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LAYSA ACP7-GA-2008-213267 Multifunctional layers for safer aircraft composite structures

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Page 1: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSAACP7-GA-2008-213267

Multifunctional layers for safer aircraft composite structures

Page 2: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

OBJECTIVE

To establish the scientific and technological basis for the development of a new multifunctional layer, based on nano-reinforcements with

-ice protection-fire protection -and health monitoring capacity

to be integrated into composite structures.

DESCRIPTION

Page 3: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA PROJECT’s INTERACTIONS

FROM NANOTECHNOLOGY

BASED PROJECTS

• Synthesis of CNTs

• Functionalisation Treatements

• Compatibilization Methods

• Dispersion Optimisation

• Adhesion Assessment

• Characterisation Procedures

FROM COMPOSITE BASED

PROJECTS

• Integration in composite structures

• Adaptation and Optimization of manufacturing processes

• Characterization Procedures

• Validation of parts

Page 4: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Electro/Thermal Functionality. Materials

UPPA-CANBIO 10%CNTs dispersions

ACG produces

7,5% CNT epoxy flims

TECNALIA set-up of buckypapers production

Φ = 70 mm Φ = 280 mm

Weight (g)

Epoxy resin CNT

Speed (rpm)

High Shear Mixer

Temperaturespeed

High Mechanical Energy Mixer

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V2

V1

CNTs doped Gelcoat from HUNSTMAN

Page 5: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Electro/Thermal Functionality. Tests TECNALIA/CU TEST SET-UP

7,5% CNTs epoxy film Epoxy infiltrated CNTs Buckypaper

Page 6: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Fire Functionality. UPPA-CANBIO/ACG/ENSCL

Need of a Thermal and Electrical insulating

layer to protect composite structure

MMT has been selected

Cone calorimeter fire test

Page 7: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Sensing Functionality. CNRS-CRPP/INASCO

Dope injection [PVA – CNT – Brij]

Drying IR

Winder

Coagulation bath [Na2SO4]

Washing bath[water]

Mercader C.©

Wet spinning process

Pilot production plant at CNRS-CRPP Facilities

CNTs Fibres

We can follow mechanical properties

changes by electrical

conductivity variations.

Sensing performance

Page 8: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Final Nanocomposite Multilayer Approach. SICOMP/TECNALIA

TECNALIA-Autoclave SICOMP-Vacuum assisted oven

Page 9: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Multilayer Prototype. ARIES COMPLEX/TECNALIA

Page 10: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

LAYSA MAIN RESULTS

Prototype Characterization. CU/ENSCL/INASCO/AERNNOVA

Experimental set-up in icing tunnel

-2 ºC < T < -15 ºC

0.3 g/m3 < LWC < 0.7 g/m3

1.04 A < I < 8.14 A

1.7 W < U < 17.8 V

P ~ 20 kW/m2

Page 11: LAYSA JEC [Modo de compatibilidad] · 1/16/2013  · LAYSA JEC [Modo de compatibilidad] Author: 102952 Created Date: 1/16/2013 4:05:03 PM

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