faculty: technology and engineering department: chemical ......unit – x hydrogen power &...

The Maharaja Sayajirao University of Baroda

Faculty: Technology and Engineering

Department: Chemical Engineering

Kalabhavan, Vadodara.

Contact Details :

Email ID: [email protected]

Name of the Programme: B.E.-I Chemical

Type of the Programme :S.S. of B.E.- I Chemical

Year I CORE / ELECTIVE / FOUNDATION 1: CORE

PAPER CODE:CHL1201

PAPER NAME: PROCESS CALCULATIONS

CREDIT

Semester II HOURS 45

UNIT – I

Introduction:

Chemical Engineering and Chemical Industry.

Steady state and unsteady state processes.

Unit Operations, Unit Processes and Process Flow Diagrams.

04

UNIT – II

Basic Calculations:

State properties: Molecular weight, compositions, density, vapor pressure etc. for

gas, liquid and solid systems.

Thermal properties: Heat capacity, sensible heat, latent heat, heat of reaction, heat

of solution, enthalpy calculations etc. for gas, liquid and solid systems.

Techniques of problem Solution: Analytical, Graphical and Numerical.

12

UNIT – III

Material Balances:

Material balance equations based on conservation principle.

Material balances for non-reactive processes(Unit Operations).

Material balances for reactive processes.

10

UNIT – IV

Energy Balances:

Energy balances for closed and open systems based on energy conservation

principle.

Energy balances for non-reactive processes (Unit Operations),

Energy balances for reactive processes.

Coupled material and energy balances for single unit process.

11

UNIT – V

Multiple Unit Processes:

Introduction to processes with multiple Units.

Material balances on processes with recycle, purge, and bypass.

Introduction to DOF analysis and solution strategy for multi-unit process.

08

REFERENCES

1 Bhatt and Vora: Stoichiometry, 4th Ed, Tata McGraw-Hill

2 D.M. Himmelblau and J. B. Riggs: Basic Principles and Calculations in Chemical Engineering, 8th

Ed, Prentice Hall.

3 R.M. Felder and R.W. Rousseau ‘Elementary Principles of Chemical Processes’ 3rd Ed, John Wiley

and Sons, 2000.


Faculty : Technology and Engineering

Department : Chemical Engineering


Contact Details :

E.mail ID :[email protected]

Name of the Program: B.E.CHEMICAL

Type of the Program: S.S. of B.E. -II CHEMICAL

Year II CORE / ELECTIVE / FOUNDATION 1 : CORE

PAPER CODE :

PAPER NAME : MECHANICAL OPERATIONS

CREDIT

Semester I HOURS 45

UNIT – I

Properties of particulate solid

Introduction to particle technology, Characterization of solid particles (size,

shape, size distribution), particle size measurement techniques, Mixed

particles, specific surface of mixture, Particle population.

05

UNIT – II

Screen analysis:

Screening equipment, Method of reporting screen analysis, Capacity and

effectiveness of screens

05

UNIT – III

Size reduction and enlargement:

Principles of comminution, Energy and power required for comminution,

Laws of crushing, size reduction equipments, Industrial processes for particle

size enlargement, size enlargement equipments

05

UNIT – IV

Properties of masses of solids:

Storage of solids: Angle of repose, bulk storage, storage in bins and silos,

Conveying of solids: Codes for characterization of solids, screw conveyers,

belt conveyers, bucket elevators, pneumatic conveying of solids.

04

UNIT – V Mixing of powders and pastes:

Mixers for cohesive and non-cohesive solids, Mixing Index 03

UNIT – VI

Agitation and mixing of liquids:

Basic stirred tank design, Types of impellers, flow patterns, power

consumption and scale up

04

UNIT – VII

Filtration:

Principles of filtration, constant pressure, constant rate filtration,

compressible and incompressible cakes, cake resistance, filter media

resistance, filter media, filter aids, filtration equipments (batch, continuous),

Selection criteria, Washing of filter cakes.

05

UNIT – VIII Gravity setting and sedimentation: Gravity clarifiers, sorting clarifiers, Batch

sedimentation, rate of sedimentation, Design of thickeners and clarifiers 05

UNIT – IX Centrifugal sedimentation: Principles of centrifugal sedimentation, Solid gas

separation, liquid solid separation. 04

UNIT – X

Fluidization: Types of fluidization, Geldart classification of particles.

Minimum fluidization velocity, Pressure drop. Particulate and bubbling

fluidization. Applications of fluidization.

05

REFERENCES

1 W.L. Mc Cabe, J.C. Smith, P.Harriot ‘Unit Operations of Chemical Engineering’ 7th Ed. McGraw

Hill, 2006.

2 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol.- II, 6th Ed. Elsevier, 2003

3 G.G. Brown Ed. ‘Unit Operations’ John Wiley & Sons, 1950

4 C.G. Geankopolis ‘Transport Processes and Separation Process Principles’ 4th Ed, Prentice Hall

India, 2003.




Kalabhavan, Vadodara

Contact Details :

E.mail ID :

Name of the Programme: B.E.CHEMICAL

Type of the Programme:S.S. of B.E.-II CHEMICAL


PAPER CODE : CHL1401

PAPER NAME : FLUID FLOW OPERATIONS

CREDIT


UNIT – I Nature of Fluids, Fluid statics and its applications, Manometers, Pressure

measurements. 06

UNIT – II

Introduction to fluid dynamics, classification of fluids, concept of viscosity,

viscometers, concept of potential flow, steam lines, average velocity, mass

velocity etc. Laminar and Turbulent flow, dimensional analysis, Reynolds

number and its significance, Concept of boundary layer.

06

UNIT – III Basic equations of fluid flow, Equation of continuity, Bernoulli’s Theorem. 06

UNIT – IV

Incompressible flow in pipes and channels, Frictional losses in closed

channels and pipe fittings, contraction and expansion losses, power

requirement for flow.

08

UNIT – V

Transportation of fluids, Pipes, pipe standards, fittings, pipe joints, valves and

their constructional features, Fluid moving machinery: Positive displacement

and centrifugal pumps, centrifugal pump theory, concept of NPSH, pump

performance and characteristics.

06

UNIT – VI

Flow measurement, Classification and selection of flow meters, Variable head

and variable area meters including notched weirs, positive displacement

meters, coirolismeters, ultrasonic meters and various other quantity meters.

05

UNIT – VII Introduction to compressible flow, flow through pipes and nozzles, Fans,

Blowers ejectors and compressors. 06

UNIT – VIII Special cases: Single and two phase flow through packed beds, two-phase gas

liquid flow in pipes, Essentials of gas solid flows. 02

REFERENCES

1 W.L. Mc Cabe, J.C. Smith, P.Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw

Hill, 2006.

