evaluation of rapid methods for determining lime requirement using east texas soils
DESCRIPTION
Evaluation of Rapid Methods for Determining Lime Requirement Using East Texas Soils Leon Young & Henry Dlamini, Stephen F. Austin State University, Nacogdoches, TX. INTRODUCTION - PowerPoint PPT PresentationTRANSCRIPT
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Evaluation of Rapid Methods for Determining Lime Requirement Using East Texas SoilsLeon Young & Henry Dlamini, Stephen F. Austin State University, Nacogdoches, TXINTRODUCTIONThe Adams-Evans method (Adams & Evans, 1962) has been used for many years as the buffer pH method for determining Lime Requirement (LR) of soils in the Southeastern Region of the U.S. The buffer contains paranitrophenol which is a hazardous material requiring expensive disposal measures. Two modified Adams-Evans buffer methods have been proposed and are currently being used by Extension labs in the region. The Modified Adams-Evans developed by Huluka (2005 & 2007) substitutes monobasic potassium phosphate for the p-nitrophenol and changes the concentration of KOH and H2BO3. The Moore-Sikora ( Moore & Sikora, 2007) method uses MES (N-morpholino ethanesulfonic acid hydrate) and MOPS (3- N- Morpholino, propanesulfonic acid) to replace the p-nitrophenol. In addition, Kissel et al. (2007) have implemented a rapid single addition titration combined with 0.01 M CaCl2 salt pH method for determining lime requirement.OBEJECTIVES Evaluate different LR methodsEvaluate effects of 1:1 and 1:2 water to soil ratiosEvaluate effects of using 0.01 M CaCl2 salt pH Select best method for East Texas SoilsMETHODSSelected 51 soils from a set of 64 soils collected from the region and used in previous studies of LRMeasured soil pH using 1:1 and 1:2 soil to water ratios with and without 0.01 M CaCl2 Determined LR using a series of Ca(OH)2 incubations on each sampleDetermined Standard Lime Requirement (SLR) using Ca(OH)2 incubation data plus Ca(OH)2 titration data from the previous studiesDetermined LR using the following rapid methods:Original Adams-Evans Buffer (AE)Modified Adams-Evans (MAE)Moore-Sikora (M-S)University of Georgia single addition titration (UGA-ST)All three Adams-Evans methods use the relationships and equations developed by Adams and Evans (1962).
Lime Requirements (LR) are expressed in U.S. tons per acre of ECCE (Effective Calcium Carbonate Equivalent) which is pure calcium carbonate that passes a 60 mesh screen. Methods are compared to a Standard Lime Requirement (SLR) which is the mean lime requirement of the titrations and incubations shown in the following graph. The mean SLR for the 51 samples is 0.62 tons ECCE per acre.RESULTSThe UGA-ST method uses a basic equation developed to calculate LR and abbreviated as UGA-F1. A second equation, abbreviated as UGA-F2, adjusts for the difference in LR between the rapid addition of Ca(OH)2 and the LR determined by incubation (Thompson, 2008).Numerous combinations 1:1 and 1:2 soil to water ratios, with and without the use of salt pH were used with each method. A soil pH for use in the method formula was obtained by adding 0.6 pH units to the salt pH. Use of 1:2 ratio pH and salt pH tended to improve estimates of lime