innovations in hair care - dksh...2017/03/29 · inci name amodimethicone, c11-15 pareth-7,...

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Innovations in Hair Care

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Hair Care

• Total care coconut oil in cream

• Total care sulphate free shampoo

• Total care hair conditioner

• Total care smoothening hair cream

• Total care silicone free hair serum

• Sculpting hair spray

• Free style hair gel

• Anti- frizz natural protection serum

• Volume Boost and shine shampoo

Prototypes display at CosmoTech Expo 2019

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Total care coconut oil in cream

• DKSH key ingredients:

➢ Fiberhance (Ashland)

➢ N Hance CG 17

➢ Metroark 05

➢ Belsil ADM 8105

➢ Trehalose

➢ Belsil 350

• Key product benefits:

➢ Nourishes hair.

➢ Repaire hair damage.

➢ Makes hair super

healthy, soft & strong.

➢ Improves the texture of

the hair.

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Total care coconut oil in creamTotal care coconut oil in creamDKSHIN # TCCOC 17062019

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # DCC 12062018

Phase Ingredient INCI Supplier %

A1 Aqua --------- Q.S.

A2 Ultrathix P 100 Acrylic Acid/VP Crosspolymer Ashland 0.8

A3 1,3 BG Butylene glycol Godavari 3.0

A4 ETDA -------- 0.1

B1 Cetyl alcohol Cetyl alcohol -------- 1.2

B2 Sabowax CS 20 -------- 3

B3 Glyceryl Mono Stearate Glyceryl Mono Stearate -------- 2.0

B4 Bernel Ester TCC Tricaprylyl citrate Alzo 2.0

B5 Coconut oil Coconut oil -------- 10

B6 Purolan IHD Isohexadecane 3.0

C1 N Hance CG 17 Cationic Guar Ashland 0.1

C2 Fiberhance

Hydroxypropyl Gluconamide and

hydroxypropylammonium

gluconate

Ashland 1.0

C3 Belsil ADM 8105 Amino - functional silicone Wacker 2.0

C4 Metroark 05 Cyclopentasiloxane Wacker 2.0

C5 Trehalose Trehalose Hayashibara 2.0

C6

Gujasol

Phenoxy Ethanol

& Methyl paraben

Ethyl Paraben &

Butyl Paraben &

Propyl paraben &

Isobutyl Paraben

Gujarat Organics 0.5

C7 Belsil 350

Dimethicone Wacke 2.0

C8 Perfume Fragrance

To mask odour

Of Product Qs

C9 Puricolor Red Color BASF Qs

Description:

Pink colour viscous liquid

✓ Nourishes hair ✓ Repairs hair damage

✓ Increases hydration levels

✓ Improves the texture of the hair

Key ingredients:

Fiberhance

It strengthens hair from inside the fiber by penetrating deep into the cortex and create new hydrogen and ionic bonds that support the internal keratin structure. Its improved manageability of hair.

N Hance CG 17

Conditioning polymer and thickener for hair and skin. Excellent combing and wet and dry feel on hair.

Metroark 05

It is clear colourless fluid of low viscosity. It support easy spreading of high viscosity fluid and gums, improving wet combability

Procedure:

1 Initially take 2/3 quantity of water & add 1,3 BG in manufacturing vessel & heat upto 70 – 75 deg C.

2 In another beaker take cetyl alcohol, sabowax cs 20, GMS, coconut oil, bernel ester TCC, puolan IHD & heat it up to 70 – 75 deg C.

3 Weigh Ultrathix P-100 to the water phase to mixed well & add TEA in it with continuos stirring.

4 Then add phase oil phase to water phase under continuous stirring to get an emulsion.

5 Add N Hance CG 17 in remaining water mixed and add in emulsion.

6 At 400 C, add fiberhance, belsil DM 350, trehalose, metroark 05, belsil ADM 8105 with stirring.

7 Finally add perfume, color & adjust the product pH 4.5 - 5.5.

Specification

pH = 5.38 – Brookfield DV-II+Pro # RV , Viscosity - 24000 cps, Spindle -04, Speed - 10 rpm

Appearance – Pink colour viscous liquid

Stability test : Product has Successfully completed one months stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

Indian standards

DKSH India JUNE 2019

Formulation number:

DKSHIN # TCCOC 17062019

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➢ Fiberhance and Metroark 05

fiberHance™ bm solution - mechanism of action

the α-helix protein structure in the hair fiber provide the strength to the hair in weak hair the bonds are broken and missing fiberhance™ builds new bonds within and across the structure (dual mechanisms)

fiberHance™ bm solution: new to the world small molecule in which the chemical structure and dimension have been specifically designed to optimize multi-bond interactions within the hair keratin cortex

internal hydrogen bonding within the α-helix

the α-helix protein structure in the hair fiber provide the strength to the

Hydrogen bonding between α-helixs

Wacker- Belsil®

D5

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Metroark 05 Fluid Cyclopentasiloxane

Characteristics

Metroark 05 Fluid is a clear, colourless fluid of low viscosity, and high

volatility. It is non-polar and insoluble in water but miscible with

mineral oils, alcohols, Esters and other

solvents frequently utilised in personal-care formulations. Due to

its low heat of vaporisation, Metroark 05 Fluid evaporates from the

skin without producing a cooling or stinging effect.

Applications

Chemical Structure

CH3

Si O

CH3 n

Metroark 05 Fluid can be utilized as a delivery system in

antiperspirant and deodorant formulations as well as cuticle-coat

products and colour cosmetic compositions.

Metroark 05 Fluid acts as a diluents or carrier, helping to uniformly

spread actives and pigments over the surface of hair and skin. It

provides sufficient playtime in colour cosmetics applications, thereby

improving rub-in properties, reducing stickiness, and imparting

lubricity and a smooth skin feel.

In hair-care products, the carrier/carrier Metroark 05 Fluid supports

easy spreading of high viscosity fluids and gums, improving wet

combability, and functions as resin plasticiser in fixative products.

