yes___ No___ If ldquoyesrdquo please list 1 site identification assigned by the state of NH or MA 2 permit or license assigned 3 state agency contact information name location and telephone number

f) Is the sitefacility covered by any other EPA permit including 1 multi-sector storm water general permit Y___ N___ if Y number 2 phase I or II construction storm water general permit Y___ N___ if Y number 3 individual NPDES permit Y___ N___ if Y number 4 any other water quality related permit Y___ N___ if Y number

2 Discharge information Please provide information about the discharge (attaching additional sheets as needed) including

a) Describe the discharge activities for which the ownerapplicant is seeking coverage

b) Provide the following information about each discharge

1) Number of discharge points

2) What is the maximum and average flow rate of discharge (in cubic feet per second ft3s) Max flow____________ Average flow__________ Is maximum flow a design value Y___ N____ For average flow include the units and appropriate notation if this value is a design value or estimate if not available

3) Latitude and longitude of each discharge within 100 feet pt1long_________ lat________ pt2 long______ lat______ pt3 long______ lat______ pt4long______ lat______ pt5 long______ lat______ pt6long______ lat______ pt7 long______ lat______ pt8long______ lat______ etc

Remediation General Permit - Notice of Intent 2

4) If hydrostatic testing total volume of the discharge (gals) 5) Is the discharge intermittent______or seasonal______ Is discharge ongoing Yes ____ No______

c) Expected dates of discharge (mmddyy) start_____________ end_________________

d) Please attach a line drawing or flow schematic showing water flow through the facility including 1 sources of intake water 2 contributing flow from the operation 3 treatment units and 4 discharge points and receiving waters(s)

Remediation General Permit - Notice of Intent 3

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

0125061548 Page 6 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    10. Text10 MA
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                    13. Text13 617-965-8497
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                    15. Check Box1 Off
                    16. Check Box2 Off
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                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
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                    31. Text27 Holyoke
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                    41. Check Box39 Yes
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                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
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                    49. Text47 MADEP Jennifer Wang
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                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 2: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

If you require any further assistance please feel free to contact us at the numbers listed below

Sincerely COLER amp COLANTONIO INC

Thomas J Motsko

Mark A Germano LSP Thomas J Motsko Division Manager ndash Environmental Services Project Manager 781982-5429 413313-0131

Attachments

1 Notice of Intent 2 Figure 1 - Site Locus 3 Figure 2 ndash Process Flow and Treatment System Location 4 Laboratory Analytical Reports

101 Accord Park Drive 7819825400 Norwell MA 02061 Fax 7819825490

B Suggested Form for Notice of Intent (NOI) for the Remediation General Permit

1 General site information Please provide the following information about the site

a) Name of facilitysite Facilitysite address

Location of facilitysite longitude__________ latitude__________

Facility SIC code(s) Street

b) Name of facilitysite owner Town

Email address of owner State Zip County

Telephone noof facilitysite owner

Fax no of facilitysite owner Owner is (check one) 1 Federal____ 2 StateTribal_____ 3 Private______ 4 other if so describe

Address of owner (if different from site)

Street

Town State Zip County

c) Legal name of operator Operator telephone no

Operator fax no Operator email

Operator contact name and title

Remediation General Permit - Notice of Intent 1

Address of operator (if different from owner) Street

Town State Zip County

d) Check ldquoyesrdquo or ldquonordquo for the following 1 Has a prior NPDES permit exclusion been granted for the discharge Yes___ No___ if ldquoyesrdquo number 2 Has a prior NPDES application (Form 1 amp 2C) ever been filed for the discharge Yes___ No___ if ldquoyesrdquo date and tracking 3 Is the discharge a ldquonew dischargerdquoas defined by 40 CFR 1222 Yes___ No___ 4 For sites in Massachusetts is the discharge covered under the MA Contingency Plan (MCP) and exempt from state permitting Yes__ No__

e) Is sitefacility subject to any State permitting or other action which is causing the generation of discharge Yes___ No___ If ldquoyesrdquo please list 1 site identification assigned by the state of NH or MA 2 permit or license assigned 3 state agency contact information name location and telephone number

f) Is the sitefacility covered by any other EPA permit including 1 multi-sector storm water general permit Y___ N___ if Y number 2 phase I or II construction storm water general permit Y___ N___ if Y number 3 individual NPDES permit Y___ N___ if Y number 4 any other water quality related permit Y___ N___ if Y number

2 Discharge information Please provide information about the discharge (attaching additional sheets as needed) including

a) Describe the discharge activities for which the ownerapplicant is seeking coverage

b) Provide the following information about each discharge

1) Number of discharge points

2) What is the maximum and average flow rate of discharge (in cubic feet per second ft3s) Max flow____________ Average flow__________ Is maximum flow a design value Y___ N____ For average flow include the units and appropriate notation if this value is a design value or estimate if not available

3) Latitude and longitude of each discharge within 100 feet pt1long_________ lat________ pt2 long______ lat______ pt3 long______ lat______ pt4long______ lat______ pt5 long______ lat______ pt6long______ lat______ pt7 long______ lat______ pt8long______ lat______ etc

Remediation General Permit - Notice of Intent 2

4) If hydrostatic testing total volume of the discharge (gals) 5) Is the discharge intermittent______or seasonal______ Is discharge ongoing Yes ____ No______

c) Expected dates of discharge (mmddyy) start_____________ end_________________

d) Please attach a line drawing or flow schematic showing water flow through the facility including 1 sources of intake water 2 contributing flow from the operation 3 treatment units and 4 discharge points and receiving waters(s)

Remediation General Permit - Notice of Intent 3

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    364. Text52
                    365. Text53
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                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 3: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

B Suggested Form for Notice of Intent (NOI) for the Remediation General Permit

1 General site information Please provide the following information about the site

a) Name of facilitysite Facilitysite address

Location of facilitysite longitude__________ latitude__________

Facility SIC code(s) Street

b) Name of facilitysite owner Town

Email address of owner State Zip County

Telephone noof facilitysite owner

Fax no of facilitysite owner Owner is (check one) 1 Federal____ 2 StateTribal_____ 3 Private______ 4 other if so describe

Address of owner (if different from site)

Street

Town State Zip County

c) Legal name of operator Operator telephone no

Operator fax no Operator email

Operator contact name and title

Remediation General Permit - Notice of Intent 1

Address of operator (if different from owner) Street

Town State Zip County

d) Check ldquoyesrdquo or ldquonordquo for the following 1 Has a prior NPDES permit exclusion been granted for the discharge Yes___ No___ if ldquoyesrdquo number 2 Has a prior NPDES application (Form 1 amp 2C) ever been filed for the discharge Yes___ No___ if ldquoyesrdquo date and tracking 3 Is the discharge a ldquonew dischargerdquoas defined by 40 CFR 1222 Yes___ No___ 4 For sites in Massachusetts is the discharge covered under the MA Contingency Plan (MCP) and exempt from state permitting Yes__ No__

e) Is sitefacility subject to any State permitting or other action which is causing the generation of discharge Yes___ No___ If ldquoyesrdquo please list 1 site identification assigned by the state of NH or MA 2 permit or license assigned 3 state agency contact information name location and telephone number

f) Is the sitefacility covered by any other EPA permit including 1 multi-sector storm water general permit Y___ N___ if Y number 2 phase I or II construction storm water general permit Y___ N___ if Y number 3 individual NPDES permit Y___ N___ if Y number 4 any other water quality related permit Y___ N___ if Y number

2 Discharge information Please provide information about the discharge (attaching additional sheets as needed) including

a) Describe the discharge activities for which the ownerapplicant is seeking coverage

b) Provide the following information about each discharge

1) Number of discharge points

2) What is the maximum and average flow rate of discharge (in cubic feet per second ft3s) Max flow____________ Average flow__________ Is maximum flow a design value Y___ N____ For average flow include the units and appropriate notation if this value is a design value or estimate if not available

3) Latitude and longitude of each discharge within 100 feet pt1long_________ lat________ pt2 long______ lat______ pt3 long______ lat______ pt4long______ lat______ pt5 long______ lat______ pt6long______ lat______ pt7 long______ lat______ pt8long______ lat______ etc

Remediation General Permit - Notice of Intent 2

4) If hydrostatic testing total volume of the discharge (gals) 5) Is the discharge intermittent______or seasonal______ Is discharge ongoing Yes ____ No______

c) Expected dates of discharge (mmddyy) start_____________ end_________________

d) Please attach a line drawing or flow schematic showing water flow through the facility including 1 sources of intake water 2 contributing flow from the operation 3 treatment units and 4 discharge points and receiving waters(s)

Remediation General Permit - Notice of Intent 3

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
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                    41. Check Box39 Yes
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                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    339. Text301 grab
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                    364. Text52
                    365. Text53
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                    369. Text56 grab
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                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 4: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

Address of operator (if different from owner) Street

Town State Zip County

d) Check ldquoyesrdquo or ldquonordquo for the following 1 Has a prior NPDES permit exclusion been granted for the discharge Yes___ No___ if ldquoyesrdquo number 2 Has a prior NPDES application (Form 1 amp 2C) ever been filed for the discharge Yes___ No___ if ldquoyesrdquo date and tracking 3 Is the discharge a ldquonew dischargerdquoas defined by 40 CFR 1222 Yes___ No___ 4 For sites in Massachusetts is the discharge covered under the MA Contingency Plan (MCP) and exempt from state permitting Yes__ No__

e) Is sitefacility subject to any State permitting or other action which is causing the generation of discharge Yes___ No___ If ldquoyesrdquo please list 1 site identification assigned by the state of NH or MA 2 permit or license assigned 3 state agency contact information name location and telephone number

f) Is the sitefacility covered by any other EPA permit including 1 multi-sector storm water general permit Y___ N___ if Y number 2 phase I or II construction storm water general permit Y___ N___ if Y number 3 individual NPDES permit Y___ N___ if Y number 4 any other water quality related permit Y___ N___ if Y number

2 Discharge information Please provide information about the discharge (attaching additional sheets as needed) including

a) Describe the discharge activities for which the ownerapplicant is seeking coverage

b) Provide the following information about each discharge

1) Number of discharge points

2) What is the maximum and average flow rate of discharge (in cubic feet per second ft3s) Max flow____________ Average flow__________ Is maximum flow a design value Y___ N____ For average flow include the units and appropriate notation if this value is a design value or estimate if not available

3) Latitude and longitude of each discharge within 100 feet pt1long_________ lat________ pt2 long______ lat______ pt3 long______ lat______ pt4long______ lat______ pt5 long______ lat______ pt6long______ lat______ pt7 long______ lat______ pt8long______ lat______ etc

Remediation General Permit - Notice of Intent 2

4) If hydrostatic testing total volume of the discharge (gals) 5) Is the discharge intermittent______or seasonal______ Is discharge ongoing Yes ____ No______

c) Expected dates of discharge (mmddyy) start_____________ end_________________

d) Please attach a line drawing or flow schematic showing water flow through the facility including 1 sources of intake water 2 contributing flow from the operation 3 treatment units and 4 discharge points and receiving waters(s)

Remediation General Permit - Notice of Intent 3

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
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                    91. Text90 082906
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                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
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                    307. Check Box181 Off
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                    309. Text277 grab
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                    319. Text285 grab
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                    332. Text296 ND (lt250)
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                    339. Text301 grab
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                    342. Text304 290
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                    344. Text306
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                    349. Text33 grab
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                    352. Text37 ND (lt100)
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                    354. Text40
                    355. Text41
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                    357. Check Box311 Off
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                    359. Text43 grab
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                    362. Text49 ND (lt75)
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                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
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                    369. Text56 grab
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                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 5: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

4) If hydrostatic testing total volume of the discharge (gals) 5) Is the discharge intermittent______or seasonal______ Is discharge ongoing Yes ____ No______

c) Expected dates of discharge (mmddyy) start_____________ end_________________

d) Please attach a line drawing or flow schematic showing water flow through the facility including 1 sources of intake water 2 contributing flow from the operation 3 treatment units and 4 discharge points and receiving waters(s)

Remediation General Permit - Notice of Intent 3

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
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                    41. Check Box39 Yes
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                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    339. Text301 grab
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                    364. Text52
                    365. Text53
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                    369. Text56 grab
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                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 6: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

3 Contaminant information In order to complete this section the applicant will need to take a minimum of one sample of the untreated water and have it analyzed for all of the parameters listed in Appendix III Historical data (ie data taken no more than 2 years prior to the effective date of the permit) may be used if obtained pursuant to i Massachusettsrsquo regulations 310 CMR 400000 the Massachusetts Contingency Plan (ldquoChapter 21Erdquo) ii New Hampshirersquos Title 50 RSA 485-A Water Pollution and Waste Disposal or Title 50 RSA 485-C Groundwater Protection Act or iii an EPA permit exclusion letter issued pursuant to 40 CFR 1223 provided the data was analyzed with test methods that meet the requirements of this permit Otherwise a new sample shall be taken and analyzed

a) Based on the analysis of the sample(s) of the untreated influent the applicant must check the box of the sub-categories that the potential discharge falls within

Gasoline Only VOC Only Primarily Metals Urban Fill Sites Contaminated Sumps Mixed Contaminants Aquifer Testing

Fuel Oils (and Other Oils) only

VOC with Other Contaminants

Petroleum with Other Contaminants

Listed Contaminated Sites

Contaminated Dredge Condensates

Hydrostatic Testing of PipelinesTanks

Well Development or Rehabilitation

b) Based on the analysis of the untreated influent the applicant must indicate whether each listed chemical is believed present or believed absent in the potential discharge Attach additional sheets as needed

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

(eg grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

1 Total Suspended Solids

2 Total Residual Chlorine

3 Total Petroleum Hydrocarbons

4 Cyanide

5 Benzene

6 Toluene

7 Ethylbenzene

8 (mpo) Xylenes

9 Total BTEX4

4BTEX = Sum of Benzene Toluene Ethylbenzene total Xylenes

Remediation General Permit - Notice of Intent 4

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
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                    41. Check Box39 Yes
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                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    339. Text301 grab
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                    364. Text52
                    365. Text53
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                    369. Text56 grab
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                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 7: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

10 Ethylene Dibromide (12- Dibromo-methane)

11 Methyl-tert-Butyl Ether (MtBE)

12 tert-Butyl Alcohol (TBA)

13 tert-Amyl Methyl Ether (TAME)