2 P.K. Kundu& I.M. Cohen ‘Fluid Mechanics’ 5th Ed, Academic Press, 2002

3 G.S. Sawhney ‘Fundamentals of fluid mechanics’, 2nded,I.K. International

4 J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. I, 6th Ed, Elsevier, 2004.





Contact Details :


Name of the Program: B.E.CHEMICAL

Type of the Program:S. S of B.E.-II Chemical



PAPER NAME : THERMODYNAMICS AND ENERGY

SYSTEM

CREDIT


UNIT – I Laws of thermodynamics, thermodynamic functions & their inter relations. 06

UNIT – II PVT relationship and thermodynamic and Property estimation/calculations

(U, H, S, G etc.) property charts. 07

UNIT – III Thermodynamics of flow processes 05

UNIT – IV Refrigeration and Liquefaction 02

UNIT – V Energy / lost work analysis. 03

UNIT – VI Energy forms, Sources and Resources, flow of energy in ecosystem. 02

.

UNIT – VII Key alternative energy Sources such as Solar Energy, Wind Energy and

Tidal power etc.

09

UNIT – VIII Nuclear energy: Fission reaction, nuclear reactors including safety aspects,

Fusion reactions and their prospects. 04.

UNIT – IX Fuel cells 03

UNIT – X Hydrogen Power & aspects of energy storage and other developments. 04

REFERENCES

1 A.W. Culp ‘Principles of Energy conversion’ 2nd Ed, McGraw Hill, 1991,

2 M.M. El-Wakil ‘Power Plant Technology’2nd Ed, McGraw Hill, 1985

3 J.M. Smith, H.C. Van Ness & M.M. Abbot ‘Introduction to Chemical Engineering

Thermodynamics’, 7th Ed, McGraw Hill, 2004.

4 S.R. Turns ‘Thermodynamics concepts and applications’, Cambridge University Press, 2006.





Contact Details :


Name of the Programme: B.E.II Chemical Engineering

Type of the Programme : S.S. BE II Chemical Engineering


PAPER CODE:

PAPER NAME: UNIT PROCESSES

CREDIT


UNIT – I Concept of Unit operation and unit processes and their role in systematizing the

cognitive structure of Chemical industry.

02

UNIT – II

Classification of Unit processes. Their Characteristic features, thermochemistry

etc.

03

UNIT – III Nitration: Classification of nitro-compounds, nitrating agents, types of nitration,

equipments, typical nitration processes such as Nitrobenzene, tri nitrotoluene etc.

10

UNIT-IV Hydrogenation: Hydrogen production technologies, Hydrogenation of Fats and

oils, petroleum fractions etc.

12

UNIT-V Oxidation, Sulphonation and sulfation: General aspects, reagents, catalysts,

equipments, use of SO3, SO2, H2SO4

12

UNIT-VI Esterification and Hydrolysis, Alkylation, Halogenation: General aspects, reagents,

equipments and typical processes.

06

REFERENCES

1 Groggins, P.H., Unit Processes of Organic Synthesis, McGraw-Hill Book Company, NewYork,

1966

2 Desikan, P and Sivakumar, T.C., Unit Processes in Organic Chemical Industries, Chemical

Engineering Education Development Centre, IIT Madras, 1982.





Contact Details :


Name of the Programme: BE II Chemical Engineering

Type of the Programme : S.S. BE II Chemical Engineering

Year II CORE / ELECTIVE / FOUNDATION 1: CORE

PAPER CODE:

PAPER NAME: ENGLISH COMMUNICATION

SKILLS

CREDIT


1.

UNIT – I

GRAMMAR AND VOCABULARY

1. Contextualized grammar

2. Error analysis

3. Word formation

07

UNIT – II

READING SKILLS

1. Skimming

2. Scanning

3. Word meanings and linking devices

Inferring and predicting

07

UNIT – III

WRITING SKILLS

1. Situational Dialogues

2. Paragraph Writing

3. Transfer of information (visual/verbal)

4. Letter writing ( Job Application)

07

UNIT-IV

ORAL and Aural SKILLS

1. Situational Dialogues (oral)

2. Oral presentation

3. Group Discussion

4. Listening comprehension

07

REFERENCES

1 Achar, Deeptha, et.al. Basics of Academic English, Book 1 and 2. Hyderabad: Orient Blackswan.

2012.

2 Grains, Ruth and Redman Stuart. Oxford Word Skills. Oxford: Oxford University Press. 2008.

3 Lynch, Tony. Study Listening. Cambridge: Cambridge University Press. 2004

4 McCarthy & Felicity O’Dell: Cambridge University Press, New Delhi, 1996

5. Michael McCarthy & Felicity O’Dell. English Vocabulary in Use: Upper-Intermediate: (II

Edition): Cambridge University Press, New Delhi, 2001

6. Raman, M. and Sharma S. Technical Communication Principles and Practice. New Delhi: OUP,

2004.





Contact Details :

E.mail ID : [email protected]

Name of the Program: B.E. CHEMICAL

Type of the Program:F.S. of B.E.-III CHEMICAL

Year III CORE / ELECTIVE / FOUNDATION 1 : CORE


PAPER NAME :MASS TRANSFER OPERATIONS – I

CREDIT

Semester I HOURS 45

UNIT – I Molecular diffusion in fluids:

Stefan- Maxwell's diffusion equations Prediction of diffusion coefficients for gases and

liquids.

08

UNIT – II Fundamentals of mass transfer, mass transfer coefficients, interphase mass

transfer,mass transfer theories

04

UNIT – III

Gas absorption: Gas- liquid equilibria, solvent selection criteria, analysis of absorption

columns, graphical design of plate columns, Kremsers Soudres& Brown’s method.

Mass transfer analysis for design of packed absorption columns for gas absorption

(HETP, HTU, NTU concept) Gas-liquid contacting equipments their classification and

selection.

08

UNIT – IV Humidification and dehumidification: Basic concepts, cooling towers and their

classification and selection, cooling tower design by enthalpy potential method.

06

.

UNIT – V

Distillation: Introduction to distillation. Vapor liquid equilibria. Distillation techniques

viz. differential, flash, steam, fractionation, azeotropic and extractive distillation etc.

vapor liquid contacting equipment their constructional and operational features and

design aspects.

08

UNIT – VI

Analysis of binary distillation: Material and energy balance around a distillation

column, concept of reflux, Lewis Sorel method of calculation, McCabe & Thiele

method for determining number of ideal plates, feed stage location, optimum reflux

ratio, condenser and reboiler heat duty, Ponchon & Savarit method for design of plate

column. Concept of plate efficiencies. Distillation in packed columns.

11

REFERENCES

1. R.E. Treybal ‘Mass – Transfer Operation’ 3rd Ed, Mc Graw Hill, 1981

2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J.Wiley & Sons, 1998

3. C.G. Geankopolis ‘Transport Processes and Separation Process Principles 4th Ed, Prentice Hall

India, 2003.

4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972

5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw

Hill, 2006.

6. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol I, 6th Ed, Elsevier, 2004

7. J.M. Coulson & J.F. Richardson’Chemical Engineering’ Vol II, 5th Ed, Elsevier,2003

8. B.K. Dutta ‘Mass Transfer’ TMH, 2006.





Contact Details :


Name of the Programme : B.E. CHEMICAL

Type of the Programme: F.S. of B.E.-III CHEMICAL



PAPER NAME : HEAT TRANSFER OPERATIONS

CREDIT

Semester I HOURS 45

UNIT – I

Modes of heat Transfer: Transfer by conduction. General differential

equation for heat conduction, steady state analytical and numerical

methods for flat, cylindrical and spherical geometry. Extended surface

heat transfer, Insulation.

07

UNIT – II

Heat transfer by convection: Free & forced convection, film & overall

heat transfer coefficients, concept of convective resistances in series.

Dimensional analysis of convection, physical significance of the

dimensionless numbers. Laminar & turbulent flow heat transfer inside

tubes & outside of tubes.

07

UNIT – III

Heat exchangers: Classification and selection, double pipe heat

exchanger analysis, parallel and counter flow heat transfer, LMTD,

design considerations, NTU method of heat exchanger analysis and

design, Shell & tube heat exchanger calculations.

09

UNIT – IV

Heat transfer with phase change: Regimes of boiling heat transfer,

various correlations. Heat transfer during condensation, drop and film

condensation, Nusselt’s equation and its applications, condensation

over tube banks.

07

UNIT – V

Heat transfer by radiation: Laws of radiant heat transfer, concept of

black body and grey body. Radiation between surfaces, view factors,

radiation between reflecting surfaces, absorption and emission by

gases, luminous & non luminous gases, combined modes of heat

transfer.

09

UNIT – VI

Evaporation:Types of evaporators their classification and selection.

Single effect and multiple effect evaporators, capacity and economy,

feed arrangement to multiple effect evaporators. Evaporator

calculations for single effect and multiple effects.

06

REFERENCES

1. D.Q. Kern, Process Heat Transfer, 5th Ed, McGraw-Hill, 1965

2. Y.V.C. Rao, Heat transfer, 2nd, Ed.

3. J.M. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol.I, 6th Ed, Elsevier, 2004

4. F.P. Incropera& D.P. Dewitt ‘Fundamental of Heat and Mass transfer’, John Wiley & Sons,

1996

5. J.D. Seader and E.J. Hanley “Separation Process Principles”, J.Wiley & Sons, 1998.





Contact Details :



Type of the Program: F.S of B.E.-III CHEMICAL



PAPER NAME :CHEMICAL ENGINEERING

THERMODYNAMICS

CREDIT

Semester I HOURS 45

UNIT – I

Thermodynamic functions and relations for mixtures:

Partial molar property, chemical potential, residual properties, fugacity

& fugacity coefficients, excess functions and activity coefficients,

correlations for excess Gibbs free energy.

09

UNIT – II PVT behaviour including EOS for mixtures; Fugacity estimation/

calculations based on PVT behaviour

06

.

UNIT – III Phase equilibrium criteria and VLE calculations for different pressure

ranges including flash calculations.

03

UNIT – IV Activity coefficient calculation from experimental VLE data and data

reduction, applications of Gibbs-Duhem relation for calculations of

and consistency check for VLE data

06

UNIT – V Phase diagrams for miscible, partially miscible and immiscible liquid

mixtures, introduction to LLE and VLLE calculations.

04

UNIT – VI

Criteria of chemical equilibrium, effect of P and T on equilibrium

conversion (Xe) and equilibrium constant (K), methods of evaluation

of K &Xe, Xe charts for Exothermic, Endothermic, Reversible and

irreversible reactions etc.

06

UNIT – VII

Equilibrium of complex reactions, introduction to equilibrium

conversion calculation under adiabatic and non-isothermal conditions,

introduction to liquid phase, heterogeneous and electrochemical

reaction equilibria, thermodynamic analysis of some chemical

reactions of industrial importance.

08

UNIT – VIII Prediction of thermodynamic properties by group contribution and

other methods.

03

REFERENCES

1. B.G. Kyle ‘Chemical Process Thermodynamics 3rd Ed, Prentice Hall India, 1994

2. J.M. Smith, H.C. Van Ness & M.M. Abbot ,“Introduction to Chemical Engineering

Thermodynamics”, 7th Ed, McGraw Hill, 2004.

3. Y.V.C. Rao, Chemical Engineering Thermodynamics, Universities Press (1997)





Contact Details :


Name of the Programme : B.E. CHEMICAL

Type of the Programme: F.S. of B.E.-III CHEMICAL



PAPER NAME : CHEMICAL REACTION

ENGINEERING I

CREDIT

Semester I HOURS 45

UNIT – I Introduction to chemical kinetics, types of reactions, kinetics of

homogeneous reactions, temperature dependency of reactions.

04

UNIT – II Formulation and analysis of simple and complex rate equations.

Interpretation of rate data in constant and variable volume systems.

06

UNIT – III

Introduction to reactor design, concept of ideal reactors, development of

design expression for batch, tubular and stirred tank and semi-batch

reactors, multiple reactor systems, reactors in series and parallel, recycle

reactor, advantages and limitations in applications.

11

UNIT – IV Multiple reactions, concept of selectivity, maximizing the desired

product in series and parallel reaction system. Introduction to process

design for some industrial reactors.

09

UNIT – V

RTD and non-ideal reactor analysis, one parameter models for non-ideal

reactor RTD and their equivalence, conversion calculations using RTD

measurements. The use of RTD models for evaluation of reactor

performance.

10

UNIT – VI

Equilibrium conversions, heats of reaction and temperature, Optimum

temperatures for isothermal and non-isothermal operations, product

distribution and effect of temperature in multiple (complex) reactions.

Evaluation of adiabatic and non-adiabatic reactor performance, thermal

stability or reactors.

05

REFERENCES

1. O.Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999

2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,

2005.

3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.





Contact Details :

E.mail ID :

Name of the Programme:B.E. Chemical

Type of the Programme:F.S. of B.E.-III CHEMICAL



PAPER NAME : PROCESS EQUIPMENT DESIGN I

CREDIT

Semester I HOURS 45

UNIT – I

Selection of Materials of Construction for Process equipments and

ancillary equipments. Fabrication techniques used for process

equipments with emphasis on bending of plates, welding and various

finishing techniques. Non destructive testing of vessels.

07

UNIT – II

Design of unfired process vessels subjects to internal pressure, design of

end closures and head, nozzles, flanges, manholes etc. Design of unfired

pressure vessels subjected to external pressure. Design codes for

pressure vessels. Testing of pressure vessels.

14.

UNIT – III Design of non-pressure storage vessels with fixed and floating roofs.

Design of Horton spheres. Design codes for storage tanks and bullets.

06

UNIT – IV Design of tall vertical vessels with considerations of wind loads, seismic

activity and various eccentric loads.

04

UNIT – V Design and construction of autoclaves and high - pressure vessels. 05

UNIT – VI Design of foundation and supports, with special emphasis on skirt

supports and saddle supports.