To alter drying times for specific product requirements, Metroark

05 Fluid may be blended in all proportions with dimethicone fluids

eg. Wacker Belsil DM 0.65 and DM 1 plus and other

cyclomethicone fluids

Storage stability

Undiluted Metroark 05 Fluid have a shelf life of at

least 12 months from the date on the delivery

note if stored in tightly closed original containers

between 5 & C and 30

& C.

The containers must be protected against sunlight. Stir well before use. If the material

is kept beyond the shelf life recom-mended

on the product label, it is not necessarily

unusable, but a quality control should be

performed on the properties relevant to the

application.

Safety Information

Detailed safety information is contained in

each Material Safety Sheet , which can be

obtained from our sales offices

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➢ Belsil ADM 8105 and Trehalose

BELSIL® ADM 8105 E A M I N O - F U N C T I O N A L S I L I C O N E

Product description

BELSIL® ADM 8105 E is a nonionic microemulsion of

an aminofunctional polydimethylsiloxane.

Application

BELSIL® ADM 8105 E is an efficient conditioning

agent in hair care applications. BELSIL® ADM 8105 E

provides a silky touch and strongly reduces dry and

wet combing forces. The product is suitable for rinse -

off conditioners, hair treatments, masks, pump sprays

and conditioning shampoos for strongly damaged hair.

BELSIL® ADM 8105 E also allows the formulation of

transparent products.

Processing

Recommended use levels of BELSIL® ADM 8105 E in

hair conditioner formulations are 2.0 % to 10 %. In

shampoos, a use level of 1.0 % to 2.5 % is

recommended. The micro emulsion should be

formulated at temperatures below 35 °C.

The emulsion needs to be stirred well before use.

Storage

Minimum temperature allowed during storage and

transportation:

0 °C

Maximum temperature allowed during storage and

transportation:

35 °C

The 'Best use before end' date of each batch is shown

on the product label.

Storage beyond the date specified on the label does

not necessarily mean that the product is no longer

usable. In this case however, the properties required

for the intended use must be checked for quality

assurance reasons.

Safety notes

Comprehensive instructions are given in the

corresponding Material Safety Data Sheets. They are

available on request from WACKER subsidiaries or

may be printed via W ACKER web site

http://www.wacker.com.

.

Product data

Specification data Inspection Method Value

pH-Value at 25 °C Indicator strips approx. 5,0

Typical general characteristics Inspection Method Value

Appearance Translucent Liquid

Active ingredients content approx. 20 %

Preservative Phenoxyethanol

Emulsifier Nonionic

INCI name Amodimethicone, C11-15

Pareth-7, Laureth-9,

Glycerin, Trideceth-12

Technical data sheet for BELSIL® ADM 8105 E / Version: 1.0 / Date of last alteration: 29.03.2017 1 / 2

Trehalose from Hayashibara is nature’s

protector. Trehalose is a naturally

occurring saccharide present in a wide

variety of plant

and animal life, enabling survival in the

harshest climatic conditions.

The presence of trehalose in plants is one of

the reasons why a barren desert blooms after a

rain. A good example of this protection is

represented in the “Resurrection plant” –

selaginella lepidophylla. Natural trehalose

protects the

plant when it is dehydrated, allowing it to “come

back to life” when the plant comes in

contact with water.

We can make use of this natural function of

trehalose to help protect against human skin

and hair damage caused by exposure to harsh

and changing environments.

High stability

Trehalose from

Hayashibara is

a white crystalline

powder. Trehalose consists of two

glucose molecules bonded by a α,α−1,1 glycosidic linkage. As such it is a non-

reducing sugar, and is very stable over

extremes of pH and temperature.

Readily soluble

Trehalose is readily soluble and provides

moisture retention and protein protection

when used in skin and hair care products.

Because of its molecular structure, trehalose is

highly stable during the manufacture of

products.

Trehalose can also improve product shelf-life,

due to its ability to inhibit the formation of any

volatile aldehydes caused by the breakdown

of fatty acids.

for skin and hair protection Trehalose from Hayashibara protects skin

fibroblasts from dehydration because it

replaces water in tissues helping to retain the

natural structure of skin and hair. Thus it can

be used as an effective moisturiser affording

protection from potentially damaging climatic

conditions.

This is because trehalose replaces water in

tissue and reduces the damage from dryness,

heat and cold – retaining the natural structure

of the skin and hair.

This has been demonstrated under laboratory

conditions in which human skin fibroblasts

were cultured with or without trehalose or

maltose.

Trehalose provided the greatest protection.

Method: Culture media with or without 1% of trehalose or maltose was incubated on human fibroblasts

for 12 hours after confluence. The culture media was removed and the cells stored at room temperature

for 3 hours. Cell viability was measured.

© DKSHPage 7

Belsil 350

Technical data sheet for BELSIL® DM 350 / Version: 1.2 / Date of last alteration: 19.06.2012 1 / 2

BELSIL® DM 350 D I M E TH IC ON E

Product description

Structural formula:

BELSIL® DM 350 is a linear, non-reactive, unmodified

polydimethylsiloxane. BELSIL® DM 350 is

characterized by low surface tension and a high

spreading coefficient. Due to their flexible polymer

backbone, dimethicones have high permeability to

gases (e.g. water vapor, oxygen), which allows

respiration of the skin.

Application

BELSIL® DM 350 is used in a broad range of personal

care formulations as an emollient. It allows formulators

to adjust spreadability and conditioning effects.

Whitening and stickiness of cosmetic products can be

reduced and skin feel can be optimized.

Storage


transportation:

50 °C







assurance reasons.

Safety notes




may be printed via WACKER web site


Product data

Typical general characteristics Inspection Method Value Appearance

colorless, clear

Viscosity, kinematic at 25 °C DIN 53019 approx. 350 mm²/s

Density at 25 °C DIN 51757 approx. 0,97 g/cm³

Refractive index at 25 °C 1,4035

Flash point ISO 2592 > 300 °C

Surface tension at 25 °C 0,021 N/m

Ignition temperature (liquids) DIN 51794 approx. 450 °C

Aggregate state liquid

INCI name Dimethicone

These figures are only intended as a guide and should not be used in preparing specifications.