14 Naphthalene

15 Carbon Tetra-chloride

16 14 Dichlorobenzene

17 12 Dichlorobenzene

18 13 Dichlorobenzene

19 11 Dichloroethane

20 12 Dichloroethane

21 11 Dichloroethylene

22 cis-12 Dichloro-ethylene

23 Dichloromethane (Methylene Chloride)

24 Tetrachloroethylene

Remediation General Permit - Notice of Intent 5

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    364. Text52
                    365. Text53
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                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 8: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of Test

Maximum daily value Avg daily Value

(1 min-imum)

grab) (method ) Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

25 111 Trichloroethane

26 112 Trichloroethane

27 Trichloroethylene

28 Vinyl Chloride

29 Acetone

30 14 Dioxane

31 Total Phenols

32 Pentachlorophenol

33 Total Phthalates 5

(Phthalate esthers)

34 Bis (2-Ethylhexyl) Phthalate [Di-(ethylhexyl) Phthalate]

35 Total Group I Polycyclic Aromatic Hydrocarbons (PAH)

a Benzo(a) Anthracene

b Benzo(a) Pyrene

c Benzo(b)Fluoranthene

d Benzo(k) Fluoranthene

e Chrysene

5The sum of individual phthalate compounds

Remediation General Permit - Notice of Intent 6

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

0125061548 Page 6 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

0125061548 Page 7 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    7. Text7 Common Street Trust
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                    9. Text9
                    10. Text10 MA
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                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
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                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
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                    38. Check Box36 Off
                    39. Check Box37 Yes
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                    41. Check Box39 Yes
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                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
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                    57. Check Box56 Yes
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                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 9: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method Used

Minimum Level (ML) of

Maximum daily value Average daily value

(1 min-imum)

grab) (method ) Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

f Dibenzo(ah) anthracene

g Indeno(123-cd) Pyrene

36 Total Group II Polycyclic Aromatic Hydrocarbons (PAH)

h Acenaphthene

i Acenaphthylene

j Anthracene

k Benzo(ghi) Perylene

l Fluoranthene

m Fluorene

n Naphthalene-

o Phenanthrene

p Pyrene

37 Total Polychlorinated Biphenyls (PCBs)

38 Antimony

39 Arsenic

40 Cadmium

41 Chromium III

42 Chromium VI

Remediation General Permit - Notice of Intent 7

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

0125061548 Page 6 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

0125061548 Page 7 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

0125061548 Page 8 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

0125061548 Page 9 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 10: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

PARAMETER Believe Absent

Believe Present

of Samples

Type of Sample (eg

Analytical Method

Minimum Level (ML) of

Maximum daily value Avg daily value

(1 min-imum)

grab) Used (method )

Test Method concentration (ugl)

mass (kg) concentration (ugl)

mass (kg)

43 Copper

44 Lead

45 Mercury

46 Nickel

47 Selenium

48 Silver

49 Zinc

50 Iron

Other (describe)

c) For discharges where metals are believed present please fill out the following

Step 1 Do any of the metals in the influent have a reasonable potential to exceed the If yes which metals effluent limits in Appendix III (ie the limits set at zero to five dilutions) Y____ N____

Step 2 For any metals which have reasonable potential to exceed the Appendix III limits Look up the limit calculated at the corresponding dilution factor in calculate the dilution factor (DF) using the formula in Part IA3c) (step 2) of the NOI Appendix IV Do any of the metals in the influent have the potential to instructions or as determined by the State prior to the submission of this NOI exceed the corresponding effluent limits in Appendix IV (ie is the What is the dilution factor for applicable metals influent concentration above the limit set at the calculated dilution Metals_____________________________________________________________ factor)

Y____ N____ If ldquoYesrdquo list which metals DF _______

Remediation General Permit - Notice of Intent 8

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

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_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

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_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

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_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

0125061548 Page 6 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

0125061548 Page 7 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

0125061548 Page 8 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

0125061548 Page 9 of 11

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_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
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                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
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                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
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                    52. Text51
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                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
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                    80. Text78
                    81. Text79
                    82. Text80
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                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
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                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
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                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 11: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

4 Treatment system information Please describe the treatment system using separate sheets as necessary including

a) A description of the treatment system including a schematic of the proposed or existing treatment system

b) Identify each applicable treatment unit (check all that apply)

Frac tank Air stripper Oilwater separator Equalization tanks Bag filter GAC filter

Chlorination Dechlorination Other (please describe)

c) Proposed average and maximum flow rates (gallons per minute) for the discharge and the design flow rate(s) (gallons per minute) of the treatment system Average flow rate of discharge__________ Design flow rate of treatment system ___________ Maximum flow rate of treatment system ___________

d) A description of chemical additives being used or planned to be used (attach MSDS sheets)

5 Receiving surface water(s) Please provide information about the receiving water(s) using separate sheets as necessary

Direct_____ Within facility__ Storm drain____ Riverbrook____ Wetlands_____ a) Identify the discharge pathway Other (describe)

b) Provide a narrative description of the discharge pathway including the name(s) of the receiving waters

Remediation General Permit - Notice of Intent 9

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    129. Text103 grab
                    130. Text104 1664A
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                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
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                    143. Text115
                    144. Text116
                    145. Text117
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                    147. Check Box78 Off
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                    152. Text122 ND (lt50)
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                    154. Text124
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                    156. Check Box70 Yes
                    157. Check Box79 Off
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                    159. Text127 grab
                    160. Text128 624
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                    162. Text130 ND (lt50)
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                    164. Text132
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                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
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                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
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                    184. Text148
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                    186. Check Box73 Yes
                    187. Check Box82 Off
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                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
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                    196. Check Box158 Yes
                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
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                    202. Text192 ND (lt0019)
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                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    226. Check Box164 Yes
                    227. Check Box165 Off
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                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
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                    234. Text218
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                    236. Check Box166 Yes
                    237. Check Box167 Off
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                    239. Text221 grab
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                    242. Text224 ND (lt02)
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                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
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                    252. Text232 ND (lt50)
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                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
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                    262. Text240 ND (lt250)
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                    266. Check Box172 Yes
                    267. Check Box173 Off
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                    269. Text245 grab
                    270. Text246 624
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                    272. Text248 ND (lt250)
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                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
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                    282. Text256 ND (lt250)
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                    284. Text258
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                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
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                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
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                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
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                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 12: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

c) Attach a detailed map(s) indicating the site location and location of the outfall to the receiving water 1 For multiple discharges number the discharges sequentially 2 For indirect dischargers indicate the location of the discharge to the indirect conveyance and the discharge to surface water The map should also include the location and distance to the nearest sanitary sewer as well as the locus of nearby sensitive receptors (based on USGS topographical mapping) such as surface waters drinking water supplies and wetland areas

d) Provide the state water quality classification of the receiving water__________________________________

e) Provide the reported or calculated seven day-ten year low flow (7Q10) of the receiving water_________________________cfs Please attach any calculation sheets used to support stream flow and dilution calculations

f) Is the receiving water a listed 303(d) water quality impaired or limited water Yes____ No____ If yes for which pollutant(s)

Is there a TMDL Yes____ No____ If yes for which pollutant(s)

6 Results of Consultation with Federal Services Please provide the following information according to requirements of Part IB4 and Appendices II and VII

a) Are any listed threatened or endangered species or designated critical habitat in proximity to the discharge Yes____No____ Has any consultation with the federal services been completed No___ or is consultation underway No____

Yes ____What were the results of the consultation with the US Fish and Wildlife Service andor National Marine Fisheries Service (check one) a ldquono jeopardyrdquo opinion _____or written concurrence____ on a finding that the discharges are not likely to adversely affect any endangered species or critical habitat

Yes___

b) Are any historic properties listed or eligible for listing on the National Register of Historic Places located on the facility or site or in proximity to the discharge been consulted in this determination (Massachusetts only) Yes______ No________Yes_______ No________Have any state or tribal historic preservation officer

Remediation General Permit - Notice of Intent 10

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

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_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    364. Text52
                    365. Text53
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                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 13: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

7 Supplemental information

Please provide any supplemental information Attach any analytical data used to support the application Attach any certification(s) required by the general permit

Remediation General Permit - Notice of Intent 11

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

0125061548 Page 7 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

0125061548 Page 9 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
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                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 14: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

8 Signature Requirements The Notice of Intent must be signed by the operator in accordance with the signatory requirements of 40 CFR Section 12222 including the following certification

I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information I certify that the information submitted is to the best of my knowledge and belief true accurate and complete I certify that I am aware that there are significant penalties for submitting false information including the possibility of fine and imprisonment for knowing violations

FacilitySite Name

Operator signature

Title

Date

Remediation General Permit - Notice of Intent 12

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
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                    82. Text80
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 15: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

B Submission of NOI to EPA - All operators applying for coverage under this General Permit must submit a written Notice of Intent (NOI) to EPA Signed and completed NOI forms and attachments must be submitted to EPA-NE at

US Environmental Protection Agency RGP-NOC Processing Municipal Assistance Unit (CMU) 1 Congress Street Suite 1100 Boston MA 02114-2023

or electronically mailed to NPDESGeneralpermitsepagov or faxed to the EPA Office at 617-918-0505

If filling out the suggested NOI form electronically on EPArsquos website the signature page must be signed and faxed or mailed to EPA at the phone number or address listed in Section IB below

1 Filing with the states - A copy of any NOI form filed with EPA-NE must also be filed with state agencies The state agency may elect to develop a state specific form or other information requirements

a) Discharges in Massachusetts - In addition to the NOI permit applicants must submit copies of the State Application Form BRPWM 12 Request for General Permit coverage for the RGP The application form and the Transmittal Form for Permit Application and Payment may be obtained from the Massachusetts Department of Environmental Protection (MA DEP) website at wwwstatemausdep Municipalities are fee-exempt but should send a copy of the transmittal form to that address for project tracking purposes All applicants should keep a copy of the transmittal form and a copy of the application package for their records

1) A copy of the NOI the transmittal form a copy of the check and Form BRPWM 12 should be sent to

Massachusetts Department of Environmental Protection Division of Watershed Management 627 Main Street 2nd floor Worcester MA 01608

2) A copy of the transmittal form and the appropriate fee should be sent to

Massachusetts Department of Environmental Protection PO Box 4062 Boston MA 02111

Please note Applicants for discharges in Massachusetts should note that under 310 CMR 40000 as a matter of state law the general permit only applies to discharges that are not subject to the Massachusetts Contingency Plan (MCP) and 310 CMR 40000 Therefore discharges subject to the MCP are not required to fill out and submit the State Application Form BRPWM 12 or pay the state fees However they must submit a NOI to EPA

Remediation General Permit - Notice of Intent 13

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    364. Text52
                    365. Text53
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                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 16: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

b) Discharges in New Hampshire - applicants must provide a copy of the Notice of Intent to

New Hampshire Department of Environmental Services Water Division Wastewater Engineering Bureau PO Box 95 Concord New Hampshire 03302-0095

2 Filing with Municipalities - A copy of the NOI must be submitted to the municipality in which the proposed discharge would be located

Remediation General Permit - Notice of Intent 14

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

0125061548 Page 7 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
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                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
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                    82. Text80
                    83. Text81
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
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                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
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                    167. Check Box80 Off
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                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
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                    179. Text143 grab
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                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
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                    184. Text148
                    185. Text149
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                    187. Check Box82 Off
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                    189. Text151 grab
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                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
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                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
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                    207. Check Box161 Yes
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                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    227. Check Box165 Off
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                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
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                    237. Check Box167 Off
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                    239. Text221 grab
                    240. Text222 8270M
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                    242. Text224 ND (lt02)
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                    244. Text226
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                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
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                    254. Text234
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                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
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                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
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                    277. Check Box175 Off
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                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
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                    285. Text259
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                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
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                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
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                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
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                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
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                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 17: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

Approximate Site Location

Cushing Square Auto Parts Figure 1 102 - 104 Trapelo Road Site Locus and

Belmont Massachusetts DEP Priority Resource Map

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0125061548 Page 1 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

0125061548 Page 2 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
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                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
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                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
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                    179. Text143 grab
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                    204. Text194
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                    207. Check Box161 Yes
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                    209. Text197 grab
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                    212. Text200 5500
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                    216. Check Box162 Yes
                    217. Check Box163 Off
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                    219. Text205 grab
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                    227. Check Box165 Off
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                    229. Text213 grab
                    230. Text214 624
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                    239. Text221 grab
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                    249. Text229 grab
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                    259. Text237 grab
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                    269. Text245 grab
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                    272. Text248 ND (lt250)
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                    274. Text250
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                    276. Check Box174 Yes
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                    279. Text253 grab
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                    286. Check Box176 Yes
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                    289. Text261 grab
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                    295. Text267
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                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
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                    309. Text277 grab
                    310. Text278 624
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                    312. Text280 ND (lt50)
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                    314. Text282
                    315. Text283
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                    317. Check Box183 Off
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                    319. Text285 grab
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                    322. Text288 ND (lt50)
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                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
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                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
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                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
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                    379. Text161 grab
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                    382. Text164 ND (lt100)
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                    389. Text169 grab
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                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 18: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600756

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 17-JAN-2006

Attn Mr Mark Germano Date Reported 25-JAN-2006

Project Number 11-1226 Delivery Method Alpha

Site NPDES PERMITTOPS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600756-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 5 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
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                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    96. Check Box45 Yes
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                    100. Check Box51 Yes
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                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 19: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESNARRATIVE REPORT

Laboratory Job Number L0600756

Report Submission

This report replaces the report issued on January 242006 The report has been amended toinclude the compounds MBTE TBA TAME and 14 Dioxane for L0600756

Volatile Organics by Method 624

L0600756-01 has elevated limits of detection due to the 50x dilutions required by theelevated concentrations of non-target compounds in the sample

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
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                    82. Text80
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
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                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
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                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
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                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
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                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
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                    408. Text184 1
                    409. Text185 grab
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                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
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                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
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                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
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                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
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                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
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                    449. Text337 grab
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                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
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                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
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                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
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                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
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                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
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                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    759. Text639 grab
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                    764. Text644
                    765. Text645
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                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
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                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 20: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600756-01 Date Collected 13-JAN-2006 1530 SUMP DISCHARGE Date Received 17-JAN-2006

Sample Matrix WATER Date Reported 25-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 4-Vial

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Pesticides by GC 504 14 5041 0124 1040 0124 1336 JB

