files.nc.gov management/dwm/sf/cts mills gap... · september 27, 2010 lims use: fr - susan kelly...

APPENDIX D

LABORATORY ANALYTICAL REPORTS

September 27, 2010

LIMS USE: FR - SUSAN KELLYLIMS OBJECT ID: 9276750

9276750Project:Pace Project No.:

RE:

Ms. Susan KellyMactec Asheville1308 Patton AvenueAsheville, NC 28806

MILLS GAP 6686081744

Dear Ms. Kelly:Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2010.The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of thereport.

Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory andOrganic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. AllMicrobiological analyses were performed at the laboratory where the samples were received.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kevin Godwin

[email protected] Manager

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

Page 1 of 242

Pace Analytical Services, Inc.9800 Kincey Ave. Suite 100

Huntersville, NC 28078

(704)875-9092

Pace Analytical Services, Inc.2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176

CERTIFICATIONS

Pace Project No.:Project:

9276750MILLS GAP 6686081744

Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784

South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031

Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9

North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072



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SAMPLE SUMMARY


9276750MILLS GAP 6686081744

Lab ID Sample ID Matrix Date Collected Date Received

9276750001 SS-113A Solid 08/30/10 14:35 09/01/10 14:00

9276750002 SS-113B Solid 08/30/10 14:40 09/01/10 14:00

9276750003 SS-116A Solid 08/31/10 09:15 09/01/10 14:00

9276750004 SS-116B Solid 08/31/10 09:25 09/01/10 14:00

9276750005 SS-122 Solid 08/31/10 10:10 09/01/10 14:00

9276750006 SS-125 Solid 08/31/10 11:00 09/01/10 14:00

9276750007 SS-126 Solid 08/31/10 11:45 09/01/10 14:00

9276750008 FD-01 Solid 08/30/10 00:00 09/01/10 14:00

9276750009 FD-02 Solid 08/30/10 00:00 09/01/10 14:00

9276750010 FD-03 Solid 08/30/10 00:00 09/01/10 14:00

9276750011 FD-04 Solid 08/30/10 00:00 09/01/10 14:00

9276750012 FD-05 Solid 08/30/10 00:00 09/01/10 14:00

9276750013 SS-127 Solid 08/31/10 13:45 09/01/10 14:00

9276750014 SS-128 Solid 08/31/10 14:20 09/01/10 14:00

9276750015 SS-129 Solid 08/31/10 14:45 09/01/10 14:00

9276750016 SS-109A Solid 08/31/10 17:00 09/01/10 14:00

9276750017 SS-109B Solid 08/31/10 17:05 09/01/10 14:00

9276750018 SS-109C Solid 08/31/10 17:15 09/01/10 14:00

9276750019 SS-109D Solid 08/31/10 17:25 09/01/10 14:00

9276750020 SS-109E Solid 08/31/10 17:30 09/01/10 14:00

9276750021 SS-104A Solid 09/01/10 09:50 09/01/10 14:00

9276750022 SS-104B Solid 09/01/10 10:00 09/01/10 14:00

9276750023 SS-104C Solid 09/01/10 10:05 09/01/10 14:00

9276750024 SS-104D Solid 09/01/10 10:15 09/01/10 14:00

9276750025 SS-104E Solid 09/01/10 10:20 09/01/10 14:00

9276750026 SS-101A Solid 09/01/10 11:25 09/01/10 14:00

9276750027 SS-101B Solid 09/01/10 11:30 09/01/10 14:00

9276750028 SS-101C Solid 09/01/10 11:35 09/01/10 14:00

9276750029 SS-101D Solid 09/01/10 11:45 09/01/10 14:00

9276750030 FD-06 Solid 08/31/10 00:00 09/01/10 14:00

9276750031 FD-07 Solid 08/31/10 00:00 09/01/10 14:00

9276750032 FD-08 Solid 08/31/10 00:00 09/01/10 14:00

9276750033 FD-09 Solid 08/31/10 00:00 09/01/10 14:00

9276750034 FD-10 Solid 08/31/10 00:00 09/01/10 14:00

9276750035 FD-11 Solid 08/31/10 00:00 09/01/10 14:00

9276750036 FD-12 Solid 08/31/10 00:00 09/01/10 14:00

9276750037 FD-13 Solid 09/01/10 00:00 09/01/10 14:00



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SAMPLE SUMMARY


9276750MILLS GAP 6686081744

Lab ID Sample ID Matrix Date Collected Date Received

9276750038 FD-14 Solid 09/01/10 00:00 09/01/10 14:00

9276750039 FD-15 Solid 09/01/10 00:00 09/01/10 14:00

9276750040 MB-01 Water 08/31/10 10:30 09/01/10 14:00

9276750041 EB-01 Water 08/31/10 16:30 09/01/10 14:00

9276750042 FB-01 Water 08/31/10 16:45 09/01/10 14:00

9276750043 TB-01 Solid 08/30/10 00:00 09/01/10 14:00

9276750044 TB-02 Water 08/31/10 00:00 09/01/10 14:00

9276750045 TB-03 Solid 08/31/10 00:00 09/01/10 14:00



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SAMPLE ANALYTE COUNT


9276750MILLS GAP 6686081744

Lab ID Sample ID MethodAnalytesReportedAnalysts

9276750001 SS-113A EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750002 SS-113B EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750003 SS-116A EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750004 SS-116B EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750005 SS-122 EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750006 SS-125 EPA 6010 13JMW

EPA 7471 1JDA



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9276750MILLS GAP 6686081744


EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750007 SS-126 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750008 FD-01 ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

9276750009 FD-02 EPA 6010 13JMW

EPA 7471 1SHB

ASTM D2974-87 1KDF

9276750010 FD-03 EPA 8270 73BPJ

ASTM D2974-87 1KDF

9276750011 FD-04 EPA 8260 56DLK

ASTM D2974-87 1KDF

9276750012 FD-05 ASTM D2974-87 1TNM

EPA 7196 1EWS

9276750013 SS-127 EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750014 SS-128 EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS



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9276750MILLS GAP 6686081744


9276750015 SS-129 EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750016 SS-109A EPA 6010 13JMW

EPA 7471 1SHB

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750017 SS-109B EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750018 SS-109C EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750019 SS-109D EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750020 SS-109E EPA 6010 13JMW

EPA 7471 1JDA



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9276750MILLS GAP 6686081744


EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750021 SS-104A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750022 SS-104B EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750023 SS-104C EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750024 SS-104D EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750025 SS-104E EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73RRH

EPA 8260 56DLK



Page 8 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744


ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750026 SS-101A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750027 SS-101B EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750028 SS-101C EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750029 SS-101D EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276750030 FD-06 EPA 6010 13JMW

EPA 7471 1JDA

ASTM D2974-87 1TNM

9276750031 FD-07 EPA 8260 56DLK

ASTM D2974-87 1TNM

9276750032 FD-08 EPA 8270 73BPJ



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9276750MILLS GAP 6686081744


ASTM D2974-87 1KDF

9276750033 FD-09 ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

9276750034 FD-10 EPA 8270 73BPJ

ASTM D2974-87 1KDF

9276750035 FD-11 ASTM D2974-87 1TNM

EPA 7196 1EWS

9276750036 FD-12 EPA 8260 56DLK

ASTM D2974-87 1TNM

9276750037 FD-13 EPA 6010 13JMW

EPA 7471 1JDA

ASTM D2974-87 1TNM

9276750038 FD-14 ASTM D2974-87 1TNM

EPA 7196 1EWS

9276750039 FD-15 ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

9276750040 MB-01 EPA 6010 13JMW

EPA 7470 1SAJ

EPA 8270 73BPJ

EPA 8260 56MCK

SM 4500-CN-E 1JDA

9276750041 EB-01 EPA 6010 13JMW

EPA 7470 1JDA

EPA 8270 73BPJ

EPA 8260 56MCK

SM 4500-CN-E 1JDA

9276750042 FB-01 EPA 8260 56MCK

9276750043 TB-01 EPA 8260 56DLK

9276750044 TB-02 EPA 8260 56MCK

9276750045 TB-03 EPA 8260 56DLK



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9276750MILLS GAP 6686081744

Parameters AnalyzedResultLab Sample ID

Report Limit QualifiersUnitsMethodClient Sample ID

9276750001 SS-113AArsenic 0.34J mg/kg 09/10/10 14:470.39EPA 6010Beryllium 0.35 mg/kg 09/10/10 14:470.077EPA 6010Chromium 2.4 mg/kg 09/10/10 14:470.39EPA 6010Copper 5.1 mg/kg 09/10/10 14:470.39EPA 6010Lead 5.3 mg/kg 09/10/10 14:470.39EPA 6010Manganese 290 mg/kg 09/10/10 14:470.39EPA 6010Nickel 3.6 mg/kg 09/10/10 14:470.39EPA 6010Zinc 6.1 mg/kg 09/10/10 14:470.77EPA 6010Mercury 0.011 mg/kg 09/03/10 18:000.0038EPA 7471Acetone 13.5J ug/kg 09/05/10 15:2296.5EPA 8260Percent Moisture 3.3 % 09/02/10 17:170.10ASTM D2974-87

9276750002 SS-113BArsenic 7.2J mg/kg 09/13/10 16:10 D37.6EPA 6010Beryllium 2.6 mg/kg 09/13/10 16:10 D31.5EPA 6010Chromium 35.1 mg/kg 09/13/10 16:10 D37.6EPA 6010Copper 21.5 mg/kg 09/13/10 16:10 D37.6EPA 6010Lead 15.7 mg/kg 09/13/10 16:10 D37.6EPA 6010Manganese 514 mg/kg 09/13/10 16:10 D37.6EPA 6010Nickel 25.4 mg/kg 09/13/10 16:10 D37.6EPA 6010Zinc 120 mg/kg 09/13/10 16:10 D315.1EPA 6010Mercury 0.00050J mg/kg 09/03/10 18:030.0047EPA 7471Methylene Chloride 5.2J ug/kg 09/05/10 15:4020.5EPA 8260Percent Moisture 16.3 % 09/02/10 17:170.10ASTM D2974-87

9276750003 SS-116ABeryllium 5.1 mg/kg 09/13/10 16:39 D33.4EPA 6010Chromium 35.8 mg/kg 09/13/10 16:39 D317.1EPA 6010Copper 51.6 mg/kg 09/13/10 16:39 D317.1EPA 6010Lead 17.8 mg/kg 09/13/10 16:39 D317.1EPA 6010Manganese 833 mg/kg 09/13/10 16:39 D317.1EPA 6010Nickel 18.6 mg/kg 09/13/10 16:39 D317.1EPA 6010Silver 1.5J mg/kg 09/13/10 16:39 D317.1EPA 6010Zinc 181 mg/kg 09/13/10 16:39 D334.1EPA 6010Mercury 0.0022J mg/kg 09/03/10 16:010.0047EPA 7471Acetone 451 ug/kg 09/07/10 17:16 E102EPA 82602-Butanone (MEK) 103 ug/kg 09/07/10 17:16102EPA 82602-Hexanone 10.2J ug/kg 09/07/10 17:1650.8EPA 8260Methylene Chloride 10.6J ug/kg 09/07/10 17:1620.3EPA 8260Trichloroethene 10.1 ug/kg 09/07/10 17:165.1EPA 8260Percent Moisture 10.7 % 09/02/10 17:170.10ASTM D2974-87Cyanide 4.4 mg/kg 09/05/10 13:360.21SM 4500-CN-E

9276750004 SS-116BAntimony 3.3J mg/kg 09/13/10 15:38 D35.0EPA 6010Beryllium 11.9 mg/kg 09/13/10 15:38 D31.0EPA 6010Cadmium 4.0 mg/kg 09/13/10 15:38 D31.0EPA 6010Chromium 36.9 mg/kg 09/13/10 15:38 D35.0EPA 6010Copper 87.5 mg/kg 09/13/10 15:38 D35.0EPA 6010



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9276750004 SS-116BLead 9.4 mg/kg 09/13/10 15:38 D35.0EPA 6010Manganese 4010 mg/kg 09/13/10 15:38 D35.0EPA 6010Nickel 31.4 mg/kg 09/13/10 15:38 D35.0EPA 6010Thallium 7.3J mg/kg 09/13/10 15:38 D310.1EPA 6010Zinc 193 mg/kg 09/13/10 15:38 D310.1EPA 6010Mercury 0.00017J mg/kg 09/03/10 18:050.0047EPA 7471Acetone 12.9J ug/kg 09/07/10 17:3595.6EPA 8260Methylene Chloride 14.2J ug/kg 09/07/10 17:3519.1EPA 8260Trichloroethene 476 ug/kg 09/08/10 16:1746.1EPA 8260Percent Moisture 12.8 % 09/02/10 17:180.10ASTM D2974-87Cyanide 17.8 mg/kg 09/05/10 14:580.86SM 4500-CN-E

9276750005 SS-122Antimony 1.5 mg/kg 09/10/10 15:210.39EPA 6010Beryllium 1.6 mg/kg 09/10/10 15:210.078EPA 6010Cadmium 1.7 mg/kg 09/10/10 15:210.078EPA 6010Chromium 33.8 mg/kg 09/10/10 15:210.39EPA 6010Copper 27.0 mg/kg 09/10/10 15:210.39EPA 6010Lead 3.4 mg/kg 09/10/10 15:210.39EPA 6010Manganese 71.1 mg/kg 09/10/10 15:210.39EPA 6010Nickel 5.3 mg/kg 09/10/10 15:210.39EPA 6010Selenium 0.39J mg/kg 09/10/10 15:210.78EPA 6010Silver 0.035J mg/kg 09/10/10 15:210.39EPA 6010Thallium 0.36J mg/kg 09/10/10 15:210.78EPA 6010Zinc 52.7 mg/kg 09/10/10 15:210.78EPA 6010Mercury 0.0053 mg/kg 09/03/10 16:090.0053EPA 7471Methylene Chloride 4.1J ug/kg 09/07/10 17:5319.1EPA 8260Trichloroethene 3.2J ug/kg 09/07/10 17:534.8EPA 8260Percent Moisture 19.5 % 09/02/10 17:180.10ASTM D2974-87

9276750006 SS-125Antimony 0.71 mg/kg 09/13/10 15:180.36EPA 6010Beryllium 0.56 mg/kg 09/13/10 15:180.072EPA 6010Cadmium 1.0 mg/kg 09/13/10 15:180.072EPA 6010Chromium 18.3 mg/kg 09/13/10 15:180.36EPA 6010Copper 20.7 mg/kg 09/13/10 15:180.36EPA 6010Lead 10.8 mg/kg 09/13/10 15:180.36EPA 6010Manganese 564 mg/kg 09/13/10 15:180.36EPA 6010Nickel 15.8 mg/kg 09/13/10 15:180.36EPA 6010Selenium 0.60J mg/kg 09/13/10 15:180.72EPA 6010Silver 0.082J mg/kg 09/13/10 15:180.36EPA 6010Thallium 0.80 mg/kg 09/13/10 15:180.72EPA 6010Zinc 50.0 mg/kg 09/13/10 15:180.72EPA 6010Mercury 0.0032J mg/kg 09/07/10 16:330.0050EPA 7471Benzo(g,h,i)perylene 101J ug/kg 09/23/10 14:51386EPA 8270Dibenz(a,h)anthracene 94.0J ug/kg 09/23/10 14:51386EPA 8270Indeno(1,2,3-cd)pyrene 87.8J ug/kg 09/23/10 14:51386EPA 8270Acetone 20.9J ug/kg 09/07/10 18:1295.7EPA 8260



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9276750006 SS-125Methylene Chloride 10.1J ug/kg 09/07/10 18:1219.1EPA 8260Percent Moisture 14.5 % 09/02/10 17:180.10ASTM D2974-87

9276750007 SS-126Antimony 0.80 mg/kg 09/10/10 15:280.38EPA 6010Beryllium 0.55 mg/kg 09/10/10 15:280.076EPA 6010Cadmium 0.82 mg/kg 09/10/10 15:280.076EPA 6010Chromium 19.2 mg/kg 09/10/10 15:280.38EPA 6010Copper 6.6 mg/kg 09/10/10 15:280.38EPA 6010Lead 12.6 mg/kg 09/10/10 15:280.38EPA 6010Manganese 384 mg/kg 09/10/10 15:280.38EPA 6010Nickel 10.2 mg/kg 09/10/10 15:280.38EPA 6010Selenium 0.36J mg/kg 09/10/10 15:280.76EPA 6010Thallium 0.40J mg/kg 09/10/10 15:280.76EPA 6010Zinc 47.6 mg/kg 09/10/10 15:280.76EPA 6010Mercury 0.015 mg/kg 09/07/10 16:360.0050EPA 7471Methylene Chloride 6.9J ug/kg 09/05/10 16:0019.8EPA 8260Percent Moisture 12.4 % 09/02/10 17:180.10ASTM D2974-87

9276750008 FD-01Percent Moisture 38.6 % 09/07/10 09:070.10ASTM D2974-87

9276750009 FD-02Beryllium 1.2 mg/kg 09/13/10 15:41 D30.45EPA 6010Chromium 3.4 mg/kg 09/13/10 15:41 D32.2EPA 6010Copper 20.8 mg/kg 09/13/10 15:41 D32.2EPA 6010Lead 14.4 mg/kg 09/13/10 15:41 D32.2EPA 6010Manganese 786 mg/kg 09/13/10 15:41 D32.2EPA 6010Nickel 4.7 mg/kg 09/13/10 15:41 D32.2EPA 6010Zinc 15.6 mg/kg 09/13/10 15:41 D34.5EPA 6010Percent Moisture 18.8 % 09/02/10 17:190.10ASTM D2974-87

9276750010 FD-032,6-Dinitrotoluene 300J ug/kg 09/16/10 19:12388EPA 8270Percent Moisture 14.9 % 09/07/10 09:080.10ASTM D2974-87

9276750011 FD-04Acetone 57.7J ug/kg 09/05/10 16:1996.5EPA 8260Trichloroethene 4.0J ug/kg 09/05/10 16:194.8EPA 8260Percent Moisture 13.5 % 09/02/10 17:200.10ASTM D2974-87


9276750013 SS-127Antimony 0.66 mg/kg 09/10/10 15:350.51EPA 6010Beryllium 0.60 mg/kg 09/10/10 15:350.10EPA 6010Cadmium 0.40 mg/kg 09/10/10 15:350.10EPA 6010Chromium 9.6 mg/kg 09/10/10 15:350.51EPA 6010Copper 7.2 mg/kg 09/10/10 15:350.51EPA 6010



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HITS ONLY


9276750MILLS GAP 6686081744



9276750013 SS-127Lead 16.1 mg/kg 09/10/10 15:350.51EPA 6010Manganese 232 mg/kg 09/10/10 15:350.51EPA 6010Nickel 5.7 mg/kg 09/10/10 15:350.51EPA 6010Selenium 0.46J mg/kg 09/10/10 15:351.0EPA 6010Thallium 0.58J mg/kg 09/10/10 15:351.0EPA 6010Zinc 21.9 mg/kg 09/10/10 15:351.0EPA 6010Mercury 0.025 mg/kg 09/03/10 18:110.0048EPA 7471Acetone 11.1J ug/kg 09/07/10 18:30101EPA 8260Methylene Chloride 10.9J ug/kg 09/07/10 18:3020.2EPA 8260Trichloroethene 5.4 ug/kg 09/07/10 18:305.0EPA 8260Percent Moisture 12.9 % 09/02/10 16:560.10ASTM D2974-87

9276750014 SS-128Beryllium 0.93 mg/kg 09/10/10 15:380.10EPA 6010Cadmium 0.16 mg/kg 09/10/10 15:380.10EPA 6010Chromium 6.4 mg/kg 09/10/10 15:380.51EPA 6010Copper 4.5 mg/kg 09/10/10 15:380.51EPA 6010Lead 5.9 mg/kg 09/10/10 15:380.51EPA 6010Manganese 2160 mg/kg 09/13/10 15:225.1EPA 6010Nickel 8.1 mg/kg 09/10/10 15:380.51EPA 6010Selenium 0.41J mg/kg 09/10/10 15:381.0EPA 6010Zinc 19.1 mg/kg 09/10/10 15:381.0EPA 6010Mercury 0.025 mg/kg 09/03/10 18:130.0049EPA 7471Acetone 19.9J ug/kg 09/07/10 18:4996.5EPA 8260Methylene Chloride 7.9J ug/kg 09/07/10 18:4919.3EPA 8260Trichloroethene 8.1 ug/kg 09/07/10 18:494.8EPA 8260Percent Moisture 15.7 % 09/02/10 16:560.10ASTM D2974-87

9276750015 SS-129Beryllium 0.61 mg/kg 09/10/10 15:420.12EPA 6010Cadmium 0.21 mg/kg 09/10/10 15:420.12EPA 6010Chromium 16.8 mg/kg 09/10/10 15:420.59EPA 6010Copper 15.6 mg/kg 09/10/10 15:420.59EPA 6010Lead 19.2 mg/kg 09/10/10 15:420.59EPA 6010Manganese 307 mg/kg 09/10/10 15:420.59EPA 6010Nickel 7.4 mg/kg 09/10/10 15:420.59EPA 6010Selenium 0.74J mg/kg 09/10/10 15:421.2EPA 6010Zinc 23.8 mg/kg 09/10/10 15:421.2EPA 6010Mercury 0.028 mg/kg 09/03/10 18:160.0050EPA 7471Acetone 47.7J ug/kg 09/07/10 19:0794.1EPA 8260Methyl acetate 7.4J ug/kg 09/07/10 19:079.4EPA 8260Methylene Chloride 10.1J ug/kg 09/07/10 19:0718.8EPA 8260Percent Moisture 20.3 % 09/02/10 16:560.10ASTM D2974-87

9276750016 SS-109ABeryllium 0.94 mg/kg 09/13/10 15:59 D30.65EPA 6010Chromium 16.8 mg/kg 09/13/10 15:59 D33.3EPA 6010Copper 4.5 mg/kg 09/13/10 15:59 D33.3EPA 6010Lead 5.1 mg/kg 09/13/10 15:59 D33.3EPA 6010



Page 14 of 242



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(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744



9276750016 SS-109AManganese 133 mg/kg 09/13/10 15:59 D33.3EPA 6010Nickel 7.5 mg/kg 09/13/10 15:59 D33.3EPA 6010Zinc 38.9 mg/kg 09/13/10 15:59 D36.5EPA 6010Mercury 0.038 mg/kg 09/03/10 18:180.0046EPA 7471Acetone 101 ug/kg 09/07/10 19:26 C998.5EPA 8260Methylene Chloride 16.2J ug/kg 09/07/10 19:2619.7EPA 8260Trichloroethene 4.2J ug/kg 09/07/10 19:264.9EPA 8260Percent Moisture 15.9 % 09/02/10 16:570.10ASTM D2974-87

9276750017 SS-109BBeryllium 1.5 mg/kg 09/13/10 16:02 D31.1EPA 6010Chromium 19.0 mg/kg 09/13/10 16:02 D35.5EPA 6010Copper 0.62J mg/kg 09/13/10 16:02 D35.5EPA 6010Manganese 355 mg/kg 09/13/10 16:02 D35.5EPA 6010Nickel 11.6 mg/kg 09/13/10 16:02 D35.5EPA 6010Zinc 61.3 mg/kg 09/13/10 16:02 D311.0EPA 6010Mercury 0.00080J mg/kg 09/07/10 16:390.0046EPA 7471Methylene Chloride 12.1J ug/kg 09/07/10 19:4420.8EPA 8260Percent Moisture 15.7 % 09/02/10 16:570.10ASTM D2974-87

9276750018 SS-109CBeryllium 1.5 mg/kg 09/15/10 16:210.77EPA 6010Chromium 16.2 mg/kg 09/15/10 16:213.8EPA 6010Copper 8.1 mg/kg 09/15/10 16:213.8EPA 6010Manganese 264 mg/kg 09/15/10 16:213.8EPA 6010Nickel 7.0 mg/kg 09/15/10 16:213.8EPA 6010Zinc 49.1 mg/kg 09/15/10 16:217.7EPA 6010Mercury 0.00041J mg/kg 09/07/10 16:410.0043EPA 7471Methylene Chloride 23.9 ug/kg 09/07/10 20:03 C920.2EPA 8260Trichloroethene 5.1 ug/kg 09/07/10 20:035.1EPA 8260Percent Moisture 11.9 % 09/02/10 16:570.10ASTM D2974-87

9276750019 SS-109DBeryllium 1.9 mg/kg 09/15/10 16:250.74EPA 6010Chromium 17.6 mg/kg 09/15/10 16:253.7EPA 6010Copper 6.8 mg/kg 09/15/10 16:253.7EPA 6010Lead 6.2 mg/kg 09/15/10 16:253.7EPA 6010Manganese 480 mg/kg 09/15/10 16:253.7EPA 6010Nickel 14.2 mg/kg 09/15/10 16:253.7EPA 6010Zinc 74.5 mg/kg 09/15/10 16:257.4EPA 6010Methylene Chloride 25.8 ug/kg 09/07/10 20:21 C920.1EPA 8260Trichloroethene 9.9 ug/kg 09/07/10 20:215.0EPA 8260Percent Moisture 10.8 % 09/02/10 16:570.10ASTM D2974-87

9276750020 SS-109EBeryllium 0.86 mg/kg 09/15/10 16:280.37EPA 6010Chromium 11.9 mg/kg 09/15/10 16:281.8EPA 6010Copper 3.4 mg/kg 09/15/10 16:281.8EPA 6010Lead 4.2 mg/kg 09/15/10 16:281.8EPA 6010



Page 15 of 242



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(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744



9276750020 SS-109EManganese 552 mg/kg 09/15/10 16:281.8EPA 6010Nickel 6.1 mg/kg 09/15/10 16:281.8EPA 6010Zinc 35.0 mg/kg 09/15/10 16:283.7EPA 6010Methylene Chloride 9.3J ug/kg 09/07/10 20:4017.1EPA 8260Trichloroethene 35.5 ug/kg 09/07/10 20:404.3EPA 8260Percent Moisture 6.9 % 09/02/10 16:570.10ASTM D2974-87

9276750021 SS-104ABeryllium 0.84 mg/kg 09/15/10 16:310.39EPA 6010Chromium 22.5 mg/kg 09/15/10 16:311.9EPA 6010Copper 8.4 mg/kg 09/15/10 16:311.9EPA 6010Lead 9.4 mg/kg 09/15/10 16:311.9EPA 6010Manganese 160 mg/kg 09/15/10 16:311.9EPA 6010Nickel 8.3 mg/kg 09/15/10 16:311.9EPA 6010Selenium 2.0J mg/kg 09/15/10 16:31 D33.9EPA 6010Zinc 36.9 mg/kg 09/15/10 16:313.9EPA 6010Mercury 0.097 mg/kg 09/10/10 12:050.0050EPA 74712,6-Dinitrotoluene 305J ug/kg 09/17/10 02:40398EPA 8270Acetone 24.2J ug/kg 09/08/10 01:53106EPA 8260Methylene Chloride 7.3J ug/kg 09/08/10 01:5321.2EPA 8260Percent Moisture 17.1 % 09/02/10 16:570.10ASTM D2974-87

9276750022 SS-104BArsenic 3.2J mg/kg 09/15/10 16:35 D34.2EPA 6010Beryllium 1.1 mg/kg 09/15/10 16:350.84EPA 6010Chromium 14.9 mg/kg 09/15/10 16:354.2EPA 6010Copper 5.9 mg/kg 09/15/10 16:354.2EPA 6010Manganese 200 mg/kg 09/15/10 16:354.2EPA 6010Nickel 6.9 mg/kg 09/15/10 16:354.2EPA 6010Zinc 46.6 mg/kg 09/15/10 16:358.4EPA 6010Mercury 0.00092J mg/kg 09/07/10 16:560.0040EPA 7471Methylene Chloride 9.6J ug/kg 09/08/10 02:1120.0EPA 8260Percent Moisture 12.9 % 09/02/10 16:570.10ASTM D2974-87

9276750023 SS-104CBeryllium 1.1 mg/kg 09/15/10 16:380.76EPA 6010Chromium 16.0 mg/kg 09/15/10 16:383.8EPA 6010Copper 1.4J mg/kg 09/15/10 16:38 D33.8EPA 6010Lead 3.6J mg/kg 09/15/10 16:38 D33.8EPA 6010Manganese 278 mg/kg 09/15/10 16:383.8EPA 6010Nickel 10.1 mg/kg 09/15/10 16:383.8EPA 6010Zinc 51.7 mg/kg 09/15/10 16:387.6EPA 6010Methylene Chloride 14.8J ug/kg 09/08/10 02:3018.9EPA 8260Trichloroethene 11.4 ug/kg 09/08/10 02:304.7EPA 8260Percent Moisture 8.2 % 09/02/10 16:580.10ASTM D2974-87

9276750024 SS-104DBeryllium 1.3 mg/kg 09/15/10 16:411.2EPA 6010Chromium 13.6 mg/kg 09/15/10 16:415.9EPA 6010



Page 16 of 242



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(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744



9276750024 SS-104DCopper 3.9J mg/kg 09/15/10 16:41 D35.9EPA 6010Manganese 256 mg/kg 09/15/10 16:415.9EPA 6010Nickel 7.6 mg/kg 09/15/10 16:415.9EPA 6010Zinc 45.4 mg/kg 09/15/10 16:4111.7EPA 6010Mercury 0.00015J mg/kg 09/07/10 17:060.0046EPA 7471Methylene Chloride 9.2J ug/kg 09/08/10 02:4818.6EPA 8260Trichloroethene 20.4 ug/kg 09/08/10 02:484.7EPA 8260Percent Moisture 7.4 % 09/02/10 16:580.10ASTM D2974-87

9276750025 SS-104EBeryllium 2.1 mg/kg 09/15/10 16:580.79EPA 6010Chromium 12.9 mg/kg 09/15/10 16:583.9EPA 6010Copper 30.6 mg/kg 09/15/10 16:583.9EPA 6010Lead 6.8 mg/kg 09/15/10 16:583.9EPA 6010Manganese 342 mg/kg 09/15/10 16:583.9EPA 6010Nickel 2.8J mg/kg 09/15/10 16:58 D33.9EPA 6010Zinc 54.3 mg/kg 09/15/10 16:587.9EPA 6010Benzo(g,h,i)perylene 154J ug/kg 09/23/10 20:30405EPA 8270Dibenz(a,h)anthracene 159J ug/kg 09/23/10 20:30405EPA 8270Indeno(1,2,3-cd)pyrene 146J ug/kg 09/23/10 20:30405EPA 8270Methylene Chloride 6.6J ug/kg 09/08/10 03:0720.9EPA 8260Trichloroethene 258 ug/kg 09/08/10 18:4525.5EPA 8260Percent Moisture 18.6 % 09/02/10 16:580.10ASTM D2974-87

9276750026 SS-101ABeryllium 1.7 mg/kg 09/15/10 17:010.59EPA 6010Chromium 23.7 mg/kg 09/15/10 17:013.0EPA 6010Copper 19.6 mg/kg 09/15/10 17:013.0EPA 6010Lead 10.2 mg/kg 09/15/10 17:013.0EPA 6010Manganese 537 mg/kg 09/15/10 17:013.0EPA 6010Nickel 14.0 mg/kg 09/15/10 17:013.0EPA 6010Silver 6.4 mg/kg 09/15/10 17:013.0EPA 6010Zinc 73.7 mg/kg 09/15/10 17:015.9EPA 6010Mercury 0.018 mg/kg 09/10/10 12:080.0045EPA 7471Acetone 109 ug/kg 09/08/10 03:25 C992.5EPA 8260Methylene Chloride 11.3J ug/kg 09/08/10 03:2518.5EPA 8260Trichloroethene 9.7 ug/kg 09/08/10 03:254.6EPA 8260Percent Moisture 6.5 % 09/02/10 16:580.10ASTM D2974-87

9276750027 SS-101BBeryllium 1.5 mg/kg 09/15/10 17:140.90EPA 6010Chromium 19.1 mg/kg 09/15/10 17:144.5EPA 6010Copper 16.0 mg/kg 09/15/10 17:144.5EPA 6010Lead 9.4 mg/kg 09/15/10 17:144.5EPA 6010Manganese 692 mg/kg 09/15/10 17:144.5EPA 6010Nickel 16.8 mg/kg 09/15/10 17:144.5EPA 6010Zinc 48.9 mg/kg 09/15/10 17:149.0EPA 6010Mercury 0.00043J mg/kg 09/07/10 17:30 M10.0044EPA 7471Acetone 44.0J ug/kg 09/08/10 03:4399.7EPA 8260



Page 17 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744



9276750027 SS-101BMethylene Chloride 11.5J ug/kg 09/08/10 03:4319.9EPA 8260Percent Moisture 8.8 % 09/02/10 16:580.10ASTM D2974-87

9276750028 SS-101CBeryllium 4.2 mg/kg 09/15/10 17:242.0EPA 6010Chromium 56.0 mg/kg 09/15/10 17:249.9EPA 6010Copper 36.3 mg/kg 09/15/10 17:249.9EPA 6010Lead 14.0 mg/kg 09/15/10 17:249.9EPA 6010Manganese 371 mg/kg 09/15/10 17:249.9EPA 6010Nickel 30.6 mg/kg 09/15/10 17:249.9EPA 6010Zinc 157 mg/kg 09/15/10 17:2419.9EPA 6010Methylene Chloride 13.6J ug/kg 09/08/10 04:0223.7EPA 8260Percent Moisture 21.3 % 09/02/10 16:580.10ASTM D2974-87

9276750029 SS-101DBeryllium 5.2 mg/kg 09/15/10 17:271.0EPA 6010Chromium 26.0 mg/kg 09/15/10 17:275.1EPA 6010Copper 48.7 mg/kg 09/15/10 17:275.1EPA 6010Lead 8.7 mg/kg 09/15/10 17:275.1EPA 6010Manganese 632 mg/kg 09/15/10 17:275.1EPA 6010Nickel 8.9 mg/kg 09/15/10 17:275.1EPA 6010Zinc 107 mg/kg 09/15/10 17:2710.1EPA 6010Mercury 0.00093J mg/kg 09/07/10 17:510.0047EPA 7471Acetone 30.0J ug/kg 09/08/10 04:20111EPA 8260Methylene Chloride 19.0J ug/kg 09/08/10 04:2022.1EPA 8260Trichloroethene 3.1J ug/kg 09/08/10 04:205.5EPA 8260Percent Moisture 16.4 % 09/02/10 16:590.10ASTM D2974-87

9276750030 FD-06Beryllium 0.33 mg/kg 09/15/10 09:140.095EPA 6010Chromium 3.4 mg/kg 09/15/10 09:140.48EPA 6010Copper 2.8 mg/kg 09/15/10 09:140.48EPA 6010Lead 4.8 mg/kg 09/15/10 09:140.48EPA 6010Manganese 1560 mg/kg 09/16/10 11:534.8EPA 6010Nickel 6.1 mg/kg 09/15/10 09:140.48EPA 6010Thallium 0.48J mg/kg 09/15/10 09:140.95EPA 6010Zinc 17.5 mg/kg 09/15/10 09:140.95EPA 6010Mercury 0.014 mg/kg 09/07/10 17:120.0051EPA 7471Percent Moisture 15.3 % 09/02/10 16:590.10ASTM D2974-87

9276750031 FD-07Acetone 35.2J ug/kg 09/07/10 20:5894.3EPA 8260Methyl acetate 3.5J ug/kg 09/07/10 20:589.4EPA 8260Methylene Chloride 8.7J ug/kg 09/07/10 20:5818.9EPA 8260Percent Moisture 14.1 % 09/02/10 16:590.10ASTM D2974-87




Page 18 of 242



(704)875-9092


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(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744






9276750036 FD-12Acetone 28.1J ug/kg 09/07/10 21:17115EPA 8260Methylene Chloride 7.4J ug/kg 09/07/10 21:1723.0EPA 8260Percent Moisture 18.6 % 09/03/10 11:210.10ASTM D2974-87

9276750037 FD-13Beryllium 1.3 mg/kg 09/15/10 17:310.89EPA 6010Chromium 14.2 mg/kg 09/15/10 17:314.4EPA 6010Copper 7.9 mg/kg 09/15/10 17:314.4EPA 6010Lead 6.4 mg/kg 09/15/10 17:314.4EPA 6010Manganese 834 mg/kg 09/15/10 17:314.4EPA 6010Nickel 9.2 mg/kg 09/15/10 17:314.4EPA 6010Zinc 42.3 mg/kg 09/15/10 17:318.9EPA 6010Mercury 0.00087J mg/kg 09/07/10 17:140.0040EPA 7471Percent Moisture 10.3 % 09/03/10 11:210.10ASTM D2974-87



9276750040 MB-01Beryllium 0.11J ug/L 09/07/10 22:391.0EPA 6010Chromium 0.58J ug/L 09/07/10 22:395.0EPA 6010Copper 2.3J ug/L 09/07/10 22:395.0EPA 6010Manganese 90.6 ug/L 09/07/10 22:39 B5.0EPA 6010Thallium 3.2J ug/L 09/07/10 22:39 L010.0EPA 6010Zinc 116 ug/L 09/07/10 22:39 B10.0EPA 6010Acetone 2.5J ug/L 09/02/10 13:2725.0EPA 8260Carbon disulfide 50.4 ug/L 09/02/10 13:27 C02.0EPA 8260

9276750041 EB-01Beryllium 0.11J ug/L 09/07/10 22:421.0EPA 6010Chromium 1.1J ug/L 09/07/10 22:425.0EPA 6010Copper 0.89J ug/L 09/07/10 22:425.0EPA 6010Manganese 2.0J ug/L 09/07/10 22:425.0EPA 6010Thallium 3.7J ug/L 09/07/10 22:42 L010.0EPA 6010Zinc 24.5 ug/L 09/07/10 22:42 B10.0EPA 6010Methylene Chloride 6.3 ug/L 09/02/10 13:52 C92.0EPA 8260

9276750042 FB-01Methylene Chloride 8.7 ug/L 09/02/10 14:18 C92.0EPA 8260



Page 19 of 242



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(828)254-7176

HITS ONLY


9276750MILLS GAP 6686081744



9276750044 TB-02Acetone 2.5J ug/L 09/02/10 14:4425.0EPA 8260Chloromethane 0.16J ug/L 09/02/10 14:441.0EPA 8260

9276750045 TB-031,4-Dichlorobenzene 3.3J ug/kg 09/08/10 00:585.0EPA 8260



Page 20 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:

Client: Mactec Asheville

EPA 6010

Date: September 27, 2010

Description: 6010 MET ICP

General Information:27 samples were analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.

Hold Time:The samples were analyzed within the method required hold times with any exceptions noted below.

Sample Preparation:The samples were prepared in accordance with EPA 3050 with any exceptions noted below.

Initial Calibrations (including MS Tune as applicable):All criteria were within method requirements with any exceptions noted below.

Continuing Calibration:All criteria were within method requirements with any exceptions noted below.

Method Blank:All analytes were below the report limit in the method blank with any exceptions noted below.

Laboratory Control Spike:All laboratory control spike compounds were within QC limits with any exceptions noted below.

Matrix Spikes:All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.

QC Batch: MPRP/7021A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750003

M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• MS (Lab ID: 493842)

• Antimony• Arsenic• Chromium• Copper• Lead• Manganese• Selenium• Thallium• Zinc

• MSD (Lab ID: 493843)• Antimony• Arsenic• Chromium• Copper• Lead• Manganese



Page 21 of 242



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(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010




M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• Selenium• Thallium• Zinc

R1: RPD value was outside control limits.• MSD (Lab ID: 493843)

• Antimony• Thallium



• Antimony• Arsenic• Chromium• Manganese• Selenium• Zinc

• MSD (Lab ID: 494450)• Antimony• Arsenic• Manganese• Selenium


• Chromium• Manganese• Zinc

Duplicate Sample:All duplicate sample results were within method acceptance criteria with any exceptions noted below.

Additional Comments:Analyte Comments:

QC Batch: MPRP/7021D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.

• FD-02 (Lab ID: 9276750009)• Silver• Arsenic• Beryllium



Page 22 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• FD-02 (Lab ID: 9276750009)• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-109A (Lab ID: 9276750016)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-109B (Lab ID: 9276750017)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-113B (Lab ID: 9276750002)• Silver• Arsenic• Beryllium



Page 23 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-113B (Lab ID: 9276750002)• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-116A (Lab ID: 9276750003)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-116B (Lab ID: 9276750004)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc



Page 24 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• FD-13 (Lab ID: 9276750037)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-101A (Lab ID: 9276750026)• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-101B (Lab ID: 9276750027)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-101C (Lab ID: 9276750028)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-101D (Lab ID: 9276750029)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-104A (Lab ID: 9276750021)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-104B (Lab ID: 9276750022)• Silver



Page 25 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-104B (Lab ID: 9276750022)• Arsenic• Cadmium• Lead• Antimony• Selenium• Thallium

• SS-104C (Lab ID: 9276750023)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-104D (Lab ID: 9276750024)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-104E (Lab ID: 9276750025)• Silver• Arsenic• Cadmium• Nickel• Antimony• Selenium• Thallium

• SS-109C (Lab ID: 9276750018)• Silver• Arsenic• Cadmium• Lead• Antimony• Selenium• Thallium

• SS-109D (Lab ID: 9276750019)• Silver



Page 26 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-109D (Lab ID: 9276750019)• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-109E (Lab ID: 9276750020)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium



Page 27 of 242



(704)875-9092


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(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 6010


Description: 6010 MET ICP, 3030C



Sample Preparation:The samples were prepared in accordance with SM 3030C with any exceptions noted below.




QC Batch: MPRP/6996B: Analyte was detected in the associated method blank.

• BLANK (Lab ID: 492105)• Chromium• Copper• Lead• Manganese• Nickel• Zinc


QC Batch: MPRP/6996L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.

• LCS (Lab ID: 492106)• Thallium



Additional Comments:



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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 7470


Description: 7470 Mercury









QC Batch: MERP/3001A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276573001,9276750040

M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• MS (Lab ID: 494035)

• Mercury• MSD (Lab ID: 494036)

• Mercury





Page 29 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 7471














• Mercury


M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• MSD (Lab ID: 491980)

• Mercury






Page 30 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 7471




M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• Mercury





Page 31 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Microwave






Internal Standards:All internal standards were within QC limits with any exceptions noted below.

Surrogates:All surrogates were within QC limits with any exceptions noted below.

QC Batch: OEXT/11121S0: Surrogate recovery outside laboratory control limits.

• SS-109E (Lab ID: 9276750020)• Phenol-d6 (S)



QC Batch: OEXT/11113L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samplesmay be biased high.

• LCS (Lab ID: 494758)• 2,3,4,6-Tetrachlorophenol• bis(2-Ethylhexyl)phthalate

L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samplesmay be biased low.

• LCS (Lab ID: 494758)• Benzaldehyde



Page 32 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270



QC Batch: OEXT/11121L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samplesmay be biased low.

• LCS (Lab ID: 495531)• Atrazine• Benzaldehyde

L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.


QC Batch: OEXT/11146L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samplesmay be biased low.

• LCS (Lab ID: 496477)• Acetophenone• Benzaldehyde




QC Batch: OEXT/11113A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750005


• Acetophenone• Benzaldehyde• bis(2-Ethylhexyl)phthalate

• MSD (Lab ID: 494760)• Acetophenone• Benzaldehyde• bis(2-Ethylhexyl)phthalate


• Acetophenone• Benzaldehyde

• MSD (Lab ID: 494760)• Acetophenone• Benzaldehyde



Page 33 of 242



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PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270





• Hexachlorocyclopentadiene



• 2-Nitrophenol• Acetophenone• Atrazine• Benzaldehyde• Biphenyl (Diphenyl)• Caprolactam• Carbazole

• MSD (Lab ID: 495533)• Acetophenone• Caprolactam• Carbazole• bis(2-Ethylhexyl)phthalate


• 2-Nitrophenol• Acetophenone• Biphenyl (Diphenyl)• Caprolactam• Carbazole

• MSD (Lab ID: 495533)• Acetophenone• Caprolactam• Carbazole


• 1,2,4,5-Tetrachlorobenzene• 2,3,4,6-Tetrachlorophenol• 2,4,5-Trichlorophenol• 2,4,6-Trichlorophenol• 2,4-Dichlorophenol• 2,4-Dinitrotoluene• 2,6-Dinitrotoluene• 2-Chloronaphthalene• 2-Chlorophenol• 2-Methylnaphthalene



Page 34 of 242



(704)875-9092


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(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270




R1: RPD value was outside control limits.• 2-Methylphenol(o-Cresol)• 2-Nitrophenol• 3&4-Methylphenol(m&p Cresol)• 4-Bromophenylphenyl ether• 4-Chlorophenylphenyl ether• Acenaphthene• Acenaphthylene• Acetophenone• Atrazine• Benzaldehyde• Benzo(a)anthracene• Benzo(a)pyrene• Benzo(b)fluoranthene• Benzo(g,h,i)perylene• Benzo(k)fluoranthene• Biphenyl (Diphenyl)• Carbazole• Chrysene• Dibenz(a,h)anthracene• Dibenzofuran• Hexachloro-1,3-butadiene• Hexachlorobenzene• Hexachlorocyclopentadiene• Hexachloroethane• Indeno(1,2,3-cd)pyrene• N-Nitroso-di-n-propylamine• N-Nitrosodiphenylamine• Naphthalene• Nitrobenzene• Pentachlorophenol• Phenanthrene• Phenol• Pyrene• bis(2-Chloroethoxy)methane• bis(2-Chloroethyl) ether• bis(2-Chloroisopropyl) ether• bis(2-Ethylhexyl)phthalate



• Benzaldehyde



Page 35 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270




M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• Caprolactam


• CaprolactamR1: RPD value was outside control limits.

• MSD (Lab ID: 496479)• Atrazine• Caprolactam• Di-n-octylphthalate• Hexachlorocyclopentadiene• bis(2-Ethylhexyl)phthalate



QC Batch: OEXT/11113

• MSD (Lab ID: 494760)• bis(2-Ethylhexyl)phthalate



Page 36 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Semivolatile Organic










QC Batch: OEXT/11089L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

• LCS (Lab ID: 494099)• 2,3,4,6-Tetrachlorophenol• Atrazine




• 1,2,4,5-Tetrachlorobenzene• Acetophenone• Benzaldehyde



Page 37 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Semivolatile Organic


M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• Biphenyl (Diphenyl)• Caprolactam• Isophorone

• MSD (Lab ID: 494101)• 1,2,4,5-Tetrachlorobenzene• 2,3,4,6-Tetrachlorophenol• Benzaldehyde• Caprolactam• Isophorone


• 1,2,4,5-Tetrachlorobenzene• Acetophenone• Benzaldehyde• Biphenyl (Diphenyl)• Caprolactam• Isophorone

• MSD (Lab ID: 494101)• 1,2,4,5-Tetrachlorobenzene• 2,3,4,6-Tetrachlorophenol• Benzaldehyde• Caprolactam• Isophorone





Page 38 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260 MSV Low Level









QC Batch: MSV/12105L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

• LCS (Lab ID: 492193)• Benzene




QC Batch: MSV/12105C0: Result confirmed by second analysis.

• MB-01 (Lab ID: 9276750040)• Carbon disulfide



Page 39 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260 MSV Low Level

Analyte Comments:

QC Batch: MSV/12105C9: Common Laboratory Contaminant.

• EB-01 (Lab ID: 9276750041)• Methylene Chloride

• FB-01 (Lab ID: 9276750042)• Methylene Chloride



Page 40 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260/5035A Volatile Organics









QC Batch: MSV/12138L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

• LCS (Lab ID: 493754)• 1,1,2-Trichlorotrifluoroethane• Bromomethane• Carbon disulfide• Chloroform• Chloromethane

QC Batch: MSV/12151L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.

• LCS (Lab ID: 493934)• Methyl acetate


• LCS (Lab ID: 493934)• Bromomethane




Page 41 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260/5035A Volatile Organics

QC Batch: MSV/12135A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750007


• Benzene• Chlorobenzene• Toluene• Trichloroethene

QC Batch: MSV/12151A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750025


• Trichloroethene




• SS-109A (Lab ID: 9276750016)• Acetone

• SS-109C (Lab ID: 9276750018)• Methylene Chloride

• SS-109D (Lab ID: 9276750019)• Methylene Chloride

E: Analyte concentration exceeded the calibration range. The reported result is estimated.• SS-116A (Lab ID: 9276750003)

• Acetone


• SS-101A (Lab ID: 9276750026)• Acetone



Page 42 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


SM 4500-CN-E


Description: 4500CNE Cyanide, Total

General Information:27 samples were analyzed for SM 4500-CN-E. All samples were received in acceptable condition with any exceptions noted below.









General Information:2 samples were analyzed for SM 4500-CN-E. All samples were received in acceptable condition with any exceptions noted below.








Page 43 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


SM 4500-CN-E


Description: 4500CNE Cyanide, Total






Page 44 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 7196


Description: 7196 Chromium, Hexavalent









QC Batch: WETA/8087A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276756001,9276756003


• Chromium, Hexavalent• MS (Lab ID: 492158)

• Chromium, Hexavalent









Page 45 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276750MILLS GAP 6686081744

Method:


EPA 7196


Description: 7196 Chromium, Hexavalent



This data package has been reviewed for quality and completeness and is approved for release.