© DKSHPage 8

Total care sulphate free shampoo


➢ N Durhance AA

2000(Ashland)

➢ Pionin (Hayashibara)


➢ Stepanquat ml (Stepan)

➢ N Hance CG 17

(Ashland)


➢ Protects hair against

future damage

➢ Leaves hair feeling

soomther & shiner

➢ Improves hair texture

➢Prevent hair fall

➢Works gently on your hair

from root to tip

© DKSHPage 9

Total care sulphate free shampooTotal care sulphate free shampooDKSHIN # TCSFS 31052019


DKSHIN # CVPS 15022017


A1 Aqua _____ --------- Q.S.

A2 N Hance CG 17 Cationic Guar Ashland 0.2

B1 Amphosol HCG Cocamidopropyl Betaine Stepan 17

B2 Bio Terge AS 40 Sodium C14-16 olefin sulfonate Stepan 36

B3 Sabowax EGDS Glycol Distearate Sabo 2.0

B4 Ninol CAA Dimethyl Lauramide/Myristamide Stepan 1.8

B5 Stepan Mild L3 Lauryl Lactyl Acetate Stepan 0.5

C1N Durhance AA 2000

Acrylamidopropyltrimonium

chloride/Acrylamide crosspolymer Ashland 1.0

C2Belsil ADM 331

Hydroxypropyl gluconamide &

Hydroxypropylammonium gluconate Wacker 1.5

C3 Pionin Quaternium - 73 Hayashibara 1.0

C4 Fiberhance


hydroxypropylammonium gluconate Ashland 1.0

C5 Belsil 60082

Dimethiconal TEA-

Dodecylbenzenesulfonate Wacker 2.0

C6 Ceraphyl 41 Ester C 12-15 Alkyl Lactate Ashland 2.0

C7 Stepanquat ml Quaternium 82 Stepan 2.0

C8 Rokosal S1

Methylchloroisothiazolineand

methylisothiazoline Ashland 0.5

C9 Glycerine Glycerine 3.0

C10 Belsil DM 350 Dimethicone Wacker 2.0

C11

Perfume Fragrance

To mask

Odour of

product

QS

Description:

Lavender coloured Pearly Shampoo

✓ Protects hair against future damage✓ Leaves hair feeling soomther & shiner✓ Improves hair texture✓ Prevent hair fall

Key ingredients:

N Durhance AA 2000

It is conditioning polymer. It has been developed to provide long lasting damage repair and restore hair to its natural hydrophobic state. Protects against harmful effect of pollution and urban stress.

Fiberhance


Pionin

It acts as Anti – dandruff agent

N Hance CG 17


Steapanquat ml

It is quaternary for formulation in hair conditioners, hair styling cream and lotions. It is conditioning agent for hair care formulations.

Procedure:

1 Initially take water in Beaker and add N Hance CG 17 and 2- 3 drpos of citric acid stir it.

2 In another seprate beaker take sabowax EGDS, bio terge, amphosol HCG, ninol CAA, CAPB, stepan mild and heat upto 80 deg c until

solid is dispersed.

3 Add B phase to A phase under constant stirring

4

At 400 C, add pionin, fiberhance, N durhace AA 2000, ceraphyl 41 ester, belsil adm 331, belsil 350, belsil 60082, glycerine,

steapanquat ml and rokonsal S 1 mix well with stirring

5 Finaly add perfume with stirring & adjust the product pH 6 - 7

Specification

pH = 6.47 – Brookfield DV-II+Pro # RV, Viscosity – 9090 cps, Spindle -04, Speed - 20 rpm

Appearance – Lavender coloured Pearly Shampoo

Stability test : Product has Successfully completed one and half months stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH

as per Indian standards

DKSH India MAY 2019

Formulation number:

DKSHIN # TCSFS 31052019

© DKSHPage 10

➢ N Durhance AA 2000 and Pionin

N-DurHance ™ AA2000damaged hair repair

Mechanism ISCF™ In Situ controlled Flocculation

The positively charged N-DurHance AA2000 polymer is attracted to the highly damaged negatively charged hair leaving the hair with an excess of positive charge.

Hair is shampooed (with or without silicones) and the anionic surfactants (SLES) form flocculates on hair surface (in-situ) with the cationic polymer. During flocculate formation, hydrophobic lauryl groups from SLES coat the hair surface, creating a hydrophobic layer on the hair surface (no need necessarily for silicones). If there are silicones or other oils present in the shampoo, they are attracted to the hair surface during the flocculate formation (boosting of silicone deposition).

FFuunnccttiioonnss ooff PPIIOONNIINN™™

• Antimicrobial Effectiveness

Anti-Acne

Antiseptic

© DKSHPage 11

➢ Fiberhance and Stepanquat ML

STEPANQUAT™ ML in

Hair Care Products

Uniqueness and Benefits

Delivers excellent detangling, wet and dry

combability as well as hair feel

◦ laboratory experiments on hair tresses

expert panel

Dia-Stron

◦ salon data

Enhances performance of hair conditioners

containing other quats - 7 -

© DKSHPage 12

Belsil 60082 and Belsil ADM 331

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BELSIL®

DM 60082M Dimethiconol Emulsion ( INCI NAME - Dimethiconol and TEA-Dodecylbenzenesulfonate )

Characteristics

BELSIL®

DM 60082M is an anionic/non-ionic emulsion of a high-viscosity dimethiconol (approx. 1000000 to 1800000 mm

2 /s).

Applications

The main field of application for BELSIL®

DM 60082Mis in hair care. BELSIL

® DM 60082M is excellent condi-

tioning additives, especially when formulated into rinse-off as well as leave-in conditioners. They improve wet and dry combability as well as the wet and dry feel of the hair. BELSIL

® DM 60082M also provides

conditioning benefits when used in other formulations such as shampoos and styling aids. The recommended amount to use is 2 – 7 %.

Storage stability

Undiluted BELSIL®

DM 60082M have a shelf life of at least 12 months from the date on the delivery note if stored in tightly closed original containers between 5ºC and 30ºC. The containers must be protected against sunlight. Stir well before use. If the material is kept beyond the shelf life recommended on the product label, it is not necessarily unusable, but a quality control should be performed on the properties relevant to the application.

