fecha de reporte: 2019-01-07 página: revisión:...
TRANSCRIPT
Destino Final:
Observaciones:
ZIRACUARETIRO
Aleatorio
EUA,EUROPA,JAPON
La muestra se recibió en condiciones para su análisis.
2303-01(SECTOR 01)
Estado: Michoacán Código postal: 60330
Ext. 133
60330
[email protected], [email protected],
[email protected], [email protected]
Información de Facturación
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Fruits-Giddings SA de CV
Km. 1 Carretera los Reyes- Jacona Sn
Michoacán
Razón social:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
2019-01-07 Página: 1 de 7 Revisión: AR271-TS-70
Empresa:
Correo electrónico:
Fecha de reporte:
SUN BELLE MÉXICO S.A. DE C.V.
Dirección: Km 1 Carr. los Reyes-Jacona S/N Ciudad o Localidad: Los Reyes
Solicitante: ALFREDO OSEGUERA DÍAZ
[email protected], [email protected],
Teléfono: 3545427328
Información del Cliente
Domicilio Fiscal:
Estado:
RFC: SBM040520QN6
Ciudad o Localidad: Los Reyes
Código postal:
Analisis Multiresidual de Pesticidas
Nombre común:
Libro de registro:
Rubus Ulmifoli
ene-19P-19-177No. Reg. de Muestra:
Fecha de recepción:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Nombre científico: Variedad:
Fecha de Término:Fecha de inicio: 2019-01-04
Información de la Muestra
Zarzamora
Ext. SD Correo electrónico:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Telefono: 3545420170
2019-01-07
Menos de 1.5kg
SD
Tupy|Otras
2019-01-04
Parte analizada:
Productor:
Lugar de muestreo:
Uso comercial:
Fruto
JUAN JAVIER ALVAREZ ORTEGA
Fecha de muestreo:03 DE ENERO DEL 2018 Hora:
11:00 AM
SD
SD
Estado de la muestra:
Lugar de cosecha:
Método de muestreo:
Destino Comercial:
Cantidad recibida:
Registro SAGARPA:
RFC de Bodega:
Aduana:Mercado Nacional y Extranjero
Congelado
DIRECCION: ZIRACUARETIRO,
MICHOACÁN
Humano
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace
responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
B B
B B
B B
B B
B B
B B
B BB B
B B
B BB BB BB BB B
B B
B BB BB BB BB BB BB B
B B
B BB BB BB BB B
B B
B B
B B
B B
B B
B B
B B
B BB BB B
B B
B BB B
B B
V B
B B
B B
B B
B B
B BB BB BB B
B B
B B
B B
B B
B B
B B
B B
B B
B B
OXYDEMETON
METHYL
METABOLITE
0.02
0.01 - -
0.02 0.5
- -
0.2 0.5
0.01 0.5
0.5 2
0.05 0.1
3 1
0.05 0.05
- - - -
1
- - - -
- - - -
- - - -
0.1 0.2
- - - -
0.01 1
1
0.01 0.3
0.01 1
0.05 0.1
- - - -
- - - -
0.02 - -
3 1
0.01 0.05
- - - -
- -
0.01 1
0.01 - -
0.01 - -
0.9 0.7
0.01 0.2
0.5
0.01 0.05
0.01 1
0.1 0.1
0.01 0.05
0.01 1
0.02 0.02
0.01 - -
- - - -
- -
0.01 0.05
0.05 0.05
0.01 0.1
0.01 0.05
1 1
- - - -
0.01 0.02
0.01 - -
1
0.01 0.1
0.01 - -
0.01 - -
- -
0.01 - -
0.01 0.05
20 5
0.01 0.5
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
0.01
0.01
0.01
- -
0.02
0.01
0.01
7 7
0.01 0.05
1 0.3
0.01 1
0.01 0.1
- - - -
0.01 5
0.05 - -
5 3
- - - -
0.05 0.3
0.01 0.02
0.02 - -
0.01 0.02
0.01 - -
0.5
0.01 0.01
0.08 0.05
0.01 1
2 1
0.01 0.02
0.01 - -
0.02 1
0.01 0.05
- -
0.05 0.3
Carbetamide - - 0.01
- - < LCL
Chlordane- a GC/MSMS
- - < LCL
SD
CA EU
< LCL
- - < LCL
- - < LCL
- - < LCL
0.01
0.3 0.1 0.02 < LCL
0.1 0.1 0.02 0.1 0.02 < LCL
Chlorbromuron LC/MSMS
Fecha de reporte: 2019-01-07
Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
Reg. Sagarpa:
No. Reg. Lab.:
Cantidad obtenida en mg/kg
(ppm)MX US JP CA CHN
Cantidad obtenida en mg/kg
(ppm)Analito Analito
Analizado
mediante
equipo
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
AR271-TS-70Revisión:
Cliente:
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE C.V.
JUAN JAVIER ALVAREZ ORTEGA
P-19-177 01-06-2019.D
P-19-177
US JP
1-Naphthol GC/MSMSCARBARYL
METABOLITE
CARBARYL
METABOLITE
CARBARYL
METABOLITE
Uso autorizado
LMR (ppm)
MX US JP CA CHN
CARBARYL
METABOLITECARBARYL METABOLITE < LCL Carbendazim LC/MSMS
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
EU KOR EU KOR
CARBARYL
METABOLITE
CARBARYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - - < LCL
2,3 dihydro-2,2dimethylbenzofuran 7- GC/MSMS - - - - - -
2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1 < LCL0.1 0.05
- - - -
- - - -
Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - - < LCL
3-Hydroxy carbofuran LC/MSMS - - - - - -
- - - - < LCL
3,4 Dichloroaniline GC/MSMSLINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITELINURON METABOLITE < LCL
2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -
LINURON
METABOLITE
Aclonifen GC/MSMS - - - - 0.01 0.1 - - < LCL
Acetochlor LC/MSMS - - - -
0.1 0.50 < LCL
Acetamiprid LC/MSMS 1.6 1.6 2 4 2 < LCL
Acephate LC/MSMS - - - - 0.01
Aldicarb LC/MSMS - - - -
- -- -LC/MSMSAldicarb-sulfoxide (Aldoxicarb)
0.01
0.1 - - < LCL
Alachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Acrinathrin GC/MSMS - - - - 2
0.02 0.02
0.02 0.02
0.02 0.02
Amicarbazone LC/MSMS - - - - 0.01
0.1 - - < LCL
Ametryn GC/MSMS - - - - 0.01 0.1 - - < LCL
Ametoctradin LC/MSMS - - - - 0.01 0.05
0.01 - -
0.01 - -
Atrazine-2-hydroxy LC/MSMS - - - - - - - - - - < LCL
Atrazine GC/MSMS - - - - 0.02
Aminocarb LC/MSMS - - - - - - - - - - < LCL- - - -
0.05 - -
- - - -
Azoxystrobin GC/MSMS 5 5 5 5 - - < LCL
Azinphos-Methyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Azamethiphos LC/MSMS - - - - 0.01 0.01 - -
0.02
Benfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL
Bendiocarb LC/MSMS - - - - 0.01
- - - - < LCL
Benalaxyl GC/MSMS - - - - 0.05 0.1 - - < LCL
Baycarb LC/MSMS - - - - - -
Benzoximate LC/MSMS - - - - 0.01 0.1 - - < LCL
Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Bensulide LC/MSMS - - - - 0.01 0.1 - - < LCL
Bensulfuron-methyl LC/MSMS - - - - 0.01
0.01 0.1
0.01
BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL
BHC lindane delta GC/MSMS 0.5 0.5 0.3
< LCL
BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL
BHC lindane alpha GC/MSMS 0.5 0.5 0.3
0.01 0.01
0.01 0.01
0.01
Bifenthrin GC/MSMS 1 1 1
Bifenox GC/MSMS - - - - 0.01 0.1 - - < LCL
Bifenazate LC/MSMS 5 5 7
Boscalid LC/MSMS 10 10 10 6 - - < LCL
Bolstar GC/MSMS - - - - - -
Bitertanol LC/MSMS - - - - 0.05 0.1 - - < LCL
- - - -
10 9
0.1 - -
0.1
Carboxin LC/MSMS - - - -
GC/MSMS - - - - 0.01
- - < LCL
0.1 - - < LCL
0.1 - - < LCL
2 1 < LCL
0.1 - - < LCL
0.1 - - < LCL
- -
LINURON METABOLITE
- - - -
0.1 - - < LCL
- - - - < LCL
1 1 0.011
5 7 < LCL
0.1
0.1
Carbofuran GC/MSMS - - - -
0.1
- - < LCL
- - - - < LCL
Chlorpyrifos GC/MSMS - - - - 1 0.1
LC/MSMS - -
- - - - - -
0.1 - - < LCL
Chlorantraniliprole LC/MSMS 1.8 1.8 2 0.9 1 < LCL
Chinometionate GC/MSMS - - - - 0.01
- -
- - 0.01 0.1 - - < LCL
Chloroxuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Chloropropylate GC/MSMS - - - - - - - - - - < LCL
Chloroneb GC/MSMS
< LCL- -0.1 0.01 - -
0.01 - -
0.01 0.05
Chlortal dimethyl GC/MSMS - - - - - - - - - - < LCL
0.1 - - < LCL
Clomazone LC/MSMS - - - - 0.02 0.1 - - < LCL
Clofentezine LC/MSMS - - - - 0.01
- - - - < LCL
Clodinafop-propargyl LC/MSMS - - - - 0.02 0.1 - - < LCL
Chlorthiophos GC/MSMS - - - - - -
0.1 0.05 < LCL
Crimidine LC/MSMS - - - - - - - - - - < LCL
Coumaphos GC/MSMS - - - - - -
0.1 - - < LCL
Clothianidin LC/MSMS - - - - 0.2 0.1 - - < LCL
Cloquintocet-mexyl LC/MSMS - - - - 0.01
0.02 - - < LCL
Cycloate LC/MSMS - - - - 0.01 0.1 - - < LCL
Cyazofamid LC/MSMS - - - - 0.01
0.1 - - < LCL
Cyantraniliprole LC/MSMS 4 4 0.01 0.1 - - < LCL
Cyanazine LC/MSMS - - - - 0.01
0.1 - - < LCL
Cyhalothrin (Isomero Lambda
y gamma)**GC/MSMS - - - - 0.5 0.01 0.2 < LCL
Cyfluthrin GC/MSMS - - - - 0.02
0.1 - - < LCL
Cyflumetofen LC/MSMS - - - - 0.01 0.1 - - < LCL
Cyflufenamid GC/MSMS - - - - 0.01
10 10 10 - - < LCL
Cyproconazole LC/MSMS - - - - 0.5
4 - - < LCL
Cypermethrin a (Zeta-
Cypermethrin)**GC/MSMS 0.8 0.8 0.5 0.1 - - < LCL
Cymoxanil LC/MSMS 4 4
0.1 - - < LCL
Cyprodinil
- - - - < LCLDDD-p,p GC/MSMS - - - - - -
0.1 - - < LCL
DDD-o,p GC/MSMS - - - - - - - - - - < LCL
Cyromazine LC/MSMS - - - - 0.01
- - - -
- - < LCL
Bupirimate LC/MSMS - - - - 0.01 0.1 - - < LCL DDE-o,p GC/MSMS - - - - - - - - - - < LCL
Buprofezin GC/MSMS - - - - 0.01 0.1 - - - - - -
- - - -1.5 - -
0.05
- - < LCL
Butocarboxim* LC/MSMS - - - - 0.01 0.1 - - < LCL DDT-p,p GC/MSMS - - - - - - - - - - < LCL
Butachlor GC/MSMS - - - - 0.01 0.1 - - < LCL
- - < LCL
Buturon LC/MSMS - - - - - - - - - - < LCL Deltamethrin GC/MSMS - - - - 0.1 0.1 - - < LCL
Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - < LCLDEET (Diethyl-m-toluamide,
N,N-)
- -
- - < LCL
Cadusafos GC/MSMS - - - - 0.01 0.1 0.02 < LCL Demeton S GC/MSMS - - - - 0.4 0.1 0.02 < LCL
Butylate GC/MSMS - - - - 0.01 0.1 - - < LCL Demeton O
0.01 0.1
Bromacil
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE< LCL
Carbaryl GC/MSMS 12 12 10 10 - - < LCL Desmedipham LC/MSMS - - - - 0.01 0.1 - - < LCL
Captan GC/MSMS 25 25 0.01 0.1 - - < LCL Demeton-s-methyl-sulfone
Bromuconazole* LC/MSMS - - - - 0.01 0.1 - - < LCL
Bromopropylate GC/MSMS - - - - 2
Bromophos methyl GC/MSMS - - - - - -
0.1 - - < LCL
- - - - < LCL
0.1
- -0.01 0.01
OXYDEMETON
METHYL
METABOLITE
GC/MSMS - -
GC/MSMS - -
GC/MSMS - -
< LCL DDE-p,p GC/MSMS - -
GC/MSMS 10
LC/MSMS
- - - - - -
DDT-o,p
- - - - - -
- - - - - -
- - - - - -
4
0.05
0.01
< LCL0.05
< LCL0.020.1
0.1 - - < LCL
Chlorobenzilate GC/MSMS - - - - 0.01
0.01
0.01
GC/MSMSAldrin
Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1
0.01
0.1 0.02 < LCL
Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 Chlormequat LC/MSMS - - - - 0.05
Chlorimuron-ethyl LC/MSMS - - - - 0.01
Chloridazon (Pyrazon) LC/MSMS - - - - 0.01
< LCL
0.050.05
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
Chlorfluazuron LC/MSMS - - - - 2 0.1 - - < LCL
Chlorfenvinphos LC/MSMS - - - - 0.05
0.02 < LCL
- -0.1
GC/MSMS - -
Página:
Muestra:
Huerto:
Cromatograma LC:
2 de 7
Zarzamora
ZIRACUARETIRO
P-19-177 01-04-2019.d
10- -- -GC/MSMSChlorothalonil
0.1 0.01 < LCL
Chlorfenapyr GC/MSMS - - - - 0.01 0.1 - - < LCL
Chlordimeform GC/MSMS - - - - 0.01
KOR CHN
Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - - < LCL
Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL
MX
0.01- -- -LC/MSMSChlorotoluron
- -0.1
- - < LCL
0.1 - - < LCL
Chlorpropham
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto.
Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
B BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B B
B B
B B
B BB B
B B
B BB B
B B
B B
B B
B B
B B
B BB B
0.05
1
0.01 - -
0.01 - -
0.01 - -
0.01 - -
- -
0.01 0.5
3
0.01 0.05
0.01 0.5
5
0.01 5
- -
1.5Imidacloprid
Imazaquin
LC/MSMS - - - - 0.01 0.1
- -
0.01 - -
0.03 0.5
0.01
5
0.05 0.05
3
0.05
0.01 0.02
0.01 0.05
0.01 0.01
0.01 0.01
0.01 - -
0.01 - -
0.01 0.3
0.01 0.5
- - - -
0.02 0.05
0.01
- -
0.01 - -
0.7 0.7
- - - -
0.01 0.02
0.01 0.2
- - - -
0.005 0.05
0.01 - -
0.05
5
0.05
0.01 5
- - - -
0.01
0.01
0.01
5
0.3
0.01 - -
0.01 - -
3 0.7
3 6
- -
0.05 5
0.01 0.1
- - - -
- - - -
0.01 1
0.01
0.01 5
0.01
0.01
0.050.01
0.01
- -
0.05
0.01
0.01
0.01
0.5
0.05
0.01
0.03
- -
0.01 - -
- -
0.01 0.05
0.02 0.02
- - - -
0.01 0.01
1 1
0.01
0.05 0.05
0.05 0.05
0.05 0.05
0.01 0.01
0.05 0.5
0.01 - -
0.02 - -
- - - -
0.01 0.05
0.01
0.01 2
1.5 0.5
- - - -
0.01 - -
- - - -
- - - -
0.01 0.2
0.01 0.03
0.01 - -
0.01 0.01
0.01 1
0.05 1
- - - -
0.01 1
0.01 2
0.01
EU KOR
- - - -
- - - -
0.01 0.1
0.01 15
- - - -
0.01 0.05- - - -
- -
- -
15
0.3
0.05
0.50.5
CHN MX US JP CA
0.01
- -
15
Revisión: AR271-TS-70
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm) Cantidad obtenida en
mg/kg (ppm)Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
Reg. Sagarpa: SD
No. Reg. Lab.:
CHN
Fecha de reporte:
Cantidad obtenida en
mg/kg (ppm)MX US JP CA
Cliente: P-19-177
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE
C.V.
JUAN JAVIER ALVAREZ
ORTEGA
EU
< LCL
Dialifos LC/MSMS - - - - - - - - - - < LCL Fenfuram
GC/MSMS - - - - 0.01 0.1 - -Desmetryn GC/MSMS - - - - - - - - - - < LCL Fenchlorphos
< LCL
Dichlofluanid GC/MSMS - - - - 10 0.1 - - < LCL Fenitrothion
LC/MSMS 20 20 15 20 15
< LCL
Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1 < LCL Fenhexamid
LC/MSMS - - - - - - - - - -
< LCL
Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2 < LCL Fenoxycarb
LC/MSMS - - - - 0.1 0.1 - -
< LCL
Dichloran GC/MSMS - - - - - - - - - - < LCL Fenoxaprop-ethyl
GC/MSMS - - - - 0.8 0.1 0.5
< LCL
Diclofop methyl GC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropidin
GC/MSMS 12 12 5 12 5< LCL
Diclobutrazol* LC/MSMS - - - - - - - - - - < LCL Fenpropathrin
LC/MSMS - - - - 0.05 0.1 - -
< LCL
Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02 < LCL Fenpyroximate
LC/MSMS - - - - 0.05 0.1 - -
< LCL
Dicrotophos LC/MSMS - - - - 0.01 0.1 - - < LCL Fenpropimorph
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Difenoconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fensulfothion
GC/MSMS - - - - - - - - - -
< LCL
Diethofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fenson
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Diflufenican LC/MSMS - - - - 0.01 0.1 - - < LCL Fenuron
GC/MSMS - - - - 0.01 0.1 0.05
< LCL
Difenoxuron LC/MSMS - - - - - - - - - - < LCL Fenthion
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Dimepax GC/MSMS - - - - - - - - - - < LCL Flamprop methyl
GC/MSMS - - - - 0.01 0.1 0.02
< LCL
Dimefuron LC/MSMS - - - - - - - - - - < LCL Fipronil
LC/MSMS - - - - - - - - - -
< LCL
Dimethenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flazasulfuron
LC/MSMS - - - - - - - - - -
< LCLLC/MSMS - - - - 0.01 0.1 - -
Flamprop-isopropyl< LCL- -0.10.01- -- -LC/MSMSDimethachlor
< LCL
Dimethomorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluazifop-butyl
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Dimethoate GC/MSMS - - - - 1 0.1 - - < LCL Flonicamid
LC/MSMS - - - - 0.1 0.1 - -
< LCL
Dimethylphenol, 2,4- (2,4-xylenol) GC/MSMS - - - - - - - - - - < LCL Flubendiamide
LC/MSMS - - - - 0.01 0.1 - -
- -0.10.01- -- -LC/MSMS < LCL
0.2
1
< LCL
Dinotefuran LC/MSMS - - - - 0.01 0.1 - - < LCL Flucythrinate
GC/MSMS - - - - 0.01 0.1 - -< LCL Fluchloralin - -
0.05
Diniconazole - - 0.01 0.1 - -
< LCL
Diphenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenacet
GC/MSMS 5 5 5 7 - -
< LCL
Dioxathion GC/MSMS - - - - 0.01 0.1 - - < LCL Fludioxonil
GC/MSMS - - - - 0.05 0.1 - -
< LCL
Disulfoton GC/MSMS - - - - 0.05 0.1 - - < LCL Flumiclorac-pentyl
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Diphenylamine GC/MSMS - - - - 0.05 0.1 - - < LCL Flufenoxuron
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Disulfoton sulfoxide GC/MSMS - - - - - - - - - - < LCL Fluopicolide
LC/MSMS - - - - 0.02 0.1 - -
< LCL
Disulfoton sulfone GC/MSMS - - - - - - - - - - < LCL Fluometuron
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Dodemorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoroglycofen-ethyl
GC/MSMS 5 5 5 5 - -
< LCL
Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL Fluopyram
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Edifenphos LC/MSMS - - - - 0.01 0.1 - - < LCL Fluridone
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Dyfonate GC/MSMS - - - - 0.01 0.1 0.01 < LCL Fluoxastrobin
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flusilazole
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - - < LCL Flurtamone
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - - < LCL Flutriafol
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Flutolanil
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Epoxiconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluxapyroxad
GC/MSMS - - - - - - - - - -
< LCL
Endrin GC/MSMS - - - - 0.01 0.1 0.05 < LCL Fluvalinate
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2 < LCL Forchlorfenuron
GC/MSMS - - - - 0.01 25 - -
< LCL
EPTC GC/MSMS - - - - 0.1 0.1 - - < LCL Folpet
LC/MSMS 5 5 5 5 - -
< LCL
Ethalfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL Fosthiazate
LC/MSMS - - - - - - - - - -
< LCL
Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - - < LCL Formetanate
LC/MSMS - - - - 0.1 0.1 - -
< LCL
Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - - < LCL Furathiocarb
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Ethiofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Fuberidazole
LC/MSMS - - - - 0.05 0.1 - -
< LCL
Ethoprop GC/MSMS - - - - 0.01 0.1 0.02 < LCL Haloxyfop-methyl
GC/MSMS 0.1 0.1 0.02 0.1 0.02
< LCL
Ethirimol LC/MSMS - - - - - - - - - - < LCL g Chlordan
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Etion GC/MSMS - - - - 0.3 0.1 - - < LCL Heptachlor exo-epoxide (isomer
GC/MSMS 0.05 0.05 0.01 0.1 0.01
< LCL
Ethylan GC/MSMS - - - - - - - - - - < LCL Heptachlor
LC/MSMS - - - - 0.05 0.1 - -
- -
< LCL
Etofenprox GC/MSMS 5 5 0.01 0.1 - - < LCL Heptenophos
GC/MSMS 0.05 0.05 0.01 0.1 0.01
Famoxadone LC/MSMS 10 10 10 10 - - < LCL Hexaconazole
Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - - < LCL Hexachlorobenzene0.3
0.01 2
- - 0.01 0.1LC/MSMS
Fenamidone GC/MSMS - - - - 0.01 0.1 - - < LCL Hexaflumuron - - 0.01 0.10.01 0.7
- - - - < LCL Hexythiazox
GC/MSMS - - - - 0.1 - -
Fenbuconazol LC/MSMS - -
Fenamiphos Sulfoxide
Fenazaquin LC/MSMS - - - - 0.01 0.1 - - < LCL
- -
- - - -
- - - -
0.02 0.2
0.01 1.5 - -
< LCL
0.05
- - 0.02 0.1
0.01 0.5
< LCL Imazapyr
GC/MSMS - - - - 0.1 0.1 - -
< LCL
Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - - < LCL Imidan
LC/MSMS 2.5 2.5 4 2.5 - -0.05 0.5
5 2 < LCL
- - 0.01 0.1 - -
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LC/MSMS - -LC/MSMS - - - - - - - - - - < LCL Imazalil
LC/MSMS 1
2019-01-07
LC/MSMS - -
LC/MSMS - -
KOR
0.05 0.1
0.01 - -
0.01
CHNKOR
< LCLLC/MSMS - - - - 0.05 0.1 - -
< LCL
- - 0.02 0.1 - -2
0.05
1
US JP CA EUMX
< LCL
LC/MSMS - - - - 0.01 0.1 - -
< LCL- -
< LCL
< LCL
< LCLGC/MSMS 0.05 0.05 0.01 0.1 - -
< LCL
< LCL
Fenarimol LC/MSMS - - - - 1 0.1 - - - -
0.02 < LCL HexazinoneFenamiphos LC/MSMS - - 0.02 0.1
Fenamiphos Sulfone LC/MSMS - - - - - -
0.01
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del
resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
B BB BB BB BB BB BB BB BB B
B B
B B
B B
B BB BB BB BB BB B
B B
B B
B B
B B
B B
B B
B B
V B
B B
B B
B BB B
B B
B R
B B
B BB BB BB BB BB BB BB BB B
B B
B
B
B
B
B
BBBBBBBBBB
B
B
- - - -
0.02 - -
- - - -
0.01 0.1
0.01 0.02
0.01 1
0.01 - -
0.05 3
0.01 2
0.01 2
- - - -
- - - -
- - - -
0.01 0.05
0.01 0.05
0.01 5
0.01 0.2
0.01 0.05
0.01 - -
0.01 2
- - - -
- - 0.2
0.2
0.1 0.2
0.05 2
0.05 0.05
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
- - - -
0.02 0.010.01 - -
0.01 0.5
- - - -
0.1 0.05
- - - -
0.01 0.3
0.01 0.2
0.01 - -
0.01 0.1
- - - -
0.01 2
0.01 3
- - - -
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
0.02 1
- - - -
0.05 0.05
0.01 1
0.01 0.5
- - - -
- - - -
0.01 - -
0.01 0.05
0.01 0.2
0.01 - -
0.01 - -
1 1
- -
0.01 0.2
0.05 0.1
0.01 0.05
0.01 - -
- - - -
0.01 5
0.1 0.05
0.01 0.1
- - - -
0.01 0.01
0.01 - -
0.01 0.02
0.01 0.3
0.01 0.05
0.01 - -
0.02 0.02
0.02 1
< LCL
Metrafenone LC/MSMS - - - - 0.01 0.1 - - < LCL
Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL
< LCL
Metosulam
Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL
Pirimicarb LC/MSMS - - - - 0.5
- - - - 0.01 0.1 - - < LCL
Phoxim LC/MSMS - - - - 0.02 0.1 0.05 < LCL
LC/MSMS
LC/MSMS - - - - 0.01 0.1 - -
Picoxystrobin
LC/MSMS
< LCL
Picolinafen
Piperalin LC/MSMS
- - - - 0.01 0.1 - -
Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL
op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL
Ovex GC/MSMS - - - - - - - - - - < LCL
Oxadiazon GC/MSMS - - - - 0.01 0.1
Oxadixyl LC/MSMS
Fecha de reporte: 2019-01-07 Revisión: AR271-TS-70
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Reg. Sagarpa: SD
No. Reg. Lab.:Cliente:
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE C.V.