Page 46 of 242



(704)875-9092


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ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: SS-113A Lab ID: 9276750001 Collected: 08/30/10 14:35 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimitReport

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050

Antimony ND mg/kg 1 09/10/10 14:47 7440-36-009/07/10 15:200.39 0.22Arsenic 0.34J mg/kg 1 09/10/10 14:47 7440-38-209/07/10 15:200.39 0.25Beryllium 0.35 mg/kg 1 09/10/10 14:47 7440-41-709/07/10 15:200.077 0.015Cadmium ND mg/kg 1 09/10/10 14:47 7440-43-909/07/10 15:200.077 0.046Chromium 2.4 mg/kg 1 09/10/10 14:47 7440-47-309/07/10 15:200.39 0.023Copper 5.1 mg/kg 1 09/10/10 14:47 7440-50-809/07/10 15:200.39 0.031Lead 5.3 mg/kg 1 09/10/10 14:47 7439-92-109/07/10 15:200.39 0.37Manganese 290 mg/kg 1 09/10/10 14:47 7439-96-509/07/10 15:200.39 0.023Nickel 3.6 mg/kg 1 09/10/10 14:47 7440-02-009/07/10 15:200.39 0.14Selenium ND mg/kg 1 09/10/10 14:47 7782-49-209/07/10 15:200.77 0.29Silver ND mg/kg 1 09/10/10 14:47 7440-22-409/07/10 15:200.39 0.023Thallium ND mg/kg 1 09/10/10 14:47 7440-28-009/07/10 15:200.77 0.20Zinc 6.1 mg/kg 1 09/10/10 14:47 7440-66-609/07/10 15:200.77 0.20

7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471

Mercury 0.011 mg/kg 1 09/03/10 18:00 7439-97-609/01/10 02:500.0038 0.000076

8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546

Acenaphthene ND ug/kg 1 09/10/10 11:38 83-32-909/09/10 00:00341 78.6Acenaphthylene ND ug/kg 1 09/10/10 11:38 208-96-809/09/10 00:00341 80.7Acetophenone ND ug/kg 1 09/10/10 11:38 98-86-209/09/10 00:00341 176Anthracene ND ug/kg 1 09/10/10 11:38 120-12-709/09/10 00:00341 76.6Atrazine ND ug/kg 1 09/10/10 11:38 1912-24-909/09/10 00:00683 134Benzaldehyde ND ug/kg 1 09/10/10 11:38 100-52-709/09/10 00:00683 341Benzo(a)anthracene ND ug/kg 1 09/10/10 11:38 56-55-309/09/10 00:00341 63.1Benzo(a)pyrene ND ug/kg 1 09/10/10 11:38 50-32-809/09/10 00:00341 65.2Benzo(b)fluoranthene ND ug/kg 1 09/10/10 11:38 205-99-209/09/10 00:00341 59.0Benzo(g,h,i)perylene ND ug/kg 1 09/10/10 11:38 191-24-209/09/10 00:00341 86.9Benzo(k)fluoranthene ND ug/kg 1 09/10/10 11:38 207-08-909/09/10 00:00341 67.2Biphenyl (Diphenyl) ND ug/kg 1 09/10/10 11:38 92-52-409/09/10 00:00341 1084-Bromophenylphenyl ether ND ug/kg 1 09/10/10 11:38 101-55-309/09/10 00:00341 62.1Butylbenzylphthalate ND ug/kg 1 09/10/10 11:38 85-68-709/09/10 00:00341 72.4Caprolactam ND ug/kg 1 09/10/10 11:38 105-60-209/09/10 00:00341 59.0Carbazole ND ug/kg 1 09/10/10 11:38 86-74-809/09/10 00:00341 65.24-Chloro-3-methylphenol ND ug/kg 1 09/10/10 11:38 59-50-709/09/10 00:00683 70.34-Chloroaniline ND ug/kg 1 09/10/10 11:38 106-47-809/09/10 00:001710 95.2bis(2-Chloroethoxy)methane ND ug/kg 1 09/10/10 11:38 111-91-109/09/10 00:00341 79.7bis(2-Chloroethyl) ether ND ug/kg 1 09/10/10 11:38 111-44-409/09/10 00:00341 86.9bis(2-Chloroisopropyl) ether ND ug/kg 1 09/10/10 11:38 108-60-109/09/10 00:00341 91.02-Chloronaphthalene ND ug/kg 1 09/10/10 11:38 91-58-709/09/10 00:00341 67.22-Chlorophenol ND ug/kg 1 09/10/10 11:38 95-57-809/09/10 00:00341 93.14-Chlorophenylphenyl ether ND ug/kg 1 09/10/10 11:38 7005-72-309/09/10 00:00341 70.3Chrysene ND ug/kg 1 09/10/10 11:38 218-01-909/09/10 00:00341 45.5Dibenz(a,h)anthracene ND ug/kg 1 09/10/10 11:38 53-70-309/09/10 00:00341 72.4Dibenzofuran ND ug/kg 1 09/10/10 11:38 132-64-909/09/10 00:00341 55.9



Date: 09/27/2010 06:23 PM Page 47 of 242



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ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/10/10 11:38 91-94-109/09/10 00:001710 74.52,4-Dichlorophenol ND ug/kg 1 09/10/10 11:38 120-83-209/09/10 00:00341 74.5Diethylphthalate ND ug/kg 1 09/10/10 11:38 84-66-209/09/10 00:00341 52.82,4-Dimethylphenol ND ug/kg 1 09/10/10 11:38 105-67-909/09/10 00:00341 134Dimethylphthalate ND ug/kg 1 09/10/10 11:38 131-11-309/09/10 00:00341 69.3Di-n-butylphthalate ND ug/kg 1 09/10/10 11:38 84-74-209/09/10 00:00341 55.94,6-Dinitro-2-methylphenol ND ug/kg 1 09/10/10 11:38 534-52-109/09/10 00:00683 68.32,4-Dinitrophenol ND ug/kg 1 09/10/10 11:38 51-28-509/09/10 00:001710 55.92,4-Dinitrotoluene ND ug/kg 1 09/10/10 11:38 121-14-209/09/10 00:00341 64.12,6-Dinitrotoluene ND ug/kg 1 09/10/10 11:38 606-20-209/09/10 00:00341 71.4Di-n-octylphthalate ND ug/kg 1 09/10/10 11:38 117-84-009/09/10 00:00341 71.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/10/10 11:38 117-81-709/09/10 00:00341 93.1Fluoranthene ND ug/kg 1 09/10/10 11:38 206-44-009/09/10 00:00341 49.7Fluorene ND ug/kg 1 09/10/10 11:38 86-73-709/09/10 00:00341 70.3Hexachloro-1,3-butadiene ND ug/kg 1 09/10/10 11:38 87-68-309/09/10 00:00341 59.0Hexachlorobenzene ND ug/kg 1 09/10/10 11:38 118-74-109/09/10 00:00341 43.4Hexachlorocyclopentadiene ND ug/kg 1 09/10/10 11:38 77-47-409/09/10 00:00341 63.1Hexachloroethane ND ug/kg 1 09/10/10 11:38 67-72-109/09/10 00:00341 90.0Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/10/10 11:38 193-39-509/09/10 00:00341 70.3Isophorone ND ug/kg 1 09/10/10 11:38 78-59-109/09/10 00:00341 76.62-Methylnaphthalene ND ug/kg 1 09/10/10 11:38 91-57-609/09/10 00:00341 73.42-Methylphenol(o-Cresol) ND ug/kg 1 09/10/10 11:38 95-48-709/09/10 00:00341 1033&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/10/10 11:3809/09/10 00:00341 134Naphthalene ND ug/kg 1 09/10/10 11:38 91-20-309/09/10 00:00341 83.82-Nitroaniline ND ug/kg 1 09/10/10 11:38 88-74-409/09/10 00:001710 1063-Nitroaniline ND ug/kg 1 09/10/10 11:38 99-09-209/09/10 00:001710 93.14-Nitroaniline ND ug/kg 1 09/10/10 11:38 100-01-609/09/10 00:00683 96.2Nitrobenzene ND ug/kg 1 09/10/10 11:38 98-95-309/09/10 00:00341 93.12-Nitrophenol ND ug/kg 1 09/10/10 11:38 88-75-509/09/10 00:00341 82.84-Nitrophenol ND ug/kg 1 09/10/10 11:38 100-02-709/09/10 00:001710 61.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/10/10 11:38 621-64-709/09/10 00:00341 65.2N-Nitrosodiphenylamine ND ug/kg 1 09/10/10 11:38 86-30-609/09/10 00:00341 101Pentachlorophenol ND ug/kg 1 09/10/10 11:38 87-86-509/09/10 00:001710 62.1Phenanthrene ND ug/kg 1 09/10/10 11:38 85-01-809/09/10 00:00341 56.9Phenol ND ug/kg 1 09/10/10 11:38 108-95-209/09/10 00:00341 102Pyrene ND ug/kg 1 09/10/10 11:38 129-00-009/09/10 00:00341 57.91,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/10/10 11:38 95-94-309/09/10 00:00341 1242,3,4,6-Tetrachlorophenol ND ug/kg 1 09/10/10 11:38 58-90-209/09/10 00:00341 1342,4,5-Trichlorophenol ND ug/kg 1 09/10/10 11:38 95-95-409/09/10 00:00341 1062,4,6-Trichlorophenol ND ug/kg 1 09/10/10 11:38 88-06-209/09/10 00:00341 75.52-Fluorobiphenyl (S) 37 % 1 09/10/10 11:38 321-60-809/09/10 00:0030-110Terphenyl-d14 (S) 57 % 1 09/10/10 11:38 1718-51-009/09/10 00:0028-110Phenol-d6 (S) 38 % 1 09/10/10 11:38 13127-88-309/09/10 00:0022-1102-Fluorophenol (S) 35 % 1 09/10/10 11:38 367-12-409/09/10 00:0013-1102,4,6-Tribromophenol (S) 40 % 1 09/10/10 11:38 118-79-609/09/10 00:0027-110



Date: 09/27/2010 06:23 PM Page 48 of 242



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ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 36 % 1 09/10/10 11:38 4165-60-009/09/10 00:0023-110

8260/5035A Volatile Organics Analytical Method: EPA 8260

Acetone 13.5J ug/kg 1 09/05/10 15:22 67-64-196.5 9.7Benzene ND ug/kg 1 09/05/10 15:22 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/05/10 15:22 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/05/10 15:22 75-27-44.8 1.8Bromoform ND ug/kg 1 09/05/10 15:22 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/05/10 15:22 74-83-99.7 2.42-Butanone (MEK) ND ug/kg 1 09/05/10 15:22 78-93-396.5 2.8Carbon disulfide ND ug/kg 1 09/05/10 15:22 75-15-09.7 2.9Carbon tetrachloride ND ug/kg 1 09/05/10 15:22 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/05/10 15:22 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/05/10 15:22 75-00-39.7 2.3Chloroform ND ug/kg 1 09/05/10 15:22 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/05/10 15:22 74-87-39.7 2.3Cyclohexane ND ug/kg 1 09/05/10 15:22 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/05/10 15:22 96-12-84.8 3.5Dibromochloromethane ND ug/kg 1 09/05/10 15:22 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/05/10 15:22 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/05/10 15:22 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/05/10 15:22 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/05/10 15:22 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/05/10 15:22 75-71-89.7 3.51,1-Dichloroethane ND ug/kg 1 09/05/10 15:22 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/05/10 15:22 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/05/10 15:22 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/05/10 15:22 156-59-24.8 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/05/10 15:22 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/05/10 15:22 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/05/10 15:22 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/05/10 15:22 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/05/10 15:22 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/05/10 15:22 591-78-648.3 3.8Isopropylbenzene (Cumene) ND ug/kg 1 09/05/10 15:22 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/05/10 15:22 79-20-99.7 1.4Methylcyclohexane ND ug/kg 1 09/05/10 15:22 108-87-29.7 1.4Methylene Chloride ND ug/kg 1 09/05/10 15:22 75-09-219.3 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/05/10 15:22 108-10-148.3 3.6Methyl-tert-butyl ether ND ug/kg 1 09/05/10 15:22 1634-04-44.8 1.4Styrene ND ug/kg 1 09/05/10 15:22 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/05/10 15:22 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/05/10 15:22 127-18-44.8 1.6Toluene ND ug/kg 1 09/05/10 15:22 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/05/10 15:22 87-61-64.8 2.1



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(828)254-7176

ANALYTICAL RESULTS


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1,2,4-Trichlorobenzene ND ug/kg 1 09/05/10 15:22 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/05/10 15:22 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/05/10 15:22 79-00-54.8 2.0Trichloroethene ND ug/kg 1 09/05/10 15:22 79-01-64.8 2.0Trichlorofluoromethane ND ug/kg 1 09/05/10 15:22 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/05/10 15:22 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/05/10 15:22 75-01-49.7 1.7Xylene (Total) ND ug/kg 1 09/05/10 15:22 1330-20-79.7 3.5m&p-Xylene ND ug/kg 1 09/05/10 15:22 179601-23-19.7 3.5o-Xylene ND ug/kg 1 09/05/10 15:22 95-47-64.8 1.8Dibromofluoromethane (S) 99 % 1 09/05/10 15:22 1868-53-770-130Toluene-d8 (S) 99 % 1 09/05/10 15:22 2037-26-570-1304-Bromofluorobenzene (S) 97 % 1 09/05/10 15:22 460-00-470-1301,2-Dichloroethane-d4 (S) 105 % 1 09/05/10 15:22 17060-07-070-132

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 3.3 % 1 09/02/10 17:170.10 0.10

4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E

Cyanide ND mg/kg 1 09/05/10 13:27 57-12-50.21 0.21

7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196

Chromium, Hexavalent ND mg/kg 1 09/02/10 15:49 18540-29-909/02/10 14:522.1 2.1



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Sample: SS-113B Lab ID: 9276750002 Collected: 08/30/10 14:40 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis



Antimony ND mg/kg 20 09/13/10 16:10 7440-36-0 D309/07/10 15:207.6 4.2Arsenic 7.2J mg/kg 20 09/13/10 16:10 7440-38-2 D309/07/10 15:207.6 4.8Beryllium 2.6 mg/kg 20 09/13/10 16:10 7440-41-7 D309/07/10 15:201.5 0.30Cadmium ND mg/kg 20 09/13/10 16:10 7440-43-9 D309/07/10 15:201.5 0.91Chromium 35.1 mg/kg 20 09/13/10 16:10 7440-47-3 D309/07/10 15:207.6 0.45Copper 21.5 mg/kg 20 09/13/10 16:10 7440-50-8 D309/07/10 15:207.6 0.60Lead 15.7 mg/kg 20 09/13/10 16:10 7439-92-1 D309/07/10 15:207.6 7.3Manganese 514 mg/kg 20 09/13/10 16:10 7439-96-5 D309/07/10 15:207.6 0.45Nickel 25.4 mg/kg 20 09/13/10 16:10 7440-02-0 D309/07/10 15:207.6 2.7Selenium ND mg/kg 20 09/13/10 16:10 7782-49-2 D309/07/10 15:2015.1 5.7Silver ND mg/kg 20 09/13/10 16:10 7440-22-4 D309/07/10 15:207.6 0.45Thallium ND mg/kg 20 09/13/10 16:10 7440-28-0 D309/07/10 15:2015.1 3.9Zinc 120 mg/kg 20 09/13/10 16:10 7440-66-6 D309/07/10 15:2015.1 3.9


Mercury 0.00050J mg/kg 1 09/03/10 18:03 7439-97-609/01/10 02:500.0047 0.000094


Acenaphthene ND ug/kg 1 09/12/10 19:42 83-32-909/09/10 00:00394 90.8Acenaphthylene ND ug/kg 1 09/12/10 19:42 208-96-809/09/10 00:00394 93.2Acetophenone ND ug/kg 1 09/12/10 19:42 98-86-209/09/10 00:00394 203Anthracene ND ug/kg 1 09/12/10 19:42 120-12-709/09/10 00:00394 88.4Atrazine ND ug/kg 1 09/10/10 12:13 1912-24-909/09/10 00:00788 155Benzaldehyde ND ug/kg 1 09/10/10 12:13 100-52-709/09/10 00:00788 394Benzo(a)anthracene ND ug/kg 1 09/12/10 19:42 56-55-309/09/10 00:00394 72.9Benzo(a)pyrene ND ug/kg 1 09/12/10 19:42 50-32-809/09/10 00:00394 75.2Benzo(b)fluoranthene ND ug/kg 1 09/12/10 19:42 205-99-209/09/10 00:00394 68.1Benzo(g,h,i)perylene ND ug/kg 1 09/12/10 19:42 191-24-209/09/10 00:00394 100Benzo(k)fluoranthene ND ug/kg 1 09/12/10 19:42 207-08-909/09/10 00:00394 77.6Biphenyl (Diphenyl) ND ug/kg 1 09/12/10 19:42 92-52-409/09/10 00:00394 1244-Bromophenylphenyl ether ND ug/kg 1 09/12/10 19:42 101-55-309/09/10 00:00394 71.7Butylbenzylphthalate ND ug/kg 1 09/12/10 19:42 85-68-709/09/10 00:00394 83.6Caprolactam ND ug/kg 1 09/10/10 12:13 105-60-209/09/10 00:00394 68.1Carbazole ND ug/kg 1 09/12/10 19:42 86-74-809/09/10 00:00394 75.24-Chloro-3-methylphenol ND ug/kg 1 09/12/10 19:42 59-50-709/09/10 00:00788 81.24-Chloroaniline ND ug/kg 1 09/12/10 19:42 106-47-809/09/10 00:001970 110bis(2-Chloroethoxy)methane ND ug/kg 1 09/12/10 19:42 111-91-109/09/10 00:00394 92.0bis(2-Chloroethyl) ether ND ug/kg 1 09/12/10 19:42 111-44-409/09/10 00:00394 100bis(2-Chloroisopropyl) ether ND ug/kg 1 09/12/10 19:42 108-60-109/09/10 00:00394 1052-Chloronaphthalene ND ug/kg 1 09/12/10 19:42 91-58-709/09/10 00:00394 77.62-Chlorophenol ND ug/kg 1 09/12/10 19:42 95-57-809/09/10 00:00394 1074-Chlorophenylphenyl ether ND ug/kg 1 09/12/10 19:42 7005-72-309/09/10 00:00394 81.2Chrysene ND ug/kg 1 09/12/10 19:42 218-01-909/09/10 00:00394 52.5Dibenz(a,h)anthracene ND ug/kg 1 09/12/10 19:42 53-70-309/09/10 00:00394 83.6Dibenzofuran ND ug/kg 1 09/12/10 19:42 132-64-909/09/10 00:00394 64.5



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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/12/10 19:42 91-94-109/09/10 00:001970 86.02,4-Dichlorophenol ND ug/kg 1 09/12/10 19:42 120-83-209/09/10 00:00394 86.0Diethylphthalate ND ug/kg 1 09/12/10 19:42 84-66-209/09/10 00:00394 60.92,4-Dimethylphenol ND ug/kg 1 09/12/10 19:42 105-67-909/09/10 00:00394 155Dimethylphthalate ND ug/kg 1 09/12/10 19:42 131-11-309/09/10 00:00394 80.0Di-n-butylphthalate ND ug/kg 1 09/12/10 19:42 84-74-209/09/10 00:00394 64.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/12/10 19:42 534-52-109/09/10 00:00788 78.82,4-Dinitrophenol ND ug/kg 1 09/12/10 19:42 51-28-509/09/10 00:001970 64.52,4-Dinitrotoluene ND ug/kg 1 09/12/10 19:42 121-14-209/09/10 00:00394 74.02,6-Dinitrotoluene ND ug/kg 1 09/12/10 19:42 606-20-209/09/10 00:00394 82.4Di-n-octylphthalate ND ug/kg 1 09/12/10 19:42 117-84-009/09/10 00:00394 82.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/12/10 19:42 117-81-709/09/10 00:00394 107Fluoranthene ND ug/kg 1 09/12/10 19:42 206-44-009/09/10 00:00394 57.3Fluorene ND ug/kg 1 09/12/10 19:42 86-73-709/09/10 00:00394 81.2Hexachloro-1,3-butadiene ND ug/kg 1 09/12/10 19:42 87-68-309/09/10 00:00394 68.1Hexachlorobenzene ND ug/kg 1 09/12/10 19:42 118-74-109/09/10 00:00394 50.2Hexachlorocyclopentadiene ND ug/kg 1 09/12/10 19:42 77-47-409/09/10 00:00394 72.9Hexachloroethane ND ug/kg 1 09/12/10 19:42 67-72-109/09/10 00:00394 104Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/12/10 19:42 193-39-509/09/10 00:00394 81.2Isophorone ND ug/kg 1 09/12/10 19:42 78-59-109/09/10 00:00394 88.42-Methylnaphthalene ND ug/kg 1 09/12/10 19:42 91-57-609/09/10 00:00394 84.82-Methylphenol(o-Cresol) ND ug/kg 1 09/12/10 19:42 95-48-709/09/10 00:00394 1193&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/12/10 19:4209/09/10 00:00394 155Naphthalene ND ug/kg 1 09/12/10 19:42 91-20-309/09/10 00:00394 96.72-Nitroaniline ND ug/kg 1 09/12/10 19:42 88-74-409/09/10 00:001970 1223-Nitroaniline ND ug/kg 1 09/12/10 19:42 99-09-209/09/10 00:001970 1074-Nitroaniline ND ug/kg 1 09/12/10 19:42 100-01-609/09/10 00:00788 111Nitrobenzene ND ug/kg 1 09/12/10 19:42 98-95-309/09/10 00:00394 1072-Nitrophenol ND ug/kg 1 09/12/10 19:42 88-75-509/09/10 00:00394 95.54-Nitrophenol ND ug/kg 1 09/12/10 19:42 100-02-709/09/10 00:001970 70.5N-Nitroso-di-n-propylamine ND ug/kg 1 09/12/10 19:42 621-64-709/09/10 00:00394 75.2N-Nitrosodiphenylamine ND ug/kg 1 09/12/10 19:42 86-30-609/09/10 00:00394 117Pentachlorophenol ND ug/kg 1 09/12/10 19:42 87-86-509/09/10 00:001970 71.7Phenanthrene ND ug/kg 1 09/12/10 19:42 85-01-809/09/10 00:00394 65.7Phenol ND ug/kg 1 09/12/10 19:42 108-95-209/09/10 00:00394 118Pyrene ND ug/kg 1 09/12/10 19:42 129-00-009/09/10 00:00394 66.91,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/10/10 12:13 95-94-309/09/10 00:00394 1432,3,4,6-Tetrachlorophenol ND ug/kg 1 09/12/10 19:42 58-90-209/09/10 00:00394 1552,4,5-Trichlorophenol ND ug/kg 1 09/12/10 19:42 95-95-409/09/10 00:00394 1222,4,6-Trichlorophenol ND ug/kg 1 09/12/10 19:42 88-06-209/09/10 00:00394 87.22-Fluorobiphenyl (S) 46 % 1 09/12/10 19:42 321-60-809/09/10 00:0030-110Terphenyl-d14 (S) 51 % 1 09/12/10 19:42 1718-51-009/09/10 00:0028-110Phenol-d6 (S) 46 % 1 09/12/10 19:42 13127-88-309/09/10 00:0022-1102-Fluorophenol (S) 45 % 1 09/12/10 19:42 367-12-409/09/10 00:0013-1102,4,6-Tribromophenol (S) 46 % 1 09/12/10 19:42 118-79-609/09/10 00:0027-110



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 47 % 1 09/12/10 19:42 4165-60-009/09/10 00:0023-110


Acetone ND ug/kg 1 09/05/10 15:40 67-64-1103 10.3Benzene ND ug/kg 1 09/05/10 15:40 71-43-25.1 1.6Bromochloromethane ND ug/kg 1 09/05/10 15:40 74-97-55.1 1.7Bromodichloromethane ND ug/kg 1 09/05/10 15:40 75-27-45.1 1.9Bromoform ND ug/kg 1 09/05/10 15:40 75-25-25.1 2.4Bromomethane ND ug/kg 1 09/05/10 15:40 74-83-910.3 2.62-Butanone (MEK) ND ug/kg 1 09/05/10 15:40 78-93-3103 3.0Carbon disulfide ND ug/kg 1 09/05/10 15:40 75-15-010.3 3.1Carbon tetrachloride ND ug/kg 1 09/05/10 15:40 56-23-55.1 2.7Chlorobenzene ND ug/kg 1 09/05/10 15:40 108-90-75.1 1.9Chloroethane ND ug/kg 1 09/05/10 15:40 75-00-310.3 2.5Chloroform ND ug/kg 1 09/05/10 15:40 67-66-35.1 1.6Chloromethane ND ug/kg 1 09/05/10 15:40 74-87-310.3 2.5Cyclohexane ND ug/kg 1 09/05/10 15:40 110-82-75.1 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/05/10 15:40 96-12-85.1 3.7Dibromochloromethane ND ug/kg 1 09/05/10 15:40 124-48-15.1 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/05/10 15:40 106-93-45.1 1.81,2-Dichlorobenzene ND ug/kg 1 09/05/10 15:40 95-50-15.1 1.91,3-Dichlorobenzene ND ug/kg 1 09/05/10 15:40 541-73-15.1 2.11,4-Dichlorobenzene ND ug/kg 1 09/05/10 15:40 106-46-75.1 1.7Dichlorodifluoromethane ND ug/kg 1 09/05/10 15:40 75-71-810.3 3.71,1-Dichloroethane ND ug/kg 1 09/05/10 15:40 75-34-35.1 1.51,2-Dichloroethane ND ug/kg 1 09/05/10 15:40 107-06-25.1 2.31,1-Dichloroethene ND ug/kg 1 09/05/10 15:40 75-35-45.1 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/05/10 15:40 156-59-25.1 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/05/10 15:40 156-60-55.1 1.91,2-Dichloropropane ND ug/kg 1 09/05/10 15:40 78-87-55.1 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/05/10 15:40 10061-01-55.1 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/05/10 15:40 10061-02-65.1 1.5Ethylbenzene ND ug/kg 1 09/05/10 15:40 100-41-45.1 1.82-Hexanone ND ug/kg 1 09/05/10 15:40 591-78-651.3 4.0Isopropylbenzene (Cumene) ND ug/kg 1 09/05/10 15:40 98-82-85.1 1.9Methyl acetate ND ug/kg 1 09/05/10 15:40 79-20-910.3 1.4Methylcyclohexane ND ug/kg 1 09/05/10 15:40 108-87-210.3 1.5Methylene Chloride 5.2J ug/kg 1 09/05/10 15:40 75-09-220.5 3.14-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/05/10 15:40 108-10-151.3 3.8Methyl-tert-butyl ether ND ug/kg 1 09/05/10 15:40 1634-04-45.1 1.5Styrene ND ug/kg 1 09/05/10 15:40 100-42-55.1 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/05/10 15:40 79-34-55.1 1.9Tetrachloroethene ND ug/kg 1 09/05/10 15:40 127-18-45.1 1.7Toluene ND ug/kg 1 09/05/10 15:40 108-88-35.1 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/05/10 15:40 87-61-65.1 2.3



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Cyanide ND mg/kg 1 09/05/10 13:28 57-12-50.24 0.24





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 50 09/13/10 16:39 7440-36-0 D309/07/10 15:2017.1 9.6Arsenic ND mg/kg 50 09/13/10 16:39 7440-38-2 D309/07/10 15:2017.1 10.9Beryllium 5.1 mg/kg 50 09/13/10 16:39 7440-41-7 D309/07/10 15:203.4 0.68Cadmium ND mg/kg 50 09/13/10 16:39 7440-43-9 D309/07/10 15:203.4 2.0Chromium 35.8 mg/kg 50 09/13/10 16:39 7440-47-3 D309/07/10 15:2017.1 1.0Copper 51.6 mg/kg 50 09/13/10 16:39 7440-50-8 D309/07/10 15:2017.1 1.4Lead 17.8 mg/kg 50 09/13/10 16:39 7439-92-1 D309/07/10 15:2017.1 16.4Manganese 833 mg/kg 50 09/13/10 16:39 7439-96-5 D309/07/10 15:2017.1 1.0Nickel 18.6 mg/kg 50 09/13/10 16:39 7440-02-0 D309/07/10 15:2017.1 6.1Selenium ND mg/kg 50 09/13/10 16:39 7782-49-2 D309/07/10 15:2034.1 13.0Silver 1.5J mg/kg 50 09/13/10 16:39 7440-22-4 D309/07/10 15:2017.1 1.0Thallium ND mg/kg 50 09/13/10 16:39 7440-28-0 D309/07/10 15:2034.1 8.9Zinc 181 mg/kg 50 09/13/10 16:39 7440-66-6 D309/07/10 15:2034.1 8.9


Mercury 0.0022J mg/kg 1 09/03/10 16:01 7439-97-609/01/10 02:500.0047 0.000093


Acenaphthene ND ug/kg 1 09/10/10 12:49 83-32-909/09/10 00:00370 85.1Acenaphthylene ND ug/kg 1 09/10/10 12:49 208-96-809/09/10 00:00370 87.3Acetophenone ND ug/kg 1 09/10/10 12:49 98-86-209/09/10 00:00370 190Anthracene ND ug/kg 1 09/10/10 12:49 120-12-709/09/10 00:00370 82.9Atrazine ND ug/kg 1 09/10/10 12:49 1912-24-909/09/10 00:00739 146Benzaldehyde ND ug/kg 1 09/10/10 12:49 100-52-709/09/10 00:00739 370Benzo(a)anthracene ND ug/kg 1 09/10/10 12:49 56-55-309/09/10 00:00370 68.3Benzo(a)pyrene ND ug/kg 1 09/10/10 12:49 50-32-809/09/10 00:00370 70.5Benzo(b)fluoranthene ND ug/kg 1 09/10/10 12:49 205-99-209/09/10 00:00370 63.8Benzo(g,h,i)perylene ND ug/kg 1 09/10/10 12:49 191-24-209/09/10 00:00370 94.1Benzo(k)fluoranthene ND ug/kg 1 09/10/10 12:49 207-08-909/09/10 00:00370 72.8Biphenyl (Diphenyl) ND ug/kg 1 09/10/10 12:49 92-52-409/09/10 00:00370 1164-Bromophenylphenyl ether ND ug/kg 1 09/10/10 12:49 101-55-309/09/10 00:00370 67.2Butylbenzylphthalate ND ug/kg 1 09/10/10 12:49 85-68-709/09/10 00:00370 78.4Caprolactam ND ug/kg 1 09/10/10 12:49 105-60-209/09/10 00:00370 63.8Carbazole ND ug/kg 1 09/10/10 12:49 86-74-809/09/10 00:00370 70.54-Chloro-3-methylphenol ND ug/kg 1 09/10/10 12:49 59-50-709/09/10 00:00739 76.14-Chloroaniline ND ug/kg 1 09/10/10 12:49 106-47-809/09/10 00:001850 103bis(2-Chloroethoxy)methane ND ug/kg 1 09/10/10 12:49 111-91-109/09/10 00:00370 86.2bis(2-Chloroethyl) ether ND ug/kg 1 09/10/10 12:49 111-44-409/09/10 00:00370 94.1bis(2-Chloroisopropyl) ether ND ug/kg 1 09/10/10 12:49 108-60-109/09/10 00:00370 98.52-Chloronaphthalene ND ug/kg 1 09/10/10 12:49 91-58-709/09/10 00:00370 72.82-Chlorophenol ND ug/kg 1 09/10/10 12:49 95-57-809/09/10 00:00370 1014-Chlorophenylphenyl ether ND ug/kg 1 09/10/10 12:49 7005-72-309/09/10 00:00370 76.1Chrysene ND ug/kg 1 09/10/10 12:49 218-01-909/09/10 00:00370 49.3Dibenz(a,h)anthracene ND ug/kg 1 09/10/10 12:49 53-70-309/09/10 00:00370 78.4Dibenzofuran ND ug/kg 1 09/10/10 12:49 132-64-909/09/10 00:00370 60.5



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/10/10 12:49 91-94-109/09/10 00:001850 80.62,4-Dichlorophenol ND ug/kg 1 09/10/10 12:49 120-83-209/09/10 00:00370 80.6Diethylphthalate ND ug/kg 1 09/10/10 12:49 84-66-209/09/10 00:00370 57.12,4-Dimethylphenol ND ug/kg 1 09/10/10 12:49 105-67-909/09/10 00:00370 146Dimethylphthalate ND ug/kg 1 09/10/10 12:49 131-11-309/09/10 00:00370 75.0Di-n-butylphthalate ND ug/kg 1 09/10/10 12:49 84-74-209/09/10 00:00370 60.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/10/10 12:49 534-52-109/09/10 00:00739 73.92,4-Dinitrophenol ND ug/kg 1 09/10/10 12:49 51-28-509/09/10 00:001850 60.52,4-Dinitrotoluene ND ug/kg 1 09/10/10 12:49 121-14-209/09/10 00:00370 69.42,6-Dinitrotoluene ND ug/kg 1 09/10/10 12:49 606-20-209/09/10 00:00370 77.3Di-n-octylphthalate ND ug/kg 1 09/10/10 12:49 117-84-009/09/10 00:00370 77.3bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/10/10 12:49 117-81-709/09/10 00:00370 101Fluoranthene ND ug/kg 1 09/10/10 12:49 206-44-009/09/10 00:00370 53.7Fluorene ND ug/kg 1 09/10/10 12:49 86-73-709/09/10 00:00370 76.1Hexachloro-1,3-butadiene ND ug/kg 1 09/10/10 12:49 87-68-309/09/10 00:00370 63.8Hexachlorobenzene ND ug/kg 1 09/10/10 12:49 118-74-109/09/10 00:00370 47.0Hexachlorocyclopentadiene ND ug/kg 1 09/10/10 12:49 77-47-409/09/10 00:00370 68.3Hexachloroethane ND ug/kg 1 09/10/10 12:49 67-72-109/09/10 00:00370 97.4Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/10/10 12:49 193-39-509/09/10 00:00370 76.1Isophorone ND ug/kg 1 09/10/10 12:49 78-59-109/09/10 00:00370 82.92-Methylnaphthalene ND ug/kg 1 09/10/10 12:49 91-57-609/09/10 00:00370 79.52-Methylphenol(o-Cresol) ND ug/kg 1 09/10/10 12:49 95-48-709/09/10 00:00370 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/10/10 12:4909/09/10 00:00370 146Naphthalene ND ug/kg 1 09/10/10 12:49 91-20-309/09/10 00:00370 90.72-Nitroaniline ND ug/kg 1 09/10/10 12:49 88-74-409/09/10 00:001850 1143-Nitroaniline ND ug/kg 1 09/10/10 12:49 99-09-209/09/10 00:001850 1014-Nitroaniline ND ug/kg 1 09/10/10 12:49 100-01-609/09/10 00:00739 104Nitrobenzene ND ug/kg 1 09/10/10 12:49 98-95-309/09/10 00:00370 1012-Nitrophenol ND ug/kg 1 09/10/10 12:49 88-75-509/09/10 00:00370 89.64-Nitrophenol ND ug/kg 1 09/10/10 12:49 100-02-709/09/10 00:001850 66.1N-Nitroso-di-n-propylamine ND ug/kg 1 09/10/10 12:49 621-64-709/09/10 00:00370 70.5N-Nitrosodiphenylamine ND ug/kg 1 09/10/10 12:49 86-30-609/09/10 00:00370 110Pentachlorophenol ND ug/kg 1 09/10/10 12:49 87-86-509/09/10 00:001850 67.2Phenanthrene ND ug/kg 1 09/10/10 12:49 85-01-809/09/10 00:00370 61.6Phenol ND ug/kg 1 09/10/10 12:49 108-95-209/09/10 00:00370 111Pyrene ND ug/kg 1 09/10/10 12:49 129-00-009/09/10 00:00370 62.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/10/10 12:49 95-94-309/09/10 00:00370 1342,3,4,6-Tetrachlorophenol ND ug/kg 1 09/10/10 12:49 58-90-209/09/10 00:00370 1462,4,5-Trichlorophenol ND ug/kg 1 09/10/10 12:49 95-95-409/09/10 00:00370 1142,4,6-Trichlorophenol ND ug/kg 1 09/10/10 12:49 88-06-209/09/10 00:00370 81.72-Fluorobiphenyl (S) 47 % 1 09/10/10 12:49 321-60-809/09/10 00:0030-110Terphenyl-d14 (S) 57 % 1 09/10/10 12:49 1718-51-009/09/10 00:0028-110Phenol-d6 (S) 43 % 1 09/10/10 12:49 13127-88-309/09/10 00:0022-1102-Fluorophenol (S) 40 % 1 09/10/10 12:49 367-12-409/09/10 00:0013-1102,4,6-Tribromophenol (S) 40 % 1 09/10/10 12:49 118-79-609/09/10 00:0027-110



Date: 09/27/2010 06:23 PM Page 56 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 43 % 1 09/10/10 12:49 4165-60-009/09/10 00:0023-110


Acetone 451 ug/kg 1 09/07/10 17:16 67-64-1 E102 10.2Benzene ND ug/kg 1 09/07/10 17:16 71-43-25.1 1.6Bromochloromethane ND ug/kg 1 09/07/10 17:16 74-97-55.1 1.7Bromodichloromethane ND ug/kg 1 09/07/10 17:16 75-27-45.1 1.9Bromoform ND ug/kg 1 09/07/10 17:16 75-25-25.1 2.3Bromomethane ND ug/kg 1 09/07/10 17:16 74-83-910.2 2.52-Butanone (MEK) 103 ug/kg 1 09/07/10 17:16 78-93-3102 2.9Carbon disulfide ND ug/kg 1 09/07/10 17:16 75-15-010.2 3.0Carbon tetrachloride ND ug/kg 1 09/07/10 17:16 56-23-55.1 2.6Chlorobenzene ND ug/kg 1 09/07/10 17:16 108-90-75.1 1.9Chloroethane ND ug/kg 1 09/07/10 17:16 75-00-310.2 2.4Chloroform ND ug/kg 1 09/07/10 17:16 67-66-35.1 1.6Chloromethane ND ug/kg 1 09/07/10 17:16 74-87-310.2 2.4Cyclohexane ND ug/kg 1 09/07/10 17:16 110-82-75.1 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 17:16 96-12-85.1 3.7Dibromochloromethane ND ug/kg 1 09/07/10 17:16 124-48-15.1 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 17:16 106-93-45.1 1.81,2-Dichlorobenzene ND ug/kg 1 09/07/10 17:16 95-50-15.1 1.91,3-Dichlorobenzene ND ug/kg 1 09/07/10 17:16 541-73-15.1 2.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 17:16 106-46-75.1 1.7Dichlorodifluoromethane ND ug/kg 1 09/07/10 17:16 75-71-810.2 3.71,1-Dichloroethane ND ug/kg 1 09/07/10 17:16 75-34-35.1 1.51,2-Dichloroethane ND ug/kg 1 09/07/10 17:16 107-06-25.1 2.21,1-Dichloroethene ND ug/kg 1 09/07/10 17:16 75-35-45.1 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:16 156-59-25.1 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:16 156-60-55.1 1.91,2-Dichloropropane ND ug/kg 1 09/07/10 17:16 78-87-55.1 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:16 10061-01-55.1 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:16 10061-02-65.1 1.5Ethylbenzene ND ug/kg 1 09/07/10 17:16 100-41-45.1 1.82-Hexanone 10.2J ug/kg 1 09/07/10 17:16 591-78-650.8 4.0Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 17:16 98-82-85.1 1.9Methyl acetate ND ug/kg 1 09/07/10 17:16 79-20-910.2 1.4Methylcyclohexane ND ug/kg 1 09/07/10 17:16 108-87-210.2 1.5Methylene Chloride 10.6J ug/kg 1 09/07/10 17:16 75-09-220.3 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 17:16 108-10-150.8 3.8Methyl-tert-butyl ether ND ug/kg 1 09/07/10 17:16 1634-04-45.1 1.5Styrene ND ug/kg 1 09/07/10 17:16 100-42-55.1 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 17:16 79-34-55.1 1.9Tetrachloroethene ND ug/kg 1 09/07/10 17:16 127-18-45.1 1.7Toluene ND ug/kg 1 09/07/10 17:16 108-88-35.1 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 17:16 87-61-65.1 2.2



Date: 09/27/2010 06:23 PM Page 57 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 17:16 120-82-15.1 1.61,1,1-Trichloroethane ND ug/kg 1 09/07/10 17:16 71-55-65.1 1.81,1,2-Trichloroethane ND ug/kg 1 09/07/10 17:16 79-00-55.1 2.1Trichloroethene 10.1 ug/kg 1 09/07/10 17:16 79-01-65.1 2.1Trichlorofluoromethane ND ug/kg 1 09/07/10 17:16 75-69-45.1 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/07/10 17:16 76-13-15.1 1.9Vinyl chloride ND ug/kg 1 09/07/10 17:16 75-01-410.2 1.8Xylene (Total) ND ug/kg 1 09/07/10 17:16 1330-20-710.2 3.7m&p-Xylene ND ug/kg 1 09/07/10 17:16 179601-23-110.2 3.7o-Xylene ND ug/kg 1 09/07/10 17:16 95-47-65.1 1.9Dibromofluoromethane (S) 100 % 1 09/07/10 17:16 1868-53-770-130Toluene-d8 (S) 102 % 1 09/07/10 17:16 2037-26-570-1304-Bromofluorobenzene (S) 98 % 1 09/07/10 17:16 460-00-470-1301,2-Dichloroethane-d4 (S) 104 % 1 09/07/10 17:16 17060-07-070-132




Cyanide 4.4 mg/kg 1 09/05/10 13:36 57-12-50.21 0.21





Date: 09/27/2010 06:23 PM Page 58 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony 3.3J mg/kg 10 09/13/10 15:38 7440-36-0 D309/07/10 15:205.0 2.8Arsenic ND mg/kg 10 09/13/10 15:38 7440-38-2 D309/07/10 15:205.0 3.2Beryllium 11.9 mg/kg 10 09/13/10 15:38 7440-41-7 D309/07/10 15:201.0 0.20Cadmium 4.0 mg/kg 10 09/13/10 15:38 7440-43-9 D309/07/10 15:201.0 0.60Chromium 36.9 mg/kg 10 09/13/10 15:38 7440-47-3 D309/07/10 15:205.0 0.30Copper 87.5 mg/kg 10 09/13/10 15:38 7440-50-8 D309/07/10 15:205.0 0.40Lead 9.4 mg/kg 10 09/13/10 15:38 7439-92-1 D309/07/10 15:205.0 4.8Manganese 4010 mg/kg 10 09/13/10 15:38 7439-96-5 D309/07/10 15:205.0 0.30Nickel 31.4 mg/kg 10 09/13/10 15:38 7440-02-0 D309/07/10 15:205.0 1.8Selenium ND mg/kg 10 09/13/10 15:38 7782-49-2 D309/07/10 15:2010.1 3.8Silver ND mg/kg 10 09/13/10 15:38 7440-22-4 D309/07/10 15:205.0 0.30Thallium 7.3J mg/kg 10 09/13/10 15:38 7440-28-0 D309/07/10 15:2010.1 2.6Zinc 193 mg/kg 10 09/13/10 15:38 7440-66-6 D309/07/10 15:2010.1 2.6


Mercury 0.00017J mg/kg 1 09/03/10 18:05 7439-97-609/01/10 02:500.0047 0.000093


Acenaphthene ND ug/kg 1 09/10/10 15:00 83-32-909/09/10 00:00379 87.2Acenaphthylene ND ug/kg 1 09/10/10 15:00 208-96-809/09/10 00:00379 89.5Acetophenone ND ug/kg 1 09/10/10 15:00 98-86-209/09/10 00:00379 195Anthracene ND ug/kg 1 09/10/10 15:00 120-12-709/09/10 00:00379 84.9Atrazine ND ug/kg 1 09/10/10 15:00 1912-24-909/09/10 00:00757 149Benzaldehyde ND ug/kg 1 09/10/10 15:00 100-52-709/09/10 00:00757 379Benzo(a)anthracene ND ug/kg 1 09/10/10 15:00 56-55-309/09/10 00:00379 70.0Benzo(a)pyrene ND ug/kg 1 09/10/10 15:00 50-32-809/09/10 00:00379 72.3Benzo(b)fluoranthene ND ug/kg 1 09/10/10 15:00 205-99-209/09/10 00:00379 65.4Benzo(g,h,i)perylene ND ug/kg 1 09/10/10 15:00 191-24-209/09/10 00:00379 96.4Benzo(k)fluoranthene ND ug/kg 1 09/10/10 15:00 207-08-909/09/10 00:00379 74.6Biphenyl (Diphenyl) ND ug/kg 1 09/10/10 15:00 92-52-409/09/10 00:00379 1194-Bromophenylphenyl ether ND ug/kg 1 09/10/10 15:00 101-55-309/09/10 00:00379 68.8Butylbenzylphthalate ND ug/kg 1 09/10/10 15:00 85-68-709/09/10 00:00379 80.3Caprolactam ND ug/kg 1 09/10/10 15:00 105-60-209/09/10 00:00379 65.4Carbazole ND ug/kg 1 09/10/10 15:00 86-74-809/09/10 00:00379 72.34-Chloro-3-methylphenol ND ug/kg 1 09/10/10 15:00 59-50-709/09/10 00:00757 78.04-Chloroaniline ND ug/kg 1 09/10/10 15:00 106-47-809/09/10 00:001890 106bis(2-Chloroethoxy)methane ND ug/kg 1 09/10/10 15:00 111-91-109/09/10 00:00379 88.4bis(2-Chloroethyl) ether ND ug/kg 1 09/10/10 15:00 111-44-409/09/10 00:00379 96.4bis(2-Chloroisopropyl) ether ND ug/kg 1 09/10/10 15:00 108-60-109/09/10 00:00379 1012-Chloronaphthalene ND ug/kg 1 09/10/10 15:00 91-58-709/09/10 00:00379 74.62-Chlorophenol ND ug/kg 1 09/10/10 15:00 95-57-809/09/10 00:00379 1034-Chlorophenylphenyl ether ND ug/kg 1 09/10/10 15:00 7005-72-309/09/10 00:00379 78.0Chrysene ND ug/kg 1 09/10/10 15:00 218-01-909/09/10 00:00379 50.5Dibenz(a,h)anthracene ND ug/kg 1 09/10/10 15:00 53-70-309/09/10 00:00379 80.3Dibenzofuran ND ug/kg 1 09/10/10 15:00 132-64-909/09/10 00:00379 62.0



Date: 09/27/2010 06:23 PM Page 59 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 60 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 33 % 1 09/10/10 15:00 4165-60-009/09/10 00:0023-110


Acetone 12.9J ug/kg 1 09/07/10 17:35 67-64-195.6 9.6Benzene ND ug/kg 1 09/07/10 17:35 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/07/10 17:35 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/07/10 17:35 75-27-44.8 1.8Bromoform ND ug/kg 1 09/07/10 17:35 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/07/10 17:35 74-83-99.6 2.42-Butanone (MEK) ND ug/kg 1 09/07/10 17:35 78-93-395.6 2.8Carbon disulfide ND ug/kg 1 09/07/10 17:35 75-15-09.6 2.9Carbon tetrachloride ND ug/kg 1 09/07/10 17:35 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/07/10 17:35 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/07/10 17:35 75-00-39.6 2.3Chloroform ND ug/kg 1 09/07/10 17:35 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/07/10 17:35 74-87-39.6 2.3Cyclohexane ND ug/kg 1 09/07/10 17:35 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 17:35 96-12-84.8 3.4Dibromochloromethane ND ug/kg 1 09/07/10 17:35 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 17:35 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/07/10 17:35 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/07/10 17:35 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/07/10 17:35 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/07/10 17:35 75-71-89.6 3.41,1-Dichloroethane ND ug/kg 1 09/07/10 17:35 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/07/10 17:35 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/07/10 17:35 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:35 156-59-24.8 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:35 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/07/10 17:35 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:35 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:35 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/07/10 17:35 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/07/10 17:35 591-78-647.8 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 17:35 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/07/10 17:35 79-20-99.6 1.3Methylcyclohexane ND ug/kg 1 09/07/10 17:35 108-87-29.6 1.4Methylene Chloride 14.2J ug/kg 1 09/07/10 17:35 75-09-219.1 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 17:35 108-10-147.8 3.5Methyl-tert-butyl ether ND ug/kg 1 09/07/10 17:35 1634-04-44.8 1.4Styrene ND ug/kg 1 09/07/10 17:35 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 17:35 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/07/10 17:35 127-18-44.8 1.6Toluene ND ug/kg 1 09/07/10 17:35 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 17:35 87-61-64.8 2.1



Date: 09/27/2010 06:23 PM Page 61 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 17:35 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/07/10 17:35 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/07/10 17:35 79-00-54.8 2.0Trichloroethene 476 ug/kg 10 09/08/10 16:17 79-01-646.1 19.4Trichlorofluoromethane ND ug/kg 1 09/07/10 17:35 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/07/10 17:35 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/07/10 17:35 75-01-49.6 1.7Xylene (Total) ND ug/kg 1 09/07/10 17:35 1330-20-79.6 3.4m&p-Xylene ND ug/kg 1 09/07/10 17:35 179601-23-19.6 3.4o-Xylene ND ug/kg 1 09/07/10 17:35 95-47-64.8 1.8Dibromofluoromethane (S) 102 % 1 09/07/10 17:35 1868-53-770-130Toluene-d8 (S) 96 % 1 09/07/10 17:35 2037-26-570-1304-Bromofluorobenzene (S) 90 % 1 09/07/10 17:35 460-00-470-1301,2-Dichloroethane-d4 (S) 106 % 1 09/07/10 17:35 17060-07-070-132




Cyanide 17.8 mg/kg 5 09/05/10 14:58 57-12-50.86 0.86





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: SS-122 Lab ID: 9276750005 Collected: 08/31/10 10:10 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis



Antimony 1.5 mg/kg 1 09/10/10 15:21 7440-36-009/07/10 15:200.39 0.22Arsenic ND mg/kg 1 09/10/10 15:21 7440-38-209/07/10 15:200.39 0.25Beryllium 1.6 mg/kg 1 09/10/10 15:21 7440-41-709/07/10 15:200.078 0.016Cadmium 1.7 mg/kg 1 09/10/10 15:21 7440-43-909/07/10 15:200.078 0.047Chromium 33.8 mg/kg 1 09/10/10 15:21 7440-47-309/07/10 15:200.39 0.023Copper 27.0 mg/kg 1 09/10/10 15:21 7440-50-809/07/10 15:200.39 0.031Lead 3.4 mg/kg 1 09/10/10 15:21 7439-92-109/07/10 15:200.39 0.37Manganese 71.1 mg/kg 1 09/10/10 15:21 7439-96-509/07/10 15:200.39 0.023Nickel 5.3 mg/kg 1 09/10/10 15:21 7440-02-009/07/10 15:200.39 0.14Selenium 0.39J mg/kg 1 09/10/10 15:21 7782-49-209/07/10 15:200.78 0.30Silver 0.035J mg/kg 1 09/10/10 15:21 7440-22-409/07/10 15:200.39 0.023Thallium 0.36J mg/kg 1 09/10/10 15:21 7440-28-009/07/10 15:200.78 0.20Zinc 52.7 mg/kg 1 09/10/10 15:21 7440-66-609/07/10 15:200.78 0.20


Mercury 0.0053 mg/kg 1 09/03/10 16:09 7439-97-609/01/10 02:500.0053 0.00011





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/10/10 15:36 91-94-109/09/10 00:002050 89.52,4-Dichlorophenol ND ug/kg 1 09/10/10 15:36 120-83-209/09/10 00:00410 89.5Diethylphthalate ND ug/kg 1 09/10/10 15:36 84-66-209/09/10 00:00410 63.42,4-Dimethylphenol ND ug/kg 1 09/10/10 15:36 105-67-909/09/10 00:00410 162Dimethylphthalate ND ug/kg 1 09/10/10 15:36 131-11-309/09/10 00:00410 83.2Di-n-butylphthalate ND ug/kg 1 09/10/10 15:36 84-74-209/09/10 00:00410 67.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/10/10 15:36 534-52-109/09/10 00:00820 82.02,4-Dinitrophenol ND ug/kg 1 09/10/10 15:36 51-28-509/09/10 00:002050 67.12,4-Dinitrotoluene ND ug/kg 1 09/10/10 15:36 121-14-209/09/10 00:00410 77.02,6-Dinitrotoluene ND ug/kg 1 09/10/10 15:36 606-20-209/09/10 00:00410 85.7Di-n-octylphthalate ND ug/kg 1 09/10/10 15:36 117-84-009/09/10 00:00410 85.7bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/10/10 15:36 117-81-709/09/10 00:00410 112Fluoranthene ND ug/kg 1 09/10/10 15:36 206-44-009/09/10 00:00410 59.6Fluorene ND ug/kg 1 09/10/10 15:36 86-73-709/09/10 00:00410 84.5Hexachloro-1,3-butadiene ND ug/kg 1 09/10/10 15:36 87-68-309/09/10 00:00410 70.8Hexachlorobenzene ND ug/kg 1 09/10/10 15:36 118-74-109/09/10 00:00410 52.2Hexachlorocyclopentadiene ND ug/kg 1 09/10/10 15:36 77-47-409/09/10 00:00410 75.8Hexachloroethane ND ug/kg 1 09/10/10 15:36 67-72-109/09/10 00:00410 108Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/10/10 15:36 193-39-509/09/10 00:00410 84.5Isophorone ND ug/kg 1 09/10/10 15:36 78-59-109/09/10 00:00410 91.92-Methylnaphthalene ND ug/kg 1 09/10/10 15:36 91-57-609/09/10 00:00410 88.22-Methylphenol(o-Cresol) ND ug/kg 1 09/10/10 15:36 95-48-709/09/10 00:00410 1243&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/10/10 15:3609/09/10 00:00410 162Naphthalene ND ug/kg 1 09/10/10 15:36 91-20-309/09/10 00:00410 1012-Nitroaniline ND ug/kg 1 09/10/10 15:36 88-74-409/09/10 00:002050 1273-Nitroaniline ND ug/kg 1 09/10/10 15:36 99-09-209/09/10 00:002050 1124-Nitroaniline ND ug/kg 1 09/10/10 15:36 100-01-609/09/10 00:00820 116Nitrobenzene ND ug/kg 1 09/10/10 15:36 98-95-309/09/10 00:00410 1122-Nitrophenol ND ug/kg 1 09/10/10 15:36 88-75-509/09/10 00:00410 99.44-Nitrophenol ND ug/kg 1 09/10/10 15:36 100-02-709/09/10 00:002050 73.3N-Nitroso-di-n-propylamine ND ug/kg 1 09/10/10 15:36 621-64-709/09/10 00:00410 78.3N-Nitrosodiphenylamine ND ug/kg 1 09/10/10 15:36 86-30-609/09/10 00:00410 122Pentachlorophenol ND ug/kg 1 09/10/10 15:36 87-86-509/09/10 00:002050 74.5Phenanthrene ND ug/kg 1 09/10/10 15:36 85-01-809/09/10 00:00410 68.3Phenol ND ug/kg 1 09/10/10 15:36 108-95-209/09/10 00:00410 123Pyrene ND ug/kg 1 09/10/10 15:36 129-00-009/09/10 00:00410 69.61,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/10/10 15:36 95-94-309/09/10 00:00410 1492,3,4,6-Tetrachlorophenol ND ug/kg 1 09/10/10 15:36 58-90-209/09/10 00:00410 1622,4,5-Trichlorophenol ND ug/kg 1 09/10/10 15:36 95-95-409/09/10 00:00410 1272,4,6-Trichlorophenol ND ug/kg 1 09/10/10 15:36 88-06-209/09/10 00:00410 90.72-Fluorobiphenyl (S) 55 % 1 09/10/10 15:36 321-60-809/09/10 00:0030-110Terphenyl-d14 (S) 57 % 1 09/10/10 15:36 1718-51-009/09/10 00:0028-110Phenol-d6 (S) 53 % 1 09/10/10 15:36 13127-88-309/09/10 00:0022-1102-Fluorophenol (S) 51 % 1 09/10/10 15:36 367-12-409/09/10 00:0013-1102,4,6-Tribromophenol (S) 51 % 1 09/10/10 15:36 118-79-609/09/10 00:0027-110