12-Dibromoethane ND ugl 0019 12-Dibromo-3-chloropropane ND ugl 0019

Volatile Organics by GCMS 624 5 624 0120 1431 MM

Methylene chloride ND ugl 250 11-Dichloroethane ND ugl 75 Chloroform ND ugl 75 Carbon tetrachloride ND ugl 50 12-Dichloropropane ND ugl 180 Dibromochloromethane ND ugl 50 112-Trichloroethane ND ugl 75 2-Chloroethylvinyl ether ND ugl 500 Tetrachloroethene 290 ugl 75 Chlorobenzene ND ugl 180 Trichlorofluoromethane ND ugl 250 12-Dichloroethane ND ugl 75 111-Trichloroethane ND ugl 100 Bromodichloromethane ND ugl 50 trans-13-Dichloropropene ND ugl 75 cis-13-Dichloropropene ND ugl 75 Bromoform ND ugl 50 1122-Tetrachloroethane ND ugl 50 Benzene ND ugl 50 Toluene ND ugl 50 Ethylbenzene ND ugl 50 Chloromethane ND ugl 500 Bromomethane ND ugl 250 Vinyl chloride ND ugl 100 Chloroethane ND ugl 100 11-Dichloroethene ND ugl 50 trans-12-Dichloroethene ND ugl 75 cis-12-Dichloroethene ND ugl 50 Trichloroethene ND ugl 50 12-Dichlorobenzene ND ugl 250 13-Dichlorobenzene ND ugl 250 14-Dichlorobenzene ND ugl 250 pm-Xylene ND ugl 100 o-xylene ND ugl 50

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 3 of 11

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
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                    7. Text7 Common Street Trust
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                    9. Text9
                    10. Text10 MA
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                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
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                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
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                    38. Check Box36 Off
                    39. Check Box37 Yes
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                    41. Check Box39 Yes
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                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
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                    57. Check Box56 Yes
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                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 21: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600756-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Volatile Organics by GCMS 624 contd 5 624 0120 1431 MM

Xylene (Total) ND ugl 100 Styrene ND ugl 50 Acetone ND ugl 500 Carbon disulfide ND ugl 250 2-Butanone ND ugl 500 Vinyl acetate ND ugl 1000 4-Methyl-2-pentanone ND ugl 500 2-Hexanone ND ugl 500 Acrolein ND ugl 400 Acrylonitrile ND ugl 500 Methyl tert butyl ether 5500 ugl 1000 14-Dioxane ND ugl 100000 Tert-Butyl Alcohol ND ugl 5000 Tertiary-Amyl Methyl Ether ND ugl 1000

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 104 80-120 Fluorobenzene 106 80-120 4-Bromofluorobenzene 101 80-120

Comments Complete list of References and Glossary of Terms found in Addendum I

0125061548 Page 4 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
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                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 22: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600756

Parameter Value 1 Value 2 Units RPD RPD Limits

Volatile Organics by GCMS 624 for sample(s) 01 (L0600573-01 WG227088-2)Methylene chloride ND ND ugl NC 30 11-Dichloroethane ND ND ugl NC 30 Chloroform ND ND ugl NC 30 Carbon tetrachloride ND ND ugl NC 30 12-Dichloropropane ND ND ugl NC 30 Dibromochloromethane ND ND ugl NC 30 112-Trichloroethane ND ND ugl NC 30 Tetrachloroethene ND ND ugl NC 30 Chlorobenzene ND ND ugl NC 30 Trichlorofluoromethane ND ND ugl NC 30 12-Dichloroethane ND ND ugl NC 30 111-Trichloroethane ND ND ugl NC 30 Bromodichloromethane ND ND ugl NC 30 trans-13-Dichloropropene ND ND ugl NC 30 cis-13-Dichloropropene ND ND ugl NC 30 Bromoform 12 14 ugl 15 30 1122-Tetrachloroethane ND ND ugl NC 30 Benzene ND ND ugl NC 30 Toluene ND ND ugl NC 30 Ethylbenzene ND ND ugl NC 30 Chloromethane ND ND ugl NC 30 Bromomethane ND ND ugl NC 30 Vinyl chloride ND ND ugl NC 30 Chloroethane ND ND ugl NC 30 11-Dichloroethene ND ND ugl NC 30 trans-12-Dichloroethene ND ND ugl NC 30 cis-12-Dichloroethene ND ND ugl NC 30 Trichloroethene ND ND ugl NC 30 12-Dichlorobenzene ND ND ugl NC 30 13-Dichlorobenzene ND ND ugl NC 30 14-Dichlorobenzene ND ND ugl NC 30 pm-Xylene ND ND ugl NC 30 o-Xylene ND ND ugl NC 30 XYLENE (TOTAL) ND ND ugl NC 30 Styrene ND ND ugl NC 30 Acetone ND ND ugl NC 30 Carbon disulfide ND ND ugl NC 30 2-Butanone ND ND ugl NC 30 Vinyl acetate ND ND ugl NC 30 4-Methyl-2-pentanone ND ND ugl NC 30 2-Hexanone ND ND ugl NC 30 Acrolein ND ND ugl NC 30 Acrylonitrile ND ND ugl NC 30

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 101 910 80-120 Fluorobenzene 102 940 80-120 4-Bromofluorobenzene 111 990 80-120

0125061548 Page 5 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

0125061548 Page 6 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
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                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    117. Check Box75 Off
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                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    130. Text104 1664A
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                    132. Text106 ND (lt4000)
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                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
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                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
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                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
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                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
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                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
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                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
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                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
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                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
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                    259. Text237 grab
                    260. Text238 624
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                    262. Text240 ND (lt250)
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                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
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                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
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                    289. Text261 grab
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                    291. Text263 1 ugL
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                    294. Text266
                    295. Text267
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                    297. Check Box179 Off
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
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                    324. Text290
                    325. Text291
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                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
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                    334. Text298
                    335. Text299
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                    337. Check Box187 Yes
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                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
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                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
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                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
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                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
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                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
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                    387. Check Box317 Off
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                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
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                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
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                    409. Text185 grab
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                    412. Text308 ND (lt003)
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                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
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                    419. Text313 grab
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                    422. Text316 ND (lt20)
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                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
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                    429. Text321 grab
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                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
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                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
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                    439. Text329 grab
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                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
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                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
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                    449. Text337 grab
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                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
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                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
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                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
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                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
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                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
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                    481. Text363 01 ugL
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                    484. Text366
                    485. Text367
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                    487. Check Box337 Off
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                    489. Text369 grab
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                    492. Text372 ND (lt02)
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                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
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                    499. Text377 grab
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                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
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                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
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                    509. Text421 grab
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                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
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                    514. Text426
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                    517. Check Box387 Off
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                    519. Text429 grab
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                    521. Text431 015 ugL
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                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
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                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
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                    539. Text445 grab
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                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
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                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
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                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
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                    559. Text461 grab
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                    562. Text464 ND (lt02)
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                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
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                    569. Text469 grab
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                    572. Text472 ND (lt02)
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                    574. Text474
                    575. Text475
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                    577. Check Box399 Off
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                    579. Text477 grab
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                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
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                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
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                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
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                    594. Text490
                    595. Text491
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                    597. Check Box403 Off
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                    599. Text493 grab
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                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
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                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
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                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
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                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
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                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
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                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
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                    642. Text528 ND (lt5)
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                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
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                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
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                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
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                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
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                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
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                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
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                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 23: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756

Parameter Recovery QC Criteria

Pesticides by GC 504 LCS for sample(s) 01 (WG227604-2)12-Dibromoethane 99 12-Dibromo-3-chloropropane 108

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)Methylene chloride 103 10-221 11-Dichloroethane 90 59-155 Chloroform 81 51-138 Carbon tetrachloride 79 70-140 12-Dichloropropane 96 10-210 Dibromochloromethane 87 53-149 112-Trichloroethane 95 52-150 2-Chloroethylvinyl ether 107 10-305 Tetrachloroethene 92 64-148 Chlorobenzene 96 37-160 Trichlorofluoromethane 87 17-181 12-Dichloroethane 84 49-155 111-Trichloroethane 84 52-162 Bromodichloromethane 83 35-155 trans-13-Dichloropropene 85 17-183 cis-13-Dichloropropene 92 10-227 Bromoform 84 45-169 1122-Tetrachloroethane 94 46-157 Benzene 98 37-151 Toluene 97 47-150 Ethylbenzene 100 37-162 Chloromethane 67 10-273 Bromomethane 88 10-242 Vinyl chloride 81 10-251 Chloroethane 104 14-230 11-Dichloroethene 91 10-234 trans-12-Dichloroethene 93 54-156 cis-12-Dichloroethene 95 60-140 Trichloroethene 95 71-157 12-Dichlorobenzene 94 18-190 13-Dichlorobenzene 95 59-156 14-Dichlorobenzene 96 18-190 pm-Xylene 103 40-160 o-Xylene 102 40-160 XYLENE (TOTAL) 103 40-160 Styrene 90 40-160 Acetone 93 40-160 Carbon disulfide 83 40-160 2-Butanone 88 40-160 Vinyl acetate 69 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 103 40-160 Acrolein 110 40-160 Acrylonitrile 106 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    364. Text52
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                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 24: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 LCS for sample(s) 01 (WG227088-11)

Surrogate(s) Pentafluorobenzene 104 80-120 Fluorobenzene 103 80-120 4-Bromofluorobenzene 98 80-120

Pesticides by GC 504 SPIKE for sample(s) 01 (L0600756-01 WG227604-3)12-Dibromoethane 100 12-Dibromo-3-chloropropane 107

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Methylene chloride 80 10-221 11-Dichloroethane 78 59-155 Chloroform 75 51-138 Carbon tetrachloride 72 70-140 12-Dichloropropane 81 10-210 Dibromochloromethane 90 53-149 112-Trichloroethane 94 52-150 2-Chloroethylvinyl ether 76 10-305 Tetrachloroethene 86 64-148 Chlorobenzene 85 37-160 Trichlorofluoromethane 83 17-181 12-Dichloroethane 83 49-155 111-Trichloroethane 79 52-162 Bromodichloromethane 81 35-155 trans-13-Dichloropropene 80 17-183 cis-13-Dichloropropene 82 10-227 Bromoform 92 45-169 1122-Tetrachloroethane 93 46-157 Benzene 85 35-151 Toluene 86 47-150 Ethylbenzene 90 37-162 Chloromethane 71 10-273 Bromomethane 77 10-242 Vinyl chloride 79 10-251 Chloroethane 89 14-230 11-Dichloroethene 77 10-234 trans-12-Dichloroethene 79 54-156 cis-12-Dichloroethene 82 60-140 Trichloroethene 82 71-157 12-Dichlorobenzene 89 18-190 13-Dichlorobenzene 87 59-156 14-Dichlorobenzene 89 18-190 pm-Xylene 93 40-160 o-Xylene 92 40-160 XYLENE (TOTAL) 93 40-160 Styrene 81 40-160 Acetone 80 40-160

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 4 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    117. Check Box75 Off
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                    119. Text95 grab
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                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
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                    149. Text119 grab
                    150. Text120 624
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                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
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                    156. Check Box70 Yes
                    157. Check Box79 Off
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                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
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                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
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                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
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                    252. Text232 ND (lt50)
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                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
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                    262. Text240 ND (lt250)
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                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
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                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
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                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
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                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
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                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
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                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
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                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
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                    419. Text313 grab
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                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
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                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
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                    439. Text329 grab
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                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
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                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
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                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
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                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 25: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600756Continued

Parameter Recovery QC Criteria

Volatile Organics by GCMS 624 SPIKE for sample(s) 01 (L0600573-01 WG227088-1)Carbon disulfide 94 40-160 2-Butanone 82 40-160 Vinyl acetate 116 40-160 4-Methyl-2-pentanone 113 40-160 2-Hexanone 104 40-160 Acrolein 90 40-160 Acrylonitrile 100 40-160

Surrogate(s) Pentafluorobenzene 101 80-120 Fluorobenzene 99 80-120 4-Bromofluorobenzene 100 80-120

0125061548 Page 8 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

0125061548 Page 9 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 4 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
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                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
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                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
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                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
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                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
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                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
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                    219. Text205 grab
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                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
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                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
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                    247. Check Box169 Off
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                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
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                    267. Check Box173 Off
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                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
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                    277. Check Box175 Off
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                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
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                    287. Check Box177 Off
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                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
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                    307. Check Box181 Off
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                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
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                    314. Text282
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                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
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                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 26: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227604-1)Pesticides by GC 504 14 5041 0124 1040 0124 1229 JB

12-Dibromoethane ND ugl 0020 12-Dibromo-3-chloropropane ND ugl 0020

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 5 624 0120 1354 MM

Methylene chloride ND ugl 50 11-Dichloroethane ND ugl 15 Chloroform ND ugl 15 Carbon tetrachloride ND ugl 10 12-Dichloropropane ND ugl 35 Dibromochloromethane ND ugl 10 112-Trichloroethane ND ugl 15 2-Chloroethylvinyl ether ND ugl 10 Tetrachloroethene ND ugl 15 Chlorobenzene ND ugl 35 Trichlorofluoromethane ND ugl 50 12-Dichloroethane ND ugl 15 111-Trichloroethane ND ugl 20 Bromodichloromethane ND ugl 10 trans-13-Dichloropropene ND ugl 15 cis-13-Dichloropropene ND ugl 15 Bromoform ND ugl 10 1122-Tetrachloroethane ND ugl 10 Benzene ND ugl 10 Toluene ND ugl 10 Ethylbenzene ND ugl 10 Chloromethane ND ugl 10 Bromomethane ND ugl 50 Vinyl chloride ND ugl 20 Chloroethane ND ugl 20 11-Dichloroethene ND ugl 10 trans-12-Dichloroethene ND ugl 15 cis-12-Dichloroethene ND ugl 10 Trichloroethene ND ugl 10 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 pm-Xylene ND ugl 20 o-xylene ND ugl 10 Xylene (Total) ND ugl 20 Styrene ND ugl 10 Acetone ND ugl 10 Carbon disulfide ND ugl 50 2-Butanone ND ugl 10 Vinyl acetate ND ugl 20 4-Methyl-2-pentanone ND ugl 10

0125061548 Page 9 of 11

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
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                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
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                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
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                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 27: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600756Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227088-12)Volatile Organics by GCMS 624 contd 5 624 0120 1354 MM

2-Hexanone ND ugl 10 Acrolein ND ugl 80 Acrylonitrile ND ugl 10

Surrogate(s) Recovery QC CriteriaPentafluorobenzene 102 80-120 Fluorobenzene 104 80-120 4-Bromofluorobenzene 990 80-120

0125061548 Page 10 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

0119061636 Page 1 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 28: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

14 Methods for the Determination of Organic Compounds in Finished Drinking Waterand Raw Source Water EPA6004-88039 Revised July 1991