JUAN JAVIER ALVAREZ ORTEGA
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Se han detectado residuos de pesticidas prohibidos
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm) Cantidad obtenida en
mg/kg (ppm)Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
CHN
Cantidad obtenida
en mg/kg (ppm)MX US JP CA CHN MX US JP CAEU KOR EU KOR
Imiprothrin GC/MSMS - - - - - - - - - - < LCL Neburon
Iprodione GC/MSMS 25 25 12 25 - - < LCL Nitrapyrin
Indoxacarb GC/MSMS - - - -
- - - -
0.5 0.5
30 30
< LCL
- -
LC/MSMS - - - - 0.01 0.10.01 0.1 - - < LCL Nicosulfuron
LC/MSMS - - - - - -
0.01 0.1GC/MSMS - - - -
0.01 1
0.1
GC/MSMS - - - - 0.01 0.1
GC/MSMS - - - - - - - -
GC/MSMS
LC/MSMS - - - -
Isazophos LC/MSMS - - - - 0.01 0.1 0.01 < LCL
Isofenphos LC/MSMS
< LCL
Norflurazon-Desmethyl
O Phenylphenol
Nitrothal-isopropyl
Irgarol LC/MSMS
- -
- - - - - - - - - - < LCL Norflurazon
Iprovalicarb LC/MSMS - - - - 0.01 0.1
< LCLNovaluron*
- - - - 0.01 0.1
Isocarbophos GC/MSMS - - - - 0.01 0.1 0.05
- - - - 0.01 0.1 0.01
LC/MSMS
Isoprothiolane GC/MSMS - - - - 0.01 0.1 - - < LCL
< LCL< LCL
Isoprocarb LC/MSMS - - - - 0.01 0.1 - - < LCL Ofurace LC/MSMS - - - - - - - - - - < LCL
Omethoate LC/MSMSDIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
Kelthane*** GC/MSMS - - - - 3 3 - - < LCL
Isoxaflutole LC/MSMS - - - - 0.01 0.1 - - < LCL
Isoproturon LC/MSMS - - - - 0.01 0.1 - - < LCL
Leptophos GC/MSMS - - - - - - - - - - < LCL
Lenacil LC/MSMS - - - - 0.3 0.1 - - < LCL
Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 2
0.1 - -
- - - -
Malaoxon LC/MSMSMALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE< LCL
Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Linuron LC/MSMS - - - - 0.2 0.1 - - < LCL0.05 0.05
0.01 0.3
MALATHION
METABOLITE
MALATHION
METABOLITE
Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL
Mancozeb LC/MSMS - - - - 5 0.1 5 < LCL
Malathion GC/MSMS 8 8 8 8 - - < LCL0.02 0.5
0.05 5
0.01 0.1
Mepanipyrim LC/MSMS - - - - 0.01 0.1 - - < LCL
Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL
Mebendazole LC/MSMS - - - - - - - - - - < LCL- - - -
0.01 0.05
4 3
Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Metamitron LC/MSMS - - - - 0.01 0.1 - - < LCL
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2 0.1 - - 0.6750.02 - -
0.1 - -
0.02 - -
Methamidophos LC/MSMS - - - - 0.01 0.1 0.05 < LCL
Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCLMetconazole LC/MSMS - - - - 0.01 0.1 - - < LCL0.02 0.4
0.01 0.05
0.01 0.1
Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL
Methiocarb GC/MSMS - - - - 0.05 0.1 - - < LCL
Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL0.02 0.01
0.2 0.05
0.2 0.05
Methoprene GC/MSMS - - - - 0.01 0.1 - - < LCL
Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL
Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1 - - < LCL0.2 0.05
0.01 1
0.02 0.2
Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL
Methoxychlor GC/MSMS - - - - 7 0.1 - - < LCL
Methoprotryne LC/MSMS - - - - - - - - - - < LCL- - - -
0.01 14
0.01 1
GC/MSMS - - - - 0.01 0.1 - - < LCL
Methylpentachlophenyl Sulfide GC/MSMS - - - - - - - - - - < LCL
Metolachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL
- -
< LCL
Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL
Metoxuron LC/MSMS - - - - - - - - - -
Mexacarbate LC/MSMS - - - - - - - - - -
Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Metribuzin
Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL
Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL
MGK-264 GC/MSMS - - - - - - - - - - < LCL
- - - - 0.01 0.1 - - < LCL
Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Monocrotophos LC/MSMS - - - - 0.01 0.1 0.03 < LCL
Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL Propamocarb LC/MSMS - - - - 0.01 0.1 - - < LCL
- - - - 1 0.1 - - < LCL
N-2,4-Dimethylphenyl formamide
(2,4-DMPF)LC/MSMS - - - - - - - - - - < LCL
Myclobutanil GC/MSMS 2 2 1 2 - - < LCL
Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1
Monuron LC/MSMS
Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL
Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Oxamyl Oxime LC/MSMS - - - - - - - - - - < LCL
0.01 0.5
- - - -
0.01 - -
0.05 0.05
- -
< LCL
- -
- -
- -
< LCL
< LCL
Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL
Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL
Paraoxon LC/MSMS - - - - - - - - - - < LCL
- -
0.01 0.1 - - < LCL
- - < LCL
0.01 0.1 - -
0.1 0.1 0.1
< LCL
< LCL
- -
- -
< LCL- -
< LCL
- - < LCL
DIMETHOATE
METABOLITE< LCL
0.5 0.05
- - - -
- - - -
0.05 0.3
0.01
0.01 0.1 - -
- -
Resultados de análisis
Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL
< LCL
Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL
Penconazol LC/MSMS - - - - 0.2 0.1
Pencycuron LC/MSMS - - - -
- - 0.05 0.024 0.01
Permethrin
Phenmedipham
Phenthoate
Phenyl valerate
Pendimethalin LC/MSMS 0.1 0.1 0.05 0.1 - -
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
- - - - - - - - - -
- - - - 0.02 0.1 - -- - - -
Phorate
Phorate-sulfone
Phorate-sulfoxide
Phosalone
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
Pentachloroaniline
Pentachloroanisol
Pentachloronitrobenzene
Pentachlorophenol
Penthiopyrad
- - - - 0.05 0.024 0.01
- - - - 1 0.1 1
- - - - 0.01 0.1 - -
- - 0.01 0.1 - -
0.1 - -
0.05 5
0.01 - -
0.01 0.5
0.01 0.05
- - - - 0.01 0.1 - -
< LCL
< LCL
< LCL< LCL
< LCL
0.179
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
- - - - 0.05 0.024 0.01
- -
- - - - 0.01
- - - - - - - - - -
- - - - - - - - - - < LCL
Piperonyl Butoxide LC/MSMS 8 8 8 8 - - < LCL
0.01 0.05
4 1
Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL
0.1 1 < LCL
Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL
Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL
Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL
< LCL
Profluoralin GC/MSMS - - - - - - - - - - < LCL
Promecarb GC/MSMS - - - - - - - - - - < LCL
0.01 0.05
KOR
Pronamide LC/MSMS - - - - - - - - - - < LCL
Propachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Prometon GC/MSMS - - - - - - - - - - < LCL
Prometryn GC/MSMS - - - - 0.01 0.1 - -
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad
del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
B BB BB BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB B
B B
B B
B B
B B
B BB B
B B
B B
B B
B B
B B
B
B
B VB VB VB VB VB VB VB VB V
B V
B
B
B
B
B
BBB
B
B
B
B
B
BBBB0.01 0.05 - - < LCLThifensulfuron-methyl LC/MSMS - - - - 0.01 0.1
- - < LCLThidiazuron LC/MSMS - - - - 0.01 0.1 0.01 0.2
0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5
1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7
0.01 3 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1
- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 - -
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE < LCLTetrahydrophthalimide, cis-1,2,3,6-
(THPI)GC/MSMS
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE
- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 1
0.01 - - - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1
- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -
0.01 0.05 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1
- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -
0.05 0.1 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1
- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -
0.01 0.1 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1
- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2
0.01 1 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1
- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 - -
0.01 - - - - < LCLTebutam LC/MSMS - - - - 0.01 0.1
- - < LCLTebufenpyrad GC/MSMS - - - - 2 0.1 0.05 0.5
0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1
- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5
0.02 0.1 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1
- - < LCLSulfoxaflor LC/MSMS - - - - 0.01 0.1 0.01 0.5
0.01 - - 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1
- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -
0.01 0.05 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15
- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 3
0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2
5 0.1 0.01 5 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -
- - < LCL
Spiromesifen LC/MSMS - - - - 0.01 0.1 0.02 2
- - - - 0.01 0.1 0.01 0.050.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1
0.01 0.1 0.01 - - - - < LCL1 < LCL Uniconazole GC/MSMS - - - -
- - < LCL
Spinosad A LC/MSMS 1 1 1 0.5 1.5 1
- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5
0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -
- - < LCL
S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.1
- - - - 0.01 0.1 0.01 - -0.01 0.05 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1
0.05 0.1 0.01 0.05 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -
- - < LCL
Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.25
- - - - 0.02 0.1 0.01 0.50.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5
0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -
- - < LCL
Sebuthylazine GC/MSMS - - - - - - - - - - - -
- - - - 0.01 0.1 3 10.01 - - - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1
- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -
- - < LCL
Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 - -
- - - - 0.01 0.1 0.01 0.20.05 0.05 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1
- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -
- - < LCL
Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 2
- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1
0.5 0.1 0.01 0.05 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -
- - < LCL
Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 1
- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15
0.01 0.1 0.01 - - - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -
- - < LCL
Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.2
- - - - 0.01 0.1 0.01 0.050.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1
0.01 0.1 0.05 - - - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -
- - < LCL
Pyridaben LC/MSMS - - - - 0.01 0.1 0.5 1
- - - - - - - - - - - -0.01 1 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1
0.5 0.1 0.01 0.5 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -
- - < LCL
Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3
- - - - 0.1 0.1 0.01 0.053 0.5 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1
5 0.1 0.02 2 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -
- - < LCL
Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -
- - - - - - - - - - - -0.01 0.08 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1
- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -
- - < LCL
Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.05
- - - - 3 6 0.1 20.05 0.05 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1
- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -
< LCL
- - < LCL
Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.3
- - - - - - - - - - - -0.01 - - - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1
0.05
1 0.1 0.01 1 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -
- - < LCL
Propazin GC/MSMS - - - - 0.01 0.1 0.01 - -
- - - - 3 0.1 0.01 10.01 7 - -
Cantidad obtenida en
mg/kg (ppm)Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm) Cantidad obtenida
en mg/kg (ppm)
Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1
0.01 0.1 0.01 0.05 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -Propanil LC/MSMS - - - - 0.1 0.1 0.01
KOR CHN
Productor: JUAN JAVIER ALVAREZ ORTEGA Huerto: ZIRACUARETIRO Reg. Sagarpa: SD
Cliente: SUN BELLE MÉXICO S.A. DE C.V. Muestra: Zarzamora No. Reg. Lab.: P-19-177
CHN MX US JP CA EUMX US JP CA EU KOR
Resultados de análisisSe han detectado residuos de pesticidas prohibidos
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
Fecha de reporte: 2019-01-07 Página: 5 de 7 Revisión: AR271-TS-70
JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Cromatograma GC: P-19-177 01-06-2019.D Cromatograma LC: P-19-177 01-04-2019.d MX US
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del
resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
0.005
0.010
Vamidothion
Vinclozolin
Heptachlor exo-epoxide (isomer B) 0.020
Heptenophos 0.005
Fuberidazole 0.005
Furathiocarb 0.005
g Chlordan 0.010
Haloxyfop-methyl 0.005
Heptachlor 0.010
Fluxapyroxad 0.005
Folpet 0.010
Forchlorfenuron 0.005
Formetanate 0.005
Fosthiazate 0.005
Flurtamone 0.005
Flusilazole 0.005
Flutolanil 0.010
Flutriafol 0.005
Fluvalinate 0.010
Fluopicolide 0.005
Fluopyram 0.010
Fluoroglycofen-ethyl 0.005
Fluoxastrobin 0.005
Fluridone 0.010
Fludioxonil 0.010
Flufenacet 0.005
Flufenoxuron 0.005
Flumiclorac-pentyl 0.010
Fluometuron 0.005
Flonicamid 0.010
Fluazifop-butyl 0.005
Flubendiamide 0.010
Fluchloralin 0.010
Flucythrinate 0.010
Fenuron 0.005
Fipronil 0.020
Flamprop methyl 0.010
Flamprop-isopropyl 0.010
Flazasulfuron 0.005
Fenpropimorph 0.005
Fenpyroximate 0.005
Fenson 0.020
Fensulfothion 0.010
Fenthion 0.010
Analito LCL (ppm)
Fenoxaprop-ethyl 0.005
Fenoxycarb 0.005
Fenpropathrin 0.010
Fenpropidin 0.005
Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005
Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005
Metconazole 0.005 Pentachloroanisol 0.010 S-Metolachlor 0.005
Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005 Trifluralin 0.010
Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005
Mecarbam 0.005 Parathion methyl 0.010 Rotenone 0.005
Uniconazole 0.010
Triflusulfuron-methyl 0.005
Triforine 0.010
Trimidal 0.005
Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010
Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020
Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005
Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005
Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005
Analito LCL (ppm)
Dimethylphenol, 2,4- (2,4-xylenol) 0.010
2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Diniconazole 0.005
2,3 dihydro-2,2dimethylbenzofuran
7-ol0.020
Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005
Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005
Piperalin 0.005 Tebuthiuron 0.005
Metolcarb 0.010 Picoxystrobin 0.005 Tebutam 0.005
Metolachlor 0.005 Picolinafen 0.005 Tebufenpyrad 0.010
Metobromuron 0.010 Phoxim 0.010 Tebufenozide 0.005
Fecha de reporte: 2019-01-07 Página: 6 de 7 Revisión:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
AR271-TS-70
Analito LCL (ppm)
Dimethoate 0.010
2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethomorph 0.005
1-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005
Lowest Calibration Level (Nivel Mínimo de Calibración) por analitoAnalito LCL (ppm) Analito LCL (ppm)
Bromopropylate 0.010 Crimidine 0.005
Dinotefuran 0.005
3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dioxathion 0.0102,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005
Diphenamid 0.005
Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenylamine 0.0103-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005
Disulfoton 0.010
Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton sulfone 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005
Disulfoton sulfoxide 0.010
Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Diuron (Karmex) 0.005
Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y
gamma)**0.010
Dodemorph 0.005
Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dyfonate 0.010
Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-
Cypermethrin)**0.010
Edifenphos 0.005
Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Emamectin Benzoate 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010
Endosulfan I (alpha isomer) 0.010
Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan II (beta isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010
Endosulfan sulfato 0.010
Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endrin 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010
Epoxiconazole 0.005
Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 EPTC 0.010Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010
Esfenvalerate + Fenvalerate (**) 0.010
Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Etaconazole (Etaconazole I y II) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010
Ethalfluralin 0.010
Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethiofencarb 0.005Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010
Ethiofencarb-sulfone 0.005
Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethirimol 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005
Ethoprop 0.010
Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethylan 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010
Etion 0.010
Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etofenprox 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010
Etoxazole 0.005
Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Famoxadone 0.010Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010
Fenamidone 0.010
Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamiphos 0.005Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010
Fenamiphos Sulfone 0.005
BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfoxide 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005
Fenarimol 0.005Chlorpyrifos 0.010
BHC lindane gamma 0.010 Difenoconazole 0.005 Fenazaquin 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010
Chlorsulfuron 0.005
Fenbuconazol 0.005
Bifenox 0.020 Chlorthiophos 0.020 Diflufenican 0.005 Fenbutatin oxide* 0.010Bifenazate 0.005 Chlortal dimethyl 0.010 Difenoxuron 0.005
Fenchlorphos 0.010
Bitertanol 0.005 Clofentezine 0.005 Dimepax 0.010 Fenfuram 0.005Bifenthrin 0.010 Clodinafop-propargyl 0.005 Dimefuron 0.005
Fenhexamid 0.005
Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethenamid 0.005 Fenitrothion 0.020
Bolstar 0.010 Clomazone 0.005 Dimethachlor 0.005
Analito LCL (ppm)
Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010
Analito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)
Terbuthylazine-desethyl 0.005
Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010
Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005
Terrazole 0.010
Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010
Hexazinone 0.010 Mirex 0.010 Procymidone 0.010
Tetradifon 0.010
Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-
(THPI)0.010
Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020
Tetramethrin 0.005
Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005
Imazaquin 0.005 Monuron 0.005 Prometon 0.010
Thiacloprid 0.005
Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005
Imidan 0.010N-2,4-Dimethylphenyl formamide
(2,4-DMPF)0.010 Pronamide 0.005
Thidiazuron 0.005
Iprodione 0.010 Nicosulfuron 0.005 Propanil 0.005 Thifensulfuron-methyl 0.005
Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005
0.010
Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005
Thiodicarb 0.005
Thiobencarb 0.010
Irgarol 0.005 Nitrothal-isopropyl 0.010
Isazophos 0.010 Norflurazon 0.005 Propetamphos 0.005
Propazin 0.010 Thiocyclam hydrogen oxalate
Prosulfocarb 0.005
Isoprocarb 0.005 O Phenylphenol 0.010
Isocarbophos 0.010 Norflurazon-Desmethyl 0.010 Propiconazole 0.010
Isofenphos 0.005 Novaluron* 0.010 Propoxur
Propyzamide
0.005
0.005
Isoprothiolane 0.010 Ofurace 0.005
Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005
Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005
Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005
Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005
Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010
Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005
Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005
Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010
Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005
Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010
Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005
Mancozeb 0.005 Paraoxon 0.005 Quinoxyfen 0.005
Mebendazole 0.005 Parathion 0.010 Rimsulfuron 0.005
Simazine 0.010
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)0.010 Pencycuron 0.005 Sethoxydim* 0.010
Mepanipyrim 0.010 Penconazol 0.005 Sebuthylazine 0.010
Metamitron 0.005 Pendimethalin 0.005
Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005 Terbumeton 0.005
Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005
Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010
Metrafenone 0.005 Piperophos 0.005 Teflubenzuron 0.010
Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010
Metosulam 0.005
Thiofanox Sulfoxide
Thionazin
Thiophanate-methyl
Tokution
Tolchlofos methyl
Tolyfluanid
Triadimefon
Triadimenol
Triallate
0.005
0.005
0.005
0.010
0.010
0.010
0.010
0.010
0.010
Triasulfuron
Triazophos
Tribenuron-methyl
Tributyl phosphate
0.005
0.010
0.005
0.010
Tricyclazole 0.010
Triclocarban 0.010
Trichloronate 0.010
Trichlorfon 0.005
Triflumuron 0.010
Trietazine 0.005
Trifloxystrobin 0.005
Triflumizole 0.005
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A.