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 54 % 1 09/10/10 15:36 4165-60-009/09/10 00:0023-110


Acetone ND ug/kg 1 09/07/10 17:53 67-64-195.6 9.6Benzene ND ug/kg 1 09/07/10 17:53 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/07/10 17:53 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/07/10 17:53 75-27-44.8 1.8Bromoform ND ug/kg 1 09/07/10 17:53 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/07/10 17:53 74-83-99.6 2.42-Butanone (MEK) ND ug/kg 1 09/07/10 17:53 78-93-395.6 2.8Carbon disulfide ND ug/kg 1 09/07/10 17:53 75-15-09.6 2.9Carbon tetrachloride ND ug/kg 1 09/07/10 17:53 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/07/10 17:53 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/07/10 17:53 75-00-39.6 2.3Chloroform ND ug/kg 1 09/07/10 17:53 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/07/10 17:53 74-87-39.6 2.3Cyclohexane ND ug/kg 1 09/07/10 17:53 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 17:53 96-12-84.8 3.4Dibromochloromethane ND ug/kg 1 09/07/10 17:53 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 17:53 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/07/10 17:53 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/07/10 17:53 75-71-89.6 3.41,1-Dichloroethane ND ug/kg 1 09/07/10 17:53 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/07/10 17:53 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/07/10 17:53 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:53 156-59-24.8 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 17:53 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/07/10 17:53 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:53 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 17:53 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/07/10 17:53 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/07/10 17:53 591-78-647.8 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 17:53 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/07/10 17:53 79-20-99.6 1.3Methylcyclohexane ND ug/kg 1 09/07/10 17:53 108-87-29.6 1.4Methylene Chloride 4.1J ug/kg 1 09/07/10 17:53 75-09-219.1 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 17:53 108-10-147.8 3.5Methyl-tert-butyl ether ND ug/kg 1 09/07/10 17:53 1634-04-44.8 1.4Styrene ND ug/kg 1 09/07/10 17:53 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 17:53 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/07/10 17:53 127-18-44.8 1.6Toluene ND ug/kg 1 09/07/10 17:53 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 17:53 87-61-64.8 2.1



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 17:53 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/07/10 17:53 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/07/10 17:53 79-00-54.8 2.0Trichloroethene 3.2J ug/kg 1 09/07/10 17:53 79-01-64.8 2.0Trichlorofluoromethane ND ug/kg 1 09/07/10 17:53 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/07/10 17:53 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/07/10 17:53 75-01-49.6 1.7Xylene (Total) ND ug/kg 1 09/07/10 17:53 1330-20-79.6 3.4m&p-Xylene ND ug/kg 1 09/07/10 17:53 179601-23-19.6 3.4o-Xylene ND ug/kg 1 09/07/10 17:53 95-47-64.8 1.8Dibromofluoromethane (S) 100 % 1 09/07/10 17:53 1868-53-770-130Toluene-d8 (S) 100 % 1 09/07/10 17:53 2037-26-570-1304-Bromofluorobenzene (S) 96 % 1 09/07/10 17:53 460-00-470-1301,2-Dichloroethane-d4 (S) 103 % 1 09/07/10 17:53 17060-07-070-132




Cyanide ND mg/kg 1 09/05/10 13:38 57-12-50.17 0.17





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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony 0.71 mg/kg 1 09/13/10 15:18 7440-36-009/07/10 15:200.36 0.20Arsenic ND mg/kg 1 09/13/10 15:18 7440-38-209/07/10 15:200.36 0.23Beryllium 0.56 mg/kg 1 09/13/10 15:18 7440-41-709/07/10 15:200.072 0.014Cadmium 1.0 mg/kg 1 09/13/10 15:18 7440-43-909/07/10 15:200.072 0.043Chromium 18.3 mg/kg 1 09/13/10 15:18 7440-47-309/07/10 15:200.36 0.022Copper 20.7 mg/kg 1 09/13/10 15:18 7440-50-809/07/10 15:200.36 0.029Lead 10.8 mg/kg 1 09/13/10 15:18 7439-92-109/07/10 15:200.36 0.35Manganese 564 mg/kg 1 09/13/10 15:18 7439-96-509/07/10 15:200.36 0.022Nickel 15.8 mg/kg 1 09/13/10 15:18 7440-02-009/07/10 15:200.36 0.13Selenium 0.60J mg/kg 1 09/13/10 15:18 7782-49-209/07/10 15:200.72 0.27Silver 0.082J mg/kg 1 09/13/10 15:18 7440-22-409/07/10 15:200.36 0.022Thallium 0.80 mg/kg 1 09/13/10 15:18 7440-28-009/07/10 15:200.72 0.19Zinc 50.0 mg/kg 1 09/13/10 15:18 7440-66-609/07/10 15:200.72 0.19


Mercury 0.0032J mg/kg 1 09/07/10 16:33 7439-97-609/02/10 19:200.0050 0.00010


Acenaphthene ND ug/kg 1 09/23/10 14:51 83-32-909/10/10 09:30386 88.9Acenaphthylene ND ug/kg 1 09/23/10 14:51 208-96-809/10/10 09:30386 91.2Acetophenone ND ug/kg 1 09/23/10 14:51 98-86-209/10/10 09:30386 199Anthracene ND ug/kg 1 09/23/10 14:51 120-12-709/10/10 09:30386 86.5Atrazine ND ug/kg 1 09/23/10 14:51 1912-24-909/10/10 09:30772 152Benzaldehyde ND ug/kg 1 09/23/10 14:51 100-52-709/10/10 09:30772 386Benzo(a)anthracene ND ug/kg 1 09/23/10 14:51 56-55-309/10/10 09:30386 71.3Benzo(a)pyrene ND ug/kg 1 09/23/10 14:51 50-32-809/10/10 09:30386 73.7Benzo(b)fluoranthene ND ug/kg 1 09/23/10 14:51 205-99-209/10/10 09:30386 66.7Benzo(g,h,i)perylene 101J ug/kg 1 09/23/10 14:51 191-24-209/10/10 09:30386 98.2Benzo(k)fluoranthene ND ug/kg 1 09/23/10 14:51 207-08-909/10/10 09:30386 76.0Biphenyl (Diphenyl) ND ug/kg 1 09/23/10 14:51 92-52-409/10/10 09:30386 1224-Bromophenylphenyl ether ND ug/kg 1 09/23/10 14:51 101-55-309/10/10 09:30386 70.2Butylbenzylphthalate ND ug/kg 1 09/23/10 14:51 85-68-709/10/10 09:30386 81.9Caprolactam ND ug/kg 1 09/23/10 14:51 105-60-209/10/10 09:30386 66.7Carbazole ND ug/kg 1 09/23/10 14:51 86-74-809/10/10 09:30386 73.74-Chloro-3-methylphenol ND ug/kg 1 09/23/10 14:51 59-50-709/10/10 09:30772 79.54-Chloroaniline ND ug/kg 1 09/23/10 14:51 106-47-809/10/10 09:301930 108bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/10 14:51 111-91-109/10/10 09:30386 90.0bis(2-Chloroethyl) ether ND ug/kg 1 09/23/10 14:51 111-44-409/10/10 09:30386 98.2bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/10 14:51 108-60-109/10/10 09:30386 1032-Chloronaphthalene ND ug/kg 1 09/23/10 14:51 91-58-709/10/10 09:30386 76.02-Chlorophenol ND ug/kg 1 09/23/10 14:51 95-57-809/10/10 09:30386 1054-Chlorophenylphenyl ether ND ug/kg 1 09/23/10 14:51 7005-72-309/10/10 09:30386 79.5Chrysene ND ug/kg 1 09/23/10 14:51 218-01-909/10/10 09:30386 51.5Dibenz(a,h)anthracene 94.0J ug/kg 1 09/23/10 14:51 53-70-309/10/10 09:30386 81.9Dibenzofuran ND ug/kg 1 09/23/10 14:51 132-64-909/10/10 09:30386 63.1



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/23/10 14:51 91-94-109/10/10 09:301930 84.22,4-Dichlorophenol ND ug/kg 1 09/23/10 14:51 120-83-209/10/10 09:30386 84.2Diethylphthalate ND ug/kg 1 09/23/10 14:51 84-66-209/10/10 09:30386 59.62,4-Dimethylphenol ND ug/kg 1 09/23/10 14:51 105-67-909/10/10 09:30386 152Dimethylphthalate ND ug/kg 1 09/23/10 14:51 131-11-309/10/10 09:30386 78.4Di-n-butylphthalate ND ug/kg 1 09/23/10 14:51 84-74-209/10/10 09:30386 63.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/10 14:51 534-52-109/10/10 09:30772 77.22,4-Dinitrophenol ND ug/kg 1 09/23/10 14:51 51-28-509/10/10 09:301930 63.12,4-Dinitrotoluene ND ug/kg 1 09/23/10 14:51 121-14-209/10/10 09:30386 72.52,6-Dinitrotoluene ND ug/kg 1 09/23/10 14:51 606-20-209/10/10 09:30386 80.7Di-n-octylphthalate ND ug/kg 1 09/23/10 14:51 117-84-009/10/10 09:30386 80.7bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/10 14:51 117-81-709/10/10 09:30386 105Fluoranthene ND ug/kg 1 09/23/10 14:51 206-44-009/10/10 09:30386 56.1Fluorene ND ug/kg 1 09/23/10 14:51 86-73-709/10/10 09:30386 79.5Hexachloro-1,3-butadiene ND ug/kg 1 09/23/10 14:51 87-68-309/10/10 09:30386 66.7Hexachlorobenzene ND ug/kg 1 09/23/10 14:51 118-74-109/10/10 09:30386 49.1Hexachlorocyclopentadiene ND ug/kg 1 09/23/10 14:51 77-47-409/10/10 09:30386 71.3Hexachloroethane ND ug/kg 1 09/23/10 14:51 67-72-109/10/10 09:30386 102Indeno(1,2,3-cd)pyrene 87.8J ug/kg 1 09/23/10 14:51 193-39-509/10/10 09:30386 79.5Isophorone ND ug/kg 1 09/23/10 14:51 78-59-109/10/10 09:30386 86.52-Methylnaphthalene ND ug/kg 1 09/23/10 14:51 91-57-609/10/10 09:30386 83.02-Methylphenol(o-Cresol) ND ug/kg 1 09/23/10 14:51 95-48-709/10/10 09:30386 1173&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/23/10 14:5109/10/10 09:30386 152Naphthalene ND ug/kg 1 09/23/10 14:51 91-20-309/10/10 09:30386 94.72-Nitroaniline ND ug/kg 1 09/23/10 14:51 88-74-409/10/10 09:301930 1193-Nitroaniline ND ug/kg 1 09/23/10 14:51 99-09-209/10/10 09:301930 1054-Nitroaniline ND ug/kg 1 09/23/10 14:51 100-01-609/10/10 09:30772 109Nitrobenzene ND ug/kg 1 09/23/10 14:51 98-95-309/10/10 09:30386 1052-Nitrophenol ND ug/kg 1 09/23/10 14:51 88-75-509/10/10 09:30386 93.64-Nitrophenol ND ug/kg 1 09/23/10 14:51 100-02-709/10/10 09:301930 69.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/10 14:51 621-64-709/10/10 09:30386 73.7N-Nitrosodiphenylamine ND ug/kg 1 09/23/10 14:51 86-30-609/10/10 09:30386 115Pentachlorophenol ND ug/kg 1 09/23/10 14:51 87-86-509/10/10 09:301930 70.2Phenanthrene ND ug/kg 1 09/23/10 14:51 85-01-809/10/10 09:30386 64.3Phenol ND ug/kg 1 09/23/10 14:51 108-95-209/10/10 09:30386 116Pyrene ND ug/kg 1 09/23/10 14:51 129-00-009/10/10 09:30386 65.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/23/10 14:51 95-94-309/10/10 09:30386 1402,3,4,6-Tetrachlorophenol ND ug/kg 1 09/23/10 14:51 58-90-209/10/10 09:30386 1522,4,5-Trichlorophenol ND ug/kg 1 09/23/10 14:51 95-95-409/10/10 09:30386 1192,4,6-Trichlorophenol ND ug/kg 1 09/23/10 14:51 88-06-209/10/10 09:30386 85.42-Fluorobiphenyl (S) 38 % 1 09/23/10 14:51 321-60-809/10/10 09:3030-110Terphenyl-d14 (S) 55 % 1 09/23/10 14:51 1718-51-009/10/10 09:3028-110Phenol-d6 (S) 25 % 1 09/23/10 14:51 13127-88-309/10/10 09:3022-1102-Fluorophenol (S) 24 % 1 09/23/10 14:51 367-12-409/10/10 09:3013-1102,4,6-Tribromophenol (S) 47 % 1 09/23/10 14:51 118-79-609/10/10 09:3027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 30 % 1 09/23/10 14:51 4165-60-009/10/10 09:3023-110





Date: 09/27/2010 06:23 PM Page 69 of 242



(704)875-9092


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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:39 57-12-50.18 0.18





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony 0.80 mg/kg 1 09/10/10 15:28 7440-36-009/07/10 15:200.38 0.21Arsenic ND mg/kg 1 09/10/10 15:28 7440-38-209/07/10 15:200.38 0.24Beryllium 0.55 mg/kg 1 09/10/10 15:28 7440-41-709/07/10 15:200.076 0.015Cadmium 0.82 mg/kg 1 09/10/10 15:28 7440-43-909/07/10 15:200.076 0.046Chromium 19.2 mg/kg 1 09/10/10 15:28 7440-47-309/07/10 15:200.38 0.023Copper 6.6 mg/kg 1 09/10/10 15:28 7440-50-809/07/10 15:200.38 0.030Lead 12.6 mg/kg 1 09/10/10 15:28 7439-92-109/07/10 15:200.38 0.37Manganese 384 mg/kg 1 09/10/10 15:28 7439-96-509/07/10 15:200.38 0.023Nickel 10.2 mg/kg 1 09/10/10 15:28 7440-02-009/07/10 15:200.38 0.14Selenium 0.36J mg/kg 1 09/10/10 15:28 7782-49-209/07/10 15:200.76 0.29Silver ND mg/kg 1 09/10/10 15:28 7440-22-409/07/10 15:200.38 0.023Thallium 0.40J mg/kg 1 09/10/10 15:28 7440-28-009/07/10 15:200.76 0.20Zinc 47.6 mg/kg 1 09/10/10 15:28 7440-66-609/07/10 15:200.76 0.20


Mercury 0.015 mg/kg 1 09/07/10 16:36 7439-97-609/02/10 19:200.0050 0.00010





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Nitrobenzene-d5 (S) 47 % 1 09/16/10 18:35 4165-60-009/10/10 09:3023-110





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Cyanide ND mg/kg 1 09/05/10 13:41 57-12-50.19 0.19





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Sample: FD-01 Lab ID: 9276750008 Collected: 08/30/10 00:00 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis





Cyanide ND mg/kg 1 09/05/10 13:29 57-12-50.44 0.44



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Antimony ND mg/kg 5 09/13/10 15:41 7440-36-0 D309/07/10 15:202.2 1.3Arsenic 2.2 mg/kg 5 09/13/10 15:41 7440-38-2 D309/07/10 15:202.2 1.4Beryllium 1.2 mg/kg 5 09/13/10 15:41 7440-41-7 D309/07/10 15:200.45 0.089Cadmium ND mg/kg 5 09/13/10 15:41 7440-43-9 D309/07/10 15:200.45 0.27Chromium 3.4 mg/kg 5 09/13/10 15:41 7440-47-3 D309/07/10 15:202.2 0.13Copper 20.8 mg/kg 5 09/13/10 15:41 7440-50-8 D309/07/10 15:202.2 0.18Lead 14.4 mg/kg 5 09/13/10 15:41 7439-92-1 D309/07/10 15:202.2 2.1Manganese 786 mg/kg 5 09/13/10 15:41 7439-96-5 D309/07/10 15:202.2 0.13Nickel 4.7 mg/kg 5 09/13/10 15:41 7440-02-0 D309/07/10 15:202.2 0.80Selenium ND mg/kg 5 09/13/10 15:41 7782-49-2 D309/07/10 15:204.5 1.7Silver ND mg/kg 5 09/13/10 15:41 7440-22-4 D309/07/10 15:202.2 0.13Thallium ND mg/kg 5 09/13/10 15:41 7440-28-0 D309/07/10 15:204.5 1.2Zinc 15.6 mg/kg 5 09/13/10 15:41 7440-66-6 D309/07/10 15:204.5 1.2


Mercury ND mg/kg 1 09/03/10 18:08 7439-97-609/01/10 02:500.0045 0.000090





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Acenaphthene ND ug/kg 1 09/16/10 19:12 83-32-909/10/10 09:30388 89.3Acenaphthylene ND ug/kg 1 09/16/10 19:12 208-96-809/10/10 09:30388 91.6Acetophenone ND ug/kg 1 09/16/10 19:12 98-86-209/10/10 09:30388 200Anthracene ND ug/kg 1 09/16/10 19:12 120-12-709/10/10 09:30388 86.9Atrazine ND ug/kg 1 09/16/10 19:12 1912-24-909/10/10 09:30775 153Benzaldehyde ND ug/kg 1 09/16/10 19:12 100-52-709/10/10 09:30775 388Benzo(a)anthracene ND ug/kg 1 09/16/10 19:12 56-55-309/10/10 09:30388 71.7Benzo(a)pyrene ND ug/kg 1 09/16/10 19:12 50-32-809/10/10 09:30388 74.0Benzo(b)fluoranthene ND ug/kg 1 09/16/10 19:12 205-99-209/10/10 09:30388 67.0Benzo(g,h,i)perylene ND ug/kg 1 09/16/10 19:12 191-24-209/10/10 09:30388 98.7Benzo(k)fluoranthene ND ug/kg 1 09/16/10 19:12 207-08-909/10/10 09:30388 76.4Biphenyl (Diphenyl) ND ug/kg 1 09/16/10 19:12 92-52-409/10/10 09:30388 1224-Bromophenylphenyl ether ND ug/kg 1 09/16/10 19:12 101-55-309/10/10 09:30388 70.5Butylbenzylphthalate ND ug/kg 1 09/16/10 19:12 85-68-709/10/10 09:30388 82.2Caprolactam ND ug/kg 1 09/16/10 19:12 105-60-209/10/10 09:30388 67.0Carbazole ND ug/kg 1 09/16/10 19:12 86-74-809/10/10 09:30388 74.04-Chloro-3-methylphenol ND ug/kg 1 09/16/10 19:12 59-50-709/10/10 09:30775 79.94-Chloroaniline ND ug/kg 1 09/16/10 19:12 106-47-809/10/10 09:301940 108bis(2-Chloroethoxy)methane ND ug/kg 1 09/16/10 19:12 111-91-109/10/10 09:30388 90.4bis(2-Chloroethyl) ether ND ug/kg 1 09/16/10 19:12 111-44-409/10/10 09:30388 98.7bis(2-Chloroisopropyl) ether ND ug/kg 1 09/16/10 19:12 108-60-109/10/10 09:30388 1032-Chloronaphthalene ND ug/kg 1 09/16/10 19:12 91-58-709/10/10 09:30388 76.42-Chlorophenol ND ug/kg 1 09/16/10 19:12 95-57-809/10/10 09:30388 1064-Chlorophenylphenyl ether ND ug/kg 1 09/16/10 19:12 7005-72-309/10/10 09:30388 79.9Chrysene ND ug/kg 1 09/16/10 19:12 218-01-909/10/10 09:30388 51.7Dibenz(a,h)anthracene ND ug/kg 1 09/16/10 19:12 53-70-309/10/10 09:30388 82.2Dibenzofuran ND ug/kg 1 09/16/10 19:12 132-64-909/10/10 09:30388 63.43,3'-Dichlorobenzidine ND ug/kg 1 09/16/10 19:12 91-94-109/10/10 09:301940 84.62,4-Dichlorophenol ND ug/kg 1 09/16/10 19:12 120-83-209/10/10 09:30388 84.6Diethylphthalate ND ug/kg 1 09/16/10 19:12 84-66-209/10/10 09:30388 59.92,4-Dimethylphenol ND ug/kg 1 09/16/10 19:12 105-67-909/10/10 09:30388 153Dimethylphthalate ND ug/kg 1 09/16/10 19:12 131-11-309/10/10 09:30388 78.7Di-n-butylphthalate ND ug/kg 1 09/16/10 19:12 84-74-209/10/10 09:30388 63.44,6-Dinitro-2-methylphenol ND ug/kg 1 09/16/10 19:12 534-52-109/10/10 09:30775 77.52,4-Dinitrophenol ND ug/kg 1 09/16/10 19:12 51-28-509/10/10 09:301940 63.42,4-Dinitrotoluene ND ug/kg 1 09/16/10 19:12 121-14-209/10/10 09:30388 72.82,6-Dinitrotoluene 300J ug/kg 1 09/16/10 19:12 606-20-209/10/10 09:30388 81.1Di-n-octylphthalate ND ug/kg 1 09/16/10 19:12 117-84-009/10/10 09:30388 81.1bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/16/10 19:12 117-81-709/10/10 09:30388 106Fluoranthene ND ug/kg 1 09/16/10 19:12 206-44-009/10/10 09:30388 56.4Fluorene ND ug/kg 1 09/16/10 19:12 86-73-709/10/10 09:30388 79.9Hexachloro-1,3-butadiene ND ug/kg 1 09/16/10 19:12 87-68-309/10/10 09:30388 67.0Hexachlorobenzene ND ug/kg 1 09/16/10 19:12 118-74-109/10/10 09:30388 49.3Hexachlorocyclopentadiene ND ug/kg 1 09/16/10 19:12 77-47-409/10/10 09:30388 71.7Hexachloroethane ND ug/kg 1 09/16/10 19:12 67-72-109/10/10 09:30388 102



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(828)254-7176

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Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/16/10 19:12 193-39-509/10/10 09:30388 79.9Isophorone ND ug/kg 1 09/16/10 19:12 78-59-109/10/10 09:30388 86.92-Methylnaphthalene ND ug/kg 1 09/16/10 19:12 91-57-609/10/10 09:30388 83.42-Methylphenol(o-Cresol) ND ug/kg 1 09/16/10 19:12 95-48-709/10/10 09:30388 1173&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/16/10 19:1209/10/10 09:30388 153Naphthalene ND ug/kg 1 09/16/10 19:12 91-20-309/10/10 09:30388 95.12-Nitroaniline ND ug/kg 1 09/16/10 19:12 88-74-409/10/10 09:301940 1203-Nitroaniline ND ug/kg 1 09/16/10 19:12 99-09-209/10/10 09:301940 1064-Nitroaniline ND ug/kg 1 09/16/10 19:12 100-01-609/10/10 09:30775 109Nitrobenzene ND ug/kg 1 09/16/10 19:12 98-95-309/10/10 09:30388 1062-Nitrophenol ND ug/kg 1 09/16/10 19:12 88-75-509/10/10 09:30388 94.04-Nitrophenol ND ug/kg 1 09/16/10 19:12 100-02-709/10/10 09:301940 69.3N-Nitroso-di-n-propylamine ND ug/kg 1 09/16/10 19:12 621-64-709/10/10 09:30388 74.0N-Nitrosodiphenylamine ND ug/kg 1 09/16/10 19:12 86-30-609/10/10 09:30388 115Pentachlorophenol ND ug/kg 1 09/16/10 19:12 87-86-509/10/10 09:301940 70.5Phenanthrene ND ug/kg 1 09/16/10 19:12 85-01-809/10/10 09:30388 64.6Phenol ND ug/kg 1 09/16/10 19:12 108-95-209/10/10 09:30388 116Pyrene ND ug/kg 1 09/16/10 19:12 129-00-009/10/10 09:30388 65.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/16/10 19:12 95-94-309/10/10 09:30388 1412,3,4,6-Tetrachlorophenol ND ug/kg 1 09/16/10 19:12 58-90-209/10/10 09:30388 1532,4,5-Trichlorophenol ND ug/kg 1 09/16/10 19:12 95-95-409/10/10 09:30388 1202,4,6-Trichlorophenol ND ug/kg 1 09/16/10 19:12 88-06-209/10/10 09:30388 85.72-Fluorobiphenyl (S) 62 % 1 09/16/10 19:12 321-60-809/10/10 09:3030-110Terphenyl-d14 (S) 68 % 1 09/16/10 19:12 1718-51-009/10/10 09:3028-110Phenol-d6 (S) 48 % 1 09/16/10 19:12 13127-88-309/10/10 09:3022-1102-Fluorophenol (S) 49 % 1 09/16/10 19:12 367-12-409/10/10 09:3013-1102,4,6-Tribromophenol (S) 80 % 1 09/16/10 19:12 118-79-609/10/10 09:3027-110Nitrobenzene-d5 (S) 55 % 1 09/16/10 19:12 4165-60-009/10/10 09:3023-110





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acetone 57.7J ug/kg 1 09/05/10 16:19 67-64-196.5 9.7Benzene ND ug/kg 1 09/05/10 16:19 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/05/10 16:19 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/05/10 16:19 75-27-44.8 1.8Bromoform ND ug/kg 1 09/05/10 16:19 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/05/10 16:19 74-83-99.7 2.42-Butanone (MEK) ND ug/kg 1 09/05/10 16:19 78-93-396.5 2.8Carbon disulfide ND ug/kg 1 09/05/10 16:19 75-15-09.7 2.9Carbon tetrachloride ND ug/kg 1 09/05/10 16:19 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/05/10 16:19 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/05/10 16:19 75-00-39.7 2.3Chloroform ND ug/kg 1 09/05/10 16:19 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/05/10 16:19 74-87-39.7 2.3Cyclohexane ND ug/kg 1 09/05/10 16:19 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/05/10 16:19 96-12-84.8 3.5Dibromochloromethane ND ug/kg 1 09/05/10 16:19 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/05/10 16:19 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/05/10 16:19 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/05/10 16:19 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/05/10 16:19 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/05/10 16:19 75-71-89.7 3.51,1-Dichloroethane ND ug/kg 1 09/05/10 16:19 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/05/10 16:19 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/05/10 16:19 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/05/10 16:19 156-59-24.8 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/05/10 16:19 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/05/10 16:19 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/05/10 16:19 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/05/10 16:19 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/05/10 16:19 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/05/10 16:19 591-78-648.3 3.8Isopropylbenzene (Cumene) ND ug/kg 1 09/05/10 16:19 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/05/10 16:19 79-20-99.7 1.4Methylcyclohexane ND ug/kg 1 09/05/10 16:19 108-87-29.7 1.4Methylene Chloride ND ug/kg 1 09/05/10 16:19 75-09-219.3 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/05/10 16:19 108-10-148.3 3.6Methyl-tert-butyl ether ND ug/kg 1 09/05/10 16:19 1634-04-44.8 1.4Styrene ND ug/kg 1 09/05/10 16:19 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/05/10 16:19 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/05/10 16:19 127-18-44.8 1.6Toluene ND ug/kg 1 09/05/10 16:19 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/05/10 16:19 87-61-64.8 2.11,2,4-Trichlorobenzene ND ug/kg 1 09/05/10 16:19 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/05/10 16:19 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/05/10 16:19 79-00-54.8 2.0



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Trichloroethene 4.0J ug/kg 1 09/05/10 16:19 79-01-64.8 2.0Trichlorofluoromethane ND ug/kg 1 09/05/10 16:19 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/05/10 16:19 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/05/10 16:19 75-01-49.7 1.7Xylene (Total) ND ug/kg 1 09/05/10 16:19 1330-20-79.7 3.5m&p-Xylene ND ug/kg 1 09/05/10 16:19 179601-23-19.7 3.5o-Xylene ND ug/kg 1 09/05/10 16:19 95-47-64.8 1.8Dibromofluoromethane (S) 101 % 1 09/05/10 16:19 1868-53-770-130Toluene-d8 (S) 99 % 1 09/05/10 16:19 2037-26-570-1304-Bromofluorobenzene (S) 95 % 1 09/05/10 16:19 460-00-470-1301,2-Dichloroethane-d4 (S) 106 % 1 09/05/10 16:19 17060-07-070-132





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony 0.66 mg/kg 1 09/10/10 15:35 7440-36-009/07/10 15:200.51 0.29Arsenic ND mg/kg 1 09/10/10 15:35 7440-38-209/07/10 15:200.51 0.33Beryllium 0.60 mg/kg 1 09/10/10 15:35 7440-41-709/07/10 15:200.10 0.021Cadmium 0.40 mg/kg 1 09/10/10 15:35 7440-43-909/07/10 15:200.10 0.062Chromium 9.6 mg/kg 1 09/10/10 15:35 7440-47-309/07/10 15:200.51 0.031Copper 7.2 mg/kg 1 09/10/10 15:35 7440-50-809/07/10 15:200.51 0.041Lead 16.1 mg/kg 1 09/10/10 15:35 7439-92-109/07/10 15:200.51 0.49Manganese 232 mg/kg 1 09/10/10 15:35 7439-96-509/07/10 15:200.51 0.031Nickel 5.7 mg/kg 1 09/10/10 15:35 7440-02-009/07/10 15:200.51 0.18Selenium 0.46J mg/kg 1 09/10/10 15:35 7782-49-209/07/10 15:201.0 0.39Silver ND mg/kg 1 09/10/10 15:35 7440-22-409/07/10 15:200.51 0.031Thallium 0.58J mg/kg 1 09/10/10 15:35 7440-28-009/07/10 15:201.0 0.27Zinc 21.9 mg/kg 1 09/10/10 15:35 7440-66-609/07/10 15:201.0 0.27


Mercury 0.025 mg/kg 1 09/03/10 18:11 7439-97-609/01/10 02:500.0048 0.000096





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9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 60 % 1 09/16/10 19:49 4165-60-009/10/10 09:3023-110


Acetone 11.1J ug/kg 1 09/07/10 18:30 67-64-1101 10.1Benzene ND ug/kg 1 09/07/10 18:30 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/07/10 18:30 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/07/10 18:30 75-27-45.0 1.9Bromoform ND ug/kg 1 09/07/10 18:30 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/07/10 18:30 74-83-910.1 2.52-Butanone (MEK) ND ug/kg 1 09/07/10 18:30 78-93-3101 2.9Carbon disulfide ND ug/kg 1 09/07/10 18:30 75-15-010.1 3.0Carbon tetrachloride ND ug/kg 1 09/07/10 18:30 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/07/10 18:30 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/07/10 18:30 75-00-310.1 2.4Chloroform ND ug/kg 1 09/07/10 18:30 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/07/10 18:30 74-87-310.1 2.4Cyclohexane ND ug/kg 1 09/07/10 18:30 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 18:30 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/07/10 18:30 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 18:30 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 18:30 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/07/10 18:30 75-71-810.1 3.61,1-Dichloroethane ND ug/kg 1 09/07/10 18:30 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/07/10 18:30 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/07/10 18:30 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 18:30 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 18:30 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/07/10 18:30 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 18:30 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 18:30 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/07/10 18:30 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/07/10 18:30 591-78-650.4 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 18:30 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/07/10 18:30 79-20-910.1 1.4Methylcyclohexane ND ug/kg 1 09/07/10 18:30 108-87-210.1 1.5Methylene Chloride 10.9J ug/kg 1 09/07/10 18:30 75-09-220.2 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 18:30 108-10-150.4 3.7Methyl-tert-butyl ether ND ug/kg 1 09/07/10 18:30 1634-04-45.0 1.5Styrene ND ug/kg 1 09/07/10 18:30 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 18:30 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/07/10 18:30 127-18-45.0 1.7Toluene ND ug/kg 1 09/07/10 18:30 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 18:30 87-61-65.0 2.2



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(828)254-7176

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Cyanide ND mg/kg 1 09/05/10 13:43 57-12-50.16 0.16





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(828)254-7176

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Antimony ND mg/kg 1 09/10/10 15:38 7440-36-009/07/10 15:200.51 0.29Arsenic ND mg/kg 1 09/10/10 15:38 7440-38-209/07/10 15:200.51 0.33Beryllium 0.93 mg/kg 1 09/10/10 15:38 7440-41-709/07/10 15:200.10 0.020Cadmium 0.16 mg/kg 1 09/10/10 15:38 7440-43-909/07/10 15:200.10 0.061Chromium 6.4 mg/kg 1 09/10/10 15:38 7440-47-309/07/10 15:200.51 0.031Copper 4.5 mg/kg 1 09/10/10 15:38 7440-50-809/07/10 15:200.51 0.041Lead 5.9 mg/kg 1 09/10/10 15:38 7439-92-109/07/10 15:200.51 0.49Manganese 2160 mg/kg 10 09/13/10 15:22 7439-96-509/07/10 15:205.1 0.31Nickel 8.1 mg/kg 1 09/10/10 15:38 7440-02-009/07/10 15:200.51 0.18Selenium 0.41J mg/kg 1 09/10/10 15:38 7782-49-209/07/10 15:201.0 0.39Silver ND mg/kg 1 09/10/10 15:38 7440-22-409/07/10 15:200.51 0.031Thallium ND mg/kg 1 09/10/10 15:38 7440-28-009/07/10 15:201.0 0.27Zinc 19.1 mg/kg 1 09/10/10 15:38 7440-66-609/07/10 15:201.0 0.27


Mercury 0.025 mg/kg 1 09/03/10 18:13 7439-97-609/01/10 02:500.0049 0.000099





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(828)254-7176

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9276750MILLS GAP 6686081744







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(704)875-9092


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(828)254-7176

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Nitrobenzene-d5 (S) 42 % 1 09/16/10 22:28 4165-60-009/10/10 09:3023-110





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(828)254-7176

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Cyanide ND mg/kg 1 09/05/10 13:47 57-12-50.13 0.13





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(828)254-7176

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9276750MILLS GAP 6686081744




Antimony ND mg/kg 1 09/10/10 15:42 7440-36-009/07/10 15:200.59 0.33Arsenic ND mg/kg 1 09/10/10 15:42 7440-38-209/07/10 15:200.59 0.38Beryllium 0.61 mg/kg 1 09/10/10 15:42 7440-41-709/07/10 15:200.12 0.024Cadmium 0.21 mg/kg 1 09/10/10 15:42 7440-43-909/07/10 15:200.12 0.071Chromium 16.8 mg/kg 1 09/10/10 15:42 7440-47-309/07/10 15:200.59 0.036Copper 15.6 mg/kg 1 09/10/10 15:42 7440-50-809/07/10 15:200.59 0.047Lead 19.2 mg/kg 1 09/10/10 15:42 7439-92-109/07/10 15:200.59 0.57Manganese 307 mg/kg 1 09/10/10 15:42 7439-96-509/07/10 15:200.59 0.036Nickel 7.4 mg/kg 1 09/10/10 15:42 7440-02-009/07/10 15:200.59 0.21Selenium 0.74J mg/kg 1 09/10/10 15:42 7782-49-209/07/10 15:201.2 0.45Silver ND mg/kg 1 09/10/10 15:42 7440-22-409/07/10 15:200.59 0.036Thallium ND mg/kg 1 09/10/10 15:42 7440-28-009/07/10 15:201.2 0.31Zinc 23.8 mg/kg 1 09/10/10 15:42 7440-66-609/07/10 15:201.2 0.31


Mercury 0.028 mg/kg 1 09/03/10 18:16 7439-97-609/01/10 02:500.0050 0.000099





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(828)254-7176

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9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/16/10 23:04 91-94-109/10/10 09:302070 90.42,4-Dichlorophenol ND ug/kg 1 09/16/10 23:04 120-83-209/10/10 09:30414 90.4Diethylphthalate ND ug/kg 1 09/16/10 23:04 84-66-209/10/10 09:30414 64.02,4-Dimethylphenol ND ug/kg 1 09/16/10 23:04 105-67-909/10/10 09:30414 163Dimethylphthalate ND ug/kg 1 09/16/10 23:04 131-11-309/10/10 09:30414 84.1Di-n-butylphthalate ND ug/kg 1 09/16/10 23:04 84-74-209/10/10 09:30414 67.84,6-Dinitro-2-methylphenol ND ug/kg 1 09/16/10 23:04 534-52-109/10/10 09:30828 82.82,4-Dinitrophenol ND ug/kg 1 09/16/10 23:04 51-28-509/10/10 09:302070 67.82,4-Dinitrotoluene ND ug/kg 1 09/16/10 23:04 121-14-209/10/10 09:30414 77.82,6-Dinitrotoluene ND ug/kg 1 09/16/10 23:04 606-20-209/10/10 09:30414 86.6Di-n-octylphthalate ND ug/kg 1 09/16/10 23:04 117-84-009/10/10 09:30414 86.6bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/16/10 23:04 117-81-709/10/10 09:30414 113Fluoranthene ND ug/kg 1 09/16/10 23:04 206-44-009/10/10 09:30414 60.2Fluorene ND ug/kg 1 09/16/10 23:04 86-73-709/10/10 09:30414 85.4Hexachloro-1,3-butadiene ND ug/kg 1 09/16/10 23:04 87-68-309/10/10 09:30414 71.5Hexachlorobenzene ND ug/kg 1 09/16/10 23:04 118-74-109/10/10 09:30414 52.7Hexachlorocyclopentadiene ND ug/kg 1 09/16/10 23:04 77-47-409/10/10 09:30414 76.6Hexachloroethane ND ug/kg 1 09/16/10 23:04 67-72-109/10/10 09:30414 109Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/16/10 23:04 193-39-509/10/10 09:30414 85.4Isophorone ND ug/kg 1 09/16/10 23:04 78-59-109/10/10 09:30414 92.92-Methylnaphthalene ND ug/kg 1 09/16/10 23:04 91-57-609/10/10 09:30414 89.12-Methylphenol(o-Cresol) ND ug/kg 1 09/16/10 23:04 95-48-709/10/10 09:30414 1263&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/16/10 23:0409/10/10 09:30414 163Naphthalene ND ug/kg 1 09/16/10 23:04 91-20-309/10/10 09:30414 1022-Nitroaniline ND ug/kg 1 09/16/10 23:04 88-74-409/10/10 09:302070 1283-Nitroaniline ND ug/kg 1 09/16/10 23:04 99-09-209/10/10 09:302070 1134-Nitroaniline ND ug/kg 1 09/16/10 23:04 100-01-609/10/10 09:30828 117Nitrobenzene ND ug/kg 1 09/16/10 23:04 98-95-309/10/10 09:30414 1132-Nitrophenol ND ug/kg 1 09/16/10 23:04 88-75-509/10/10 09:30414 1004-Nitrophenol ND ug/kg 1 09/16/10 23:04 100-02-709/10/10 09:302070 74.1N-Nitroso-di-n-propylamine ND ug/kg 1 09/16/10 23:04 621-64-709/10/10 09:30414 79.1N-Nitrosodiphenylamine ND ug/kg 1 09/16/10 23:04 86-30-609/10/10 09:30414 123Pentachlorophenol ND ug/kg 1 09/16/10 23:04 87-86-509/10/10 09:302070 75.3Phenanthrene ND ug/kg 1 09/16/10 23:04 85-01-809/10/10 09:30414 69.0Phenol ND ug/kg 1 09/16/10 23:04 108-95-209/10/10 09:30414 124Pyrene ND ug/kg 1 09/16/10 23:04 129-00-009/10/10 09:30414 70.31,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/16/10 23:04 95-94-309/10/10 09:30414 1512,3,4,6-Tetrachlorophenol ND ug/kg 1 09/16/10 23:04 58-90-209/10/10 09:30414 1632,4,5-Trichlorophenol ND ug/kg 1 09/16/10 23:04 95-95-409/10/10 09:30414 1282,4,6-Trichlorophenol ND ug/kg 1 09/16/10 23:04 88-06-209/10/10 09:30414 91.62-Fluorobiphenyl (S) 55 % 1 09/16/10 23:04 321-60-809/10/10 09:3030-110Terphenyl-d14 (S) 68 % 1 09/16/10 23:04 1718-51-009/10/10 09:3028-110Phenol-d6 (S) 44 % 1 09/16/10 23:04 13127-88-309/10/10 09:3022-1102-Fluorophenol (S) 45 % 1 09/16/10 23:04 367-12-409/10/10 09:3013-1102,4,6-Tribromophenol (S) 75 % 1 09/16/10 23:04 118-79-609/10/10 09:3027-110



Date: 09/27/2010 06:23 PM Page 91 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 50 % 1 09/16/10 23:04 4165-60-009/10/10 09:3023-110


Acetone 47.7J ug/kg 1 09/07/10 19:07 67-64-194.1 9.4Benzene ND ug/kg 1 09/07/10 19:07 71-43-24.7 1.5Bromochloromethane ND ug/kg 1 09/07/10 19:07 74-97-54.7 1.6Bromodichloromethane ND ug/kg 1 09/07/10 19:07 75-27-44.7 1.8Bromoform ND ug/kg 1 09/07/10 19:07 75-25-24.7 2.2Bromomethane ND ug/kg 1 09/07/10 19:07 74-83-99.4 2.42-Butanone (MEK) ND ug/kg 1 09/07/10 19:07 78-93-394.1 2.7Carbon disulfide ND ug/kg 1 09/07/10 19:07 75-15-09.4 2.8Carbon tetrachloride ND ug/kg 1 09/07/10 19:07 56-23-54.7 2.4Chlorobenzene ND ug/kg 1 09/07/10 19:07 108-90-74.7 1.8Chloroethane ND ug/kg 1 09/07/10 19:07 75-00-39.4 2.3Chloroform ND ug/kg 1 09/07/10 19:07 67-66-34.7 1.5Chloromethane ND ug/kg 1 09/07/10 19:07 74-87-39.4 2.3Cyclohexane ND ug/kg 1 09/07/10 19:07 110-82-74.7 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 19:07 96-12-84.7 3.4Dibromochloromethane ND ug/kg 1 09/07/10 19:07 124-48-14.7 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 19:07 106-93-44.7 1.71,2-Dichlorobenzene ND ug/kg 1 09/07/10 19:07 95-50-14.7 1.81,3-Dichlorobenzene ND ug/kg 1 09/07/10 19:07 541-73-14.7 1.91,4-Dichlorobenzene ND ug/kg 1 09/07/10 19:07 106-46-74.7 1.6Dichlorodifluoromethane ND ug/kg 1 09/07/10 19:07 75-71-89.4 3.41,1-Dichloroethane ND ug/kg 1 09/07/10 19:07 75-34-34.7 1.41,2-Dichloroethane ND ug/kg 1 09/07/10 19:07 107-06-24.7 2.11,1-Dichloroethene ND ug/kg 1 09/07/10 19:07 75-35-44.7 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 19:07 156-59-24.7 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 19:07 156-60-54.7 1.81,2-Dichloropropane ND ug/kg 1 09/07/10 19:07 78-87-54.7 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 19:07 10061-01-54.7 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 19:07 10061-02-64.7 1.4Ethylbenzene ND ug/kg 1 09/07/10 19:07 100-41-44.7 1.72-Hexanone ND ug/kg 1 09/07/10 19:07 591-78-647.0 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 19:07 98-82-84.7 1.8Methyl acetate 7.4J ug/kg 1 09/07/10 19:07 79-20-99.4 1.3Methylcyclohexane ND ug/kg 1 09/07/10 19:07 108-87-29.4 1.4Methylene Chloride 10.1J ug/kg 1 09/07/10 19:07 75-09-218.8 2.84-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 19:07 108-10-147.0 3.5Methyl-tert-butyl ether ND ug/kg 1 09/07/10 19:07 1634-04-44.7 1.4Styrene ND ug/kg 1 09/07/10 19:07 100-42-54.7 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 19:07 79-34-54.7 1.8Tetrachloroethene ND ug/kg 1 09/07/10 19:07 127-18-44.7 1.6Toluene ND ug/kg 1 09/07/10 19:07 108-88-34.7 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 19:07 87-61-64.7 2.1



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:48 57-12-50.18 0.18





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/13/10 15:59 7440-36-0 D309/07/10 15:203.3 1.8Arsenic ND mg/kg 10 09/13/10 15:59 7440-38-2 D309/07/10 15:203.3 2.1Beryllium 0.94 mg/kg 10 09/13/10 15:59 7440-41-7 D309/07/10 15:200.65 0.13Cadmium ND mg/kg 10 09/13/10 15:59 7440-43-9 D309/07/10 15:200.65 0.39Chromium 16.8 mg/kg 10 09/13/10 15:59 7440-47-3 D309/07/10 15:203.3 0.20Copper 4.5 mg/kg 10 09/13/10 15:59 7440-50-8 D309/07/10 15:203.3 0.26Lead 5.1 mg/kg 10 09/13/10 15:59 7439-92-1 D309/07/10 15:203.3 3.1Manganese 133 mg/kg 10 09/13/10 15:59 7439-96-5 D309/07/10 15:203.3 0.20Nickel 7.5 mg/kg 10 09/13/10 15:59 7440-02-0 D309/07/10 15:203.3 1.2Selenium ND mg/kg 10 09/13/10 15:59 7782-49-2 D309/07/10 15:206.5 2.5Silver ND mg/kg 10 09/13/10 15:59 7440-22-4 D309/07/10 15:203.3 0.20Thallium ND mg/kg 10 09/13/10 15:59 7440-28-0 D309/07/10 15:206.5 1.7Zinc 38.9 mg/kg 10 09/13/10 15:59 7440-66-6 D309/07/10 15:206.5 1.7


Mercury 0.038 mg/kg 1 09/03/10 18:18 7439-97-609/01/10 02:500.0046 0.000092





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 95 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 64 % 1 09/16/10 23:40 4165-60-009/10/10 09:3023-110


Acetone 101 ug/kg 1 09/07/10 19:26 67-64-1 C998.5 9.8Benzene ND ug/kg 1 09/07/10 19:26 71-43-24.9 1.6Bromochloromethane ND ug/kg 1 09/07/10 19:26 74-97-54.9 1.7Bromodichloromethane ND ug/kg 1 09/07/10 19:26 75-27-44.9 1.9Bromoform ND ug/kg 1 09/07/10 19:26 75-25-24.9 2.3Bromomethane ND ug/kg 1 09/07/10 19:26 74-83-99.8 2.52-Butanone (MEK) ND ug/kg 1 09/07/10 19:26 78-93-398.5 2.9Carbon disulfide ND ug/kg 1 09/07/10 19:26 75-15-09.8 3.0Carbon tetrachloride ND ug/kg 1 09/07/10 19:26 56-23-54.9 2.6Chlorobenzene ND ug/kg 1 09/07/10 19:26 108-90-74.9 1.9Chloroethane ND ug/kg 1 09/07/10 19:26 75-00-39.8 2.4Chloroform ND ug/kg 1 09/07/10 19:26 67-66-34.9 1.6Chloromethane ND ug/kg 1 09/07/10 19:26 74-87-39.8 2.4Cyclohexane ND ug/kg 1 09/07/10 19:26 110-82-74.9 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 19:26 96-12-84.9 3.5Dibromochloromethane ND ug/kg 1 09/07/10 19:26 124-48-14.9 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 19:26 106-93-44.9 1.81,2-Dichlorobenzene ND ug/kg 1 09/07/10 19:26 95-50-14.9 1.91,3-Dichlorobenzene ND ug/kg 1 09/07/10 19:26 541-73-14.9 2.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 19:26 106-46-74.9 1.7Dichlorodifluoromethane ND ug/kg 1 09/07/10 19:26 75-71-89.8 3.51,1-Dichloroethane ND ug/kg 1 09/07/10 19:26 75-34-34.9 1.51,2-Dichloroethane ND ug/kg 1 09/07/10 19:26 107-06-24.9 2.21,1-Dichloroethene ND ug/kg 1 09/07/10 19:26 75-35-44.9 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 19:26 156-59-24.9 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 19:26 156-60-54.9 1.91,2-Dichloropropane ND ug/kg 1 09/07/10 19:26 78-87-54.9 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 19:26 10061-01-54.9 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 19:26 10061-02-64.9 1.5Ethylbenzene ND ug/kg 1 09/07/10 19:26 100-41-44.9 1.82-Hexanone ND ug/kg 1 09/07/10 19:26 591-78-649.2 3.8Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 19:26 98-82-84.9 1.9Methyl acetate ND ug/kg 1 09/07/10 19:26 79-20-99.8 1.4Methylcyclohexane ND ug/kg 1 09/07/10 19:26 108-87-29.8 1.5Methylene Chloride 16.2J ug/kg 1 09/07/10 19:26 75-09-219.7 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 19:26 108-10-149.2 3.6Methyl-tert-butyl ether ND ug/kg 1 09/07/10 19:26 1634-04-44.9 1.5Styrene ND ug/kg 1 09/07/10 19:26 100-42-54.9 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 19:26 79-34-54.9 1.9Tetrachloroethene ND ug/kg 1 09/07/10 19:26 127-18-44.9 1.7Toluene ND ug/kg 1 09/07/10 19:26 108-88-34.9 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 19:26 87-61-64.9 2.2



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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:49 57-12-50.099 0.099





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(704)875-9092


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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/13/10 16:02 7440-36-0 D309/07/10 15:205.5 3.1Arsenic ND mg/kg 10 09/13/10 16:02 7440-38-2 D309/07/10 15:205.5 3.5Beryllium 1.5 mg/kg 10 09/13/10 16:02 7440-41-7 D309/07/10 15:201.1 0.22Cadmium ND mg/kg 10 09/13/10 16:02 7440-43-9 D309/07/10 15:201.1 0.66Chromium 19.0 mg/kg 10 09/13/10 16:02 7440-47-3 D309/07/10 15:205.5 0.33Copper 0.62J mg/kg 10 09/13/10 16:02 7440-50-8 D309/07/10 15:205.5 0.44Lead ND mg/kg 10 09/13/10 16:02 7439-92-1 D309/07/10 15:205.5 5.3Manganese 355 mg/kg 10 09/13/10 16:02 7439-96-5 D309/07/10 15:205.5 0.33Nickel 11.6 mg/kg 10 09/13/10 16:02 7440-02-0 D309/07/10 15:205.5 2.0Selenium ND mg/kg 10 09/13/10 16:02 7782-49-2 D309/07/10 15:2011.0 4.2Silver ND mg/kg 10 09/13/10 16:02 7440-22-4 D309/07/10 15:205.5 0.33Thallium ND mg/kg 10 09/13/10 16:02 7440-28-0 D309/07/10 15:2011.0 2.9Zinc 61.3 mg/kg 10 09/13/10 16:02 7440-66-6 D309/07/10 15:2011.0 2.9


Mercury 0.00080J mg/kg 1 09/07/10 16:39 7439-97-609/02/10 19:200.0046 0.000091





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Nitrobenzene-d5 (S) 43 % 1 09/17/10 00:16 4165-60-009/10/10 09:3023-110