04

UNIT – VII Design of ancillary equipments: Agitator design, tube sheet design,

ejector design etc. 04.

UNIT – VIII Layout of process equipment in the chemical process industries.

01

REFERENCES

1. L.E. Brownell and E.H. Young, ‘Process Equipment Design’, Wiley, 1959

2. B.C. Bhattacharya, ‘Introduction to chemical equipment design – Mechanical aspects’. CBS

publishing Co., 2008

3. B.C. Bhattacharya and C.M. Narayanan, ’Computer aided design of chemical process

equipment’, New Central Book Agency, 1992.

4. M.V. Joshi and V.V. Mahajani, ‘Process equipment design’, 3rd Ed.





Contact Details :


Name of the Program: B.E. Chemical

Type of the Program:S.S of B.E.-III CHEMICAL



PAPER NAME : PROCESS EQUIPMENT DESIGN II

USE OF PERRY’S CHEMICAL ENGINEERS HANDBOOK

IS PERMITTED DURING EXAMINATION.

CREDIT


UNIT – I

Design of piping systems for single phase and two-phase flows, piping colours

and codes. Selection and specifications of pipes, fittings, valves, pumps and

compressors.

12

UNIT – II Design of gas – liquid, gas – solid, liquid – liquid and solid – liquid separators. 07

UNIT – III Design of the heat exchanges (Kern’s method and Bell’s method), condensers

and reboilers. 08

UNIT – IV Design of vapour – liquid contacting equipments: Plate columns and packed

columns. 08

UNIT – V Specification of design variables. Design of multi-component distillation

systems: FUG method and elements of rigorous methods. 07

UNIT – VI Design of absorbers, driers and crystallizers. 03

REFERENCES

1. Don Green and Robert H.Perry, ‘Perry’s Chemical Engineers Handbook’, 8th Ed, Mc-Graw Hill, 2008

2. S.M. Walas ‘Chemical Process Equipment’ Butterworth- Heinemann, 1999.

3. E.E. Ludwig ‘Applied Process Design of Chemical and Petrochemical Plants’ 4th Ed, Vol. I,II,III, Gulf

professional Publications, 1999.

4. N.P. Chopey ‘Handbook of Chemical Engineering Calculations’ 4nd Ed, McGraw Hill, 1994.





Contact Details :


Name of the Program : B.E. Chemical

Type of the Program: S.S. of B.E.-III Chemical



PAPER NAME : CHEMICAL REACTION

ENGINEERING II

CREDIT


UNIT – I

Fundamentals of heterogeneous reacting systems, the influence of mass

transfer on reaction rates, introduction and analysis of fluid-fluid

systems, kinetic regimes and rate analysis.

08

UNIT – II Classification and selection of fluid-fluid reactors based on reaction

regimes. Design of fluid-fluid reactors.

05

UNIT – III

Kinetics of fluid-solid non catalytic reactions, determination of rate

determining steps, various models of gas solid reactions. Classification

and design of non catalytic fluid particle reactors.

11

UNIT – IV

Heterogeneous catalysis, nature of catalysis, components of commercial

catalysts, catalyst preparation characterization of catalysts, catalyst

poisoning and regeneration.

03

UNIT – V

Fluid solid catalytic reaction kinetics (surface catalysis intrinsic

kinetics), kinetics in porous catalyst particles, effective diffusivity,

particle effectiveness factors, temperature dependency, Laboratory

reactors and analysis of rate data.

09

UNIT – VI Design outline of fixed-bed, fluid-bed, trickle-bed and slurry reactors,

isothermal and adiabatic operations. Selected case studies in design.

09

REFERENCES

1. O.Levenspiel “Chemical Reaction Engineering”, 3rd Ed, John Wiley & Sons, 1999

2. H. Scott Fogler ‘Elements of Chemical Reaction Engineering’, 4th Ed, Prentice Hall India,

2005.

3. L Schmidt, ‘The Engineering of Chemical Reactions’, 2nd Ed, Oxford, 2008.

4. J.M. Smith, ‘Chemical Engineering Kinetics’, 3rd Ed, McGraw-Hill, 1981

5. C.N. Satterfield ‘Heterogeneous Catalysis in Industrial Practice 2nd Ed, McGraw-Hill 1993.





Contact Details :


Name of the Program : B.E. CHEMICAL

Type of the Program: S.S. of B.E.-III CHEMICAL



PAPER NAME : CHEMICAL PROCESS

INDUSTRIES

CREDIT


UNIT – I Chemical Industries in India: An overview, Unit Process concept,

Flow sheet symbols. 02

UNIT – II Industrial acids and gases:

Sulfuric acid, Phosphoric acid, hydrogen etc. 06

UNIT – III

Nitrogenous and Phosphatic Fertilizers:

Ammonia, Urea, Diammonium phosphate, triple super phosphate

etc.

06

UNIT – IV Chlor-alkali Industries: Soda ash, Caustic soda 06

UNIT – V Pulp and paper: Pulping techniques, paper making, paper

machines, black liquor, recovery etc. 02

UNIT – VI Cement and Lime:

Types of cement, manufacture by wet process and dry process, etc. 02

UNIT – VII Petroleum and petrochemicals:

General outlook, various products and derivatives 09

UNIT – VIII Polymerization processes:

Polyolefins, polystyrene, nylons etc. 04

UNIT – IX Pharmaceuticals and pesticides:

Bulk drugs and antibiotics, DDT,BHC, malathion etc. 02

UNIT – X Detergents, oils and fats:

LAB derivatives, fat splitting, transesterification, biodiesel etc. 02

UNIT – XI Dyes, intermediates and pigments: Classification, chromophores,

synthesis techniques, H acid, titanium dioxide etc. 02

UNIT – XII Coal and coal chemicals:

Classification, coking, liquefaction, destructive distillation. 02

REFERENCES

1. R.N. Shreve, ‘Chemical Process Industries’, 5th Ed, McGraw-Hill, 1997

2. C. Dryden, ‘Outline of Chemical Technology’,3rd Ed, TMH, 1974

3. J.A. Kent ‘Riegel’s Handbook of Industrial Chemistry’10th Ed., Springer Science &

Business Media, 2003

4. Kirk and Othmer, ‘Encyclopedia of Chemical Technology’, 5th Ed, 24 volumes, 2006.





Contact Details :



Type of the Program: S.S. of B.E.- III CHEMICAL



PAPER NAME : MASS TRANSFER OPERATIONS II

CREDIT


UNIT – I

Liquid–Liquid extraction: Extraction equilibria and its graphical

representation, tie line correlations, prediction of 1-1 equilibria. Stage wise &

continuous contacting equipments their classification and selection, design of

multistage counter current extraction with and without reflux.

12

UNIT – II Leaching: Principles and leaching equilibria, unsteady state & steady state

operations, design of leaching systems, leaching equipment and systems.

05

UNIT – III

Membrane Separation Processes: Reverse osmosis, ultra filtration, micro

filtration, dialysis, per vaporation etc. concepts and analysis, flux equations,

fouling and concentration polarization. Membrane modules their fabrication

and design.