de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
ppm = Partes por millón = mg/kg Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91
International Maximum Residue Level Database
http://www.mrldatabase.com/
EU Pesticides Database
http://ec.europa.eu/sanco_pesticides/public/index.cfm
Electronic Code of Federal Regulation
http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?
Health Canada
http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php
Normas Alimentarias FAO/OMS
http://www.codexalimentarius.net/pestres/data/pesticides/search.html
Positive List System for Agricultural Chemical Residues in Foods (Japón)
http://m5.ws001.squarestart.ne.jp/foundation/search.html
Información correspondiente a la página 2, página 3, página 4 y página 5
Información correspondiente a la página 5 y 6
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Referencias
Glosario
Trazas = < 0.010 ppm.
MX= México
US= Estados Unidos
JP= Japón
CA= Canadá
EU= Union Europea
KOR=Corea
CHN= China
GC/MSMS = Gases/Masas/Masas AGILENT 225/MS, 240/MS
LC/MSMS = Líquidos/Masas/Masas QQQ (AGILENT 6460)
LCL = Lowest Calibration Level (Nivel Mínimo de Calibración)
LMR = Límite Máximo de Residuos
ppm = Partes por millón = mg/Kg
SD = Sin dato
1. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y
semillas (incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el sistema ISO/IEC 17015:2005. 7890
2. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y
semillas (incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el sistema ISO/IEC 17015:2005.
3. * = Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado.
4. Uso autorizado del plaguicida en el país correspondiente indicado en código ISO 3166-1 alfa-2. Los LMR de cada país se indican en la misma tabla de resultados.
5. En caso de no haber sido detectado algun pesticida se observa una banda verde fuerte. En caso de haber detectado algun pesticida dentro de los límites permitidos se observa una banda
amarilla. En caso de haber detectado algun pesticida fuera de los límites permitidos se observará una banda roja. En caso de haber detectado algún pesticida prohibido se observará una
banda roja.
6. Las bandas de colores son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.
7. ** = Se toma el LMR de Isomero Lambda para la molécula Cyhalothrin (Isomero Gamma y Lambda) , para Cypermethrin a (Zeta-Cypermethrin) se toma el LMR de Zeta-Cypermethrin y
para el LMR de Esfenvalerate + Fenvalerate se toma el de Esfenvalerate.
8. 2 = Para Canadá se considera el default LMR de 0.1 ppm según el punto 5.2.1.4.2 Food and Drug Regulations de Canada Food Inspection Agency http://www.inspection.gc.ca/food/meat-
and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.
9. Las bandas de colores de cada molécula son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.
10. **El LMR de Dicofol es la suma de Kelthane(Dicofol) y op Dicofol
1. En las tablas correspondientes se presenta el punto más bajo de la calibración (LCL).
2. Las tablas correspondientes NO REPRESENTAN UN RESULTADO. Son datos informativos de calidad.
3.Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91
Límites Máximos de Residuos (LMR) para Zarzamora indicados en El Catálogo Oficial
de Plaguicidas de México 2004.
Límites Máximos de Residuos (LMR) para Zarzamora indicados en Enviromental
Protection Agency (EPA) Estados Unidos.
Límites Máximos de Residuos (LMR) para Zarzamora indicados en Electronic Code of
Federal Regulations, (e-CFR TM) Estados Unidos.
1. El cliente tiene cinco días naturales posteriores a la emisión de resultados**** para poder hacer alguna observación o reclamación al respecto, ya que en caso de no hacerlo en este
periodo de tiempo se considerará este informe como aceptado.
2. Las muestras podrán ser desechadas a los 5 días después de la emisión de resultados****, únicamente las muestras para análisis microbiológico serán desechadas 24 h después de ser
recibidas.
3. La información inscrita en el presente "Informe de resultados de análisis" se trata con estricto apego al aviso de privacidad de Análisis Técnicos S.A. de C.V. acatando a los artículos
tercero transitorio, 16 y 17 de la Ley Federa de Protección de Datos Personales en Posesión de los Particulares, con la finalidad de regular su tratamiento legítimo, controlado e informado, a
efecto de garantizar la privacidad y el derecho a la autodeterminación informativa de las personas.
4. Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas.
5. Análisis Técnicos S.A. de C.V. no se encuentra acreditado en muestreo.
6. Los LMR de los paises son un dato de referencia, solicitando revisar los sitios oficiales de cada país ya que pueden cambiar o modificarse.
7. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V., por lo cual no se hace responsable de la representatividad del resultado para el
total del producto
8. Este formato de interpretación está protegido y registrado ante el Instituto Nacional del Derecho de Autor (INDAUTOR), así mismo, los logotipos y nombre de Agrolab y sus filiales se
encuentran registrados ante el Instituto Mexicano de la propiedad Industrial (IMPI). Se prohibe su reproducción total o parcial, para otro fin que no sea la interpretación de resultados, sin
previa autorización.
9. El presente informe de resultados no será válido si presenta raspaduras, tachaduras o enmendaduras.
10. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
11. El laboratorio Análisis Técnicos S.A. de C.V. no es responsable de la actualización de los LMR's ya que son considerados como un dato informativo. Es responsabilidad del usuario del
Informe revisar los sitios oficiales para LMR de cada país ya que la información puede cambiar o modificarse.
12. La detección del residuo del plaguicida por arriba del límite de cuantificación se reporta como ppm (mg//Kg) , por debajo del límite de cuantificación se reportar como <LCL ppm (mg/Kg)
y por debajo del LD se considera como no determinado.
****La emisión del resultados, contempla el informe final destinado a ser enviado al cliente (PDF). La entrega de resultados al cliente, se encuentra sujeta a confirmación de pago.
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Información adicional y complementaria
Información general
Fecha de reporte: 2019-01-07 7 de 7 Revisión:Página:
Final del informe
AR271-TS-70
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de
Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Report Date: 2019-01-07 Page: 1 of 7 Revision AR272-TS-70
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Client Information
Applicant: ALFREDO OSEGUERA DÍAZ Company: SUN BELLE MÉXICO S.A. DE C.V.
[email protected], [email protected],
Address: Km 1 Carr. los Reyes-Jacona S/N City or Town: Los Reyes
State: Michoacán ZIP Code: 60330
Telephone: 3545427328 Ext. 133 E-mail:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Billing Information
Corporate name: Fruits-Giddings SA de CV RFC SBM040520QN6
Address: Km. 1 Carretera los Reyes- Jacona Sn City or Town: Los Reyes
State: Michoacán ZIP Code: 60330
Sample Reg. No. P-19-177 Registry Book: ene-19
Receipt Date: 2019-01-04 Start Date: Termination Day: 2019-01-072019-01-04
Sample Information
Telephone: 3545420170 Ext. SD E-mail:[email protected], [email protected],
[email protected], [email protected]
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Pesticides Multiresidual Analysis
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Tupy|Otras
Analyzed part: Fruit Sample status: Frozen Less Than 1.5Kg
Variety:
Amount recieved:
Common Name: Blackberry Scientific Name: Rubus Ulmifoli
Sampling Place: DIRECCION: ZIRACUARETIRO,
MICHOACÁNSampling Method: Random SDWarehouse RFC:
Producer: JUAN JAVIER ALVAREZ ORTEGA Harvest Place: ZIRACUARETIRO SDSAGARPA Reg.:
Commercial use: Human Commercial Destination: National And Foreign Market
Sampling date:03 DE ENERO DEL 2018 Hora:
11:00 AM
Sample received in conditions for analysis.
2303-01(SECTOR 01)
Final Destination:
Observations:
SDCustoms House:
USA,EUROPE AND JAPAN
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the
representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad IntelectualIts total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
B B
B B
B B
B B
B B
B B
B BB B
B B
B BB BB BB BB B
B B
B BB BB BB BB BB BB B
B B
B BB BB BB BB B
B B
B B
B B
B B
B B
B B
B B
B BB BB B
B B
B BB B
B B
V B
B B
B B
B B
B B
B BB BB BB B
B B
B B
B B
B B
B B
B B
B B
B B
B B
KOR CHN
OXYDEMETON
METHYL
METABOLITE
0.02
- - - -
0.01 - -
- - - -
- - - -
- - - -
- - - -
- - - -
- - - -
0.1 0.2
- - - -
0.01 0.1
0.01 1
0.02 1
0.2 0.5
0.5
0.02 - -
3 1
0.5 2
0.05 0.1
3 1
0.05 0.05
- - - -
0.01 0.05
- - - -
0.01 1
0.01 - -
0.01 - -
0.9 0.7
0.01 0.2
0.01 - -
- -
0.01 0.5
0.01 0.05
0.01 1
0.1 0.1
0.02 0.5
0.01 0.05
0.01 1
0.02 0.02
0.01 - -
- - - -
0.01 1
0.01 - -
0.01 - -
0.01 0.05
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
0.01 - -
0.01 0.05
0.05 0.05
0.01 0.1
0.01 0.05
1 1
- - - -
0.01 0.02
1.5 - -
0.05 1
0.01 0.1
0.01 - -
0.01 - -
- - - -
20 5
0.01 0.5
THIOPHANATE
METHYL/
BENOMYL
METABOLITE
0.01
0.01
0.01 0.01
0.01 0.01
7 7
0.01 0.05
1 0.3
0.01 1
- - - -
10 9
0.01 0.1
0.05 0.3
0.01 0.02
0.02 - -
0.01 0.02
0.01 - -
0.01 0.1
0.01 0.5
0.01 0.01
0.01 0.01
0.01 - -
0.01 - -
- - - -
0.05 - -
- - - -
0.01 - -
0.02 - -
0.05 0.3
5 3
0.01 0.02
0.01 - -
0.02 1
0.01 0.05
0.02 0.02
0.02 0.02
0.02 0.02
0.01 0.01
0.01 0.05
0.1 0.05
- - - -
- - - -
- - - -
LINURON
METABOLITELINURON METABOLITE
- - - -
0.08 0.05
0.01 1
2 1
Report Date: 2019-01-07 Page: 2 of 7 Revision: AR272-TS-70
Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Analysis Results
Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard: ZIRACUARETIRO SAGARPA Reg.: SD
Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-19-177
US JPMX CA EU
JP CA CHN
1-Naphthol GC/MSMSCARBARYL
METABOLITE
CARBARYL
METABOLITE
CARBARYL
METABOLITE
CARBARYL
METABOLITECARBARYL METABOLITE
US JP CA CHN MX US
Banned pesticides residues have been detected
Analyte Analyzed by
Authorized use
MRL (ppm) Obtained amount in mg/kg
(ppm)Analyte Analyzed by
Authorized use
MRL (ppm) Obtained amount in mg/kg
(ppm)MX EU KOR EU KOR
CARBARYL
METABOLITE
CARBARYL
METABOLITE
0.1 - - < LCL
2,3 dihydro-2,2dimethylbenzofuran 7-ol GC/MSMS - - - - - - - - - -
< LCL Carbetamide LC/MSMS - - - - 0.01
THIOPHANATE
METHYL/
BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
< LCL
2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1
< LCL Carbendazim LC/MSMSTHIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
0.1 - - < LCL
2,6-Dichlorobenzamide LC/MSMS - - - - - - - - - -
< LCL Carboxin LC/MSMS - - - - 0.01
0.1 0.02 < LCL
2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - -
< LCL Carbofuran GC/MSMS - - - - 0.3