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0125061548 Page 11 of 11

_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
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                    66. Check Box64 Yes
                    67. Check Box65 Off
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                    69. Text67 -71174938
                    70. Text68 42380484
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                    83. Text81
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
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                    122. Text98 ND (lt50)
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                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
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                    151. Text121 2 ugL
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                    174. Text140
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                    179. Text143 grab
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                    181. Text145 10 ugL
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                    184. Text148
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                    186. Check Box73 Yes
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                    189. Text151 grab
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                    192. Text154 ND
                    193. Text155
                    194. Text156
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                    199. Text189 grab
                    200. Text190 5041
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                    202. Text192 ND (lt0019)
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                    207. Check Box161 Yes
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                    211. Text199 50 ugL
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                    213. Text201
                    214. Text202
                    215. Text203
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                    218. Text204 1
                    219. Text205 grab
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                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
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                    244. Text226
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                    259. Text237 grab
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                    264. Text242
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                    269. Text245 grab
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                    272. Text248 ND (lt250)
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                    274. Text250
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                    277. Check Box175 Off
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                    279. Text253 grab
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                    282. Text256 ND (lt250)
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                    284. Text258
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                    289. Text261 grab
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                    304. Text274
                    305. Text275
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                    309. Text277 grab
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                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
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                    319. Text285 grab
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                    339. Text301 grab
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                    349. Text33 grab
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                    354. Text40
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                    359. Text43 grab
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                    364. Text52
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                    369. Text56 grab
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                    379. Text161 grab
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                    389. Text169 grab
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                    392. Text172 ND (lt500)
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                    399. Text177 grab
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                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
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                    424. Text318
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                    449. Text337 grab
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                    452. Text340 ND
                    453. Text341
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                    467. Check Box333 Off
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                    479. Text361 grab
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                    499. Text377 grab
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                    504. Text382
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                    507. Check Box385 Off
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                    509. Text421 grab
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                    531. Text439
                    532. Text440 ND
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                    554. Text458
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                    559. Text461 grab
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                    564. Text466
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                    574. Text474
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                    579. Text477 grab
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                    584. Text482
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                    619. Text509 grab
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                    639. Text525 grab
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                    645. Text531
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                    649. Text533 grab
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                    659. Text541 grab
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                    662. Text544 ND (lt02)
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                    664. Text546
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                    669. Text549 grab
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                    679. Text557 grab
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                    689. Text583 grab
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                    699. Text591 grab
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                    703. Text595
                    704. Text596
                    705. Text597
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                    708. Text598 1
                    709. Text599 grab
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                    712. Text602 ND (lt02)
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                    714. Text604
                    715. Text605
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                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
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                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
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                    724. Text612
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                    727. Check Box573 Off
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                    729. Text615 grab
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                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
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                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
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                    744. Text628
                    745. Text629
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                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
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                    754. Text636
                    755. Text637
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                    759. Text639 grab
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                    764. Text644
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                    769. Text647
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                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
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                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 29: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIES

Eight Walkup DriveWestborough Massachusetts 01581-1019(508) 898-9220 wwwalphalabcom

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

CERTIFICATE OF ANALYSIS

Client Coler amp Colantonio Laboratory Job Number L0600518

Address 101 Accord Park Drive

Norwell MA 02061 Date Received 12-JAN-2006

Attn Mr Paul Cinquegrano Date Reported 19-JAN-2006

Project Number 11-12 Delivery Method Alpha

Site TOPS CLEANERS

ALPHA SAMPLE NUMBER CLIENT IDENTIFICATION SAMPLE LOCATION

L0600518-01 SUMP DISCHARGE BELMONT MA

I the undersigned attest under the pains and penalties of perjury that based upon my personal inquiry of those responsible

for obtaining the information the material contained in this report is to the best of my knowledge and belief accurate and

complete This certificate of analysis is not complete unless this page accompanies any and all pages of this report

Authorized by_______________________________ Technical Director

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 4 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 5 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

0119061636 Page 6 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
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                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    96. Check Box45 Yes
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                    100. Check Box51 Yes
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                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 30: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

MAM-MA086 NH200301-A CTPH-0574 MEMA086 RI65 NY11148 NJMA935 ArmyUSACE

Laboratory Sample Number L0600518-01 Date Collected 12-JAN-2006 1400 SUMP DISCHARGE Date Received 12-JAN-2006

Sample Matrix WATER Date Reported 19-JAN-2006

Condition of Sample Satisfactory Field Prep None

Number amp Type of Containers 10-Amber4-Plastic

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Solids Total Suspended 84 mgl 50 4 1602 0118 1000 DT

Cyanide Total 0035 mgl 0005 4 3352 0117 1000 0117 1549 ED

Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1505 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1224 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1357 RW

Iron Total 043 mgl 005 19 2007 0116 1840 0117 1357 RW

Lead Total 0002 mgl 0001 3 2009 0116 1840 0118 1948 PY

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 1012 DM

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1357 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1357 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2208 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1357 RW

SVOCs by GCMS 8270 1 8270C 0113 1230 0116 2007 RL

Acenaphthene ND ugl 49 Benzidine ND ugl 49 124-Trichlorobenzene ND ugl 49 Hexachlorobenzene ND ugl 49 Bis(2-chloroethyl)ether ND ugl 49 1-Chloronaphthalene ND ugl 49 2-Chloronaphthalene ND ugl 59 12-Dichlorobenzene ND ugl 49 13-Dichlorobenzene ND ugl 49 14-Dichlorobenzene ND ugl 49 33-Dichlorobenzidine ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 2 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 4 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 5 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

0119061636 Page 6 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

0119061636 Page 7 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

0119061636 Page 8 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
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                    34. Text30 Hamden
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                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    96. Check Box45 Yes
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                    100. Check Box51 Yes
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                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 31: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

24-Dinitrotoluene ND ugl 59 26-Dinitrotoluene ND ugl 49 Azobenzene ND ugl 49 Fluoranthene ND ugl 49 4-Chlorophenyl phenyl ether ND ugl 49 4-Bromophenyl phenyl ether ND ugl 49 Bis(2-chloroisopropyl)ether ND ugl 49 Bis(2-chloroethoxy)methane ND ugl 49 Hexachlorobutadiene ND ugl 98 Hexachlorocyclopentadiene ND ugl 98 Hexachloroethane ND ugl 49 Isophorone ND ugl 49 Naphthalene ND ugl 49 Nitrobenzene ND ugl 49 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 49 Bis(2-ethylhexyl)phthalate ND ugl 98 Butyl benzyl phthalate ND ugl 49 Di-n-butylphthalate ND ugl 49 Di-n-octylphthalate ND ugl 49 Diethyl phthalate ND ugl 49 Dimethyl phthalate ND ugl 49 Benzo(a)anthracene ND ugl 49 Benzo(a)pyrene ND ugl 49 Benzo(b)fluoranthene ND ugl 49 Benzo(k)fluoranthene ND ugl 49 Chrysene ND ugl 49 Acenaphthylene ND ugl 49 Anthracene ND ugl 49 Benzo(ghi)perylene ND ugl 49 Fluorene ND ugl 49 Phenanthrene ND ugl 49 Dibenzo(ah)anthracene ND ugl 49 Indeno(123-cd)pyrene ND ugl 68 Pyrene ND ugl 49 Benzo(e)pyrene ND ugl 49 Biphenyl ND ugl 49 Perylene ND ugl 49 Aniline ND ugl 98 4-Chloroaniline ND ugl 49 1-Methylnaphthalene ND ugl 49 2-Nitroaniline ND ugl 49 3-Nitroaniline ND ugl 49 4-Nitroaniline ND ugl 68 Dibenzofuran ND ugl 49 aa-Dimethylphenethylamine ND ugl 49 Hexachloropropene ND ugl 98 Nitrosodi-n-butylamine ND ugl 98 2-Methylnaphthalene ND ugl 49

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 3 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 4 of 16

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 5 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

0119061636 Page 6 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

0119061636 Page 7 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
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                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    129. Text103 grab
                    130. Text104 1664A
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                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
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                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
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                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
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                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
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                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
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                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
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                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 32: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 2007 RL

1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 98 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 98 Pentachloronitrobenzene ND ugl 98 Isodrin ND ugl 98 p-Dimethylaminoazobenzene ND ugl 98 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 98 n-Nitrosodimethylamine ND ugl 49 246-Trichlorophenol ND ugl 49 p-Chloro-m-cresol ND ugl 49 2-Chlorophenol ND ugl 59 24-Dichlorophenol ND ugl 98 24-Dimethylphenol ND ugl 98 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 98 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 68 2-Methylphenol ND ugl 59 3-Methylphenol4-Methylphenol ND ugl 59 245-Trichlorophenol ND ugl 49 26-Dichlorophenol ND ugl 98 Benzoic Acid ND ugl 49 Benzyl Alcohol ND ugl 98 Carbazole ND ugl 49 Pyridine ND ugl 49 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 370 21-120 Phenol-d6 300 10-120 Nitrobenzene-d5 640 23-120 2-Fluorobiphenyl 620 43-120 246-Tribromophenol 810 10-120 4-Terphenyl-d14 860 33-120

PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1322 RL

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

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  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
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                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
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                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
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                    52. Text51
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                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
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                    80. Text78
                    81. Text79
                    82. Text80
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                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
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                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
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                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
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                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
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                    159. Text127 grab
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                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
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                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
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                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
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                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
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                    237. Check Box167 Off
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                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
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                    244. Text226
                    245. Text227
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                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
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                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
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                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
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                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
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                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
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                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
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                    334. Text298
                    335. Text299
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                    337. Check Box187 Yes
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                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
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                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 33: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESCERTIFICATE OF ANALYSIS

Laboratory Sample Number L0600518-01 SUMP DISCHARGE

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1322 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 049 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 078 Hexachlorobenzene ND ugl 078 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 078

Surrogate(s) Recovery QC Criteria2-Fluorophenol 430 21-120 Phenol-d6 340 10-120 Nitrobenzene-d5 650 23-120 2-Fluorobiphenyl 560 43-120 246-Tribromophenol 610 10-120 4-Terphenyl-d14 580 33-120

Polychlorinated Biphenyls 5 608 0113 1045 0117 0304 SS

Aroclor 1221 ND ugl 0258 Aroclor 1232 ND ugl 0258 Aroclor 12421016 ND ugl 0258 Aroclor 1248 ND ugl 0258 Aroclor 1254 ND ugl 0258 Aroclor 1260 ND ugl 0258

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 30-150 Decachlorobiphenyl 680 30-150

Comments Complete list of References and Glossary of Terms found in Addendum I

0119061636 Page 5 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

0119061636 Page 6 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
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                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    129. Text103 grab
                    130. Text104 1664A
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                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
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                    143. Text115
                    144. Text116
                    145. Text117
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                    147. Check Box78 Off
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                    152. Text122 ND (lt50)
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                    154. Text124
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                    156. Check Box70 Yes
                    157. Check Box79 Off
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                    159. Text127 grab
                    160. Text128 624
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                    162. Text130 ND (lt50)
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                    164. Text132
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                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
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                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
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                    184. Text148
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                    186. Check Box73 Yes
                    187. Check Box82 Off
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                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
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                    196. Check Box158 Yes
                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
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                    202. Text192 ND (lt0019)
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                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    226. Check Box164 Yes
                    227. Check Box165 Off
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                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
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                    234. Text218
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                    236. Check Box166 Yes
                    237. Check Box167 Off
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                    239. Text221 grab
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                    242. Text224 ND (lt02)
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                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
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                    252. Text232 ND (lt50)
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                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
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                    262. Text240 ND (lt250)
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                    266. Check Box172 Yes
                    267. Check Box173 Off
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                    269. Text245 grab
                    270. Text246 624
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                    272. Text248 ND (lt250)
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                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
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                    282. Text256 ND (lt250)
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                    284. Text258
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                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
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                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
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                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
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                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 34: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH DUPLICATE ANALYSIS

Laboratory Job Number L0600518

Parameter Value 1 Value 2 Units RPD RPD Limits

Solids Total Suspended for sample(s) 01 (L0600451-01 WG227043-2)Solids Total Suspended 160 160 mgl 0 20

Cyanide Total for sample(s) 01 (L0600488-04 WG226776-4)Cyanide Total 0138 0137 mgl 1 30

Chlorine Total Residual for sample(s) 01 (L0600518-01 WG226604-3)Chlorine Total Residual ND ND mgl NC

TPH for sample(s) 01 (L0600518-01 WG227211-4)TPH ND ND mgl NC 34

Phenolics Total for sample(s) 01 (L0600518-01 WG226902-4)Phenolics Total ND ND mgl NC

Chromium Hexavalent for sample(s) 01 (L0600518-01 WG226611-4)Chromium Hexavalent ND ND mgl NC

Total Metals for sample(s) 01 (L0600518-01 WG226877-1)Antimony Total ND ND mgl NC Arsenic Total ND ND mgl NC Cadmium Total ND ND mgl NC Chromium Total ND ND mgl NC Copper Total ND ND mgl NC Iron Total 043 043 mgl 0 Lead Total 0002 0003 mgl 11 Nickel Total ND ND mgl NC Selenium Total ND ND mgl NC Silver Total ND ND mgl NC Zinc Total ND 0056 mgl NC

Total Metals for sample(s) 01 (L0600137-01 WG226850-3)Mercury Total ND ND mgl NC

Polychlorinated Biphenyls for sample(s) 01 (L0600518-01 WG226718-4)Aroclor 1221 ND ND ugl NC 30 Aroclor 1232 ND ND ugl NC 30 Aroclor 12421016 ND ND ugl NC 30 Aroclor 1248 ND ND ugl NC 30 Aroclor 1254 ND ND ugl NC 30 Aroclor 1260 ND ND ugl NC 30

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 510 620 30-150 Decachlorobiphenyl 680 740 30-150

0119061636 Page 6 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

0119061636 Page 7 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

0119061636 Page 8 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    10. Text10 MA
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                    13. Text13 617-965-8497
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                    15. Check Box1 Off
                    16. Check Box2 Off
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                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
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                    31. Text27 Holyoke
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                    41. Check Box39 Yes
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                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
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                    49. Text47 MADEP Jennifer Wang
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                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 35: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518

Parameter Recovery QC Criteria

Cyanide Total LCS for sample(s) 01 (WG226776-2)Cyanide Total 103 90-110

Chlorine Total Residual LCS for sample(s) 01 (WG226604-2)Chlorine Total Residual 105