08

UNIT – IV Drying: Concepts, calculations of rate of drying, classification and selection of

drying equipment. Design of batch and continuous driers.

07

UNIT – V

Crystallization: Crystal geometry, solubility curves, supersaturation, theories

of nucleation & crystal growth, calculation of yield, classification and

selection of equipment for solution crystallization, MSMPR crystallization

model, melt crystallization.

05

UNIT – VI

Adsorption & Ion exchange: Equilibrium considerations, stage wise

adsorption and continuous contact adsorption. Fixed bed adsorption, scale up

for constant pattern front, Thermal swing and pressure swing adsorption.

Counter current adsorption, simulated moving bed. Chromatographic

separations.

08

REFERENCES

1. R.E. Treybal ‘Mass-Transfer Operation’ 3rd Ed. Mc Graw Hill, 1981

2. J.D. Seader and E.J. Henley “Separation Process Principles”, 3rd Ed, J.Wiley & Sons,

3. C.G. Geankopolis’Transport Process and Separation Process Principles’ 4th Ed, Prentice Hall India

2003.

4. A.S. Foust et.al. ‘Principles of Unit Operations, 2nd Ed, John Wiley, 1972

5. W.L. Mc Cabe, J.C. Smith, P. Harriot, ‘Unit Operations of Chemical Engineering’ 7th Ed, McGraw

Hill, 2006.

6. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 1, 6th Ed, Elsevier 2004.

7. J.K. Coulson & J.F. Richardson ‘Chemical Engineering’ Vol. 2, 5th Ed, Elsevier 2003.

8. B.K.Dutta ‘Mass transfer’ TMH, 2006





Contact Details :



Type of the Program: F.S of B.E.-IV CHEMICAL

Year IV CORE / ELECTIVE / FOUNDATION 1 :

PAPER CODE : 1702

PAPER NAME : INDUSTRIAL TRAINING

CREDIT

Semester I HOURS

UNIT – I

Each student will undergo industrial training for minimum period

of two weeks during summer vacations after appearing in S.S. BE

III examinations. After the training students will prepare a report

on the training incurred by them in the industry, this report has to

be duly certified by the trainers from the industry where training

was undertaken.

UNIT - II

During the time of training the students will either identify a

suitable product to prepare a detailed project report or the product

will be assigned to them by the department to work out a project

report that has to be submitted by the end of SS BE IV for

evaluation.





Contact Details :


Name of the Programme: B.E. CHEMICAL

Type of the Programme: F.S. of B.E.- CHEMICAL

Year IV CORE / ELECTIVE / FOUNDATION 1 : CORE

PAPER CODE : CHL 1703

PAPER NAME : INSTRUMENTATION AND PROCESS

CONTROL

CREDIT

Semester I HOURS 45

UNIT – I

Introduction to measurement: instruments for measurement of process

variables such as, temperature, flow, liquid level, Pressure.

Instrumentation symbols and labels, Essentials of error analysis.

12

UNIT – II

Introduction to process control, block diagram representation of control loop,

control strategies, mathematical modelling of physical systems, linear system

analysis, dynamics of first order, second order and higher order systems

using transfer functions, transient response, linearization of non linear

models.

08

UNIT – III

Open loop and closed loop transfer functions. Design of single loop feedback

control system. Stability of closed loop, effect of loop parameters on ultimate

gain, effect of dead time, Routh’s test.

06

UNIT – IV

Basic components of control system, sensors and transmitters, control valves,

feedback controllers, actions, types, reset-windup. Tuning of feedback

controllers, tuning controllers for integrating processes, synthesis of

feedback controllers, tuning rules.

07

UNIT – V Stability of control systems, Frequency response analysis, Bode and Nyquist

stability criteria. 06

UNIT – VI

Advanced control strategies, feed forward, cascade, advanced supervisory,

model predictive control, multivariable control, introduction to digital

control principles, microprocessor based control.

06

REFERENCES

1. Luyben, ‘Process Modeling, Simulation and Control for Chemical Engineers’, 2nd Ed, McGraw-

Hill – 1990.

2. Bequette, ‘Process Dynamics’, Prentice Hall, 1998.

3. Coughanor ‘Process systems analysis and control’ 2nd Ed, McGraw-Hill, 1991.





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Type of the Program: F.S. of B.E. - IV CHEMICAL



PAPER NAME : POLYMER SCIENCE AND

TECHNOLOGY

CREDIT

Semester I HOURS 45

UNIT – I Introduction & Basic Concepts, Polymer based industries and feed stocks.

Classification of Polymers. 02

UNIT – II

State of polymer, structure property relations and transition temperatures.

Polymer solutions and characterization of polymers (MW & its experimental

determination), polymer fractionation.

11

UNIT – III

Chain polymerization: Mechanism and kinetics; copolymerization.

Condensation polymerization, coordination polymerization, Techniques of

polymerization.

08

UNIT – IV Plastics–Materials & some typical manufacturing process, (poly olefins,

PVC, PS, PMMA, Epoxy resins etc.) Testing of Polymers. 09

UNIT – V

Rubbers and fibres, materials & some typical manufacturing process, Testing

of rubbers and elastomers. Mechanical properties: Elasticity, visco elasticity,

factors affecting mechanical behaviour etc.

08

UNIT – VI Processing of plastics and rubbers. 07

REFERENCES

1. F.W. Billmeyer, Text book of Polymer Science, 3rd Ed, Wiley, 1984

2. C.E. Carraher, Introduction to polymer chemistry, Traylor and Francis, 2007

3. F. Rodriguez, ‘Principles of polymer systems’ 4th Ed, Traylor and Francis, 1996.





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Type of the Program:F.S. of B.E.-IV Chemical


PAPER CODE: CHL1705

PAPER NAME: SAFETY HEALTH AND

ENVIRONMENT

CREDIT

Semester I HOURS 45

UNIT – I Types of hazards in the chemical industry, accident and loss statistics,

nature of the accident process.

Toxicology and industrial hygiene, models for toxic release.

04

UNIT – II General aspects of fires and explosions, design to prevent fires and

explosions, Fire and explosion indices, Phenomena of vapour cloud

explosion, flash fires and BLEVE

06

UNIT – III Safety considerations in design, installation, operation and maintenance of

selected process equipment, relief system and flares etc.

05

UNIT – IV Hazard and operability studies Hazard analysis ‘What if’ analysis.

Failure modes and effect analysis, fault tree analysis, event tree analysis.

04

UNIT – V

Acceptable risk and safety properties, protective equipment for personal

and plant for various hazards, safety procedure, emergency response.

Disaster management, insurance, workers safety and public liability, other

liabilities.

04

UNIT – VI

Ecology, classification of ecological factors, fundamental ecological

variables, Ecological principles governing use of natural resources,

Atmosphere, hydrosphere and climates, cycles of principal biogenetic

elements and water cycle, perturbation of cycles due to human

interference, its consequences and mitigation.