0.1 - - < LCL
3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -
< LCL Chinometionate GC/MSMS - - - - 0.01
0.1 - - < LCL
3,4 Dichloroaniline GC/MSMS LINURON METABOLITELINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITELINURON METABOLITE
< LCL Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1
- - - - < LCL
Acephate LC/MSMS - - - - 0.01 0.1 0.50
< LCL Chlorbromuron LC/MSMS - - - - - -
0.9 1 < LCL
Abamectin LC/MSMS 0.2 0.2 0.05 0.2 - -
< LCL Chlorantraniliprole LC/MSMS 1.8 1.8 2
0.1 0.01 < LCL
Acetochlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Chlordimeform GC/MSMS - - - - 0.01
0.1 0.02 < LCL
Acetamiprid LC/MSMS 1.6 1.6 2 4 2
< LCL Chlordane- a GC/MSMS 0.1 0.1 0.02
0.1 - - < LCL
Acrinathrin GC/MSMS - - - - 2 0.1 - -
< LCL Chlorfenvinphos LC/MSMS - - - - 0.05
0.1 - - < LCL
Aclonifen GC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorfenapyr GC/MSMS - - - - 0.01
0.1 - - < LCL
Aldicarb LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chloridazon (Pyrazon) LC/MSMS - - - - 0.01
0.1 - - < LCL
Alachlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorfluazuron LC/MSMS - - - - 2
0.1 - - < LCL
Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chlormequat LC/MSMS - - - - 0.05
0.1 - - < LCL
Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chlorimuron-ethyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Ametoctradin LC/MSMS - - - - 0.01 0.1 - -
< LCL Chloroneb GC/MSMS - - - - 0.01
0.1 - - < LCL
Aldrin GC/MSMS 0.05 0.05 0.05 0.1 0.05
< LCL Chlorobenzilate GC/MSMS - - - - 0.01
0.1 - - < LCL
Amicarbazone LC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorothalonil GC/MSMS - - - - 10
- - - - < LCL
Ametryn GC/MSMS - - - - 0.01 0.1 - -
< LCL Chloropropylate GC/MSMS - - - - - -
0.1 - - < LCL
Atrazine GC/MSMS - - - - 0.02 0.1 - -
< LCL Chloroxuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Aminocarb LC/MSMS - - - - - - - - - -
< LCL Chlorotoluron LC/MSMS - - - - 0.01
< LCL
0.1 - - < LCL
Atrazine-2-hydroxy LC/MSMS - - - - - - - - - -
< LCL Chlorpropham GC/MSMS - - - - 0.01
Chlorpyrifos GC/MSMS - - - - 1 0.1 - - < LCL0.01 0.3
< LCLAzinphos-ethyl LC/MSMS - - - - 0.01 0.1 - -
- - - -
Azamethiphos LC/MSMS - - - - 0.01 0.1 - - < LCL Chlorpyrifos methyl GC/MSMS - - - - 0.05 0.1 - -
- - - -
0.01 1
0.05 0.1
- - < LCL
Azoxystrobin GC/MSMS 5 5 5 5 - -
< LCL Chlortal dimethyl GC/MSMS - - - - - -Azinphos-Methyl LC/MSMS - - - - 0.01 2 1 - -
- - - -
0.1 - - < LCL
Benalaxyl GC/MSMS - - - - 0.05 0.1 - -
< LCL Clodinafop-propargyl LC/MSMS - - - - 0.02
< LCL
Baycarb LC/MSMS - - - - - - - - - -
< LCL Chlorthiophos GC/MSMS - - - - - -
- - - -
0.1 - - < LCL
Benfluralin GC/MSMS - - - - 0.01 0.1 - -
< LCL Clomazone LC/MSMS - - - - 0.02
0.1 - - < LCL
Bendiocarb LC/MSMS - - - - 0.01 0.1 - -
< LCL Clofentezine LC/MSMS - - - - 0.01
0.1 - - < LCL
Bensulide LC/MSMS - - - - 0.01 0.1 - -
< LCL Clothianidin LC/MSMS - - - - 0.2
0.1 - - < LCL
Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Cloquintocet-mexyl LC/MSMS - - - - 0.01
- - - - < LCL
Benzoximate LC/MSMS - - - - 0.01 0.1 - -
< LCL Crimidine LC/MSMS - - - - - -
0.1 0.05 < LCL
Benthiavalicarb-isopropyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Coumaphos GC/MSMS - - - - - -
0.1 - - < LCL
BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cyantraniliprole LC/MSMS 4 4 0.01
0.1 - - < LCL
BHC lindane alpha GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cyanazine LC/MSMS - - - - 0.01
0.1 - - < LCL
BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cycloate LC/MSMS - - - - 0.01
0.02 - - < LCL
BHC lindane delta GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cyazofamid LC/MSMS - - - - 0.01
0.1 - - < LCL
Bifenox GC/MSMS - - - - 0.01 0.1 - -
< LCL Cyflumetofen LC/MSMS - - - - 0.01
0.1 - - < LCL
Bifenazate LC/MSMS 5 5 7 5 7
< LCL Cyflufenamid GC/MSMS - - - - 0.01
0.01 0.2 < LCL
Bitertanol LC/MSMS - - - - 0.05 0.1 - -
0.011Cyhalothrin (Isomero Lambda
y gamma)**GC/MSMS - - - - 0.5
0.1 - - < LCL
Bifenthrin GC/MSMS 1 1 1 1 1
< LCL Cyfluthrin GC/MSMS - - - - 0.02
0.1 - - < LCL
Boscalid LC/MSMS 10 10 10 6 - -
< LCLCypermethrin a (Zeta-
Cypermethrin)**GC/MSMS 0.8 0.8 0.5
4 - - < LCL
Bolstar GC/MSMS - - - - - - - - - -
< LCL Cymoxanil LC/MSMS 4 4 4
- - < LCL
Bromophos methyl GC/MSMS - - - - - - - - - -
< LCL Cyprodinil GC/MSMS 10 10 10
0.1 - - < LCL
Bromacil GC/MSMS - - - - 0.01 0.1 - -
< LCL Cyproconazole LC/MSMS - - - - 0.5
- -
0.1 - -
< LCL DDD-o,p GC/MSMS - - - - - -
0.1 - - < LCL
Bromopropylate GC/MSMS - - - - 2 0.1 - -
< LCL Cyromazine LC/MSMS - - - - 0.01- -
0.01 5
0.05 - -
- - - - 0.01 0.1 - -
< LCL DDE-o,p GC/MSMS - - - - - -
- - - - < LCL
Bupirimate LC/MSMS - - - - 0.01 0.1 - -
< LCL DDD-p,p GC/MSMS - - - - - -Bromuconazole* LC/MSMS - - - - 0.01
Butocarboxim* LC/MSMS - - - - 0.01 0.1 - -
< LCL DDT-o,p GC/MSMS - - - - - -
- - - - < LCL
Butachlor GC/MSMS - - - - 0.01 0.1 - -
< LCL DDE-p,p GC/MSMS - - - - - -
< LCL
Buprofezin GC/MSMS
- - 0.01 0.1 0.02
- - < LCL
Buturon LC/MSMS - - - - - - - - - -
< LCLDEET (Diethyl-m-toluamide,
N,N-)GC/MSMS - - - - - -Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - - - -
- - - - < LCL< LCL Demeton O
25 0.01 0.1 - -
- - - -
0.1 0.02 < LCL
0.1 - - < LCL
Butylate GC/MSMS - - - - 0.01 0.1 - -
< LCL Deltamethrin GC/MSMS - - - - 0.1
0.01 - -
0.01 0.05Cadusafos GC/MSMS - -
< LCL Desmedipham LC/MSMS - - - - 0.01
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
< LCL
< LCL Demeton S GC/MSMS - - - - 0.4
Carbaryl GC/MSMS 12 12 10 10 - -
< LCL Demeton-s-methyl-sulfone LC/MSMSOXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITECaptan GC/MSMS 25
GC/MSMS - -
< LCL
Chlorsulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL
0.1 - - < LCL
- - - - < LCLDDT-p,p GC/MSMS - - - - - -
- - - - < LCL
- - - - < LCL
- - - - < LCL
10
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.
Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
B BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B B
B B
B B
B BB B
B B
B BB B
B B
B B
B B
B B
B B
B BB B
0.01 0.02
0.01 0.05
0.01 0.01
0.05 3
0.01 0.01
0.01 - -
0.01 - -
0.01 0.3
0.01 0.5
0.01 0.05
0.5 1
0.05 2
0.01 0.05
0.1
0.1
0.1
0.1
- - - -
0.01 0.5
0.01 0.5
0.02 0.05
0.01 - -
0.01 0.05
0.03 3
0.01 0.05
- - - -
5 5
0.05 0.05
0.05 0.3
0.01 - -
0.01 - -
3 0.7
0.01 - -
0.01 5
0.01 5
3 6
0.01 - -
0.01 - -
0.01 - -
0.01 0.02
0.01 0.2
- - - -
0.005 0.05
0.01 - -
- - - -
0.01 - -
0.03 0.5
0.01 0.2
0.01 1
0.01 - -
0.01 0.05
- - - -
0.02 0.2
0.01 0.5
0.05 0.5
5 2
0.01 - -
- - - -
15 15
0.01 0.3
0.01 0.05
0.05 0.50.01 0.5
0.01 - -
0.01 - -
0.7 0.7
- - - -
0.02 0.02
- - - -
0.01 0.01
1 1
0.01 0.3
0.01 2
- - - -
0.01 1
0.01 - -
0.01 - -
0.01 0.2
0.01 0.03
0.05 0.05
0.7
0.02 0.1
- - - -
0.01 0.01
0.05 0.5
0.01 - -
0.02 - -
- - - -
0.01 0.05
0.01 5
0.01 5
- - - -
0.05 0.05
0.05 0.05
0.05 1
- - - -
0.01 1
0.01 2
0.01 - -
0.01 0.05
0.05 5
0.01 0.1
- - - -
0.01 2
1.5 0.5
- - - -
0.01 - -
- - - -
- - - -
0.01 - -
0.01 0.01
0.01 1
- - - -
0.01 0.1
0.01 15
- - - -
0.01 0.05- - - -
0.05 0.1
0.01 - -
0.01 0.01
Report Date: 2019-01-07 Page: 3 of 7 Revision: AR272-TS-70
Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Analysis Results
Producer:JUAN JAVIER ALVAREZ
ORTEGAOrchard: ZIRACUARETIRO SAGARPA Reg.: SD
Client:SUN BELLE MÉXICO S.A. DE
C.V.Sample: Blackberry Lab Reg. No.: P-19-177
US JP CA EUMX
JP CA CHN
Desmetryn GC/MSMS - - - - - - - - - -
US JP CA CHN MX US
Banned pesticides residues have been detected
AnalyteAnalyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)Analyte
Analyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)MX EU KOR EU KOR
- - - -
- - - - < LCL
Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1
< LCL Fenfuram LC/MSMS - - - - - -
0.1 - - < LCL
Dialifos LC/MSMS - - - - - - - - - -
< LCL Fenchlorphos GC/MSMS - - - - 0.01
0.1 0.5 < LCL
Dichloran GC/MSMS - - - - - - - - - -
< LCL Fenitrothion GC/MSMS - - - - 0.8
20 15 < LCL
Dichlofluanid GC/MSMS - - - - 10 0.1 - -
< LCL Fenhexamid LC/MSMS 20 20 15
0.1 - - < LCL
Diclobutrazol* LC/MSMS - - - - - - - - - -< LCL Fenoxycarb LC/MSMS - - - - 0.05
0.1 - - < LCL
Dichlorvos GC/MSMS - - - - 0.1 0.1 0.2
< LCL Fenoxaprop-ethyl LC/MSMS - - - - 0.1
0.1 - - < LCL
Dicrotophos LC/MSMS - - - - 0.01 0.1 - -
< LCL Fenpropidin LC/MSMS - - - - 0.01
12 5 < LCL
Diclofop methyl GC/MSMS - - - - 0.01 0.1 - -
< LCL Fenpropathrin GC/MSMS 12 12 5
0.1 - - < LCL
Diethofencarb LC/MSMS - - - - 0.01 0.1 - -
< LCL Fenpyroximate LC/MSMS - - - - 0.01
0.1 - - < LCL
Dieldrin GC/MSMS 0.05 0.05 0.05 0.1 0.02
< LCL Fenpropimorph LC/MSMS - - - - 0.05
0.1 - - < LCL
Difenoxuron LC/MSMS - - - - - - - - - -
< LCL Fensulfothion GC/MSMS - - - - 0.01
- - - - < LCL
Difenoconazole LC/MSMS - - - - 0.01 0.1 - -
< LCL Fenson GC/MSMS - - - - - -
- - - - < LCL
Dimefuron LC/MSMS - - - - - - - - - -
< LCL Fenuron LC/MSMS - - - - - -
0.1 0.05 < LCL
Diflufenican LC/MSMS - - - - 0.01 0.1 - -
< LCL Fenthion GC/MSMS - - - - 0.01
0.1 - - < LCL
Dimethachlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Flamprop methyl LC/MSMS - - - - 0.01
0.1 0.02 < LCL
Dimepax GC/MSMS - - - - - - - - - -
< LCL Fipronil GC/MSMS - - - - 0.01
0.1 - - < LCL
Dimethoate GC/MSMS - - - - 1 0.1 - -
< LCL Flazasulfuron LC/MSMS - - - - 0.1
- - - - < LCL
Dimethenamid LC/MSMS - - - - 0.01 0.1 - -
< LCL Flamprop-isopropyl LC/MSMS - - - - - -
0.1 - - < LCL
Dimethylphenol, 2,4- (2,4-xylenol) GC/MSMS - - - - - - - - - -
< LCL Fluazifop-butyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Dimethomorph LC/MSMS - - - - 0.01 0.1 - -
< LCL Flonicamid LC/MSMS - - - - 0.01
0.1 - - < LCL
Dinotefuran LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluchloralin GC/MSMS - - - - 0.01
0.1 - - < LCL
Diniconazole LC/MSMS - - - - 0.01 0.1 - -
< LCL Flubendiamide LC/MSMS - - - - 0.01
7 - - < LCL
Diphenamid LC/MSMS - - - - 0.01 0.1 - -
< LCL Fludioxonil GC/MSMS 5 5 5
0.1 - - < LCL
Dioxathion GC/MSMS - - - - 0.01 0.1 - -
< LCL Flucythrinate GC/MSMS - - - - 0.05
0.1 - - < LCL
Disulfoton GC/MSMS - - - - 0.05 0.1 - -
< LCL Flufenoxuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Diphenylamine GC/MSMS - - - - 0.05 0.1 - -
< LCL Flufenacet LC/MSMS - - - - 0.01
0.1 - - < LCL
Disulfoton sulfoxide GC/MSMS - - - - - - - - - -
< LCL Fluometuron LC/MSMS - - - - 0.02
0.1 - - < LCL
Disulfoton sulfone GC/MSMS - - - - - - - - - -
< LCL Flumiclorac-pentyl GC/MSMS - - - - 0.01
5 - - < LCL
Dodemorph LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluopyram GC/MSMS 5 5 5
0.1 - - < LCL
Diuron (Karmex) LC/MSMS 0.1 0.1 0.05 0.1 - -
< LCL Fluopicolide LC/MSMS - - - - 0.01
0.1 - - < LCL
Edifenphos LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluoxastrobin LC/MSMS - - - - 0.01
0.1 - - < LCL
Dyfonate GC/MSMS - - - - 0.01 0.1 0.01
< LCL Fluoroglycofen-ethyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - -
< LCL Flurtamone LC/MSMS - - - - 0.01
0.1 - - < LCL
Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - -
< LCL Fluridone GC/MSMS - - - - 0.01
0.1 - - < LCL
Endosulfan sulfato GC/MSMS - - - - 0.5 0.1 - -
< LCL Flutolanil GC/MSMS - - - - 0.01
0.1 - - < LCL
Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - -
< LCL Flusilazole LC/MSMS - - - - 0.01
- - - - < LCL
Epoxiconazole LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluvalinate GC/MSMS - - - - - -
0.1 - - < LCL
Endrin GC/MSMS - - - - 0.01 0.1 0.05
< LCL Flutriafol LC/MSMS - - - - 0.01
25 - - < LCL
Esfenvalerate + Fenvalerate (**) GC/MSMS 1 1 1 0.1 0.2
< LCL Folpet GC/MSMS - - - - 0.01
5 - - < LCL
EPTC GC/MSMS - - - - 0.1 0.1 - -
< LCL Fluxapyroxad LC/MSMS 5 5 5
- - - - < LCL
Ethalfluralin GC/MSMS - - - - 0.01 0.1 - -
< LCL Formetanate LC/MSMS - - - - - -
0.1 - - < LCL
Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - -
< LCL Forchlorfenuron LC/MSMS - - - - 0.1
0.1 - - < LCL
Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - -
< LCL Fuberidazole LC/MSMS - - - - 0.01
0.1 - - < LCL
Ethiofencarb LC/MSMS - - - - 0.01 0.1 - -
< LCL Fosthiazate LC/MSMS - - - - 0.05
0.02 < LCL
Ethoprop GC/MSMS - - - - 0.01 0.1 0.02
< LCL g Chlordan GC/MSMS 0.1 0.1 0.02
0.1 - - < LCL
Ethirimol LC/MSMS - - - - - - - - - -
< LCL Furathiocarb LC/MSMS - - - - 0.01
0.01 < LCL
Etion GC/MSMS - - - - 0.3 0.1 - -
< LCL Heptachlor GC/MSMS 0.05 0.05 0.01
0.1 - - < LCL
Ethylan GC/MSMS - - - - - - - - - -
< LCL Haloxyfop-methyl LC/MSMS - - - - 0.05
- - < LCL
Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - -
< LCL Heptenophos LC/MSMS - - - - 0.01
0.1 0.01 < LCL
Etofenprox GC/MSMS 5 5 0.01 0.1 - -
< LCL Heptachlor exo-epoxide (isomer GC/MSMS 0.05 0.05 0.01
- - < LCL
Fenamidone GC/MSMS - - - - 0.01 0.1 - -
< LCL Hexaconazole LC/MSMS - - - - 0.01
0.1 - - < LCL
Famoxadone LC/MSMS 10 10 10 10 - -
< LCL Hexachlorobenzene GC/MSMS 0.05 0.05 0.01
0.01
0.1 - - < LCL
Fenamiphos Sulfone LC/MSMS - - - - - - - - - -
< LCL Hexazinone GC/MSMS - - - - 0.01
0.1 - - < LCL
Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02
< LCL Hexaflumuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenarimol LC/MSMS - - - - 1 0.1 - -
< LCL Imazalil LC/MSMS - - - - 0.02
1.5 - - < LCL
Fenamiphos Sulfoxide LC/MSMS - - - - - - - - - -
< LCL Hexythiazox LC/MSMS 1 1 0.01
LC/MSMS - - - - 0.01 0.1 - -
< LCL Imazaquin LC/MSMS - - - - 0.05
0.1 - - < LCL
Fenazaquin LC/MSMS - - - - 0.01 0.1 - -
< LCL Imazapyr LC/MSMS - - - - 0.01
0.05 0.05
5 1.5
CHNKOR
0.1 - - < LCL< LCL Imidan GC/MSMS - - - - 0.1
2.5 - - < LCL
Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - -
< LCL Imidacloprid LC/MSMS 2.5 2.5 4
0.1 - - < LCL
Fenbuconazol
*Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it´s not responsible for the
representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
B BB BB BB BB BB BB BB BB B
B B
B B
B B
B BB BB BB BB BB B
B B
B B
B B
B B
B B
B B
B B
V B
B B
B B
B BB B
B B
B R
B B
B BB BB BB BB BB BB BB BB B
B B
B
B
B
B
B
BBBBBBBBBB
B
B
0.01 2
0.01 2
- - - -
- - - -
- - - -
0.01 0.05
- - - -
0.02 - -
- - - -
0.01 2
- - - -
- - 0.2
0.01 0.05
4 1
0.01 0.02
0.01 1
0.01 - -
0.05 3
0.01 - -
0.01 0.5
0.01 0.05
0.01 0.05
0.01 0.05
0.01 5
0.01 0.2
0.01 0.05
0.01 - -
0.5 0.05
- - - -
- - - -
0.05 0.3
0.01 0.2
0.1 0.2
0.05 2
0.05 0.05
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
0.02 1
- - - -
0.05 0.05
0.01 1
0.01 0.5
- - - -
0.01 - -
0.05 0.05
0.01 0.1
0.01 0.5
- - - -
- - - -
0.01 - -
0.01 0.05
0.01 0.2
0.01 - -
0.01 - -
0.01 1
- - - -
0.01 0.2
0.05 0.1
0.01 0.05
0.01 - -
- - - -
0.01 5
0.1 0.05
0.01 0.05
0.01 0.1
0.02 0.01
0.2 0.05
0.2 0.05
0.2 0.05
0.01 1
0.02 0.2
- - - -
0.05 5
0.01 0.1
- - - -
0.01 0.05
4 3
0.02 - -
0.1 - -
0.02 - -
0.02 0.4
0.01 0.05
0.01 - -
0.02 0.02
0.02 1
0.01 2
0.1 - -
- - - -
0.05 0.05
0.01 0.3
EU KOR EU KOR
- - - -
0.5 0.5
30 30
0.01 1
- - - -
0.01 0.01
0.01 - -
- - - -
0.01 0.3
0.01 0.2
0.01 - -
0.01 0.1
- - - -
0.01 2
Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL
Metolachlor LC/MSMS - - - - 0.01
ZIRACUARETIRO SAGARPA Reg.: SD
US JP CA EU
Nicosulfuron
Banned pesticides residues have been detected
AnalyteAnalyzed
by
Authorized use
MRL (ppm)
MX JP CA CHN
- -
0.01 0.1 0.01
- - - -
0.02 0.1 0.05
- -< LCL Norflurazon-Desmethyl
0.1< LCL Norflurazon - -
0.05
< LCL O Phenylphenol
- -
- -
- - < LCL
MALATHION
METABOLITE
Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05
Phoxim LC/MSMS
0.1 - -
Analysis Results
AnalyteAnalyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)CA CHN
GC/MSMS - - - - 0.01
Indoxacarb GC/MSMS - - - - 0.01
Irgarol LC/MSMS - - - - - -
Iprovalicarb LC/MSMS - - - -
Iprodione GC/MSMS
Isocarbophos
Isazophos LC/MSMS - - - -
- -
< LCL Neburon
Report Date: 2019-01-07 Page: 4 of 7 Revision: AR272-TS-70
P-19-177SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.:Client:
Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard:
US JP MX US
Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC:
Obtained amount in
mg/kg (ppm)
P-19-177 01-04-2019.d MXAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
- - 0.01
LC/MSMS - - - - - - < LCL
0.01 < LCL
0.1
- -GC/MSMS - - - - 0.1
- -
Imiprothrin GC/MSMS - - - - - - - - - -
- - < LCL0.1< LCL
- - - -
LC/MSMS - -0.1
25 25 12 25 - -
0.010.01 GC/MSMS - - - -0.1 - -
< LCL Nitrapyrin
< LCL Nitrothal-isopropyl < LCL
< LCLLC/MSMS - - - - 0.01< LCL Novaluron*0.1
0.1 - - < LCLGC/MSMS - - - - 0.01
Isoprocarb LC/MSMS - -- - - - 0.01 0.1 - -
0.01 0.02
0.01 0.3
0.01 3
- - - -
Isoprothiolane GC/MSMS - - - - 0.01 0.1 - -
< LCL Ofurace < LCLLC/MSMS - -
< LCLLC/MSMS 0.1 0.1 0.1
Isofenphos LC/MSMS - - - - 0.01 0.1 0.01
- - - - < LCLGC/MSMS - - - -
< LCL Omethoate
3
DIMETHOATE
METABOLITE
- - - -
DIMETHOATE
METABOLITE< LCLLC/MSMS
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
< LCL Ovex
< LCL Oxadiazon
< LCL
Isoxaflutole LC/MSMS - - - - 0.01 0.1 - -
< LCL op Dicofol*** GC/MSMS - - - - 3
- - - - < LCLGC/MSMS - - - - - -
Isoproturon LC/MSMS - - - - 0.01 0.1 - -
Kresoxim-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL
GC/MSMS - - - - 0.01
- - < LCL
Kelthane*** GC/MSMS - - - - 3 3 - -
Linuron LC/MSMS - - - - 0.2 0.1
Leptophos GC/MSMS - - - - - - - - - - < LCL
Lenacil LC/MSMS - - - - 0.3 0.1
< LCL
Malathion GC/MSMS 8 8 8 8 - - < LCL
Malaoxon LC/MSMSMALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
Lufenuron LC/MSMS - - - - 0.01 0.1 - - < LCL
MALATHION
METABOLITE
MALATHION
METABOLITE
0.02 0.5
- - < LCL
Mecarbam LC/MSMS - - - - 0.01 0.1 - - < LCL
Mebendazole LC/MSMS - - - - - - - -
5 < LCL
Mandipropamid LC/MSMS - - - - 0.01 0.1 - - < LCL
Mancozeb LC/MSMS - - - - 5 0.1
- - < LCL
Metazachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Metamitron LC/MSMS - - - - 0.01 0.1
- - < LCL
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2 0.1 - - 0.675
Mepanipyrim LC/MSMS - - - - 0.01 0.1
0.05 < LCL
Methidathion LC/MSMS - - - - 0.2 0.1 0.05 < LCL
Methamidophos LC/MSMS - - - - 0.01 0.1
- - < LCL
Methabenzthiazuron LC/MSMS - - - - 0.01 0.1 - - < LCLMetconazole LC/MSMS - - - - 0.01 0.1
< LCL
Methomyl LC/MSMS - - - - 1 0.01 0.2 < LCL
Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1
- - < LCL
Methiocarb sulfone GC/MSMS - - - - 0.05 0.1 - - < LCL
Methiocarb GC/MSMS - - - - 0.05 0.1
Methoxyfenozide LC/MSMS 6 6 0.01 6 - - < LCL
Methoxychlor GC/MSMS - - - - 7 0.1
- - < LCL
Methoprotryne LC/MSMS - - - - - - - - - - < LCL
Methoprene GC/MSMS - - - - 0.01 0.1
0.01 14
LC/MSMS - - - - 0.01 0.1 - -
- - < LCL
Metobromuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Methylpentachlophenyl Sulfide GC/MSMS - - - - - - - -
- - < LCLMetosulam LC/MSMS - - - - 0.01 0.1
- - < LCL
Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL
Metsulfuron-methyl LC/MSMS - - - - 0.01 0.1
0.1
Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL
Metoxuron LC/MSMS - - - - - - - - - - < LCL
Metrafenone
Molinate LC/MSMS - - - - 0.01 0.1 - - < LCL
Mirex GC/MSMS - - - - 0.01 0.1
- - < LCL
MGK-264 GC/MSMS - - - - - - - - - - < LCL
Mexacarbate LC/MSMS - - - - - - - -
Myclobutanil GC/MSMS 2 2 1 2 - - < LCL
Monuron LC/MSMS - - - - 0.01 0.1
0.03 < LCL
Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Monocrotophos LC/MSMS - - - - 0.01 0.1
1 1
Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL
N-2,4-Dimethylphenyl formamide
(2,4-DMPF)LC/MSMS - - - - - - - - Propachlor LC/MSMS - -- - - -
0.1 0.05
0.1 - - < LCL
Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL
- - < LCL - - 0.01 0.1 - -
- - < LCL
0.01 < LCL
< LCL
- - < LCL
- - < LCL
- -
Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL
Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL
Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Oxamyl Oxime LC/MSMS - - - - - - - - - - < LCL
Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL
Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL
Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL
Paraoxon LC/MSMS - - - - - - - - - - < LCL
Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL
Penconazol LC/MSMS - - - - 0.2 0.1 - - < LCL
Pencycuron LC/MSMS - - - - 0.01 0.1 - -
- - - - 0.01 0.1 - -
- - - - 0.01 0.1
< LCL
Pendimethalin LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL
- -
- - - - 0.01 0.1 - -
< LCL
< LCL
< LCL< LCL
< LCL
0.179
< LCL
- -
Phorate-sulfoxide
Phosalone
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
Pentachloroaniline
Pentachloroanisol
Pentachloronitrobenzene
Pentachlorophenol
Penthiopyrad
Permethrin
Phenmedipham
Phenthoate
Phenyl valerate
Phorate
Phorate-sulfone
- - 0.02 0.1 - -
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
- - - - - - - - - -
- - - - 1 0.1 1
- - - -
0.02 0.010.01 - -
0.01 0.5
0.05 5
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
- - - - 0.05 0.024 0.01
- -
- - - - 0.01 0.1 - -
- - 0.05 0.024 0.01
- - - - - - - - - -
- - - - 0.05 0.024 0.01
Picoxystrobin LC/MSMS - - - - 0.01 0.1 - - < LCL
Piperalin LC/MSMS - - - - - - - - - - < LCL
- - - - 0.01 0.1 - -
< LCL
< LCL
- -
LC/MSMS - - - - 0.01 0.1 - - < LCLPicolinafen
Pirimicarb LC/MSMS - - - - 0.5 0.1 1 < LCL
Pirimiphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Piperonyl Butoxide LC/MSMS 8 8 8 8 - - < LCL
Piperophos LC/MSMS - - - - 0.01 0.1 - - < LCL
Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL
Procymidone GC/MSMS - - - - 0.01 0.1 - - < LCL
Pirimiphos-methyl LC/MSMS - - - - 0.1 0.1 - - < LCL
Primisulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL
- - - - - - - - < LCL
Prometon GC/MSMS - - - - - - - - - - < LCL
Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL
Profluoralin GC/MSMS - - - - - - - - - - < LCL
CHNKOR
< LCL
Propamocarb LC/MSMS - - - - 0.01 0.1 - - < LCL
Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL
Pronamide LC/MSMS - - - - - - - - - - < LCL