TPH LCS for sample(s) 01 (WG227211-2)TPH 85 64-132

Phenolics Total LCS for sample(s) 01 (WG226902-2)Phenolics Total 94

Chromium Hexavalent LCS for sample(s) 01 (WG226611-2)Chromium Hexavalent 99

Total Metals LCS for sample(s) 01 (WG226877-4)Antimony Total 99 Arsenic Total 102 Cadmium Total 90 Chromium Total 100 Copper Total 96 Iron Total 95 Lead Total 107 Nickel Total 98 Selenium Total 102 Silver Total 104 Zinc Total 97

Total Metals LCS for sample(s) 01 (WG226850-1)Mercury Total 102

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)Acenaphthene 76 46-118 124-Trichlorobenzene 72 39-98 2-Chloronaphthalene 80 40-140 12-Dichlorobenzene 59 40-140 14-Dichlorobenzene 56 36-97 24-Dinitrotoluene 96 24-96 26-Dinitrotoluene 100 40-140 Fluoranthene 90 40-140 4-Chlorophenyl phenyl ether 84 40-140 n-Nitrosodi-n-propylamine 66 41-116 Butyl benzyl phthalate 88 40-140 Anthracene 54 40-140 Pyrene 85 26-127 Hexachloropropene 66 40-140 P-Chloro-M-Cresol 82 23-97 2-Chlorophenol 64 27-123 2-Nitrophenol 74 30-130

0119061636 Page 7 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

0119061636 Page 8 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
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                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
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                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
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                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
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                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
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                    197. Check Box159 Off
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                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
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                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
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                    237. Check Box167 Off
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                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
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                    247. Check Box169 Off
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                    249. Text229 grab
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                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
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                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
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                    267. Check Box173 Off
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                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
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                    277. Check Box175 Off
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                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
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                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
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                    295. Text267
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                    297. Check Box179 Off
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
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                    307. Check Box181 Off
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                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
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                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
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                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
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                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
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                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
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                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
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                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
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                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
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                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
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                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
                    438. Text328 1
                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
                    447. Check Box329 Off
                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
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                    462. Text348 ND (lt02)
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                    464. Text350
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                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
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                    486. Check Box336 Yes
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                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
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                    494. Text374
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                    496. Check Box338 Yes
                    497. Check Box339 Off
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                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
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                    504. Text382
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                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
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                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
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                    522. Text432 ND (lt02)
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                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
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                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
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                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
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                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
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                    572. Text472 ND (lt02)
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                    574. Text474
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                    576. Check Box398 Yes
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                    579. Text477 grab
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                    582. Text480 ND (lt02)
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                    584. Text482
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                    586. Check Box400 Yes
                    587. Check Box401 Off
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                    589. Text485 grab
                    590. Text486 8270C-M
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                    592. Text488 ND (lt02)
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                    596. Check Box402 Yes
                    597. Check Box403 Off
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                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
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                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
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                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
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                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
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                    632. Text520 ND (lt0258)
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                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
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                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
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                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 36: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

SVOCs by GCMS 8270 LCS for sample(s) 01 (WG226714-2)4-Nitrophenol 46 10-80 24-Dinitrophenol 92 30-130 Pentachlorophenol 80 9-103 Phenol 28 12-110

Surrogate(s) 2-Fluorophenol 42 21-120 Phenol-d6 37 10-120 Nitrobenzene-d5 68 23-120 2-Fluorobiphenyl 81 43-120 246-Tribromophenol 97 10-120 4-Terphenyl-d14 99 33-120

PAH by GCMS SIM 8270M LCS for sample(s) 01 (WG226715-2)Acenaphthene 59 46-118 2-Chloronaphthalene 70 Fluoranthene 84 Anthracene 56 Pyrene 92 26-127 Pentachlorophenol 72 9-103

Surrogate(s) 2-Fluorophenol 51 21-120 Phenol-d6 41 10-120 Nitrobenzene-d5 71 23-120 2-Fluorobiphenyl 57 43-120 246-Tribromophenol 61 10-120 4-Terphenyl-d14 59 33-120

Polychlorinated Biphenyls LCS for sample(s) 01 (WG226718-2)Aroclor 12421016 76 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 70 30-150 Decachlorobiphenyl 54 30-150

Cyanide Total SPIKE for sample(s) 01 (L0600455-02 WG226776-3)Cyanide Total 4 80-120

TPH SPIKE for sample(s) 01 (L0600575-01 WG227211-3)TPH 84 64-132

Phenolics Total SPIKE for sample(s) 01 (L0600384-02 WG226902-3)Phenolics Total 90

0119061636 Page 8 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
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                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
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                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
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                    53. Check Box52 Off
                    54. Check Box53 Yes
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                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    354. Text40
                    355. Text41
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                    359. Text43 grab
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                    362. Text49 ND (lt75)
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                    364. Text52
                    365. Text53
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                    369. Text56 grab
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                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
                    578. Text476 1
                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 37: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH SPIKE ANALYSES

Laboratory Job Number L0600518Continued

Parameter Recovery QC Criteria

Chromium Hexavalent SPIKE for sample(s) 01 (L0600518-01 WG226611-3)Chromium Hexavalent 95

Total Metals SPIKE for sample(s) 01 (L0600518-01 WG226877-2)Antimony Total 103 Arsenic Total 109 Cadmium Total 100 Chromium Total 100 Copper Total 104 Iron Total 97 Lead Total 116 Nickel Total 101 Selenium Total 106 Silver Total 110 Zinc Total 114

Total Metals SPIKE for sample(s) 01 (L0600137-01 WG226850-2)Mercury Total 117

Polychlorinated Biphenyls SPIKE for sample(s) 01 (L0600518-01 WG226718-3)Aroclor 12421016 63 40-140 Aroclor 1260 76 40-140

Surrogate(s) 2456-Tetrachloro-m-xylene 53 30-150 Decachlorobiphenyl 74 30-150

0119061636 Page 9 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
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                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
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                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
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                    267. Check Box173 Off
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                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
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                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
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                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
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                    294. Text266
                    295. Text267
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
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                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
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                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
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                    337. Check Box187 Yes
                    338. Text300 1
                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
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                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
                    393. Text173
                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
                    408. Text184 1
                    409. Text185 grab
                    410. Text186 8270C
                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
                    418. Text312 1
                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
                    428. Text320 1
                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
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                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
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                    448. Text336 1
                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
                    488. Text368 1
                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
                    498. Text376 1
                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
                    523. Text433
                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
                    528. Text436 1
                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
                    538. Text444 1
                    539. Text445 grab
                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
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                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
                    598. Text492 1
                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
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                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 38: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH MSMSD ANALYSIS

Laboratory Job Number L0600518

Parameter MS MSD RPD RPD Limit MSMSD Limits

SVOCs by GCMS 8270 for sample(s) 01 (L0600518-01 WG226714-4)Acenaphthene 71 71 0 30 46-118 124-Trichlorobenzene 66 66 0 30 39-98 2-Chloronaphthalene 75 75 0 30 40-140 12-Dichlorobenzene 56 61 9 30 40-140 14-Dichlorobenzene 52 56 7 30 36-97 24-Dinitrotoluene 94 94 0 30 24-96 26-Dinitrotoluene 99 94 5 30 40-140 Fluoranthene 94 89 5 30 40-140 4-Chlorophenyl phenyl ether 80 80 0 30 40-140 n-Nitrosodi-n-propylamine 61 61 0 30 41-116 Butyl benzyl phthalate 94 85 10 30 40-140 Anthracene 56 56 0 30 40-140 Pyrene 85 85 0 30 26-127 Hexachloropropene 66 66 0 30 40-140 P-Chloro-M-Cresol 78 80 3 30 23-97 2-Chlorophenol 63 66 5 30 27-123 2-Nitrophenol 73 75 3 30 30-130 4-Nitrophenol 71 71 0 30 10-80 24-Dinitrophenol 96 100 4 30 30-130 Pentachlorophenol 85 82 4 30 9-103 Phenol 40 42 5 30 12-110

Surrogate(s) 2-Fluorophenol 49 56 13 21-120 Phenol-d6 51 57 11 10-120 Nitrobenzene-d5 62 67 8 23-120 2-Fluorobiphenyl 73 74 1 43-120 246-Tribromophenol 94 93 1 10-120 4-Terphenyl-d14 96 94 2 33-120

PAH by GCMS SIM 8270M for sample(s) 01 (L0600518-01 WG226715-4)Acenaphthene 52 56 7 40 46-118 2-Chloronaphthalene 61 61 0 40 Fluoranthene 89 89 0 40 Anthracene 52 47 10 40 Pyrene 89 85 5 40 26-127 Pentachlorophenol 80 80 0 40 9-103

Surrogate(s) 2-Fluorophenol 64 71 10 21-120 Phenol-d6 61 68 11 10-120 Nitrobenzene-d5 77 83 8 23-120 2-Fluorobiphenyl 62 63 2 43-120 246-Tribromophenol 68 70 3 10-120 4-Terphenyl-d14 68 71 4 33-120

0119061636 Page 10 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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_____________________________________________________________________________________________

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
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                    10. Text10 MA
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                    13. Text13 617-965-8497
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                    15. Check Box1 Off
                    16. Check Box2 Off
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                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
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                    31. Text27 Holyoke
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                    41. Check Box39 Yes
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                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
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                    49. Text47 MADEP Jennifer Wang
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                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 39: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG227043-1)Solids Total Suspended ND mgl 50 4 1602 0118 1000 DT

Blank Analysis for sample(s) 01 (WG226776-1)Cyanide Total ND mgl 0005 4 3352 0117 1000 0117 1541 ED

Blank Analysis for sample(s) 01 (WG226604-1)Chlorine Total Residual ND mgl 005 4 3301 0112 2040 HG

Blank Analysis for sample(s) 01 (WG227211-1)TPH ND mgl 400 74 1664A 0118 1015 0119 1430 AT

Blank Analysis for sample(s) 01 (WG226902-1)Phenolics Total ND mgl 003 4 4201 0116 1100 AT

Blank Analysis for sample(s) 01 (WG226611-1)Chromium Hexavalent ND mgl 002 30 3500CR-D 0112 2140 0112 2140 HG

Blank Analysis for sample(s) 01 (WG226877-3)Total Metals 19 2007

Antimony Total ND mgl 0005 3 2009 0116 1840 0118 1452 PY

Arsenic Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Cadmium Total ND mgl 00002 4 2132 0116 1840 0118 1213 PY

Chromium Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Copper Total ND mgl 001 19 2007 0116 1840 0117 1351 RW

Iron Total ND mgl 005 19 2007 0116 1840 0117 1351 RW

Lead Total ND mgl 0001 3 2009 0116 1840 0118 1934 PY

Nickel Total ND mgl 0025 19 2007 0116 1840 0117 1351 RW

Selenium Total ND mgl 0005 19 2007 0116 1840 0117 1351 RW

Silver Total ND mgl 00002 4 2722 0116 1840 0118 2155 RC

Zinc Total ND mgl 0050 19 2007 0116 1840 0117 1351 RW

Blank Analysis for sample(s) 01 (WG226850-4)Total Metals

Mercury Total ND mgl 00002 4 2452 0116 1605 0117 0943 DM

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 1 8270C 0113 1230 0116 1827 RL

Acenaphthene ND ugl 50 Benzidine ND ugl 50

0119061636 Page 11 of 16

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_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
                    118. Text94 1
                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
                    128. Text102 1
                    129. Text103 grab
                    130. Text104 1664A
                    131. Text105 5 mgL
                    132. Text106 ND (lt4000)
                    133. Text107
                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
                    138. Text110 1
                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
                    148. Text118 1
                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
                    153. Text123
                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
                    241. Text223 02 ugL
                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
                    263. Text241
                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
                    288. Text260 1
                    289. Text261 grab
                    290. Text262 624
                    291. Text263 1 ugL
                    292. Text264 ND (lt75)
                    293. Text265
                    294. Text266
                    295. Text267
                    296. Check Box178 Yes
                    297. Check Box179 Off
                    298. Text268 1
                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
                    303. Text273
                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
                    323. Text289
                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
                    333. Text297
                    334. Text298
                    335. Text299
                    336. Check Box186 Off
                    337. Check Box187 Yes
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                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
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                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
                    353. Text39
                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
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                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
                    373. Text65
                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
                    380. Text162 624
                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
                    383. Text165
                    384. Text166
                    385. Text167
                    386. Check Box316 Yes
                    387. Check Box317 Off
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                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
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                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
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                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
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                    407. Check Box321 Off
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                    409. Text185 grab
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                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
                    413. Text309
                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
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                    419. Text313 grab
                    420. Text314 8270C
                    421. Text315 10 ugL
                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
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                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
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                    439. Text329 grab
                    440. Text330 8270C
                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
                    443. Text333
                    444. Text334
                    445. Text335
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                    447. Check Box329 Off
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                    449. Text337 grab
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                    452. Text340 ND
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                    454. Text342
                    455. Text343
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                    457. Check Box331 Off
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                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
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                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
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                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
                    473. Text357
                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
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                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
                    483. Text365
                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
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                    490. Text370 8270C-M
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                    493. Text373
                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
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                    499. Text377 grab
                    500. Text378 8270C-M
                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
                    503. Text381
                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
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                    509. Text421 grab
                    510. Text422 8270C-M
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                    512. Text424 ND (lt02)
                    513. Text425
                    514. Text426
                    515. Text427
                    516. Check Box386 Yes
                    517. Check Box387 Off
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                    520. Text430 8270C-M
                    521. Text431 015 ugL
                    522. Text432 ND (lt02)
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                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
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                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
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                    540. Text446 8270C-M
                    541. Text447 05 ugL
                    542. Text448 ND (lt02)
                    543. Text449
                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
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                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
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                    559. Text461 grab
                    560. Text462 8270C-M
                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
                    563. Text465
                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
                    568. Text468 1
                    569. Text469 grab
                    570. Text470 8270C-M
                    571. Text471 01 ugL
                    572. Text472 ND (lt02)
                    573. Text473
                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
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                    579. Text477 grab
                    580. Text478 8270C-M
                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
                    588. Text484 1
                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
                    593. Text489
                    594. Text490
                    595. Text491
                    596. Check Box402 Yes
                    597. Check Box403 Off
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                    599. Text493 grab
                    600. Text494 8270C-M
                    601. Text495 02 ugL
                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
                    613. Text505
                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
                    628. Text516 1
                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
                    641. Text527 50 ugL
                    642. Text528 ND (lt5)
                    643. Text529
                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
                    653. Text537
                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
                    657. Check Box415 Off
                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
                    661. Text543 05 ugL
                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
                    696. Check Box566 Off
                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
                    756. Check Box578 Off
                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
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                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 40: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

