final report_wan ibrahim bin wan mamat me 11526_petronas gas berhad_terengganu
TRANSCRIPT
DEPARTMENT OF MECHANICAL ENGINEERING
UNIVERSITI TEKNOLOGI PETRONAS
STATEMENT OF VERIFICATION
INDUSTRIAL INTERNSHIP REPORT
STUDENT’S NAME : WAN IBRAHIM BIN WAN MAMAT
MATRIC NUMBER : 11526
This is to certify that the above mentioned report is approved and all information
and project involved are NOT confidential.
Supervisor’s Signature : …………………………………..
Supervisor’s Name : Ir. Hj Khairil Nizam b. Khirudin
Senior Inspection Engineer
Gas Plant Processing B, Petronas Gas Berhad
Date :
ACKNOWLEDGEMENT
EXECUTIVE SUMMARY
TABLE OF CONTENT
1. INTRODUCTION
1.1 Introduction to Industrial Internship Program 1
1.1.1 Objective of Industrial Program 1
1.1.2 Scope of Work 3
1.2 Introduction to Host Company (Petronas Gas Berhad) 4
1.2.1 Company Profile 4
1.2.2 PETRONAS Corporate Value 6
1.3 Organization Background
1.3.1 Inspection Section Jobscopes 6
1.3.2 Department Organization Chart 7
2. WORK EXPOSURES 8
2.1 Damage Mechanisms (Refinery and Process Industry)
2.1.1 Corrosion Under Insulation 8
2.1.2 Galvanic Corrosion 10
2.2 Non Destructive Testings (NDT)
2.2.1 Dye Penetrant Testing 11
2.2.2 Magnetic Particle Testing 15
2.2.3 Ultrasonic Testing 18
2.2.4 Radiography Testing 19
2.3 PETRONAS Risk-Based Inspection (P-RBI) 21
2.4 Inspection Reference Plan 24
3. PROJECT AND ASSIGNMENT
3.1 Project Background 27
3.2 Objectives 29
3.3 Root Cause Failure Analysis (RCFA)
5 Why Analysis on Wet Gas Separator 29
3.4 RCFA Problem Statement 31
3.5 Conclusion 33
4. OTHER INVOLVEMENTS 34
5. LESSON LEARNT
5.1 Challenges faced and solutions to overcome 35
6. RECOMMENDATION 36
7. CONCLUSION 37
REFERENCES 38
APPENDICES
Appendix 1: Piping Integrity Management System 39
Appendix 2: Simplified Block Flow Diagram of gas processing 40
Appendix 3: DOSH Registered Equipments for Gas Plant Processing B 41
Appendix 4: Equipment Certificate of Fitness (CF) 42
Appendix 5: RBI Criticality Ranking 43
Appendix 6: Laboratory Analysis Test result 43
Appendix 7: External Visual Inspection equipment report 44
LIST OF FIGURES
Figure 1 : Inspection Section – GPPB 7
Figure 2 : Application of penetrant on the surface 12
Figure 3 : Removal of excess penetrant 13
Figure 4 : Application of developer 13
Figure 5 : Indications of surface breaking 14
Figure 6 : Indication on the weldment 14
Figure 7 : Student demonstrating DPI 14
Figure 8 : Working principle of MPT 15
Figure 9 : Dry method 16
Figure 10 : Wet method 16
Figure 11 : Crane Hook with service induced crack 17
Figure 12 : Gear with service induced crack 17
Figure 13 : Drive Shaft with heat treatment induced crack 17
Figure 14: Lack of fusion in SMAW weld 17
Figure 15: The sound reflected to the probe is displayed on the flaw detector 18
Figure 16 : Illustration of Radiographic test 19
Figure 17 : Result produced 20
Figure 18 : RBI Risk Matrix 21
Figure 19 : Three distinct level namely qualitative , semi-quantitative and
quantitative 22
Figure 20: Simplified Block diagram of RBI Process 23
Figure 21: Before and after internal modification in 2008 29
Figure 22: 2008- No erosion observed 30
Figure 23: 2010 – severe corrosion observed 30
Figure 24: Chronology of Events (Events and Causal Factors) 32
Figure 25: 5 – WHY Analysis 32
LIST OF TABLES
Table 1 : Scopes of Works 3
Table 2 : Yearly Inspection Service Program 7
Table 3 : Comparison of Gamma rays and X-rays 20
Table 4: Continuum of RBI approaches 22
Table 5: Wet Gas Separator equipment data 28
Table 6 : Lab Analysis as per taken on 2 April 2011 at V6-0401 boot 33
Table 7 : Others involvement 34
ACKNOWLEDGEMENT
Alhamdulillah. I would like to express my greatest gratitude to Allah SWT for His
will upon the completion of this final internship report.
My deepest appreciation to PETRONAS Gas Berhad (Gas Plant Processing
B) for the opportunity given to me in order to acquire knowledge during the eight
months of industrial training. Greatful acknowledgement to my personal guidance
and dedicated supervisor Ir. Hj Khairil Nizam B Khirudin, Senior Inspection
Engineer of GPPB who has helping and influence me a lot on my personnal
development.
During my internship, I have also received many guidance and assistance
from many colleagues in Inspection Section, and my special thanks goes to all of
them.
1- Mr. Khairul b Ismail - Inspection Manager, GPPB
2- Mr. Rozaimee Ahamad Zakaria - Senior Inspection Engineer (GPP5)
3- Mr. Zubir b Mat Dahan - Inspection Engineer (DPCU3)
4- Ms. Fatihanum Abdul Rahman - Technical Clerk
5- Mr. Anis B Jusoh - Inspection Technician (GPP6)
6- Mr. M Kamah Md Noor - Inspection Technician (GPP5)
7- Mr. M Azman b Jusoh - Inspection Technician (GPP5)
8- Mr. M Syuraihan b Aziz - Inspection Technician (DPCU3)
9- Mr. M Nazeri Ahmad Sofian - Inspection Technician (Common)
10- Mr. Raja Anuar Raja Ahmad - Inspection Technician (DPCU3
My appreciation also goes to Mechanical Engineering Department and
Student Industrial Internship Unit (SIIU) of Universiti Teknologi PETRONAS for
arranging and guiding me from the beginning till the end of internship program. I
also would like to express special thanks to my UTP supervisor, Dr. Ridzuan Abdul
Latif for his supervision and advice. Not to be forgotten, my appreciation also goes
to my colleagues and family for their continuos supports upon my completion of
internship. Thank you.