0.01 0.1
Promecarb GC/MSMS - -
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total
product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
B BB BB BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB B
B B
B B
B B
B B
B BB B
B B
B B
B B
B B
B B
B
B
B VB VB VB VB VB VB VB VB V
B V
B
B
B
B
B
BBB
B
B
B
B
B
BBBB0.01 0.05 - - < LCLThifensulfuron-methyl LC/MSMS - - - - 0.01 0.1
- - < LCLThidiazuron LC/MSMS - - - - 0.01 0.1 0.01 0.2
0.01 1 - - < LCLThiamethoxam LC/MSMS 0.35 0.35 0.5 0.5
1 < LCLThiacloprid LC/MSMS - - - - 5 0.1 1 0.7
0.01 3 - - < LCLThiabendazole LC/MSMS - - - - 3 0.1
- - < LCLTetramethrin LC/MSMS - - - - 0.01 0.1 0.01 - -
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE< LCL
Tetrahydrophthalimide, cis-1,2,3,6-
(THPI)GC/MSMS
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE
CAPTAN
METABOLITE
- - < LCLTetradifon GC/MSMS - - - - 1 0.1 0.01 1
0.01 - - - - < LCLTetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 0.1
- - < LCLTerrazole GC/MSMS - - - - - - - - - - - -
0.01 0.05 - - < LCLTerbutryn GC/MSMS - - - - 0.01 0.1
- - < LCLTerbuthylazine-desethyl LC/MSMS - - - - - - - - - - - -
0.05 0.1 - - < LCLTerbuthylazine GC/MSMS - - - - 0.01 0.1
- - < LCLTerbumeton LC/MSMS - - - - - - - - - - - -
0.01 0.1 - - < LCLTerbacil GC/MSMS 0.2 0.2 0.1 0.1
- - < LCLTeflubenzuron LC/MSMS - - - - 0.01 0.1 0.01 2
0.01 1 - - < LCLTecnazene GC/MSMS - - - - 0.05 0.1
- - < LCLTebuthiuron LC/MSMS - - - - 0.01 0.1 0.01 - -
0.01 - - - - < LCLTebutam LC/MSMS - - - - 0.01 0.1
- - < LCLTebufenpyrad GC/MSMS - - - - 2 0.1 0.05 0.5
0.05 2 - - < LCLTebufenozide LC/MSMS 3 3 3 0.1
- - < LCLTebuconazole GC/MSMS - - - - 0.01 0.1 0.5 0.5
0.02 0.1 - - < LCLSumithrin GC/MSMS - - - - 0.01 0.1
- - < LCLSulfoxaflor LC/MSMS - - - - 0.01 0.1 0.01 0.5
0.01 - - 0.01 < LCLSulfotep LC/MSMS - - - - 0.01 0.1
- - < LCLSulfosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -
0.01 0.05 - - < LCLSulfentrazone LC/MSMS 0.15 0.15 0.05 0.15
- - < LCLSpiroxamine LC/MSMS - - - - 0.01 0.1 0.01 3
0.1 3 - - < LCLSpirotetramat LC/MSMS - - - - 0.01 2
5 0.1 0.01 5 - - < LCL- - < LCL Vinclozolin GC/MSMS - - - -
- - < LCL
Spiromesifen LC/MSMS - - - - 0.01 0.1 0.02 2
- - - - 0.01 0.1 0.01 0.050.02 1 - - < LCL Vamidothion LC/MSMSSpirodiclofen LC/MSMS - - - - 0.01 0.1
0.01 0.1 0.01 - - - - < LCL1 < LCL Uniconazole GC/MSMS - - - -
- - < LCL
Spinosad A LC/MSMS 1 1 1 0.5 1.5 1
- - - - - - - - - - - -1 0.7 - - < LCL Trimidal LC/MSMSSpinetoram J LC/MSMS 0.8 0.8 0.7 0.5
0.01 0.1 0.01 0.5 - - < LCL- - < LCL Triforine LC/MSMS - - - -
- - < LCL
S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 0.05 0.1
- - - - 0.01 0.1 0.01 - -0.01 0.05 - - < LCL Triflusulfuron-methyl LC/MSMSSimetryn LC/MSMS - - - - 0.01 0.1
0.05 0.1 0.01 0.05 - - < LCL- - < LCL Trifluralin GC/MSMS - - - -
- - < LCL
Simazine GC/MSMS 0.2 0.2 0.2 0.1 0.01 0.25
- - - - 0.02 0.1 0.01 0.50.1 1 - - < LCL Triflumuron LC/MSMSSethoxydim* LC/MSMS 5 5 1 5
0.01 0.1 0.02 2 - - < LCL- - < LCL Triflumizole LC/MSMS - - - -
- - < LCL
Sebuthylazine GC/MSMS - - - - - - - - - - - -
- - - - 0.01 0.1 3 10.01 - - - - < LCL Trifloxystrobin LC/MSMSRotenone LC/MSMS - - - - 0.01 0.1
- - - - - - - - - - < LCL- - < LCL Trietazine LC/MSMS - - - -
- - < LCL
Rimsulfuron LC/MSMS 0.01 0.01 0.01 0.01 0.01 - -
- - - - 0.01 0.1 0.01 0.20.05 0.05 - - < LCL Tricyclazole GC/MSMSQuizalofop-ethyl LC/MSMS - - - - 0.05 0.1
- - - - - - - - - - < LCL- - < LCL Triclocarban LC/MSMS - - - -
- - < LCL
Quinoxyfen LC/MSMS - - - - 0.01 0.1 0.02 2
- - - - - - - - - - - -0.01 0.01 - - < LCL Trichloronate GC/MSMSQuinalphos LC/MSMS - - - - 0.02 0.1
0.5 0.1 0.01 0.05 0.2 < LCL- - < LCL Trichlorfon LC/MSMS - - - -
- - < LCL
Pyriproxyfen GC/MSMS 1 1 0.01 0.1 0.05 1
- - - - - - - - - - - -15 15 - - < LCL Tributyl phosphate GC/MSMSPyrimethanil LC/MSMS 15 15 10 15
0.01 0.1 0.01 - - - - < LCL- - < LCL Tribenuron-methyl LC/MSMS - - - -
- - < LCL
Pyridaphenthion GC/MSMS - - - - 0.01 0.1 0.01 0.2
- - - - 0.01 0.1 0.01 0.050.01 1 - - < LCL Triazophos GC/MSMSPyridalyl GC/MSMS - - - - 0.01 0.1
0.01 0.1 0.05 - - - - < LCL- - < LCL Triasulfuron LC/MSMS - - - -
- - < LCL
Pyridaben LC/MSMS - - - - 0.01 0.1 0.5 1
- - - - - - - - - - - -0.01 1 - - < LCL Triallate GC/MSMSPyrazophos LC/MSMS - - - - 0.01 0.1
0.5 0.1 0.01 0.5 - - < LCL- - < LCL Triadimenol GC/MSMS - - - -
- - < LCL
Pyraclostrobin LC/MSMS 4 4 3 3.5 3 3
- - - - 0.1 0.1 0.01 0.053 0.5 - - < LCL Triadimefon GC/MSMSPymetrozine LC/MSMS - - - - 0.01 0.1
5 0.1 0.02 2 5 < LCL- - < LCL Tolyfluanid GC/MSMS - - - -
- - < LCL
Prosulfuron LC/MSMS - - - - 0.01 0.1 0.01 - -
- - - - - - - - - - - -0.01 0.08 - - < LCL Tolchlofos methyl GC/MSMSProsulfocarb LC/MSMS - - - - 0.01 0.1
- - - - - - - - - - < LCL- - < LCL Tokution GC/MSMS - - - -
- - < LCL
Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 0.01 0.05
- - - - 3 6 0.1 20.05 0.05 - - < LCL Thiophanate-methyl LC/MSMSPropoxur LC/MSMS - - - - 1 0.1
- - - - - - - - - - < LCL- - < LCL Thionazin LC/MSMS - - - -
< LCL
- - < LCL
Propiconazole GC/MSMS 1 1 0.05 1 0.01 0.3
- - - - - - - - - - - -0.01 - - - - < LCL Thiofanox Sulfoxide LC/MSMSPropetamphos LC/MSMS - - - - 0.01 0.1
0.05
1 0.1 0.01 1 - - < LCL- - < LCL Thiodicarb LC/MSMS - - - -
- - < LCL
Propazin GC/MSMS - - - - 0.01 0.1 0.01 - -
- - - - 3 0.1 0.01 10.01 7 - -
Obtained amount in
mg/kg (ppm)Analyte
Analyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)
Thiocyclam hydrogen oxalate GC/MSMSPropargite (Omite) LC/MSMS - - - - 0.01 0.1
0.01 0.1 0.01 0.05 - - < LCL- - < LCL Thiobencarb LC/MSMS - - - -Propanil LC/MSMS - - - - 0.1 0.1 0.01
KOR CHN
Producer: JUAN JAVIER ALVAREZ ORTEGA Orchard: ZIRACUARETIRO SAGARPA Reg.: SD
Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-19-177
CHN MX US JP CA EUMX US JP CA EU KOR
Analysis ResultsBanned pesticides residues have been detected
AnalyteAnalyzed
by
Authorized use
MRL (ppm)
Report Date: 2019-01-07 Page: 5 of 7 Revision: AR272-TS-70
JP CA EU KOR CHNAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Chromatogram GC: P-19-177 01-06-2019.D Chromatogram LC: P-19-177 01-04-2019.d MX US
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total
product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
Vamidothion
Vinclozolin
Triflumuron 0.010
Heptachlor 0.010
Heptachlor exo-epoxide (isomer B) 0.020
Heptenophos 0.005
Fosthiazate 0.005
Fuberidazole 0.005Furathiocarb 0.005g Chlordan 0.010Haloxyfop-methyl 0.005
Fluvalinate 0.010
Fluxapyroxad 0.005
Folpet 0.010
Forchlorfenuron 0.005
Formetanate 0.005
Fluridone 0.010
Flurtamone 0.005
Flusilazole 0.005
Flutolanil 0.010
Flutriafol 0.005
Fluometuron 0.005
Fluopicolide 0.005
Fluopyram 0.010
Fluoroglycofen-ethyl 0.005
Fluoxastrobin 0.005
Flucythrinate 0.010
Fludioxonil 0.010
Flufenacet 0.005
Flufenoxuron 0.005
Flumiclorac-pentyl 0.010
Flazasulfuron 0.005
Flonicamid 0.010
Fluazifop-butyl 0.005
Flubendiamide 0.010
Fluchloralin 0.010
Fenthion 0.010
Fenuron 0.005
Fipronil 0.020
Flamprop methyl 0.010
Flamprop-isopropyl 0.010
Fenpropidin 0.005
Fenpropimorph 0.005
Fenpyroximate 0.005
Fenson 0.020
Fensulfothion 0.010
Analyte LCL (ppm)
Fenoxaprop-ethyl 0.005
Fenoxycarb 0.005
Fenpropathrin 0.010
Trietazine 0.005
Trifloxystrobin 0.005
Methidathion 0.005 Penthiopyrad 0.010 Spirodiclofen 0.005
0.010 Pencycuron 0.005 Sethoxydim* 0.010
Mecarbam 0.005 Parathion methyl 0.010 Rotenone 0.005
Triflumizole 0.005
Methiocarb sulfone 0.010 Phenmedipham 0.005 Spirotetramat 0.005
Methiocarb 0.020 Permethrin 0.010 Spiromesifen 0.005
Trifluralin 0.010
Triflusulfuron-methyl 0.005
Triforine 0.010
Trimidal 0.005
Uniconazole 0.010
0.005
0.010
Methomyl 0.005 Phenyl valerate 0.010 Sulfentrazone 0.005
Methiocarb sulfoxide 0.020 Phenthoate 0.005 Spiroxamine 0.005
Methoprotryne 0.005 Phorate-sulfone 0.005 Sulfotep 0.005
Methoprene 0.010 Phorate 0.010 Sulfosulfuron 0.005
Methoxyfenozide 0.005 Phosalone 0.010 Sumithrin 0.020
Methoxychlor 0.010 Phorate-sulfoxide 0.005 Sulfoxaflor 0.005
Metobromuron 0.010 Phoxim 0.010 Tebufenozide 0.005
Methylpentachlophenyl Sulfide 0.010 Phosphamidon 0.005 Tebuconazole 0.010
0.005 Tebutam 0.005
Metolachlor 0.005 Picolinafen 0.005 Tebufenpyrad 0.010
Metoxuron 0.005 Piperonyl Butoxide 0.005 Tecnazene 0.010
Metosulam 0.005 Piperalin 0.005 Tebuthiuron 0.005
Tricyclazole 0.010
Triclocarban 0.010
Trichloronate 0.010
Trichlorfon 0.005
Report Date 2019-01-07 Page 6 of 7 Revision: AR272-TS-70
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Lowest Calibration Level per analyteAnalyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)
Dimethoate 0.010
2, 4-D Methyl ester 0.010 Bromophos methyl 0.010 Coumaphos 0.010 Dimethomorph 0.0051-Naphthol 0.010 Bromacil 0.010 Clothianidin 0.005
Dimethylphenol, 2,4- (2,4-xylenol) 0.010
2,6 Dichlorobenzonitrilo 0.010 Bromuconazole* 0.010 Cyanazine 0.005 Diniconazole 0.005
2,3 dihydro-2,2dimethylbenzofuran
7-ol0.020 Bromopropylate 0.010 Crimidine 0.005
Dinotefuran 0.005
3,4 Dichloroaniline 0.010 Buprofezin 0.010 Cyazofamid 0.005 Dioxathion 0.0102,6-Dichlorobenzamide 0.005 Bupirimate 0.005 Cyantraniliprole 0.005
Diphenamid 0.005
Abamectin 0.005 Butocarboxim* 0.010 Cyflufenamid 0.010 Diphenylamine 0.0103-Hydroxy carbofuran 0.005 Butachlor 0.010 Cycloate 0.005
Disulfoton 0.010
Acetamiprid 0.005 Buturon 0.005 Cyfluthrin 0.010 Disulfoton sulfone 0.010Acephate 0.005 Butocarboxim-sulfoxide 0.005 Cyflumetofen 0.005
Disulfoton sulfoxide 0.010
Aclonifen 0.010 Cadusafos 0.010 Cymoxanil 0.005 Diuron (Karmex) 0.005
Acetochlor 0.005 Butylate 0.020Cyhalothrin (Isomero Lambda y
gamma)**0.010
Dodemorph 0.005
Alachlor 0.005 Carbaryl 0.010 Cyproconazole 0.005 Dyfonate 0.010
Acrinathrin 0.020 Captan 0.010Cypermethrin a (Zeta-
Cypermethrin)**0.010
Edifenphos 0.005
Aldicarb sulfone 0.005 Carbetamide 0.005 Cyromazine 0.005 Emamectin Benzoate 0.005Aldicarb 0.005 Carbendazim 0.005 Cyprodinil 0.010
Endosulfan I (alpha isomer) 0.010
Aldrin 0.010 Carboxin 0.005 DDD-p,p 0.010 Endosulfan II (beta isomer) 0.010Aldicarb-sulfoxide (Aldoxicarb) 0.005 Carbofuran 0.010 DDD-o,p 0.010
Endosulfan sulfato 0.010
Ametryn 0.010 Chinometionate 0.010 DDE-p,p 0.010 Endrin 0.010Ametoctradin 0.005 Carfentrazone ethyl 0.005 DDE-o,p 0.010
Epoxiconazole 0.005
Aminocarb 0.005 Chlorbromuron 0.005 DDT-p,p 0.010 EPTC 0.010Amicarbazone 0.005 Chlorantraniliprole 0.005 DDT-o,p 0.010
Esfenvalerate + Fenvalerate (**) 0.010
Atrazine-2-hydroxy 0.005 Chlordimeform 0.010 Deltamethrin 0.010 Etaconazole (Etaconazole I y II) 0.010Atrazine 0.010 Chlordane- a 0.010 DEET (Diethyl-m-toluamide, N,N-) 0.010
Ethalfluralin 0.010
Azinphos-ethyl 0.005 Chlorfenvinphos 0.005 Demeton S 0.010 Ethiofencarb 0.005Azamethiphos 0.005 Chlorfenapyr 0.010 Demeton O 0.010
Ethiofencarb-sulfone 0.005
