lab supply tradeshow presentation
TRANSCRIPT
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XRF Sample Preparation Specialists
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www.premierlabsupply.com
Profile & Mission
PREMIER is a Florida based manufacturer and supplier specializing in XRF Sample Preparation
PREMIER is committed to a primary market focus of Applications, Products, Service and Solutions for the XRF Sample Preparation Industry.
One of the Fastest Growing Manufacturer & Supplier of XRF Sample Preparations Solutions
Our steady growth & success is directly attributed to ensuring complete customer satisfaction for products & services it provides.
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Services Our company’s commitment to clients extends beyond the initial
supply of labware as it can offer a complete range of services:
Metal Exchange Program Repair and Reshaping Service Cleaning & Polishing Engraving Service Refining Services Technical Support Custom Items
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Materials Platinum and its alloys are widely utilized in the analytical
laboratory because of their unique properties. Items offered are as follows:
Platinum Platinum 5% Gold Platinum 3% Rhodium Platinum 10% Rhodium Platinum Gold Rhodium (87/3/10)
Other Metals
Gold Silver
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Crucibles Standard Form
2.5 – 700ml Larger sizes made to order Lids Reinforce rims and/or bases
Low Form Crucibles
8 – 125ml Larger sizes made to order Lids Reinforce rims and/or bases
Low Form
Standard Form
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Dishes Reinforced rim and heavy base optional. The additional cost for reinforcement is
far outweighed by longer life and ease of handling.
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Fusion Labware Manufacturers:
Claisse® Herzog Leco ® Perl’X Phoenix Shoeps Universal/Multi Vulcan
Claisse ®
Vulcan
Perl’X
Phoenix
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Specialty Items Premier can supply a wide range of specialty items to supplement
our product range of labware:
Boats Electrodes Filter Cones Foil Sheets Gauze Inoculating Loops Tongs Reshapers Pan Kits Tweezers Wire
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Applications for a wide range of industry:
• Cement• Lime• Limestone• Sand• Kiln Feed• Clinker• Mild Meal
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Fusion Applications for a Wide Range of Industry:
Iron Ores & Steel Manufacturers, Bauxite - Alumina & Aluminum industry, Mineral Sands including Rutile - Ilmenite - Zircon Glass & Ceramics Cement industry Industrial minerals - lime, limestone, dolomite, magnesite &
magnesia Geological materials such as aluminosilicates, Base metal (Pb, Zn, Cu, Ni) sulphides, sinters, silicate slags,
mattes, Ferro Alloys.
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Fusion Apparatus Multiple Position Fusion Machines:
Features: Up to 6 Samples simultaneously Auto shutdown in case of loss of pressure Individual burner selection Separate mould timer Variable speed swirling/mixing Adjustable pour delay Auto locking crucible holder Reset at any time Capable of heating heavy duty moulds (up to 150gm)
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Fusion Single Position Fusion Machines
Ideal for: Intro-Fusion Machine R & D Educational Institutions Back up Low Cost
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Fusion Fluxes Fusion Re-agents
Anhydrous, Homogenous, Pre-Fused Fluxes Easy to Handle & Weigh; Ideal fro Automatic Weighing Systems Defined Geometry & Low Loss of Ignition Non Hydroscopic Dust Free >99.98% Purity ( please ask for analysis) Specials Mixes and Fluxes on Request
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Sample Storage Sample Storage containers choices suitable for
all your reference materials prepared as pellets, glass beads or cups
Ideal for the XRF user Dust Free Dry Storage Easy Labeling for Organization
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Glassware Charging Columns Cylinders FIA Flasks Glassware repair service MCRT Vials Rams Bottom RTFO Bottles Viscometers
D-86 Flask
Rams Bottom 524
MCRT Vials
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Applications for a wide range of industry:
• Iron Ore Manufacturers• Steel Manufacturers• Slag• Silicate Slag• Magnesites• Base Metals• Sinters
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Press Powder Technique
Samples are prepared as pressed powders to improve producibility.
Tools and Accessories required: Aluminum Caps Binding/Grinding Additives Die Sets Grinder/Mixer Mill Filling Tool for Boric Acid Pellet Film Press
*Ask about our application note “Press Powder Technique”
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Hydraulic Presses for XRF Ideal for briquetting samples for XRF, XRD and Halide disks for
Infrared analysis.
Product Specifications: Max Pressure 15 / 25 tons, electrical 25 tons Pressure display 0 - 20 t / 0 - 30 t Piston 108 mm Piston Stroke, max 25 mm Bolster Screw diameter 30 mm Bolster Screw Travel, max 90 mm Minimum Distance Between Pressing Faces 35 mm Maximum Distance Between Pressing Faces 125 mm Area size D310 x W290 mm Weight 50.5 kg, electrical 60 kg
Manual
Electric
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Die SetsPremier Stainless Steel Die Sets are complete sets which
include: Detachable main body Integrated valve port A base "O" ring and plunger Two polished Stainless Steel Pellets
Applications at a Glance: Ideal for briquetting samples for XRF and XRD
analysis Ideal for briquetting Halide disks for infrared analysis Fits into most commonly used presses. High Quality Stainless Steel Material allowing Load
Limits of Up to 50 tons. Pellets offered in Stainless Steel and Tungsten Carbide
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Filling Tool/Backing Method The backing technique is commonly utilized for low quantity
samples
Tool Highlights: Ensures the sample is “centered” when poured into the die. A piston presses before filling the cellulose or boric acid on top. Produces Picture Perfect Pellets Fast Easy Clean up
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Aluminum Caps Aluminum Caps are utilized to stabilize samples from both sides. Features at a Glance:
Finest Quality Thin Wall Material ensures minimal back pressure Resistance to accidental damage Easy to handle, label and store
Taper Design
Straight-Wall Design
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Pellet Film XRD and XRF Press Pellet Advantages:
Avoids sample sticking of the die set Eliminates Chromium contamination from the die Eliminates sample dusting in Instrument Clean up is fast & easy
Hot Pressing Advantages: The use of PelletFilm allows pressing polymers using
a standard die set and press. It is not necessary to buy a hot plate Clean up is fast & easy
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Grinding & Binding Additives
Typical industries used in:
Cement Industry Sand Limestone Kiln Feed Clinker Milled Meal
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Grinding & Binding Additives
Typical industries used in: Glass & Ceramic Industry Refractories Steel Industry
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Applications for a wide range of industry:• Energy/Power• Environmental• Petrochemical• Plastics • Refineries
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Liquid Preparation XRF Sample Cups: Manufactured In-House Ability to fit many Spectrometers Contaminant - free polyethylene Disposable Standard universal sizes of:
32, 35, 40, & 45mm.
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SOP 3000 Series
1. To prepare your sample cup for analysis, you will require• an Inner Ring
(1)• an Outer Ring
(2)• and a Cap
2. Place Ring (1) with the larger end downward onto the table. Then, place the film on top.
3. Place the Outer Ring (2) on top of the Inner (1) Ring...
...And now use the PREMIER Tool to push the Ring all the way down. The hole in the middle of the Tool allows air to escape, preventing sagging of the film.
4. be certain that there are no folds or creases in the Film. It should look perfect. Now fill your cup with a liquid or solid sample. The Inner Ring contains a "Fill Line" (SC-3345: 5.5ml or 11ml; SC-3340: 9.3ml).
5. Finally, close your sample cup with the snap on cap. There is a "Labeling Area" for you to write your sample description right on the cap.