Chemical Structure

Me Me Me

HO Si O Si O Si OH

Me Me Me n

Safety Information

Detailed safety information is contained in each Material Safety Sheet, which can be obtained from our sales offices

BELSIL®

Seite 1 von 2

BELSIL®ADM 331

INCI NAME: Amodimethicone (and) Trideceth-12 (and) Cetrimonium chloride

Characteristics

BELSIL®

ADM 331 is an oil-in-water macro-emulsion of an amodimethicone fluid of low amine content, containing a cationic/nonionic surfactant pair. Due to the chemical structure of the aminofunctional active ingredient and the emulsifier system, BELSIL

® ADM 331 has excellent affinity as a

conditioner for hair care application

Applications

The most important field of application of BELSIL®

ADM 331 is hair care, especially in hair conditioning. The ability of amodimethicone to coat and protect hair is particularly evident in shampoo and conditioner formulations. They also improve wet and dry combability and provide a soft feel to Hair. BELSIL

® ADM 331 does not lead to an unde-

sirable build-up effect even after repeated use because it is easily re-emulsified and thus easily

washed out. BELSIL

® ADM 331 is also suitable for hair condi-

tioning formulation and the recommended amount varies from 1-5 % depending on the formulation.

Storage stability

BELSIL®

ADM 331 have a shelf life of at least 12 months from the date on the delivery note if stored in tightly closed original containers between 5˚C and 30˚C. The containers must be protected against sunlight. Stir well before use. If the material is kept beyond the shelf life recommended on the product label, it is not necessarily unusable, but a quality control should be performed on the properties relevant to the application.

Chemical Structure

Safety Information

Detailed safety information is contained in each Material Safety Sheet , which can be obtained from our sales offices

© DKSHPage 13

Total care hair conditioner


➢ N DurHance AA 2000

(Ashland)

➢ Fiberhnce

➢ N Hance BF17 (Ashland)

➢ Steapanquat ML

➢ Belsil 60082

➢ Belsil ADM 331


➢ Imparts shine lustre.

➢ Repairs hair damage.

➢ Increases hydration level.

➢Prevents hair breakage.

➢Deeply nourishes

damaged hair from root

to tip.

© DKSHPage 14

Total care hair conditionerTotal care hair conditionerDKSHIN # TCHC30052019




A1 Aqua --------- Q.S.

A2 1,3 BG Butylene glycol Godavari 4.0

A3 Ultrathix P-100 Acrylic Acid/VP Crosspolymer Ashland 0.8

A4 Miconium BTAC 80 Behentrimonium Chloride Miwon 1.5

A6 TEA Triethanolamine ---------

A7 D. EDTA Disodium EDTA ---------

B1 Cetyl alcohol Cetyl alcohol --------- 4.0

B2 Prolipid 161

Behenyl alcohol(and)Cetearyl

alcohl(and)Hydroxyethyl

cetearamidoprpyldimonium chloride

Ashland 3.0

B3 Purolan IHD Isohxadecane Lanxes 2.0

C1 N Hance BF 17 Cationic Guar Ashland 0.1

C2 N Durhance AA 2000 Acrylamidopropyltrimonium

chloride/Acrylamide crosspolymer Ashland 1.0

C3Fiberhance



C4 Miconium CTAC 29 Cetrimonium Chloride Miwon 1.5

C5 Steapanquat ml Quaternium 82 Stepan 2.0

C6Belsil 60082

Dimethiconal TEA-

Dodecylbenzenesulfonate Wacker 2.5

C7 Belsil ADM 331

Hydroxypropyl gluconamide &

Hydroxypropylammonium gluconate Wacker 2.0

C8 Optiphen 200

Phenoxyethenol(and)Caprylyl Glycol Ashland 0.75


To mask odour

Of Product Qs

Description:

White coloured glossy soft cream

✓ Imparts shine & lustre

✓ Repairs hair damage


✓ Prevents hair breakage

Key ingredients:

N-Durhance AA2000

It is a A highly charged cationic copolymer of Acrylamide-N-propyl trimethylammonium chloride/ Acrylamide. It provides long-lasting hair damage repair, Improves dry and wet conditioning for smooth and silky hair.

Fiberhnce

It strengthens hair from inside the fiber by penetrating deep into the cortex and create new hydrogen and ionic bonds that support the internal keratin structure. Its improved manageability of hair. .

N Hance BF 17


Steapanquat ml


Procedure:

1 Initially take 2/3 quantity of water & add 1,3 BG, EDTA in manufacturing vessel & heat upto 70 – 75 deg C.

2 In another beaker take cetyl alcohol, prolipid 161, purolan IHD & heat it up to 70 – 75 deg C.

3 Weigh Ultrathix P-100 and add water phase to mixed well & add TEA in it with continuos stirring.

4 Then add phase oil phase to water phase under continuous stirring to get an emulsion.

5 Add N Hance BF 17 in remaining water mixed well and add in emulsion.

6 At 400 C, add N Durhance AA 2000, fiberhance, miconium CTAC 29, stepanquat ml, belsil 60082, belsil ADM 331, optiphen 200 with

stirring.

7 Finally add perfume & adjust the product pH 4.5 - 5.5.

Specification

pH = 5.30 – Brookfield DV-II+Pro # RV, Viscosity - 31452 cps, Spindle -04, Speed - 10 rpm

Appearance – White coloured glossy soft cream



DKSH India May 2019

Formulation number:

DKSHIN # TRC30052019

© DKSHPage 15

N DurHance AA 2000 and Fiberhnce

© DKSHPage 16

Steapanquat ml and Belsil ADM 331

© DKSHPage 17

Belsil ADM 331

© DKSHPage 18

Total care smoothening hair cream



➢ Steapanquat ml(Stepan)

➢ Belsil CM 1000 (Wacker)

➢ Metroark 05(Wacker)

➢ Belsil DM 350

➢ Trehalose

➢ Vegetable Petrolatum 67


➢ Nourishes hair

➢ Repairs hair damage

➢ Increases hydration

levels

➢ Improves the texture of

the hair

➢ Retains moisture and

gets rid of split ends.