I
EXECUTIVE SUMMARY
Industrial Internship Program coordinated by the Student Industrial
Internship Unit of Universiti Teknologi Petronas (UTP) is aimed to produce well
rounded students which is part of the effort in achieving UTP’s mission. Despite of
as an exposure towards the working life, the rationale of this program is to provide
undergraduates with necessary technical and soft skills.
This Industrial Internship Final Report compiles all activities and tasks that
the author had undergone through during the Industrial Internship Period. The final
report is divided into few sections whereby the first section briefly introduce the host
company background, objectives as well as the scope of work done during the
Industrial Internship Program.
Next, the main section illustrate in details of the projects and tasks involved during
the internship period as following:
I. Damage Mechanisms
II. Non-Destructive Testing
III. Risk-Based Inspection
IV. Inspection Reference Plan
V. Analysis of the Project
Lastly, the final section contains the lesson learned, discussions, conclusions
and recommendations to the Host Company and UTP. All related standards, tables,
figures and references are attached in the appendices section for better overview of
the tasks explained.
II
1. INTRODUCTION
1.1 Introduction to Industrial Internship Program
1.1.1 Objective of Industrial Program
The Industrial Internship Training Programme (IITP) is a core course offered to all
third-year student of Universiti Teknologi Petronas (UTP). The students undergo
practical training from 6th December 2010 until 15th July 2011 prior to the
completion of their study. During these 32 weeks of training programme, UTP
students are exposed to the real working environment where they can relate
theoretical knowledge with application in industry. It is the University hopes that the
students will be able to develop skills in work ethics, communication, leadership,
management and other skills during these 32 weeks. There are five main objectives
of the IITP:
1) To integrate theory with practice
In University, student had studied so many theories and the IITP is the chances for
the students to apply and see the application of all those theories. The experience
gain in integrating the theory and hands-on during this IITP had given the author a
better understanding towards the theories and enables the author to appreciate the
theories learnt at the University.
2) To introduce students to work culture and industrial practices
The period of 32 weeks of training programme is a good start for the student to
prepare themselves before entering the real life working environment. Students have
the opportunity to improved the communication and interpersonal skills among the
staffs and advance themselves in using the software and tools related.
3) To give opportunity to students to work with industrial practitioners
The involvement of students in several projects will give them the opportunities to
work with various industrial practitioners from different engineering background.
This will help the students in identi1 their interest and choosing 8 their career path
later on.
1
4) To expose students to potential employers
During these 32 weeks of internship period, students will be working not only with
the staff from the host company itself but also with the client, staff from other
company. With this experience, student will know lots of people from different
companies which later can be the potential employer when students finished their
study.
5) To acquaint UTP students with industry and its programs
Students who undergo the internship program will have the experience of working in
the industry. This is a good opportunity for students to create good acquaintances
with the host company. Students have chances to apply the knowledge they gain in
University and see the applications of every program that they had learnt.
2
1.1.2 Scope of Work
Generally, the scope of works, tasks or projects undertaken during this period is
according to the training shcedule planned at the very first week of internship period.
Both supervisor and author had agreed on several fields to be covered at the
respective weeks. The training schedule is as follows :
Scopes Month
Dis Jan Feb Mac Apr May June July
Introduction to POD/PGB
P-Risk Based Inspection (P-
RBI)
Damage Mechanisms
Non-Destructive Testing (NDT)
Dye Penetrant Testing (DPT)
Thermography
Welding
Pressure Test
Ultrasonic Thickness Test (UT)
Steam Condensate Line
Corrosion Under Insulation
Stress Corrosion Cracking
Pressure Relief Device (PRD)
Plant Turnaround/Shutdown
Extra Tasks
Root Cause Failure Analysis
(RCFA)
Inspection Confidence
Inspection Reference Plan (IRP)
Piping Integrity Management
System
DOSH Packages
Piping Circuit
Corrosion Monitoring
Internship Project (Wet Gas
Separator)
Final Presentation
Table 1 : Scopes of Works
3
1.2 Introduction to Host Company (GPP Complex B, Petronas Gas Berhad)
1.2.1 Company Profile
PETRONAS Gas Berhad (PGB)
PETRONAS Gas Berhad (PGB) was incorporated on 23rd May 1983 and
being among the top subsidiaries of PETRONAS since establishment. PGB’s main
business porfolio is divided into four major divisions namely – Plant Operations,
Transmission Operations, Centralised Utility Facilities and Technical and Facilities
Division. The principle activities of the company are processing of natural gas
produced from the gas fields and transmission of the processed gas to end-users
throughout peninsular Malaysia and some for export to Singapore. The first two are
directly related , the third division supports the gas value chain by supplying
industrial utilities to the various petrochemical plants operating in Kerteh and
Gebeng and the fourth division is a technical services outfit for PGB, which also
extend its expertise in engineering and project management to other entities within
the PETRONAS Group of Companies.
As the sole supplier of processed gad, PGB plays a prominent role in the gas
business value chain. PGB operates as a throughout service company providing the
services of processing and transmission of gas to the various customers on behalf of
PETRONAS for a fee as set out in the gas Processing Transmission Agreement
(GPTA).
Sales gas (Methane, ethane, propane , butane and condensates ) are delivered
through the peninsular Gas Utilisation pipeline system. PGB supplies sales gas to
power stations which account for more than 70% of the consumption of processed
gas. The balance is for the non0-power sector and export to Singapore. The Plant
Operations Division (POD) handles all activities pertaining to the processing of feed
gas whilst the Transmission Operation Division (TOD) comprising of a chain of
regional offices, is responsible for the transmission and delivery of sales gas to end
customers. Apart from the PGU system in Peninsular Malaysia, PGB also owns and
operates two gas distribution systems in Miri and Bintulu, Sarawak.
4
The third division involves marketing, manufacturing and supplying of
industrial utility products to the Integrated Petrochemical Complexes (IPCs) in
Kerteh and Gebeng through the Centralised Utilities Facilities (CUF) Operations.
With regard to its CUF business, PGB operates as a commercial provider of
industrial utility products services to its own customers. The commercial operations
of CUF has commenced in January 2000.
The fourth division involves in engineering and project management services.
Technical and Facilities Development Division (TFDD) is the engineering and
project management arm of PETRONAS Gas Berhad. TFDD also provides services
to other companies within the Petronas Group such as Petronas Carigali Sdn Bhd for
the Sabah-Sarawak Gas Pipeline.