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Cyanide ND mg/kg 1 09/05/10 13:50 57-12-50.24 0.24





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Sample: SS-109C Lab ID: 9276750018 Collected: 08/31/10 17:15 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis



Antimony ND mg/kg 10 09/15/10 16:21 7440-36-0 D309/08/10 15:403.8 2.1Arsenic ND mg/kg 10 09/15/10 16:21 7440-38-2 D309/08/10 15:403.8 2.5Beryllium 1.5 mg/kg 10 09/15/10 16:21 7440-41-709/08/10 15:400.77 0.15Cadmium ND mg/kg 10 09/15/10 16:21 7440-43-9 D309/08/10 15:400.77 0.46Chromium 16.2 mg/kg 10 09/15/10 16:21 7440-47-309/08/10 15:403.8 0.23Copper 8.1 mg/kg 10 09/15/10 16:21 7440-50-809/08/10 15:403.8 0.31Lead ND mg/kg 10 09/15/10 16:21 7439-92-1 D309/08/10 15:403.8 3.7Manganese 264 mg/kg 10 09/15/10 16:21 7439-96-509/08/10 15:403.8 0.23Nickel 7.0 mg/kg 10 09/15/10 16:21 7440-02-009/08/10 15:403.8 1.4Selenium ND mg/kg 10 09/15/10 16:21 7782-49-2 D309/08/10 15:407.7 2.9Silver ND mg/kg 10 09/15/10 16:21 7440-22-4 D309/08/10 15:403.8 0.23Thallium ND mg/kg 10 09/15/10 16:21 7440-28-0 D309/08/10 15:407.7 2.0Zinc 49.1 mg/kg 10 09/15/10 16:21 7440-66-609/08/10 15:407.7 2.0


Mercury 0.00041J mg/kg 1 09/07/10 16:41 7439-97-609/02/10 19:200.0043 0.000085





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Nitrobenzene-d5 (S) 27 % 1 09/23/10 15:29 4165-60-009/10/10 09:3023-110


Acetone ND ug/kg 1 09/07/10 20:03 67-64-1101 10.1Benzene ND ug/kg 1 09/07/10 20:03 71-43-25.1 1.6Bromochloromethane ND ug/kg 1 09/07/10 20:03 74-97-55.1 1.7Bromodichloromethane ND ug/kg 1 09/07/10 20:03 75-27-45.1 1.9Bromoform ND ug/kg 1 09/07/10 20:03 75-25-25.1 2.3Bromomethane ND ug/kg 1 09/07/10 20:03 74-83-910.1 2.52-Butanone (MEK) ND ug/kg 1 09/07/10 20:03 78-93-3101 2.9Carbon disulfide ND ug/kg 1 09/07/10 20:03 75-15-010.1 3.0Carbon tetrachloride ND ug/kg 1 09/07/10 20:03 56-23-55.1 2.6Chlorobenzene ND ug/kg 1 09/07/10 20:03 108-90-75.1 1.9Chloroethane ND ug/kg 1 09/07/10 20:03 75-00-310.1 2.4Chloroform ND ug/kg 1 09/07/10 20:03 67-66-35.1 1.6Chloromethane ND ug/kg 1 09/07/10 20:03 74-87-310.1 2.4Cyclohexane ND ug/kg 1 09/07/10 20:03 110-82-75.1 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 20:03 96-12-85.1 3.6Dibromochloromethane ND ug/kg 1 09/07/10 20:03 124-48-15.1 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 20:03 106-93-45.1 1.81,2-Dichlorobenzene ND ug/kg 1 09/07/10 20:03 95-50-15.1 1.91,3-Dichlorobenzene ND ug/kg 1 09/07/10 20:03 541-73-15.1 2.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 20:03 106-46-75.1 1.7Dichlorodifluoromethane ND ug/kg 1 09/07/10 20:03 75-71-810.1 3.61,1-Dichloroethane ND ug/kg 1 09/07/10 20:03 75-34-35.1 1.51,2-Dichloroethane ND ug/kg 1 09/07/10 20:03 107-06-25.1 2.21,1-Dichloroethene ND ug/kg 1 09/07/10 20:03 75-35-45.1 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:03 156-59-25.1 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:03 156-60-55.1 1.91,2-Dichloropropane ND ug/kg 1 09/07/10 20:03 78-87-55.1 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:03 10061-01-55.1 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:03 10061-02-65.1 1.5Ethylbenzene ND ug/kg 1 09/07/10 20:03 100-41-45.1 1.82-Hexanone ND ug/kg 1 09/07/10 20:03 591-78-650.6 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 20:03 98-82-85.1 1.9Methyl acetate ND ug/kg 1 09/07/10 20:03 79-20-910.1 1.4Methylcyclohexane ND ug/kg 1 09/07/10 20:03 108-87-210.1 1.5Methylene Chloride 23.9 ug/kg 1 09/07/10 20:03 75-09-2 C920.2 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 20:03 108-10-150.6 3.7Methyl-tert-butyl ether ND ug/kg 1 09/07/10 20:03 1634-04-45.1 1.5Styrene ND ug/kg 1 09/07/10 20:03 100-42-55.1 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 20:03 79-34-55.1 1.9Tetrachloroethene ND ug/kg 1 09/07/10 20:03 127-18-45.1 1.7Toluene ND ug/kg 1 09/07/10 20:03 108-88-35.1 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 20:03 87-61-65.1 2.2



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Cyanide ND mg/kg 1 09/05/10 13:50 57-12-50.17 0.17





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(828)254-7176

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9276750MILLS GAP 6686081744

Sample: SS-109D Lab ID: 9276750019 Collected: 08/31/10 17:25 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis



Antimony ND mg/kg 10 09/15/10 16:25 7440-36-0 D309/08/10 15:403.7 2.1Arsenic ND mg/kg 10 09/15/10 16:25 7440-38-2 D309/08/10 15:403.7 2.4Beryllium 1.9 mg/kg 10 09/15/10 16:25 7440-41-709/08/10 15:400.74 0.15Cadmium ND mg/kg 10 09/15/10 16:25 7440-43-9 D309/08/10 15:400.74 0.44Chromium 17.6 mg/kg 10 09/15/10 16:25 7440-47-309/08/10 15:403.7 0.22Copper 6.8 mg/kg 10 09/15/10 16:25 7440-50-809/08/10 15:403.7 0.30Lead 6.2 mg/kg 10 09/15/10 16:25 7439-92-109/08/10 15:403.7 3.5Manganese 480 mg/kg 10 09/15/10 16:25 7439-96-509/08/10 15:403.7 0.22Nickel 14.2 mg/kg 10 09/15/10 16:25 7440-02-009/08/10 15:403.7 1.3Selenium ND mg/kg 10 09/15/10 16:25 7782-49-2 D309/08/10 15:407.4 2.8Silver ND mg/kg 10 09/15/10 16:25 7440-22-4 D309/08/10 15:403.7 0.22Thallium ND mg/kg 10 09/15/10 16:25 7440-28-0 D309/08/10 15:407.4 1.9Zinc 74.5 mg/kg 10 09/15/10 16:25 7440-66-609/08/10 15:407.4 1.9


Mercury ND mg/kg 1 09/07/10 16:44 7439-97-609/02/10 19:200.0047 0.000093





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9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 31 % 1 09/17/10 01:29 4165-60-009/10/10 09:3023-110


Acetone ND ug/kg 1 09/07/10 20:21 67-64-1100 10.0Benzene ND ug/kg 1 09/07/10 20:21 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/07/10 20:21 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/07/10 20:21 75-27-45.0 1.9Bromoform ND ug/kg 1 09/07/10 20:21 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/07/10 20:21 74-83-910.0 2.52-Butanone (MEK) ND ug/kg 1 09/07/10 20:21 78-93-3100 2.9Carbon disulfide ND ug/kg 1 09/07/10 20:21 75-15-010.0 3.0Carbon tetrachloride ND ug/kg 1 09/07/10 20:21 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/07/10 20:21 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/07/10 20:21 75-00-310.0 2.4Chloroform ND ug/kg 1 09/07/10 20:21 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/07/10 20:21 74-87-310.0 2.4Cyclohexane ND ug/kg 1 09/07/10 20:21 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 20:21 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/07/10 20:21 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 20:21 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/07/10 20:21 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/07/10 20:21 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/07/10 20:21 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/07/10 20:21 75-71-810.0 3.61,1-Dichloroethane ND ug/kg 1 09/07/10 20:21 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/07/10 20:21 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/07/10 20:21 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:21 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:21 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/07/10 20:21 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:21 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:21 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/07/10 20:21 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/07/10 20:21 591-78-650.2 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 20:21 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/07/10 20:21 79-20-910.0 1.4Methylcyclohexane ND ug/kg 1 09/07/10 20:21 108-87-210.0 1.5Methylene Chloride 25.8 ug/kg 1 09/07/10 20:21 75-09-2 C920.1 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 20:21 108-10-150.2 3.7Methyl-tert-butyl ether ND ug/kg 1 09/07/10 20:21 1634-04-45.0 1.5Styrene ND ug/kg 1 09/07/10 20:21 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 20:21 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/07/10 20:21 127-18-45.0 1.7Toluene ND ug/kg 1 09/07/10 20:21 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 20:21 87-61-65.0 2.2



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Cyanide ND mg/kg 1 09/05/10 13:52 57-12-50.13 0.13





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(704)875-9092


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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: SS-109E Lab ID: 9276750020 Collected: 08/31/10 17:30 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis





Mercury ND mg/kg 1 09/07/10 16:46 7439-97-609/02/10 19:200.0037 0.000073





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(828)254-7176

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9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/23/10 16:06 91-94-109/10/10 09:301770 77.42,4-Dichlorophenol ND ug/kg 1 09/23/10 16:06 120-83-209/10/10 09:30355 77.4Diethylphthalate ND ug/kg 1 09/23/10 16:06 84-66-209/10/10 09:30355 54.82,4-Dimethylphenol ND ug/kg 1 09/23/10 16:06 105-67-909/10/10 09:30355 140Dimethylphthalate ND ug/kg 1 09/23/10 16:06 131-11-309/10/10 09:30355 72.0Di-n-butylphthalate ND ug/kg 1 09/23/10 16:06 84-74-209/10/10 09:30355 58.04,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/10 16:06 534-52-109/10/10 09:30709 70.92,4-Dinitrophenol ND ug/kg 1 09/23/10 16:06 51-28-509/10/10 09:301770 58.02,4-Dinitrotoluene ND ug/kg 1 09/23/10 16:06 121-14-209/10/10 09:30355 66.62,6-Dinitrotoluene ND ug/kg 1 09/23/10 16:06 606-20-209/10/10 09:30355 74.2Di-n-octylphthalate ND ug/kg 1 09/23/10 16:06 117-84-009/10/10 09:30355 74.2bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/10 16:06 117-81-709/10/10 09:30355 96.7Fluoranthene ND ug/kg 1 09/23/10 16:06 206-44-009/10/10 09:30355 51.6Fluorene ND ug/kg 1 09/23/10 16:06 86-73-709/10/10 09:30355 73.1Hexachloro-1,3-butadiene ND ug/kg 1 09/23/10 16:06 87-68-309/10/10 09:30355 61.3Hexachlorobenzene ND ug/kg 1 09/23/10 16:06 118-74-109/10/10 09:30355 45.1Hexachlorocyclopentadiene ND ug/kg 1 09/23/10 16:06 77-47-409/10/10 09:30355 65.6Hexachloroethane ND ug/kg 1 09/23/10 16:06 67-72-109/10/10 09:30355 93.5Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/10 16:06 193-39-509/10/10 09:30355 73.1Isophorone ND ug/kg 1 09/23/10 16:06 78-59-109/10/10 09:30355 79.52-Methylnaphthalene ND ug/kg 1 09/23/10 16:06 91-57-609/10/10 09:30355 76.32-Methylphenol(o-Cresol) ND ug/kg 1 09/23/10 16:06 95-48-709/10/10 09:30355 1073&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/23/10 16:0609/10/10 09:30355 140Naphthalene ND ug/kg 1 09/23/10 16:06 91-20-309/10/10 09:30355 87.02-Nitroaniline ND ug/kg 1 09/23/10 16:06 88-74-409/10/10 09:301770 1103-Nitroaniline ND ug/kg 1 09/23/10 16:06 99-09-209/10/10 09:301770 96.74-Nitroaniline ND ug/kg 1 09/23/10 16:06 100-01-609/10/10 09:30709 99.9Nitrobenzene ND ug/kg 1 09/23/10 16:06 98-95-309/10/10 09:30355 96.72-Nitrophenol ND ug/kg 1 09/23/10 16:06 88-75-509/10/10 09:30355 86.04-Nitrophenol ND ug/kg 1 09/23/10 16:06 100-02-709/10/10 09:301770 63.4N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/10 16:06 621-64-709/10/10 09:30355 67.7N-Nitrosodiphenylamine ND ug/kg 1 09/23/10 16:06 86-30-609/10/10 09:30355 105Pentachlorophenol ND ug/kg 1 09/23/10 16:06 87-86-509/10/10 09:301770 64.5Phenanthrene ND ug/kg 1 09/23/10 16:06 85-01-809/10/10 09:30355 59.1Phenol ND ug/kg 1 09/23/10 16:06 108-95-209/10/10 09:30355 106Pyrene ND ug/kg 1 09/23/10 16:06 129-00-009/10/10 09:30355 60.21,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/23/10 16:06 95-94-309/10/10 09:30355 1292,3,4,6-Tetrachlorophenol ND ug/kg 1 09/23/10 16:06 58-90-209/10/10 09:30355 1402,4,5-Trichlorophenol ND ug/kg 1 09/23/10 16:06 95-95-409/10/10 09:30355 1102,4,6-Trichlorophenol ND ug/kg 1 09/23/10 16:06 88-06-209/10/10 09:30355 78.42-Fluorobiphenyl (S) 31 % 1 09/23/10 16:06 321-60-809/10/10 09:3030-110Terphenyl-d14 (S) 47 % 1 09/23/10 16:06 1718-51-009/10/10 09:3028-110Phenol-d6 (S) 18 % 1 09/23/10 16:06 13127-88-3 S009/10/10 09:3022-1102-Fluorophenol (S) 19 % 1 09/23/10 16:06 367-12-409/10/10 09:3013-1102,4,6-Tribromophenol (S) 32 % 1 09/23/10 16:06 118-79-609/10/10 09:3027-110



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(828)254-7176

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Nitrobenzene-d5 (S) 23 % 1 09/23/10 16:06 4165-60-009/10/10 09:3023-110





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:52 57-12-50.067 0.067





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 5 09/15/10 16:31 7440-36-0 D309/08/10 15:401.9 1.1Arsenic ND mg/kg 5 09/15/10 16:31 7440-38-2 D309/08/10 15:401.9 1.2Beryllium 0.84 mg/kg 5 09/15/10 16:31 7440-41-709/08/10 15:400.39 0.077Cadmium ND mg/kg 5 09/15/10 16:31 7440-43-9 D309/08/10 15:400.39 0.23Chromium 22.5 mg/kg 5 09/15/10 16:31 7440-47-309/08/10 15:401.9 0.12Copper 8.4 mg/kg 5 09/15/10 16:31 7440-50-809/08/10 15:401.9 0.15Lead 9.4 mg/kg 5 09/15/10 16:31 7439-92-109/08/10 15:401.9 1.9Manganese 160 mg/kg 5 09/15/10 16:31 7439-96-509/08/10 15:401.9 0.12Nickel 8.3 mg/kg 5 09/15/10 16:31 7440-02-009/08/10 15:401.9 0.70Selenium 2.0J mg/kg 5 09/15/10 16:31 7782-49-2 D309/08/10 15:403.9 1.5Silver ND mg/kg 5 09/15/10 16:31 7440-22-4 D309/08/10 15:401.9 0.12Thallium ND mg/kg 5 09/15/10 16:31 7440-28-0 D309/08/10 15:403.9 1.0Zinc 36.9 mg/kg 5 09/15/10 16:31 7440-66-609/08/10 15:403.9 1.0


Mercury 0.097 mg/kg 1 09/10/10 12:05 7439-97-609/08/10 10:010.0050 0.00010





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ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 02:40 91-94-109/10/10 09:301990 86.92,4-Dichlorophenol ND ug/kg 1 09/17/10 02:40 120-83-209/10/10 09:30398 86.9Diethylphthalate ND ug/kg 1 09/17/10 02:40 84-66-209/10/10 09:30398 61.52,4-Dimethylphenol ND ug/kg 1 09/17/10 02:40 105-67-909/10/10 09:30398 157Dimethylphthalate ND ug/kg 1 09/17/10 02:40 131-11-309/10/10 09:30398 80.8Di-n-butylphthalate ND ug/kg 1 09/17/10 02:40 84-74-209/10/10 09:30398 65.24,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 02:40 534-52-109/10/10 09:30796 79.62,4-Dinitrophenol ND ug/kg 1 09/17/10 02:40 51-28-509/10/10 09:301990 65.22,4-Dinitrotoluene ND ug/kg 1 09/17/10 02:40 121-14-209/10/10 09:30398 74.82,6-Dinitrotoluene 305J ug/kg 1 09/17/10 02:40 606-20-209/10/10 09:30398 83.3Di-n-octylphthalate ND ug/kg 1 09/17/10 02:40 117-84-009/10/10 09:30398 83.3bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 02:40 117-81-709/10/10 09:30398 109Fluoranthene ND ug/kg 1 09/17/10 02:40 206-44-009/10/10 09:30398 57.9Fluorene ND ug/kg 1 09/17/10 02:40 86-73-709/10/10 09:30398 82.1Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 02:40 87-68-309/10/10 09:30398 68.8Hexachlorobenzene ND ug/kg 1 09/17/10 02:40 118-74-109/10/10 09:30398 50.7Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 02:40 77-47-409/10/10 09:30398 73.6Hexachloroethane ND ug/kg 1 09/17/10 02:40 67-72-109/10/10 09:30398 105Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 02:40 193-39-509/10/10 09:30398 82.1Isophorone ND ug/kg 1 09/17/10 02:40 78-59-109/10/10 09:30398 89.32-Methylnaphthalene ND ug/kg 1 09/17/10 02:40 91-57-609/10/10 09:30398 85.72-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 02:40 95-48-709/10/10 09:30398 1213&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 02:4009/10/10 09:30398 157Naphthalene ND ug/kg 1 09/17/10 02:40 91-20-309/10/10 09:30398 97.72-Nitroaniline ND ug/kg 1 09/17/10 02:40 88-74-409/10/10 09:301990 1233-Nitroaniline ND ug/kg 1 09/17/10 02:40 99-09-209/10/10 09:301990 1094-Nitroaniline ND ug/kg 1 09/17/10 02:40 100-01-609/10/10 09:30796 112Nitrobenzene ND ug/kg 1 09/17/10 02:40 98-95-309/10/10 09:30398 1092-Nitrophenol ND ug/kg 1 09/17/10 02:40 88-75-509/10/10 09:30398 96.54-Nitrophenol ND ug/kg 1 09/17/10 02:40 100-02-709/10/10 09:301990 71.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 02:40 621-64-709/10/10 09:30398 76.0N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 02:40 86-30-609/10/10 09:30398 118Pentachlorophenol ND ug/kg 1 09/17/10 02:40 87-86-509/10/10 09:301990 72.4Phenanthrene ND ug/kg 1 09/17/10 02:40 85-01-809/10/10 09:30398 66.4Phenol ND ug/kg 1 09/17/10 02:40 108-95-209/10/10 09:30398 119Pyrene ND ug/kg 1 09/17/10 02:40 129-00-009/10/10 09:30398 67.61,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 02:40 95-94-309/10/10 09:30398 1452,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 02:40 58-90-209/10/10 09:30398 1572,4,5-Trichlorophenol ND ug/kg 1 09/17/10 02:40 95-95-409/10/10 09:30398 1232,4,6-Trichlorophenol ND ug/kg 1 09/17/10 02:40 88-06-209/10/10 09:30398 88.12-Fluorobiphenyl (S) 41 % 1 09/17/10 02:40 321-60-809/10/10 09:3030-110Terphenyl-d14 (S) 44 % 1 09/17/10 02:40 1718-51-009/10/10 09:3028-110Phenol-d6 (S) 32 % 1 09/17/10 02:40 13127-88-309/10/10 09:3022-1102-Fluorophenol (S) 31 % 1 09/17/10 02:40 367-12-409/10/10 09:3013-1102,4,6-Tribromophenol (S) 49 % 1 09/17/10 02:40 118-79-609/10/10 09:3027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 34 % 1 09/17/10 02:40 4165-60-009/10/10 09:3023-110





Date: 09/27/2010 06:23 PM Page 116 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:56 57-12-50.18 0.18





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 16:35 7440-36-0 D309/08/10 15:404.2 2.4Arsenic 3.2J mg/kg 10 09/15/10 16:35 7440-38-2 D309/08/10 15:404.2 2.7Beryllium 1.1 mg/kg 10 09/15/10 16:35 7440-41-709/08/10 15:400.84 0.17Cadmium ND mg/kg 10 09/15/10 16:35 7440-43-9 D309/08/10 15:400.84 0.51Chromium 14.9 mg/kg 10 09/15/10 16:35 7440-47-309/08/10 15:404.2 0.25Copper 5.9 mg/kg 10 09/15/10 16:35 7440-50-809/08/10 15:404.2 0.34Lead ND mg/kg 10 09/15/10 16:35 7439-92-1 D309/08/10 15:404.2 4.1Manganese 200 mg/kg 10 09/15/10 16:35 7439-96-509/08/10 15:404.2 0.25Nickel 6.9 mg/kg 10 09/15/10 16:35 7440-02-009/08/10 15:404.2 1.5Selenium ND mg/kg 10 09/15/10 16:35 7782-49-2 D309/08/10 15:408.4 3.2Silver ND mg/kg 10 09/15/10 16:35 7440-22-4 D309/08/10 15:404.2 0.25Thallium ND mg/kg 10 09/15/10 16:35 7440-28-0 D309/08/10 15:408.4 2.2Zinc 46.6 mg/kg 10 09/15/10 16:35 7440-66-609/08/10 15:408.4 2.2


Mercury 0.00092J mg/kg 1 09/07/10 16:56 7439-97-609/02/10 19:200.0040 0.000080





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 119 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 42 % 1 09/23/10 16:43 4165-60-009/10/10 09:3023-110





Date: 09/27/2010 06:23 PM Page 120 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:57 57-12-50.16 0.16





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 16:38 7440-36-0 D309/08/10 15:403.8 2.1Arsenic ND mg/kg 10 09/15/10 16:38 7440-38-2 D309/08/10 15:403.8 2.4Beryllium 1.1 mg/kg 10 09/15/10 16:38 7440-41-709/08/10 15:400.76 0.15Cadmium ND mg/kg 10 09/15/10 16:38 7440-43-9 D309/08/10 15:400.76 0.45Chromium 16.0 mg/kg 10 09/15/10 16:38 7440-47-309/08/10 15:403.8 0.23Copper 1.4J mg/kg 10 09/15/10 16:38 7440-50-8 D309/08/10 15:403.8 0.30Lead 3.6J mg/kg 10 09/15/10 16:38 7439-92-1 D309/08/10 15:403.8 3.6Manganese 278 mg/kg 10 09/15/10 16:38 7439-96-509/08/10 15:403.8 0.23Nickel 10.1 mg/kg 10 09/15/10 16:38 7440-02-009/08/10 15:403.8 1.4Selenium ND mg/kg 10 09/15/10 16:38 7782-49-2 D309/08/10 15:407.6 2.9Silver ND mg/kg 10 09/15/10 16:38 7440-22-4 D309/08/10 15:403.8 0.23Thallium ND mg/kg 10 09/15/10 16:38 7440-28-0 D309/08/10 15:407.6 2.0Zinc 51.7 mg/kg 10 09/15/10 16:38 7440-66-609/08/10 15:407.6 2.0


Mercury ND mg/kg 1 09/07/10 16:58 7439-97-609/02/10 19:200.0043 0.000086


Acenaphthene ND ug/kg 1 09/17/10 06:51 83-32-909/13/10 12:30359 82.8Acenaphthylene ND ug/kg 1 09/17/10 06:51 208-96-809/13/10 12:30359 84.9Acetophenone ND ug/kg 1 09/17/10 06:51 98-86-209/13/10 12:30359 185Anthracene ND ug/kg 1 09/17/10 06:51 120-12-709/13/10 12:30359 80.6Atrazine ND ug/kg 1 09/17/10 06:51 1912-24-909/13/10 12:30719 142Benzaldehyde ND ug/kg 1 09/17/10 06:51 100-52-709/13/10 12:30719 359Benzo(a)anthracene ND ug/kg 1 09/17/10 06:51 56-55-309/13/10 12:30359 66.4Benzo(a)pyrene ND ug/kg 1 09/17/10 06:51 50-32-809/13/10 12:30359 68.6Benzo(b)fluoranthene ND ug/kg 1 09/17/10 06:51 205-99-209/13/10 12:30359 62.1Benzo(g,h,i)perylene ND ug/kg 1 09/17/10 06:51 191-24-209/13/10 12:30359 91.5Benzo(k)fluoranthene ND ug/kg 1 09/17/10 06:51 207-08-909/13/10 12:30359 70.8Biphenyl (Diphenyl) ND ug/kg 1 09/17/10 06:51 92-52-409/13/10 12:30359 1134-Bromophenylphenyl ether ND ug/kg 1 09/17/10 06:51 101-55-309/13/10 12:30359 65.3Butylbenzylphthalate ND ug/kg 1 09/17/10 06:51 85-68-709/13/10 12:30359 76.2Caprolactam ND ug/kg 1 09/17/10 06:51 105-60-209/13/10 12:30359 62.1Carbazole ND ug/kg 1 09/17/10 06:51 86-74-809/13/10 12:30359 68.64-Chloro-3-methylphenol ND ug/kg 1 09/17/10 06:51 59-50-709/13/10 12:30719 74.14-Chloroaniline ND ug/kg 1 09/17/10 06:51 106-47-809/13/10 12:301800 100bis(2-Chloroethoxy)methane ND ug/kg 1 09/17/10 06:51 111-91-109/13/10 12:30359 83.9bis(2-Chloroethyl) ether ND ug/kg 1 09/17/10 06:51 111-44-409/13/10 12:30359 91.5bis(2-Chloroisopropyl) ether ND ug/kg 1 09/17/10 06:51 108-60-109/13/10 12:30359 95.82-Chloronaphthalene ND ug/kg 1 09/17/10 06:51 91-58-709/13/10 12:30359 70.82-Chlorophenol ND ug/kg 1 09/17/10 06:51 95-57-809/13/10 12:30359 98.04-Chlorophenylphenyl ether ND ug/kg 1 09/17/10 06:51 7005-72-309/13/10 12:30359 74.1Chrysene ND ug/kg 1 09/17/10 06:51 218-01-909/13/10 12:30359 47.9Dibenz(a,h)anthracene ND ug/kg 1 09/17/10 06:51 53-70-309/13/10 12:30359 76.2Dibenzofuran ND ug/kg 1 09/17/10 06:51 132-64-909/13/10 12:30359 58.8



Date: 09/27/2010 06:23 PM Page 122 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 06:51 91-94-109/13/10 12:301800 78.42,4-Dichlorophenol ND ug/kg 1 09/17/10 06:51 120-83-209/13/10 12:30359 78.4Diethylphthalate ND ug/kg 1 09/17/10 06:51 84-66-209/13/10 12:30359 55.52,4-Dimethylphenol ND ug/kg 1 09/17/10 06:51 105-67-909/13/10 12:30359 142Dimethylphthalate ND ug/kg 1 09/17/10 06:51 131-11-309/13/10 12:30359 73.0Di-n-butylphthalate ND ug/kg 1 09/17/10 06:51 84-74-209/13/10 12:30359 58.84,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 06:51 534-52-109/13/10 12:30719 71.92,4-Dinitrophenol ND ug/kg 1 09/17/10 06:51 51-28-509/13/10 12:301800 58.82,4-Dinitrotoluene ND ug/kg 1 09/17/10 06:51 121-14-209/13/10 12:30359 67.52,6-Dinitrotoluene ND ug/kg 1 09/17/10 06:51 606-20-209/13/10 12:30359 75.1Di-n-octylphthalate ND ug/kg 1 09/17/10 06:51 117-84-009/13/10 12:30359 75.1bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 06:51 117-81-709/13/10 12:30359 98.0Fluoranthene ND ug/kg 1 09/17/10 06:51 206-44-009/13/10 12:30359 52.3Fluorene ND ug/kg 1 09/17/10 06:51 86-73-709/13/10 12:30359 74.1Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 06:51 87-68-309/13/10 12:30359 62.1Hexachlorobenzene ND ug/kg 1 09/17/10 06:51 118-74-109/13/10 12:30359 45.7Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 06:51 77-47-409/13/10 12:30359 66.4Hexachloroethane ND ug/kg 1 09/17/10 06:51 67-72-109/13/10 12:30359 94.8Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 06:51 193-39-509/13/10 12:30359 74.1Isophorone ND ug/kg 1 09/17/10 06:51 78-59-109/13/10 12:30359 80.62-Methylnaphthalene ND ug/kg 1 09/17/10 06:51 91-57-609/13/10 12:30359 77.32-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 06:51 95-48-709/13/10 12:30359 1093&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 06:5109/13/10 12:30359 142Naphthalene ND ug/kg 1 09/17/10 06:51 91-20-309/13/10 12:30359 88.22-Nitroaniline ND ug/kg 1 09/17/10 06:51 88-74-409/13/10 12:301800 1113-Nitroaniline ND ug/kg 1 09/17/10 06:51 99-09-209/13/10 12:301800 98.04-Nitroaniline ND ug/kg 1 09/17/10 06:51 100-01-609/13/10 12:30719 101Nitrobenzene ND ug/kg 1 09/17/10 06:51 98-95-309/13/10 12:30359 98.02-Nitrophenol ND ug/kg 1 09/17/10 06:51 88-75-509/13/10 12:30359 87.14-Nitrophenol ND ug/kg 1 09/17/10 06:51 100-02-709/13/10 12:301800 64.3N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 06:51 621-64-709/13/10 12:30359 68.6N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 06:51 86-30-609/13/10 12:30359 107Pentachlorophenol ND ug/kg 1 09/17/10 06:51 87-86-509/13/10 12:301800 65.3Phenanthrene ND ug/kg 1 09/17/10 06:51 85-01-809/13/10 12:30359 59.9Phenol ND ug/kg 1 09/17/10 06:51 108-95-209/13/10 12:30359 108Pyrene ND ug/kg 1 09/17/10 06:51 129-00-009/13/10 12:30359 61.01,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 06:51 95-94-309/13/10 12:30359 1312,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 06:51 58-90-209/13/10 12:30359 1422,4,5-Trichlorophenol ND ug/kg 1 09/17/10 06:51 95-95-409/13/10 12:30359 1112,4,6-Trichlorophenol ND ug/kg 1 09/17/10 06:51 88-06-209/13/10 12:30359 79.52-Fluorobiphenyl (S) 38 % 1 09/17/10 06:51 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 55 % 1 09/17/10 06:51 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 30 % 1 09/17/10 06:51 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 31 % 1 09/17/10 06:51 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 58 % 1 09/17/10 06:51 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:23 PM Page 123 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 35 % 1 09/17/10 06:51 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 124 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:58 57-12-50.14 0.14





Date: 09/27/2010 06:23 PM Page 125 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 20 09/15/10 16:41 7440-36-0 D309/08/10 15:405.9 3.3Arsenic ND mg/kg 20 09/15/10 16:41 7440-38-2 D309/08/10 15:405.9 3.8Beryllium 1.3 mg/kg 20 09/15/10 16:41 7440-41-709/08/10 15:401.2 0.23Cadmium ND mg/kg 20 09/15/10 16:41 7440-43-9 D309/08/10 15:401.2 0.70Chromium 13.6 mg/kg 20 09/15/10 16:41 7440-47-309/08/10 15:405.9 0.35Copper 3.9J mg/kg 20 09/15/10 16:41 7440-50-8 D309/08/10 15:405.9 0.47Lead ND mg/kg 20 09/15/10 16:41 7439-92-1 D309/08/10 15:405.9 5.6Manganese 256 mg/kg 20 09/15/10 16:41 7439-96-509/08/10 15:405.9 0.35Nickel 7.6 mg/kg 20 09/15/10 16:41 7440-02-009/08/10 15:405.9 2.1Selenium ND mg/kg 20 09/15/10 16:41 7782-49-2 D309/08/10 15:4011.7 4.5Silver ND mg/kg 20 09/15/10 16:41 7440-22-4 D309/08/10 15:405.9 0.35Thallium ND mg/kg 20 09/15/10 16:41 7440-28-0 D309/08/10 15:4011.7 3.1Zinc 45.4 mg/kg 20 09/15/10 16:41 7440-66-609/08/10 15:4011.7 3.1


Mercury 0.00015J mg/kg 1 09/07/10 17:06 7439-97-609/02/10 19:200.0046 0.000093





Date: 09/27/2010 06:23 PM Page 126 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 127 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/23/10 17:22 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 128 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:59 57-12-50.17 0.17





Date: 09/27/2010 06:23 PM Page 129 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 16:58 7440-36-0 D309/08/10 15:403.9 2.2Arsenic ND mg/kg 10 09/15/10 16:58 7440-38-2 D309/08/10 15:403.9 2.5Beryllium 2.1 mg/kg 10 09/15/10 16:58 7440-41-709/08/10 15:400.79 0.16Cadmium ND mg/kg 10 09/15/10 16:58 7440-43-9 D309/08/10 15:400.79 0.47Chromium 12.9 mg/kg 10 09/15/10 16:58 7440-47-309/08/10 15:403.9 0.24Copper 30.6 mg/kg 10 09/15/10 16:58 7440-50-809/08/10 15:403.9 0.32Lead 6.8 mg/kg 10 09/15/10 16:58 7439-92-109/08/10 15:403.9 3.8Manganese 342 mg/kg 10 09/15/10 16:58 7439-96-509/08/10 15:403.9 0.24Nickel 2.8J mg/kg 10 09/15/10 16:58 7440-02-0 D309/08/10 15:403.9 1.4Selenium ND mg/kg 10 09/15/10 16:58 7782-49-2 D309/08/10 15:407.9 3.0Silver ND mg/kg 10 09/15/10 16:58 7440-22-4 D309/08/10 15:403.9 0.24Thallium ND mg/kg 10 09/15/10 16:58 7440-28-0 D309/08/10 15:407.9 2.0Zinc 54.3 mg/kg 10 09/15/10 16:58 7440-66-609/08/10 15:407.9 2.0


Mercury ND mg/kg 1 09/07/10 17:09 7439-97-609/02/10 19:200.0051 0.00010


Acenaphthene ND ug/kg 1 09/23/10 20:30 83-32-909/13/10 12:30405 93.4Acenaphthylene ND ug/kg 1 09/23/10 20:30 208-96-809/13/10 12:30405 95.8Acetophenone ND ug/kg 1 09/23/10 20:30 98-86-209/13/10 12:30405 209Anthracene ND ug/kg 1 09/23/10 20:30 120-12-709/13/10 12:30405 90.9Atrazine ND ug/kg 1 09/23/10 20:30 1912-24-909/13/10 12:30811 160Benzaldehyde ND ug/kg 1 09/23/10 20:30 100-52-709/13/10 12:30811 405Benzo(a)anthracene ND ug/kg 1 09/23/10 20:30 56-55-309/13/10 12:30405 74.9Benzo(a)pyrene ND ug/kg 1 09/23/10 20:30 50-32-809/13/10 12:30405 77.4Benzo(b)fluoranthene ND ug/kg 1 09/23/10 20:30 205-99-209/13/10 12:30405 70.0Benzo(g,h,i)perylene 154J ug/kg 1 09/23/10 20:30 191-24-209/13/10 12:30405 103Benzo(k)fluoranthene ND ug/kg 1 09/23/10 20:30 207-08-909/13/10 12:30405 79.9Biphenyl (Diphenyl) ND ug/kg 1 09/23/10 20:30 92-52-409/13/10 12:30405 1284-Bromophenylphenyl ether ND ug/kg 1 09/23/10 20:30 101-55-309/13/10 12:30405 73.7Butylbenzylphthalate ND ug/kg 1 09/23/10 20:30 85-68-709/13/10 12:30405 86.0Caprolactam ND ug/kg 1 09/23/10 20:30 105-60-209/13/10 12:30405 70.0Carbazole ND ug/kg 1 09/23/10 20:30 86-74-809/13/10 12:30405 77.44-Chloro-3-methylphenol ND ug/kg 1 09/23/10 20:30 59-50-709/13/10 12:30811 83.64-Chloroaniline ND ug/kg 1 09/23/10 20:30 106-47-809/13/10 12:302030 113bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/10 20:30 111-91-109/13/10 12:30405 94.6bis(2-Chloroethyl) ether ND ug/kg 1 09/23/10 20:30 111-44-409/13/10 12:30405 103bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/10 20:30 108-60-109/13/10 12:30405 1082-Chloronaphthalene ND ug/kg 1 09/23/10 20:30 91-58-709/13/10 12:30405 79.92-Chlorophenol ND ug/kg 1 09/23/10 20:30 95-57-809/13/10 12:30405 1114-Chlorophenylphenyl ether ND ug/kg 1 09/23/10 20:30 7005-72-309/13/10 12:30405 83.6Chrysene ND ug/kg 1 09/23/10 20:30 218-01-909/13/10 12:30405 54.1Dibenz(a,h)anthracene 159J ug/kg 1 09/23/10 20:30 53-70-309/13/10 12:30405 86.0Dibenzofuran ND ug/kg 1 09/23/10 20:30 132-64-909/13/10 12:30405 66.3



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/23/10 20:30 91-94-109/13/10 12:302030 88.52,4-Dichlorophenol ND ug/kg 1 09/23/10 20:30 120-83-209/13/10 12:30405 88.5Diethylphthalate ND ug/kg 1 09/23/10 20:30 84-66-209/13/10 12:30405 62.72,4-Dimethylphenol ND ug/kg 1 09/23/10 20:30 105-67-909/13/10 12:30405 160Dimethylphthalate ND ug/kg 1 09/23/10 20:30 131-11-309/13/10 12:30405 82.3Di-n-butylphthalate ND ug/kg 1 09/23/10 20:30 84-74-209/13/10 12:30405 66.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/10 20:30 534-52-109/13/10 12:30811 81.12,4-Dinitrophenol ND ug/kg 1 09/23/10 20:30 51-28-509/13/10 12:302030 66.32,4-Dinitrotoluene ND ug/kg 1 09/23/10 20:30 121-14-209/13/10 12:30405 76.22,6-Dinitrotoluene ND ug/kg 1 09/23/10 20:30 606-20-209/13/10 12:30405 84.8Di-n-octylphthalate ND ug/kg 1 09/23/10 20:30 117-84-009/13/10 12:30405 84.8bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/10 20:30 117-81-709/13/10 12:30405 111Fluoranthene ND ug/kg 1 09/23/10 20:30 206-44-009/13/10 12:30405 59.0Fluorene ND ug/kg 1 09/23/10 20:30 86-73-709/13/10 12:30405 83.6Hexachloro-1,3-butadiene ND ug/kg 1 09/23/10 20:30 87-68-309/13/10 12:30405 70.0Hexachlorobenzene ND ug/kg 1 09/23/10 20:30 118-74-109/13/10 12:30405 51.6Hexachlorocyclopentadiene ND ug/kg 1 09/23/10 20:30 77-47-409/13/10 12:30405 74.9Hexachloroethane ND ug/kg 1 09/23/10 20:30 67-72-109/13/10 12:30405 107Indeno(1,2,3-cd)pyrene 146J ug/kg 1 09/23/10 20:30 193-39-509/13/10 12:30405 83.6Isophorone ND ug/kg 1 09/23/10 20:30 78-59-109/13/10 12:30405 90.92-Methylnaphthalene ND ug/kg 1 09/23/10 20:30 91-57-609/13/10 12:30405 87.22-Methylphenol(o-Cresol) ND ug/kg 1 09/23/10 20:30 95-48-709/13/10 12:30405 1233&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/23/10 20:3009/13/10 12:30405 160Naphthalene ND ug/kg 1 09/23/10 20:30 91-20-309/13/10 12:30405 99.52-Nitroaniline ND ug/kg 1 09/23/10 20:30 88-74-409/13/10 12:302030 1253-Nitroaniline ND ug/kg 1 09/23/10 20:30 99-09-209/13/10 12:302030 1114-Nitroaniline ND ug/kg 1 09/23/10 20:30 100-01-609/13/10 12:30811 114Nitrobenzene ND ug/kg 1 09/23/10 20:30 98-95-309/13/10 12:30405 1112-Nitrophenol ND ug/kg 1 09/23/10 20:30 88-75-509/13/10 12:30405 98.34-Nitrophenol ND ug/kg 1 09/23/10 20:30 100-02-709/13/10 12:302030 72.5N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/10 20:30 621-64-709/13/10 12:30405 77.4N-Nitrosodiphenylamine ND ug/kg 1 09/23/10 20:30 86-30-609/13/10 12:30405 120Pentachlorophenol ND ug/kg 1 09/23/10 20:30 87-86-509/13/10 12:302030 73.7Phenanthrene ND ug/kg 1 09/23/10 20:30 85-01-809/13/10 12:30405 67.6Phenol ND ug/kg 1 09/23/10 20:30 108-95-209/13/10 12:30405 122Pyrene ND ug/kg 1 09/23/10 20:30 129-00-009/13/10 12:30405 68.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/23/10 20:30 95-94-309/13/10 12:30405 1472,3,4,6-Tetrachlorophenol ND ug/kg 1 09/23/10 20:30 58-90-209/13/10 12:30405 1602,4,5-Trichlorophenol ND ug/kg 1 09/23/10 20:30 95-95-409/13/10 12:30405 1252,4,6-Trichlorophenol ND ug/kg 1 09/23/10 20:30 88-06-209/13/10 12:30405 89.72-Fluorobiphenyl (S) 52 % 1 09/23/10 20:30 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 60 % 1 09/23/10 20:30 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 33 % 1 09/23/10 20:30 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 34 % 1 09/23/10 20:30 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 61 % 1 09/23/10 20:30 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:23 PM Page 131 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 39 % 1 09/23/10 20:30 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 132 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 03:07 120-82-15.2 1.71,1,1-Trichloroethane ND ug/kg 1 09/08/10 03:07 71-55-65.2 1.91,1,2-Trichloroethane ND ug/kg 1 09/08/10 03:07 79-00-55.2 2.2Trichloroethene 258 ug/kg 5 09/08/10 18:45 79-01-625.5 10.7Trichlorofluoromethane ND ug/kg 1 09/08/10 03:07 75-69-45.2 2.31,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/08/10 03:07 76-13-15.2 2.0Vinyl chloride ND ug/kg 1 09/08/10 03:07 75-01-410.4 1.9Xylene (Total) ND ug/kg 1 09/08/10 03:07 1330-20-710.4 3.8m&p-Xylene ND ug/kg 1 09/08/10 03:07 179601-23-110.4 3.8o-Xylene ND ug/kg 1 09/08/10 03:07 95-47-65.2 2.0Dibromofluoromethane (S) 101 % 1 09/08/10 03:07 1868-53-770-130Toluene-d8 (S) 99 % 1 09/08/10 03:07 2037-26-570-1304-Bromofluorobenzene (S) 96 % 1 09/08/10 03:07 460-00-470-1301,2-Dichloroethane-d4 (S) 105 % 1 09/08/10 03:07 17060-07-070-132




Cyanide ND mg/kg 1 09/05/10 13:59 57-12-50.25 0.25





Date: 09/27/2010 06:23 PM Page 133 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 17:01 7440-36-0 D309/08/10 15:403.0 1.7Arsenic ND mg/kg 10 09/15/10 17:01 7440-38-2 D309/08/10 15:403.0 1.9Beryllium 1.7 mg/kg 10 09/15/10 17:01 7440-41-709/08/10 15:400.59 0.12Cadmium ND mg/kg 10 09/15/10 17:01 7440-43-9 D309/08/10 15:400.59 0.36Chromium 23.7 mg/kg 10 09/15/10 17:01 7440-47-309/08/10 15:403.0 0.18Copper 19.6 mg/kg 10 09/15/10 17:01 7440-50-809/08/10 15:403.0 0.24Lead 10.2 mg/kg 10 09/15/10 17:01 7439-92-109/08/10 15:403.0 2.9Manganese 537 mg/kg 10 09/15/10 17:01 7439-96-509/08/10 15:403.0 0.18Nickel 14.0 mg/kg 10 09/15/10 17:01 7440-02-009/08/10 15:403.0 1.1Selenium ND mg/kg 10 09/15/10 17:01 7782-49-2 D309/08/10 15:405.9 2.3Silver 6.4 mg/kg 10 09/15/10 17:01 7440-22-409/08/10 15:403.0 0.18Thallium ND mg/kg 10 09/15/10 17:01 7440-28-0 D309/08/10 15:405.9 1.5Zinc 73.7 mg/kg 10 09/15/10 17:01 7440-66-609/08/10 15:405.9 1.5


Mercury 0.018 mg/kg 1 09/10/10 12:08 7439-97-609/08/10 10:010.0045 0.000089





Date: 09/27/2010 06:23 PM Page 134 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/23/10 21:07 91-94-109/13/10 12:301760 77.02,4-Dichlorophenol ND ug/kg 1 09/23/10 21:07 120-83-209/13/10 12:30353 77.0Diethylphthalate ND ug/kg 1 09/23/10 21:07 84-66-209/13/10 12:30353 54.62,4-Dimethylphenol ND ug/kg 1 09/23/10 21:07 105-67-909/13/10 12:30353 139Dimethylphthalate ND ug/kg 1 09/23/10 21:07 131-11-309/13/10 12:30353 71.7Di-n-butylphthalate ND ug/kg 1 09/23/10 21:07 84-74-209/13/10 12:30353 57.84,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/10 21:07 534-52-109/13/10 12:30706 70.62,4-Dinitrophenol ND ug/kg 1 09/23/10 21:07 51-28-509/13/10 12:301760 57.82,4-Dinitrotoluene ND ug/kg 1 09/23/10 21:07 121-14-209/13/10 12:30353 66.32,6-Dinitrotoluene ND ug/kg 1 09/23/10 21:07 606-20-209/13/10 12:30353 73.8Di-n-octylphthalate ND ug/kg 1 09/23/10 21:07 117-84-009/13/10 12:30353 73.8bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/10 21:07 117-81-709/13/10 12:30353 96.3Fluoranthene ND ug/kg 1 09/23/10 21:07 206-44-009/13/10 12:30353 51.3Fluorene ND ug/kg 1 09/23/10 21:07 86-73-709/13/10 12:30353 72.7Hexachloro-1,3-butadiene ND ug/kg 1 09/23/10 21:07 87-68-309/13/10 12:30353 61.0Hexachlorobenzene ND ug/kg 1 09/23/10 21:07 118-74-109/13/10 12:30353 44.9Hexachlorocyclopentadiene ND ug/kg 1 09/23/10 21:07 77-47-409/13/10 12:30353 65.3Hexachloroethane ND ug/kg 1 09/23/10 21:07 67-72-109/13/10 12:30353 93.1Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/10 21:07 193-39-509/13/10 12:30353 72.7Isophorone ND ug/kg 1 09/23/10 21:07 78-59-109/13/10 12:30353 79.22-Methylnaphthalene ND ug/kg 1 09/23/10 21:07 91-57-609/13/10 12:30353 75.92-Methylphenol(o-Cresol) ND ug/kg 1 09/23/10 21:07 95-48-709/13/10 12:30353 1073&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/23/10 21:0709/13/10 12:30353 139Naphthalene ND ug/kg 1 09/23/10 21:07 91-20-309/13/10 12:30353 86.62-Nitroaniline ND ug/kg 1 09/23/10 21:07 88-74-409/13/10 12:301760 1093-Nitroaniline ND ug/kg 1 09/23/10 21:07 99-09-209/13/10 12:301760 96.34-Nitroaniline ND ug/kg 1 09/23/10 21:07 100-01-609/13/10 12:30706 99.5Nitrobenzene ND ug/kg 1 09/23/10 21:07 98-95-309/13/10 12:30353 96.32-Nitrophenol ND ug/kg 1 09/23/10 21:07 88-75-509/13/10 12:30353 85.64-Nitrophenol ND ug/kg 1 09/23/10 21:07 100-02-709/13/10 12:301760 63.1N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/10 21:07 621-64-709/13/10 12:30353 67.4N-Nitrosodiphenylamine ND ug/kg 1 09/23/10 21:07 86-30-609/13/10 12:30353 105Pentachlorophenol ND ug/kg 1 09/23/10 21:07 87-86-509/13/10 12:301760 64.2Phenanthrene ND ug/kg 1 09/23/10 21:07 85-01-809/13/10 12:30353 58.8Phenol ND ug/kg 1 09/23/10 21:07 108-95-209/13/10 12:30353 106Pyrene ND ug/kg 1 09/23/10 21:07 129-00-009/13/10 12:30353 59.91,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/23/10 21:07 95-94-309/13/10 12:30353 1282,3,4,6-Tetrachlorophenol ND ug/kg 1 09/23/10 21:07 58-90-209/13/10 12:30353 1392,4,5-Trichlorophenol ND ug/kg 1 09/23/10 21:07 95-95-409/13/10 12:30353 1092,4,6-Trichlorophenol ND ug/kg 1 09/23/10 21:07 88-06-209/13/10 12:30353 78.12-Fluorobiphenyl (S) 39 % 1 09/23/10 21:07 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 52 % 1 09/23/10 21:07 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 24 % 1 09/23/10 21:07 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 24 % 1 09/23/10 21:07 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 50 % 1 09/23/10 21:07 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:23 PM Page 135 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/23/10 21:07 4165-60-009/13/10 12:3023-110


Acetone 109 ug/kg 1 09/08/10 03:25 67-64-1 C992.5 9.3Benzene ND ug/kg 1 09/08/10 03:25 71-43-24.6 1.5Bromochloromethane ND ug/kg 1 09/08/10 03:25 74-97-54.6 1.6Bromodichloromethane ND ug/kg 1 09/08/10 03:25 75-27-44.6 1.8Bromoform ND ug/kg 1 09/08/10 03:25 75-25-24.6 2.1Bromomethane ND ug/kg 1 09/08/10 03:25 74-83-99.3 2.32-Butanone (MEK) ND ug/kg 1 09/08/10 03:25 78-93-392.5 2.7Carbon disulfide ND ug/kg 1 09/08/10 03:25 75-15-09.3 2.8Carbon tetrachloride ND ug/kg 1 09/08/10 03:25 56-23-54.6 2.4Chlorobenzene ND ug/kg 1 09/08/10 03:25 108-90-74.6 1.8Chloroethane ND ug/kg 1 09/08/10 03:25 75-00-39.3 2.2Chloroform ND ug/kg 1 09/08/10 03:25 67-66-34.6 1.5Chloromethane ND ug/kg 1 09/08/10 03:25 74-87-39.3 2.2Cyclohexane ND ug/kg 1 09/08/10 03:25 110-82-74.6 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 03:25 96-12-84.6 3.3Dibromochloromethane ND ug/kg 1 09/08/10 03:25 124-48-14.6 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 03:25 106-93-44.6 1.71,2-Dichlorobenzene ND ug/kg 1 09/08/10 03:25 95-50-14.6 1.81,3-Dichlorobenzene ND ug/kg 1 09/08/10 03:25 541-73-14.6 1.91,4-Dichlorobenzene ND ug/kg 1 09/08/10 03:25 106-46-74.6 1.6Dichlorodifluoromethane ND ug/kg 1 09/08/10 03:25 75-71-89.3 3.31,1-Dichloroethane ND ug/kg 1 09/08/10 03:25 75-34-34.6 1.41,2-Dichloroethane ND ug/kg 1 09/08/10 03:25 107-06-24.6 2.01,1-Dichloroethene ND ug/kg 1 09/08/10 03:25 75-35-44.6 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 03:25 156-59-24.6 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 03:25 156-60-54.6 1.81,2-Dichloropropane ND ug/kg 1 09/08/10 03:25 78-87-54.6 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 03:25 10061-01-54.6 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 03:25 10061-02-64.6 1.4Ethylbenzene ND ug/kg 1 09/08/10 03:25 100-41-44.6 1.72-Hexanone ND ug/kg 1 09/08/10 03:25 591-78-646.3 3.6Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 03:25 98-82-84.6 1.8Methyl acetate ND ug/kg 1 09/08/10 03:25 79-20-99.3 1.3Methylcyclohexane ND ug/kg 1 09/08/10 03:25 108-87-29.3 1.4Methylene Chloride 11.3J ug/kg 1 09/08/10 03:25 75-09-218.5 2.84-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 03:25 108-10-146.3 3.4Methyl-tert-butyl ether ND ug/kg 1 09/08/10 03:25 1634-04-44.6 1.4Styrene ND ug/kg 1 09/08/10 03:25 100-42-54.6 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 03:25 79-34-54.6 1.8Tetrachloroethene ND ug/kg 1 09/08/10 03:25 127-18-44.6 1.6Toluene ND ug/kg 1 09/08/10 03:25 108-88-34.6 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 03:25 87-61-64.6 2.0