124-Trichlorobenzene ND ugl 50 Hexachlorobenzene ND ugl 50 Bis(2-chloroethyl)ether ND ugl 50 1-Chloronaphthalene ND ugl 50 2-Chloronaphthalene ND ugl 60 12-Dichlorobenzene ND ugl 50 13-Dichlorobenzene ND ugl 50 14-Dichlorobenzene ND ugl 50 33-Dichlorobenzidine ND ugl 50 24-Dinitrotoluene ND ugl 60 26-Dinitrotoluene ND ugl 50 Azobenzene ND ugl 50 Fluoranthene ND ugl 50 4-Chlorophenyl phenyl ether ND ugl 50 4-Bromophenyl phenyl ether ND ugl 50 Bis(2-chloroisopropyl)ether ND ugl 50 Bis(2-chloroethoxy)methane ND ugl 50 Hexachlorobutadiene ND ugl 10 Hexachlorocyclopentadiene ND ugl 10 Hexachloroethane ND ugl 50 Isophorone ND ugl 50 Naphthalene ND ugl 50 Nitrobenzene ND ugl 50 NDPADPA ND ugl 15 n-Nitrosodi-n-propylamine ND ugl 50 Bis(2-ethylhexyl)phthalate ND ugl 10 Butyl benzyl phthalate ND ugl 50 Di-n-butylphthalate ND ugl 50 Di-n-octylphthalate ND ugl 50 Diethyl phthalate ND ugl 50 Dimethyl phthalate ND ugl 50 Benzo(a)anthracene ND ugl 50 Benzo(a)pyrene ND ugl 50 Benzo(b)fluoranthene ND ugl 50 Benzo(k)fluoranthene ND ugl 50 Chrysene ND ugl 50 Acenaphthylene ND ugl 50 Anthracene ND ugl 50 Benzo(ghi)perylene ND ugl 50 Fluorene ND ugl 50 Phenanthrene ND ugl 50 Dibenzo(ah)anthracene ND ugl 50 Indeno(123-cd)pyrene ND ugl 70 Pyrene ND ugl 50 Benzo(e)pyrene ND ugl 50 Biphenyl ND ugl 50

0119061636 Page 12 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

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ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
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                    88. Check Box86 Off
                    89. Check Box87 Yes
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                    91. Text90 082906
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                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
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                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
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                    119. Text95 grab
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                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
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                    124. Text100
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                    129. Text103 grab
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                    132. Text106 ND (lt4000)
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                    134. Text108
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                    137. Check Box77 Yes
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                    139. Text111 grab
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                    141. Text113 10 ugL
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                    143. Text115
                    144. Text116
                    145. Text117
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                    149. Text119 grab
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                    154. Text124
                    155. Text125
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                    164. Text132
                    165. Text133
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                    169. Text135 grab
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                    172. Text138 ND (lt50)
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                    174. Text140
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                    179. Text143 grab
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                    181. Text145 10 ugL
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                    184. Text148
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                    189. Text151 grab
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                    199. Text189 grab
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                    214. Text202
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                    219. Text205 grab
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                    221. Text207 100 ugL
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                    229. Text213 grab
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                    239. Text221 grab
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                    249. Text229 grab
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                    257. Check Box171 Off
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                    259. Text237 grab
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                    262. Text240 ND (lt250)
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                    264. Text242
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                    269. Text245 grab
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                    272. Text248 ND (lt250)
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                    279. Text253 grab
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                    289. Text261 grab
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                    299. Text269 grab
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                    309. Text277 grab
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                    319. Text285 grab
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                    332. Text296 ND (lt250)
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                    339. Text301 grab
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                    349. Text33 grab
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                    352. Text37 ND (lt100)
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                    354. Text40
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                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
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                    364. Text52
                    365. Text53
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                    369. Text56 grab
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                    371. Text59 2 ugL
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                    379. Text161 grab
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                    382. Text164 ND (lt100)
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                    389. Text169 grab
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                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
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                    399. Text177 grab
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                    402. Text180 ND (lt100000)
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                    409. Text185 grab
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                    411. Text187 10 ugL
                    412. Text308 ND (lt003)
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                    419. Text313 grab
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                    422. Text316 ND (lt20)
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                    424. Text318
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                    429. Text321 grab
                    430. Text322 8270C
                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
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                    439. Text329 grab
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                    442. Text332 ND (lt98)
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                    449. Text337 grab
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                    451. Text339
                    452. Text340 ND
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                    459. Text345 grab
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                    462. Text348 ND (lt02)
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                    469. Text353 grab
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                    472. Text356 ND (lt02)
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                    479. Text361 grab
                    480. Text362 8270C-M
                    481. Text363 01 ugL
                    482. Text364 ND (lt02)
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                    489. Text369 grab
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                    492. Text372 ND (lt02)
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                    499. Text377 grab
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                    502. Text380 ND (lt02)
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                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
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                    516. Check Box386 Yes
                    517. Check Box387 Off
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                    519. Text429 grab
                    520. Text430 8270C-M
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                    529. Text437 grab
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                    531. Text439
                    532. Text440 ND
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                    535. Text443
                    536. Check Box390 Yes
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                    539. Text445 grab
                    540. Text446 8270C-M
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                    542. Text448 ND (lt02)
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                    545. Text451
                    546. Check Box392 Yes
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                    549. Text453 grab
                    550. Text454 8270C-M
                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
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                    554. Text458
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                    559. Text461 grab
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                    562. Text464 ND (lt02)
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                    564. Text466
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                    566. Check Box396 Yes
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                    569. Text469 grab
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                    572. Text472 ND (lt02)
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                    579. Text477 grab
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                    584. Text482
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                    589. Text485 grab
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                    599. Text493 grab
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                    609. Text501 grab
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                    615. Text507
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                    619. Text509 grab
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                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
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                    629. Text517 grab
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                    632. Text520 ND (lt0258)
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                    639. Text525 grab
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                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
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                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
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                    652. Text536 ND (lt5)
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                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
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                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
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                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
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                    668. Text548 1
                    669. Text549 grab
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                    672. Text552 ND (lt10)
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                    674. Text554
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                    676. Check Box418 Yes
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                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
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                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
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                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
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                    694. Text588
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                    697. Check Box567 Yes
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                    699. Text591 grab
                    700. Text592 2009
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                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
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                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
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                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
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                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
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                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
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                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
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                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 41: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Perylene ND ugl 50 Aniline ND ugl 10 4-Chloroaniline ND ugl 50 1-Methylnaphthalene ND ugl 50 2-Nitroaniline ND ugl 50 3-Nitroaniline ND ugl 50 4-Nitroaniline ND ugl 70 Dibenzofuran ND ugl 50 aa-Dimethylphenethylamine ND ugl 50 Hexachloropropene ND ugl 10 Nitrosodi-n-butylamine ND ugl 10 2-Methylnaphthalene ND ugl 50 1245-Tetrachlorobenzene ND ugl 20 Pentachlorobenzene ND ugl 20 a-Naphthylamine ND ugl 20 b-Naphthylamine ND ugl 20 Phenacetin ND ugl 10 Dimethoate ND ugl 20 4-Aminobiphenyl ND ugl 10 Pentachloronitrobenzene ND ugl 10 Isodrin ND ugl 10 p-Dimethylaminoazobenzene ND ugl 10 Chlorobenzilate ND ugl 20 3-Methylcholanthrene ND ugl 20 Ethyl Methanesulfonate ND ugl 15 Acetophenone ND ugl 20 Nitrosodipiperidine ND ugl 20 712-Dimethylbenz(a)anthracene ND ugl 10 n-Nitrosodimethylamine ND ugl 50 246-Trichlorophenol ND ugl 50 p-Chloro-m-cresol ND ugl 50 2-Chlorophenol ND ugl 60 24-Dichlorophenol ND ugl 10 24-Dimethylphenol ND ugl 10 2-Nitrophenol ND ugl 20 4-Nitrophenol ND ugl 10 24-Dinitrophenol ND ugl 20 46-Dinitro-o-cresol ND ugl 20 Pentachlorophenol ND ugl 20 Phenol ND ugl 70 2-Methylphenol ND ugl 60 3-Methylphenol4-Methylphenol ND ugl 60 245-Trichlorophenol ND ugl 50 26-Dichlorophenol ND ugl 10 Benzoic Acid ND ugl 50 Benzyl Alcohol ND ugl 10