requirement.The original A-E method had an R2 value of 0.85 when regressed on the SLR and overestimated LR approximately 224 kg ha-1. The Moore-Sikora had an R2 value of 0.81 and over estimated LR approximately 300 kg ha-1. The UGA had an R2 value of 0.74 and under estimated LR approximately 400 kg ha-1. Using Thompsons adjustment formula came very close to the SLR mean but the R2 was not improved.The MAE had an R2 value of 0.67 and over estimated LR approximately 500 kg ha-1. The Moore-Sikora requires the use of two expensive chemicals. A cost comparison using current prices for MOPS and MES, current lab procedure at the SFASU Soil, Plant and Water Analysis Laboratory and current disposal charges for paranitrophenol. The results indicate that the MOPS plus MES cost about $117 per 1000 soil samples while disposal of paranitrophenol costs between $63 and $97 per 1000 samples. The Material Safety Data Sheet (MSDS) from Mallinckrodt Baker (2009) indicates that the half life of the paranitrophenol is less than one day in soil. With further study, incubation of the soil with A-E buffer may provide an even less expensive method of disposal.CONCLUSIONBased on this work, the original Adams-Evans method is superior to the other methods tested in predicting LR on East Texas Soils. In addition, the cost of disposing of the paranitrophenol is somewhat less than using the expensive chemical in the Moore-Sikora method.LITERATUREAdams, F. and C.E. Evans. 1962. A rapid method for measuring lime requirement of yellow podzolic soils. Soil Sci. Soc. of Amer. J. 36:355-337.Huluka, G. 2005. A modification to the Adams-Evans soil buffer determination solution. Comm. in Soil and Plant Anal. 36:2005-2014.Huluka, G. 2007. A modification to the Adams-Evans soil buffer solution. http://www.clemson.edu/agsrvlb/sera6/publications1.htmKissel, D.E., R.A. Isaac, R. Hitchkock,. L.S. Sonon, and P.V. Vendrell. 2007. Implementation of soil lime requirement by a single addition titration method. Soil Sci. and Pl. Anal J. 38:1341-1352.Mallinckrodt Baker, Inc., 2009. Material Safety Data Sheet for p-nitrophenol, CAS No.:100-02-07,5 May 2009. http://www.jtbaker.com/msds/englishhtml/n6040.htmMoore, K.P. and F.J. Sikora. 2007. Replacing Adams-Evans with Moore-Sikora buffer for determining lime requirement of soil http://www.clemson.edu/agsrvlb/sera6/publications1.htmThompson, J. 2008. Reaction equilibration from single-addition base titration for lime requirement. Personal communication, M.S. Thesis, University of Georgia.
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Titration vs Incubation
Incubations
Titrations
Standard Lime Requirement, SLR (tons ECCE/acre)
Lime Requirement (tons ECCE/acre)
Data
University of Georgia 2-1 MethodUniversity of Georgia 1-1 MethodUGA Method on Sample sent to Georgia
2:1 H2O pH1:1 Soil Water pHEquivDr. Young's Formulaweighed soilEquivour formulaGeorgia
Shake,Seat & ReadStir,Seat & ReadStir & ReadShake,Seat & ReadStir,Seat & ReadStir & Read0.01M CaCl2 pHA-E Buffer pHA-E BufferModified A-EModiied A-EMooore,Sikora bufferpH1pH2Water pHLBCLime (lbs/acreJohn's formulaLBCLime (lbs/acre)Lime(tons/acre)pH1pH2Equiv. Water pHLBCLime (tons/acreJohn's Formulasoil wt (g)LBCLime(tons/acre)John's FormulapH1pH2soil wt(g)Water pHLBCLR(tons/acre)Data