Date: 09/27/2010 06:23 PM Page 136 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 14:01 57-12-50.16 0.16





Date: 09/27/2010 06:23 PM Page 137 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744






Mercury 0.00043J mg/kg 1 09/07/10 17:30 7439-97-6 M109/02/10 19:200.0044 0.000089


Acenaphthene ND ug/kg 1 09/23/10 18:00 83-32-909/10/10 09:30362 83.3Acenaphthylene ND ug/kg 1 09/23/10 18:00 208-96-809/10/10 09:30362 85.5Acetophenone ND ug/kg 1 09/23/10 18:00 98-86-209/10/10 09:30362 186Anthracene ND ug/kg 1 09/23/10 18:00 120-12-709/10/10 09:30362 81.1Atrazine ND ug/kg 1 09/23/10 18:00 1912-24-909/10/10 09:30724 143Benzaldehyde ND ug/kg 1 09/23/10 18:00 100-52-709/10/10 09:30724 362Benzo(a)anthracene ND ug/kg 1 09/23/10 18:00 56-55-309/10/10 09:30362 66.9Benzo(a)pyrene ND ug/kg 1 09/23/10 18:00 50-32-809/10/10 09:30362 69.1Benzo(b)fluoranthene ND ug/kg 1 09/23/10 18:00 205-99-209/10/10 09:30362 62.5Benzo(g,h,i)perylene ND ug/kg 1 09/23/10 18:00 191-24-209/10/10 09:30362 92.1Benzo(k)fluoranthene ND ug/kg 1 09/23/10 18:00 207-08-909/10/10 09:30362 71.3Biphenyl (Diphenyl) ND ug/kg 1 09/23/10 18:00 92-52-409/10/10 09:30362 1144-Bromophenylphenyl ether ND ug/kg 1 09/23/10 18:00 101-55-309/10/10 09:30362 65.8Butylbenzylphthalate ND ug/kg 1 09/23/10 18:00 85-68-709/10/10 09:30362 76.8Caprolactam ND ug/kg 1 09/23/10 18:00 105-60-209/10/10 09:30362 62.5Carbazole ND ug/kg 1 09/23/10 18:00 86-74-809/10/10 09:30362 69.14-Chloro-3-methylphenol ND ug/kg 1 09/23/10 18:00 59-50-709/10/10 09:30724 74.64-Chloroaniline ND ug/kg 1 09/23/10 18:00 106-47-809/10/10 09:301810 101bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/10 18:00 111-91-109/10/10 09:30362 84.4bis(2-Chloroethyl) ether ND ug/kg 1 09/23/10 18:00 111-44-409/10/10 09:30362 92.1bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/10 18:00 108-60-109/10/10 09:30362 96.52-Chloronaphthalene ND ug/kg 1 09/23/10 18:00 91-58-709/10/10 09:30362 71.32-Chlorophenol ND ug/kg 1 09/23/10 18:00 95-57-809/10/10 09:30362 98.74-Chlorophenylphenyl ether ND ug/kg 1 09/23/10 18:00 7005-72-309/10/10 09:30362 74.6Chrysene ND ug/kg 1 09/23/10 18:00 218-01-909/10/10 09:30362 48.2Dibenz(a,h)anthracene ND ug/kg 1 09/23/10 18:00 53-70-309/10/10 09:30362 76.8Dibenzofuran ND ug/kg 1 09/23/10 18:00 132-64-909/10/10 09:30362 59.2



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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 139 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 34 % 1 09/23/10 18:00 4165-60-009/10/10 09:3023-110


Acetone 44.0J ug/kg 1 09/08/10 03:43 67-64-199.7 10Benzene ND ug/kg 1 09/08/10 03:43 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/08/10 03:43 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/08/10 03:43 75-27-45.0 1.9Bromoform ND ug/kg 1 09/08/10 03:43 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/08/10 03:43 74-83-910 2.52-Butanone (MEK) ND ug/kg 1 09/08/10 03:43 78-93-399.7 2.9Carbon disulfide ND ug/kg 1 09/08/10 03:43 75-15-010 3.0Carbon tetrachloride ND ug/kg 1 09/08/10 03:43 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/08/10 03:43 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/08/10 03:43 75-00-310 2.4Chloroform ND ug/kg 1 09/08/10 03:43 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/08/10 03:43 74-87-310 2.4Cyclohexane ND ug/kg 1 09/08/10 03:43 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 03:43 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/08/10 03:43 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 03:43 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/08/10 03:43 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/08/10 03:43 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/08/10 03:43 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/08/10 03:43 75-71-810 3.61,1-Dichloroethane ND ug/kg 1 09/08/10 03:43 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/08/10 03:43 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/08/10 03:43 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 03:43 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 03:43 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/08/10 03:43 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 03:43 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 03:43 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/08/10 03:43 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/08/10 03:43 591-78-649.8 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 03:43 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/08/10 03:43 79-20-910 1.4Methylcyclohexane ND ug/kg 1 09/08/10 03:43 108-87-210 1.5Methylene Chloride 11.5J ug/kg 1 09/08/10 03:43 75-09-219.9 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 03:43 108-10-149.8 3.7Methyl-tert-butyl ether ND ug/kg 1 09/08/10 03:43 1634-04-45.0 1.5Styrene ND ug/kg 1 09/08/10 03:43 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 03:43 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/08/10 03:43 127-18-45.0 1.7Toluene ND ug/kg 1 09/08/10 03:43 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 03:43 87-61-65.0 2.2



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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 03:43 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/08/10 03:43 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/08/10 03:43 79-00-55.0 2.1Trichloroethene ND ug/kg 1 09/08/10 03:43 79-01-65.0 2.1Trichlorofluoromethane ND ug/kg 1 09/08/10 03:43 75-69-45.0 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/08/10 03:43 76-13-15.0 1.9Vinyl chloride ND ug/kg 1 09/08/10 03:43 75-01-410 1.8Xylene (Total) ND ug/kg 1 09/08/10 03:43 1330-20-710 3.6m&p-Xylene ND ug/kg 1 09/08/10 03:43 179601-23-110 3.6o-Xylene ND ug/kg 1 09/08/10 03:43 95-47-65.0 1.9Dibromofluoromethane (S) 102 % 1 09/08/10 03:43 1868-53-770-130Toluene-d8 (S) 101 % 1 09/08/10 03:43 2037-26-570-1304-Bromofluorobenzene (S) 98 % 1 09/08/10 03:43 460-00-470-1301,2-Dichloroethane-d4 (S) 105 % 1 09/08/10 03:43 17060-07-070-132




Cyanide ND mg/kg 1 09/05/10 14:01 57-12-50.19 0.19





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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 20 09/15/10 17:24 7440-36-0 D309/08/10 15:409.9 5.6Arsenic ND mg/kg 20 09/15/10 17:24 7440-38-2 D309/08/10 15:409.9 6.4Beryllium 4.2 mg/kg 20 09/15/10 17:24 7440-41-709/08/10 15:402.0 0.40Cadmium ND mg/kg 20 09/15/10 17:24 7440-43-9 D309/08/10 15:402.0 1.2Chromium 56.0 mg/kg 20 09/15/10 17:24 7440-47-309/08/10 15:409.9 0.60Copper 36.3 mg/kg 20 09/15/10 17:24 7440-50-809/08/10 15:409.9 0.79Lead 14.0 mg/kg 20 09/15/10 17:24 7439-92-109/08/10 15:409.9 9.5Manganese 371 mg/kg 20 09/15/10 17:24 7439-96-509/08/10 15:409.9 0.60Nickel 30.6 mg/kg 20 09/15/10 17:24 7440-02-009/08/10 15:409.9 3.6Selenium ND mg/kg 20 09/15/10 17:24 7782-49-2 D309/08/10 15:4019.9 7.5Silver ND mg/kg 20 09/15/10 17:24 7440-22-4 D309/08/10 15:409.9 0.60Thallium ND mg/kg 20 09/15/10 17:24 7440-28-0 D309/08/10 15:4019.9 5.2Zinc 157 mg/kg 20 09/15/10 17:24 7440-66-609/08/10 15:4019.9 5.2


Mercury ND mg/kg 1 09/07/10 17:43 7439-97-609/02/10 19:200.0053 0.00011





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 12:27 91-94-109/13/10 12:302100 91.52,4-Dichlorophenol ND ug/kg 1 09/17/10 12:27 120-83-209/13/10 12:30419 91.5Diethylphthalate ND ug/kg 1 09/17/10 12:27 84-66-209/13/10 12:30419 64.82,4-Dimethylphenol ND ug/kg 1 09/17/10 12:27 105-67-909/13/10 12:30419 165Dimethylphthalate ND ug/kg 1 09/17/10 12:27 131-11-309/13/10 12:30419 85.1Di-n-butylphthalate ND ug/kg 1 09/17/10 12:27 84-74-209/13/10 12:30419 68.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 12:27 534-52-109/13/10 12:30839 83.92,4-Dinitrophenol ND ug/kg 1 09/17/10 12:27 51-28-509/13/10 12:302100 68.62,4-Dinitrotoluene ND ug/kg 1 09/17/10 12:27 121-14-209/13/10 12:30419 78.82,6-Dinitrotoluene ND ug/kg 1 09/17/10 12:27 606-20-209/13/10 12:30419 87.7Di-n-octylphthalate ND ug/kg 1 09/17/10 12:27 117-84-009/13/10 12:30419 87.7bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 12:27 117-81-709/13/10 12:30419 114Fluoranthene ND ug/kg 1 09/17/10 12:27 206-44-009/13/10 12:30419 61.0Fluorene ND ug/kg 1 09/17/10 12:27 86-73-709/13/10 12:30419 86.4Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 12:27 87-68-309/13/10 12:30419 72.4Hexachlorobenzene ND ug/kg 1 09/17/10 12:27 118-74-109/13/10 12:30419 53.4Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 12:27 77-47-409/13/10 12:30419 77.5Hexachloroethane ND ug/kg 1 09/17/10 12:27 67-72-109/13/10 12:30419 111Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 12:27 193-39-509/13/10 12:30419 86.4Isophorone ND ug/kg 1 09/17/10 12:27 78-59-109/13/10 12:30419 94.02-Methylnaphthalene ND ug/kg 1 09/17/10 12:27 91-57-609/13/10 12:30419 90.22-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 12:27 95-48-709/13/10 12:30419 1273&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 12:2709/13/10 12:30419 165Naphthalene ND ug/kg 1 09/17/10 12:27 91-20-309/13/10 12:30419 1032-Nitroaniline ND ug/kg 1 09/17/10 12:27 88-74-409/13/10 12:302100 1303-Nitroaniline ND ug/kg 1 09/17/10 12:27 99-09-209/13/10 12:302100 1144-Nitroaniline ND ug/kg 1 09/17/10 12:27 100-01-609/13/10 12:30839 118Nitrobenzene ND ug/kg 1 09/17/10 12:27 98-95-309/13/10 12:30419 1142-Nitrophenol ND ug/kg 1 09/17/10 12:27 88-75-509/13/10 12:30419 1024-Nitrophenol ND ug/kg 1 09/17/10 12:27 100-02-709/13/10 12:302100 75.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 12:27 621-64-709/13/10 12:30419 80.0N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 12:27 86-30-609/13/10 12:30419 125Pentachlorophenol ND ug/kg 1 09/17/10 12:27 87-86-509/13/10 12:302100 76.2Phenanthrene ND ug/kg 1 09/17/10 12:27 85-01-809/13/10 12:30419 69.9Phenol ND ug/kg 1 09/17/10 12:27 108-95-209/13/10 12:30419 126Pyrene ND ug/kg 1 09/17/10 12:27 129-00-009/13/10 12:30419 71.21,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 12:27 95-94-309/13/10 12:30419 1522,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 12:27 58-90-209/13/10 12:30419 1652,4,5-Trichlorophenol ND ug/kg 1 09/17/10 12:27 95-95-409/13/10 12:30419 1302,4,6-Trichlorophenol ND ug/kg 1 09/17/10 12:27 88-06-209/13/10 12:30419 92.82-Fluorobiphenyl (S) 37 % 1 09/17/10 12:27 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 52 % 1 09/17/10 12:27 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 29 % 1 09/17/10 12:27 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 30 % 1 09/17/10 12:27 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 56 % 1 09/17/10 12:27 118-79-609/13/10 12:3027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 32 % 1 09/17/10 12:27 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 144 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 14:03 57-12-50.19 0.19





Date: 09/27/2010 06:23 PM Page 145 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 17:27 7440-36-0 D309/08/10 15:405.1 2.8Arsenic ND mg/kg 10 09/15/10 17:27 7440-38-2 D309/08/10 15:405.1 3.2Beryllium 5.2 mg/kg 10 09/15/10 17:27 7440-41-709/08/10 15:401.0 0.20Cadmium ND mg/kg 10 09/15/10 17:27 7440-43-9 D309/08/10 15:401.0 0.61Chromium 26.0 mg/kg 10 09/15/10 17:27 7440-47-309/08/10 15:405.1 0.30Copper 48.7 mg/kg 10 09/15/10 17:27 7440-50-809/08/10 15:405.1 0.41Lead 8.7 mg/kg 10 09/15/10 17:27 7439-92-109/08/10 15:405.1 4.9Manganese 632 mg/kg 10 09/15/10 17:27 7439-96-509/08/10 15:405.1 0.30Nickel 8.9 mg/kg 10 09/15/10 17:27 7440-02-009/08/10 15:405.1 1.8Selenium ND mg/kg 10 09/15/10 17:27 7782-49-2 D309/08/10 15:4010.1 3.9Silver ND mg/kg 10 09/15/10 17:27 7440-22-4 D309/08/10 15:405.1 0.30Thallium ND mg/kg 10 09/15/10 17:27 7440-28-0 D309/08/10 15:4010.1 2.6Zinc 107 mg/kg 10 09/15/10 17:27 7440-66-609/08/10 15:4010.1 2.6


Mercury 0.00093J mg/kg 1 09/07/10 17:51 7439-97-609/02/10 19:200.0047 0.000094





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 147 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Nitrobenzene-d5 (S) 48 % 1 09/17/10 13:04 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 148 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 14:03 57-12-50.18 0.18





Date: 09/27/2010 06:23 PM Page 149 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Antimony ND mg/kg 1 09/15/10 09:14 7440-36-009/08/10 15:400.48 0.27Arsenic ND mg/kg 1 09/15/10 09:14 7440-38-209/08/10 15:400.48 0.30Beryllium 0.33 mg/kg 1 09/15/10 09:14 7440-41-709/08/10 15:400.095 0.019Cadmium ND mg/kg 1 09/15/10 09:14 7440-43-909/08/10 15:400.095 0.057Chromium 3.4 mg/kg 1 09/15/10 09:14 7440-47-309/08/10 15:400.48 0.029Copper 2.8 mg/kg 1 09/15/10 09:14 7440-50-809/08/10 15:400.48 0.038Lead 4.8 mg/kg 1 09/15/10 09:14 7439-92-109/08/10 15:400.48 0.46Manganese 1560 mg/kg 10 09/16/10 11:53 7439-96-509/08/10 15:404.8 0.29Nickel 6.1 mg/kg 1 09/15/10 09:14 7440-02-009/08/10 15:400.48 0.17Selenium ND mg/kg 1 09/15/10 09:14 7782-49-209/08/10 15:400.95 0.36Silver ND mg/kg 1 09/15/10 09:14 7440-22-409/08/10 15:400.48 0.029Thallium 0.48J mg/kg 1 09/15/10 09:14 7440-28-009/08/10 15:400.95 0.25Zinc 17.5 mg/kg 1 09/15/10 09:14 7440-66-609/08/10 15:400.95 0.25


Mercury 0.014 mg/kg 1 09/07/10 17:12 7439-97-609/02/10 19:200.0051 0.00010





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acetone 35.2J ug/kg 1 09/07/10 20:58 67-64-194.3 9.4Benzene ND ug/kg 1 09/07/10 20:58 71-43-24.7 1.5Bromochloromethane ND ug/kg 1 09/07/10 20:58 74-97-54.7 1.6Bromodichloromethane ND ug/kg 1 09/07/10 20:58 75-27-44.7 1.8Bromoform ND ug/kg 1 09/07/10 20:58 75-25-24.7 2.2Bromomethane ND ug/kg 1 09/07/10 20:58 74-83-99.4 2.42-Butanone (MEK) ND ug/kg 1 09/07/10 20:58 78-93-394.3 2.7Carbon disulfide ND ug/kg 1 09/07/10 20:58 75-15-09.4 2.8Carbon tetrachloride ND ug/kg 1 09/07/10 20:58 56-23-54.7 2.5Chlorobenzene ND ug/kg 1 09/07/10 20:58 108-90-74.7 1.8Chloroethane ND ug/kg 1 09/07/10 20:58 75-00-39.4 2.3Chloroform ND ug/kg 1 09/07/10 20:58 67-66-34.7 1.5Chloromethane ND ug/kg 1 09/07/10 20:58 74-87-39.4 2.3Cyclohexane ND ug/kg 1 09/07/10 20:58 110-82-74.7 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 20:58 96-12-84.7 3.4Dibromochloromethane ND ug/kg 1 09/07/10 20:58 124-48-14.7 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 20:58 106-93-44.7 1.71,2-Dichlorobenzene ND ug/kg 1 09/07/10 20:58 95-50-14.7 1.81,3-Dichlorobenzene ND ug/kg 1 09/07/10 20:58 541-73-14.7 1.91,4-Dichlorobenzene ND ug/kg 1 09/07/10 20:58 106-46-74.7 1.6Dichlorodifluoromethane ND ug/kg 1 09/07/10 20:58 75-71-89.4 3.41,1-Dichloroethane ND ug/kg 1 09/07/10 20:58 75-34-34.7 1.41,2-Dichloroethane ND ug/kg 1 09/07/10 20:58 107-06-24.7 2.11,1-Dichloroethene ND ug/kg 1 09/07/10 20:58 75-35-44.7 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:58 156-59-24.7 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 20:58 156-60-54.7 1.81,2-Dichloropropane ND ug/kg 1 09/07/10 20:58 78-87-54.7 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:58 10061-01-54.7 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 20:58 10061-02-64.7 1.4Ethylbenzene ND ug/kg 1 09/07/10 20:58 100-41-44.7 1.72-Hexanone ND ug/kg 1 09/07/10 20:58 591-78-647.2 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 20:58 98-82-84.7 1.8Methyl acetate 3.5J ug/kg 1 09/07/10 20:58 79-20-99.4 1.3Methylcyclohexane ND ug/kg 1 09/07/10 20:58 108-87-29.4 1.4Methylene Chloride 8.7J ug/kg 1 09/07/10 20:58 75-09-218.9 2.84-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 20:58 108-10-147.2 3.5Methyl-tert-butyl ether ND ug/kg 1 09/07/10 20:58 1634-04-44.7 1.4Styrene ND ug/kg 1 09/07/10 20:58 100-42-54.7 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 20:58 79-34-54.7 1.8Tetrachloroethene ND ug/kg 1 09/07/10 20:58 127-18-44.7 1.6Toluene ND ug/kg 1 09/07/10 20:58 108-88-34.7 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 20:58 87-61-64.7 2.11,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 20:58 120-82-14.7 1.51,1,1-Trichloroethane ND ug/kg 1 09/07/10 20:58 71-55-64.7 1.71,1,2-Trichloroethane ND ug/kg 1 09/07/10 20:58 79-00-54.7 2.0



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Trichloroethene ND ug/kg 1 09/07/10 20:58 79-01-64.7 2.0Trichlorofluoromethane ND ug/kg 1 09/07/10 20:58 75-69-44.7 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/07/10 20:58 76-13-14.7 1.8Vinyl chloride ND ug/kg 1 09/07/10 20:58 75-01-49.4 1.7Xylene (Total) ND ug/kg 1 09/07/10 20:58 1330-20-79.4 3.4m&p-Xylene ND ug/kg 1 09/07/10 20:58 179601-23-19.4 3.4o-Xylene ND ug/kg 1 09/07/10 20:58 95-47-64.7 1.8Dibromofluoromethane (S) 102 % 1 09/07/10 20:58 1868-53-770-130Toluene-d8 (S) 101 % 1 09/07/10 20:58 2037-26-570-1304-Bromofluorobenzene (S) 95 % 1 09/07/10 20:58 460-00-470-1301,2-Dichloroethane-d4 (S) 103 % 1 09/07/10 20:58 17060-07-070-132





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/18/10 11:38 83-32-909/13/10 12:30414 95.3Acenaphthylene ND ug/kg 1 09/18/10 11:38 208-96-809/13/10 12:30414 97.8Acetophenone ND ug/kg 1 09/18/10 11:38 98-86-209/13/10 12:30414 213Anthracene ND ug/kg 1 09/18/10 11:38 120-12-709/13/10 12:30414 92.8Atrazine ND ug/kg 1 09/18/10 11:38 1912-24-909/13/10 12:30828 163Benzaldehyde ND ug/kg 1 09/18/10 11:38 100-52-709/13/10 12:30828 414Benzo(a)anthracene ND ug/kg 1 09/18/10 11:38 56-55-309/13/10 12:30414 76.5Benzo(a)pyrene ND ug/kg 1 09/18/10 11:38 50-32-809/13/10 12:30414 79.0Benzo(b)fluoranthene ND ug/kg 1 09/18/10 11:38 205-99-209/13/10 12:30414 71.5Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 11:38 191-24-209/13/10 12:30414 105Benzo(k)fluoranthene ND ug/kg 1 09/18/10 11:38 207-08-909/13/10 12:30414 81.5Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 11:38 92-52-409/13/10 12:30414 1304-Bromophenylphenyl ether ND ug/kg 1 09/18/10 11:38 101-55-309/13/10 12:30414 75.3Butylbenzylphthalate ND ug/kg 1 09/18/10 11:38 85-68-709/13/10 12:30414 87.8Caprolactam ND ug/kg 1 09/18/10 11:38 105-60-209/13/10 12:30414 71.5Carbazole ND ug/kg 1 09/18/10 11:38 86-74-809/13/10 12:30414 79.04-Chloro-3-methylphenol ND ug/kg 1 09/18/10 11:38 59-50-709/13/10 12:30828 85.34-Chloroaniline ND ug/kg 1 09/18/10 11:38 106-47-809/13/10 12:302070 115bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 11:38 111-91-109/13/10 12:30414 96.6bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 11:38 111-44-409/13/10 12:30414 105bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 11:38 108-60-109/13/10 12:30414 1102-Chloronaphthalene ND ug/kg 1 09/18/10 11:38 91-58-709/13/10 12:30414 81.52-Chlorophenol ND ug/kg 1 09/18/10 11:38 95-57-809/13/10 12:30414 1134-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 11:38 7005-72-309/13/10 12:30414 85.3Chrysene ND ug/kg 1 09/18/10 11:38 218-01-909/13/10 12:30414 55.2Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 11:38 53-70-309/13/10 12:30414 87.8Dibenzofuran ND ug/kg 1 09/18/10 11:38 132-64-909/13/10 12:30414 67.73,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 11:38 91-94-109/13/10 12:302070 90.32,4-Dichlorophenol ND ug/kg 1 09/18/10 11:38 120-83-209/13/10 12:30414 90.3Diethylphthalate ND ug/kg 1 09/18/10 11:38 84-66-209/13/10 12:30414 64.02,4-Dimethylphenol ND ug/kg 1 09/18/10 11:38 105-67-909/13/10 12:30414 163Dimethylphthalate ND ug/kg 1 09/18/10 11:38 131-11-309/13/10 12:30414 84.0Di-n-butylphthalate ND ug/kg 1 09/18/10 11:38 84-74-209/13/10 12:30414 67.74,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 11:38 534-52-109/13/10 12:30828 82.82,4-Dinitrophenol ND ug/kg 1 09/18/10 11:38 51-28-509/13/10 12:302070 67.72,4-Dinitrotoluene ND ug/kg 1 09/18/10 11:38 121-14-209/13/10 12:30414 77.82,6-Dinitrotoluene ND ug/kg 1 09/18/10 11:38 606-20-209/13/10 12:30414 86.6Di-n-octylphthalate ND ug/kg 1 09/18/10 11:38 117-84-009/13/10 12:30414 86.6bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 11:38 117-81-709/13/10 12:30414 113Fluoranthene ND ug/kg 1 09/18/10 11:38 206-44-009/13/10 12:30414 60.2Fluorene ND ug/kg 1 09/18/10 11:38 86-73-709/13/10 12:30414 85.3Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 11:38 87-68-309/13/10 12:30414 71.5Hexachlorobenzene ND ug/kg 1 09/18/10 11:38 118-74-109/13/10 12:30414 52.7Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 11:38 77-47-409/13/10 12:30414 76.5Hexachloroethane ND ug/kg 1 09/18/10 11:38 67-72-109/13/10 12:30414 109



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 11:38 193-39-509/13/10 12:30414 85.3Isophorone ND ug/kg 1 09/18/10 11:38 78-59-109/13/10 12:30414 92.82-Methylnaphthalene ND ug/kg 1 09/18/10 11:38 91-57-609/13/10 12:30414 89.12-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 11:38 95-48-709/13/10 12:30414 1253&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 11:3809/13/10 12:30414 163Naphthalene ND ug/kg 1 09/18/10 11:38 91-20-309/13/10 12:30414 1022-Nitroaniline ND ug/kg 1 09/18/10 11:38 88-74-409/13/10 12:302070 1283-Nitroaniline ND ug/kg 1 09/18/10 11:38 99-09-209/13/10 12:302070 1134-Nitroaniline ND ug/kg 1 09/18/10 11:38 100-01-609/13/10 12:30828 117Nitrobenzene ND ug/kg 1 09/18/10 11:38 98-95-309/13/10 12:30414 1132-Nitrophenol ND ug/kg 1 09/18/10 11:38 88-75-509/13/10 12:30414 1004-Nitrophenol ND ug/kg 1 09/18/10 11:38 100-02-709/13/10 12:302070 74.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 11:38 621-64-709/13/10 12:30414 79.0N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 11:38 86-30-609/13/10 12:30414 123Pentachlorophenol ND ug/kg 1 09/18/10 11:38 87-86-509/13/10 12:302070 75.3Phenanthrene ND ug/kg 1 09/18/10 11:38 85-01-809/13/10 12:30414 69.0Phenol ND ug/kg 1 09/18/10 11:38 108-95-209/13/10 12:30414 124Pyrene ND ug/kg 1 09/18/10 11:38 129-00-009/13/10 12:30414 70.21,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 11:38 95-94-309/13/10 12:30414 1512,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 11:38 58-90-209/13/10 12:30414 1632,4,5-Trichlorophenol ND ug/kg 1 09/18/10 11:38 95-95-409/13/10 12:30414 1282,4,6-Trichlorophenol ND ug/kg 1 09/18/10 11:38 88-06-209/13/10 12:30414 91.62-Fluorobiphenyl (S) 45 % 1 09/18/10 11:38 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 51 % 1 09/18/10 11:38 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 32 % 1 09/18/10 11:38 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 31 % 1 09/18/10 11:38 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 46 % 1 09/18/10 11:38 118-79-609/13/10 12:3027-110Nitrobenzene-d5 (S) 35 % 1 09/18/10 11:38 4165-60-009/13/10 12:3023-110





Date: 09/27/2010 06:23 PM Page 154 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/05/10 13:54 57-12-50.17 0.17



Date: 09/27/2010 06:23 PM Page 155 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/18/10 12:13 83-32-909/13/10 12:30374 86.2Acenaphthylene ND ug/kg 1 09/18/10 12:13 208-96-809/13/10 12:30374 88.5Acetophenone ND ug/kg 1 09/18/10 12:13 98-86-209/13/10 12:30374 193Anthracene ND ug/kg 1 09/18/10 12:13 120-12-709/13/10 12:30374 84.0Atrazine ND ug/kg 1 09/18/10 12:13 1912-24-909/13/10 12:30749 147Benzaldehyde ND ug/kg 1 09/18/10 12:13 100-52-709/13/10 12:30749 374Benzo(a)anthracene ND ug/kg 1 09/18/10 12:13 56-55-309/13/10 12:30374 69.2Benzo(a)pyrene ND ug/kg 1 09/18/10 12:13 50-32-809/13/10 12:30374 71.5Benzo(b)fluoranthene ND ug/kg 1 09/18/10 12:13 205-99-209/13/10 12:30374 64.7Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 12:13 191-24-209/13/10 12:30374 95.3Benzo(k)fluoranthene ND ug/kg 1 09/18/10 12:13 207-08-909/13/10 12:30374 73.7Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 12:13 92-52-409/13/10 12:30374 1184-Bromophenylphenyl ether ND ug/kg 1 09/18/10 12:13 101-55-309/13/10 12:30374 68.1Butylbenzylphthalate ND ug/kg 1 09/18/10 12:13 85-68-709/13/10 12:30374 79.4Caprolactam ND ug/kg 1 09/18/10 12:13 105-60-209/13/10 12:30374 64.7Carbazole ND ug/kg 1 09/18/10 12:13 86-74-809/13/10 12:30374 71.54-Chloro-3-methylphenol ND ug/kg 1 09/18/10 12:13 59-50-709/13/10 12:30749 77.14-Chloroaniline ND ug/kg 1 09/18/10 12:13 106-47-809/13/10 12:301870 104bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 12:13 111-91-109/13/10 12:30374 87.4bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 12:13 111-44-409/13/10 12:30374 95.3bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 12:13 108-60-109/13/10 12:30374 99.82-Chloronaphthalene ND ug/kg 1 09/18/10 12:13 91-58-709/13/10 12:30374 73.72-Chlorophenol ND ug/kg 1 09/18/10 12:13 95-57-809/13/10 12:30374 1024-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 12:13 7005-72-309/13/10 12:30374 77.1Chrysene ND ug/kg 1 09/18/10 12:13 218-01-909/13/10 12:30374 49.9Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 12:13 53-70-309/13/10 12:30374 79.4Dibenzofuran ND ug/kg 1 09/18/10 12:13 132-64-909/13/10 12:30374 61.33,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 12:13 91-94-109/13/10 12:301870 81.72,4-Dichlorophenol ND ug/kg 1 09/18/10 12:13 120-83-209/13/10 12:30374 81.7Diethylphthalate ND ug/kg 1 09/18/10 12:13 84-66-209/13/10 12:30374 57.92,4-Dimethylphenol ND ug/kg 1 09/18/10 12:13 105-67-909/13/10 12:30374 147Dimethylphthalate ND ug/kg 1 09/18/10 12:13 131-11-309/13/10 12:30374 76.0Di-n-butylphthalate ND ug/kg 1 09/18/10 12:13 84-74-209/13/10 12:30374 61.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 12:13 534-52-109/13/10 12:30749 74.92,4-Dinitrophenol ND ug/kg 1 09/18/10 12:13 51-28-509/13/10 12:301870 61.32,4-Dinitrotoluene ND ug/kg 1 09/18/10 12:13 121-14-209/13/10 12:30374 70.32,6-Dinitrotoluene ND ug/kg 1 09/18/10 12:13 606-20-209/13/10 12:30374 78.3Di-n-octylphthalate ND ug/kg 1 09/18/10 12:13 117-84-009/13/10 12:30374 78.3bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 12:13 117-81-709/13/10 12:30374 102Fluoranthene ND ug/kg 1 09/18/10 12:13 206-44-009/13/10 12:30374 54.5Fluorene ND ug/kg 1 09/18/10 12:13 86-73-709/13/10 12:30374 77.1Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 12:13 87-68-309/13/10 12:30374 64.7Hexachlorobenzene ND ug/kg 1 09/18/10 12:13 118-74-109/13/10 12:30374 47.7Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 12:13 77-47-409/13/10 12:30374 69.2Hexachloroethane ND ug/kg 1 09/18/10 12:13 67-72-109/13/10 12:30374 98.7



Date: 09/27/2010 06:23 PM Page 156 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 12:13 193-39-509/13/10 12:30374 77.1Isophorone ND ug/kg 1 09/18/10 12:13 78-59-109/13/10 12:30374 84.02-Methylnaphthalene ND ug/kg 1 09/18/10 12:13 91-57-609/13/10 12:30374 80.62-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 12:13 95-48-709/13/10 12:30374 1133&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 12:1309/13/10 12:30374 147Naphthalene ND ug/kg 1 09/18/10 12:13 91-20-309/13/10 12:30374 91.92-Nitroaniline ND ug/kg 1 09/18/10 12:13 88-74-409/13/10 12:301870 1163-Nitroaniline ND ug/kg 1 09/18/10 12:13 99-09-209/13/10 12:301870 1024-Nitroaniline ND ug/kg 1 09/18/10 12:13 100-01-609/13/10 12:30749 106Nitrobenzene ND ug/kg 1 09/18/10 12:13 98-95-309/13/10 12:30374 1022-Nitrophenol ND ug/kg 1 09/18/10 12:13 88-75-509/13/10 12:30374 90.84-Nitrophenol ND ug/kg 1 09/18/10 12:13 100-02-709/13/10 12:301870 66.9N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 12:13 621-64-709/13/10 12:30374 71.5N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 12:13 86-30-609/13/10 12:30374 111Pentachlorophenol ND ug/kg 1 09/18/10 12:13 87-86-509/13/10 12:301870 68.1Phenanthrene ND ug/kg 1 09/18/10 12:13 85-01-809/13/10 12:30374 62.4Phenol ND ug/kg 1 09/18/10 12:13 108-95-209/13/10 12:30374 112Pyrene ND ug/kg 1 09/18/10 12:13 129-00-009/13/10 12:30374 63.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 12:13 95-94-309/13/10 12:30374 1362,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 12:13 58-90-209/13/10 12:30374 1472,4,5-Trichlorophenol ND ug/kg 1 09/18/10 12:13 95-95-409/13/10 12:30374 1162,4,6-Trichlorophenol ND ug/kg 1 09/18/10 12:13 88-06-209/13/10 12:30374 82.82-Fluorobiphenyl (S) 65 % 1 09/18/10 12:13 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 61 % 1 09/18/10 12:13 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 50 % 1 09/18/10 12:13 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 49 % 1 09/18/10 12:13 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 63 % 1 09/18/10 12:13 118-79-609/13/10 12:3027-110Nitrobenzene-d5 (S) 57 % 1 09/18/10 12:13 4165-60-009/13/10 12:3023-110





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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744









Date: 09/27/2010 06:23 PM Page 158 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acetone 28.1J ug/kg 1 09/07/10 21:17 67-64-1115 11.5Benzene ND ug/kg 1 09/07/10 21:17 71-43-25.7 1.8Bromochloromethane ND ug/kg 1 09/07/10 21:17 74-97-55.7 2.0Bromodichloromethane ND ug/kg 1 09/07/10 21:17 75-27-45.7 2.2Bromoform ND ug/kg 1 09/07/10 21:17 75-25-25.7 2.6Bromomethane ND ug/kg 1 09/07/10 21:17 74-83-911.5 2.92-Butanone (MEK) ND ug/kg 1 09/07/10 21:17 78-93-3115 3.3Carbon disulfide ND ug/kg 1 09/07/10 21:17 75-15-011.5 3.4Carbon tetrachloride ND ug/kg 1 09/07/10 21:17 56-23-55.7 3.0Chlorobenzene ND ug/kg 1 09/07/10 21:17 108-90-75.7 2.2Chloroethane ND ug/kg 1 09/07/10 21:17 75-00-311.5 2.8Chloroform ND ug/kg 1 09/07/10 21:17 67-66-35.7 1.8Chloromethane ND ug/kg 1 09/07/10 21:17 74-87-311.5 2.8Cyclohexane ND ug/kg 1 09/07/10 21:17 110-82-75.7 1.81,2-Dibromo-3-chloropropane ND ug/kg 1 09/07/10 21:17 96-12-85.7 4.1Dibromochloromethane ND ug/kg 1 09/07/10 21:17 124-48-15.7 2.11,2-Dibromoethane (EDB) ND ug/kg 1 09/07/10 21:17 106-93-45.7 2.11,2-Dichlorobenzene ND ug/kg 1 09/07/10 21:17 95-50-15.7 2.21,3-Dichlorobenzene ND ug/kg 1 09/07/10 21:17 541-73-15.7 2.31,4-Dichlorobenzene ND ug/kg 1 09/07/10 21:17 106-46-75.7 2.0Dichlorodifluoromethane ND ug/kg 1 09/07/10 21:17 75-71-811.5 4.11,1-Dichloroethane ND ug/kg 1 09/07/10 21:17 75-34-35.7 1.71,2-Dichloroethane ND ug/kg 1 09/07/10 21:17 107-06-25.7 2.51,1-Dichloroethene ND ug/kg 1 09/07/10 21:17 75-35-45.7 2.1cis-1,2-Dichloroethene ND ug/kg 1 09/07/10 21:17 156-59-25.7 1.6trans-1,2-Dichloroethene ND ug/kg 1 09/07/10 21:17 156-60-55.7 2.21,2-Dichloropropane ND ug/kg 1 09/07/10 21:17 78-87-55.7 2.0cis-1,3-Dichloropropene ND ug/kg 1 09/07/10 21:17 10061-01-55.7 2.1trans-1,3-Dichloropropene ND ug/kg 1 09/07/10 21:17 10061-02-65.7 1.7Ethylbenzene ND ug/kg 1 09/07/10 21:17 100-41-45.7 2.12-Hexanone ND ug/kg 1 09/07/10 21:17 591-78-657.4 4.5Isopropylbenzene (Cumene) ND ug/kg 1 09/07/10 21:17 98-82-85.7 2.2Methyl acetate ND ug/kg 1 09/07/10 21:17 79-20-911.5 1.6Methylcyclohexane ND ug/kg 1 09/07/10 21:17 108-87-211.5 1.7Methylene Chloride 7.4J ug/kg 1 09/07/10 21:17 75-09-223.0 3.44-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/07/10 21:17 108-10-157.4 4.2Methyl-tert-butyl ether ND ug/kg 1 09/07/10 21:17 1634-04-45.7 1.7Styrene ND ug/kg 1 09/07/10 21:17 100-42-55.7 2.11,1,2,2-Tetrachloroethane ND ug/kg 1 09/07/10 21:17 79-34-55.7 2.2Tetrachloroethene ND ug/kg 1 09/07/10 21:17 127-18-45.7 2.0Toluene ND ug/kg 1 09/07/10 21:17 108-88-35.7 2.11,2,3-Trichlorobenzene ND ug/kg 1 09/07/10 21:17 87-61-65.7 2.51,2,4-Trichlorobenzene ND ug/kg 1 09/07/10 21:17 120-82-15.7 1.81,1,1-Trichloroethane ND ug/kg 1 09/07/10 21:17 71-55-65.7 2.11,1,2-Trichloroethane ND ug/kg 1 09/07/10 21:17 79-00-55.7 2.4



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Mercury 0.00087J mg/kg 1 09/07/10 17:14 7439-97-609/02/10 19:200.0040 0.000080





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Cyanide ND mg/kg 1 09/12/10 16:20 57-12-50.11 0.11



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Sample: MB-01 Lab ID: 9276750040 Collected: 08/31/10 10:30 Received: 09/01/10 14:00 Matrix: Water


6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C

Antimony ND ug/L 1 09/07/10 22:39 7440-36-009/02/10 10:355.0 2.6Arsenic ND ug/L 1 09/07/10 22:39 7440-38-209/02/10 10:355.0 2.7Beryllium 0.11J ug/L 1 09/07/10 22:39 7440-41-709/02/10 10:351.0 0.10Cadmium ND ug/L 1 09/07/10 22:39 7440-43-909/02/10 10:351.0 0.50Chromium 0.58J ug/L 1 09/07/10 22:39 7440-47-309/02/10 10:355.0 0.40Copper 2.3J ug/L 1 09/07/10 22:39 7440-50-809/02/10 10:355.0 0.30Lead ND ug/L 1 09/07/10 22:39 7439-92-109/02/10 10:355.0 4.0Manganese 90.6 ug/L 1 09/07/10 22:39 7439-96-5 B09/02/10 10:355.0 0.30Nickel ND ug/L 1 09/07/10 22:39 7440-02-009/02/10 10:355.0 1.7Selenium ND ug/L 1 09/07/10 22:39 7782-49-209/02/10 10:3510.0 3.8Silver ND ug/L 1 09/07/10 22:39 7440-22-409/02/10 10:355.0 0.10Thallium 3.2J ug/L 1 09/07/10 22:39 7440-28-0 L009/02/10 10:3510.0 3.0Zinc 116 ug/L 1 09/07/10 22:39 7440-66-6 B09/02/10 10:3510.0 0.40


Mercury ND ug/L 1 09/09/10 10:05 7439-97-609/07/10 19:490.20 0.070

8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510

Acenaphthene ND ug/L 1 09/16/10 13:06 83-32-909/07/10 17:3011.0 2.1Acenaphthylene ND ug/L 1 09/16/10 13:06 208-96-809/07/10 17:3011.0 3.5Acetophenone ND ug/L 1 09/16/10 13:06 98-86-209/07/10 17:3011.0 4.1Anthracene ND ug/L 1 09/16/10 13:06 120-12-709/07/10 17:3011.0 2.7Atrazine ND ug/L 1 09/16/10 13:06 1912-24-909/07/10 17:3022.0 7.1Benzaldehyde ND ug/L 1 09/16/10 13:06 100-52-709/07/10 17:3022.0 13.2Benzo(a)anthracene ND ug/L 1 09/16/10 13:06 56-55-309/07/10 17:3011.0 2.5Benzo(a)pyrene ND ug/L 1 09/16/10 13:06 50-32-809/07/10 17:3011.0 2.2Benzo(b)fluoranthene ND ug/L 1 09/16/10 13:06 205-99-209/07/10 17:3011.0 2.0Benzo(g,h,i)perylene ND ug/L 1 09/16/10 13:06 191-24-209/07/10 17:3011.0 2.9Benzo(k)fluoranthene ND ug/L 1 09/16/10 13:06 207-08-909/07/10 17:3011.0 2.2Biphenyl (Diphenyl) ND ug/L 1 09/16/10 13:06 92-52-409/07/10 17:3011.0 3.54-Bromophenylphenyl ether ND ug/L 1 09/16/10 13:06 101-55-309/07/10 17:3011.0 3.4Butylbenzylphthalate ND ug/L 1 09/16/10 13:06 85-68-709/07/10 17:3011.0 2.2Caprolactam ND ug/L 1 09/16/10 13:06 105-60-209/07/10 17:3011.0 2.3Carbazole ND ug/L 1 09/16/10 13:06 86-74-809/07/10 17:3011.0 2.64-Chloro-3-methylphenol ND ug/L 1 09/16/10 13:06 59-50-709/07/10 17:3022.0 8.94-Chloroaniline ND ug/L 1 09/16/10 13:06 106-47-809/07/10 17:3022.0 18.7bis(2-Chloroethoxy)methane ND ug/L 1 09/16/10 13:06 111-91-109/07/10 17:3011.0 3.5bis(2-Chloroethyl) ether ND ug/L 1 09/16/10 13:06 111-44-409/07/10 17:3011.0 3.8bis(2-Chloroisopropyl) ether ND ug/L 1 09/16/10 13:06 108-60-109/07/10 17:3011.0 3.22-Chloronaphthalene ND ug/L 1 09/16/10 13:06 91-58-709/07/10 17:3011.0 4.02-Chlorophenol ND ug/L 1 09/16/10 13:06 95-57-809/07/10 17:3011.0 3.84-Chlorophenylphenyl ether ND ug/L 1 09/16/10 13:06 7005-72-309/07/10 17:3011.0 3.8Chrysene ND ug/L 1 09/16/10 13:06 218-01-909/07/10 17:3011.0 2.5Dibenz(a,h)anthracene ND ug/L 1 09/16/10 13:06 53-70-309/07/10 17:3011.0 3.1Dibenzofuran ND ug/L 1 09/16/10 13:06 132-64-909/07/10 17:3011.0 3.63,3'-Dichlorobenzidine ND ug/L 1 09/16/10 13:06 91-94-109/07/10 17:3022.0 10.4



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2,4-Dichlorophenol ND ug/L 1 09/16/10 13:06 120-83-209/07/10 17:3011.0 4.8Diethylphthalate ND ug/L 1 09/16/10 13:06 84-66-209/07/10 17:3011.0 3.02,4-Dimethylphenol ND ug/L 1 09/16/10 13:06 105-67-909/07/10 17:3011.0 9.9Dimethylphthalate ND ug/L 1 09/16/10 13:06 131-11-309/07/10 17:3011.0 2.5Di-n-butylphthalate ND ug/L 1 09/16/10 13:06 84-74-209/07/10 17:3011.0 2.24,6-Dinitro-2-methylphenol ND ug/L 1 09/16/10 13:06 534-52-109/07/10 17:3022.0 4.22,4-Dinitrophenol ND ug/L 1 09/16/10 13:06 51-28-509/07/10 17:3054.9 9.72,4-Dinitrotoluene ND ug/L 1 09/16/10 13:06 121-14-209/07/10 17:3011.0 2.72,6-Dinitrotoluene ND ug/L 1 09/16/10 13:06 606-20-209/07/10 17:3011.0 2.7Di-n-octylphthalate ND ug/L 1 09/16/10 13:06 117-84-009/07/10 17:3011.0 1.6bis(2-Ethylhexyl)phthalate ND ug/L 1 09/16/10 13:06 117-81-709/07/10 17:306.6 2.4Fluoranthene ND ug/L 1 09/16/10 13:06 206-44-009/07/10 17:3011.0 2.6Fluorene ND ug/L 1 09/16/10 13:06 86-73-709/07/10 17:3011.0 3.4Hexachloro-1,3-butadiene ND ug/L 1 09/16/10 13:06 87-68-309/07/10 17:3011.0 3.2Hexachlorobenzene ND ug/L 1 09/16/10 13:06 118-74-109/07/10 17:3011.0 3.5Hexachlorocyclopentadiene ND ug/L 1 09/16/10 13:06 77-47-409/07/10 17:3011.0 2.5Hexachloroethane ND ug/L 1 09/16/10 13:06 67-72-109/07/10 17:3011.0 3.0Indeno(1,2,3-cd)pyrene ND ug/L 1 09/16/10 13:06 193-39-509/07/10 17:3011.0 3.0Isophorone ND ug/L 1 09/16/10 13:06 78-59-109/07/10 17:3011.0 3.62-Methylnaphthalene ND ug/L 1 09/16/10 13:06 91-57-609/07/10 17:3011.0 4.62-Methylphenol(o-Cresol) ND ug/L 1 09/16/10 13:06 95-48-709/07/10 17:3011.0 4.03&4-Methylphenol(m&p Cresol) ND ug/L 1 09/16/10 13:0609/07/10 17:3011.0 3.6Naphthalene ND ug/L 1 09/16/10 13:06 91-20-309/07/10 17:3011.0 4.42-Nitroaniline ND ug/L 1 09/16/10 13:06 88-74-409/07/10 17:3054.9 14.33-Nitroaniline ND ug/L 1 09/16/10 13:06 99-09-209/07/10 17:3054.9 14.34-Nitroaniline ND ug/L 1 09/16/10 13:06 100-01-609/07/10 17:3022.0 15.4Nitrobenzene ND ug/L 1 09/16/10 13:06 98-95-309/07/10 17:3011.0 3.82-Nitrophenol ND ug/L 1 09/16/10 13:06 88-75-509/07/10 17:3011.0 3.74-Nitrophenol ND ug/L 1 09/16/10 13:06 100-02-709/07/10 17:3054.9 5.4N-Nitroso-di-n-propylamine ND ug/L 1 09/16/10 13:06 621-64-709/07/10 17:3011.0 4.1N-Nitrosodiphenylamine ND ug/L 1 09/16/10 13:06 86-30-609/07/10 17:3011.0 3.3Pentachlorophenol ND ug/L 1 09/16/10 13:06 87-86-509/07/10 17:3027.5 19.8Phenanthrene ND ug/L 1 09/16/10 13:06 85-01-809/07/10 17:3011.0 2.7Phenol ND ug/L 1 09/16/10 13:06 108-95-209/07/10 17:3011.0 1.8Pyrene ND ug/L 1 09/16/10 13:06 129-00-009/07/10 17:3011.0 2.31,2,4,5-Tetrachlorobenzene ND ug/L 1 09/16/10 13:06 95-94-309/07/10 17:3011.0 4.42,3,4,6-Tetrachlorophenol ND ug/L 1 09/16/10 13:06 58-90-209/07/10 17:3011.0 1.82,4,5-Trichlorophenol ND ug/L 1 09/16/10 13:06 95-95-409/07/10 17:3011.0 2.32,4,6-Trichlorophenol ND ug/L 1 09/16/10 13:06 88-06-209/07/10 17:3011.0 2.0Nitrobenzene-d5 (S) 42 % 1 09/16/10 13:06 4165-60-009/07/10 17:3021-1102-Fluorobiphenyl (S) 45 % 1 09/16/10 13:06 321-60-809/07/10 17:3027-110Terphenyl-d14 (S) 64 % 1 09/16/10 13:06 1718-51-009/07/10 17:3031-107Phenol-d6 (S) 13 % 1 09/16/10 13:06 13127-88-309/07/10 17:3010-1102-Fluorophenol (S) 19 % 1 09/16/10 13:06 367-12-409/07/10 17:3012-1102,4,6-Tribromophenol (S) 72 % 1 09/16/10 13:06 118-79-609/07/10 17:3027-110



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8260 MSV Low Level Analytical Method: EPA 8260

Acetone 2.5J ug/L 1 09/02/10 13:27 67-64-125.0 2.2Benzene ND ug/L 1 09/02/10 13:27 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/02/10 13:27 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/02/10 13:27 75-27-41.0 0.18Bromoform ND ug/L 1 09/02/10 13:27 75-25-21.0 0.26Bromomethane ND ug/L 1 09/02/10 13:27 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/02/10 13:27 78-93-35.0 0.96Carbon disulfide 50.4 ug/L 1 09/02/10 13:27 75-15-0 C02.0 1.2Carbon tetrachloride ND ug/L 1 09/02/10 13:27 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/02/10 13:27 108-90-71.0 0.23Chloroethane ND ug/L 1 09/02/10 13:27 75-00-31.0 0.54Chloroform ND ug/L 1 09/02/10 13:27 67-66-31.0 0.14Chloromethane ND ug/L 1 09/02/10 13:27 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/02/10 13:27 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/02/10 13:27 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/02/10 13:27 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/02/10 13:27 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/02/10 13:27 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/02/10 13:27 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/02/10 13:27 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/02/10 13:27 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/02/10 13:27 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/02/10 13:27 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/02/10 13:27 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/02/10 13:27 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/02/10 13:27 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/02/10 13:27 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/02/10 13:27 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/02/10 13:27 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/02/10 13:27 100-41-41.0 0.302-Hexanone ND ug/L 1 09/02/10 13:27 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/02/10 13:27 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/02/10 13:27 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/02/10 13:27 108-87-210.0 1.9Methylene Chloride ND ug/L 1 09/02/10 13:27 75-09-22.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/02/10 13:27 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/02/10 13:27 1634-04-41.0 0.21Styrene ND ug/L 1 09/02/10 13:27 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/02/10 13:27 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/02/10 13:27 127-18-41.0 0.46Toluene ND ug/L 1 09/02/10 13:27 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/02/10 13:27 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/02/10 13:27 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/02/10 13:27 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/02/10 13:27 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/02/10 13:27 79-01-61.0 0.47