➢

© DKSHPage 19

Total care smoothening hair creamTotal Care Smoothening Hair CreamDKSHIN # TCSHC 06072019




A1 Aqua --------- Q.S.


A3 TEA Triethanolamine --------- Q.S.

B1 Cetyl alcohol Cetyl alcohol --------- 2.0

B2 Sabowax CS 20 Ceteareth- 20 Sabo 2.0

B3 Glycerylmonostearate Glycerylmonostearate --------- 2.0

B4 Argan Butter Argania spinosa (argan)kernel oil and

hydrogenated vegetable oil Efp Biotek 0.5

B5 Vegetable Petrolatum 67

Ricinus communis(castor) seed oil and

hydrogenated castor oil and

copernicia cerifera(carnauba)wax

Efp Biotek 3.0

C1 Fiberhance Hydroxypropyl Gluconamide and



C3Trehalose

Maltooligosyl glucoside and

hydrogenated starch hydrolysate Hayashibara 2.0

C4 Steapanquat ml Quaternium 82 Stepan 1.4

C5 Optiphen 200 Phenoxyethanol and Caprylyl Glycol Ashland 0.75

C6 Belsil CM 1000 Cyclopentasiloxane, Dimethiconal Wacker 5

C7 Metroark 05 Cyclopentasiloxane Wacker 2


To mask odour

Of Product QS

Description:

White coloured glossy cream

✓ Nourishes hair ✓ Repairs hair damage


✓ Improves the texture of the hair

Key ingredients:

Fiberhance


Steapanquat ml


Belsil CM 1000

In hair-care products yields sleek, shiny hair. Damaged hair regains a natural, healthy appearance. Wet and dry combability are improved, and further damage to the hair cuticles is prevented. It is also widely used in hair-tip fluids.

Metroark 05

It is clear colourless fluid of low viscosity. It support easy spreading of high viscosity fluid and gums, improving wet combability.

Procedure:

1 Initially take total quantity of water and add Ultrathix P 100 and TEA in it continuons stirring & heat it up to 70 – 75 deg C.

2 In another beaker take cetyl alcohol, sabowax cs 20, argan butter, GMS, vegetable petroltum 67 & heat it up to 70 – 75 deg C.

3 Then add oil phase in to water phase Under agitation.

4

At 400 C, add Trehalose, Belsil DM 350, stepanquart ml, fiberhance, metroark 05, belsil cm 1000 & optiphen 200 under constant

stirring.

5 Finally add perfume with stirring & adjust the product pH 4.5- 5.5

Specification

pH = 5.41 – Brookfield DV-II+Pro # RV, Viscosity - 31500cps, Spindle -04, Speed - 10 rpm

Appearance – White coloured glossy cream



DKSH India June 2019

Formulation number:

DKSHIN # TCSHC 06072019

© DKSHPage 20

Fiberhance and Steapanquat ml

© DKSHPage 21

Belsil CM 1000 and Metroark 05

Version 2.0 / 19-08-03 / CS Page 1 / 2

Wacker-Belsil®

CM 1000 Cyclopentasiloxane, Dimethiconol

Characteristics Wacker-Belsil® CM 1000 is a blend of cylcopenta- siloxane and a high molecular silicone gum. Due to its composition, it combines the properties of the low- viscose , volatile fluid, cyclopentasiloxane and the extremely high-viscose dimethiconol. The excellent spreading of cyclopentasiloxane allows a good distribution of the high-viscose conditioning agent dimethiconol.

Application Wacker-Belsil® CM 1000 is used in hair care and in skin care applications. Skin-care and skin-protection preparations containing Wacker-Belsil® CM 1000 impart a pleasant, supple feel to skin; it eases the distribution of the formulations and

improves skin elasticity. At the same time, it forms a water-resistant, but breathable protective barrier. This provides good substantivity and fixation of active ingredients. Use of Wacker-Belsil® CM 1000 in hair-care products yields sleek, shiny hair. Damaged hair regains a natural, healthy appearance. Wet and dry combability are improved, and further damage to the hair cuticles is prevented.

Storage Wacker-Belsil® CM 1000 has a shelf life of at least 12 months when stored between 5°C and 40°C in the originally sealed container. The 'Best use before end' date of each batch appears on the product label.

Storage beyond the date specified on the label does not necessarily mean that the product is no longer usable.

In this case however, the properties required for the intended use must be checked for quality assurance reasons.

Chemical structure

Safety information Detailed safety information is contained in each material safety data sheet, which can be obtained from our sales offices.

Product data

Properties Unit Wacker-Belsil®

CM 1000

Appearance colorless, clear

Viscosity approx. [mm2/s] 5200

Refractive index

Density

approx.

approx.

n 25

D

[g/cm3]

1.398

0,96Solids content approx. [%] 18

INCI name Cyclopentasiloxane, Dimethiconol

Wacker- Belsil®

D5

Seite 1 von 2

Metroark 05 Fluid Cyclopentasiloxane

Characteristics

Metroark 05 Fluid is a clear, colourless fluid of low viscosity, and high

volatility. It is non-polar and insoluble in water but miscible with

mineral oils, alcohols, Esters and other

solvents frequently utilised in personal-care formulations. Due to

its low heat of vaporisation, Metroark 05 Fluid evaporates from the

skin without producing a cooling or stinging effect.

Applications

Chemical Structure

CH3

Si O

CH3 n

Metroark 05 Fluid can be utilized as a delivery system in

antiperspirant and deodorant formulations as well as cuticle-coat

products and colour cosmetic compositions.

Metroark 05 Fluid acts as a diluents or carrier, helping to uniformly

spread actives and pigments over the surface of hair and skin. It

provides sufficient playtime in colour cosmetics applications, thereby

improving rub-in properties, reducing stickiness, and imparting

lubricity and a smooth skin feel.

In hair-care products, the carrier/carrier Metroark 05 Fluid supports

easy spreading of high viscosity fluids and gums, improving wet

combability, and functions as resin plasticiser in fixative products.