12121211223312121212Titrations
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R0025.705.665.685.505.525.595.515.445.465.465.525.445.494.814.917.777.797.357.567.737.74.847.395.441850.310.400.00018546150.314.965.9685.562350.360.4782290.350.460.514.946.5122.95.541550.240.27
R0035.305.45.355.335.35.285.275.345.345.235.285.235.274.534.607.847.827.777.757.817.774.607.845.201460.280.380.00014595540.284.656.018.75.251730.320.448.71550.290.390.984.716.7823.35.311170.210.23
R0045.265.345.305.225.195.185.175.165.105.095.135.145.134.554.617.637.677.397.327.597.584.636.605.232400.450.660.00023998970.454.655.477.15.252870.530.807.13150.580.900.67
R0055.035.055.044.934.954.874.904.874.874.764.864.824.784.194.237.717.697.517.437.67.594.276.334.872290.510.800.000229410230.514.194.977.44.793010.701.167.43180.731.251.024.225.6421.54.821710.390.46
R0065.255.165.215.255.105.185.115.155.255.015.084.995.054.424.467.657.687.537.587.627.634.396.414.992340.490.760.00023409870.494.465.177.55.063310.681.107.53450.701.160.804.585.9723.05.181740.340.37
R0075.425.385.405.425.295.335.285.25.254.145.165.235.134.514.577.527.537.317.217.427.444.586.255.182830.540.830.000283010870.544.565.308.15.163170.620.978.13060.590.931.204.565.6324.35.162270.440.46
R0085.535.55.525.415.365.405.355.355.325.255.275.385.234.74.747.657.707.257.277.577.644.756.775.352340.410.580.00023408190.414.755.507.65.353130.550.827.63220.560.851.064.835.9722.75.432120.360.40
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R0105.175.155.165.745.135.075.164.125.305.024.995.045.004.484.567.777.787.577.737.797.775.237.305.832280.290.330.00022835800.294.525.878.55.121740.340.498.51600.320.440.694.576.6721.35.171150.220.27
R0115.405.265.335.305.335.195.305.215.255.335.225.245.254.624.567.787.747.447.537.657.724.726.915.322160.380.540.00021587680.384.665.518.15.262760.510.768.12670.490.730.274.616.1025.25.211620.310.31
R0124.504.584.544.494.484.454.474.384.405.374.385.334.403.963.917.157.206.866.777.077.123.934.764.535691.463.080.000569529271.463.934.288.14.536711.733.878.16471.663.683.094.084.5418.44.685321.291.76
R0136.025.935.985.925.885.955.925.855.755.915.905.895.935.385.367.787.837.537.607.777.795.417.756.012020.220.210.00020204400.225.436.327.56.032640.280.277.52750.290.290.485.467.2222.16.061370.140.16
4.045.0521.34.642400.590.70
R0154.634.744.694.554.624.564.614.544.464.534.474.564.493.953.887.707.657.197.347.567.614.026.124.622250.560.900.000225111160.563.984.697.94.583310.831.477.93270.821.451.20
R0164.845.014.934.824.954.814.854.785.984.824.754.854.804.324.227.537.567.397.387.567.524.305.944.902880.631.030.000288212680.634.245.027.64.843010.681.137.63100.701.171.074.285.4620.74.882060.460.56
R0176.286.376.336.236.216.266.226.096.126.206.186.256.185.685.657.797.787.377.517.747.765.717.516.312630.210.110.00026264150.215.766.467.66.363360.250.117.63450.260.110.325.817.0120.26.412020.140.18
R0186.036.036.035.985.916.015.915.865.845.835.825.835.805.405.457.727.727.597.607.727.765.457.386.052450.260.240.00024495140.265.546.308.26.143090.300.258.22950.280.240.525.446.7621.96.041830.190.22
R0195.905.885.895.785.855.785.795.765.635.685.735.745.785.135.067.727.747.327.507.747.764.856.615.452690.440.620.00026868860.445.176.018.25.772800.370.458.22660.350.430.425.276.6322.75.871790.220.24