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Trichlorofluoromethane ND ug/L 1 09/02/10 13:27 75-69-41.0 0.201,1,2-Trichlorotrifluoroethane ND ug/L 1 09/02/10 13:27 76-13-11.0 0.19Vinyl chloride ND ug/L 1 09/02/10 13:27 75-01-41.0 0.62Xylene (Total) ND ug/L 1 09/02/10 13:27 1330-20-72.0 0.66m&p-Xylene ND ug/L 1 09/02/10 13:27 179601-23-12.0 0.66o-Xylene ND ug/L 1 09/02/10 13:27 95-47-61.0 0.234-Bromofluorobenzene (S) 93 % 1 09/02/10 13:27 460-00-470-130Dibromofluoromethane (S) 100 % 1 09/02/10 13:27 1868-53-770-1301,2-Dichloroethane-d4 (S) 100 % 1 09/02/10 13:27 17060-07-070-130Toluene-d8 (S) 101 % 1 09/02/10 13:27 2037-26-570-130


Cyanide ND mg/L 1 09/05/10 14:13 57-12-50.0050 0.0050



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Sample: EB-01 Lab ID: 9276750041 Collected: 08/31/10 16:30 Received: 09/01/10 14:00 Matrix: Water


6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C

Antimony ND ug/L 1 09/07/10 22:42 7440-36-009/02/10 10:355.0 2.6Arsenic ND ug/L 1 09/07/10 22:42 7440-38-209/02/10 10:355.0 2.7Beryllium 0.11J ug/L 1 09/07/10 22:42 7440-41-709/02/10 10:351.0 0.10Cadmium ND ug/L 1 09/07/10 22:42 7440-43-909/02/10 10:351.0 0.50Chromium 1.1J ug/L 1 09/07/10 22:42 7440-47-309/02/10 10:355.0 0.40Copper 0.89J ug/L 1 09/07/10 22:42 7440-50-809/02/10 10:355.0 0.30Lead ND ug/L 1 09/07/10 22:42 7439-92-109/02/10 10:355.0 4.0Manganese 2.0J ug/L 1 09/07/10 22:42 7439-96-509/02/10 10:355.0 0.30Nickel ND ug/L 1 09/07/10 22:42 7440-02-009/02/10 10:355.0 1.7Selenium ND ug/L 1 09/07/10 22:42 7782-49-209/02/10 10:3510.0 3.8Silver ND ug/L 1 09/07/10 22:42 7440-22-409/02/10 10:355.0 0.10Thallium 3.7J ug/L 1 09/07/10 22:42 7440-28-0 L009/02/10 10:3510.0 3.0Zinc 24.5 ug/L 1 09/07/10 22:42 7440-66-6 B09/02/10 10:3510.0 0.40


Mercury ND ug/L 1 09/07/10 18:47 7439-97-609/02/10 18:300.20 0.070


Acenaphthene ND ug/L 1 09/16/10 21:52 83-32-909/07/10 17:3010.0 1.9Acenaphthylene ND ug/L 1 09/16/10 21:52 208-96-809/07/10 17:3010.0 3.2Acetophenone ND ug/L 1 09/16/10 21:52 98-86-209/07/10 17:3010.0 3.7Anthracene ND ug/L 1 09/16/10 21:52 120-12-709/07/10 17:3010.0 2.5Atrazine ND ug/L 1 09/16/10 21:52 1912-24-909/07/10 17:3020.0 6.5Benzaldehyde ND ug/L 1 09/16/10 21:52 100-52-709/07/10 17:3020.0 12.0Benzo(a)anthracene ND ug/L 1 09/16/10 21:52 56-55-309/07/10 17:3010.0 2.3Benzo(a)pyrene ND ug/L 1 09/16/10 21:52 50-32-809/07/10 17:3010.0 2.0Benzo(b)fluoranthene ND ug/L 1 09/16/10 21:52 205-99-209/07/10 17:3010.0 1.8Benzo(g,h,i)perylene ND ug/L 1 09/16/10 21:52 191-24-209/07/10 17:3010.0 2.6Benzo(k)fluoranthene ND ug/L 1 09/16/10 21:52 207-08-909/07/10 17:3010.0 2.0Biphenyl (Diphenyl) ND ug/L 1 09/16/10 21:52 92-52-409/07/10 17:3010.0 3.24-Bromophenylphenyl ether ND ug/L 1 09/16/10 21:52 101-55-309/07/10 17:3010.0 3.1Butylbenzylphthalate ND ug/L 1 09/16/10 21:52 85-68-709/07/10 17:3010.0 2.0Caprolactam ND ug/L 1 09/16/10 21:52 105-60-209/07/10 17:3010.0 2.1Carbazole ND ug/L 1 09/16/10 21:52 86-74-809/07/10 17:3010.0 2.44-Chloro-3-methylphenol ND ug/L 1 09/16/10 21:52 59-50-709/07/10 17:3020.0 8.14-Chloroaniline ND ug/L 1 09/16/10 21:52 106-47-809/07/10 17:3020.0 17.0bis(2-Chloroethoxy)methane ND ug/L 1 09/16/10 21:52 111-91-109/07/10 17:3010.0 3.2bis(2-Chloroethyl) ether ND ug/L 1 09/16/10 21:52 111-44-409/07/10 17:3010.0 3.5bis(2-Chloroisopropyl) ether ND ug/L 1 09/16/10 21:52 108-60-109/07/10 17:3010.0 2.92-Chloronaphthalene ND ug/L 1 09/16/10 21:52 91-58-709/07/10 17:3010.0 3.62-Chlorophenol ND ug/L 1 09/16/10 21:52 95-57-809/07/10 17:3010.0 3.54-Chlorophenylphenyl ether ND ug/L 1 09/16/10 21:52 7005-72-309/07/10 17:3010.0 3.5Chrysene ND ug/L 1 09/16/10 21:52 218-01-909/07/10 17:3010.0 2.3Dibenz(a,h)anthracene ND ug/L 1 09/16/10 21:52 53-70-309/07/10 17:3010.0 2.8Dibenzofuran ND ug/L 1 09/16/10 21:52 132-64-909/07/10 17:3010.0 3.33,3'-Dichlorobenzidine ND ug/L 1 09/16/10 21:52 91-94-109/07/10 17:3020.0 9.5



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(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




2,4-Dichlorophenol ND ug/L 1 09/16/10 21:52 120-83-209/07/10 17:3010.0 4.4Diethylphthalate ND ug/L 1 09/16/10 21:52 84-66-209/07/10 17:3010.0 2.72,4-Dimethylphenol ND ug/L 1 09/16/10 21:52 105-67-909/07/10 17:3010.0 9.0Dimethylphthalate ND ug/L 1 09/16/10 21:52 131-11-309/07/10 17:3010.0 2.3Di-n-butylphthalate ND ug/L 1 09/16/10 21:52 84-74-209/07/10 17:3010.0 2.04,6-Dinitro-2-methylphenol ND ug/L 1 09/16/10 21:52 534-52-109/07/10 17:3020.0 3.82,4-Dinitrophenol ND ug/L 1 09/16/10 21:52 51-28-509/07/10 17:3050.0 8.82,4-Dinitrotoluene ND ug/L 1 09/16/10 21:52 121-14-209/07/10 17:3010.0 2.52,6-Dinitrotoluene ND ug/L 1 09/16/10 21:52 606-20-209/07/10 17:3010.0 2.5Di-n-octylphthalate ND ug/L 1 09/16/10 21:52 117-84-009/07/10 17:3010.0 1.5bis(2-Ethylhexyl)phthalate ND ug/L 1 09/16/10 21:52 117-81-709/07/10 17:306.0 2.2Fluoranthene ND ug/L 1 09/16/10 21:52 206-44-009/07/10 17:3010.0 2.4Fluorene ND ug/L 1 09/16/10 21:52 86-73-709/07/10 17:3010.0 3.1Hexachloro-1,3-butadiene ND ug/L 1 09/16/10 21:52 87-68-309/07/10 17:3010.0 2.9Hexachlorobenzene ND ug/L 1 09/16/10 21:52 118-74-109/07/10 17:3010.0 3.2Hexachlorocyclopentadiene ND ug/L 1 09/16/10 21:52 77-47-409/07/10 17:3010.0 2.3Hexachloroethane ND ug/L 1 09/16/10 21:52 67-72-109/07/10 17:3010.0 2.7Indeno(1,2,3-cd)pyrene ND ug/L 1 09/16/10 21:52 193-39-509/07/10 17:3010.0 2.7Isophorone ND ug/L 1 09/16/10 21:52 78-59-109/07/10 17:3010.0 3.32-Methylnaphthalene ND ug/L 1 09/16/10 21:52 91-57-609/07/10 17:3010.0 4.22-Methylphenol(o-Cresol) ND ug/L 1 09/16/10 21:52 95-48-709/07/10 17:3010.0 3.63&4-Methylphenol(m&p Cresol) ND ug/L 1 09/16/10 21:5209/07/10 17:3010.0 3.3Naphthalene ND ug/L 1 09/16/10 21:52 91-20-309/07/10 17:3010.0 4.02-Nitroaniline ND ug/L 1 09/16/10 21:52 88-74-409/07/10 17:3050.0 13.03-Nitroaniline ND ug/L 1 09/16/10 21:52 99-09-209/07/10 17:3050.0 13.04-Nitroaniline ND ug/L 1 09/16/10 21:52 100-01-609/07/10 17:3020.0 14.0Nitrobenzene ND ug/L 1 09/16/10 21:52 98-95-309/07/10 17:3010.0 3.52-Nitrophenol ND ug/L 1 09/16/10 21:52 88-75-509/07/10 17:3010.0 3.44-Nitrophenol ND ug/L 1 09/16/10 21:52 100-02-709/07/10 17:3050.0 4.9N-Nitroso-di-n-propylamine ND ug/L 1 09/16/10 21:52 621-64-709/07/10 17:3010.0 3.7N-Nitrosodiphenylamine ND ug/L 1 09/16/10 21:52 86-30-609/07/10 17:3010.0 3.0Pentachlorophenol ND ug/L 1 09/16/10 21:52 87-86-509/07/10 17:3025.0 18.0Phenanthrene ND ug/L 1 09/16/10 21:52 85-01-809/07/10 17:3010.0 2.5Phenol ND ug/L 1 09/16/10 21:52 108-95-209/07/10 17:3010.0 1.6Pyrene ND ug/L 1 09/16/10 21:52 129-00-009/07/10 17:3010.0 2.11,2,4,5-Tetrachlorobenzene ND ug/L 1 09/16/10 21:52 95-94-309/07/10 17:3010.0 4.02,3,4,6-Tetrachlorophenol ND ug/L 1 09/16/10 21:52 58-90-209/07/10 17:3010.0 1.62,4,5-Trichlorophenol ND ug/L 1 09/16/10 21:52 95-95-409/07/10 17:3010.0 2.12,4,6-Trichlorophenol ND ug/L 1 09/16/10 21:52 88-06-209/07/10 17:3010.0 1.8Nitrobenzene-d5 (S) 46 % 1 09/16/10 21:52 4165-60-009/07/10 17:3021-1102-Fluorobiphenyl (S) 50 % 1 09/16/10 21:52 321-60-809/07/10 17:3027-110Terphenyl-d14 (S) 71 % 1 09/16/10 21:52 1718-51-009/07/10 17:3031-107Phenol-d6 (S) 14 % 1 09/16/10 21:52 13127-88-309/07/10 17:3010-1102-Fluorophenol (S) 24 % 1 09/16/10 21:52 367-12-409/07/10 17:3012-1102,4,6-Tribromophenol (S) 86 % 1 09/16/10 21:52 118-79-609/07/10 17:3027-110



Date: 09/27/2010 06:23 PM Page 169 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744




Acetone ND ug/L 1 09/02/10 13:52 67-64-125.0 2.2Benzene ND ug/L 1 09/02/10 13:52 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/02/10 13:52 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/02/10 13:52 75-27-41.0 0.18Bromoform ND ug/L 1 09/02/10 13:52 75-25-21.0 0.26Bromomethane ND ug/L 1 09/02/10 13:52 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/02/10 13:52 78-93-35.0 0.96Carbon disulfide ND ug/L 1 09/02/10 13:52 75-15-02.0 1.2Carbon tetrachloride ND ug/L 1 09/02/10 13:52 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/02/10 13:52 108-90-71.0 0.23Chloroethane ND ug/L 1 09/02/10 13:52 75-00-31.0 0.54Chloroform ND ug/L 1 09/02/10 13:52 67-66-31.0 0.14Chloromethane ND ug/L 1 09/02/10 13:52 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/02/10 13:52 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/02/10 13:52 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/02/10 13:52 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/02/10 13:52 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/02/10 13:52 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/02/10 13:52 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/02/10 13:52 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/02/10 13:52 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/02/10 13:52 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/02/10 13:52 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/02/10 13:52 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/02/10 13:52 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/02/10 13:52 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/02/10 13:52 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/02/10 13:52 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/02/10 13:52 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/02/10 13:52 100-41-41.0 0.302-Hexanone ND ug/L 1 09/02/10 13:52 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/02/10 13:52 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/02/10 13:52 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/02/10 13:52 108-87-210.0 1.9Methylene Chloride 6.3 ug/L 1 09/02/10 13:52 75-09-2 C92.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/02/10 13:52 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/02/10 13:52 1634-04-41.0 0.21Styrene ND ug/L 1 09/02/10 13:52 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/02/10 13:52 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/02/10 13:52 127-18-41.0 0.46Toluene ND ug/L 1 09/02/10 13:52 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/02/10 13:52 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/02/10 13:52 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/02/10 13:52 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/02/10 13:52 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/02/10 13:52 79-01-61.0 0.47



Date: 09/27/2010 06:23 PM Page 170 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744






Cyanide ND mg/L 1 09/05/10 14:14 57-12-50.0050 0.0050



Date: 09/27/2010 06:23 PM Page 171 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: FB-01 Lab ID: 9276750042 Collected: 08/31/10 16:45 Received: 09/01/10 14:00 Matrix: Water



Acetone ND ug/L 1 09/02/10 14:18 67-64-125.0 2.2Benzene ND ug/L 1 09/02/10 14:18 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/02/10 14:18 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/02/10 14:18 75-27-41.0 0.18Bromoform ND ug/L 1 09/02/10 14:18 75-25-21.0 0.26Bromomethane ND ug/L 1 09/02/10 14:18 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/02/10 14:18 78-93-35.0 0.96Carbon disulfide ND ug/L 1 09/02/10 14:18 75-15-02.0 1.2Carbon tetrachloride ND ug/L 1 09/02/10 14:18 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/02/10 14:18 108-90-71.0 0.23Chloroethane ND ug/L 1 09/02/10 14:18 75-00-31.0 0.54Chloroform ND ug/L 1 09/02/10 14:18 67-66-31.0 0.14Chloromethane ND ug/L 1 09/02/10 14:18 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/02/10 14:18 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/02/10 14:18 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/02/10 14:18 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/02/10 14:18 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/02/10 14:18 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/02/10 14:18 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/02/10 14:18 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/02/10 14:18 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/02/10 14:18 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/02/10 14:18 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/02/10 14:18 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/02/10 14:18 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/02/10 14:18 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/02/10 14:18 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/02/10 14:18 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/02/10 14:18 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/02/10 14:18 100-41-41.0 0.302-Hexanone ND ug/L 1 09/02/10 14:18 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/02/10 14:18 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/02/10 14:18 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/02/10 14:18 108-87-210.0 1.9Methylene Chloride 8.7 ug/L 1 09/02/10 14:18 75-09-2 C92.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/02/10 14:18 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/02/10 14:18 1634-04-41.0 0.21Styrene ND ug/L 1 09/02/10 14:18 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/02/10 14:18 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/02/10 14:18 127-18-41.0 0.46Toluene ND ug/L 1 09/02/10 14:18 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/02/10 14:18 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/02/10 14:18 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/02/10 14:18 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/02/10 14:18 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/02/10 14:18 79-01-61.0 0.47



Date: 09/27/2010 06:23 PM Page 172 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: FB-01 Lab ID: 9276750042 Collected: 08/31/10 16:45 Received: 09/01/10 14:00 Matrix: Water






Date: 09/27/2010 06:23 PM Page 173 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: TB-01 Lab ID: 9276750043 Collected: 08/30/10 00:00 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "wet-weight" basis



Acetone ND ug/kg 1 09/05/10 11:35 67-64-1100 10.0Benzene ND ug/kg 1 09/05/10 11:35 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/05/10 11:35 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/05/10 11:35 75-27-45.0 1.9Bromoform ND ug/kg 1 09/05/10 11:35 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/05/10 11:35 74-83-910.0 2.52-Butanone (MEK) ND ug/kg 1 09/05/10 11:35 78-93-3100 2.9Carbon disulfide ND ug/kg 1 09/05/10 11:35 75-15-010.0 3.0Carbon tetrachloride ND ug/kg 1 09/05/10 11:35 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/05/10 11:35 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/05/10 11:35 75-00-310.0 2.4Chloroform ND ug/kg 1 09/05/10 11:35 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/05/10 11:35 74-87-310.0 2.4Cyclohexane ND ug/kg 1 09/05/10 11:35 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/05/10 11:35 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/05/10 11:35 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/05/10 11:35 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/05/10 11:35 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/05/10 11:35 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/05/10 11:35 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/05/10 11:35 75-71-810.0 3.61,1-Dichloroethane ND ug/kg 1 09/05/10 11:35 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/05/10 11:35 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/05/10 11:35 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/05/10 11:35 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/05/10 11:35 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/05/10 11:35 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/05/10 11:35 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/05/10 11:35 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/05/10 11:35 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/05/10 11:35 591-78-650.0 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/05/10 11:35 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/05/10 11:35 79-20-910.0 1.4Methylcyclohexane ND ug/kg 1 09/05/10 11:35 108-87-210.0 1.5Methylene Chloride ND ug/kg 1 09/05/10 11:35 75-09-220.0 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/05/10 11:35 108-10-150.0 3.7Methyl-tert-butyl ether ND ug/kg 1 09/05/10 11:35 1634-04-45.0 1.5Styrene ND ug/kg 1 09/05/10 11:35 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/05/10 11:35 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/05/10 11:35 127-18-45.0 1.7Toluene ND ug/kg 1 09/05/10 11:35 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/05/10 11:35 87-61-65.0 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/05/10 11:35 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/05/10 11:35 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/05/10 11:35 79-00-55.0 2.1



Date: 09/27/2010 06:23 PM Page 174 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744







Date: 09/27/2010 06:23 PM Page 175 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276750MILLS GAP 6686081744

Sample: TB-02 Lab ID: 9276750044 Collected: 08/31/10 00:00 Received: 09/01/10 14:00 Matrix: Water



Acetone 2.5J ug/L 1 09/02/10 14:44 67-64-125.0 2.2Benzene ND ug/L 1 09/02/10 14:44 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/02/10 14:44 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/02/10 14:44 75-27-41.0 0.18Bromoform ND ug/L 1 09/02/10 14:44 75-25-21.0 0.26Bromomethane ND ug/L 1 09/02/10 14:44 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/02/10 14:44 78-93-35.0 0.96Carbon disulfide ND ug/L 1 09/02/10 14:44 75-15-02.0 1.2Carbon tetrachloride ND ug/L 1 09/02/10 14:44 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/02/10 14:44 108-90-71.0 0.23Chloroethane ND ug/L 1 09/02/10 14:44 75-00-31.0 0.54Chloroform ND ug/L 1 09/02/10 14:44 67-66-31.0 0.14Chloromethane 0.16J ug/L 1 09/02/10 14:44 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/02/10 14:44 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/02/10 14:44 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/02/10 14:44 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/02/10 14:44 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/02/10 14:44 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/02/10 14:44 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/02/10 14:44 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/02/10 14:44 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/02/10 14:44 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/02/10 14:44 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/02/10 14:44 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/02/10 14:44 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/02/10 14:44 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/02/10 14:44 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/02/10 14:44 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/02/10 14:44 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/02/10 14:44 100-41-41.0 0.302-Hexanone ND ug/L 1 09/02/10 14:44 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/02/10 14:44 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/02/10 14:44 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/02/10 14:44 108-87-210.0 1.9Methylene Chloride ND ug/L 1 09/02/10 14:44 75-09-22.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/02/10 14:44 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/02/10 14:44 1634-04-41.0 0.21Styrene ND ug/L 1 09/02/10 14:44 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/02/10 14:44 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/02/10 14:44 127-18-41.0 0.46Toluene ND ug/L 1 09/02/10 14:44 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/02/10 14:44 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/02/10 14:44 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/02/10 14:44 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/02/10 14:44 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/02/10 14:44 79-01-61.0 0.47



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Acetone ND ug/kg 1 09/08/10 00:58 67-64-1100 10.0Benzene ND ug/kg 1 09/08/10 00:58 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/08/10 00:58 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/08/10 00:58 75-27-45.0 1.9Bromoform ND ug/kg 1 09/08/10 00:58 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/08/10 00:58 74-83-910.0 2.52-Butanone (MEK) ND ug/kg 1 09/08/10 00:58 78-93-3100 2.9Carbon disulfide ND ug/kg 1 09/08/10 00:58 75-15-010.0 3.0Carbon tetrachloride ND ug/kg 1 09/08/10 00:58 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/08/10 00:58 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/08/10 00:58 75-00-310.0 2.4Chloroform ND ug/kg 1 09/08/10 00:58 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/08/10 00:58 74-87-310.0 2.4Cyclohexane ND ug/kg 1 09/08/10 00:58 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 00:58 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/08/10 00:58 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 00:58 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/08/10 00:58 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/08/10 00:58 541-73-15.0 2.01,4-Dichlorobenzene 3.3J ug/kg 1 09/08/10 00:58 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/08/10 00:58 75-71-810.0 3.61,1-Dichloroethane ND ug/kg 1 09/08/10 00:58 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/08/10 00:58 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/08/10 00:58 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 00:58 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 00:58 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/08/10 00:58 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 00:58 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 00:58 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/08/10 00:58 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/08/10 00:58 591-78-650.0 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 00:58 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/08/10 00:58 79-20-910.0 1.4Methylcyclohexane ND ug/kg 1 09/08/10 00:58 108-87-210.0 1.5Methylene Chloride ND ug/kg 1 09/08/10 00:58 75-09-220.0 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 00:58 108-10-150.0 3.7Methyl-tert-butyl ether ND ug/kg 1 09/08/10 00:58 1634-04-45.0 1.5Styrene ND ug/kg 1 09/08/10 00:58 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 00:58 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/08/10 00:58 127-18-45.0 1.7Toluene ND ug/kg 1 09/08/10 00:58 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 00:58 87-61-65.0 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 00:58 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/08/10 00:58 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/08/10 00:58 79-00-55.0 2.1



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QUALITY CONTROL DATA


9276750MILLS GAP 6686081744

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

MPRP/7021EPA 3050

EPA 60106010 MET

Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005, 9276750006, 9276750007, 9276750009,9276750013, 9276750014, 9276750015, 9276750016, 9276750017

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 493840


Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/10/10 14:01Arsenic mg/kg ND 0.50 09/10/10 14:01Beryllium mg/kg ND 0.10 09/10/10 14:01Cadmium mg/kg ND 0.10 09/10/10 14:01Chromium mg/kg ND 0.50 09/10/10 14:01Copper mg/kg ND 0.50 09/10/10 14:01Lead mg/kg ND 0.50 09/10/10 14:01Manganese mg/kg 0.17J 0.50 09/10/10 14:01Nickel mg/kg ND 0.50 09/10/10 14:01Selenium mg/kg ND 1.0 09/10/10 14:01Silver mg/kg ND 0.50 09/10/10 14:01Thallium mg/kg ND 1.0 09/10/10 14:01Zinc mg/kg ND 1.0 09/10/10 14:01

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

493841LABORATORY CONTROL SAMPLE:LCSSpike

Antimony mg/kg 51.150 102 80-120Arsenic mg/kg 51.350 103 80-120Beryllium mg/kg 51.350 103 80-120Cadmium mg/kg 51.150 102 80-120Chromium mg/kg 51.650 103 80-120Copper mg/kg 52.250 104 80-120Lead mg/kg 51.450 103 80-120Manganese mg/kg 51.250 102 80-120Nickel mg/kg 51.350 103 80-120Selenium mg/kg 49.750 99 80-120Silver mg/kg 24.025 96 80-120Thallium mg/kg 50.950 102 80-120Zinc mg/kg 51.350 103 80-120

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

493842MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

9276750003

493843

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M0,R135.9 19 75-12527 37 2044.5ND 11.3 16.4Arsenic mg/kg M035.9 60 75-12556 12 2044.5ND 27.3 30.7Beryllium mg/kg 35.9 80 75-12578 17 2044.55.1 33.9 40.0



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Parameter UnitsMS



MSSpikeResult

9276750003

493843

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Cadmium mg/kg 35.9 81 75-12580 19 2044.5ND 29.1 35.4Chromium mg/kg M035.9 48 75-12543 4 2044.535.8 53.0 55.1Copper mg/kg M035.9 63 75-12552 1 2044.551.6 74.2 74.7Lead mg/kg M035.9 74 75-12569 8 2044.517.8 44.5 48.4Manganese mg/kg M035.9 -305 75-125-303 4 2044.5833 724 699Nickel mg/kg 35.9 90 75-12577 4 2044.518.6 51.0 52.8Selenium mg/kg M035.9 66 75-12563 18 2044.5ND 23.5 28.1Silver mg/kg 17.9 76 75-12577 20 2022.21.5J 15.2 18.7Thallium mg/kg M0,R135.9 65 75-12571 26 2044.5ND 27.3 35.5Zinc mg/kg M035.9 -120 75-125-117 7 2044.5181 138 129



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MPRP/7030EPA 3050

EPA 60106010 MET

Associated Lab Samples: 9276750018, 9276750019, 9276750020, 9276750021, 9276750022, 9276750023, 9276750024, 9276750025,9276750026, 9276750027, 9276750028, 9276750029, 9276750030, 9276750037





Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/15/10 07:52Arsenic mg/kg ND 0.50 09/15/10 07:52Beryllium mg/kg ND 0.10 09/15/10 07:52Cadmium mg/kg ND 0.10 09/15/10 07:52Chromium mg/kg ND 0.50 09/15/10 07:52Copper mg/kg ND 0.50 09/15/10 07:52Lead mg/kg ND 0.50 09/15/10 07:52Manganese mg/kg 0.33J 0.50 09/15/10 07:52Nickel mg/kg ND 0.50 09/15/10 07:52Selenium mg/kg ND 1.0 09/15/10 07:52Silver mg/kg ND 0.50 09/15/10 07:52Thallium mg/kg ND 1.0 09/15/10 07:52Zinc mg/kg 0.31J 1.0 09/15/10 07:52

Parameter UnitsLCS



Antimony mg/kg 49.850 100 80-120Arsenic mg/kg 50.250 100 80-120Beryllium mg/kg 50.850 102 80-120Cadmium mg/kg 50.650 101 80-120Chromium mg/kg 50.450 101 80-120Copper mg/kg 51.950 104 80-120Lead mg/kg 50.850 102 80-120Manganese mg/kg 51.050 102 80-120Nickel mg/kg 50.450 101 80-120Selenium mg/kg 49.650 99 80-120Silver mg/kg 22.925 92 80-120Thallium mg/kg 48.950 98 80-120Zinc mg/kg 50.650 101 80-120

Parameter UnitsMS



MSSpikeResult

9276750027

494450

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M045.7 45 75-12548 16 2050.8ND 21.5 25.1Arsenic mg/kg M045.7 62 75-12559 5 2050.8ND 31.0 32.6Beryllium mg/kg 45.7 90 75-12588 8 2050.81.5 42.4 45.9



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Parameter UnitsMS



MSSpikeResult

9276750027

494450

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Cadmium mg/kg 45.7 83 75-12582 9 2050.8ND 38.0 41.7Chromium mg/kg M0,R145.7 137 75-12585 27 2050.819.1 82.0 62.4Copper mg/kg 45.7 87 75-12580 2 2050.816.0 55.6 56.9Lead mg/kg 45.7 104 75-12582 11 2050.89.4 57.1 51.3Manganese mg/kg M0,R145.7 669 75-125-46 40 2050.8692 998 669Nickel mg/kg 45.7 110 75-12581 15 2050.816.8 67.2 57.9Selenium mg/kg M045.7 63 75-12556 0 2050.8ND 30.8 30.8Silver mg/kg 22.8 79 75-12577 8 2025.3ND 18.0 19.6Thallium mg/kg 45.7 76 75-12577 12 2050.8ND 34.5 38.9Zinc mg/kg M0,R145.7 149 75-12581 26 2050.848.9 117 89.9



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MPRP/6996SM 3030C

EPA 60106010 MET 3030C

Associated Lab Samples: 9276750040, 9276750041





Matrix: Water

Analyzed

Antimony ug/L ND 5.0 09/07/10 21:37Arsenic ug/L ND 5.0 09/07/10 21:37Beryllium ug/L ND 1.0 09/07/10 21:37Cadmium ug/L ND 1.0 09/07/10 21:37Chromium ug/L 7.7 5.0 B09/07/10 21:37Copper ug/L 7.6 5.0 B09/07/10 21:37Lead ug/L 48.7 5.0 B09/07/10 21:37Manganese ug/L 5.7 5.0 B09/07/10 21:37Nickel ug/L 5.9 5.0 B09/07/10 21:37Selenium ug/L ND 10.0 09/07/10 21:37Silver ug/L 0.25J 5.0 09/07/10 21:37Thallium ug/L 5.2J 10.0 09/07/10 21:37Zinc ug/L 25.9 10.0 B09/07/10 21:37

Parameter UnitsLCS



Antimony ug/L 498500 100 80-120Arsenic ug/L 518500 104 80-120Beryllium ug/L 530500 106 80-120Cadmium ug/L 537500 107 80-120Chromium ug/L 503500 101 80-120Copper ug/L 476500 95 80-120Lead ug/L 531500 106 80-120Manganese ug/L 504500 101 80-120Nickel ug/L 514500 103 80-120Selenium ug/L 553500 111 80-120Silver ug/L 229250 92 80-120Thallium ug/L 343 L0500 69 80-120Zinc ug/L 574500 115 80-120

Parameter UnitsMS


492107MATRIX SPIKE SAMPLE:MSSpike

Result9276650013

Antimony ug/L 520500 104 75-125NDArsenic ug/L 550500 109 75-1255.6Beryllium ug/L 545500 109 75-1251.2Cadmium ug/L 559500 112 75-1251.0Chromium ug/L 533500 106 75-125NDCopper ug/L 498500 99 75-125ND



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Parameter UnitsMS



Result9276650013

Lead ug/L 538500 106 75-1258.2Manganese ug/L 586500 105 75-12563.1Nickel ug/L 532500 106 75-125NDSelenium ug/L 551500 109 75-125NDSilver ug/L 237250 93 75-125NDThallium ug/L 422500 79 75-12527.8Zinc ug/L 598500 117 75-12514.2

Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

9276650014492108SAMPLE DUPLICATE:

Antimony ug/L ND 20NDArsenic ug/L ND 20NDBeryllium ug/L 0.12J 20NDCadmium ug/L ND 20NDChromium ug/L ND 20NDCopper ug/L ND 20NDLead ug/L ND 20NDManganese ug/L 20.2 2 2020.6Nickel ug/L ND 20NDSelenium ug/L ND 20NDSilver ug/L 1.3J 20NDThallium ug/L 8.4J 2019.8Zinc ug/L 8.7J 2010.0



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MERP/2998EPA 7470

EPA 74707470 Mercury

Associated Lab Samples: 9276750041





Matrix: Water

Analyzed

Mercury ug/L ND 0.20 09/07/10 17:54

Parameter UnitsLCS



Mercury ug/L 2.82.5 111 80-120

Parameter UnitsMS



MSSpikeResult

9276397002

492495

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 2.5 97 75-12591 7 252.5ND 2.4 2.3

Parameter UnitsMS



MSSpikeResult

9276590003

492497

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 2.5 121 75-125119 2 252.5ND 3.0 3.0



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MERP/3001EPA 7470







Matrix: Water

Analyzed

Mercury ug/L ND 0.20 09/09/10 09:59

Parameter UnitsLCS



Mercury ug/L 2.72.5 109 80-120

Parameter UnitsMS



MSSpikeResult

9276750040

494034

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L 2.5 110 75-125111 0 252.5ND 2.8 2.8

Parameter UnitsMS



MSSpikeResult

9276573001

494036

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L M12.5 64 75-12565 1 252.5ND 1.6 1.6



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MERP/2995EPA 7471


Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005, 9276750009, 9276750013, 9276750014,9276750015, 9276750016





Matrix: Solid

Analyzed

Mercury mg/kg 0.0016J 0.0050 09/03/10 15:27

Parameter UnitsLCS



Mercury mg/kg 0.056.067 84 80-120

Parameter UnitsMS



MSSpikeResult

9276750003

491966

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .06 90 75-12584 1 20.0660.0022J 0.057 0.058

Parameter UnitsMS



MSSpikeResult

9276750005

491968

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M0.07 -8 75-125-8 20.070.0053 ND ND



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MERP/2996EPA 7471


Associated Lab Samples: 9276750006, 9276750007, 9276750017, 9276750018, 9276750019, 9276750020, 9276750022, 9276750023,9276750024, 9276750025, 9276750027, 9276750028, 9276750029, 9276750030, 9276750037




Associated Lab Samples: 9276750006, 9276750007, 9276750017, 9276750018, 9276750019, 9276750020, 9276750022, 9276750023,9276750024, 9276750025, 9276750027, 9276750028, 9276750029, 9276750030, 9276750037

Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/07/10 16:28

Parameter UnitsLCS



Mercury mg/kg 0.072.067 108 80-120

Parameter UnitsMS



MSSpikeResult

9276750027

491980

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg D6,M1.056 85 75-125190 80 20.0590.00043J

0.048 0.11

Parameter UnitsMS



MSSpikeResult

9276750028

491982

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .069 107 75-12588 17 20.071ND 0.073 0.062



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MERP/3004EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/10/10 11:28

Parameter UnitsLCS



Mercury mg/kg 0.062.067 93 80-120

Parameter UnitsMS



MSSpikeResult

9276750026

494572

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .058 85 75-12595 10 20.060.018 0.067 0.074

Parameter UnitsMS



MSSpikeResult

9276872001

494718

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M1.069 58 75-12549 9 20.0670.041 0.080 0.074



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OEXT/11113EPA 3546

EPA 82708270 Solid MSSV Microwave

Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005





Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/09/10 23:332,3,4,6-Tetrachlorophenol ug/kg ND 330 09/09/10 23:332,4,5-Trichlorophenol ug/kg ND 330 09/09/10 23:332,4,6-Trichlorophenol ug/kg ND 330 09/09/10 23:332,4-Dichlorophenol ug/kg ND 330 09/09/10 23:332,4-Dimethylphenol ug/kg ND 330 09/09/10 23:332,4-Dinitrophenol ug/kg ND 1650 09/09/10 23:332,4-Dinitrotoluene ug/kg ND 330 09/09/10 23:332,6-Dinitrotoluene ug/kg ND 330 09/09/10 23:332-Chloronaphthalene ug/kg ND 330 09/09/10 23:332-Chlorophenol ug/kg ND 330 09/09/10 23:332-Methylnaphthalene ug/kg ND 330 09/09/10 23:332-Methylphenol(o-Cresol) ug/kg ND 330 09/09/10 23:332-Nitroaniline ug/kg ND 1650 09/09/10 23:332-Nitrophenol ug/kg ND 330 09/09/10 23:333&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/09/10 23:333,3'-Dichlorobenzidine ug/kg ND 1650 09/09/10 23:333-Nitroaniline ug/kg ND 1650 09/09/10 23:334,6-Dinitro-2-methylphenol ug/kg ND 660 09/09/10 23:334-Bromophenylphenyl ether ug/kg ND 330 09/09/10 23:334-Chloro-3-methylphenol ug/kg ND 660 09/09/10 23:334-Chloroaniline ug/kg ND 1650 09/09/10 23:334-Chlorophenylphenyl ether ug/kg ND 330 09/09/10 23:334-Nitroaniline ug/kg ND 660 09/09/10 23:334-Nitrophenol ug/kg ND 1650 09/09/10 23:33Acenaphthene ug/kg ND 330 09/09/10 23:33Acenaphthylene ug/kg ND 330 09/09/10 23:33Acetophenone ug/kg ND 330 09/09/10 23:33Anthracene ug/kg ND 330 09/09/10 23:33Atrazine ug/kg ND 660 09/09/10 23:33Benzaldehyde ug/kg ND 660 09/09/10 23:33Benzo(a)anthracene ug/kg ND 330 09/09/10 23:33Benzo(a)pyrene ug/kg ND 330 09/09/10 23:33Benzo(b)fluoranthene ug/kg ND 330 09/09/10 23:33Benzo(g,h,i)perylene ug/kg ND 330 09/09/10 23:33Benzo(k)fluoranthene ug/kg ND 330 09/09/10 23:33Biphenyl (Diphenyl) ug/kg ND 330 09/09/10 23:33bis(2-Chloroethoxy)methane ug/kg ND 330 09/09/10 23:33bis(2-Chloroethyl) ether ug/kg ND 330 09/09/10 23:33bis(2-Chloroisopropyl) ether ug/kg ND 330 09/09/10 23:33bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/09/10 23:33Butylbenzylphthalate ug/kg ND 330 09/09/10 23:33Caprolactam ug/kg ND 330 09/09/10 23:33



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(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Carbazole ug/kg ND 330 09/09/10 23:33Chrysene ug/kg ND 330 09/09/10 23:33Di-n-butylphthalate ug/kg ND 330 09/09/10 23:33Di-n-octylphthalate ug/kg ND 330 09/09/10 23:33Dibenz(a,h)anthracene ug/kg ND 330 09/09/10 23:33Dibenzofuran ug/kg ND 330 09/09/10 23:33Diethylphthalate ug/kg ND 330 09/09/10 23:33Dimethylphthalate ug/kg ND 330 09/09/10 23:33Fluoranthene ug/kg ND 330 09/09/10 23:33Fluorene ug/kg ND 330 09/09/10 23:33Hexachloro-1,3-butadiene ug/kg ND 330 09/09/10 23:33Hexachlorobenzene ug/kg ND 330 09/09/10 23:33Hexachlorocyclopentadiene ug/kg ND 330 09/09/10 23:33Hexachloroethane ug/kg ND 330 09/09/10 23:33Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/09/10 23:33Isophorone ug/kg ND 330 09/09/10 23:33N-Nitroso-di-n-propylamine ug/kg ND 330 09/09/10 23:33N-Nitrosodiphenylamine ug/kg ND 330 09/09/10 23:33Naphthalene ug/kg ND 330 09/09/10 23:33Nitrobenzene ug/kg ND 330 09/09/10 23:33Pentachlorophenol ug/kg ND 1650 09/09/10 23:33Phenanthrene ug/kg ND 330 09/09/10 23:33Phenol ug/kg ND 330 09/09/10 23:33Pyrene ug/kg ND 330 09/09/10 23:332,4,6-Tribromophenol (S) % 71 27-110 09/09/10 23:332-Fluorobiphenyl (S) % 77 30-110 09/09/10 23:332-Fluorophenol (S) % 65 13-110 09/09/10 23:33Nitrobenzene-d5 (S) % 68 23-110 09/09/10 23:33Phenol-d6 (S) % 69 22-110 09/09/10 23:33Terphenyl-d14 (S) % 83 28-110 09/09/10 23:33

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 12602,3,4,6-Tetrachlorophenol ug/kg 2460 L11670 148 39-1122,4,5-Trichlorophenol ug/kg 13001670 78 48-1092,4,6-Trichlorophenol ug/kg 13901670 83 45-1112,4-Dichlorophenol ug/kg 11801670 71 51-1162,4-Dimethylphenol ug/kg 11401670 69 42-1032,4-Dinitrophenol ug/kg 60608330 73 28-1032,4-Dinitrotoluene ug/kg 14401670 87 46-1142,6-Dinitrotoluene ug/kg 15101670 90 48-1122-Chloronaphthalene ug/kg 15901670 96 44-1052-Chlorophenol ug/kg 13801670 83 36-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 11301670 68 39-1122-Methylphenol(o-Cresol) ug/kg 14701670 88 39-1012-Nitroaniline ug/kg 29603330 89 44-1112-Nitrophenol ug/kg 11201670 67 41-1003&4-Methylphenol(m&p Cresol) ug/kg 14301670 86 43-1033,3'-Dichlorobenzidine ug/kg 23703330 71 10-1503-Nitroaniline ug/kg 26203330 79 35-1104,6-Dinitro-2-methylphenol ug/kg 26203330 78 38-1184-Bromophenylphenyl ether ug/kg 13101670 79 47-1154-Chloro-3-methylphenol ug/kg 24503330 74 43-1274-Chloroaniline ug/kg 18803330 57 34-1094-Chlorophenylphenyl ether ug/kg 13801670 83 44-1154-Nitroaniline ug/kg 26803330 80 37-1114-Nitrophenol ug/kg 72208330 87 21-152Acenaphthene ug/kg 14301670 86 38-117Acenaphthylene ug/kg 14201670 85 46-107Acetophenone ug/kg 14103330 42 39-112Anthracene ug/kg 13601670 82 50-110Atrazine ug/kg 17001670 102 39-112Benzaldehyde ug/kg ND L21670 2 39-112Benzo(a)anthracene ug/kg 13201670 79 47-116Benzo(a)pyrene ug/kg 13101670 78 47-106Benzo(b)fluoranthene ug/kg 14101670 85 47-109Benzo(g,h,i)perylene ug/kg 13701670 82 39-115Benzo(k)fluoranthene ug/kg 13501670 81 45-117Biphenyl (Diphenyl) ug/kg 13601670 81 39-112bis(2-Chloroethoxy)methane ug/kg 14201670 85 39-110bis(2-Chloroethyl) ether ug/kg 14701670 88 19-119bis(2-Chloroisopropyl) ether ug/kg 14501670 87 21-110bis(2-Ethylhexyl)phthalate ug/kg 10700 L11670 642 35-116Butylbenzylphthalate ug/kg 13701670 82 38-110Caprolactam ug/kg 15601670 94 39-112Carbazole ug/kg 14001670 84 39-112Chrysene ug/kg 12601670 75 49-110Di-n-butylphthalate ug/kg 14101670 84 43-109Di-n-octylphthalate ug/kg 14101670 85 37-109Dibenz(a,h)anthracene ug/kg 14001670 84 43-116Dibenzofuran ug/kg 13801670 83 45-106Diethylphthalate ug/kg 14201670 85 41-114Dimethylphthalate ug/kg 13701670 82 43-110Fluoranthene ug/kg 13801670 83 50-114Fluorene ug/kg 13901670 84 46-114Hexachloro-1,3-butadiene ug/kg 9791670 59 28-111Hexachlorobenzene ug/kg 13101670 79 46-120Hexachlorocyclopentadiene ug/kg 14701670 88 18-119Hexachloroethane ug/kg 14301670 86 33-110Indeno(1,2,3-cd)pyrene ug/kg 13601670 82 42-115Isophorone ug/kg 12201670 73 44-109



Date: 09/27/2010 06:23 PM Page 193 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



N-Nitroso-di-n-propylamine ug/kg 15401670 92 43-104N-Nitrosodiphenylamine ug/kg 13501670 81 48-113Naphthalene ug/kg 11201670 67 41-110Nitrobenzene ug/kg 11201670 67 38-110Pentachlorophenol ug/kg 26803330 80 32-128Phenanthrene ug/kg 13201670 79 50-110Phenol ug/kg 14201670 85 28-106Pyrene ug/kg 12501670 75 45-1142,4,6-Tribromophenol (S) % 78 27-1102-Fluorobiphenyl (S) % 79 30-1102-Fluorophenol (S) % 75 13-110Nitrobenzene-d5 (S) % 65 23-110Phenol-d6 (S) % 82 22-110Terphenyl-d14 (S) % 75 28-110

Parameter UnitsMS



MSSpikeResult

9276750005

494760

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 10 30ND 885 9782,3,4,6-Tetrachlorophenol ug/kg 2070 117 50-150105 11 302070ND 2430 21702,4,5-Trichlorophenol ug/kg 2070 59 28-11055 8 302070ND 1220 11302,4,6-Trichlorophenol ug/kg 2070 59 17-11758 2 302070ND 1220 12002,4-Dichlorophenol ug/kg 2070 45 21-12848 5 302070ND 938 9842,4-Dimethylphenol ug/kg 2070 39 10-12047 18 302070ND 810 9682,4-Dinitrophenol ug/kg 10300 45 10-10752 14 3010300ND 4680 53502,4-Dinitrotoluene ug/kg 2070 66 36-10962 6 302070ND 1360 12702,6-Dinitrotoluene ug/kg 2070 68 32-11065 4 302070ND 1400 13502-Chloronaphthalene ug/kg 2070 59 30-10762 5 302070ND 1230 12902-Chlorophenol ug/kg 2070 46 14-10647 2 302070ND 953 9702-Methylnaphthalene ug/kg 2070 42 10-13544 4 302070ND 871 9062-Methylphenol(o-Cresol) ug/kg 2070 48 10-12451 7 302070ND 987 10602-Nitroaniline ug/kg 4140 61 26-11663 2 304140ND 2540 26002-Nitrophenol ug/kg 2070 42 28-10342 1 302070ND 865 8713&4-Methylphenol(m&pCresol)

ug/kg 2070 50 10-10951 3 302070ND 1030 1060

3,3'-Dichlorobenzidine ug/kg 4140 59 10-15058 2 304140ND 2440 23903-Nitroaniline ug/kg 4140 62 22-11059 6 304140ND 2570 24304,6-Dinitro-2-methylphenol ug/kg 4140 57 13-12160 5 304140ND 2380 24904-Bromophenylphenyl ether ug/kg 2070 58 31-10956 3 302070ND 1200 11604-Chloro-3-methylphenol ug/kg 4140 54 13-12855 1 304140ND 2240 22604-Chloroaniline ug/kg 4140 40 18-10245 304140ND 1670J 1850J4-Chlorophenylphenyl ether ug/kg 2070 60 29-11258 4 302070ND 1240 12004-Nitroaniline ug/kg 4140 68 16-11161 12 304140ND 2830 25104-Nitrophenol ug/kg 10300 68 14-13559 14 3010300ND 7050 6140Acenaphthene ug/kg 2070 57 26-11459 4 302070ND 1180 1220Acenaphthylene ug/kg 2070 55 32-10859 7 302070ND 1140 1220



Date: 09/27/2010 06:23 PM Page 194 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750005

494760

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg M0,M14140 25 50-15024 4 304140ND 1050 1010Anthracene ug/kg 2070 61 32-11160 2 302070ND 1260 1230Atrazine ug/kg 2070 84 50-15080 5 302070ND 1740 1660Benzaldehyde ug/kg M0,M12070 21 50-1502 302070ND 444J NDBenzo(a)anthracene ug/kg 2070 55 25-11758 5 302070ND 1140 1200Benzo(a)pyrene ug/kg 2070 54 25-10654 0 302070ND 1120 1110Benzo(b)fluoranthene ug/kg 2070 56 24-11057 2 302070ND 1160 1190Benzo(g,h,i)perylene ug/kg 2070 58 19-11257 2 302070ND 1200 1180Benzo(k)fluoranthene ug/kg 2070 53 24-11458 7 302070ND 1110 1190Biphenyl (Diphenyl) ug/kg 2070 51 50-15054 5 302070ND 1060 1110bis(2-Chloroethoxy)methane ug/kg 2070 51 13-11954 6 302070ND 1060 1130bis(2-Chloroethyl) ether ug/kg 2070 50 10-13451 1 302070ND 1040 1050bis(2-Chloroisopropyl) ether ug/kg 2070 43 10-11351 16 302070ND 895 1050bis(2-Ethylhexyl)phthalate ug/kg M02070 479 10-125485 1 302070ND 9990 10100Butylbenzylphthalate ug/kg 2070 60 18-11060 1 302070ND 1250 1240Caprolactam ug/kg 2070 80 50-15068 16 302070ND 1650 1410Carbazole ug/kg 2070 68 50-15061 10 302070ND 1410 1270Chrysene ug/kg 2070 56 30-11056 1 302070ND 1170 1160Di-n-butylphthalate ug/kg 2070 63 19-11260 5 302070ND 1300 1240Di-n-octylphthalate ug/kg 2070 69 17-10559 15 302070ND 1420 1220Dibenz(a,h)anthracene ug/kg 2070 60 23-11157 4 302070ND 1230 1180Dibenzofuran ug/kg 2070 56 35-10358 3 302070ND 1170 1200Diethylphthalate ug/kg 2070 64 27-11361 5 302070ND 1330 1260Dimethylphthalate ug/kg 2070 63 26-11159 6 302070ND 1300 1220Fluoranthene ug/kg 2070 67 33-10959 12 302070ND 1380 1220Fluorene ug/kg 2070 61 32-11359 3 302070ND 1260 1220Hexachloro-1,3-butadiene ug/kg 2070 37 16-11635 6 302070ND 775 730Hexachlorobenzene ug/kg 2070 57 27-12057 1 302070ND 1190 1180Hexachlorocyclopentadiene ug/kg R12070 29 10-10848 51 302070ND 598 1000Hexachloroethane ug/kg 2070 47 10-11749 5 302070ND 969 1010Indeno(1,2,3-cd)pyrene ug/kg 2070 59 10-12256 6 302070ND 1220 1150Isophorone ug/kg 2070 47 28-11449 4 302070ND 968 1010N-Nitroso-di-n-propylamine ug/kg 2070 54 27-11356 3 302070ND 1120 1160N-Nitrosodiphenylamine ug/kg 2070 58 10-12860 4 302070ND 1200 1250Naphthalene ug/kg 2070 40 25-11042 4 302070ND 831 867Nitrobenzene ug/kg 2070 41 18-11442 2 302070ND 842 862Pentachlorophenol ug/kg 4140 44 10-12256 304140ND 1820J 2300Phenanthrene ug/kg 2070 60 30-11458 2 302070ND 1230 1210Phenol ug/kg 2070 46 11-10249 8 302070ND 942 1020Pyrene ug/kg 2070 59 25-11656 5 302070ND 1230 11602,4,6-Tribromophenol (S) % 70 27-110622-Fluorobiphenyl (S) % 57 30-110552-Fluorophenol (S) % 48 13-11046Nitrobenzene-d5 (S) % 45 23-11043Phenol-d6 (S) % 52 22-11050Terphenyl-d14 (S) % 64 28-11058



Date: 09/27/2010 06:23 PM Page 195 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



OEXT/11121EPA 3546






Associated Lab Samples: 9276750007, 9276750010, 9276750013, 9276750014, 9276750015, 9276750016, 9276750017, 9276750019,9276750021

Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/16/10 16:452,3,4,6-Tetrachlorophenol ug/kg ND 330 09/16/10 16:452,4,5-Trichlorophenol ug/kg ND 330 09/16/10 16:452,4,6-Trichlorophenol ug/kg ND 330 09/16/10 16:452,4-Dichlorophenol ug/kg ND 330 09/16/10 16:452,4-Dimethylphenol ug/kg ND 330 09/16/10 16:452,4-Dinitrophenol ug/kg ND 1650 09/16/10 16:452,4-Dinitrotoluene ug/kg ND 330 09/16/10 16:452,6-Dinitrotoluene ug/kg ND 330 09/16/10 16:452-Chloronaphthalene ug/kg ND 330 09/16/10 16:452-Chlorophenol ug/kg ND 330 09/16/10 16:452-Methylnaphthalene ug/kg ND 330 09/16/10 16:452-Methylphenol(o-Cresol) ug/kg ND 330 09/16/10 16:452-Nitroaniline ug/kg ND 1650 09/16/10 16:452-Nitrophenol ug/kg ND 330 09/16/10 16:453&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/16/10 16:453,3'-Dichlorobenzidine ug/kg ND 1650 09/16/10 16:453-Nitroaniline ug/kg ND 1650 09/16/10 16:454,6-Dinitro-2-methylphenol ug/kg ND 660 09/16/10 16:454-Bromophenylphenyl ether ug/kg ND 330 09/16/10 16:454-Chloro-3-methylphenol ug/kg ND 660 09/16/10 16:454-Chloroaniline ug/kg ND 1650 09/16/10 16:454-Chlorophenylphenyl ether ug/kg ND 330 09/16/10 16:454-Nitroaniline ug/kg ND 660 09/16/10 16:454-Nitrophenol ug/kg ND 1650 09/16/10 16:45Acenaphthene ug/kg ND 330 09/16/10 16:45Acenaphthylene ug/kg ND 330 09/16/10 16:45Acetophenone ug/kg ND 330 09/16/10 16:45Anthracene ug/kg ND 330 09/16/10 16:45Atrazine ug/kg ND 660 09/16/10 16:45Benzaldehyde ug/kg ND 660 09/16/10 16:45Benzo(a)anthracene ug/kg ND 330 09/16/10 16:45Benzo(a)pyrene ug/kg ND 330 09/16/10 16:45Benzo(b)fluoranthene ug/kg ND 330 09/16/10 16:45Benzo(g,h,i)perylene ug/kg ND 330 09/16/10 16:45Benzo(k)fluoranthene ug/kg ND 330 09/16/10 16:45Biphenyl (Diphenyl) ug/kg ND 330 09/16/10 16:45bis(2-Chloroethoxy)methane ug/kg ND 330 09/16/10 16:45bis(2-Chloroethyl) ether ug/kg ND 330 09/16/10 16:45bis(2-Chloroisopropyl) ether ug/kg ND 330 09/16/10 16:45bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/16/10 16:45



Date: 09/27/2010 06:23 PM Page 196 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Butylbenzylphthalate ug/kg ND 330 09/16/10 16:45Caprolactam ug/kg ND 330 09/16/10 16:45Carbazole ug/kg ND 330 09/16/10 16:45Chrysene ug/kg ND 330 09/16/10 16:45Di-n-butylphthalate ug/kg ND 330 09/16/10 16:45Di-n-octylphthalate ug/kg ND 330 09/16/10 16:45Dibenz(a,h)anthracene ug/kg ND 330 09/16/10 16:45Dibenzofuran ug/kg ND 330 09/16/10 16:45Diethylphthalate ug/kg ND 330 09/16/10 16:45Dimethylphthalate ug/kg ND 330 09/16/10 16:45Fluoranthene ug/kg ND 330 09/16/10 16:45Fluorene ug/kg ND 330 09/16/10 16:45Hexachloro-1,3-butadiene ug/kg ND 330 09/16/10 16:45Hexachlorobenzene ug/kg ND 330 09/16/10 16:45Hexachlorocyclopentadiene ug/kg ND 330 09/16/10 16:45Hexachloroethane ug/kg ND 330 09/16/10 16:45Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/16/10 16:45Isophorone ug/kg ND 330 09/16/10 16:45N-Nitroso-di-n-propylamine ug/kg ND 330 09/16/10 16:45N-Nitrosodiphenylamine ug/kg ND 330 09/16/10 16:45Naphthalene ug/kg ND 330 09/16/10 16:45Nitrobenzene ug/kg ND 330 09/16/10 16:45Pentachlorophenol ug/kg ND 1650 09/16/10 16:45Phenanthrene ug/kg ND 330 09/16/10 16:45Phenol ug/kg ND 330 09/16/10 16:45Pyrene ug/kg ND 330 09/16/10 16:452,4,6-Tribromophenol (S) % 77 27-110 09/16/10 16:452-Fluorobiphenyl (S) % 55 30-110 09/16/10 16:452-Fluorophenol (S) % 47 13-110 09/16/10 16:45Nitrobenzene-d5 (S) % 50 23-110 09/16/10 16:45Phenol-d6 (S) % 45 22-110 09/16/10 16:45Terphenyl-d14 (S) % 70 28-110 09/16/10 16:45

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 13202,3,4,6-Tetrachlorophenol ug/kg 3140 L31670 188 39-1122,4,5-Trichlorophenol ug/kg 14401670 87 48-1092,4,6-Trichlorophenol ug/kg 15001670 90 45-1112,4-Dichlorophenol ug/kg 12201670 73 51-1162,4-Dimethylphenol ug/kg 11501670 69 42-1032,4-Dinitrophenol ug/kg 69208330 83 28-1032,4-Dinitrotoluene ug/kg 13501670 81 46-114



Date: 09/27/2010 06:23 PM Page 197 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



2,6-Dinitrotoluene ug/kg 13201670 79 48-1122-Chloronaphthalene ug/kg 15501670 93 44-1052-Chlorophenol ug/kg 13601670 82 36-1102-Methylnaphthalene ug/kg 11501670 69 39-1122-Methylphenol(o-Cresol) ug/kg 13601670 81 39-1012-Nitroaniline ug/kg 21603330 65 44-1112-Nitrophenol ug/kg 10801670 65 41-1003&4-Methylphenol(m&p Cresol) ug/kg 14201670 85 43-1033,3'-Dichlorobenzidine ug/kg 31403330 94 10-1503-Nitroaniline ug/kg 21803330 65 35-1104,6-Dinitro-2-methylphenol ug/kg 32003330 96 38-1184-Bromophenylphenyl ether ug/kg 16801670 101 47-1154-Chloro-3-methylphenol ug/kg 24003330 72 43-1274-Chloroaniline ug/kg 17103330 51 34-1094-Chlorophenylphenyl ether ug/kg 15501670 93 44-1154-Nitroaniline ug/kg 25503330 76 37-1114-Nitrophenol ug/kg 76008330 91 21-152Acenaphthene ug/kg 13601670 81 38-117Acenaphthylene ug/kg 13101670 79 46-107Acetophenone ug/kg 14003330 42 39-112Anthracene ug/kg 13501670 81 50-110Atrazine ug/kg 410J L21670 25 39-112Benzaldehyde ug/kg 458J L21670 27 39-112Benzo(a)anthracene ug/kg 17601670 105 47-116Benzo(a)pyrene ug/kg 13901670 83 47-106Benzo(b)fluoranthene ug/kg 17901670 108 47-109Benzo(g,h,i)perylene ug/kg 15301670 92 39-115Benzo(k)fluoranthene ug/kg 14001670 84 45-117Biphenyl (Diphenyl) ug/kg 13101670 79 39-112bis(2-Chloroethoxy)methane ug/kg 13501670 81 39-110bis(2-Chloroethyl) ether ug/kg 13001670 78 19-119bis(2-Chloroisopropyl) ether ug/kg 10101670 60 21-110bis(2-Ethylhexyl)phthalate ug/kg 4300 L31670 258 35-116Butylbenzylphthalate ug/kg 12801670 77 38-110Caprolactam ug/kg 11101670 67 39-112Carbazole ug/kg 13101670 79 39-112Chrysene ug/kg 14101670 85 49-110Di-n-butylphthalate ug/kg 13401670 80 43-109Di-n-octylphthalate ug/kg 12601670 76 37-109Dibenz(a,h)anthracene ug/kg 17401670 104 43-116Dibenzofuran ug/kg 14101670 85 45-106Diethylphthalate ug/kg 13601670 81 41-114Dimethylphthalate ug/kg 13301670 80 43-110Fluoranthene ug/kg 14101670 85 50-114Fluorene ug/kg 15101670 91 46-114Hexachloro-1,3-butadiene ug/kg 13201670 79 28-111Hexachlorobenzene ug/kg 16301670 98 46-120Hexachlorocyclopentadiene ug/kg 14401670 86 18-119



Date: 09/27/2010 06:23 PM Page 198 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



Hexachloroethane ug/kg 15301670 92 33-110Indeno(1,2,3-cd)pyrene ug/kg 16101670 96 42-115Isophorone ug/kg 10201670 61 44-109N-Nitroso-di-n-propylamine ug/kg 13301670 80 43-104N-Nitrosodiphenylamine ug/kg 15001670 90 48-113Naphthalene ug/kg 11101670 67 41-110Nitrobenzene ug/kg 10301670 62 38-110Pentachlorophenol ug/kg 37803330 113 32-128Phenanthrene ug/kg 14601670 87 50-110Phenol ug/kg 13601670 82 28-106Pyrene ug/kg 13201670 79 45-1142,4,6-Tribromophenol (S) % 107 27-1102-Fluorobiphenyl (S) % 82 30-1102-Fluorophenol (S) % 73 13-110Nitrobenzene-d5 (S) % 57 23-110Phenol-d6 (S) % 72 22-110Terphenyl-d14 (S) % 87 28-110

Parameter UnitsMS



MSSpikeResult

9276750027

495533

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg R158 30ND 505 9142,3,4,6-Tetrachlorophenol ug/kg R11830 77 50-150114 39 301830ND 1400 20902,4,5-Trichlorophenol ug/kg R11830 39 28-11055 33 301830ND 714 9982,4,6-Trichlorophenol ug/kg R11830 39 17-11756 34 301830ND 718 10202,4-Dichlorophenol ug/kg R11830 33 21-12846 33 301830ND 598 8382,4-Dimethylphenol ug/kg 1830 30 10-12032 7 301830ND 548 5902,4-Dinitrophenol ug/kg 9130 39 10-10747 18 309130ND 3540 42502,4-Dinitrotoluene ug/kg R11830 39 36-10953 31 301830ND 712 9682,6-Dinitrotoluene ug/kg R11830 38 32-11051 31 301830ND 686 9392-Chloronaphthalene ug/kg R11830 40 30-10761 41 301830ND 732 11102-Chlorophenol ug/kg R11830 27 14-10650 60 301830ND 486 9052-Methylnaphthalene ug/kg R11830 30 10-13544 38 301830ND 546 8062-Methylphenol(o-Cresol) ug/kg R11830 30 10-12445 39 301830ND 549 8162-Nitroaniline ug/kg 3650 84 26-116110 28 303650ND 3050 40402-Nitrophenol ug/kg M0,

M1,R11830 27 28-10343 44 301830ND 499 780

3&4-Methylphenol(m&pCresol)

ug/kg R11830 32 10-10946 37 301830ND 583 847

3,3'-Dichlorobenzidine ug/kg 3650 91 10-150113 22 303650ND 3310 41203-Nitroaniline ug/kg 3650 80 22-11094 16 303650ND 2910 34204,6-Dinitro-2-methylphenol ug/kg 3650 40 13-12152 26 303650ND 1460 19104-Bromophenylphenyl ether ug/kg R11830 40 31-10957 35 301830ND 723 10304-Chloro-3-methylphenol ug/kg 3650 34 13-12846 28 303650ND 1260 16704-Chloroaniline ug/kg 3650 71 18-10283 16 303650ND 2600 30404-Chlorophenylphenyl ether ug/kg R11830 42 29-11259 33 301830ND 774 1080



Date: 09/27/2010 06:23 PM Page 199 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750027

495533

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

4-Nitroaniline ug/kg 3650 81 16-111105 26 303650ND 2960 38404-Nitrophenol ug/kg 9130 43 14-13558 29 309130ND 3930 5260Acenaphthene ug/kg R11830 37 26-11453 34 301830ND 682 966Acenaphthylene ug/kg R11830 36 32-10851 35 301830ND 662 940Acetophenone ug/kg M0,

M1,R13650 16 50-15026 48 303650ND 575 941

Anthracene ug/kg 1830 36 32-11148 29 301830ND 651 877Atrazine ug/kg M0,R11830 44 50-15072 48 301830ND 808 1320Benzaldehyde ug/kg M0,R11830 40 50-15068 52 301830ND 725 1230Benzo(a)anthracene ug/kg R11830 41 25-11759 36 301830ND 752 1080Benzo(a)pyrene ug/kg R11830 35 25-10650 34 301830ND 646 907Benzo(b)fluoranthene ug/kg R11830 39 24-11058 38 301830ND 719 1050Benzo(g,h,i)perylene ug/kg R11830 39 19-11255 34 301830ND 715 1000Benzo(k)fluoranthene ug/kg R11830 37 24-11451 32 301830ND 677 931Biphenyl (Diphenyl) ug/kg M0,

M1,R11830 35 50-15051 39 301830ND 633 937

bis(2-Chloroethoxy)methane ug/kg R11830 33 13-11952 44 301830ND 606 950bis(2-Chloroethyl) ether ug/kg R11830 23 10-13448 70 301830ND 421 870bis(2-Chloroisopropyl) ether ug/kg R11830 20 10-11338 62 301830ND 364 694bis(2-Ethylhexyl)phthalate ug/kg M0,R11830 103 10-125155 41 301830ND 1880 2840Butylbenzylphthalate ug/kg 1830 33 18-11044 29 301830ND 595 800Caprolactam ug/kg M0,M11830 28 50-15035 22 301830ND 508 632Carbazole ug/kg M0,

M1,R11830 35 50-15046 27 301830ND 642 844

Chrysene ug/kg R11830 36 30-11050 32 301830ND 662 916Di-n-butylphthalate ug/kg 1830 36 19-11247 27 301830ND 657 861Di-n-octylphthalate ug/kg 1830 33 17-10545 30 301830ND 608 826Dibenz(a,h)anthracene ug/kg R11830 42 23-11160 36 301830ND 766 1100Dibenzofuran ug/kg R11830 38 35-10353 34 301830ND 690 977Diethylphthalate ug/kg 1830 39 27-11353 28 301830ND 722 961Dimethylphthalate ug/kg 1830 39 26-11151 28 301830ND 705 939Fluoranthene ug/kg 1830 37 33-10948 26 301830ND 676 878Fluorene ug/kg 1830 39 32-11355 35 301830ND 712 1010Hexachloro-1,3-butadiene ug/kg R11830 28 16-11653 61 301830ND 515 969Hexachlorobenzene ug/kg R11830 43 27-12060 33 301830ND 793 1100Hexachlorocyclopentadiene ug/kg R11830 35 10-10865 60 301830ND 643 1190Hexachloroethane ug/kg R11830 24 10-11758 84 301830ND 432 1060Indeno(1,2,3-cd)pyrene ug/kg R11830 40 10-12257 36 301830ND 729 1050Isophorone ug/kg 1830 30 28-11440 30 301830ND 545 740N-Nitroso-di-n-propylamine ug/kg R11830 32 27-11348 41 301830ND 581 882N-Nitrosodiphenylamine ug/kg R11830 36 10-12849 31 301830ND 664 904Naphthalene ug/kg R11830 27 25-11044 49 301830ND 490 810Nitrobenzene ug/kg R11830 25 18-11442 49 301830ND 460 763Pentachlorophenol ug/kg R13650 106 10-122151 35 303650ND 3870 5510Phenanthrene ug/kg R11830 37 30-11451 32 301830ND 673 925Phenol ug/kg R11830 29 11-10246 46 301830ND 526 839Pyrene ug/kg R11830 33 25-11646 33 301830ND 605 8472,4,6-Tribromophenol (S) % 53 27-11065



Date: 09/27/2010 06:23 PM Page 200 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750027

495533

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

2-Fluorobiphenyl (S) % 43 30-110552-Fluorophenol (S) % 26 13-11046Nitrobenzene-d5 (S) % 28 23-11041Phenol-d6 (S) % 32 22-11044Terphenyl-d14 (S) % 43 28-11054



Date: 09/27/2010 06:23 PM Page 201 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



OEXT/11146EPA 3546


Associated Lab Samples: 9276750023, 9276750024, 9276750025, 9276750026, 9276750028, 9276750029, 9276750032, 9276750034





Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/17/10 05:392,3,4,6-Tetrachlorophenol ug/kg ND 330 09/17/10 05:392,4,5-Trichlorophenol ug/kg ND 330 09/17/10 05:392,4,6-Trichlorophenol ug/kg ND 330 09/17/10 05:392,4-Dichlorophenol ug/kg ND 330 09/17/10 05:392,4-Dimethylphenol ug/kg ND 330 09/17/10 05:392,4-Dinitrophenol ug/kg ND 1650 09/17/10 05:392,4-Dinitrotoluene ug/kg ND 330 09/17/10 05:392,6-Dinitrotoluene ug/kg ND 330 09/17/10 05:392-Chloronaphthalene ug/kg ND 330 09/17/10 05:392-Chlorophenol ug/kg ND 330 09/17/10 05:392-Methylnaphthalene ug/kg ND 330 09/17/10 05:392-Methylphenol(o-Cresol) ug/kg ND 330 09/17/10 05:392-Nitroaniline ug/kg ND 1650 09/17/10 05:392-Nitrophenol ug/kg ND 330 09/17/10 05:393&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/17/10 05:393,3'-Dichlorobenzidine ug/kg ND 1650 09/17/10 05:393-Nitroaniline ug/kg ND 1650 09/17/10 05:394,6-Dinitro-2-methylphenol ug/kg ND 660 09/17/10 05:394-Bromophenylphenyl ether ug/kg ND 330 09/17/10 05:394-Chloro-3-methylphenol ug/kg ND 660 09/17/10 05:394-Chloroaniline ug/kg ND 1650 09/17/10 05:394-Chlorophenylphenyl ether ug/kg ND 330 09/17/10 05:394-Nitroaniline ug/kg ND 660 09/17/10 05:394-Nitrophenol ug/kg ND 1650 09/17/10 05:39Acenaphthene ug/kg ND 330 09/17/10 05:39Acenaphthylene ug/kg ND 330 09/17/10 05:39Acetophenone ug/kg ND 330 09/17/10 05:39Anthracene ug/kg ND 330 09/17/10 05:39Atrazine ug/kg ND 660 09/17/10 05:39Benzaldehyde ug/kg ND 660 09/17/10 05:39Benzo(a)anthracene ug/kg ND 330 09/17/10 05:39Benzo(a)pyrene ug/kg ND 330 09/17/10 05:39Benzo(b)fluoranthene ug/kg ND 330 09/17/10 05:39Benzo(g,h,i)perylene ug/kg ND 330 09/17/10 05:39Benzo(k)fluoranthene ug/kg ND 330 09/17/10 05:39Biphenyl (Diphenyl) ug/kg ND 330 09/17/10 05:39bis(2-Chloroethoxy)methane ug/kg ND 330 09/17/10 05:39bis(2-Chloroethyl) ether ug/kg ND 330 09/17/10 05:39bis(2-Chloroisopropyl) ether ug/kg ND 330 09/17/10 05:39bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/17/10 05:39Butylbenzylphthalate ug/kg ND 330 09/17/10 05:39Caprolactam ug/kg ND 330 09/17/10 05:39



Date: 09/27/2010 06:23 PM Page 202 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Carbazole ug/kg ND 330 09/17/10 05:39Chrysene ug/kg ND 330 09/17/10 05:39Di-n-butylphthalate ug/kg ND 330 09/17/10 05:39Di-n-octylphthalate ug/kg ND 330 09/17/10 05:39Dibenz(a,h)anthracene ug/kg ND 330 09/17/10 05:39Dibenzofuran ug/kg ND 330 09/17/10 05:39Diethylphthalate ug/kg ND 330 09/17/10 05:39Dimethylphthalate ug/kg ND 330 09/17/10 05:39Fluoranthene ug/kg ND 330 09/17/10 05:39Fluorene ug/kg ND 330 09/17/10 05:39Hexachloro-1,3-butadiene ug/kg ND 330 09/17/10 05:39Hexachlorobenzene ug/kg ND 330 09/17/10 05:39Hexachlorocyclopentadiene ug/kg ND 330 09/17/10 05:39Hexachloroethane ug/kg ND 330 09/17/10 05:39Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/17/10 05:39Isophorone ug/kg ND 330 09/17/10 05:39N-Nitroso-di-n-propylamine ug/kg ND 330 09/17/10 05:39N-Nitrosodiphenylamine ug/kg ND 330 09/17/10 05:39Naphthalene ug/kg ND 330 09/17/10 05:39Nitrobenzene ug/kg ND 330 09/17/10 05:39Pentachlorophenol ug/kg ND 1650 09/17/10 05:39Phenanthrene ug/kg ND 330 09/17/10 05:39Phenol ug/kg ND 330 09/17/10 05:39Pyrene ug/kg ND 330 09/17/10 05:392,4,6-Tribromophenol (S) % 98 27-110 09/17/10 05:392-Fluorobiphenyl (S) % 73 30-110 09/17/10 05:392-Fluorophenol (S) % 61 13-110 09/17/10 05:39Nitrobenzene-d5 (S) % 65 23-110 09/17/10 05:39Phenol-d6 (S) % 59 22-110 09/17/10 05:39Terphenyl-d14 (S) % 82 28-110 09/17/10 05:39

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 9612,3,4,6-Tetrachlorophenol ug/kg 2480 L31670 149 39-1122,4,5-Trichlorophenol ug/kg 11001670 66 48-1092,4,6-Trichlorophenol ug/kg 11501670 69 45-1112,4-Dichlorophenol ug/kg 9091670 55 51-1162,4-Dimethylphenol ug/kg 8691670 52 42-1032,4-Dinitrophenol ug/kg 52408330 63 28-1032,4-Dinitrotoluene ug/kg 10601670 63 46-1142,6-Dinitrotoluene ug/kg 10301670 62 48-1122-Chloronaphthalene ug/kg 11801670 71 44-1052-Chlorophenol ug/kg 8521670 51 36-110



Date: 09/27/2010 06:23 PM Page 203 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 8291670 50 39-1122-Methylphenol(o-Cresol) ug/kg 9031670 54 39-1012-Nitroaniline ug/kg 18203330 55 44-1112-Nitrophenol ug/kg 7581670 45 41-1003&4-Methylphenol(m&p Cresol) ug/kg 9391670 56 43-1033,3'-Dichlorobenzidine ug/kg 25003330 75 10-1503-Nitroaniline ug/kg 17703330 53 35-1104,6-Dinitro-2-methylphenol ug/kg 23103330 69 38-1184-Bromophenylphenyl ether ug/kg 12501670 75 47-1154-Chloro-3-methylphenol ug/kg 18603330 56 43-1274-Chloroaniline ug/kg 1620J3330 49 34-1094-Chlorophenylphenyl ether ug/kg 11901670 72 44-1154-Nitroaniline ug/kg 18703330 56 37-1114-Nitrophenol ug/kg 60608330 73 21-152Acenaphthene ug/kg 10501670 63 38-117Acenaphthylene ug/kg 10201670 61 46-107Acetophenone ug/kg 917 L23330 28 39-112Anthracene ug/kg 10101670 61 50-110Atrazine ug/kg 15301670 92 39-112Benzaldehyde ug/kg 628J L21670 38 39-112Benzo(a)anthracene ug/kg 13201670 79 47-116Benzo(a)pyrene ug/kg 10501670 63 47-106Benzo(b)fluoranthene ug/kg 12401670 74 47-109Benzo(g,h,i)perylene ug/kg 11401670 68 39-115Benzo(k)fluoranthene ug/kg 11301670 68 45-117Biphenyl (Diphenyl) ug/kg 9961670 60 39-112bis(2-Chloroethoxy)methane ug/kg 9491670 57 39-110bis(2-Chloroethyl) ether ug/kg 8141670 49 19-119bis(2-Chloroisopropyl) ether ug/kg 6471670 39 21-110bis(2-Ethylhexyl)phthalate ug/kg 3320 L31670 199 35-116Butylbenzylphthalate ug/kg 9641670 58 38-110Caprolactam ug/kg 8351670 50 39-112Carbazole ug/kg 9831670 59 39-112Chrysene ug/kg 10701670 64 49-110Di-n-butylphthalate ug/kg 9961670 60 43-109Di-n-octylphthalate ug/kg 9441670 57 37-109Dibenz(a,h)anthracene ug/kg 12701670 76 43-116Dibenzofuran ug/kg 10801670 65 45-106Diethylphthalate ug/kg 10601670 63 41-114Dimethylphthalate ug/kg 10301670 62 43-110Fluoranthene ug/kg 10501670 63 50-114Fluorene ug/kg 11601670 70 46-114Hexachloro-1,3-butadiene ug/kg 8841670 53 28-111Hexachlorobenzene ug/kg 12401670 74 46-120Hexachlorocyclopentadiene ug/kg 10001670 60 18-119Hexachloroethane ug/kg 9651670 58 33-110Indeno(1,2,3-cd)pyrene ug/kg 11901670 71 42-115Isophorone ug/kg 7681670 46 44-109



Date: 09/27/2010 06:23 PM Page 204 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



N-Nitroso-di-n-propylamine ug/kg 8931670 54 43-104N-Nitrosodiphenylamine ug/kg 10901670 66 48-113Naphthalene ug/kg 7591670 46 41-110Nitrobenzene ug/kg 7121670 43 38-110Pentachlorophenol ug/kg 27103330 81 32-128Phenanthrene ug/kg 10801670 65 50-110Phenol ug/kg 8691670 52 28-106Pyrene ug/kg 9711670 58 45-1142,4,6-Tribromophenol (S) % 78 27-1102-Fluorobiphenyl (S) % 62 30-1102-Fluorophenol (S) % 46 13-110Nitrobenzene-d5 (S) % 41 23-110Phenol-d6 (S) % 48 22-110Terphenyl-d14 (S) % 63 28-110

Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 16 30ND 967 8262,3,4,6-Tetrachlorophenol ug/kg 1790 125 50-15094 28 301790ND 2230 16802,4,5-Trichlorophenol ug/kg 1790 61 28-11051 18 301790ND 1090 9092,4,6-Trichlorophenol ug/kg 1790 63 17-11754 17 301790ND 1130 9542,4-Dichlorophenol ug/kg 1790 53 21-12845 15 301790ND 937 8072,4-Dimethylphenol ug/kg 1790 43 10-12040 9 301790ND 772 7092,4-Dinitrophenol ug/kg 8910 49 10-10741 17 308910ND 4370 36902,4-Dinitrotoluene ug/kg 1790 58 36-10954 6 301790ND 1030 9712,6-Dinitrotoluene ug/kg 1790 57 32-11054 5 301790ND 1010 9602-Chloronaphthalene ug/kg 1790 68 30-10764 6 301790ND 1210 11502-Chlorophenol ug/kg 1790 54 14-10646 16 301790ND 958 8192-Methylnaphthalene ug/kg 1790 49 10-13547 5 301790ND 876 8312-Methylphenol(o-Cresol) ug/kg 1790 51 10-12445 13 301790ND 917 8072-Nitroaniline ug/kg 3560 50 26-11652 3 303560ND 1790 18402-Nitrophenol ug/kg 1790 47 28-10343 9 301790ND 837 7623&4-Methylphenol(m&pCresol)

ug/kg 1790 54 10-10942 25 301790ND 964 747

3,3'-Dichlorobenzidine ug/kg 3560 52 10-15040 303560ND 1840 1430J3-Nitroaniline ug/kg 3560 43 22-11049 303560ND 1530J 1730J4,6-Dinitro-2-methylphenol ug/kg 3560 57 13-12147 19 303560ND 2020 16704-Bromophenylphenyl ether ug/kg 1790 66 31-10953 23 301790ND 1180 9414-Chloro-3-methylphenol ug/kg 3560 51 13-12847 8 303560ND 1820 16804-Chloroaniline ug/kg 3560 41 18-10242 303560ND 1470J 1490J4-Chlorophenylphenyl ether ug/kg 1790 66 29-11256 16 301790ND 1180 10004-Nitroaniline ug/kg 3560 48 16-11151 6 303560ND 1720 18204-Nitrophenol ug/kg 8910 63 14-13556 11 308910ND 5600 5030Acenaphthene ug/kg 1790 59 26-11458 2 301790ND 1060 1040Acenaphthylene ug/kg 1790 57 32-10857 0 301790ND 1020 1020



Date: 09/27/2010 06:23 PM Page 205 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg 3560 28 50-15025 14 303560ND 1010 878Anthracene ug/kg 1790 54 32-11153 2 301790ND 955 939Atrazine ug/kg R11790 66 50-150117 55 301790ND 1180 2090Benzaldehyde ug/kg M01790 33 50-15039 301790ND 584J 693JBenzo(a)anthracene ug/kg 1790 67 25-11751 26 301790ND 1190 915Benzo(a)pyrene ug/kg 1790 55 25-10650 9 301790ND 973 892Benzo(b)fluoranthene ug/kg 1790 69 24-11051 30 301790ND 1230 912Benzo(g,h,i)perylene ug/kg 1790 58 19-11254 8 301790ND 1100 1010Benzo(k)fluoranthene ug/kg 1790 54 24-11455 2 301790ND 969 988Biphenyl (Diphenyl) ug/kg 1790 58 50-15057 1 301790ND 1030 1010bis(2-Chloroethoxy)methane ug/kg 1790 57 13-11952 10 301790ND 1020 919bis(2-Chloroethyl) ether ug/kg 1790 51 10-13449 4 301790ND 904 870bis(2-Chloroisopropyl) ether ug/kg 1790 40 10-11342 5 301790ND 712 751bis(2-Ethylhexyl)phthalate ug/kg R11790 165 10-125110 40 301790ND 2940 1960Butylbenzylphthalate ug/kg 1790 49 18-11042 15 301790ND 867 749Caprolactam ug/kg M0,

M1,R11790 41 50-15058 35 301790ND 729 1040

Carbazole ug/kg 1790 52 50-15055 7 301790ND 919 981Chrysene ug/kg 1790 56 30-11053 6 301790ND 999 939Di-n-butylphthalate ug/kg 1790 51 19-11244 14 301790ND 908 789Di-n-octylphthalate ug/kg R11790 49 17-10535 35 301790ND 880 616Dibenz(a,h)anthracene ug/kg 1790 64 23-11153 18 301790ND 1200 1000Dibenzofuran ug/kg 1790 60 35-10359 3 301790ND 1080 1050Diethylphthalate ug/kg 1790 57 27-11352 10 301790ND 1020 926Dimethylphthalate ug/kg 1790 57 26-11155 4 301790ND 1010 972Fluoranthene ug/kg 1790 54 33-10953 2 301790ND 956 938Fluorene ug/kg 1790 63 32-11356 12 301790ND 1130 995Hexachloro-1,3-butadiene ug/kg 1790 56 16-11652 8 301790ND 1000 922Hexachlorobenzene ug/kg 1790 66 27-12055 18 301790ND 1180 989Hexachlorocyclopentadiene ug/kg R11790 68 10-10844 43 301790ND 1210 776Hexachloroethane ug/kg 1790 60 10-11755 8 301790ND 1060 976Indeno(1,2,3-cd)pyrene ug/kg 1790 60 10-12251 16 301790ND 1130 969Isophorone ug/kg 1790 45 28-11445 0 301790ND 802 805N-Nitroso-di-n-propylamine ug/kg 1790 53 27-11346 15 301790ND 946 816N-Nitrosodiphenylamine ug/kg 1790 57 10-12851 12 301790ND 1020 906Naphthalene ug/kg 1790 49 25-11049 1 301790ND 866 871Nitrobenzene ug/kg 1790 46 18-11446 2 301790ND 812 825Pentachlorophenol ug/kg 3560 68 10-12243 303560ND 2420 1520JPhenanthrene ug/kg 1790 57 30-11454 6 301790ND 1020 960Phenol ug/kg 1790 52 11-10246 12 301790ND 931 825Pyrene ug/kg 1790 52 25-11653 2 301790ND 927 9442,4,6-Tribromophenol (S) % 69 27-110572-Fluorobiphenyl (S) % 62 30-110612-Fluorophenol (S) % 50 13-11049Nitrobenzene-d5 (S) % 44 23-11047Phenol-d6 (S) % 49 22-11047Terphenyl-d14 (S) % 56 28-11054



Date: 09/27/2010 06:23 PM Page 206 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



OEXT/11089EPA 3510

EPA 82708270 Water MSSV






Matrix: Water

Analyzed

1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/16/10 11:542,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/16/10 11:542,4,5-Trichlorophenol ug/L ND 10.0 09/16/10 11:542,4,6-Trichlorophenol ug/L ND 10.0 09/16/10 11:542,4-Dichlorophenol ug/L ND 10.0 09/16/10 11:542,4-Dimethylphenol ug/L ND 10.0 09/16/10 11:542,4-Dinitrophenol ug/L ND 50.0 09/16/10 11:542,4-Dinitrotoluene ug/L ND 10.0 09/16/10 11:542,6-Dinitrotoluene ug/L ND 10.0 09/16/10 11:542-Chloronaphthalene ug/L ND 10.0 09/16/10 11:542-Chlorophenol ug/L ND 10.0 09/16/10 11:542-Methylnaphthalene ug/L ND 10.0 09/16/10 11:542-Methylphenol(o-Cresol) ug/L ND 10.0 09/16/10 11:542-Nitroaniline ug/L ND 50.0 09/16/10 11:542-Nitrophenol ug/L ND 10.0 09/16/10 11:543&4-Methylphenol(m&p Cresol) ug/L ND 10.0 09/16/10 11:543,3'-Dichlorobenzidine ug/L ND 20.0 09/16/10 11:543-Nitroaniline ug/L ND 50.0 09/16/10 11:544,6-Dinitro-2-methylphenol ug/L ND 20.0 09/16/10 11:544-Bromophenylphenyl ether ug/L ND 10.0 09/16/10 11:544-Chloro-3-methylphenol ug/L ND 20.0 09/16/10 11:544-Chloroaniline ug/L ND 20.0 09/16/10 11:544-Chlorophenylphenyl ether ug/L ND 10.0 09/16/10 11:544-Nitroaniline ug/L ND 20.0 09/16/10 11:544-Nitrophenol ug/L ND 50.0 09/16/10 11:54Acenaphthene ug/L ND 10.0 09/16/10 11:54Acenaphthylene ug/L ND 10.0 09/16/10 11:54Acetophenone ug/L ND 10.0 09/16/10 11:54Anthracene ug/L ND 10.0 09/16/10 11:54Atrazine ug/L ND 20.0 09/16/10 11:54Benzaldehyde ug/L ND 20.0 09/16/10 11:54Benzo(a)anthracene ug/L ND 10.0 09/16/10 11:54Benzo(a)pyrene ug/L ND 10.0 09/16/10 11:54Benzo(b)fluoranthene ug/L ND 10.0 09/16/10 11:54Benzo(g,h,i)perylene ug/L ND 10.0 09/16/10 11:54Benzo(k)fluoranthene ug/L ND 10.0 09/16/10 11:54Biphenyl (Diphenyl) ug/L ND 10.0 09/16/10 11:54bis(2-Chloroethoxy)methane ug/L ND 10.0 09/16/10 11:54bis(2-Chloroethyl) ether ug/L ND 10.0 09/16/10 11:54bis(2-Chloroisopropyl) ether ug/L ND 10.0 09/16/10 11:54bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/16/10 11:54Butylbenzylphthalate ug/L ND 10.0 09/16/10 11:54Caprolactam ug/L ND 10.0 09/16/10 11:54



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Matrix: Water

Analyzed

Carbazole ug/L ND 10.0 09/16/10 11:54Chrysene ug/L ND 10.0 09/16/10 11:54Di-n-butylphthalate ug/L ND 10.0 09/16/10 11:54Di-n-octylphthalate ug/L ND 10.0 09/16/10 11:54Dibenz(a,h)anthracene ug/L ND 10.0 09/16/10 11:54Dibenzofuran ug/L ND 10.0 09/16/10 11:54Diethylphthalate ug/L ND 10.0 09/16/10 11:54Dimethylphthalate ug/L ND 10.0 09/16/10 11:54Fluoranthene ug/L ND 10.0 09/16/10 11:54Fluorene ug/L ND 10.0 09/16/10 11:54Hexachloro-1,3-butadiene ug/L ND 10.0 09/16/10 11:54Hexachlorobenzene ug/L ND 10.0 09/16/10 11:54Hexachlorocyclopentadiene ug/L ND 10.0 09/16/10 11:54Hexachloroethane ug/L ND 10.0 09/16/10 11:54Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/16/10 11:54Isophorone ug/L ND 10.0 09/16/10 11:54N-Nitroso-di-n-propylamine ug/L ND 10.0 09/16/10 11:54N-Nitrosodiphenylamine ug/L ND 10.0 09/16/10 11:54Naphthalene ug/L ND 10.0 09/16/10 11:54Nitrobenzene ug/L ND 10.0 09/16/10 11:54Pentachlorophenol ug/L ND 25.0 09/16/10 11:54Phenanthrene ug/L ND 10.0 09/16/10 11:54Phenol ug/L ND 10.0 09/16/10 11:54Pyrene ug/L ND 10.0 09/16/10 11:542,4,6-Tribromophenol (S) % 102 27-110 09/16/10 11:542-Fluorobiphenyl (S) % 66 27-110 09/16/10 11:542-Fluorophenol (S) % 33 12-110 09/16/10 11:54Nitrobenzene-d5 (S) % 61 21-110 09/16/10 11:54Phenol-d6 (S) % 21 10-110 09/16/10 11:54Terphenyl-d14 (S) % 78 31-107 09/16/10 11:54

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/L 29.050 58 17-1152,3,4,6-Tetrachlorophenol ug/L 88.5 L350 177 17-1152,4,5-Trichlorophenol ug/L 41.550 83 23-1162,4,6-Trichlorophenol ug/L 45.450 91 21-1142,4-Dichlorophenol ug/L 31.550 63 22-1202,4-Dimethylphenol ug/L 30.150 60 15-1092,4-Dinitrophenol ug/L 116250 47 10-1032,4-Dinitrotoluene ug/L 38.350 77 24-1192,6-Dinitrotoluene ug/L 37.950 76 25-1162-Chloronaphthalene ug/L 39.150 78 18-1102-Chlorophenol ug/L 31.150 62 10-104



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(704)875-9092


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(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/L 25.450 51 16-1102-Methylphenol(o-Cresol) ug/L 29.850 60 13-1102-Nitroaniline ug/L 160250 64 20-1172-Nitrophenol ug/L 28.050 56 16-1083&4-Methylphenol(m&p Cresol) ug/L 28.350 57 14-1103,3'-Dichlorobenzidine ug/L 194250 78 13-1313-Nitroaniline ug/L 159250 63 15-1174,6-Dinitro-2-methylphenol ug/L 82.8100 83 13-1194-Bromophenylphenyl ether ug/L 46.550 93 23-1204-Chloro-3-methylphenol ug/L 62.9100 63 21-1194-Chloroaniline ug/L 140250 56 10-1224-Chlorophenylphenyl ether ug/L 43.350 87 22-1124-Nitroaniline ug/L 158250 63 14-1184-Nitrophenol ug/L 95.5250 38 10-110Acenaphthene ug/L 37.150 74 20-105Acenaphthylene ug/L 36.050 72 23-106Acetophenone ug/L 35.050 70 17-115Anthracene ug/L 36.950 74 25-120Atrazine ug/L 65.6 L350 131 17-115Benzaldehyde ug/L 14.2J50 28 17-115Benzo(a)anthracene ug/L 42.650 85 21-128Benzo(a)pyrene ug/L 38.750 77 25-116Benzo(b)fluoranthene ug/L 52.450 105 23-117Benzo(g,h,i)perylene ug/L 43.550 87 17-128Benzo(k)fluoranthene ug/L 36.550 73 25-127Biphenyl (Diphenyl) ug/L 33.950 68 17-115bis(2-Chloroethoxy)methane ug/L 34.950 70 19-107bis(2-Chloroethyl) ether ug/L 31.350 63 10-108bis(2-Chloroisopropyl) ether ug/L 24.650 49 10-108bis(2-Ethylhexyl)phthalate ug/L 40.250 80 16-123Butylbenzylphthalate ug/L 34.750 69 20-118Caprolactam ug/L 11.350 23 17-115Carbazole ug/L 36.050 72 17-115Chrysene ug/L 39.150 78 24-125Di-n-butylphthalate ug/L 36.450 73 23-115Di-n-octylphthalate ug/L 34.450 69 20-115Dibenz(a,h)anthracene ug/L 48.050 96 18-131Dibenzofuran ug/L 37.950 76 23-106Diethylphthalate ug/L 38.550 77 24-115Dimethylphthalate ug/L 37.450 75 22-113Fluoranthene ug/L 38.850 78 24-125Fluorene ug/L 41.850 84 24-114Hexachloro-1,3-butadiene ug/L 18.450 37 10-110Hexachlorobenzene ug/L 44.950 90 22-127Hexachlorocyclopentadiene ug/L 28.950 58 10-110Hexachloroethane ug/L 21.950 44 10-110Indeno(1,2,3-cd)pyrene ug/L 45.350 91 18-130Isophorone ug/L 27.450 55 23-114



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(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



N-Nitroso-di-n-propylamine ug/L 34.050 68 21-114N-Nitrosodiphenylamine ug/L 40.150 80 24-123Naphthalene ug/L 25.450 51 14-110Nitrobenzene ug/L 27.250 54 16-106Pentachlorophenol ug/L 91.2250 36 10-123Phenanthrene ug/L 39.950 80 25-119Phenol ug/L 15.850 32 10-110Pyrene ug/L 34.650 69 22-1272,4,6-Tribromophenol (S) % 95 27-1102-Fluorobiphenyl (S) % 77 27-1102-Fluorophenol (S) % 35 12-110Nitrobenzene-d5 (S) % 50 21-110Phenol-d6 (S) % 24 10-110Terphenyl-d14 (S) % 74 31-107

Parameter UnitsMS



MSSpikeResult

9276915001

494101

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/L M0,M1100 41 50-15048 17 30100ND 40.8 48.52,3,4,6-Tetrachlorophenol ug/L M0,M1100 149 50-150160 7 30100ND 149 1602,4,5-Trichlorophenol ug/L 100 67 19-10572 8 30100ND 67.1 72.42,4,6-Trichlorophenol ug/L 100 71 13-10878 10 30100ND 70.5 78.02,4-Dichlorophenol ug/L 100 47 29-11156 18 30100ND 47.1 56.22,4-Dimethylphenol ug/L 100 45 21-10353 17 30100ND 44.6 52.92,4-Dinitrophenol ug/L 500 70 10-10976 9 30500ND 348 3802,4-Dinitrotoluene ug/L 100 64 27-10472 12 30100ND 64.1 72.22,6-Dinitrotoluene ug/L 100 63 28-10169 10 30100ND 62.6 69.52-Chloronaphthalene ug/L 100 56 14-10268 19 30100ND 56.2 68.32-Chlorophenol ug/L 100 43 16-11048 10 30100ND 43.4 47.72-Methylnaphthalene ug/L 100 38 13-11045 18 30100ND 37.9 45.42-Methylphenol(o-Cresol) ug/L 100 43 19-11052 18 30100ND 43.2 52.02-Nitroaniline ug/L 500 54 26-10361 11 30500ND 271 3032-Nitrophenol ug/L 100 39 20-11045 14 30100ND 39.1 44.93&4-Methylphenol(m&pCresol)

ug/L 100 44 20-11054 20 30100ND 44.2 54.1

3,3'-Dichlorobenzidine ug/L 500 50 25-11251 2 30500ND 249 2543-Nitroaniline ug/L 500 52 29-11059 12 30500ND 262 2954,6-Dinitro-2-methylphenol ug/L 200 77 10-11777 1 30200ND 154 1544-Bromophenylphenyl ether ug/L 100 78 20-10580 3 30100ND 77.7 80.14-Chloro-3-methylphenol ug/L 200 55 22-11061 10 30200ND 111 1234-Chloroaniline ug/L 500 40 20-10046 14 30500ND 200 2304-Chlorophenylphenyl ether ug/L 100 69 19-10278 13 30100ND 68.7 78.44-Nitroaniline ug/L 500 58 29-11063 8 30500ND 292 3154-Nitrophenol ug/L 500 49 10-11058 16 30500ND 246 288Acenaphthene ug/L 100 57 17-10066 15 30100ND 56.7 66.0Acenaphthylene ug/L 100 55 21-10064 16 30100ND 54.7 63.9



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(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276915001

494101

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/L M0,M1100 46 50-15054 15 30100ND 46.4 53.8Anthracene ug/L 100 63 24-10967 6 30100ND 63.1 66.9Atrazine ug/L 100 69 50-15067 3 30100ND 68.9 66.9Benzaldehyde ug/L M0,M1100 16 50-15026 30100ND ND 26.1JBenzo(a)anthracene ug/L 100 70 22-11774 5 30100ND 70.4 73.7Benzo(a)pyrene ug/L 100 65 23-10469 6 30100ND 65.1 69.0Benzo(b)fluoranthene ug/L 100 84 23-10382 2 30100ND 83.8 82.2Benzo(g,h,i)perylene ug/L 100 75 18-11177 3 30100ND 74.9 77.1Benzo(k)fluoranthene ug/L 100 63 22-11374 15 30100ND 63.4 73.6Biphenyl (Diphenyl) ug/L M0,M1100 48 50-15058 20 30100ND 48.0 58.4bis(2-Chloroethoxy)methane ug/L 100 48 22-11056 15 30100ND 48.0 55.8bis(2-Chloroethyl) ether ug/L 100 43 16-11047 9 30100ND 42.7 46.6bis(2-Chloroisopropyl) ether ug/L 100 33 14-11038 12 30100ND 33.2 37.6bis(2-Ethylhexyl)phthalate ug/L 100 66 23-10272 10 30100ND 65.8 72.4Butylbenzylphthalate ug/L 100 56 25-11063 11 30100ND 56.4 63.1Caprolactam ug/L M0,M1100 25 50-15032 27 30100ND 24.8 32.4Carbazole ug/L 100 61 50-15067 9 30100ND 61.4 67.3Chrysene ug/L 100 67 23-11571 5 30100ND 67.2 70.9Di-n-butylphthalate ug/L 100 61 26-11069 13 30100ND 60.8 69.3Di-n-octylphthalate ug/L 100 58 22-11064 10 30100ND 57.7 64.0Dibenz(a,h)anthracene ug/L 100 84 21-11286 2 30100ND 84.0 85.9Dibenzofuran ug/L 100 60 19-10269 14 30100ND 60.2 69.2Diethylphthalate ug/L 100 64 29-11073 13 30100ND 63.9 73.0Dimethylphthalate ug/L 100 62 27-11070 12 30100ND 61.8 70.0Fluoranthene ug/L 100 65 23-11274 14 30100ND 64.8 74.4Fluorene ug/L 100 68 22-10475 10 30100ND 67.9 75.3Hexachloro-1,3-butadiene ug/L 100 33 10-11033 2 30100ND 32.6 33.4Hexachlorobenzene ug/L 100 76 21-11680 5 30100ND 76.2 80.1Hexachlorocyclopentadiene ug/L 100 43 10-11049 12 30100ND 43.3 48.7Hexachloroethane ug/L 100 36 10-11036 1 30100ND 35.9 36.1Indeno(1,2,3-cd)pyrene ug/L 100 78 20-11380 2 30100ND 77.9 79.9Isophorone ug/L M0,M1100 39 50-15048 20 30100ND 39.3 47.9N-Nitroso-di-n-propylamine ug/L 100 44 21-10554 20 30100ND 44.4 54.5N-Nitrosodiphenylamine ug/L 100 70 23-10769 1 30100ND 69.7 69.2Naphthalene ug/L 100 37 10-11041 10 30100ND 37.0 41.0Nitrobenzene ug/L 100 37 20-11041 11 30100ND 37.1 41.2Pentachlorophenol ug/L 500 90 10-11890 1 30500ND 450 452Phenanthrene ug/L 100 69 24-10672 5 30100ND 68.9 72.1Phenol ug/L 100 29 12-11034 16 30100ND 29.0 34.2Pyrene ug/L 100 61 24-11464 5 30100ND 60.6 63.62,4,6-Tribromophenol (S) % 82 27-110832-Fluorobiphenyl (S) % 52 27-110612-Fluorophenol (S) % 32 12-11034Nitrobenzene-d5 (S) % 36 21-11039Phenol-d6 (S) % 24 10-11029Terphenyl-d14 (S) % 64 31-10768



Date: 09/27/2010 06:23 PM Page 211 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



MSV/12105EPA 8260

EPA 82608260 MSV Low Level

Associated Lab Samples: 9276750040, 9276750041, 9276750042, 9276750044





Matrix: Water

Analyzed

1,1,1-Trichloroethane ug/L ND 1.0 09/02/10 12:361,1,2,2-Tetrachloroethane ug/L ND 1.0 09/02/10 12:361,1,2-Trichloroethane ug/L ND 1.0 09/02/10 12:361,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/02/10 12:361,1-Dichloroethane ug/L ND 1.0 09/02/10 12:361,1-Dichloroethene ug/L ND 1.0 09/02/10 12:361,2,3-Trichlorobenzene ug/L ND 1.0 09/02/10 12:361,2,4-Trichlorobenzene ug/L ND 1.0 09/02/10 12:361,2-Dibromo-3-chloropropane ug/L ND 5.0 09/02/10 12:361,2-Dibromoethane (EDB) ug/L ND 1.0 09/02/10 12:361,2-Dichlorobenzene ug/L ND 1.0 09/02/10 12:361,2-Dichloroethane ug/L ND 1.0 09/02/10 12:361,2-Dichloropropane ug/L ND 1.0 09/02/10 12:361,3-Dichlorobenzene ug/L ND 1.0 09/02/10 12:361,4-Dichlorobenzene ug/L ND 1.0 09/02/10 12:362-Butanone (MEK) ug/L ND 5.0 09/02/10 12:362-Hexanone ug/L ND 5.0 09/02/10 12:364-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/02/10 12:36Acetone ug/L ND 25.0 09/02/10 12:36Benzene ug/L ND 1.0 09/02/10 12:36Bromochloromethane ug/L ND 1.0 09/02/10 12:36Bromodichloromethane ug/L ND 1.0 09/02/10 12:36Bromoform ug/L ND 1.0 09/02/10 12:36Bromomethane ug/L ND 2.0 09/02/10 12:36Carbon disulfide ug/L ND 2.0 09/02/10 12:36Carbon tetrachloride ug/L ND 1.0 09/02/10 12:36Chlorobenzene ug/L ND 1.0 09/02/10 12:36Chloroethane ug/L ND 1.0 09/02/10 12:36Chloroform ug/L ND 1.0 09/02/10 12:36Chloromethane ug/L ND 1.0 09/02/10 12:36cis-1,2-Dichloroethene ug/L ND 1.0 09/02/10 12:36cis-1,3-Dichloropropene ug/L ND 1.0 09/02/10 12:36Cyclohexane ug/L ND 1.0 09/02/10 12:36Dibromochloromethane ug/L ND 1.0 09/02/10 12:36Dichlorodifluoromethane ug/L ND 1.0 09/02/10 12:36Ethylbenzene ug/L ND 1.0 09/02/10 12:36Isopropylbenzene (Cumene) ug/L ND 1.0 09/02/10 12:36m&p-Xylene ug/L ND 2.0 09/02/10 12:36Methyl acetate ug/L ND 10.0 09/02/10 12:36Methyl-tert-butyl ether ug/L ND 1.0 09/02/10 12:36Methylcyclohexane ug/L ND 10.0 09/02/10 12:36Methylene Chloride ug/L ND 2.0 09/02/10 12:36o-Xylene ug/L ND 1.0 09/02/10 12:36



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Matrix: Water

Analyzed

Styrene ug/L ND 1.0 09/02/10 12:36Tetrachloroethene ug/L ND 1.0 09/02/10 12:36Toluene ug/L ND 1.0 09/02/10 12:36trans-1,2-Dichloroethene ug/L ND 1.0 09/02/10 12:36trans-1,3-Dichloropropene ug/L ND 1.0 09/02/10 12:36Trichloroethene ug/L ND 1.0 09/02/10 12:36Trichlorofluoromethane ug/L ND 1.0 09/02/10 12:36Vinyl chloride ug/L ND 1.0 09/02/10 12:36Xylene (Total) ug/L ND 2.0 09/02/10 12:361,2-Dichloroethane-d4 (S) % 99 70-130 09/02/10 12:364-Bromofluorobenzene (S) % 87 70-130 09/02/10 12:36Dibromofluoromethane (S) % 97 70-130 09/02/10 12:36Toluene-d8 (S) % 99 70-130 09/02/10 12:36