Due to integrated nature and interdependence of the gas business, it is crusial for
PGB to ensure its operations support the requirement of its customers. The company
will continue to focus on sustaining the reliability and efficiency of its facilities with
optimal utilization of resourced.
Gas Plant Processing (GPP)
Since the implementation of the PGU Project 1984, PGB’s gas processing
operations are an integral component of this project. Feedgas from offshore
Terengganu is landed at the GPPs in Kerteh and extracted into various component
namely salesgas, ethane, propane, butane and condensate. The GPP Complex in
Kerteh comprises GPP 1,2,3,4 with a combined salesgas production capacity of 1000
million standard cubic feet per day (mmscfd).
To ensure reliability and availability of gas supply to end users, PGB has
constructed two additional GPPs in Kg Tok Arun, which is approximately 15 km to
the north of existing GPP Complex in Kerteh.
The completion of GPP 5 and 6 in December 1998 and July 1999 respectively each
with a 500 mmscfd salegas processing capacity has boosted PGB’s total gas
processing capacity to 2000 mmscfd.
5
Function/Design Basis of a GPP
1. To produce on-specification products in accordance with customers
requirements namely methane, propane, butane and condensate.
2. To process a wide range of feedstocks from the offshore fields and offgas
from a crude oil terminal
1.2.2 PETRONAS Vision and Mission, Corporate Value
PETRONAS has its very clear vision and achievable mission statement
which define its organisation, guiding our corporate activities and policies.
Vision : To be a Leading Oil and Gas Multinational of Choice
Mission :
- We are a business entity
- Petroleum is our core business
- Our primary responsibility is to develop and add value to this national
resource
- Our objective is to contribute to the well-being of the people and the nation.
Shared Values :
Loyalty - Loyal to nation and corporation
Integrity - Honest and Upright
Professionalism - Committed, Innovative & Proactive and always striving for
Excellence
Cohesiveness - United in Purpose and Fellowship
1.3 Organization Background
1.3.1 Inspection Section Jobscope
The author has been attached to the Inspection Section of Technical Services
Department. Inspection section is an important section in oil and gas industry in
order to enable the operation is complying with The Factory and Machinery Act
1967 and Occupational Safety and Health Association OSHA and working closely
with the Department of Occupational Safety and Health DOSH to ensure plant and
operation integrity.
6
Inspection focus areas are as below :
Yearly Inspection Service Program (ISIP)
Managing Loss of Containment, LOC
DOSH registered equipment
Non-DOSH registered equipment
Piping : P-PIMS
Tankage
Non Standard Repair
Statutory/Insurance/Audit
Turnaround, TA
Certificate of Fitness Renewal
Certificate of Fitness Extension
P- Risk Based Inspection, RBI
PRD : ECA
Initiatives WP/WI Updates
5S PMT
Ad-Hoc
Day-to-day ad-hoc
Slowdown
Mini-shutdown
Others 5S PMT Number
Condensate Tank Assessment
Contract Renewal
Table 2: Yearly Inspection Service Program
1.3.2 Department Organization Chart
Figure 1: Inspection Section – GPPB
7
2. WORK EXPOSURES
2.1 Damage Mechanisms
2.1.1 Corrosion Under Insulation (CUI)
Desciption of Damage
Corrosion of piping, pressure vessels and structure componnets resulting
from water trapped under insulation or fireproofing
Affected Materials
Carbon steel. Low alloy steels, 300 series SS and duplex stainless steels.
Critical Factors
a) Design of insulation system, insulation type, temperature,
environment (humidity, rainfall and chlorides from marine
environment, industrial environments containing SO2) are critical
factors
b) Poor design and/or installations that allow water to become trapped
will increase CUI
c) Corrosion rates increase with increasing metal temperature up to the
point where the water evaporates quickly.
d) Corrosion become more severe at metal temperature between the
boiling 1000C-120
0C, where water is less likely to vaporize and
insulation stays wet longer.
e) Insulating materials that hold moisture can be more of the problem.
f) Equipment that opertaes below the water dewpoint tends to condense
water on the metal surface thus providing a wet environment and
increasing the risk of corrosion.
g) Damage is aggravated by containants that may be leached out of the
insulation such as chlorides.
h) Plants located in areas with high annual rainfall or warmer, marine
location are more prone to CUI
i) Environment that provide airborne contaminants such as chlorides or
SO2 can accelerate corrosion.
8
Affected units or equipment
a) Carbon and alloy steels are subject to pitting and loss in thickness
b) 300 series SS, 400 series SS and duplex SS are subject to pitting and
localized corrosion.
Causal Factors
a) Location issues
Common area of concern in process units are higher moisture areas
such as those areas down-wind from cooling towers, near stream
vents, deluge systems, acid vapors, or near supplemental cooling with
water spray.
b) Design issues
i. CUI can be found on equipment with damaged insulation,
vapor barriers, weatherproofing or mastic, or prostrusions
through the insulation or at insulation termination points such
as flanges.
ii. Equipment design with insulation support rings welded
directly to the vessel wall, particularly around ladder and
platform clips, and lifting lugs, nozzles and stiffener rings.
iii. Piping or equipment with damage/leaking steam tracing
iv. Localized damage at paint and/or coating systems.
v. Locations where moisture will naturally collected and
improperly terminated fireproofing.
vi. The first few feet of a horizontal pipe run adjacent to the
bottom of a vertical run is a typical CUI location.
Morphology of Damage
a) After insulation is removed from carbon and low alloy steels, CUI damage
often appears as loose, falky scale covering the corroded component. Damage
may be highly localized.
b) In some localized cases, the corrosion can be appear to carbuncle type pitting
c) Tell tale signs of insulation and/paint damage often accompany CUI
9
Prevention/ Mitigation
a) Since the majority of construction materials used in plants are
susceptible to CUI degradation, mitigation is best achieved by using
appropriate paint/coating and maintaining the insulation barriers to
prevent moisture ingress.
b) High quality coatings, properly applied can provide long term
protection
c) Careful selection of insulating materials is important
d) Low chloride insulation should be used on 300 SS to minimize the
potential for pitting and chloride SCC
e) It is not usually possible to modify operating conditions.