Azoxystrobin 0.010 Chloridazon (Pyrazon) 0.005 Desmedipham 0.005 Ethirimol 0.005Azinphos-Methyl 0.005 Chlorfluazuron 0.005 Demeton-s-methyl-sulfone 0.005
Ethoprop 0.010
Benalaxyl 0.010 Chlormequat 0.005 Dialifos 0.005 Ethylan 0.010Baycarb 0.005 Chlorimuron-ethyl 0.005 Desmetryn 0.010
Etion 0.010
Benfluralin 0.010 Chloroneb 0.010 Dichlofluanid 0.010 Etofenprox 0.010Bendiocarb 0.005 Chlorobenzilate 0.010 Diazinon 0.010
Etoxazole 0.005
Bensulide 0.005 Chlorothalonil 0.010 Dichlorvos 0.010 Famoxadone 0.010Bensulfuron-methyl 0.005 Chloropropylate 0.010 Dichloran 0.010
Fenamidone 0.010
Benzoximate 0.005 Chloroxuron 0.005 Diclofop methyl 0.020 Fenamiphos 0.005Benthiavalicarb-isopropyl 0.005 Chlorotoluron 0.005 Diclobutrazol* 0.010
Fenamiphos Sulfone 0.005
BHC lindane beta 0.010 Dieldrin 0.010 Fenamiphos Sulfoxide 0.005BHC lindane alpha 0.010 Chlorpropham 0.010 Dicrotophos 0.005
Fenarimol 0.005Chlorpyrifos 0.010
BHC lindane gamma 0.010 Difenoconazole 0.005 Fenazaquin 0.005BHC lindane delta 0.010 Diethofencarb 0.005Chlorpyrifos methyl 0.010
Chlorsulfuron 0.005Fenbuconazol 0.005
Bifenox 0.020 Chlorthiophos 0.020 Diflufenican 0.005 Fenbutatin oxide* 0.010Bifenazate 0.005 Chlortal dimethyl 0.010 Difenoxuron 0.005
Fenchlorphos 0.010Bitertanol 0.005 Clofentezine 0.005 Dimepax 0.010 Fenfuram 0.005Bifenthrin 0.010 Clodinafop-propargyl 0.005 Dimefuron 0.005
Fenhexamid 0.005
Boscalid 0.005 Cloquintocet-mexyl 0.005 Dimethenamid 0.005 Fenitrothion 0.020
Bolstar 0.010 Clomazone 0.005 Dimethachlor 0.005
Analyte LCL (ppm)
Hexachlorobenzene 0.010 Mevinphos 0.010 Pirimiphos-methyl 0.005 Terbuthylazine 0.010
Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)
Terbuthylazine-desethyl 0.005
Hexaflumuron 0.005 MGK-264 0.010 Prochloraz 0.005 Terbutryn 0.010
Hexaconazole 0.005 Mexacarbate 0.005 Primisulfuron-methyl 0.005
Terrazole 0.010
Hexythiazox 0.005 Molinate 0.005 Profenofos 0.010 Tetrachlorvinphos, E-isomer 0.010
Hexazinone 0.010 Mirex 0.010 Procymidone 0.010
Tetradifon 0.010
Imazapyr 0.005 Monolinuron 0.005 Promecarb 0.010Tetrahydrophthalimide, cis-1,2,3,6-
(THPI)0.010
Imazalil 0.005 Monocrotophos 0.005 Profluoralin 0.020
Tetramethrin 0.005
Imidacloprid 0.005 Myclobutanil 0.010 Prometryn 0.010 Thiabendazole 0.005
Imazaquin 0.005 Monuron 0.005 Prometon 0.010
Thiacloprid 0.005
Imiprothrin 0.020 Napropamide 0.005 Propachlor 0.005 Thiamethoxam 0.005
Imidan 0.010N-2,4-Dimethylphenyl formamide
(2,4-DMPF)0.010 Pronamide 0.005
Thiodicarb 0.005
Thidiazuron 0.005
Iprodione 0.010 Nicosulfuron 0.005 Propanil 0.005 Thifensulfuron-methyl 0.005
Indoxacarb 0.010 Neburon 0.005 Propamocarb 0.005
Thiobencarb 0.010
Irgarol 0.005 Nitrothal-isopropyl 0.010 Propazin 0.010 Thiocyclam hydrogen oxalate 0.010
Iprovalicarb 0.005 Nitrapyrin 0.010 Propargite (Omite) 0.005
Isocarbophos 0.010 Norflurazon-Desmethyl 0.010 Propiconazole 0.010Isazophos 0.010 Norflurazon 0.005 Propetamphos 0.005
0.005
0.005
Isoproturon 0.005 Omethoate 0.005 Prosulfuron 0.005
Isoprothiolane 0.010 Ofurace 0.005 Prosulfocarb 0.005
Isoprocarb 0.005 O Phenylphenol 0.010
Isofenphos 0.005 Novaluron* 0.010 Propoxur
Propyzamide
Kelthane*** 0.010 Ovex 0.010 Pyraclostrobin 0.005
Isoxaflutole 0.010 op Dicofol*** 0.010 Pymetrozine 0.005
Lenacil 0.005 Oxadixyl 0.005 Pyridaben 0.005
Kresoxim-methyl 0.005 Oxadiazon 0.010 Pyrazophos 0.005
Linuron 0.005 Oxamyl Oxime 0.005 Pyridaphenthion 0.010
Leptophos 0.010 Oxamyl 0.005 Pyridalyl 0.010
Malaoxon 0.005 Oxyfluorfen 0.010 Pyriproxyfen 0.010
Lufenuron 0.005 Oxydemeton-methyl 0.005 Pyrimethanil 0.005
Mancozeb 0.005 Paraoxon 0.005 Quinoxyfen 0.005
Malathion 0.010 Paclobutrazol (Bonzi) 0.005 Quinalphos 0.005
0.010 Rimsulfuron 0.005
Mandipropamid 0.005 Paraoxon-methyl 0.005 Quizalofop-ethyl 0.005
Metsulfuron-methyl 0.005 Pirimiphos-ethyl 0.005 Terbumeton 0.005
Methamidophos 0.005 Pentachlorophenol 0.010 Spinosad A 0.005
Metribuzin 0.010 Pirimicarb 0.005 Terbacil 0.010
Metrafenone 0.005
Metolcarb 0.010 Picoxystrobin
Piperophos 0.005 Teflubenzuron 0.010
0.005
0.010
0.005
0.010
Thiofanox Sulfoxide
Thionazin
Thiophanate-methyl
Tokution
Methabenzthiazuron 0.005 Pentachloronitrobenzene 0.010 Spinetoram J 0.005
0.010
Metazachlor 0.005 Pentachloroaniline 0.010 Simetryn 0.005
Triadimenol
Triallate
Metconazole
0.005
0.005
0.005
0.010
0.010
0.010
0.010
0.010
0.010
Tolchlofos methyl
Tolyfluanid
Triadimefon
0.005
Metamitron 0.005
Triasulfuron
Triazophos
Tribenuron-methyl
Tributyl phosphate
0.005 Pentachloroanisol 0.010
Mepanipyrim 0.010 Penconazol 0.005 Sebuthylazine
Pendimethalin 0.005 Simazine
S-Metolachlor
0.010
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)
Mebendazole 0.005 Parathion
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s
not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
ppm = Parts per million = mg/kg Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91
Data corresponding to page 2, page 3, page 4 and page 5
Report Date: 2019-01-07 Page: 7 of 7 Revision AR272-TS-70
End of Report
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Additional and complementary information
General Information
1. The customer has five calendar days of issuance of the results**** in order to make any comment or complaint about it, because if not done within this time period will be considered this
report has been accepted.
2. Samples may be disposed within 5 days after the issue of results**** only samples for microbiological analysis shall be discarded 24 hours after being received
3. The information recorded in this "Report test results" is treated with strict adherence to privacy notice Análisis Técnicos S.A. de C.V complying with Articles third transient, 16 and 17 of Law
Protection Federation Personal Data Held by Private Parties, in order to regulate their treatment legitimate, controlled and reported, in order to ensure privacy and the right to self-determination
informative individuals.
4.Análisis Técnicos S.A. de C.V not have the authority, or the right to deny, accept or approve cuts or harvests.
5. Análisis Técnicos S.A. de C.V. is not accredited in sampling.
6. MRLs of the countries are a reference data, requesting check the official sites of each country and that can be changed or modified.
7. The result represents the sample that was received on the premises of Análisis Técnicos S.A. de C.V , which is not responsible for the representation of the result for the total product
8. This form of interpretation is protected and registered with the Instituto Nacional del Derecho de Autor (INDAUTOR), likewise, logos and Agrolab name and its subsidiaries are registered with
the Instituto Mexicano de la Propiedad Intelectual (IMPI). Reproduction is prohibited in whole or in part, for any purpose other than the interpretation of results, without permission.
9. This report is not valid if you have scratches, erasures or amendments.
10. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
11. Análisis Técnicos S.A. de C.V. It is not responsible for updating the MRL's because they are considered as a piece of information. It is your responsibility to review the report LMR official
sites for each country since the information can be changed or modified.
12. The detection of the pesticide residue above the quantification limit is reported as ppm (mg / kg), below the limit of quantification reported as <LCL ppm (mg / kg) and below the LD is
considered as undetermined.
**** The issuance of the results includes the final report in PDF format. Delivering results to the client, is subject to confirmation of payment.
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References
International Maximum Residue Level Database
http://www.mrldatabase.com/
EU Pesticides Database
http://ec.europa.eu/sanco_pesticides/public/index.cfm
Electronic Code of Federal Regulation
http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?
Health Canada
http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php
Normas Alimentarias FAO/OMS
http://www.codexalimentarius.net/pestres/data/pesticides/search.html
Positive List System for Agricultural Chemical Residues in Foods (Japón)
http://m5.ws001.squarestart.ne.jp/foundation/search.html
1. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating
QuEChERS extraction), by GASS CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.
2. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating
QuEChERS extraction), by LIQUID CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.
3. * = Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized.
4.Authorized use of the pesticide in the relevant country code specified in ISO 3166-1 alpha-2. RML for each country are indicated in the same results table.
5. If no pesticide was detected a green band is shown. If a pesticide was detected within the allowed limits a yellow band is shown. If a pesticide was detected outside of the allowed limits a red
band is shown. If a forbidden pesticide was detected a red band is shown.
6. The colored bands are visual aids based on MRLs of each country and are not a result.
7. ** = The MRL of Isomero Lambda is taken for the molecule Cyhalothrin (Isomero Gamma and Lambda), for Cypermethrin a (Zeta-Cypermethrin) the MRL for Zeta-Cypermethrin is taken and
for the MRL for Esfenvalerate + Fenvalerate, the one for Esfenvalerate is taken.
8. 2 =For Canada the MRL of 0.1 ppm default is considered according to the point 5.2.1.4.2 Food and Drug Regulations of the Canada Food Inspection Agency
http://www.inspection.gc.ca/food/meat-and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.
9. *** = Dicofol MRL is the sum of p, p-dicofol and o, p-dicofol.
10. The color bands of each molecule are visual support based on the MRLs of each country and do not represent a result.
Information corresponding to page 5 and 6
1. In the corresponding table it´s represented the lower calibration poing (LCL).
2.The correspondig table is NOT A RESULT. It represents quality information data.
3. Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. point 91
Glosario
GC/MSMS = Gass/Mass/Mass AGILENT 225/MS, 240/MS
LC/MSMS = Liquid/Mass/Mass QQQ (AGILENT 6460)
LCL = Lowest Calibration Level
MRL = Maximum Resuide Limits
ppm = Parts per million = mg/Kg
SD = No Data
Traces = < 0.010 ppm.
MX= Mexico
US= United States
JP= Japan
CA= Canada
EU= European Union
KOR= Korea
CHN= China
Maximum Residue Limits (MRLs) for Blackberry listed in The Official Catalog of Mexico
Pesticide 2004.
Maximum Residue Limits (MRLs) for Blackberry indicated in Environmental Protection
Agency (EPA) United States.
Maximum Residue Limits (MRLs) for Blackberry indicated in Electronic Code of Federal
Regulations (e-CFR TM) United States.
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A.
de C.V, therefore it´s not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]