Parameter UnitsLCS



1,1,1-Trichloroethane ug/L 61.250 122 70-1301,1,2,2-Tetrachloroethane ug/L 55.550 111 70-1301,1,2-Trichloroethane ug/L 60.150 120 70-1301,1,2-Trichlorotrifluoroethane ug/L 54.550 109 70-1301,1-Dichloroethane ug/L 62.650 125 70-1301,1-Dichloroethene ug/L 59.750 119 70-1321,2,3-Trichlorobenzene ug/L 53.750 107 70-1351,2,4-Trichlorobenzene ug/L 52.650 105 70-1341,2-Dibromo-3-chloropropane ug/L 52.950 106 70-1301,2-Dibromoethane (EDB) ug/L 54.550 109 70-1301,2-Dichlorobenzene ug/L 53.950 108 70-1301,2-Dichloroethane ug/L 62.150 124 70-1301,2-Dichloropropane ug/L 56.850 114 70-1301,3-Dichlorobenzene ug/L 52.850 106 70-1301,4-Dichlorobenzene ug/L 52.450 105 70-1302-Butanone (MEK) ug/L 112100 112 70-1452-Hexanone ug/L 107100 107 70-1444-Methyl-2-pentanone (MIBK) ug/L 113100 113 70-140Acetone ug/L 113100 113 50-175Benzene ug/L 66.8 L350 134 70-130Bromochloromethane ug/L 62.850 126 70-130Bromodichloromethane ug/L 58.450 117 70-130Bromoform ug/L 55.850 112 70-130Bromomethane ug/L 48.050 96 54-130Carbon disulfide ug/L 61.750 123 70-131Carbon tetrachloride ug/L 61.250 122 70-132Chlorobenzene ug/L 58.350 117 70-130Chloroethane ug/L 58.350 117 64-134



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9276750MILLS GAP 6686081744

Parameter UnitsLCS



Chloroform ug/L 59.250 118 70-130Chloromethane ug/L 48.650 97 64-130cis-1,2-Dichloroethene ug/L 60.450 121 70-131cis-1,3-Dichloropropene ug/L 52.150 104 70-130Cyclohexane ug/L 62.850 126 70-130Dibromochloromethane ug/L 54.250 108 70-130Dichlorodifluoromethane ug/L 53.750 107 56-130Ethylbenzene ug/L 57.550 115 70-130Isopropylbenzene (Cumene) ug/L 52.650 105 70-130m&p-Xylene ug/L 116100 116 70-130Methyl acetate ug/L 62.150 124 70-130Methyl-tert-butyl ether ug/L 54.350 109 70-130Methylcyclohexane ug/L 59.150 118 70-130Methylene Chloride ug/L 55.350 111 63-130o-Xylene ug/L 53.450 107 70-130Styrene ug/L 53.550 107 70-130Tetrachloroethene ug/L 55.250 110 70-130Toluene ug/L 59.950 120 70-130trans-1,2-Dichloroethene ug/L 60.450 121 70-130trans-1,3-Dichloropropene ug/L 53.550 107 70-132Trichloroethene ug/L 58.450 117 70-130Trichlorofluoromethane ug/L 57.650 115 62-133Vinyl chloride ug/L 57.850 116 69-130Xylene (Total) ug/L 169150 113 70-1301,2-Dichloroethane-d4 (S) % 104 70-1304-Bromofluorobenzene (S) % 99 70-130Dibromofluoromethane (S) % 103 70-130Toluene-d8 (S) % 102 70-130

Parameter UnitsMS



MSSpikeResult

9276703002

492928

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/L 50 100 70-16695 5 3050ND 49.8 47.3Benzene ug/L 50 110 70-148107 2 3050ND 55.0 53.7Chlorobenzene ug/L 50 110 70-146110 0 3050ND 55.1 55.0Toluene ug/L 50 109 70-155106 3 3050ND 54.5 53.1Trichloroethene ug/L 50 113 69-151110 2 3050ND 56.5 55.11,2-Dichloroethane-d4 (S) % 84 70-130874-Bromofluorobenzene (S) % 95 70-130102Dibromofluoromethane (S) % 100 70-130102Toluene-d8 (S) % 92 70-13091



Date: 09/27/2010 06:23 PM Page 214 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



MSV/12135EPA 8260

EPA 82608260 MSV 5035A Volatile Organics






Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/05/10 11:161,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/05/10 11:161,1,2-Trichloroethane ug/kg ND 5.0 09/05/10 11:161,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/05/10 11:161,1-Dichloroethane ug/kg ND 5.0 09/05/10 11:161,1-Dichloroethene ug/kg ND 5.0 09/05/10 11:161,2,3-Trichlorobenzene ug/kg ND 5.0 09/05/10 11:161,2,4-Trichlorobenzene ug/kg ND 5.0 09/05/10 11:161,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/05/10 11:161,2-Dibromoethane (EDB) ug/kg ND 5.0 09/05/10 11:161,2-Dichlorobenzene ug/kg ND 5.0 09/05/10 11:161,2-Dichloroethane ug/kg ND 5.0 09/05/10 11:161,2-Dichloropropane ug/kg ND 5.0 09/05/10 11:161,3-Dichlorobenzene ug/kg ND 5.0 09/05/10 11:161,4-Dichlorobenzene ug/kg ND 5.0 09/05/10 11:162-Butanone (MEK) ug/kg ND 100 09/05/10 11:162-Hexanone ug/kg ND 50.0 09/05/10 11:164-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/05/10 11:16Acetone ug/kg ND 100 09/05/10 11:16Benzene ug/kg ND 5.0 09/05/10 11:16Bromochloromethane ug/kg ND 5.0 09/05/10 11:16Bromodichloromethane ug/kg ND 5.0 09/05/10 11:16Bromoform ug/kg ND 5.0 09/05/10 11:16Bromomethane ug/kg ND 10.0 09/05/10 11:16Carbon disulfide ug/kg ND 10.0 09/05/10 11:16Carbon tetrachloride ug/kg ND 5.0 09/05/10 11:16Chlorobenzene ug/kg ND 5.0 09/05/10 11:16Chloroethane ug/kg ND 10.0 09/05/10 11:16Chloroform ug/kg ND 5.0 09/05/10 11:16Chloromethane ug/kg ND 10.0 09/05/10 11:16cis-1,2-Dichloroethene ug/kg ND 5.0 09/05/10 11:16cis-1,3-Dichloropropene ug/kg ND 5.0 09/05/10 11:16Cyclohexane ug/kg ND 5.0 09/05/10 11:16Dibromochloromethane ug/kg ND 5.0 09/05/10 11:16Dichlorodifluoromethane ug/kg ND 10.0 09/05/10 11:16Ethylbenzene ug/kg ND 5.0 09/05/10 11:16Isopropylbenzene (Cumene) ug/kg ND 5.0 09/05/10 11:16m&p-Xylene ug/kg ND 10.0 09/05/10 11:16Methyl acetate ug/kg ND 10.0 09/05/10 11:16Methyl-tert-butyl ether ug/kg ND 5.0 09/05/10 11:16Methylcyclohexane ug/kg ND 10.0 09/05/10 11:16Methylene Chloride ug/kg ND 20.0 09/05/10 11:16o-Xylene ug/kg ND 5.0 09/05/10 11:16



Date: 09/27/2010 06:23 PM Page 215 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Styrene ug/kg ND 5.0 09/05/10 11:16Tetrachloroethene ug/kg ND 5.0 09/05/10 11:16Toluene ug/kg ND 5.0 09/05/10 11:16trans-1,2-Dichloroethene ug/kg ND 5.0 09/05/10 11:16trans-1,3-Dichloropropene ug/kg ND 5.0 09/05/10 11:16Trichloroethene ug/kg ND 5.0 09/05/10 11:16Trichlorofluoromethane ug/kg ND 5.0 09/05/10 11:16Vinyl chloride ug/kg ND 10.0 09/05/10 11:16Xylene (Total) ug/kg ND 10.0 09/05/10 11:161,2-Dichloroethane-d4 (S) % 102 70-132 09/05/10 11:164-Bromofluorobenzene (S) % 96 70-130 09/05/10 11:16Dibromofluoromethane (S) % 101 70-130 09/05/10 11:16Toluene-d8 (S) % 100 70-130 09/05/10 11:16

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 48.650 97 70-1411,1,2,2-Tetrachloroethane ug/kg 51.850 104 70-1301,1,2-Trichloroethane ug/kg 50.650 101 70-1321,1,2-Trichlorotrifluoroethane ug/kg 52.450 105 70-1301,1-Dichloroethane ug/kg 53.050 106 70-1431,1-Dichloroethene ug/kg 55.250 110 70-1371,2,3-Trichlorobenzene ug/kg 47.250 94 69-1531,2,4-Trichlorobenzene ug/kg 47.150 94 55-1711,2-Dibromo-3-chloropropane ug/kg 48.750 97 68-1411,2-Dibromoethane (EDB) ug/kg 50.050 100 70-1301,2-Dichlorobenzene ug/kg 50.550 101 70-1401,2-Dichloroethane ug/kg 50.050 100 70-1371,2-Dichloropropane ug/kg 48.150 96 70-1331,3-Dichlorobenzene ug/kg 50.550 101 70-1441,4-Dichlorobenzene ug/kg 47.650 95 70-1422-Butanone (MEK) ug/kg 101100 101 70-1492-Hexanone ug/kg 107100 107 70-1494-Methyl-2-pentanone (MIBK) ug/kg 98.6100 99 70-153Acetone ug/kg 117100 117 70-157Benzene ug/kg 49.650 99 70-130Bromochloromethane ug/kg 56.550 113 70-149Bromodichloromethane ug/kg 49.050 98 70-130Bromoform ug/kg 45.850 92 70-131Bromomethane ug/kg 54.750 109 64-136Carbon disulfide ug/kg 51.450 103 70-130Carbon tetrachloride ug/kg 55.650 111 70-154Chlorobenzene ug/kg 50.150 100 70-135Chloroethane ug/kg 56.850 114 68-151



Date: 09/27/2010 06:23 PM Page 216 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



Chloroform ug/kg 51.050 102 70-130Chloromethane ug/kg 50.150 100 70-132cis-1,2-Dichloroethene ug/kg 51.450 103 70-140cis-1,3-Dichloropropene ug/kg 48.550 97 70-137Cyclohexane ug/kg 51.250 102 70-130Dibromochloromethane ug/kg 45.950 92 70-130Dichlorodifluoromethane ug/kg 49.350 99 36-148Ethylbenzene ug/kg 51.850 104 70-137Isopropylbenzene (Cumene) ug/kg 52.750 105 70-141m&p-Xylene ug/kg 104100 104 70-140Methyl acetate ug/kg 41.750 83 70-130Methyl-tert-butyl ether ug/kg 50.450 101 45-150Methylcyclohexane ug/kg 52.550 105 70-130Methylene Chloride ug/kg 40.050 80 70-133o-Xylene ug/kg 52.250 104 70-141Styrene ug/kg 51.350 103 70-138Tetrachloroethene ug/kg 50.950 102 70-140Toluene ug/kg 50.750 101 70-130trans-1,2-Dichloroethene ug/kg 51.850 104 70-136trans-1,3-Dichloropropene ug/kg 49.150 98 70-138Trichloroethene ug/kg 50.650 101 70-132Trichlorofluoromethane ug/kg 56.650 113 69-134Vinyl chloride ug/kg 53.550 107 55-140Xylene (Total) ug/kg 156150 104 70-1411,2-Dichloroethane-d4 (S) % 98 70-1324-Bromofluorobenzene (S) % 97 70-130Dibromofluoromethane (S) % 98 70-130Toluene-d8 (S) % 99 70-130

Parameter UnitsMS



MSSpikeResult

9276750007

493680

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg 53 104 49-180142 27 3050.9ND 55.2 72.5Benzene ug/kg R153 96 50-166146 37 3050.9ND 50.9 74.2Chlorobenzene ug/kg R153 92 43-169143 40 3050.9ND 48.7 72.9Toluene ug/kg R153 97 52-163145 36 3050.9ND 51.6 73.9Trichloroethene ug/kg R153 104 49-167153 35 3050.9ND 55.0 78.11,2-Dichloroethane-d4 (S) % 107 70-1321004-Bromofluorobenzene (S) % 98 70-13099Dibromofluoromethane (S) % 101 70-13099Toluene-d8 (S) % 97 70-130101



Date: 09/27/2010 06:23 PM Page 217 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



MSV/12138EPA 8260







Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/07/10 13:281,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/07/10 13:281,1,2-Trichloroethane ug/kg ND 5.0 09/07/10 13:281,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/07/10 13:281,1-Dichloroethane ug/kg ND 5.0 09/07/10 13:281,1-Dichloroethene ug/kg ND 5.0 09/07/10 13:281,2,3-Trichlorobenzene ug/kg ND 5.0 09/07/10 13:281,2,4-Trichlorobenzene ug/kg ND 5.0 09/07/10 13:281,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/07/10 13:281,2-Dibromoethane (EDB) ug/kg ND 5.0 09/07/10 13:281,2-Dichlorobenzene ug/kg ND 5.0 09/07/10 13:281,2-Dichloroethane ug/kg ND 5.0 09/07/10 13:281,2-Dichloropropane ug/kg ND 5.0 09/07/10 13:281,3-Dichlorobenzene ug/kg ND 5.0 09/07/10 13:281,4-Dichlorobenzene ug/kg ND 5.0 09/07/10 13:282-Butanone (MEK) ug/kg ND 100 09/07/10 13:282-Hexanone ug/kg ND 50.0 09/07/10 13:284-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/07/10 13:28Acetone ug/kg ND 100 09/07/10 13:28Benzene ug/kg ND 5.0 09/07/10 13:28Bromochloromethane ug/kg ND 5.0 09/07/10 13:28Bromodichloromethane ug/kg ND 5.0 09/07/10 13:28Bromoform ug/kg ND 5.0 09/07/10 13:28Bromomethane ug/kg ND 10.0 09/07/10 13:28Carbon disulfide ug/kg ND 10.0 09/07/10 13:28Carbon tetrachloride ug/kg ND 5.0 09/07/10 13:28Chlorobenzene ug/kg ND 5.0 09/07/10 13:28Chloroethane ug/kg ND 10.0 09/07/10 13:28Chloroform ug/kg ND 5.0 09/07/10 13:28Chloromethane ug/kg ND 10.0 09/07/10 13:28cis-1,2-Dichloroethene ug/kg ND 5.0 09/07/10 13:28cis-1,3-Dichloropropene ug/kg ND 5.0 09/07/10 13:28Cyclohexane ug/kg ND 5.0 09/07/10 13:28Dibromochloromethane ug/kg ND 5.0 09/07/10 13:28Dichlorodifluoromethane ug/kg ND 10.0 09/07/10 13:28Ethylbenzene ug/kg ND 5.0 09/07/10 13:28Isopropylbenzene (Cumene) ug/kg ND 5.0 09/07/10 13:28m&p-Xylene ug/kg ND 10.0 09/07/10 13:28Methyl acetate ug/kg ND 10.0 09/07/10 13:28Methyl-tert-butyl ether ug/kg ND 5.0 09/07/10 13:28Methylcyclohexane ug/kg ND 10.0 09/07/10 13:28



Date: 09/27/2010 06:23 PM Page 218 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Methylene Chloride ug/kg ND 20.0 09/07/10 13:28o-Xylene ug/kg ND 5.0 09/07/10 13:28Styrene ug/kg ND 5.0 09/07/10 13:28Tetrachloroethene ug/kg ND 5.0 09/07/10 13:28Toluene ug/kg ND 5.0 09/07/10 13:28trans-1,2-Dichloroethene ug/kg ND 5.0 09/07/10 13:28trans-1,3-Dichloropropene ug/kg ND 5.0 09/07/10 13:28Trichloroethene ug/kg ND 5.0 09/07/10 13:28Trichlorofluoromethane ug/kg ND 5.0 09/07/10 13:28Vinyl chloride ug/kg ND 10.0 09/07/10 13:28Xylene (Total) ug/kg ND 10.0 09/07/10 13:281,2-Dichloroethane-d4 (S) % 99 70-132 09/07/10 13:284-Bromofluorobenzene (S) % 96 70-130 09/07/10 13:28Dibromofluoromethane (S) % 101 70-130 09/07/10 13:28Toluene-d8 (S) % 101 70-130 09/07/10 13:28

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 65.550 131 70-1411,1,2,2-Tetrachloroethane ug/kg 63.350 127 70-1301,1,2-Trichloroethane ug/kg 63.450 127 70-1321,1,2-Trichlorotrifluoroethane ug/kg 67.1 L350 134 70-1301,1-Dichloroethane ug/kg 65.250 130 70-1431,1-Dichloroethene ug/kg 65.650 131 70-1371,2,3-Trichlorobenzene ug/kg 67.650 135 69-1531,2,4-Trichlorobenzene ug/kg 64.350 129 55-1711,2-Dibromo-3-chloropropane ug/kg 60.050 120 68-1411,2-Dibromoethane (EDB) ug/kg 59.650 119 70-1301,2-Dichlorobenzene ug/kg 63.650 127 70-1401,2-Dichloroethane ug/kg 64.050 128 70-1371,2-Dichloropropane ug/kg 61.450 123 70-1331,3-Dichlorobenzene ug/kg 63.050 126 70-1441,4-Dichlorobenzene ug/kg 63.550 127 70-1422-Butanone (MEK) ug/kg 125100 125 70-1492-Hexanone ug/kg 128100 128 70-1494-Methyl-2-pentanone (MIBK) ug/kg 120100 120 70-153Acetone ug/kg 120100 120 70-157Benzene ug/kg 63.950 128 70-130Bromochloromethane ug/kg 64.250 128 70-149Bromodichloromethane ug/kg 64.550 129 70-130Bromoform ug/kg 59.950 120 70-131Bromomethane ug/kg 78.5 L350 157 64-136Carbon disulfide ug/kg 65.8 L350 132 70-130



Date: 09/27/2010 06:23 PM Page 219 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



Carbon tetrachloride ug/kg 68.250 136 70-154Chlorobenzene ug/kg 65.150 130 70-135Chloroethane ug/kg 61.950 124 68-151Chloroform ug/kg 65.3 L350 131 70-130Chloromethane ug/kg 66.3 L350 133 70-132cis-1,2-Dichloroethene ug/kg 64.650 129 70-140cis-1,3-Dichloropropene ug/kg 61.150 122 70-137Cyclohexane ug/kg 63.950 128 70-130Dibromochloromethane ug/kg 62.650 125 70-130Dichlorodifluoromethane ug/kg 62.250 124 36-148Ethylbenzene ug/kg 65.450 131 70-137Isopropylbenzene (Cumene) ug/kg 66.950 134 70-141m&p-Xylene ug/kg 132100 132 70-140Methyl acetate ug/kg 39.950 80 70-130Methyl-tert-butyl ether ug/kg 60.350 121 45-150Methylcyclohexane ug/kg 64.750 129 70-130Methylene Chloride ug/kg 59.750 119 70-133o-Xylene ug/kg 67.050 134 70-141Styrene ug/kg 61.550 123 70-138Tetrachloroethene ug/kg 64.750 129 70-140Toluene ug/kg 63.550 127 70-130trans-1,2-Dichloroethene ug/kg 63.350 127 70-136trans-1,3-Dichloropropene ug/kg 61.250 122 70-138Trichloroethene ug/kg 65.050 130 70-132Trichlorofluoromethane ug/kg 65.350 131 69-134Vinyl chloride ug/kg 65.050 130 55-140Xylene (Total) ug/kg 199150 133 70-1411,2-Dichloroethane-d4 (S) % 100 70-1324-Bromofluorobenzene (S) % 101 70-130Dibromofluoromethane (S) % 101 70-130Toluene-d8 (S) % 98 70-130

Parameter UnitsMS



Result9276750005

1,1-Dichloroethene ug/kg 63.048 131 49-180NDBenzene ug/kg 64.948 135 50-166NDChlorobenzene ug/kg 64.748 135 43-169NDToluene ug/kg 64.648 135 52-163NDTrichloroethene ug/kg 68.748 137 49-1673.2J1,2-Dichloroethane-d4 (S) % 99 70-1324-Bromofluorobenzene (S) % 96 70-130Dibromofluoromethane (S) % 98 70-130Toluene-d8 (S) % 99 70-130



Date: 09/27/2010 06:23 PM Page 220 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsDup



1,1,1-Trichloroethane ug/kg ND 30ND1,1,2,2-Tetrachloroethane ug/kg ND 30ND1,1,2-Trichloroethane ug/kg ND 30ND1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND1,1-Dichloroethane ug/kg ND 30ND1,1-Dichloroethene ug/kg ND 30ND1,2,3-Trichlorobenzene ug/kg ND 30ND1,2,4-Trichlorobenzene ug/kg ND 30ND1,2-Dibromo-3-chloropropane ug/kg ND 30ND1,2-Dibromoethane (EDB) ug/kg ND 30ND1,2-Dichlorobenzene ug/kg ND 30ND1,2-Dichloroethane ug/kg ND 30ND1,2-Dichloropropane ug/kg ND 30ND1,3-Dichlorobenzene ug/kg ND 30ND1,4-Dichlorobenzene ug/kg ND 30ND2-Butanone (MEK) ug/kg 5.8J 30ND2-Hexanone ug/kg ND 30ND4-Methyl-2-pentanone (MIBK) ug/kg ND 30NDAcetone ug/kg 38.6J 30NDBenzene ug/kg ND 30NDBromochloromethane ug/kg ND 30NDBromodichloromethane ug/kg ND 30NDBromoform ug/kg ND 30NDBromomethane ug/kg ND 30NDCarbon disulfide ug/kg ND 30NDCarbon tetrachloride ug/kg ND 30NDChlorobenzene ug/kg ND 30NDChloroethane ug/kg ND 30NDChloroform ug/kg ND 30NDChloromethane ug/kg ND 30NDcis-1,2-Dichloroethene ug/kg ND 30NDcis-1,3-Dichloropropene ug/kg ND 30NDCyclohexane ug/kg ND 30NDDibromochloromethane ug/kg ND 30NDDichlorodifluoromethane ug/kg ND 30NDEthylbenzene ug/kg ND 30NDIsopropylbenzene (Cumene) ug/kg ND 30NDm&p-Xylene ug/kg ND 30NDMethyl acetate ug/kg ND 30NDMethyl-tert-butyl ether ug/kg ND 30NDMethylcyclohexane ug/kg ND 30NDMethylene Chloride ug/kg ND 30NDo-Xylene ug/kg ND 30NDStyrene ug/kg ND 30NDTetrachloroethene ug/kg ND 30NDToluene ug/kg ND 30NDtrans-1,2-Dichloroethene ug/kg ND 30NDtrans-1,3-Dichloropropene ug/kg ND 30ND



Date: 09/27/2010 06:23 PM Page 221 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsDup



Trichloroethene ug/kg ND 30NDTrichlorofluoromethane ug/kg ND 30NDVinyl chloride ug/kg ND 30NDXylene (Total) ug/kg ND 30ND1,2-Dichloroethane-d4 (S) % 96 41004-Bromofluorobenzene (S) % 96 096Dibromofluoromethane (S) % 97 3100Toluene-d8 (S) % 100 1100



Date: 09/27/2010 06:23 PM Page 222 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744



MSV/12151EPA 8260







Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/08/10 00:391,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/08/10 00:391,1,2-Trichloroethane ug/kg ND 5.0 09/08/10 00:391,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/08/10 00:391,1-Dichloroethane ug/kg ND 5.0 09/08/10 00:391,1-Dichloroethene ug/kg ND 5.0 09/08/10 00:391,2,3-Trichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2,4-Trichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/08/10 00:391,2-Dibromoethane (EDB) ug/kg ND 5.0 09/08/10 00:391,2-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2-Dichloroethane ug/kg ND 5.0 09/08/10 00:391,2-Dichloropropane ug/kg ND 5.0 09/08/10 00:391,3-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:391,4-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:392-Butanone (MEK) ug/kg ND 100 09/08/10 00:392-Hexanone ug/kg ND 50.0 09/08/10 00:394-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/08/10 00:39Acetone ug/kg ND 100 09/08/10 00:39Benzene ug/kg ND 5.0 09/08/10 00:39Bromochloromethane ug/kg ND 5.0 09/08/10 00:39Bromodichloromethane ug/kg ND 5.0 09/08/10 00:39Bromoform ug/kg ND 5.0 09/08/10 00:39Bromomethane ug/kg ND 10.0 09/08/10 00:39Carbon disulfide ug/kg ND 10.0 09/08/10 00:39Carbon tetrachloride ug/kg ND 5.0 09/08/10 00:39Chlorobenzene ug/kg ND 5.0 09/08/10 00:39Chloroethane ug/kg ND 10.0 09/08/10 00:39Chloroform ug/kg ND 5.0 09/08/10 00:39Chloromethane ug/kg ND 10.0 09/08/10 00:39cis-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 00:39cis-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 00:39Cyclohexane ug/kg ND 5.0 09/08/10 00:39Dibromochloromethane ug/kg ND 5.0 09/08/10 00:39Dichlorodifluoromethane ug/kg ND 10.0 09/08/10 00:39Ethylbenzene ug/kg ND 5.0 09/08/10 00:39Isopropylbenzene (Cumene) ug/kg ND 5.0 09/08/10 00:39m&p-Xylene ug/kg ND 10.0 09/08/10 00:39Methyl acetate ug/kg ND 10.0 09/08/10 00:39Methyl-tert-butyl ether ug/kg ND 5.0 09/08/10 00:39Methylcyclohexane ug/kg ND 10.0 09/08/10 00:39



Date: 09/27/2010 06:23 PM Page 223 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744





Matrix: Solid

Analyzed

Methylene Chloride ug/kg ND 20.0 09/08/10 00:39o-Xylene ug/kg ND 5.0 09/08/10 00:39Styrene ug/kg ND 5.0 09/08/10 00:39Tetrachloroethene ug/kg ND 5.0 09/08/10 00:39Toluene ug/kg ND 5.0 09/08/10 00:39trans-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 00:39trans-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 00:39Trichloroethene ug/kg ND 5.0 09/08/10 00:39Trichlorofluoromethane ug/kg ND 5.0 09/08/10 00:39Vinyl chloride ug/kg ND 10.0 09/08/10 00:39Xylene (Total) ug/kg ND 10.0 09/08/10 00:391,2-Dichloroethane-d4 (S) % 99 70-132 09/08/10 00:394-Bromofluorobenzene (S) % 96 70-130 09/08/10 00:39Dibromofluoromethane (S) % 99 70-130 09/08/10 00:39Toluene-d8 (S) % 101 70-130 09/08/10 00:39

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 61.550 123 70-1411,1,2,2-Tetrachloroethane ug/kg 63.550 127 70-1301,1,2-Trichloroethane ug/kg 61.750 123 70-1321,1,2-Trichlorotrifluoroethane ug/kg 57.650 115 70-1301,1-Dichloroethane ug/kg 61.650 123 70-1431,1-Dichloroethene ug/kg 56.850 114 70-1371,2,3-Trichlorobenzene ug/kg 59.050 118 69-1531,2,4-Trichlorobenzene ug/kg 55.850 112 55-1711,2-Dibromo-3-chloropropane ug/kg 62.250 124 68-1411,2-Dibromoethane (EDB) ug/kg 59.550 119 70-1301,2-Dichlorobenzene ug/kg 58.550 117 70-1401,2-Dichloroethane ug/kg 61.850 124 70-1371,2-Dichloropropane ug/kg 59.950 120 70-1331,3-Dichlorobenzene ug/kg 56.650 113 70-1441,4-Dichlorobenzene ug/kg 56.950 114 70-1422-Butanone (MEK) ug/kg 128100 128 70-1492-Hexanone ug/kg 131100 131 70-1494-Methyl-2-pentanone (MIBK) ug/kg 126100 126 70-153Acetone ug/kg 126100 126 70-157Benzene ug/kg 61.350 123 70-130Bromochloromethane ug/kg 64.350 129 70-149Bromodichloromethane ug/kg 61.550 123 70-130Bromoform ug/kg 57.250 114 70-131Bromomethane ug/kg 79.0 L350 158 64-136Carbon disulfide ug/kg 58.750 117 70-130



Date: 09/27/2010 06:23 PM Page 224 of 242



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276750MILLS GAP 6686081744

Parameter UnitsLCS



Carbon tetrachloride ug/kg 62.650 125 70-154Chlorobenzene ug/kg 60.850 122 70-135Chloroethane ug/kg 61.550 123 68-151Chloroform ug/kg 61.250 122 70-130Chloromethane ug/kg 58.050 116 70-132cis-1,2-Dichloroethene ug/kg 60.250 120 70-140cis-1,3-Dichloropropene ug/kg 56.550 113 70-137Cyclohexane ug/kg 57.450 115 70-130Dibromochloromethane ug/kg 60.050 120 70-130Dichlorodifluoromethane ug/kg 50.950 102 36-148Ethylbenzene ug/kg 59.050 118 70-137Isopropylbenzene (Cumene) ug/kg 60.850 122 70-141m&p-Xylene ug/kg 120100 120 70-140Methyl acetate ug/kg 19.3 L050 39 70-130Methyl-tert-butyl ether ug/kg 58.350 117 45-150Methylcyclohexane ug/kg 58.650 117 70-130Methylene Chloride ug/kg 62.650 125 70-133o-Xylene ug/kg 61.350 123 70-141Styrene ug/kg 57.450 115 70-138Tetrachloroethene ug/kg 57.750 115 70-140Toluene ug/kg 59.150 118 70-130trans-1,2-Dichloroethene ug/kg 57.650 115 70-136trans-1,3-Dichloropropene ug/kg 56.250 112 70-138Trichloroethene ug/kg 59.850 120 70-132Trichlorofluoromethane ug/kg 57.250 114 69-134Vinyl chloride ug/kg 60.450 121 55-140Xylene (Total) ug/kg 181150 121 70-1411,2-Dichloroethane-d4 (S) % 102 70-1324-Bromofluorobenzene (S) % 102 70-130Dibromofluoromethane (S) % 100 70-130Toluene-d8 (S) % 100 70-130

Parameter UnitsMS



MSSpikeResult

9276750025

493936

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg 53 155 49-180131 16 3053.3ND 82.1 70.0Benzene ug/kg 53 148 50-166127 14 3053.3ND 78.2 67.8Chlorobenzene ug/kg 53 147 43-169122 18 3053.3ND 77.9 64.8Toluene ug/kg 53 146 52-163125 15 3053.3ND 77.4 66.7Trichloroethene ug/kg R153 133 49-167382 34 3053.3258 329 4621,2-Dichloroethane-d4 (S) % 99 70-132984-Bromofluorobenzene (S) % 100 70-13098Dibromofluoromethane (S) % 97 70-13099Toluene-d8 (S) % 98 70-13099



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PMST/3390ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture

Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005, 9276750006, 9276750007, 9276750009,9276750011, 9276750033, 9276750034

Parameter UnitsDup



Percent Moisture % 29.5 2 2529.0

Parameter UnitsDup






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Associated Lab Samples: 9276750012, 9276750013, 9276750014, 9276750015, 9276750016, 9276750017, 9276750018, 9276750019,9276750020, 9276750021, 9276750022, 9276750023, 9276750024, 9276750025, 9276750026, 9276750027,9276750028, 9276750029, 9276750030, 9276750031

Parameter UnitsDup




Parameter UnitsDup






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Parameter UnitsDup




Parameter UnitsDup






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Parameter UnitsDup




Parameter UnitsDup






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WETA/8109SM 4500-CN-E

SM 4500-CN-E4500CNE Cyanide, Total






Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/05/10 13:23

Parameter UnitsLCS



Cyanide mg/kg 3.23 106 80-120

Parameter UnitsMS



Result9276750006

Cyanide mg/kg 3.02.9 102 75-125ND

Parameter UnitsDup



Cyanide mg/kg ND 20ND



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Associated Lab Samples: 9276750014, 9276750015, 9276750016, 9276750017, 9276750018, 9276750019, 9276750020, 9276750021,9276750022, 9276750023, 9276750024, 9276750025, 9276750026, 9276750027, 9276750028, 9276750029,9276750033




Associated Lab Samples: 9276750014, 9276750015, 9276750016, 9276750017, 9276750018, 9276750019, 9276750020, 9276750021,9276750022, 9276750023, 9276750024, 9276750025, 9276750026, 9276750027, 9276750028, 9276750029,9276750033

Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/05/10 13:45

Parameter UnitsLCS



Cyanide mg/kg 3.13 103 80-120

Parameter UnitsMS



Result9276750029

Cyanide mg/kg 2.92.9 103 75-125ND

Parameter UnitsDup






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Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/12/10 16:15

Parameter UnitsLCS



Cyanide mg/kg 3.23 108 80-120

Parameter UnitsMS



Result9276872011

Cyanide mg/kg 2.32.5 87 75-125ND

Parameter UnitsDup






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Matrix: Water

Analyzed

Cyanide mg/L ND 0.0050 09/05/10 14:08

Parameter UnitsLCS



Cyanide mg/L 0.11.1 108 80-120

Parameter UnitsMS



Result9276599001

Cyanide mg/L 0.11.1 107 75-125ND

Parameter UnitsDup



Cyanide mg/L ND 20ND



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WETA/8087EPA 7196

EPA 71967196 Chromium, Hexavalent

Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005, 9276750007, 9276750012




Associated Lab Samples: 9276750001, 9276750002, 9276750003, 9276750004, 9276750005, 9276750007, 9276750012

Matrix: Solid

Analyzed

Chromium, Hexavalent mg/kg ND 5.0 09/02/10 15:20

Parameter UnitsLCS



Chromium, Hexavalent mg/kg 49.450 99 90-110

Parameter UnitsMS



Result9276756001

Chromium, Hexavalent mg/kg 10.6 M143.8 24 75-125ND

Parameter UnitsMS



Result9276756003

Chromium, Hexavalent mg/kg ND M144.3 0 75-125ND

Parameter UnitsDup



Chromium, Hexavalent mg/kg ND 20ND

Parameter UnitsDup






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WETA/8088EPA 7196


Associated Lab Samples: 9276750006, 9276750013, 9276750014, 9276750015, 9276750016, 9276750017, 9276750018, 9276750019,9276750020, 9276750022, 9276750023, 9276750024, 9276750025, 9276750027, 9276750028, 9276750029,9276750035, 9276750038




Associated Lab Samples: 9276750006, 9276750013, 9276750014, 9276750015, 9276750016, 9276750017, 9276750018, 9276750019,9276750020, 9276750022, 9276750023, 9276750024, 9276750025, 9276750027, 9276750028, 9276750029,9276750035, 9276750038

Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276750013

Chromium, Hexavalent mg/kg 27.1 M139.8 64 75-125ND

Parameter UnitsMS



Result9276750028

Chromium, Hexavalent mg/kg 49.349.7 98 75-125ND

Parameter UnitsDup




Parameter UnitsDup






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WETA/8098EPA 7196







Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276833001

Chromium, Hexavalent mg/kg ND M147.7 0 75-125ND

Parameter UnitsMS



Result9276872013

Chromium, Hexavalent mg/kg 46.548.5 94 75-125ND

Parameter UnitsDup




Parameter UnitsDup






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QUALIFIERS


9276750MILLS GAP 6686081744

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

ANALYTE QUALIFIERS

Analyte was detected in the associated method blank.BResult confirmed by second analysis.C0Common Laboratory Contaminant.C9Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6Analyte concentration exceeded the calibration range. The reported result is estimated.EAnalyte recovery in the laboratory control sample (LCS) was outside QC limits.L0Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.

L1

Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.

L2

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1RPD value was outside control limits.R1Surrogate recovery outside laboratory control limits.S0



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QUALITY CONTROL DATA CROSS REFERENCE TABLE


9276750MILLS GAP 6686081744

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

9276750001 MPRP/7021 ICP/6473SS-113A EPA 3050 EPA 60109276750002 MPRP/7021 ICP/6473SS-113B EPA 3050 EPA 60109276750003 MPRP/7021 ICP/6473SS-116A EPA 3050 EPA 60109276750004 MPRP/7021 ICP/6473SS-116B EPA 3050 EPA 60109276750005 MPRP/7021 ICP/6473SS-122 EPA 3050 EPA 60109276750006 MPRP/7021 ICP/6473SS-125 EPA 3050 EPA 60109276750007 MPRP/7021 ICP/6473SS-126 EPA 3050 EPA 60109276750009 MPRP/7021 ICP/6473FD-02 EPA 3050 EPA 60109276750013 MPRP/7021 ICP/6473SS-127 EPA 3050 EPA 60109276750014 MPRP/7021 ICP/6473SS-128 EPA 3050 EPA 60109276750015 MPRP/7021 ICP/6473SS-129 EPA 3050 EPA 60109276750016 MPRP/7021 ICP/6473SS-109A EPA 3050 EPA 60109276750017 MPRP/7021 ICP/6473SS-109B EPA 3050 EPA 6010

9276750018 MPRP/7030 ICP/6479SS-109C EPA 3050 EPA 60109276750019 MPRP/7030 ICP/6479SS-109D EPA 3050 EPA 60109276750020 MPRP/7030 ICP/6479SS-109E EPA 3050 EPA 60109276750021 MPRP/7030 ICP/6479SS-104A EPA 3050 EPA 60109276750022 MPRP/7030 ICP/6479SS-104B EPA 3050 EPA 60109276750023 MPRP/7030 ICP/6479SS-104C EPA 3050 EPA 60109276750024 MPRP/7030 ICP/6479SS-104D EPA 3050 EPA 60109276750025 MPRP/7030 ICP/6479SS-104E EPA 3050 EPA 60109276750026 MPRP/7030 ICP/6479SS-101A EPA 3050 EPA 60109276750027 MPRP/7030 ICP/6479SS-101B EPA 3050 EPA 60109276750028 MPRP/7030 ICP/6479SS-101C EPA 3050 EPA 60109276750029 MPRP/7030 ICP/6479SS-101D EPA 3050 EPA 60109276750030 MPRP/7030 ICP/6479FD-06 EPA 3050 EPA 60109276750037 MPRP/7030 ICP/6479FD-13 EPA 3050 EPA 6010

9276750040 MPRP/6996 ICP/6451MB-01 SM 3030C EPA 60109276750041 MPRP/6996 ICP/6451EB-01 SM 3030C EPA 6010

9276750040 MERP/3001 MERC/2959MB-01 EPA 7470 EPA 7470

9276750041 MERP/2998 MERC/2956EB-01 EPA 7470 EPA 7470

9276750001 MERP/2995 MERC/2954SS-113A EPA 7471 EPA 74719276750002 MERP/2995 MERC/2954SS-113B EPA 7471 EPA 74719276750003 MERP/2995 MERC/2954SS-116A EPA 7471 EPA 74719276750004 MERP/2995 MERC/2954SS-116B EPA 7471 EPA 74719276750005 MERP/2995 MERC/2954SS-122 EPA 7471 EPA 7471

9276750006 MERP/2996 MERC/2955SS-125 EPA 7471 EPA 74719276750007 MERP/2996 MERC/2955SS-126 EPA 7471 EPA 7471

9276750009 MERP/2995 MERC/2954FD-02 EPA 7471 EPA 74719276750013 MERP/2995 MERC/2954SS-127 EPA 7471 EPA 74719276750014 MERP/2995 MERC/2954SS-128 EPA 7471 EPA 74719276750015 MERP/2995 MERC/2954SS-129 EPA 7471 EPA 74719276750016 MERP/2995 MERC/2954SS-109A EPA 7471 EPA 7471

9276750017 MERP/2996 MERC/2955SS-109B EPA 7471 EPA 74719276750018 MERP/2996 MERC/2955SS-109C EPA 7471 EPA 7471



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9276750019 MERP/2996 MERC/2955SS-109D EPA 7471 EPA 74719276750020 MERP/2996 MERC/2955SS-109E EPA 7471 EPA 7471

9276750021 MERP/3004 MERC/2962SS-104A EPA 7471 EPA 7471

9276750022 MERP/2996 MERC/2955SS-104B EPA 7471 EPA 74719276750023 MERP/2996 MERC/2955SS-104C EPA 7471 EPA 74719276750024 MERP/2996 MERC/2955SS-104D EPA 7471 EPA 74719276750025 MERP/2996 MERC/2955SS-104E EPA 7471 EPA 7471

9276750026 MERP/3004 MERC/2962SS-101A EPA 7471 EPA 7471

9276750027 MERP/2996 MERC/2955SS-101B EPA 7471 EPA 74719276750028 MERP/2996 MERC/2955SS-101C EPA 7471 EPA 74719276750029 MERP/2996 MERC/2955SS-101D EPA 7471 EPA 74719276750030 MERP/2996 MERC/2955FD-06 EPA 7471 EPA 74719276750037 MERP/2996 MERC/2955FD-13 EPA 7471 EPA 7471

9276750001 OEXT/11113 MSSV/3970SS-113A EPA 3546 EPA 82709276750002 OEXT/11113 MSSV/3970SS-113B EPA 3546 EPA 82709276750003 OEXT/11113 MSSV/3970SS-116A EPA 3546 EPA 82709276750004 OEXT/11113 MSSV/3970SS-116B EPA 3546 EPA 82709276750005 OEXT/11113 MSSV/3970SS-122 EPA 3546 EPA 8270

9276750006 OEXT/11121 MSSV/4031SS-125 EPA 3546 EPA 82709276750007 OEXT/11121 MSSV/4002SS-126 EPA 3546 EPA 82709276750010 OEXT/11121 MSSV/4002FD-03 EPA 3546 EPA 82709276750013 OEXT/11121 MSSV/4002SS-127 EPA 3546 EPA 82709276750014 OEXT/11121 MSSV/4002SS-128 EPA 3546 EPA 82709276750015 OEXT/11121 MSSV/4002SS-129 EPA 3546 EPA 82709276750016 OEXT/11121 MSSV/4002SS-109A EPA 3546 EPA 82709276750017 OEXT/11121 MSSV/4002SS-109B EPA 3546 EPA 82709276750018 OEXT/11121 MSSV/4031SS-109C EPA 3546 EPA 82709276750019 OEXT/11121 MSSV/4002SS-109D EPA 3546 EPA 82709276750020 OEXT/11121 MSSV/4031SS-109E EPA 3546 EPA 82709276750021 OEXT/11121 MSSV/4002SS-104A EPA 3546 EPA 82709276750022 OEXT/11121 MSSV/4031SS-104B EPA 3546 EPA 8270

9276750023 OEXT/11146 MSSV/4003SS-104C EPA 3546 EPA 82709276750024 OEXT/11146 MSSV/4031SS-104D EPA 3546 EPA 82709276750025 OEXT/11146 MSSV/4035SS-104E EPA 3546 EPA 82709276750026 OEXT/11146 MSSV/4035SS-101A EPA 3546 EPA 8270

9276750027 OEXT/11121 MSSV/4031SS-101B EPA 3546 EPA 8270

9276750028 OEXT/11146 MSSV/4003SS-101C EPA 3546 EPA 82709276750029 OEXT/11146 MSSV/4003SS-101D EPA 3546 EPA 82709276750032 OEXT/11146 MSSV/4003FD-08 EPA 3546 EPA 82709276750034 OEXT/11146 MSSV/4003FD-10 EPA 3546 EPA 8270

9276750040 OEXT/11089 MSSV/3966MB-01 EPA 3510 EPA 82709276750041 OEXT/11089 MSSV/3966EB-01 EPA 3510 EPA 8270

9276750040 MSV/12105MB-01 EPA 8260



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9276750041 MSV/12105EB-01 EPA 82609276750042 MSV/12105FB-01 EPA 82609276750044 MSV/12105TB-02 EPA 8260

9276750001 MSV/12135SS-113A EPA 82609276750002 MSV/12135SS-113B EPA 8260

9276750003 MSV/12138SS-116A EPA 82609276750004 MSV/12138SS-116B EPA 82609276750005 MSV/12138SS-122 EPA 82609276750006 MSV/12138SS-125 EPA 8260

9276750007 MSV/12135SS-126 EPA 82609276750011 MSV/12135FD-04 EPA 8260

9276750013 MSV/12138SS-127 EPA 82609276750014 MSV/12138SS-128 EPA 82609276750015 MSV/12138SS-129 EPA 82609276750016 MSV/12138SS-109A EPA 82609276750017 MSV/12138SS-109B EPA 82609276750018 MSV/12138SS-109C EPA 82609276750019 MSV/12138SS-109D EPA 82609276750020 MSV/12138SS-109E EPA 8260

9276750021 MSV/12151SS-104A EPA 82609276750022 MSV/12151SS-104B EPA 82609276750023 MSV/12151SS-104C EPA 82609276750024 MSV/12151SS-104D EPA 82609276750025 MSV/12151SS-104E EPA 82609276750026 MSV/12151SS-101A EPA 82609276750027 MSV/12151SS-101B EPA 82609276750028 MSV/12151SS-101C EPA 82609276750029 MSV/12151SS-101D EPA 8260

9276750031 MSV/12138FD-07 EPA 82609276750036 MSV/12138FD-12 EPA 8260

9276750043 MSV/12135TB-01 EPA 8260

9276750045 MSV/12151TB-03 EPA 8260

9276750001 PMST/3390SS-113A ASTM D2974-879276750002 PMST/3390SS-113B ASTM D2974-879276750003 PMST/3390SS-116A ASTM D2974-879276750004 PMST/3390SS-116B ASTM D2974-879276750005 PMST/3390SS-122 ASTM D2974-879276750006 PMST/3390SS-125 ASTM D2974-879276750007 PMST/3390SS-126 ASTM D2974-87

9276750008 PMST/3398FD-01 ASTM D2974-87

9276750009 PMST/3390FD-02 ASTM D2974-87

9276750010 PMST/3398FD-03 ASTM D2974-87



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9276750011 PMST/3390FD-04 ASTM D2974-87

9276750012 PMST/3391FD-05 ASTM D2974-879276750013 PMST/3391SS-127 ASTM D2974-879276750014 PMST/3391SS-128 ASTM D2974-879276750015 PMST/3391SS-129 ASTM D2974-879276750016 PMST/3391SS-109A ASTM D2974-879276750017 PMST/3391SS-109B ASTM D2974-879276750018 PMST/3391SS-109C ASTM D2974-879276750019 PMST/3391SS-109D ASTM D2974-879276750020 PMST/3391SS-109E ASTM D2974-879276750021 PMST/3391SS-104A ASTM D2974-879276750022 PMST/3391SS-104B ASTM D2974-879276750023 PMST/3391SS-104C ASTM D2974-879276750024 PMST/3391SS-104D ASTM D2974-879276750025 PMST/3391SS-104E ASTM D2974-879276750026 PMST/3391SS-101A ASTM D2974-879276750027 PMST/3391SS-101B ASTM D2974-879276750028 PMST/3391SS-101C ASTM D2974-879276750029 PMST/3391SS-101D ASTM D2974-879276750030 PMST/3391FD-06 ASTM D2974-879276750031 PMST/3391FD-07 ASTM D2974-87

9276750032 PMST/3398FD-08 ASTM D2974-87

9276750033 PMST/3390FD-09 ASTM D2974-879276750034 PMST/3390FD-10 ASTM D2974-87

9276750035 PMST/3392FD-11 ASTM D2974-879276750036 PMST/3392FD-12 ASTM D2974-879276750037 PMST/3392FD-13 ASTM D2974-879276750038 PMST/3392FD-14 ASTM D2974-87

9276750039 PMST/3398FD-15 ASTM D2974-87

9276750001 WETA/8109SS-113A SM 4500-CN-E9276750002 WETA/8109SS-113B SM 4500-CN-E9276750003 WETA/8109SS-116A SM 4500-CN-E9276750004 WETA/8109SS-116B SM 4500-CN-E9276750005 WETA/8109SS-122 SM 4500-CN-E9276750006 WETA/8109SS-125 SM 4500-CN-E9276750007 WETA/8109SS-126 SM 4500-CN-E9276750008 WETA/8109FD-01 SM 4500-CN-E9276750013 WETA/8109SS-127 SM 4500-CN-E

9276750014 WETA/8110SS-128 SM 4500-CN-E9276750015 WETA/8110SS-129 SM 4500-CN-E9276750016 WETA/8110SS-109A SM 4500-CN-E9276750017 WETA/8110SS-109B SM 4500-CN-E9276750018 WETA/8110SS-109C SM 4500-CN-E9276750019 WETA/8110SS-109D SM 4500-CN-E9276750020 WETA/8110SS-109E SM 4500-CN-E



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9276750MILLS GAP 6686081744


9276750021 WETA/8110SS-104A SM 4500-CN-E9276750022 WETA/8110SS-104B SM 4500-CN-E9276750023 WETA/8110SS-104C SM 4500-CN-E9276750024 WETA/8110SS-104D SM 4500-CN-E9276750025 WETA/8110SS-104E SM 4500-CN-E9276750026 WETA/8110SS-101A SM 4500-CN-E9276750027 WETA/8110SS-101B SM 4500-CN-E9276750028 WETA/8110SS-101C SM 4500-CN-E9276750029 WETA/8110SS-101D SM 4500-CN-E9276750033 WETA/8110FD-09 SM 4500-CN-E

9276750039 WETA/8135FD-15 SM 4500-CN-E

9276750040 WETA/8111MB-01 SM 4500-CN-E9276750041 WETA/8111EB-01 SM 4500-CN-E

9276750001 WETA/8087 WETA/8095SS-113A EPA 7196 EPA 71969276750002 WETA/8087 WETA/8095SS-113B EPA 7196 EPA 71969276750003 WETA/8087 WETA/8095SS-116A EPA 7196 EPA 71969276750004 WETA/8087 WETA/8095SS-116B EPA 7196 EPA 71969276750005 WETA/8087 WETA/8095SS-122 EPA 7196 EPA 7196

9276750006 WETA/8088 WETA/8102SS-125 EPA 7196 EPA 7196

9276750007 WETA/8087 WETA/8095SS-126 EPA 7196 EPA 71969276750012 WETA/8087 WETA/8095FD-05 EPA 7196 EPA 7196

9276750013 WETA/8088 WETA/8102SS-127 EPA 7196 EPA 71969276750014 WETA/8088 WETA/8102SS-128 EPA 7196 EPA 71969276750015 WETA/8088 WETA/8102SS-129 EPA 7196 EPA 71969276750016 WETA/8088 WETA/8102SS-109A EPA 7196 EPA 71969276750017 WETA/8088 WETA/8102SS-109B EPA 7196 EPA 71969276750018 WETA/8088 WETA/8102SS-109C EPA 7196 EPA 71969276750019 WETA/8088 WETA/8102SS-109D EPA 7196 EPA 71969276750020 WETA/8088 WETA/8102SS-109E EPA 7196 EPA 7196

9276750021 WETA/8098 WETA/8104SS-104A EPA 7196 EPA 7196

9276750022 WETA/8088 WETA/8102SS-104B EPA 7196 EPA 71969276750023 WETA/8088 WETA/8102SS-104C EPA 7196 EPA 71969276750024 WETA/8088 WETA/8102SS-104D EPA 7196 EPA 71969276750025 WETA/8088 WETA/8102SS-104E EPA 7196 EPA 7196

9276750026 WETA/8098 WETA/8104SS-101A EPA 7196 EPA 7196

9276750027 WETA/8088 WETA/8102SS-101B EPA 7196 EPA 71969276750028 WETA/8088 WETA/8102SS-101C EPA 7196 EPA 71969276750029 WETA/8088 WETA/8102SS-101D EPA 7196 EPA 71969276750035 WETA/8088 WETA/8102FD-11 EPA 7196 EPA 71969276750038 WETA/8088 WETA/8102FD-14 EPA 7196 EPA 7196



Date: 09/27/2010 06:23 PM Page 242 of 242



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