Consideration should be given to removing the insulation on
equipment where heat conservation is not as important.
f) Utilize multiple inspection techniques to produce the most cost
effective approach, including:
i. Partial or full stripping of insulation for visual examination
ii. UT for thickness verification
iii. Real-time profile x-ray for small bore piping
iv. Neutron backscatter techniques for identifying wet insulation
v. Deep penetrating eddy-current inspection
vi. IR thermography looking for wet insulation and/or damaged
and missing insulation under the jacket.
2.1.1 Galvanic Corrosion
Description of Damage
A form of corrosion that can occur at the junction of dissimilar
metals when they are joined together in a suitable electrolyte such as
a moist or aqueous environment, or soils containing moisture
Affected Materials
All metals with the exception of noble metals
Critical factors
a) For galvanic corrosion, three conditions must be met:
i. Presence of an electrolyte, a fluid that can conduct a current.
10
Moisture or a separate water phase is usually required for the
solution to have enough conductivity.
ii. Two different materials or alloys known as the anode and the
cathode in contact with an electrolyte.
iii. An electrical connection must exist between the anode and the
cathode.
b) The more noble material (cathode) is protected by sacrificial corrosion
of the more active material (anode). The anode corrodes at a higher
rate than it would if it were not connected to the cathode.
c) The farther the alloys are apart in the galvanic series, the higher the
driving force for corrosion.
d) The relative exposed surface areas between anodic material and the
cathodic material has a significant affect.
i. Corrosion rate at the anode can be high if there is a small
anode to cathode ratio
ii. Corrosion rates of the anode will be less affected if there is a
large anode to cathode ratio
iii. If there is a galvanic couple, the more noble material may need
to be coated. If the active material were coated, a large cathode
to anode area can accelerate corrosion of the anodes at any
breaks in the coating.
iv. The same alloy may act as both and anode and a cathode due
to surface films, scale or local environment.
Affected equipment
a) Heat xchangers are susceptible if the tube material is
different from the tubesheet, particularly if salt water cooling
is utilized.
b) Buried pipeline, electrical transmission support towers and
ship hulls are a typical location for galvanic corrosion.
11
2.2 Non Destructive Testings (NDT)
2.2.1 Dye Penetrant Test DPT
Dye Penetrant Testing is a surface testing method mainly for detecting surface
breaking defects (opened to surface). This method is easy to handle and applicable to
all materials, except for excessively porous materials like ceramic
Working principle of DPT are:
1. It can only detect surface breaking defects
2. Penetrant must be able to enter the defect to form indication
3. Not suitable for porous or very absorbent materials (wood, cloth, ceramic)
4. Migrating by capillary action (cohesive force, adhesive force, surface tension)
into discontinuities opened to surface
5. Reverse capillary action due to equilibrium action
6. Blotter effect by developer
7. Contrast between the liquid dye and the developer
Basic steps:
1. Pre-cleaning (surface preparation)
- Prevent capillary action from taking place
- Ensure crack is not filled by debris and no surface contaminant
- Pre-cleaning can be done by applying mechanical cleaning, detergent
cleaning, steam cleaning, ultrasonic cleaning etc.
2. Penetrant application on the surface
Figure 2 : Application of penetrant on the surface
- Penetrating fluid (penetrant) applied to component and drawn into defect
by capillary action
- Provide a contrast for detection of indication and apply in excess
- Can be done by spraying, immersion and pouring
12
- Allow time for penetration into cracks within 5-15 minutes and not to
long for it to dry up
3. Removal of excess penetrant
- Remove excess penetrant that is not relevant to crack indication during
development.
Figure 3: Removal of excess penetrant
4. Application of developer
- Provide medium for reverse capillary action to take place
- Provide contrast to the indication (typically white color against red color
of penetrant)
- Developing time is depends on the size of discontinuities (wide crack –
immediate result)
Figure 4: Application of developer
5. Inspection
- Penetrant which pulled out from the defect by the developer forms
indication of the defect
13
6. Post-cleaning
- Removing of penetrant and developer after testing
- To avoid potential corrosion to occur
7. Results
- Final interpretation shall be made after 7-30 minutes after the
development process are satisfied.
-
Indications due to reverse capillary action
Figure 5: Indications of surface breaking
Figure 6: Indication on the weldment
Figure 7: Student demonstrating DPI
14
2.2.2 Magnetic Particle Test (MPT)
Working Principle
A ferromagnetic test specimen is magnetized with a strong field
created by a magnet or special equipment. If the specimen has a
discontinuity, the magnetic field flowing through the specimen will be
interrupted and a leakage field will occur. Finely milled iron particles coated
with a dye pigment are applied to the test specimen. These particles are
attracted to leakage fields and will cluster to form an indication directly over
the discontinuity. This indication can be visually detected under proper
lighting conditions.
Figure 8 : Working principle of MPT
Basic procedures involved the following steps:
1. Component pre-cleaning
When inspecting a test part with the magnetic particle method it is
essential for the particles to have an unimpeded path for migration to both
strong and weak leakage fields alike. The surface should be clean and dry
before inspecting. Contaminants such as oil, grease or scale may not only
prevent particles from being attracted to leakage field, they may also
interfere with interpretation of indications.
2. Introduction of magnetic field
The required magnetic field can be introduced into a component in a
number of different ways.
a) Using a permanent magnet or an electromagnet that contacts the
test piece
15
b) Flowing an electrical current through the specimen
c) Flowing an electrical current through a coil of wire around the part
or through a central conductor running near the part
Two general types of magnetic fields (longitudinal and circular)
may be established within the specimen. The type of magnetic field
established is determined by the method used to magnetize the
specimen. A longitudinal magnetic field has magnetic lines of force
that run parallel to the long axis of the part. A circular magnetic field
has magnetic lines of force that run circumferentially around the
perimeter of a part.
3. Application of magnetic media
Magnetic Particle Test can be performed using either dry particles or
particles suspended in a liquid. With the dry method, the particles are
lightly dusted on to the surface. With the wet method, the part is flooded
with a solution carrying the particles. The dry wet is however more
portable. The wet method is generally more sensitive since the liquid
carrier gives the magnetic particles additional mobility.
Figure 9: Dry method Figure 10: Wet method
4. Interpretation of magnetic particle indications
After applying the magnetic field, indications that form must interpreted.
This process requires that the inspector distinguish between relevant and non-
relevant indications. The following series of images depict relevant
indications produced from a variety of components inspected with the
magnetic particle method.