0119061636 Page 13 of 16

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

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_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
                    73. Text71
                    74. Text72
                    75. Text73
                    76. Text74
                    77. Text75
                    78. Text76
                    79. Text77
                    80. Text78
                    81. Text79
                    82. Text80
                    83. Text81
                    84. Text82
                    85. Text83
                    86. Check Box84 Yes
                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
                    108. Text84 1
                    109. Text85 grab
                    110. Text86 1602
                    111. Text87 5 mgL
                    112. Text88 8400
                    113. Text91
                    114. Text92
                    115. Text93
                    116. Check Box66 Yes
                    117. Check Box75 Off
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                    119. Text95 grab
                    120. Text96 3301
                    121. Text97 20 ugL
                    122. Text98 ND (lt50)
                    123. Text99
                    124. Text100
                    125. Text101
                    126. Check Box67 Yes
                    127. Check Box76 Off
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                    130. Text104 1664A
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                    132. Text106 ND (lt4000)
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                    134. Text108
                    135. Text109
                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    139. Text111 grab
                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
                    145. Text117
                    146. Check Box69 Yes
                    147. Check Box78 Off
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                    149. Text119 grab
                    150. Text120 624
                    151. Text121 2 ugL
                    152. Text122 ND (lt50)
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                    154. Text124
                    155. Text125
                    156. Check Box70 Yes
                    157. Check Box79 Off
                    158. Text126 1
                    159. Text127 grab
                    160. Text128 624
                    161. Text129 2 ugL
                    162. Text130 ND (lt50)
                    163. Text131
                    164. Text132
                    165. Text133
                    166. Check Box71 Yes
                    167. Check Box80 Off
                    168. Text134 1
                    169. Text135 grab
                    170. Text136 624
                    171. Text137 2 ugL
                    172. Text138 ND (lt50)
                    173. Text139
                    174. Text140
                    175. Text141
                    176. Check Box72 Yes
                    177. Check Box81 Off
                    178. Text142 1
                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
                    182. Text146 ND (lt100)
                    183. Text147
                    184. Text148
                    185. Text149
                    186. Check Box73 Yes
                    187. Check Box82 Off
                    188. Text150 1
                    189. Text151 grab
                    190. Text152 624
                    191. Text153 2 ug L
                    192. Text154 ND
                    193. Text155
                    194. Text156
                    195. Text157
                    196. Check Box158 Yes
                    197. Check Box159 Off
                    198. Text188 1
                    199. Text189 grab
                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
                    203. Text193
                    204. Text194
                    205. Text195
                    206. Check Box160 Off
                    207. Check Box161 Yes
                    208. Text196 1
                    209. Text197 grab
                    210. Text198 624
                    211. Text199 50 ugL
                    212. Text200 5500
                    213. Text201
                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
                    217. Check Box163 Off
                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
                    223. Text209
                    224. Text210
                    225. Text211
                    226. Check Box164 Yes
                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
                    233. Text217
                    234. Text218
                    235. Text219
                    236. Check Box166 Yes
                    237. Check Box167 Off
                    238. Text220 1
                    239. Text221 grab
                    240. Text222 8270M
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                    242. Text224 ND (lt02)
                    243. Text225
                    244. Text226
                    245. Text227
                    246. Check Box168 Yes
                    247. Check Box169 Off
                    248. Text228 1
                    249. Text229 grab
                    250. Text230 624
                    251. Text231 2 ugL
                    252. Text232 ND (lt50)
                    253. Text233
                    254. Text234
                    255. Text235
                    256. Check Box170 Yes
                    257. Check Box171 Off
                    258. Text236 1
                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
                    262. Text240 ND (lt250)
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                    264. Text242
                    265. Text243
                    266. Check Box172 Yes
                    267. Check Box173 Off
                    268. Text244 1
                    269. Text245 grab
                    270. Text246 624
                    271. Text247 2 ugL
                    272. Text248 ND (lt250)
                    273. Text249
                    274. Text250
                    275. Text251
                    276. Check Box174 Yes
                    277. Check Box175 Off
                    278. Text252 1
                    279. Text253 grab
                    280. Text254 624
                    281. Text255 2 ugL
                    282. Text256 ND (lt250)
                    283. Text257
                    284. Text258
                    285. Text259
                    286. Check Box176 Yes
                    287. Check Box177 Off
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                    289. Text261 grab
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                    291. Text263 1 ugL
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                    294. Text266
                    295. Text267
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                    297. Check Box179 Off
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                    299. Text269 grab
                    300. Text270 624
                    301. Text271 2 ugL
                    302. Text272 ND (lt75)
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                    304. Text274
                    305. Text275
                    306. Check Box180 Yes
                    307. Check Box181 Off
                    308. Text276 1
                    309. Text277 grab
                    310. Text278 624
                    311. Text279 2 ugL
                    312. Text280 ND (lt50)
                    313. Text281
                    314. Text282
                    315. Text283
                    316. Check Box182 Yes
                    317. Check Box183 Off
                    318. Text284 1
                    319. Text285 grab
                    320. Text286 624
                    321. Text287 2 ugL
                    322. Text288 ND (lt50)
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                    324. Text290
                    325. Text291
                    326. Check Box184 Yes
                    327. Check Box185 Off
                    328. Text292 1
                    329. Text293 grab
                    330. Text294 624
                    331. Text295 2 ugL
                    332. Text296 ND (lt250)
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                    334. Text298
                    335. Text299
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                    337. Check Box187 Yes
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                    339. Text301 grab
                    340. Text302 624
                    341. Text303 2 ugL
                    342. Text304 290
                    343. Text305
                    344. Text306
                    345. Text307
                    346. Check Box308 Yes
                    347. Check Box309 Off
                    348. Text32 1
                    349. Text33 grab
                    350. Text34 624
                    351. Text36 2 ugL
                    352. Text37 ND (lt100)
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                    354. Text40
                    355. Text41
                    356. Check Box310 Yes
                    357. Check Box311 Off
                    358. Text42 1
                    359. Text43 grab
                    360. Text44 624
                    361. Text48 2 ugL
                    362. Text49 ND (lt75)
                    363. Text50
                    364. Text52
                    365. Text53
                    366. Check Box312 Yes
                    367. Check Box313 Off
                    368. Text55 1
                    369. Text56 grab
                    370. Text58 624
                    371. Text59 2 ugL
                    372. Text64 ND (lt50)
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                    374. Text158
                    375. Text159
                    376. Check Box314 Yes
                    377. Check Box315 Off
                    378. Text160 1
                    379. Text161 grab
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                    381. Text163 2 ugL
                    382. Text164 ND (lt100)
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                    384. Text166
                    385. Text167
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                    387. Check Box317 Off
                    388. Text168 1
                    389. Text169 grab
                    390. Text170 624
                    391. Text171 50 ugL
                    392. Text172 ND (lt500)
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                    394. Text174
                    395. Text175
                    396. Check Box318 Yes
                    397. Check Box319 Off
                    398. Text176 1
                    399. Text177 grab
                    400. Text178 624
                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
                    403. Text181
                    404. Text182
                    405. Text183
                    406. Check Box320 Yes
                    407. Check Box321 Off
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                    409. Text185 grab
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                    412. Text308 ND (lt003)
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                    414. Text310
                    415. Text311
                    416. Check Box322 Yes
                    417. Check Box323 Off
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                    419. Text313 grab
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                    422. Text316 ND (lt20)
                    423. Text317
                    424. Text318
                    425. Text319
                    426. Check Box324 Yes
                    427. Check Box325 Off
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                    429. Text321 grab
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                    431. Text323 5 ugL
                    432. Text324 ND(lt49)
                    433. Text325
                    434. Text326
                    435. Text327
                    436. Check Box326 Yes
                    437. Check Box327 Off
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                    439. Text329 grab
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                    441. Text331 5 ugL
                    442. Text332 ND (lt98)
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                    444. Text334
                    445. Text335
                    446. Check Box328 Yes
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                    449. Text337 grab
                    450. Text338 8270C-M
                    451. Text339
                    452. Text340 ND
                    453. Text341
                    454. Text342
                    455. Text343
                    456. Check Box330 Yes
                    457. Check Box331 Off
                    458. Text344 1
                    459. Text345 grab
                    460. Text346 8270C-M
                    461. Text347 005 ugL
                    462. Text348 ND (lt02)
                    463. Text349
                    464. Text350
                    465. Text351
                    466. Check Box332 Yes
                    467. Check Box333 Off
                    468. Text352 1
                    469. Text353 grab
                    470. Text354 8270C-M
                    471. Text355 2 ugL
                    472. Text356 ND (lt02)
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                    474. Text358
                    475. Text359
                    476. Check Box334 Yes
                    477. Check Box335 Off
                    478. Text360 1
                    479. Text361 grab
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                    481. Text363 01 ugL
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                    484. Text366
                    485. Text367
                    486. Check Box336 Yes
                    487. Check Box337 Off
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                    489. Text369 grab
                    490. Text370 8270C-M
                    491. Text371 2 ugL
                    492. Text372 ND (lt02)
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                    494. Text374
                    495. Text375
                    496. Check Box338 Yes
                    497. Check Box339 Off
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                    499. Text377 grab
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                    501. Text379 5 ugL
                    502. Text380 ND (lt02)
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                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
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                    509. Text421 grab
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                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
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                    514. Text426
                    515. Text427
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                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
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                    522. Text432 ND (lt02)
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                    524. Text434
                    525. Text435
                    526. Check Box388 Yes
                    527. Check Box389 Off
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                    529. Text437 grab
                    530. Text438 8270C-M
                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
                    537. Check Box391 Off
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                    539. Text445 grab
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                    542. Text448 ND (lt02)
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                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
                    548. Text452 1
                    549. Text453 grab
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                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
                    553. Text457
                    554. Text458
                    555. Text459
                    556. Check Box394 Yes
                    557. Check Box395 Off
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                    559. Text461 grab
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                    561. Text463 2 ugL
                    562. Text464 ND (lt02)
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                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
                    567. Check Box397 Off
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                    569. Text469 grab
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                    572. Text472 ND (lt02)
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                    574. Text474
                    575. Text475
                    576. Check Box398 Yes
                    577. Check Box399 Off
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                    579. Text477 grab
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                    581. Text479 05 ugL
                    582. Text480 ND (lt02)
                    583. Text481
                    584. Text482
                    585. Text483
                    586. Check Box400 Yes
                    587. Check Box401 Off
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                    589. Text485 grab
                    590. Text486 8270C-M
                    591. Text487 01 ugL
                    592. Text488 ND (lt02)
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                    594. Text490
                    595. Text491
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                    597. Check Box403 Off
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                    599. Text493 grab
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                    602. Text496 ND (lt02)
                    603. Text497
                    604. Text498
                    605. Text499
                    606. Check Box404 Yes
                    607. Check Box405 Off
                    608. Text500 1
                    609. Text501 grab
                    610. Text502 8270C-M
                    611. Text503 005 ugL
                    612. Text504 ND (lt02)
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                    614. Text506
                    615. Text507
                    616. Check Box406 Yes
                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
                    620. Text510 8270C-M
                    621. Text511 005 ugL
                    622. Text512 ND (lt02)
                    623. Text513
                    624. Text514
                    625. Text515
                    626. Check Box408 Yes
                    627. Check Box409 Off
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                    629. Text517 grab
                    630. Text518 608
                    631. Text519 05 ugL
                    632. Text520 ND (lt0258)
                    633. Text521
                    634. Text522
                    635. Text523
                    636. Check Box410 Yes
                    637. Check Box411 Off
                    638. Text524 1
                    639. Text525 grab
                    640. Text526 2009
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                    642. Text528 ND (lt5)
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                    644. Text530
                    645. Text531
                    646. Check Box412 Yes
                    647. Check Box413 Off
                    648. Text532 1
                    649. Text533 grab
                    650. Text534 2007
                    651. Text535 5 ugL
                    652. Text536 ND (lt5)
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                    654. Text538
                    655. Text539
                    656. Check Box414 Yes
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                    658. Text540 1
                    659. Text541 grab
                    660. Text542 2132
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                    662. Text544 ND (lt02)
                    663. Text545
                    664. Text546
                    665. Text547
                    666. Check Box416 Yes
                    667. Check Box417 Off
                    668. Text548 1
                    669. Text549 grab
                    670. Text550 2007
                    671. Text551 10 ugL
                    672. Text552 ND (lt10)
                    673. Text553
                    674. Text554
                    675. Text555
                    676. Check Box418 Yes
                    677. Check Box419 Off
                    678. Text556 1
                    679. Text557 grab
                    680. Text558 3500CR-D
                    681. Text559 10 ugL
                    682. Text560 ND (lt20)
                    683. Text561
                    684. Text562
                    685. Text563
                    686. Check Box564 Yes
                    687. Check Box565 Off
                    688. Text582 1
                    689. Text583 grab
                    690. Text584 2007
                    691. Text585 5 ugL
                    692. Text586 ND (lt10)
                    693. Text587
                    694. Text588
                    695. Text589
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                    697. Check Box567 Yes
                    698. Text590 1
                    699. Text591 grab
                    700. Text592 2009
                    701. Text593 40 ugL
                    702. Text594 2
                    703. Text595
                    704. Text596
                    705. Text597
                    706. Check Box568 Yes
                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
                    710. Text600 2452
                    711. Text601 02 ugL
                    712. Text602 ND (lt02)
                    713. Text603
                    714. Text604
                    715. Text605
                    716. Check Box570 Yes
                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
                    725. Text613
                    726. Check Box572 Yes
                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
                    736. Check Box574 Yes
                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
                    743. Text627
                    744. Text628
                    745. Text629
                    746. Check Box576 Yes
                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
                    750. Text632 2007
                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
                    753. Text635
                    754. Text636
                    755. Text637
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                    757. Check Box579 Yes
                    758. Text638 1
                    759. Text639 grab
                    760. Text640 2007
                    761. Text641
                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
                    766. Check Box580 Yes
                    767. Check Box581 Off
                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 42: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

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ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226714-1)SVOCs by GCMS 8270 contd 1 8270C 0113 1230 0116 1827 RL

Carbazole ND ugl 50 Pyridine ND ugl 50 2-Picoline ND ugl 20 Pronamide ND ugl 20 Methyl methanesulfonate ND ugl 20

Surrogate(s) Recovery QC Criteria2-Fluorophenol 490 21-120 Phenol-d6 400 10-120 Nitrobenzene-d5 760 23-120 2-Fluorobiphenyl 730 43-120 246-Tribromophenol 880 10-120 4-Terphenyl-d14 900 33-120

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M 1 8270C-M 0113 1230 0116 1237 RL

Acenaphthene ND ugl 020 2-Chloronaphthalene ND ugl 020 Fluoranthene ND ugl 020 Hexachlorobutadiene ND ugl 050 Naphthalene ND ugl 020 Benzo(a)anthracene ND ugl 020 Benzo(a)pyrene ND ugl 020 Benzo(b)fluoranthene ND ugl 020 Benzo(k)fluoranthene ND ugl 020 Chrysene ND ugl 020 Acenaphthylene ND ugl 020 Anthracene ND ugl 020 Benzo(ghi)perylene ND ugl 020 Fluorene ND ugl 020 Phenanthrene ND ugl 020 Dibenzo(ah)anthracene ND ugl 020 Indeno(123-cd)Pyrene ND ugl 020 Pyrene ND ugl 020 1-Methylnaphthalene ND ugl 020 2-Methylnaphthalene ND ugl 020 Pentachlorophenol ND ugl 080 Hexachlorobenzene ND ugl 080 Perylene ND ugl 020 Biphenyl ND ugl 020 26-Dimethylnaphthalene ND ugl 020 1-Methylphenanthrene ND ugl 020 Benzo(e)Pyrene ND ugl 020 Hexachloroethane ND ugl 080

0119061636 Page 14 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
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                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
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                    59. Check Box58 Off
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                    89. Check Box87 Yes
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                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
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                    106. Check Box63 Off
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                    704. Text596
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                    762. Text642 430
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                    768. Text646
                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 43: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESQUALITY ASSURANCE BATCH BLANK ANALYSIS

Laboratory Job Number L0600518Continued

PARAMETER RESULT UNITS RDL REF METHOD DATE IDPREP ANAL

Blank Analysis for sample(s) 01 (WG226715-1)PAH by GCMS SIM 8270M contd 1 8270C-M 0113 1230 0116 1237 RL

Surrogate(s) Recovery QC Criteria2-Fluorophenol 570 21-120 Phenol-d6 460 10-120 Nitrobenzene-d5 820 23-120 2-Fluorobiphenyl 650 43-120 246-Tribromophenol 690 10-120 4-Terphenyl-d14 740 33-120

Blank Analysis for sample(s) 01 (WG226718-1)Polychlorinated Biphenyls 5 608 0113 1045 0117 0110 SS

Aroclor 1221 ND ugl 0250 Aroclor 1232 ND ugl 0250 Aroclor 12421016 ND ugl 0250 Aroclor 1248 ND ugl 0250 Aroclor 1254 ND ugl 0250 Aroclor 1260 ND ugl 0250

Surrogate(s) Recovery QC Criteria2456-Tetrachloro-m-xylene 600 30-150 Decachlorobiphenyl 350 30-150

0119061636 Page 15 of 16

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
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                    69. Text67 -71174938
                    70. Text68 42380484
                    71. Text69
                    72. Text70
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                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
                    92. Check Box33 Off
                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
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                    113. Text91
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                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
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                    170. Text136 624
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                    174. Text140
                    175. Text141
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                    179. Text143 grab
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                    181. Text145 10 ugL
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                    184. Text148
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                    186. Check Box73 Yes
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                    190. Text152 624
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                    192. Text154 ND
                    193. Text155
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                    200. Text190 5041
                    201. Text191 001 ugL
                    202. Text192 ND (lt0019)
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                    204. Text194
                    205. Text195
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                    207. Check Box161 Yes
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                    211. Text199 50 ugL
                    212. Text200 5500
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                    214. Text202
                    215. Text203
                    216. Check Box162 Yes
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                    218. Text204 1
                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
                    222. Text208 ND (lt5000)
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
                    232. Text216 ND (lt1000)
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                    234. Text218
                    235. Text219
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                    244. Text226
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                    254. Text234
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                    259. Text237 grab
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                    264. Text242
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                    269. Text245 grab
                    270. Text246 624
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                    274. Text250
                    275. Text251
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                    284. Text258
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                    289. Text261 grab
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                    304. Text274
                    305. Text275
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                    314. Text282
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                    349. Text33 grab
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                    354. Text40
                    355. Text41
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                    359. Text43 grab
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                    364. Text52
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                    369. Text56 grab
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                    389. Text169 grab
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                    395. Text175
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                    397. Check Box319 Off
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                    399. Text177 grab
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                    401. Text179 50 ugL
                    402. Text180 ND (lt100000)
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                    404. Text182
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                    409. Text185 grab
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                    424. Text318
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                    449. Text337 grab
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                    452. Text340 ND
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                    479. Text361 grab
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                    531. Text439
                    532. Text440 ND
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                    535. Text443
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                    544. Text450
                    545. Text451
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                    564. Text466
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                    574. Text474
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                    579. Text477 grab
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                    584. Text482
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                    609. Text501 grab
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                    629. Text517 grab
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                    639. Text525 grab
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                    649. Text533 grab
                    650. Text534 2007
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                    659. Text541 grab
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                    662. Text544 ND (lt02)
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                    665. Text547
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                    669. Text549 grab
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                    679. Text557 grab
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                    689. Text583 grab
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                    692. Text586 ND (lt10)
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                    697. Check Box567 Yes
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                    699. Text591 grab
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                    704. Text596
                    705. Text597
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                    708. Text598 1
                    709. Text599 grab
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                    712. Text602 ND (lt02)
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                    714. Text604
                    715. Text605
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                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
                    723. Text611
                    724. Text612
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                    729. Text615 grab
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                    732. Text618 ND (lt5)
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                    734. Text620
                    735. Text621
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                    771. Text649
                    772. Text650
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                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 44: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is

_____________________________________________________________________________________________

_____________________________________________________________________________________________

ALPHA ANALYTICAL LABORATORIESADDENDUM I

REFERENCES

1 Test Methods for Evaluating Solid Waste PhysicalChemical Methods EPA SWshy846 Third Edition Updates I - IIIA 1997

3 Methods for the Determination of Metals in Environmental Samples SupplementI EPA600R-94111 May 1994

4 Methods for Chemical Analysis of Water and Wastes EPA 6004-79-020 Revised March 1983

5 Methods for the Organic Chemical Analysis of Municipal and Industrial Wastewater Appendix A Part 136 40 CFR (Code of Federal Regulations)