To alter drying times for specific product requirements, Metroark

05 Fluid may be blended in all proportions with dimethicone fluids

eg. Wacker Belsil DM 0.65 and DM 1 plus and other

cyclomethicone fluids

Storage stability

Undiluted Metroark 05 Fluid have a shelf life of at

least 12 months from the date on the delivery

note if stored in tightly closed original containers

between 5 & C and 30

& C.

The containers must be protected against sunlight. Stir well before use. If the material

is kept beyond the shelf life recom-mended

on the product label, it is not necessarily

unusable, but a quality control should be

performed on the properties relevant to the

application.

Safety Information

Detailed safety information is contained in

each Material Safety Sheet , which can be

obtained from our sales offices

© DKSHPage 22

Belsil DM 350 and Trehalose

Technical data sheet for BELSIL® DM 350 / Version: 1.2 / Date of last alteration: 19.06.2012 1 / 2

BELSIL® DM 350 D I M E TH IC ON E

Product description

Structural formula:

BELSIL® DM 350 is a linear, non-reactive, unmodified

polydimethylsiloxane. BELSIL® DM 350 is

characterized by low surface tension and a high

spreading coefficient. Due to their flexible polymer

backbone, dimethicones have high permeability to

gases (e.g. water vapor, oxygen), which allows

respiration of the skin.

Application

BELSIL® DM 350 is used in a broad range of personal

care formulations as an emollient. It allows formulators

to adjust spreadability and conditioning effects.

Whitening and stickiness of cosmetic products can be

reduced and skin feel can be optimized.

Storage


transportation:

50 °C







assurance reasons.

Safety notes




may be printed via WACKER web site


Product data

Typical general characteristics Inspection Method Value Appearance

colorless, clear

Viscosity, kinematic at 25 °C DIN 53019 approx. 350 mm²/s

Density at 25 °C DIN 51757 approx. 0,97 g/cm³

Refractive index at 25 °C 1,4035

Flash point ISO 2592 > 300 °C

Surface tension at 25 °C 0,021 N/m

Ignition temperature (liquids) DIN 51794 approx. 450 °C

Aggregate state liquid

INCI name Dimethicone

These figures are only intended as a guide and should not be used in preparing specifications.

© DKSHPage 23

Total care silicone free hair serum


➢ Vegetable alternative to

highly volatile silicone

(efp biotek)

➢ Vegetable alternative to

silicone (efp biotek)

➢ Beantree


➢ Instant nourishes the

hair and softens it.

➢Grives shine to dull,

lifeless looking hair.

➢Protects the hair &

smoothens it.

➢Makes hair is strong,

supple, smooth, shiny,

protected tips.

© DKSHPage 24

Total care silicone free hair serum

Total care silicone free hair serumDKSHIN # TCSFHS 27062019


DKSHIN # HSS 15062018


A1 Vegetable alternative to

highly volatile silicone

Undecane (and) Tridecane (and)

Hydrogenated olive oil

unsaponi_ables

(and) Coco-caprylate/Caprate

efp Biotek Q.S.

A2 Vegetable alternative

solicone

Hydrogenated ethylhexyl olivate (and)

hydrogenated olive oil unsaponifiables efp Biotek 10

A3 Beantree Methylheptyl Isostearate

Alzo 5.0

A4 Argan oil Argan oil _____ 2.0

A5 Almond oil Almond oil _____ 2.0

Description:

Clear Colourless Liquid

✓ Instant nourishes the hair andsoftens it.

✓ Gives shine to dull, lifeless looking hair.

✓ Protects the hair & smoothens it.✓

✓ Hair style for long timeKey ingredients:

Vegetable alternative to highly volatile silicone

Highly stable transparent liquid emollient. Instant nourishes the hair and softens. Give shine to dull, lifeless looking hair.

Vegetable alternative to silicone

Highly stable transparent liquid emollient. Instant nourishes the hair and softens. Give shine to dull, lifeless looking hair.

Beantree

It is light. Dry feel that is non – oily and absorbed quick into skin. It nourishes the hair and softens. Give shine to dull, lifeless looking hair

Procedure:

1 Initially take Vegetable alternative to highly volatile silicone in beaker.

2 Add beantree, vegetable alternative to silicone, almond oil and argand oil under mixing.

3 Then add perfume.

Specification

Appearance – Clear Colourless Liquid

DKSH India JUNE 2019

Formulation number:

DKSHIN # TCSFHS 27062019

© DKSHPage 25

Vegetable alternative to silicone and beantree

TECHNICAL BULLETIN BEANTREE

Chemical Name

INCIName

CAS Number

ELINCS Number

Empirical Formula

: Caprylyl lsostearate

: Methylheptyllsostearate

: 209802-43-7

: 440-220-8

: Culls2

TYPICAL PROPERTIES:

Appearance, 25°C

Color, 25°C, ALPHA

Odor, 25°C

Specific Gravity, 25°C

Refractive Index, 25°C

Molecular Weight (Theoretical)

Cloud Point, °C

Acid Value

Free Fatty Acid

(Av mol wt270),%

Saponification Value

Moisture,%

Clear Liquid

75 Max

Bland

0.860

1.4475

382

© DKSHPage 26

Sculpting hair spray


➢ Aquastyle 300 M

(Ashland)

➢ N hance CG 17

(Ashland)

• Key product benefits:➢ Grives you a strong hold.

➢Long – lasting styling.

➢Helps you create any

style.

➢ Hair style for long time.

© DKSHPage 27

Sculpting hair spray

Sculpting Hair SprayDKSHIN # SHS 31052019


DKSHIN # HSS 15062018


A1 Aqua _____ --------- Q.S.

A2 Glycerin Glycerin _____ 1.0

A3 Aquastyle 300 M Polyquaternium - 69 Ashland 3.0

A4 N hance CG 17 Cationic Guar Ashland 0.1

B1 Ethanol Ethanol _____ 40

Description:

Clear Colourless Liquid

✓ Gives you a strong hold

✓ Long – lasting styling ✓ Helps you create any style

✓ Hair style for long time

Key ingredients:

Aquastyle 300 M

It gives long lasting hold, stiff, strong hold with mechanical durability. Enhance shine, reduction of frizz.