16
Figure 11: Crane Hook with service induced crack
Figure 12: Gear with service Induced Crack
Figure 13: Drive Shaft with heat Treatment Induced Cracks
Figure 14: Lack of fusion in SMAW weld
17
Advantages of Magnetic Particle Inspection:
1. Can detect both surface and near sub-surface defects.
2. Can inspect parts with irregular shapes easily.
3. Precleaning of components is not as critical as it for some other methods
4. Fast method of inspection and indications are visibly directly on the
specimen surface
5. Is a very portable inspection method especially when used with battery
powered equipment
Limitations of Magnetic Particle inspection:
1. Cannot inspect non-ferrous materials such as aluminium, magnesium or
most stainless steels.
2. Inspection of large parts may require use of equipment with special
power requirements.
3. Some parts may require removal of coating or plating to achieve desired
inspection sensitivity.
4. Limited subsurface discontinuity detection capabilities. ( maximum depth
0.6” under ideal conditions)
5. Post cleaning and post demagnetization is often necessary
6. Alignment between magnetic flux and defect is important.
2.2.3 Ultrasonic Testing
Working Principle
Ultrasonic Test apply the principle of high frequency sound waves which are
introduced into a material. The reflected sound gives information on the material
under test and signals displayed on a CRT. The sound is transmitted in the material
to be tested.
Figure 15: The sound reflected back to the probe is displayed on the Flaw Detector
18
The distance the sound travel can be displayed on the flaw detector.
The screen can be calibrated to give accurate readings of the distance. The
presence of a defect in the material shows up on the screen of the flaw
detector with a less distance than the bottom of the material. The closer the
reflector to the surface, the signal will be more to the left of the screen. The
thinner the material the less distance of sound travel.
Advantages of UT
1. Sensitive to cracks at various orientations
2. Portability
3. Safety
4. Able to penetrate thick sections
5. Measures depth and through wall extent
Disadvantages of UT
1. No permanent record (unless automated)
2. Not easily applied to complex geometries and rough surfaces
3. Unsuited to course grained materials
4. Requires highly skilled and experience technicians.
2.2.4 Radiographic Test
The radiographic testing applied the electromagnetic radiation which is
imposed upon a test object. Radiation is transmitted to varying degrees
dependent upon the density of the material through which it is travelling.
Variations in transmission detected by photographic film or fluorescent
screens. Applicable to metal, non-metals and composites
Figure 16: Illustration of Radiographic Test
19
There are two common radiographic source which are Isotopes produces
Gamma rays and X-ray tube.
Gamma Rays X-Rays
Safety Constraint emission Can be switched off/on
Capabilities Very high penetrating
power
Intensity and wavelength can
be adjusted
Quality of
images Lower quality Better quality
Handling Easier to handle
X-ray machine are bulky,
fragile and requires
electricity
Cost Cheap Expensive
Table 3 : Comparison of Gamma Rays and X-Rays
Figure 17: Result produced
20
The advantages of RT are:
1. Permanent record
2. Detection of internal flaws
3. Can be used on most materials
4. Direct image of flaws
5. Real-time imaging
6. Can detect very thin thickness (small bore piping)
The disadvantages of RT are:
1. Health hazard
2. Sensitive to defect orientation
3. Limited ability to detect fine cracks
4. Access to both sides required
5. Limited by material thickness
6. Skilled interpretation required
7. Relatively slow
8. High capital outlay and running costs.
2.3 PETRONAS Risk-Based Inspection (P-RBI)
Introduction to RBI
Risk-based Inspection is a systematic data analysis of equipment condition to
determine the associated risk with its operation. It is a method for prioritising
equipment for inspection based on risk. RBI will determine risk associated
with operation of specific items of equipment and the key issues driving the
risk. Other than that RBI is an important decision making tool for inspection
planning.
Figure 18: RBI Risk Matrix
21
Risk Definition
Risk is simply a multiplication of probability of failure and Consequences of
Failure.
Probability of failure is a measure of events per year and is referring
to types of equipment, deterioration of the equipment and the uncertainty in
the equipment condition. While consequence of failure is a measure of impact
per event and is based on the loss of containment (process safety,
environmental impact, reputation and asset)
Continuum of RBI Approaches
Figure 19: Three distinct level namely qualitative , semi-quantitative and
quantitative
Balance is required to select most suitable approach
Qualitative Quantitative
Ease of implementation
Less costly
Require presence of SME
Difficult to audit results
Sensitive to expert view
Data intensive
Sensitive to data quality
Costly
Able to audit
Executed as part of large exercise
Table 4: Continuum of RBI approaches
22
RBI Process
Simplified block diagram of RBI process showing essential elements of
inspection planning based on risk analysis regardless of approach is a below:
Figure 20: Simplified Block diagram of RBI Process
The RBI process consists of performing a risk assessment of the
equipment, then determining inspection frequencies and scopes. Many types
of RBI methods exist and are currently being applied throughout industry.
Technologies behind RBI
In developing the Risk Based Inspection, there are technologies involve in
order to enhance the reliability of the data analysis.
a) Materials and construction
b) Corrosion and failure mechanisms
c) Process and operations
d) Inspection and maintenace
e) Safety and risk analysis
f) ICT
The need of Risk Based Inspection
a) Reduce risk of high consequence failures
b) Manage risks associated with inspection programs
c) Facilitates reallocation of resources from lower to higher risk equipment
d) Plant optimization ( inspection techniques and maintenance
23
RBI Benefits to plant/end users
The RBI approach gives benefits to the plant operation and the end users. It
provides the capability to define and measure risk, creating a powerful tool for
managing many of the important elements of a process plant. It allows management
to review safety in an integrated, cost effective manner. On the other hand, it
systematically reduces the probability of failures by making better use of the
inspection resources and finally improves the integrity of plant equipement.
Impacts of RBI
a) Improves communication across organization
b) Able to translate engineering concern into management interest
c) Emphasis on importance of data management
d) Improved inspection work quality.
2.4 Inspection Reference Plan (IRP)
IRP Management
Inspection Reference Plan Management is another management practice for
inspection activities and effectiveness. This practice will relate to equipment type
and criticality category from the RBI and provide linkage to identify failure modes. It
will also create a dynamic inspection plan by concerning the methods, location,
extent and frequency. Other than that, by practicing IRP, the condition of monitoring
confidence can be evaluated and also proposed recommendation of reducing or
increasing inspection frequency.