R0205.515.475.495.415.455.385.365.415.575.375.365.425.354.914.847.457.447.157.137.427.444.815.835.414630.781.290.000463415660.784.865.246.95.466181.011.826.97001.152.171.204.915.6220.15.513430.550.68
R0215.435.535.485.335.375.375.395.325.295.265.255.285.274.734.817.487.517.217.227.367.443.946.214.542080.530.850.000208210660.534.775.417.85.373670.640.997.83680.640.990.824.905.7923.95.502730.440.46
R0224.564.664.614.514.584.504.534.534.554.424.394.544.483.883.947.477.527.167.427.437.384.205.474.803720.861.510.000372217120.863.944.717.44.543050.781.367.43220.821.450.903.944.9423.54.542420.620.66
R0234.744.864.804.704.784.704.754.794.784.654.604.704.604.204.247.537.557.287.237.57.514.205.914.802760.641.040.000276412710.644.164.937.84.763050.711.207.83060.721.210.824.035.1121.64.632240.550.64
R0245.555.595.575.485.485.495.525.515.475.315.405.485.384.854.827.747.767.707.697.767.774.817.095.412070.350.470.00020737010.354.835.958.35.432100.350.478.31970.330.440.584.215.2622.14.812290.530.60
R0255.685.735.715.685.735.715.705.675.635.535.715.655.685.085.027.687.747.427.497.677.645.136.725.732970.410.520.00029738150.415.026.077.85.622240.330.427.82240.330.421.124.906.6321.35.501400.220.27
R0266.266.36.285.316.266.336.276.26.176.176.286.236.295.645.737.897.917.847.817.927.895.748.546.341690.130.050.00016882570.135.747.149.26.341680.130.059.21430.110.050.085.086.4220.65.681800.260.31
R0275.475.545.515.445.415.565.535.465.385.395.365.275.355.175.257.427.407.277.237.347.375.286.555.883720.450.550.00037229080.455.215.707.25.814790.620.857.25200.670.951.155.777.9623.56.371110.080.09
R0285.925.975.955.845.745.875.795.725.725.665.575.695.605.215.257.547.536.776.747.357.375.286.805.883110.380.440.00031107590.383.694.067.44.296351.784.017.46701.884.330.575.296.2020.05.892660.320.41
R0294.674.714.694.604.634.544.584.524.504.494.464.504.473.663.767.387.447.127.077.297.313.704.484.306061.703.740.000606033931.703.754.197.34.355341.473.087.35711.573.372.505.316.3220.85.912410.290.35
R0305.875.845.865.865.755.905.865.515.645.645.735.784.635.425.527.587.637.397.357.517.545.576.766.173970.370.320.00039727390.375.526.147.16.123790.370.357.14170.410.390.913.764.3520.74.364101.121.36
R0314.854.884.874.604.674.694.684.614.674.574.564.574.573.974.057.587.607.547.547.547.544.015.954.612440.610.990.000243612130.613.884.898.84.482330.611.008.82070.540.871.255.626.4721.26.222850.250.30
R0324.934.934.934.874.874.934.924.814.804.784.874.834.874.624.657.457.485.795.657.317.274.665.775.264260.781.310.000425815670.784.715.196.25.314890.881.516.26171.102.081.024.054.9226.54.652780.680.65
R0335.625.645.635.605.565.635.635.575.575.485.485.515.495.035.087.807.847.797.777.857.845.107.515.701960.270.320.00019615490.275.016.538.15.611550.230.278.11490.220.260.664.745.4717.65.343290.580.83
R0345.885.955.925.835.845.915.885.785.785.755.755.745.745.255.337.457.527.397.367.467.495.356.885.953090.360.390.00030897110.365.046.288.25.641890.280.348.21810.260.320.625.157.0121.85.751300.180.20
R0356.166.176.176.156.136.146.096.096.096.056.056.066.095.425.457.787.837.757.727.817.825.487.486.082360.240.210.00023634820.245.406.478.362200.240.238.32070.230.220.025.306.5024.35.902010.240.26