N hance CG 17


Procedure:

1 Initially take 2/3 quantity of water and glycerine in beaker add aquasyle 330 M and stir it.

2 Take remaining water in another beaker add N Hance CG 17 and adjust the pH with citric acid.

3 Add N Hance CG 17 solution in above phase under stirring.

4 Add ethanol in above solution and adjust the pH.

Specification

pH =4.58

Appearance – Clear colourless Liquid


as per Indian standards.

DKSH India May 2019

Formulation number:

DKSHIN # SCH31052019

© DKSHPage 29

Free style hair gel


➢ Aquastyle SH

100(Ashland)

➢ Carbomer 980 (Ashland)


➢ Grives you a strong hold.

➢Long – lasting styling.

➢Helps you create any

style.

➢Hair style for long time.

© DKSHPage 30

Free style hair gelFree style hair gelDKSHIN # FSHG 20012015




A1 Aqua Water --------- Q.S.

A2 Carbomer 980 Carbomer Ashland 0.6

A3 TEA Trimehanol amine --------- 0.33

A4 D.EDTA Disodium EDTA --------- 0.1

B1 Aquastyle SH 100 Acrylates copolymer & water Ashland 3.34

B2 Germall Plus Diazolidinyl urea & iodopropynyl

butylcarbamate Ashland 0.2

B3 1,3 BG Butylene glycol -------- 2.0

C1 Perfume Fragrance -------- Q.S

C2 Puricolor Blue Colouring Agent BASF Q.S

Description:

Blue Colour Gel

✓ Grives you a strong hold✓ Long – lasting styling ✓ Helps you create any style✓ Hair style for long time

Key ingredients:

Aquastyle SH 100

Good initial stiff, durable, all day hold, eexcellent high humidity resistance, Smooth comb-through, No tack upon drying.

Carbomer 980

It is an extremely efficient rheology modifier capable of providing high viscosity and form sparkling clear gel. Provide clarity and high suspending ability in hair gel.

Procedure:

1 Initially take total qty of water & D.EDTA in manufacturing vessel. Add slowly carbomer 980 into it & stir for 10-15 min until completely dispersed. Then adjust the product pH with TEA.

2 Add 1,3 BG, Aqustyle SH 100 Polymer & preservative & mix it propre.

3 Finally add colour & perfume & adjust the product pH to 7.

Specification

pH = 7 – Brookfield DV-II+Pro # RV, Viscosity – 19652 cps, Spindle -05, Speed - 10 rpm

Appearance – Blue colour gel

Stability test : Product has Successfully completed 2 months stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

Indian standards

DKSH India JANUARY 2015

Formulation number:

DKSHIN # FSHG 20012015

© DKSHPage 31

➢ Aquastyle SH 100 and Carbomer 980

Description

Carbomers are a range of polymers which are used in a wide range of personal care products as thickeners. They are:

• cross-linked polyacrylic acid polymers of high molecular weight.

• extremely efficient thickeners and powerful stabilizers at low concentrations in water and aqueous ethanol.

• anionic in nature and acidic in their unneutralized state and have to be neutralized with an appropriate base to

achieve their thickening ability.

• effective across a wide pH range of 5 to 10.

Typical Uses of Carbomers

1. As a stabilizer and rheology modifier in oil-in-water emulsions, Ashland carbomer:

• Provides a stable emulsion at low concentration, due to high yield value (prevents coalescence).

• Aids spreadability on skin due to its electrolyte sensitivity.

2. As a gelling agent for aqueous-based gels such as styling gels, Ashland carbomer:

• Is efficient at low concentrations.

• Provides a transparent gel.

• Is compatible with other materials used in styling gels.

• Is easy to incorporate into finished products.

3. As a gelling agent for hydro-alcoholic gels such as hand sanitizers, Ashland carbomer:

• Has good solubility in aqueous alcohol.

• Provides transparent gels with good skin feel and slip.

• Is effective at low concentrations.

4. As a stabilizer and rheology modifier in mixed multiphase surfactant systems such as conditioning shampoos

and body washes, Ashland carbomer:

• Stabilizes emulsions and dispersions of the dispersed phases that may be used, such as silicones, anti-microbials,

anti-fungals, natural oils, physical sunscreen ingredients and beads.

Chemistry of Carbomer

1. Structure H H

The basic building block of carbomer is acrylic acid.C C

2. Physical Form

Supplied as a fine white powder, with a faint

acetic odor.

3. Viscosity characteristics

Carbomers exhibit pseudoplastic rheological

behavior.

H C n

HO O

Curl Defining Clear Gel #12460-108.2

34

• Style created: Rock your curls.

• Formula benefit: Get beautiful definition and long-lasting hold. No crunchy

feel. Nor sticky to touch. The gel is ideal for women with wavy or curly hair.

• Key products: AquaStyle™ SH-100 polymer, Natrosol™ 250 HHR

hydroxyethylcellulose, Ceraphyl™ 60 ester

• How-to-use: Apply product on damp hair. Style as desired.

• Alternative preservative system tested:

– 0.5% Optiphen™ preservative + 0.1% Methylparaben

© DKSHPage 32

Anti- frizz natural protection serum

• DKSH key ingredients

➢Stepanquat Helia

➢Nosilfix

➢N Hance CG 17


➢ Instant nourishes the hair

and softens it.

➢Gives shine to dull,

lifeless looking hair.

➢Protects the hair &

smoothens it.

© DKSHPage 33

Anti- Frizz hair serumAnti- frizz natural protection serumDKSHIN # AFNPS 31052019


Description:

White Viscous Lotion

✓ Instant nourishes the hair andsoftens it.

✓ Gives shine to dull, lifeless looking hair.

✓ Protects the hair & smoothens it.

Anti- frizz natural protection serumDKSHIN # AFNPS 31052019


jh-



A1 Aqua --------- Q.S.


