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! ""#" $$%&# ' "(( "(( $& )&* +, "-./# #%0 "1!%-"/" 2 . -( !3 4/ " + 5 5 %38 %38 9 : 955,2 9 2,, 955,2 ; :2 5 ! : -)% < # !8( )=> ( "! <! ? &( 2+: 5&5 5555 !3 -( :+5&%5: !3 / 5#&45: ! 5555 2 #6 3 ( < A:A 2 #6 3 ( %8 3 3( 3 3=> '8 8 6 - 33 8 3=> (6 " 3 8 3 8 8B( ( 33( 6 %8 " 8 ' $ " - ! #"%" "(( :, %8 ( ( ( '8 #"%" ( ?6 "(( 3 '8 /!&A/ +:,6 %8 ( 8 ( 8 8C( (( '6 8 ( 3 '8 3( 3( : - 6 ! / / 8 / ! / 8 / / 8 & 2 . -( !3 4/ " + !" E6 955,2 ###$%&'$() FOI 463/17/18 Item 9 Serial # 8 s47G s47G s47G s47G Page 2216 of 4750

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Page 1: Home : Department of Defence, Australian Government, Jobs, … · 2019-05-08 · "-./# #%0 "1!%-" /" 2 . -( !3 4/ " + 5 5 % 38 9 : % 38 9 5 5 ,2 9 2, , 9 5 5 ,2 ; : 2 5 ! : -)%

FOI 463/17/18 Item 9

Serial # 8

s47G

s47G

s47G s47G

Page 2216 of 4750

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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Serial # 8

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Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

Serial # 8

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FOI 463/17/18 Item 9

Serial # 8

s47G s47G

s47G

s47G s47G

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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LEEDER CONSULTING

Chartered Chemists

A.B.N. 540 864 910 094 - 5, 18 Redland DriveMitcham, Vic, 3132Telephone: (03) 9874 1988Fax: (03) 9874 1933

SpringvaleVIC 3168Attention:

SAMPLES:

DATE RECEIVED:

DATE COMMENCED:

METHODS:

RESULTS: Please refer to attached pages for results.

REPORTED BY:

4 Westall Road

31-Oct-2008

Three samples were received for analysis

31-Oct-2008

CERTIFICATE OF ANALYSIS

See Attached Results

Laboratory Manager

Note: Results are based on samples as received at Leeder Consulting's laboratories

ALS

13-Nov-2008REPORT NUMBER:

Site/Client Ref: Order No: 350502

M081987EM0809145

This report has been prepared in accordance with the quality system of

Leeder Consulting Pty. Ltd and may not be reproduced except in full.

Page 1 of 4Ce l ebrat i ng 10 Years 1998 - 2008

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(I) RESULTS

LEEDER CONSULTING

Report N°: M081987

Matrix: Soil

Method: MA_1523.SL.01

Sample units are expressed in g/kg on a dry weight basis unless otherwise stated

Analyte Name PQL

Client ID

Leeder ID

nd

nd

nd

43

nd

nd

nd

nd

nd

nd

nd

nd

nd

nd

nd10Perfluorononanoic acid

10Perfluorooctanoic Acid

10Perfluorooctane sulfonate

Blank

Method

2008025189

Duplicate

EM0809145-16

2008025188

EM0809145-18

2008025187

EM0809145-17

2008025186

EM0809145-16

2008025185

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(II) QUALITY CONTROL

LEEDER CONSULTING

Report N°: M081987

Matrix: Soil

Method: MA_1523.SL.01

Quality Control Results are expressed in Percent Recovery of expected result

Analyte Name PQL

Client ID

Leeder ID

110

90

114

114

94

120Perfluorononanoic acid

Perfluorooctanoic Acid

Perfluorooctane sulfonate

Spike Dup

EM0809145-16

2008025191

Spike

EM0809145-16

2008025190

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LEEDER CONSULTING

Report N°: M081987

QUALIFIERS / NOTES FOR REPORTED RESULTS

PQL Practical Quantitaion Limit

is Insufficient Sample to perform this analysis.