R0365.805.865.835.775.755.765.765.695.695.705.705.715.685.275.287.657.707.387.367.567.615.356.825.953220.370.410.00032157400.375.475.987.36.074610.470.507.34930.510.550.585.537.0923.66.131550.150.16
R0375.265.245.255.255.215.215.175.25.205.175.175.225.134.624.697.627.667.497.417.597.604.606.025.203330.631.000.000332912650.635.336.027.35.933400.400.457.33640.430.490.415.406.2322.86.002910.320.35
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R0554.604.604.604.554.484.494.364.374.374.344.344.324.323.93.887.057.026.977.457.077.213.874.994.474221.112.120.000422022201.113.774.467.54.373400.931.697.53550.971.782.83
R0564.244.304.274.294.084.174.044.044.043.993.994.103.953.663.637.317.247.167.207.347.303.554.684.154181.232.430.000418324681.233.684.176.94.284791.352.756.95431.533.252.323.764.6319.34.362800.771.00
R0574.324.384.354.384.304.354.224.234.234.174.174.174.173.683.677.027.037.027.137.047.063.644.724.244381.252.480.000437625031.253.674.297.94.273791.072.037.93751.062.004.123.694.5720.04.292750.770.97
R0585.285.245.265.255.085.255.145.085.085.155.155.125.054.554.607.297.175.996.567.377.244.575.495.175140.991.810.000513819830.994.534.937.25.135871.162.237.26371.262.504.324.715.0620.55.316911.241.52
R0595.045.025.034.924.844.954.864.764.764.674.674.744.684.244.327.177.127.007.017.157.144.234.804.838291.884.450.000829237651.884.275.9574.871400.310.4571560.350.513.584.414.8219.95.015831.221.54
R0606.065.996.035.995.866.055.985.875.875.835.835.835.945.375.457.487.467.337.437.457.445.376.705.973550.400.440.00035548030.405.466.217.66.063130.330.317.63220.330.330.765.566.4720.06.162660.250.32
R0615.154.714.934.624.524.654.504.454.454.414.414.434.483.823.867.407.395.886.407.357.313.874.414.478752.305.850.000875346042.303.844.116.84.448702.315.896.810002.667.246.99
R0624.694.694.694.664.524.664.524.434.434.514.515.574.463.953.987.057.145.896.097.347.323.994.304.5915253.8313.000.001524776543.833.924.156.74.5210212.647.196.711913.079.119.38
R0636.836.786.816.776.496.846.646.76.706.676.676.616.656.136.137.747.777.087.067.727.716.228.136.822470.07-0.170.00024751390.076.227.407.16.821990.06-0.137.12190.06-0.150.374.014.3620.64.616911.722.10
R0646.036.256.146.226.126.236.116.146.146.016.016.096.125.585.647.477.497.257.257.327.405.606.886.203690.330.260.00036936650.335.686.186.96.284700.390.276.95320.440.311.055.786.6520.06.382780.200.25
Mean5.415.425.425.385.335.385.335.274.435.235.245.295.264.734.737.557.577.257.297.527.534.736.355.330.701.390.704.725.547.615.32355.770.681.237.61377.620.731.371.494.805.955.40260.490.480.58
STDEV0.560.550.550.560.600.590.600.580.590.590.580.610.610.590.220.230.480.450.220.220.621.080.62248.330.722.370.001441.840.720.630.830.650.630.551.460.650.641.791.870.590.911.800.590.400.51
Means
2:1 H2O pH1:1 Soil Water pH
Stir 4x & ReadStir,Seat & ReadShake,Seat & ReadStir 4x & ReadStir,Seat & ReadShake,Seat & Read0.01M CaCl2 pHA-E Buffer pHModified A-EMoore-SikoraA-E BufferKCl-AlOrigional A-EOrigional A-E formulaModified A-E Formula
12Mean12Mean12Mean11Mean22mean33Mean1212Mean12MeanLR tons/acreLR (m) A-E
15.755.865.815.785.725.775.755.745.755.745.675.715.65.745.675.725.725.724.945.155.057.657.647.657.317.257.287.567.547.557.62Al3082Mn25761.16