The IRP should be designed with other mitigation plan so that all equipment will
have resultant risks that are acceptable. There are few considerations in developing
IRP which includes the following;
1. Risk ranking and drivers
2. Inspection history
3. Number and results of inspection
4. Type and effectiveness of inspection
5. Equipment in similar service
6. Remaining life 24
Risk ranking and drivers
Risk ranking is used to prioritize equipment in an inspection program. Risk
drivers ( consequence factors and probability factors) will determine the possibilities
for risk management by inspection.
Number and effectiveness of inspection
Inspection will only effective if the inspection technique chosen is sufficient for
detecting the deterioration mechanism and its severity.
The level of risk reduction will depend on :
a) Mode of failure of the deterioration mechanism
b) Rate of deterioration
c) Detection capability of the inspection technique
d) Scope of inspection
e) Frequency of inspection
Inspection Strategy
Effectiveness of past inspection impact on present risk. Future risk can only
be impacted by future inspection. The key parameters of the inspection strategy are:
a) Type of NDT selected
Types of NDT selected will depend on:
1. The deterioration mechanism to be detected and/or monitored
2. Accessibility to expected deterioration
3. Operational constraint such as temperature
Any equipment maybe subjected to a number of deterioration mechanism –
each of which will impose its own requirements for frequency and coverage.
b) Location and extent of inspection
The consequence of failure (CoF) of an equipment may be used as a
determinant in determining the appropriate location and extent, for example a
high consequence may be related to a high degree of coverage.
The location and extent shall relate to the particular part of the equipment
where the deterioration is most likely to take place.
The nature of the inspection technique chosen will also influence the location
or extent of inspection.
25
c) Frequency of inspection
Frequency of inspection should have a relationship to the rate of
deterioration and the remaining life of the equipment. Increasing the
frequency may not contribute to risk reduction
d) Internal of external inspection
Risk reduction by both internal and external inspection should be
assessed. Often external inspection with effective on-stream inspection and
process monitoring can replace the need for intrusive inspection without
unduly increasing the risk. Invasive inspection may in some case, increase the
risk of the item for example:
a) Moisture ingress
b) Lining damage
c) Risks associated with shutting down and start-up
e) Procedures and practices.
Inspection procedures and the actual inspection practices can impact
on the ability of inspection activities to identify, measure and monitor
deterioration mechanisms.
Comprehensive procedures and practices applied by a competent staff can be
highly effective. Poor procedure and practices applied by competent staff
may give moderately acceptable results. Poor procedures and practices
applied by inexperience and poorly trained staff will only serve to greatly
increase any risk.
26
3. PROJECT AND ASSIGNMENT
3.1 Project Background
In several processes for manufacturing chemicals or for processing materials
gas streams are produced that are subject to entrainment of droplets of liquid carried
over from prior processing, for example droplets of water or liquid hydrocarbons.
Entrained droplets of small size are referred to as mist. The streams containing
entrained droplets are term wet gas. Frequently, it is desirable to remove entrained
liquid as it will adversely affect further processing of the gas stream. In these cases it
is necessary to remove the entrained droplets, one method for which is to use a wet
gas separator. Such a process also may be termed de-entraining, entrainment
separation or demisting.
Several designs are known for separation of entrained droplets of liquid from
gas stream. A wet gas separator typically uses a contact system to cause the entrained
droplets to accumulate into a stream of liquid that is separated from the gas stream.
Frequently the liquid droplets are treated as particulate matter and removed using
filters, cyclones and other means, as outlined.
The internal of Wet Gas Separator was revamped to improve its separation
efficiency by installing new VDX3-4M Inlet Diffuser Device and Z-Pack De-
entraining Device. VDX3-4M Inlet Diffuser Device is installed at the inlet of the
vessel. Its function is to diffuse, distribute and deliver a uniform horizontal gas flow
above liquid level towards mist elimination internals.
Z-Pack Deentraining Device is vertically installed at the center in front of existing
wire mesh pad. Its function is to separate coarse droplets and suspended solids from
the feed gas stream. It offers first stage mist elimination and reduces the load on the
wire mesh.
Wire Mesh Mist Eliminator is installed at the center of the vessel after the Z-pack
device. It is made of fine wire mesh partitions which are arranged together vertically.
Its function is to draw liquid from the gas stream and channel it downwards.
27
Equipment Data
ITEM NAME : WET GAS SEPARATOR
ITEM NO : V6-0401
CODE : ASME SEC. VIII DIV. 1 1992ED. 1994ADD
OTHER SPEC. : PTS 31.22.20.31 W/AD. SPC NO. 056/3000/005-02, SPC NO.
056/3000/027-01 & RELEVANT PTS SPEC. W/ADD
DESIGN PRESSURE : (INTERNAL) 8.1700 MPA.G
(EXTERNAL) 0.0000 MPA.G
DESIGN TEMPERATURE : (INTERNAL) 70.00 DEG.C
(EXTERNAL) 0.00 DEG.C
OPERATING PRESSURE : 6.58 MPA.G
OPERATING TEMPERATURE : (NORM./MAX) 26.7/30.0 DEG.C
CORROSION ALLOWANCE :
SHELL : 3.000 MM (5.0 WELD OVERLAY : BTM 150 MM)
HEAD : 3.000 MM (5.0 WELD OVERLAY : BTM 150 MM)
NOZZLE : 3.000 MM
RADIOGRAPHY :
SHELL : FULL
HEAD : FULL
SHELL TO HEAD : FULL
WIND : PTS 34.00.01.30 (V10XF = 40.3 m/s
EARTHQUAKE : UBC (1994) ZONE 1, I = 1.O
MATERIAL :
SHELL : SA 516-70 & 304L PARTIAL OVERLAY
HEAD : SA 516-70 & 304L PARTIAL OVERLAY
NOZZLE : SA 350-LF2, SA350-LF2+WELD OVERLAY
SUPPORT : SA 516-70
MAX. ALLOWANCE WORKING PRESSURE (MAWP) : 8.1912 MPA.G
HYDROSTATIC TEST PRESSURE : 12.2868 MPA.G
Table 5: Wet Gas Separator equipment data
During the 2010 GPP 6 Major TA, accelerated metal loss near to the SS weld
Overlay was observed inside the GPP 6 Wet Gas Separator (V6-0401). The initial
findings indicated this could be due to pitting and Inspection team decided to apply
“Belzona” metal coating to mitigate the issue.
28
As the GPP 5 Wet Gas Separator also will undergo an internal revamp in
January 2012, an investigation team was formed to investigate the root cause of this
accelerated metal loss.