A3 TEA Trimethylamine --------- Q.S.

B1 Rapithix A 60 Sodium Polyacrylate & Hydrogenated

Polydecene & Trideceth-6 Ashland 0.8

C1 N Hance CG 17 Cationic Guar Ashland 0.1

C2 Advantage LCA

Vinyl

Caprolactum/VP/Dimethylaminoethyl

Methacrylate Copolymer

Ashland 1.0

C3

Nosilfix

Water, chondrus crispus extract,

glycerine, lecithin, aloe barbadensis

leaf juice, xathan gum, diatomaceous

earth

Ashland 1.5


C5

Stepanquat Helia

Disunfloweroylethyl Dimonium

Chloride & sunflower seed oil

glycerides & lauryl lactate

Stépan 1.5


To mask odour

Of Product Qs

Key ingredients:

Stepanquat Helia

It is a modern hair conditioning agent that is better for hair. It provides excellent wet and dry combability on hair in addition to excellent detangling and a soft, conditioned feel on the hair.

Nosilfix

It is natural plymer based on polysaccharides. It is Distributed along the hair shaft and helps to enhance active penetration on to it. Repair damage hair. Grives deep moisturizing effect.

N Hance CG 17


Procedure:

1 Initially take 2/3 quantity of water & add Ultrathix P 100 and neutralise it with TEA ans stir it.

2 Then add Rapithix A 60 under stirring.

3 In another beaker take remaining water add N Hance CG 17 adjust the pH with citric acid.

4 Then add advantage LCA, stepanquat ml and nosolfix

5 Finally add perfume with stirring & adjust the product pH 6.5 to 7

Specification

pH = 6.80 – Brookfield DV-II+Pro # RV, Viscosity - 1312 cps, Spindle -02, Speed - 10 rpm

Appearance – White Viscous Lotion



DKSH India MAY 2019

Formulation number:

DKSHIN # AFNPS 31052019

© DKSHPage 34

Anti- frizz natural protection serum

NOSILFI Fr>< and active delivery without silicones

WHATIS ANDHOW ITWORKS

NATURALPOLYMERS

BASED ON

POLYSACCHARIDES

810-INPIRED

MICROPOROUS SILICA

ABLETO CARRY

ACTIVE INGREDIENTS

AND DELIVER THEM

TO HAIR

NATURAL, PROTECTING LIGHTWEIGHT COATING

NO SEALING, FILM-FORMING EFFECT

HIGH SUSTANTIVI1YTO HAIR SHAFT

ALLOWS NATURALHYDRATION

WITH A DELIVERY SYSTEM INSIDE

EXTENDED RELEASE OFACTIVES

STEPANQUAT Helia Modern Hair Conditioning Agent

INCI Name: Disunfloweroylethyl Dimonium Chloride (and) Sunflower Seed Oil Glycerides (and)

Lauryl Lactyl Lactate

Appearance at 25°C: Soft Yellow Paste

Appearance at 40°C: Flowable Yellow Liquid

Actives: 95%

Bio-Based Carbon: 88%

Preservative: None

© DKSHPage 35

Volume boost and shine shampoo

• DKSH key ingredients

➢ N Durhance AA 2000

➢N – Hance CG 17


➢ Protects hair against

future damage.

➢Leaves hair feeling

soomther & signer

➢Leave your hair feeling

thicker, fuller, and

looking so healthy.

© DKSHPage 36

Volume boost and shine shampooVolume Boost & Shine ShampooDKSHIN # VBSS 11072019


DKSHIN # CVPS 15022017


A1 Aqua _____ --------- Q.S.

A2 EDTA DI Sodium EDTA --------- 0.05

A3 SLES Sodium Lauryl Ethyl Sulphate --------- 48

A4 Carbomer 980 Carbomer Ashland 0.3

B1 Sabowax EGDS Glycol Distearate Sabo 2.0

C1 NaOH (30 %) Sodium Hydroxide --------- 0.5

C2 CAPB Cocamidopropyl Betaine --------- 5.0

C3 N- Durhance AA 2000

Acrylamidopropyltrimonium

chloride/Acrylamide crosspolymer Ashland 1..0

C4 Aqua _____ --------- 20

C5 N – Hance CG 17 Cationic Guar Ashland 0.5

C6 Belsil 60082 Wacker 2.0

C7

Copolymer 845 VP/Dimethylaminoethylmethylacrylat

e coplymer Ashland 2.0

C8 Rokosal S1

Methylchloroisothiazolineand

methylisothiazoline Ashland 0.1

C9 Nacl Sodium Chloride --------- 1.0

C10

Perfume Fragrance

To mask

Odour of

product

QS

C11 Puricolor Red Color BASF QS

Description:

Pink coloured Pearly Shampoo

✓ Protects hair against future damage✓ Leaves hair feeling soomther & shiner

Lleave your hair feeling thicker, fuller, and looking oh, so healthy.

Key ingredients:

N Durhance AA 2000

It is conditioning polymer. It has been developed to provide long lasting damage repair and restore hair to its natural hydrophobic state. Protects against harmful effect of pollution and urban stress.

N – Hance CG 17


Procedure:

1 Initially take 2/3 qty of water in Beaker and carbomer 980, EDTA, SLES and heat it upto 800C.

2 In another seprate beaker take sabowax EGDS and heat it upto 800C.

3 Add B phase to A phase under constant stirring. When above phase cool neutralizes it with NaOH and add CAPB under stirring.

4 Take remaining water in another beaker and add N Hance CG 17 and adjust pH with citric acid.

5 AT 500 C add N Durhace AA 1000, BELSIL 60082, COPLYMER 845, Rockonsal, NaCL and perfume.

6 Finaly add perfume and color with stirring & adjust the product pH 5-6.5.

Specification

pH = 5.82 – Brookfield DV-II+Pro # RV, Viscosity -6160 cps, Spindle -04, Speed - 10 rpm

Appearance – Pink coloured Pearly Shampoo

Stability test : Product has Successfully completed 3 weeks stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

Indian standards

DKSH India JULY 2019

Formulation number:

DKSHIN # VBSS 11072019

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