Green house effect, global warming, air pollution acts & legislations.

08

UNIT – VII

Assessment of air quality, sampling and measurement. Control of dusts,

mists and aerosols in industrial processes using different equipments.

Control of toxic releases, SOX &NOX ,using absorption, and adsorption

other chemical treatment techniques.

06

UNIT VIII

Water quality assessment and water quality management, Physical,

chemical and biochemical techniques of water pollution control. Water

pollution prevention and control acts.

Solid waste management. Landfills, nuclear waste management schemes.

08

REFERENCES

1. Crowl and Louver ‘Chemical Process safety: Fundamentals with Applications:’ 3nd Ed., Prentice

Hall, 2011

2. Valsaraj, ‘Elements of environmental engineering’ CRC press, 1998

3. Sanders, ‘Chemical process safety’ 3rd Ed, Elsevier, 2005.





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Type of the Program :F.S. of B.E.-IV CHEMICAL

Year IV CORE/ELECTIVE/FOUNDATION 1 : CORE


PAPER NAME : TRANSPORT PHENOMENA

CREDIT

Semester I HOURS 45

UNIT – I

The role of transport phenomena in the understanding of chemical

engineering.

Fluids classification. Transport properties. Introduction to non-

Newtonian fluids. Two parameter models.

03

UNIT – II Lagrangian and Eulerian concept of motion, control volume

approach, overall and differential mass balances in Cartesian,

cylindrical co-ordinate systems.

04

UNIT – III Shell momentum balance approach; Application to selected problem.

06

UNIT – IV Equation of motion and its application. 04

UNIT – V Boundary Layer theory von Karman’s analysis, exact solutions using

stream functions. Turbulence concepts mixing length hypothesis,

universal velocity profile and its application.

06

UNIT – VI Shell energy balance approach: Applications to selected problems. 05

UNIT – VII Convective Heat transport : Asymptotic solutions of typical flow

problems etc.

04

UNIT – VIII Fick’s law of diffusion application of differential balances to mass

transfer, critical analysis correlations for mass transfer. 04

UNIT – IX Mass transfer theories Convection – Diffusion problems in

homogenous and heterogeneous media.

04

UNIT – X Analogy between Momentum heat and mass transfer.

05

REFERENCES

1. Bird Stewart and Lightfoot, ‘Transport Phenomena’ 2nd Ed, Wiley, 2002

2. Welty, Wicks, Wilson &Rorer ‘Fundamentals of Momentum heat & mass transfer,

Wiley, 2001.





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Type of the Program: F.S of B.E.-IV CHEMICAL


PAPER CODE : 1711L

PAPER NAME : COMPUTER AIDED DESIGN

LABORATORY

CREDIT

Semester I HOURS

UNIT – I

Students will be assigned computational / simulation exercises

to be worked out using flow sheet simulators with special

emphasis on property estimation and process optimization.





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Type of the Program:F.S. of B.E.IV CHEMICAL

Year IV CORE / ELECTIVE / FOUNDATION 1 : ELECTIVE

PAPER CODE :CHL1701

PAPER NAME ELECTIVE : C ADVANCES IN

SEPARATION SCIENCE

CREDIT

Semester I HOURS 45

UNIT – I

The structure of separation processes, definitions of separation and separative

work, characterization of concentration distribution. The morphology of

separations processes.

04

UNIT – II Adsorptive bubble separation techniques, principles, application and design. 04

UNIT – III Membrane processes, classification, principles, applications and design. 06

UNIT – IV Melt crystallization, zone refining, short path distillation and super critical

extraction. 08

UNIT – V Electrical separations: Electrophoresis, electrodialysis, protein purification

using isoelectric focusing in gels, field flow fractionation. 07

UNIT – VI Chromatographic separation principles. Applications and scale up, separations

based on simulated moving beds, affinity chromatography. 07

UNIT – VII Extractive separations using liquid membranes, reverse micelles and micro

emulsions. 05

UNIT – VIII Features of separation of isotopes, isomers and other complex molecules using

novel separation techniques.

04

REFERENCES

1. Wankat, ‘Rate based separation’, Elsevier, 2005.

2. King, ‘Separation processes’, 2nd Ed, Mc-Graw Hill, 1980.

3. Li, ‘Recent developments in separation science’, Vol I –V, CRC press, 1980





Contact Details :


Name of the Programme: B.E. CHEMICAL

Type of the Programme: F.S. of B.E.-IV CHEMICAL


PAPER CODE :CHL1707

PAPER NAMEELECTIVE:D PETROLEUM

ENGINEERING

CREDIT

Semester I HOURS 45

UNIT – I Prospecting for petroleum, exploration methods, reserve appraisals,

Exploration & production, petroleum management. 05

UNIT – II Well logging and Basin modelling, Natural gas coal bed methane, gas

hydrate and deep water exploration 09.

UNIT – III Reservoir characterization, Physico-Chemical environment of petroleum

reservoirs in relation to oil and gas recovery systems. 10

UNIT – IV Flow through porous media, mechanism of entrapment and mobilization of

oil in porous media. 05

UNIT – V Enhanced oil recovery techniques using surfactant & polymer flooding,

reservoir management techniques. 06

UNIT – VI Drilling, Production, platform engineering and transportation.

Safety aspects in Petroleum production. 06

UNIT – VII Hydrocarbon resources and petroleum supply scenario. 04

REFERENCES

1 James Speight, The Chemistry and Technology of Petroleum, CRS Press, Fifthe Edition.

2 Boyun Guo, William C. Lynos, Ali Ghalambor, Petroleum Production Engineering: A Computer

Assisted approach. Gulf Publiacation.





Contact Details :



Type of the Program: F.S. of B.E.-IV CHEMICAL


PAPER CODE: CHL 1708

PAPER NAME ELECTIVE-I : A: COLLOID AND

SURFACE SCIENCE

CREDIT

Semester I HOURS 45

UNIT – I Nature of colloidal dispersions: Scope and variables. 04

UNIT – II Particle size and shape, transport properties of suspensions, sedimentation

and diffusion. 05

UNIT – III Liquid surfaces and interfaces, thermodynamics of surfaces, surface tension,

contact angle, interfacial tensions, surface energies. 05

UNIT – IV

Colloidal structures in surfactant solutions, micellar phase diagrams,

adsorption from solution and monolayer formation, soft interfaces,

Langmuir, Blodge films.

05

UNIT – V

Dispersions, rheology of dispersions, electrical charges in dispersions, forces

of attraction and repulsion between particles Electro kinetics and zeta

potential.

06

UNIT – VI Colloidal and dispersion stability, DLVO theory, electrostatic and polymer

induces colloidal stability. 07

UNIT – VII Emulsions, foams and micro emulsion. 07

UNIT VIII Industrial applications to surface coating industry, pharmaceutical industry,

oil recovery etc.

