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 · for source parameters set sheath gas at 3500c, flow at 12l/min., nebulizer at 50psi, dry gas at...

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  •  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,
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Page 1:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,
Page 2:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,
Page 3:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,
Page 4:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,
Page 5:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,

Washington State University Food and Environmental Quality Laboratory

LC/MS: Checklist

Instrument ID: Violet

Date

Initials

SOP follow

ed (Y

/N)

Source (A

PCI or ESI)

Autotune or

Checktune

Performed

Pump B

allasted

Source Cleaned

Vacuum

pump oil

changed

Com

ments

Page 6:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,

LC Operations Log Instrument ID: Violet-LC

Pressure (bar) at initial conditions

Column temp (C)

Initial flow (ml/min)

Initial solvent composition (A2:B2)

Solvent B2

Solvent A2

Initial solvent composition (A1:B1)

Solvent B1

Solvent A1

Col B guard column

Column B

Col A guard column

Column A

SOP Followed?

Initials

Date

Page 7:  · For source parameters set sheath gas at 3500C, flow at 12L/min., nebulizer at 50psi, dry gas at 5L/min. In Optimizer edit optimization setup; fragmentor should be set at 30-200,

Washington State University Food and Environmental Quality Laboratory

LC/MS: Maintenance, Malfunctions and Repairs Instrument ID: Violet Date Initials Routine?

(Y/N) SOP followed (Y/N)

Maintenance/Repair If actions were not routine, document the nature of the defect, how and when the defect was discovered, and the remedial action taken in response


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