19 Inductively Coupled Plasma Atomic Emission Spectrometric Method for TraceElement Analysis of Water and Wastes Appendix C Part 136 40 CFR (Code ofFederal Regulations) July 1 1999 edition

30 Standard Methods for the Examination of Water and Wastewater APHA-AWWA-WPCF18th Edition 1992

74 Method 1664Revision A N-Hexane Extractable Material (HEM Oil amp Grease) andSilica Gel Treated N-Hexane Extractable Material (SGT-HEM Non-polar Material) by Extraction and Gravimetry EPA-821-R-98-002 February 1999

GLOSSARY OF TERMS AND SYMBOLS REF Reference number in which test method may be found METHOD Method number by which analysis was performed ID Initials of the analyst ND Not detected in comparison to the reported detection limit NI Not Ignitable ugcart Micrograms per Cartridge

LIMITATION OF LIABILITIES

Alpha Analytical Inc performs services with reasonable care and diligencenormal to the analytical testing laboratory industry In the event of an error thesole and exclusive responsibility of Alpha Analytical Inc shall be to re-performthe work at its own expense In no event shall Alpha Analytical Inc be heldliable for any incidental consequential or special damages including but notlimited to damages in any way connected with the use of interpretation ofinformation or analysis provided by Alpha Analytical Inc

We strongly urge our clients to comply with EPA protocol regarding samplevolume preservation cooling containers sampling procedures holding timesand splitting of samples in the field

0119061636 Page 16 of 16

  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
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                    66. Check Box64 Yes
                    67. Check Box65 Off
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                    69. Text67 -71174938
                    70. Text68 42380484
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                    87. Check Box85 Off
                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
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                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
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                    179. Text143 grab
                    180. Text144 624
                    181. Text145 10 ugL
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                    200. Text190 5041
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                    214. Text202
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                    230. Text214 624
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                    359. Text43 grab
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                    369. Text56 grab
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                    419. Text313 grab
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                    424. Text318
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                    439. Text329 grab
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                    449. Text337 grab
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                    479. Text361 grab
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                    564. Text466
                    565. Text467
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                    574. Text474
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                    579. Text477 grab
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                    584. Text482
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                    639. Text525 grab
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                    649. Text533 grab
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                    669. Text549 grab
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                    679. Text557 grab
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                    689. Text583 grab
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                    697. Check Box567 Yes
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                    699. Text591 grab
                    700. Text592 2009
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                    704. Text596
                    705. Text597
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                    708. Text598 1
                    709. Text599 grab
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                    719. Text607 grab
                    720. Text608 2007
                    721. Text609 10 ugL
                    722. Text610 ND (lt25)
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                    724. Text612
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                    727. Check Box573 Off
                    728. Text614 1
                    729. Text615 grab
                    730. Text616 2007
                    731. Text617 50 ugL
                    732. Text618 ND (lt5)
                    733. Text619
                    734. Text620
                    735. Text621
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                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
                    740. Text624 2722
                    741. Text625 2 ugL
                    742. Text626 ND (lt02)
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                    745. Text629
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                    747. Check Box577 Off
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                    749. Text631 grab
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                    751. Text633 10 ugL
                    752. Text634 ND (lt50)
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                    754. Text636
                    755. Text637
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                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
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                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
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                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
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                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko
Page 45: Letter re: Notice of Intent for Remediation General Permit ......system. Jenkins-Starr, LLC is considered the owner of the project. Contact information for the owner and operator is
  • Cover LetterDOC
    • United States Environmental Protection Agency
      • RE Notice of Intent for Remediation General Permit
        • Mark A Germano LSP Thomas J Motsko
            • NOI e-signedpdf
            • 11-1226 Resource Mapvsd
              • Page-1
                • Figure 2 Site Planpdf
                • Sump Discharge Jan 2006 VOCspdf
                • Sump Discharge Jan 2006pdf
                    1. Text1 Common Street Trust Property
                    2. Text2 102-104 Trapelo Road13Belmont MA 02478
                    3. Text3 -71174938
                    4. Text4 42380484
                    5. Text5
                    6. Text6 Trapelo Road13
                    7. Text7 Common Street Trust
                    8. Text8 Belmont
                    9. Text9
                    10. Text10 MA
                    11. Text11 02478
                    12. Text12 Middlesex
                    13. Text13 617-965-8497
                    14. Text14
                    15. Check Box1 Off
                    16. Check Box2 Off
                    17. Check Box3 Yes
                    18. Text15
                    19. Text16 8 Central Avenue
                    20. Text17 Newton
                    21. Text18 MA
                    22. Text19 02160
                    23. Text20 Plymouth
                    24. Text21 Coler amp Colantonio Inc
                    25. Text22 (413) 313-0131
                    26. Text23 (413) 313-0190
                    27. Text24 tmotskocol-colcom
                    28. Text25 Thomas J Motkso (Project Manager - Environmental Services)
                    29. box1
                    30. Text26 55 Bobala Road
                    31. Text27 Holyoke
                    32. Text28 MA
                    33. Text29 01040
                    34. Text30 Hamden
                    35. Check Box31 Off
                    36. Check Box32 Yes
                    37. Text35
                    38. Check Box36 Off
                    39. Check Box37 Yes
                    40. Text38
                    41. Check Box39 Yes
                    42. Check Box40 Off
                    43. Check Box41 Yes
                    44. Check Box42 Off
                    45. Check Box43 Yes
                    46. Check Box44 Off
                    47. Text45 RTN 3-23300
                    48. Text46
                    49. Text47 MADEP Jennifer Wang
                    50. Check Box48 Off
                    51. Check Box49 Yes
                    52. Text51
                    53. Check Box52 Off
                    54. Check Box53 Yes
                    55. Text54
                    56. Check Box55 Off
                    57. Check Box56 Yes
                    58. Text57
                    59. Check Box58 Off
                    60. Check Box59 Yes
                    61. Text60
                    62. Text61 discharge for two sumps located in the basement of the facility
                    63. Text62 1
                    64. Text31 016
                    65. Text63 016
                    66. Check Box64 Yes
                    67. Check Box65 Off
                    68. Text66
                    69. Text67 -71174938
                    70. Text68 42380484
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                    88. Check Box86 Off
                    89. Check Box87 Yes
                    90. Text89 052906
                    91. Text90 082906
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                    93. Check Box34 Off
                    94. Check Box35 Off
                    95. Check Box38 Off
                    96. Check Box45 Yes
                    97. Check Box46 Off
                    98. Check Box47 Off
                    99. Check Box50 Off
                    100. Check Box51 Yes
                    101. Check Box54 Off
                    102. Check Box57 Off
                    103. Check Box60 Off
                    104. Check Box61 Off
                    105. Check Box62 Off
                    106. Check Box63 Off
                    107. Check Box74 Yes
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                    117. Check Box75 Off
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                    126. Check Box67 Yes
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                    129. Text103 grab
                    130. Text104 1664A
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                    136. Check Box68 Off
                    137. Check Box77 Yes
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                    140. Text112 3352
                    141. Text113 10 ugL
                    142. Text114 35
                    143. Text115
                    144. Text116
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                    157. Check Box79 Off
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                    167. Check Box80 Off
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                    170. Text136 624
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                    200. Text190 5041
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                    214. Text202
                    215. Text203
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                    217. Check Box163 Off
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                    219. Text205 grab
                    220. Text206 624
                    221. Text207 100 ugL
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                    227. Check Box165 Off
                    228. Text212 1
                    229. Text213 grab
                    230. Text214 624
                    231. Text215 05 ugL
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                    236. Check Box166 Yes
                    237. Check Box167 Off
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                    247. Check Box169 Off
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                    249. Text229 grab
                    250. Text230 624
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                    257. Check Box171 Off
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                    259. Text237 grab
                    260. Text238 624
                    261. Text239 2 ugL
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                    269. Text245 grab
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                    277. Check Box175 Off
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                    279. Text253 grab
                    280. Text254 624
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                    289. Text261 grab
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                    299. Text269 grab
                    300. Text270 624
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                    309. Text277 grab
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                    319. Text285 grab
                    320. Text286 624
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                    327. Check Box185 Off
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                    330. Text294 624
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                    339. Text301 grab
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                    347. Check Box309 Off
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                    349. Text33 grab
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                    354. Text40
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                    359. Text43 grab
                    360. Text44 624
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                    364. Text52
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                    369. Text56 grab
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                    379. Text161 grab
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                    389. Text169 grab
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                    399. Text177 grab
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                    407. Check Box321 Off
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                    409. Text185 grab
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                    419. Text313 grab
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                    424. Text318
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                    429. Text321 grab
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                    437. Check Box327 Off
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                    439. Text329 grab
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                    449. Text337 grab
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                    451. Text339
                    452. Text340 ND
                    453. Text341
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                    457. Check Box331 Off
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                    459. Text345 grab
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                    464. Text350
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                    467. Check Box333 Off
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                    479. Text361 grab
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                    489. Text369 grab
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                    492. Text372 ND (lt02)
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                    494. Text374
                    495. Text375
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                    497. Check Box339 Off
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                    499. Text377 grab
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                    504. Text382
                    505. Text383
                    506. Check Box384 Yes
                    507. Check Box385 Off
                    508. Text420 1
                    509. Text421 grab
                    510. Text422 8270C-M
                    511. Text423 01 ugL
                    512. Text424 ND (lt02)
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                    514. Text426
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                    516. Check Box386 Yes
                    517. Check Box387 Off
                    518. Text428 1
                    519. Text429 grab
                    520. Text430 8270C-M
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                    524. Text434
                    525. Text435
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                    527. Check Box389 Off
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                    529. Text437 grab
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                    531. Text439
                    532. Text440 ND
                    533. Text441
                    534. Text442
                    535. Text443
                    536. Check Box390 Yes
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                    539. Text445 grab
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                    544. Text450
                    545. Text451
                    546. Check Box392 Yes
                    547. Check Box393 Off
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                    549. Text453 grab
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                    551. Text455 02 ugL
                    552. Text456 ND (lt02)
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                    554. Text458
                    555. Text459
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                    557. Check Box395 Off
                    558. Text460 1
                    559. Text461 grab
                    560. Text462 8270C-M
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                    562. Text464 ND (lt02)
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                    564. Text466
                    565. Text467
                    566. Check Box396 Yes
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                    569. Text469 grab
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                    572. Text472 ND (lt02)
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                    574. Text474
                    575. Text475
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                    577. Check Box399 Off
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                    579. Text477 grab
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                    584. Text482
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                    590. Text486 8270C-M
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                    604. Text498
                    605. Text499
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                    609. Text501 grab
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                    614. Text506
                    615. Text507
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                    617. Check Box407 Off
                    618. Text508 1
                    619. Text509 grab
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                    624. Text514
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                    629. Text517 grab
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                    632. Text520 ND (lt0258)
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                    638. Text524 1
                    639. Text525 grab
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                    644. Text530
                    645. Text531
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                    647. Check Box413 Off
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                    649. Text533 grab
                    650. Text534 2007
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                    652. Text536 ND (lt5)
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                    659. Text541 grab
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                    662. Text544 ND (lt02)
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                    664. Text546
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                    679. Text557 grab
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                    689. Text583 grab
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                    697. Check Box567 Yes
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                    699. Text591 grab
                    700. Text592 2009
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                    703. Text595
                    704. Text596
                    705. Text597
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                    707. Check Box569 Off
                    708. Text598 1
                    709. Text599 grab
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                    712. Text602 ND (lt02)
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                    714. Text604
                    715. Text605
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                    717. Check Box571 Off
                    718. Text606 1
                    719. Text607 grab
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                    722. Text610 ND (lt25)
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                    724. Text612
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                    727. Check Box573 Off
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                    729. Text615 grab
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                    733. Text619
                    734. Text620
                    735. Text621
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                    737. Check Box575 Off
                    738. Text622 1
                    739. Text623 grab
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                    744. Text628
                    745. Text629
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                    747. Check Box577 Off
                    748. Text630 1
                    749. Text631 grab
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                    754. Text636
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                    757. Check Box579 Yes
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                    759. Text639 grab
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                    762. Text642 430
                    763. Text643
                    764. Text644
                    765. Text645
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                    769. Text647
                    770. Text648
                    771. Text649
                    772. Text650
                    773. Text651
                    774. Text652
                    775. Text653
                    776. Check Box654 Off
                    777. Check Box655 Yes
                    778. Text656
                    779. Text657
                    780. Text658
                    781. Check Box659 Off
                    782. Check Box660 Off
                    783. Text661
                    784. Text662 Sump pumps are utilized to pump groundwater from the basement of the site building through two liquid phase GAC vessels A schematic is attached
                    785. Check Box664 Off
                    786. Check Box665 Off
                    787. Check Box666 Off
                    788. Check Box667 Off
                    789. Check Box668 Off
                    790. Check Box669 Yes
                    791. Check Box670 Off
                    792. Check Box671 Off
                    793. Text672
                    794. Text673 7
                    795. Text674 7
                    796. Text675 10
                    797. Text676 Not applicable
                    798. Check Box677 Off
                    799. Check Box678 Off
                    800. Check Box679 Yes
                    801. Check Box680 Off
                    802. Check Box681 Off
                    803. Text682
                    804. Text683 The sump pump removes water from the basement of the site is treated through GAC vessels and discharges the water to a catch basin located behind the building The runoff into the catch basin discharges into Wellington Brook approximately 05 miles from the catch basin Almost two miles down stream Wellington Brook discharges into Clay Pit Pond
                    805. Text684 A
                    806. Text685 NA
                    807. Check Box686 Off
                    808. Check Box687 Yes
                    809. Text688
                    810. Check Box689 Off
                    811. Check Box690 Off
                    812. Text691
                    813. Check Box692 Off
                    814. Check Box693 Yes
                    815. Check Box694 Off
                    816. Check Box695 Yes
                    817. Check Box696 Off
                    818. Check Box697 Yes
                    819. Check Box698 Off
                    820. Check Box699 Off
                    821. Check Box700 Off
                    822. Check Box701 Yes
                    823. Check Box702 Off
                    824. Check Box703 Yes
                    825. Text704 Section 4(e) No 7Q10 is provided The receiving water is intermittant flowing only during storm events
                    826. Text705 Common Street Trust Property
                    827. Text706 Project Manager
                    828. Text707 May 22 2006
                      1. 2006-05-22T160211-0400
                      2. Thomas J Motsko

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