06

REFERENCES

1. R.J. Hunter, Foundations of colloid science, 2nd Ed Oxford, 2006

2. Lyklema, ‘Fundamentals of interfacial and colloid science’, Vol. I – V Academic press, 1982

3. Cosgrove, ‘Colloid Science’ Blackwell Publishing, 2005.





Contact Details :


Name of the ProgramB.E. Chemical

Type of the Program F.S. of B.E.-IV CHEMICAL



PAPER NAME ELECTIVE : B CATALYSIS: SCIENCE &

TECHNOLOGY

CREDIT

Semester I HOURS 45

UNIT – I

Basics of Catalysis: Emergence of catalysis science & technology, a brief

history importance of catalysis and catalyst technology, Foundation catalytic

phenomena & principles.

03.

UNIT – II

Homogeneous and Enzyme catalysis: Elementary steps in homogeneous

catalysis, metal complex catalysis in liquid phase, liquid exchange dissociation

&coordination, oxidative addition, reductive elimination, insertion and

migration. Structure/Activity relationships, steric effects. A symmetric

homogeneous catalysis, industrial examples, homogeneous catalysis without

metals, cleric acid/base catalysis, organocolysis,

Essentials of enzyme catalysis –Michaelis – Mentenreaction, Scaling up

homogeneous catalysis, catalyst recovery & recycle, Hybrid catalysts.

10.

UNIT – III

Heterogeneous Catalysis: Concept of active site model catalyst systems, real

catalysts, promoters, modifiers, poisons, preparation of solid catalysts, selection

of support catalyst characterization. Surface characterization, temperature

programmed techniques, spectroscopy & microscopy, selected care studies.

10.

UNIT – IV

Catalytic Reactor Design: The LHHW model, general behavior of catalyst

particles & pellets, heat and mass transfer aspects, Thiele modulus and

effectiveness factor. Choice of reactors in lab and plants collection & analysis

of data from lab. Reactors. Fundamentals of catalytic reactor design, selected

care studies.

08.

UNIT – V

Catalyst Deactivation: Causes and mechanism of deactivation, prevention and

regenerative treatment of catalyst decay, selected care studies.

Optimal distribution of catalyst in a single pellet. Optimal distribution of

catalyst in a reactor.

07

UNIT – VI

Environmental Catalysis :

1. Mobile sources: Automotive gasoline catalytic converters, catalytic

abatement of emissions from diesel engines, Trends in emission control for

mobile sources.

2. Stationary sources: Catalytic reduction of NOy catalytic oxidation of VOC

emissions, catalytic oxidation of CO emission, Kinetics & reactor design for

CO & VOC oxidation.

07.

REFERENCES

1. Morbidelli, Cavnilidis& Varma Catalyst design Cambridge Univ. press 2001.

2. Twigg, ‘Catalyst Handbook’ Manson publications, 1996.

3. Bartholonew and Farrauto ‘Fundamentals of Industrial catalytic processes’ Wiley Interscience, 2006.





Contact Details :


Name of the Program B.E. Chemical

Type of the Program: S.S. of B.E.-IV Chemical



PAPER NAME : MODELING SIMULATION AND

OPTIMIATION

CREDIT


UNIT – I Role of Modeling, Simulation and Optimization (MSO) in process design –

Synthesis Analysis, 02

UNIT – II Modeling: Introduction, Classification of process models, Model Building,

Characteristics of mathematical models. 08

UNIT – III

Simulation: Analytical and Numerical methods for solving model equations,

Accuracy and error analysis, Approaches to Process Simulation, Commercial

simulators.

06

UNIT – IV

Optimization Introduction: Optimization problem and its formulation,

General approach for solution, Objective functions, Classification of

Optimization problems and methods. 07

UNIT – V

Optimization techniques:

-Continuity, convexity and conditions for maxima / minima

-Analytical methods: Direct search (without constraints) Lagrangian

Multiplier (with constraints),Calculus of Variation.

-Newton and quasi Newton methods for single and multivariable search

-Linear (LP) and non linear (NLP) programming with constraints

-Mixed Integer Programming: MILP and MINLP

-Global Optimization Techniques

16

UNIT – VI

Applications of modelling simulation and optimization to chemical processes

and equipments. Fluid flow, heat Transfer, separations, reaction systems and

reactors etc. Use of spreadsheets and MATLAB for Simulation and

Optimization.

06

REFERENCES

1. Edgar, Himmelblau, and Lasdon ‘Optimization of Chemical Process’ McGraw-Hill, 1990

2. Babu, ‘Process Plant Simulation’. Oxford, 2005

3. Ramiez, ‘Computational methods for process simulation’, Butterworth, 1992.





Contact Details :

E.mail ID :


Type of the Program:S.S. of B.E.-IVChemical



PAPER NAME : PETROLEUM REFINERY

ENGINEERING

CREDIT


UNIT – I Development of Petroleum Refining industry in India. Crude evaluation

and Testing of refinery products. 04

UNIT – II Primary processing of crude, preparation, atmospheric and vacuum

distillation, flow sheets process, conditions and Equipment. 05

UNIT – III Catalytic cracking and hydrocracking. Principles, feed-stocks, catalysts and

hardware 08

UNIT – IV Catalytic reforming: Principles, feed-stocks, catalysts and hardware.

Extraction of aromatics 06

UNIT – V Vis-breaking, coking, isomerization, alkylation and polymerization 06

UNIT – VI Treatment of petroleum products. Hydrodesulphurization. 04

UNIT – VII Refining of Lube distillates: Deasphalting, solvent extraction, dewaxing

etc. Production of bitumen, waxes and greases 08

UNIT – VIII Processing natural and associated gases. 04

REFERENCES

1. James Speight, "The Chemistry and technology of petroleum", 2nd ed., Marcel Dekker, 1991

2. R.A. Meyers, ’Handbook of Petroleum refining processes’, 3rd Ed., McGraw-Hill, 2004.

3. Nelson, ‘Petroleum Refining Engineering’, McGraw-Hill, 1949

4. B. K. Bhaskarrao, "Modern Petroleum Refining Processes", Oxford and IBH, 1984





Contact Details :



Type of the Program: SS BEIV CHEMICAL



PAPER NAME : PROCESS SYNTHESIS AND

ECONOMICS

CREDIT


UNIT – I

Introduction, role of process synthesis in process design, hierarchy of

synthesis steps. Synthesis Tree, approaches for synthesis, heuristics for

process synthesis. Project engineering, plant location, plant layout and

utilities.

08

UNIT – II Attainable Regions and reactor networks: Concepts and implementation

techniques, reactor – separator – recycle network. 06

UNIT – III

Heat & Power integration: Heat Exchanger Networks –Stream matching,

heat loops and minimum heat exchangers. Heat integration in

Distillation trains. Minimum energy requirement targets and pinch

analysis

08

UNIT – IV

Project scheduling. Scheduling of batch processes. Optimization of

cycle time and number of units. CPM/PERT, identification of critical

path & critical activities

08

UNIT – V

Project cost estimation and cost of production estimation. Interest,

investment costs, depreciation, profitability, criteria cash flow diagram,

cost indices.