T Tentative identification based on computer library search of mass spectra.

ND Not Detected – The analyte was not detected above the reported PQL.

nr Not Requested for analysis.

R Rejected Result – results for this analysis failed QC checks.

SQ Semi-Quantitative result – quantitation based on a generic response factor for this class of analyte.

IM Inappropriate method of analysis for this compound

U Unable to provide Quality Control data – high levels of compounds in sample interfered with analysis of QC results.

UF Unable to provide Quality Control data- Surrogates failed QCchecks due to sample matrix effects

UI Unable to provide Quality Control data – insufficient sample to perform QC checks.

B This analyte also detected in analysis of the Method Blank.

D Deviation from standard method – see notes for specific explanation.

L Analyte detected at a level above the linear response of calibration curve.

NT No blank sorbent tubes provided for QC analysis.

C1 These compounds co-elute.

C2 These compounds co-elute.

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LEEDER CONSULTING

APPENDIX ONE.

CHAIN OF CUSTODY DOCUMENT

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Client's Name: Report No: MC8/1890Contact: Client No: EM0809145Site: Purchase order # 350501

Springvale, VIC 3171 Date Received:Type of Sample: Date Reported:Container: Sampled by: N/A

Item:

The samples received were tested and the following results were obtained:

SGS Lab No.Test Method LOR(mg/L)

Client Reference IDResult Result

DuplicateResult Result

Duplicate2.4-TDI 2.4-TDI 2.6-TDI 2.6-TDI

MC8/1890-1 SGSMC 305 1 EM0809145-001 < 1 < 1 < 1 < 1MC8/1890-2 SGSMC 305 1 EM0809145-002 < 1 < 1 < 1 < 1MC8/1890-3 SGSMC 305 1 EM0809145-003 < 1 < 1 < 1 < 1MC8/1890-4 SGSMC 305 1 EM0809145-004 < 1 < 1 < 1 < 1MC8/1890-5 SGSMC 305 1 EM0809145-005 < 1 < 1 < 1 < 1MC8/1890-6 SGSMC 305 1 EM0809145-006 < 1 < 1 < 1 < 1MC8/1890-7 SGSMC 305 1 EM0809145-007 < 1 < 1 < 1 < 1MC8/1890-8 SGSMC 305 1 EM0809145-008 < 1 < 1 < 1 < 1MC8/1890-9 SGSMC 305 1 EM0809145-009 < 1 < 1 < 1 < 1MC8/1890-10 SGSMC 305 1 EM0809145-010 < 1 < 1 < 1 < 1MC8/1890-11 SGSMC 305 1 EM0809145-011 < 1 < 1 < 1 < 1MC8/1890-12 SGSMC 305 1 EM0809145-012 < 1 < 1 < 1 < 1MC8/1890-13 SGSMC 305 1 EM0809145-013 < 1 < 1 < 1 < 1MC8/1890-14 SGSMC 305 1 EM0809145-014 < 1 < 1 < 1 < 1MC8/1890-15 SGSMC 305 1 EM0809145-015 < 1 < 1 < 1 < 1

For: SGS Australia Pty. Ltd.

Laboratory Operations Manager

SGS Australia Pty. Ltd.Member of the SGS Group

Unless otherwise stated the results shown in this test report refer only to the sample(s) tested and such sample(s) are retained for 21 days only. This document cannot be reproduced except in full, without prior approval of the Company.

This document is issued by the Company under its General Conditions of Service accessible at http://www.sgs.com/terms_and_conditions.htm. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of Client’s instructions, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law

Isocynates

NB: The recovery data is not available due to the analytes rapid decomposition in the matrix.

CERTIFICATE OF ANALYSIS

Glass Jar

al

2-4 Westall Road

Soil Sample31 October 200825 November 2008

34 Norfolk Court, Coburg, VIC 3058, Australia +61 (3) 9350 4800 +61 (3) 9350 4871

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s47G s47G

s47G s47G

s47G

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s47Gs47G

s47G s47G

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LEEDER CONSULTING

Chartered Chemists

A.B.N. 540 864 910 094 - 5, 18 Redland DriveMitcham, Vic, 3132Telephone: (03) 9874 1988Fax: (03) 9874 1933

SpringvaleVIC 3168Attention:

SAMPLES:

DATE RECEIVED:

DATE COMMENCED:

METHODS:

RESULTS: Please refer to attached pages for results.