The equipment internals were modified in the June 2008 to address separation
efficiency.
The failure has caused the remnant life of the wet gas separator reduced by 4 years
and an extensive repair work needs to be performed.
Figure 21: Before and after internal modification in 2008
3.2 Objective
The objective of this project is to identify the root cause of the accelerated
metal loss at the internal of Wet Gas Separator by applying the Root Cause
Failure Analysis (RCFA).
3.3 Root Cause Failure Analysis (RCFA) – 5 Why Analysis on Wet Gas
Separator
3.3.1 Inspection report findings
By comparison between the internal condition of the separator within 2
years of revamp from 2008 to 2010, a very significant increase of metal
loss was found. In 2008, pitting corrosion was observed to be less than
1.5 mm. However, the pitting corrosion has accelerated to be 4.0 mm to
5.0 mm after 2 years in 2010. Below are the image of visual inspection at
the internal of the separator.
29
Figure 22: 2008- No erosion observe Figure 23: 2010 – severe corrosion
observed
30
Findings at the internal (2008):
c) Pitting corrosion was noted along the
bottom part of internal shell wall, adjacent
to cladding) with maximum depth
approximately < 1.5 mm
d) internal weldment noted in satisfactory
condition
e) manhole noted in satisfactory condition
3.4 RCFA Problem Statement
V6-0401 Wet Gas Separator has experienced accelerated corrosion rate of 0.45
mm/yr compared to 0.15mm/yr allowed since 2008 after major modification
performed on internals of the vessel. The impact over that period had been RM 480
000 loss profit opportunity and RM39 000 maintenance costs.
31
Findings at the internal (2010):
1) East side dish head, sustain with
severe pitting corrosion on area
adjacent to cladding, measured
with maximum depth of 4.0
mm. Appearance like wash
away of metal
2) East side shell wall. Corrosion
attack up to 1500mm from area
adjacent to cladding.
Figure 24: Chronology of Events (Events and Causal Factors)
Figure 25: 5 – WHY Analysis
32
No. Analysis parameters Result
1. pH 5.5
2. Oil & Grease 30.7 ppm
3. COD 243 ppm
4. Conductivity 53.9 uS/cm
5. TDS 24 ppm
6. NH3 0.614 ppm
7. FRC 0.03 ppm
8. Chloride 2.05 ppm
9. Total Hardness 36 ppm
10. Amine As attached
Table 6 : Lab Analysis as per taken on 2 April 2011 at V6-0401 boot
3.5 Conclusion
From the Root Cause Failure Analysis, the erosion-corrosion was identified to
be the major damage mechanism of metal loss. The failure of the equipment is
mainly contributed by the new inlet device which promotes the above damage
mechanisms by changing the floe direction at the inlet region. It has also caused
splashing of water beyond cladded area, consequently bottom vane too close to liquid
surface and acidic water formation.
33
4. OTHER INVOLVEMENTS
Throughout the eight months of internship, the host company had arranged several
programmes and courses which had given the author the opportunities to experience
an extra learning and knowledge. Followings are the involvements of the author :
Events/Training Date
P-RBI Training at NIOSH Kemaman December 2010
POD-GPPB Away Day at Peladang Agro Setiu
Resort January 2011
SAPTE Process Piping Workshop at GPPA January 2011
GPP4 & KCSB TA SOE Development Workshop
at Kelab Golf Rantau Petronas January-February 2011
Centralized Utility Facilities (CUF) ASU2 Mini
Turn Around
20th
February – 4th
March
2011
GPP B Boiler Refresher Training March 2011
GPPB Football Tournament March 2011
HSE Workgroup Champion PGB May 2011
PETRONAS Family Festival, KGRP Jun 2011
Table 7 : Others involvement
34
5. LESSONS LEARNT
Throughout the industrial training, the author had been given tasks and
assignment which are new and not familiar. In industrial application, good
theoritical and technical knowledges are very important. Thus the author has always
building positive attitudes in learning new things. The effort of learning is required
while getting information by reading and researching in completing the tasks beside
the discussion with supervisor and technical staffs. Other than that, the decision
making skills are also being practiced. During discussion and meeting, decision must
be done in the limitation of time and circumstances. Experience and good
understanding about particular subject are helpful in making decision. However,
some of the decision made are with the guidance from many parties.
In addition, being in working environment require one to deal with many
people of various background and level. Here, and excellence discipline and self
control must be developed such as to obey the company’s regulation, dress code and
others. Professionalism is one of the aspects that must be enhanced. Apart from that,
the chance to get involve with industry has encouraged the author to always adopt
good communication and management skills
5.1 Challenges faced and Solutions to overcome
a) First time working experience
The author had never worked in industry, and this industrial training is the
first exposure to the real working environment. The author had taken some
times to adapt with this new environment and had gained new things and
experience from day to day.
b) Learning hands-on engineering aspect
In inspection department jobscopes, one need to have good understanding and
knowledege about the engineering aspects. One must have the ability to
execute the technical jobs. Thus, the author had gain such a great experience
handling engineering problems and calculation.
35
6. RECOMMENDATION
The host company ( PETRONAS Gas Berhad) has provided the author
a wide range of opportunity during internship training in engineering aspects.
The author had been given many involvements and exposures which mostly
related to Inspection field. Credits also should be given to Universiti
Teknologi PETRONAS for enabling such a great medium for students in
attaining real working environment. This industrial training is sufficient for
students to lean and fit themselves in the industry.
6.1 Recommendation to the Host Company
The author would like to suggest the host company to provide
trainee with ample hands-on technical jobs and allow the students
to handle the tasks. It is also suggest that the trainee could be
entertained as staff rather than a students to create self-belonging
to the company and the task given. Besides that, proper assistance
for trainee by preparing the practical handbook would be helpful
to the trainee.
6.2 Recommendation to the University
The author feels that the university should improve the monitoring
system in order to monitor the training program that the student is
undergoing. The supervision which usually done during the first
and second visit is not sufficient. Thus, SIIU should also updated
on the student welfare at the respective company. This will make
the training programme more effective. Apart from that, the
university may revise the internship policies so that students can
get involve with confined space equipment especially for those
working at the processing and refining plant. By allowing the
students to do so, it is believe students could grab more
experience throughout the challenging work exposures.