08

UNIT – VI

Economics of selecting alternatives and replacement cost, economy of

scale, marginal cost, break even analysis and optimization. Inventory

Control, taxes and insurance, legal aspects, liabilities, patent indemnity

etc.

07

REFERENCES

1. Robin Smith, ‘Chemical Process Design and Integration’, Wiley, 2005.

2. Biegler, Grossmann and Westerberg, ‘Systematic Methods of Chemical Process Design’, Prentice

Hall, 1997.

3. Seider, Seader, Lewin, ‘Product and Process Design Principles’, 2nd Ed., Wiley 2004.

4. Peters and Timmerhaus, ‘Plant design and economics for chemical engineers’ 4th Ed,

McGraw-Hill, 1991.





Contact Details :





PAPER CODE : 1805

PAPER NAME : PROJECT

CREDIT

Semester II HOURS

UNIT – I

Identify a suitable product and prepare a detailed project report or the product will

be assigned to them by the department to work out a project report. The report has

to be submitted at the end of SS BE IV for evaluation.





Contact Details :





PAPER CODE : 1806

PAPER NAME : SEMINAR

CREDIT

Semester II HOURS

UNIT – I

Students will be assigned a topic for which a detailed literature survey has to be

carried out. Students will refer to various books and journals for the same and

prepare a report. The report has to be submitted at the end of SS BE IV for

evaluation.





Contact Details :



Type of the Program: SS. of B.EIVChemical


PAPER CODE:CHL1807

PAPER NAME ELECTIVE II: D PETROCHEMICAL

TECHNOLOGY

CREDIT


UNIT – I Scope of Petrochemical industry in India, Feedstock for petrochemicals 03

UNIT – II Naphtha cracking/Gas Cracking – separation and purification of cracker

products (olefins and diolefins) 06

UNIT – III Production and purification of synthesis gas. C1 based petrochemicals

(methanol, formaldehyde, acetic acid etc.) 06

UNIT – IV

Petrochemicals from various unit processes like oxidation, dehydrogenation, chlorination, oxychlorination, ammoxidation, hydration, dehydration, nitration, polymerization etc.

12

UNIT – V

Aromatics production, isolation of aromatics, separation of C8 aromatics.

Benzene derivatives, ethylbenzene, styrene etc, xylene derivatives, phthalic

anhydride, terpthalic acid, dimethyl terpthalate etc.

12

UNIT – VI

Miscellaneous aspects of petrochemical production: Safety and Health aspects,

environmental aspects, Clean Technologies, Future beyond Petroleum. 06

REFERENCES

1. P. Desikan and T.C. Sivakumar, ‘Unit processes in Organic Chemical Industries’, IIT Madras,

1982.

2. E.C. Leonard, ‘Vinyl and Diene Monomers’, Wiley 1969.

3. H.G. Franck & J.W. Stadelhofer, ‘Industrial Aromatic Chemistry’, Springer Verlag, 1988.





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Type of the Program: SS BE IV CHEMICAL



PAPER NAME : ELECTIVE II : A :

NANOTECHNOLOGY

CREDIT


UNIT – I Nanotechnology foundations: Definition, historical perspective, effects of

nanoscience and nanotechnology in various fields 03

UNIT – II

Properties of nanostructured materials: Shape and size dependent

properties, colour, melting point, density of states, band gap, magnetism

etc.

07

UNIT – III

Synthesis of nanoparticles: Top down and bottom up approaches, Nano

particles via colloids, micelles, vesicles, polymers, crystalline and zeolite

hosts. Mechanical attrition, high energy ball milling.

10

UNIT – IV

Characterization techniques of nanostructured materials: Scanning electron

microscopy, Transmission electron microscopy, scanning tunneling

microscopy, atomic force microscopy, X-ray diffractometer, spectroscopy,

UV-Vis, Raman, EDX, AES etc.

10

UNIT – V Fabrication : Crystal growth, epitaxy, lithography, etching, masking,

MEMs 07

UNIT – VI

Applications relevant to the chemical industry: Catalysis, fuel cells,

coatings, nanocomposite polymers, fluid inks, dyes, block copolymers and

dendrimers.

08

REFERENCES

1. K.J.Klabunde , ‘Nanoscale materials in Chemistry’, Wiley Interscience, 2001.

2. J.Poole and S. Owens, ‘ Introduction to Nanotechnology’ Wiley, 1998

3. C.N.R Rao, Chemistry of Nanomaterials’ Wiley, 2007





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Type of the Program: S.S. of B.E.-IV CHEMICAL



PAPER NAME ELECTIVE II : B BIOTECHNOLOGY

CREDIT


UNIT – I Introduction to Biotechnology. Basic microbiology and recombinant DNA

technology 04

UNIT – II Kinetics of enzyme catalysis including immobilized enzyme technology 06

UNIT – III Kinetics of substrate utilization product formation and biomass production in

cell culture. 07

UNIT – IV Transport phenomena in Bioprocess systems. 07

UNIT – V Aeration/Agitation/Mediasterilization/Air fertilization. 05

UNIT – VI Design and analysis of bioreactors. 06

UNIT – VII Downstream processing techniques. 03

UNIT – VIII

Industrial Biotech products – Ethyl alcohol based on various substrates

including lignocelluloses. Penicillin citric Acid, SCP, Bio-fertilizers, Baker’s

yeast – other modern biotech products.

07

REFERENCES

1 Bailey &Ollis, ‘Biochemical Engineering’,2nd Ed, McGraw – Hill, 1986.

2 Moo-Young, ‘Comprehensive biotechnology’ Vol I to V, Elsevier, 1984.

3 Belter, Cussler and Hu, ‘Bioseparations’ Wiley, 1988.





Contact Details :



Type of the Program:S.S. of B.E.-IV Chemical

Year IV CORE / ELECTIVE / FOUNDATION 1 :ELECTIVE

PAPER CODE: CHL1810

PAPER NAME: POLYMER PROCESSING

CREDIT


UNIT – I Basic aspects of Polymers: Functionality, types, structure-property

relationship, processing fundamentals, processing aids and additives.

04

UNIT – II Morphology, rheology and flow of polymers. 06

UNIT – III Heat and mass transfer in polymer systems, mixing of polymers, mixing

equipments.

07

UNIT – IV Extrusion of polymers, extrusion equipment, calendering. 10

UNIT – V Moulding of polymers: Blow, compression, transfer, rotational and

injection moulding techniques, analysis and equipments.

10

UNIT – VI Other processing techniques: Sheet forming, fiber spinning, pultrusion,

techniques and equipments.

08

REFERENCES

1. B.R.Gupta, ‘Polymer Processing Technology’, Asian Books Pvt. Ltd, 2008

2. Z. Tadmor and C.G.Gogos, ’Principles of Polymer Processing’ John Wiley and Sons, 1979

faculty: technology and engineering department: chemical ......unit – x hydrogen power &...

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