REPORTED BY:

4 Westall Road

7-Nov-2008

Nine samples were received for analysis

7-Nov-2008

CERTIFICATE OF ANALYSIS

See Attached Results

Laboratory Manager

Note: Results are based on samples as received at Leeder Consulting's laboratories

ALS

13-Nov-2008REPORT NUMBER:

Site/Client Ref: Order No: 350515

M082031EM0809435

This report has been prepared in accordance with the quality system of

Leeder Consulting Pty. Ltd and may not be reproduced except in full.

Page 1 of 4Ce l ebrat i ng 10 Years 1998 - 2008

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s47G

s22

s47G

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(I) RESULTS

LEEDER CONSULTING

Report N°: M082031

Matrix: Soil

Method: MA_1523.SL.01

Sample units are expressed in g/kg on a dry weight basis unless otherwise stated

Analyte Name PQL

Client ID

Leeder ID

4600

23

nd

5000

20

nd

35

nd

nd

93

nd

nd

12000

46

nd

7800

14

nd

190000

96

1410Perfluorononanoic acid

10Perfluorooctanoic Acid

10Perfluorooctane sulfonate

EM0809435-22

2008025827

EM0809435-21

2008025826

EM0809435-20

2008025825

EM0809435-19

2008025824

EM0809435-18

2008025823

EM0809435-17

2008025822

EM0809435-16

2008025821

Matrix: Soil

Method: MA_1523.SL.01

Sample units are expressed in g/kg on a dry weight basis unless otherwise stated

Analyte Name PQL

Client ID

Leeder ID

360000

510

nd

35

nd

nd

42

nd

nd

nd

nd

nd10Perfluorononanoic acid

10Perfluorooctanoic Acid

10Perfluorooctane sulfonate

Blank

Method

2008025831

Duplicate

EM0809435-18

2008025830

EM0809435-24

2008025829

EM0809435-23

2008025828

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(II) QUALITY CONTROL

LEEDER CONSULTING

Report N°: M082031

Matrix: Soil

Method: MA_1523.SL.01

Quality Control Results are expressed in Percent Recovery of expected result

Analyte Name PQL

Client ID

Leeder ID

123

90

118

124

92

114Perfluorononanoic acid

Perfluorooctanoic Acid

Perfluorooctane sulfonate

Spike Dup

EM0809435-18

2008025833

Spike

EM0809435-18

2008025832

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LEEDER CONSULTING

Report N°: M082031

QUALIFIERS / NOTES FOR REPORTED RESULTS

PQL Practical Quantitation Limit

is Insufficient Sample to perform this analysis.

T Tentative identification based on computer library search of mass spectra.

ND Not Detected – The analyte was not detected above the reported PQL.

nr Not Requested for analysis.

R Rejected Result – results for this analysis failed QC checks.

SQ Semi-Quantitative result – quantitation based on a generic response factor for this class of analyte.

IM Inappropriate method of analysis for this compound

U Unable to provide Quality Control data – high levels of compounds in sample interfered with analysis of QC results.

UF Unable to provide Quality Control data- Surrogates failed QCchecks due to sample matrix effects

UI Unable to provide Quality Control data – insufficient sample to perform QC checks.

B This analyte also detected in analysis of the Method Blank.

D Deviation from standard method – see notes for specific explanation.

L Analyte detected at a level above the linear response of calibration curve.

NT No blank sorbent tubes provided for QC analysis.

C1 These compounds co-elute.

C2 These compounds co-elute.

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LEEDER CONSULTING

APPENDIX ONE.

CHAIN OF CUSTODY DOCUMENT

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s22

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s47G s47G

s47G

s47G

s47G s47G

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s47G

s47G

s47G

s47G s47G

s47G

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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FOI 463/17/18 Item 9

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