36
7. CONCLUSION
The eight months period of Industrial Internship Training Programme (IITP)
had given the author the opportunities to learn new things and gained many
experiences through the involvement of various projects and tasks. The IITP also had
allowed the author to developed working skills and work ethics that needed by
current employers. IITP is the best platform to expose the student with the real-life
working experience besides giving them the rough picture of what to be expected
when they have graduate from the University and start a working life.
The eight months duration has not only benefit the author, but also the UTP
and the Host Company. The UTP has managed to build a good rapport with the Host
Company through this programme and the Host Company meanwhile has the
opportunity to evaluate and train their future employees. The author believes that all
the objectives of the IITP that been set by SITU were achieved during the eight
months of the industrial training with close supervision by both sides, the Host
Company (PETRONAS Gas Berhad) and also the University (UTP).
Some recommendations were made to both the Host Company and UTP in
order to improve the training programme in future. This to ensure that future trainee
will not encounter the same problems that the author had. The improvement made
will enhance relationship between both of the parties involved. The author hopes the
IITP will be keep offer in the future due to its voluminous benefit to all.
37
REFERENCES
1. API Publication 580 – Recommended Practice for Risk Based Inspection
2. George Antaki, “ Risk based Inspection in Refineries, Petrochemical Plants
and Oil/Gas Plants”.
3. API 571 – Damage Mechanisms Affecting Fixed Equipment in the Refining
Industry. Recommended Practice 571 First Edition, December 2003
4. Petronas Technical Standard (PTS)
5. API Recommended Practice 579, Fitness for Service, First Edition.
6. Principles of Magnetic Particle testing, American Society for Nondestructive
Testing
7. Charles Hellier (2003). Chapter 7 – Ultrasonic Testing. Handbook of
Nondestructive Evaluation
8. Petronas Gas Berhad, Paka, Terengganu. www.petronasgas.com
9. UTP Internship Guidelines for Student Industrial Internship Programme
38
APPENDICES
Appendix 1: Piping Integrity Management System
39
DEVELOPMENT OF CORROSION GROUP
(MARK-UP ON PFD)
(
START
CLASSIFICATION OF PIPING CIRCUIT
(MARK-UP ON P&ID)
SELECTION OF PIPING REPRESENTATIVE
INSPECTION
EXAMINATIO
N
FFS
RERATE/MOC
INPUT IN RBI
RUN ANALYSIS/CRITICALITY
REVIEW INSPECTION EFFECTIVENESS
DEVELOPMENT OF IRP/MITIGATION
PLAN
Confirm to Requirement
Confirm to Requirement
NCR
NCR
REA
SSES
SMEN
T P
RO
CES
S
Responsible Party
Corrosion Engineer
Piping Inspector
Inspection/Maintenance/
Operation/Engineering/PPL
Piping Inspector/NDE
Examiner
Inspection Engineer/ TP
Inspection
Inspection
Engineer/Operation
Engineer/Maint.Eng/PPL
Piping Inspector
RBI/GTS Engineer
Inspection Eng/ TP Inspection
Inspection Eng/TP Inspection
Interface
Operation/Technologist
Inspection Engineer
Department Manager
Inspection Engineer
TP Inspection
(Principle/Custodian)
Plant Manager
RBI/GTS Engineer
None
RBI/GTS Engineer
RBI/GTS Engineer
Appendix 2: Simplified Block Flow Diagram of gas processing
40
Appendix 3: DOSH Registered Equipments for Gas Plant Processing B
NO DOSH NO EQUIPMENT DESCRIPTION
1 PMT107915 C6-0101 HYDROCARBON STRIPPER
2 PMT107916 E6-0101 HYDROCARBON STRIPPER FEED PREHEATER
3 PMT107917 S6-0101A FEED GAS FILTER
4 PMT107918 S6-0101B FEED GAS FILTER
5 PMT107919 S6-0102A FEED LIQUID FILTER
6 PMT107920 S6-0102B FEED LIQUID FILTER
7 PMT107921 S6-0103 FILTER SEPARATOR
8 PMT107922 V6-0101 INLET SEPARATOR
9 PMT107924 V6-0103 CONDENSATE/WATER SEPARATOR
10 PMT107925 C6-0201A ABSORBER
11 PMT107926 C6-0201B ABSORBER
12 PMT107927 E6-0201 FEED/PURE GAS EXCHANGER
13 PMT107928 E6-0202 SOLUTION HEATER
14 PMT107929 E6-0203A CO2 OFF GAS COOLER
15 PMT107930 E6-0204A SOLUTION COOLER
16 PMT107931 E6-0205 FLASH GAS COOLER
17 PMT107932 S6-0201A MECHANICAL FILTERS
18 PMT107933 S6-0201B MECHANICAL FILTERS
19 PMT107934 S6-0202A CARBON FILTERS
20 PMT107935 S6-0202B CARBON FILTERS
21 PMT107936 S6-0203A GUARD FILTERS
22 PMT107937 S6-0203B GUARD FILTERS
23 PMT107939 V6-0202 LOW PRESSURE FLASH DRUM
24 PMT107940 V6-0203 ABSORBER OVERHEAD K.O. DRUM
25 PMT107941 V6-0204 CO2 OFF GAS K.O. DRUM
26 PMT107942 V6-0205 SOLUTION HEATER COND. K.O. DRUM
27 PMT107943 V6-0206 SOLUTION SUMP TANK
28 PMT107944 V6-0207 FLASH GAS SEPARATOR
29 PMT107945 E6-0301A REGENERATION OFF GAS COOLER
30 PMT107946 S6-0301A DUST FILTERS
31 PMT107947 S6-0301B DUST FILTERS
32 PMT107951 V6-0301 D DEHYDRATOR
33 PMT107953 V6-0302A MERCURY REMOVAL VESSELS
34 PMT107954 V6-0302B MERCURY REMOVAL VESSELS
35 PMT107955 V6-0303 REGENERATION OFF GAS K.O. DRUM
36 PMT107956 C6-0401 DEMETHANIZER
37 PMT107957 E6-0401 WARM GAS EXCHANGER
38 PMT107958 E6-0402 HOT GAS CHILLER
39 PMT107959 E6-0403 DEETHANIZER STEAM REBOILER
40 PMT107961 E6-0406 REBOILER
41
Appendix 4: Equipment Certificate of Fitness (CF)
41
42
Appendix 5: RBI Criticality Ranking
Appendix 6: Laboratory Analysis Test result
43
Appendix 7: External Visual Inspection equipment report
44