25.705.665.685.505.525.575.595.515.565.445.465.455.465.525.495.445.495.474.714.464.597.777.797.787.357.567.467.737.77.727.70.3785.10.98
35.305.45.355.335.35.335.285.275.295.345.345.345.235.285.265.235.275.254.554.354.457.847.827.837.777.757.767.817.777.797.780.7741.50.53
45.265.345.305.225.195.245.185.175.205.165.105.135.095.135.115.145.135.144.464.464.467.637.677.657.397.327.367.597.587.597.637.9574.71.45
55.035.055.044.934.954.974.874.904.914.874.874.874.764.864.814.824.784.804.184.114.157.717.697.707.517.437.477.67.597.607.652.4432.71.32
65.255.165.215.255.105.195.185.115.165.155.255.205.015.085.054.995.055.024.224.384.307.657.687.677.537.587.567.627.637.637.6917.464.71.04
75.425.385.405.425.295.375.335.285.335.25.255.234.145.164.655.235.135.184.354.354.357.527.537.537.317.217.267.427.447.437.514.809.71.58
85.535.55.525.415.365.435.45.355.395.355.325.345.255.275.265.385.235.314.564.564.567.657.707.687.257.277.267.577.647.617.968.4616.91.48
95.825.785.805.775.675.755.745.675.725.755.665.715.645.665.655.665.655.664.834.924.887.797.807.807.637.687.667.747.777.767.751.9718.80.56
105.175.155.165.745.135.345.075.165.194.125.304.715.024.995.015.0455.024.564.444.507.777.787.787.577.737.657.797.777.787.770.6739.40.83
115.405.265.335.305.335.325.195.305.275.215.255.235.335.225.285.245.255.254.494.534.517.787.747.767.447.537.497.657.727.697.666.6415.41.14
124.504.584.544.494.484.504.454.474.474.384.404.395.374.384.885.334.44.873.733.783.767.157.207.187.087.117.107.077.127.107.132.8129.72.65
136.025.935.985.925.885.935.955.925.935.855.755.805.915.95.915.895.935.915.265.255.267.787.837.817.537.607.577.777.797.787.8111.20212.90.58
144.634.744.694.554.624.624.564.614.604.544.464.504.534.474.504.564.494.533.783.883.837.707.657.687.717.687.707.567.617.597.598.1529.20.85
154.845.014.934.824.954.904.814.854.854.785.985.384.824.754.794.854.84.834.204.284.247.537.567.557.397.387.397.567.527.547.5642.8044.61.60
166.286.376.336.236.216.266.266.226.256.096.126.116.26.186.196.256.186.225.495.575.537.797.787.797.377.517.447.747.767.757.7615.8081.90.30
176.036.036.035.985.915.976.015.915.965.865.845.855.835.825.835.835.85.825.205.365.287.727.727.727.727.607.667.727.767.747.740.5324.10.42
185.905.885.895.785.855.845.785.795.805.765.635.705.685.735.715.745.785.764.895.004.957.727.747.737.327.507.417.747.767.757.761.0418.50.87
195.515.475.495.415.455.455.385.365.405.415.575.495.375.365.375.425.355.394.554.724.647.457.447.457.157.137.147.427.447.437.531.1144.31.75
205.435.565.505.335.375.405.375.395.395.325.295.315.265.255.265.285.275.284.584.714.657.487.517.507.217.227.227.367.447.407.445.07105.61.59
214.564.664.614.514.584.574.504.534.534.534.554.544.424.394.414.544.484.513.753.903.837.477.527.507.507.427.467.437.387.417.471.4662.41.55
224.744.864.804.704.784.764.704.754.744.794.784.794.654.604.634.704.64.654.004.274.147.537.557.547.287.237.267.57.517.517.5731.6216.42.01
235.555.595.575.485.485.515.495.525.515.515.475.495.315.45.365.485.385.434.634.694.667.747.767.757.707.697.707.767.777.777.7912.7360.20.59
245.685.735.715.685.735.715.715.705.715.675.635.655.535.715.625.655.685.674.764.874.827.687.747.717.427.497.467.677.647.667.692.1249.60.96
256.266.36.285.316.265.956.336.276.186.26.176.196.176.286.236.236.296.265.454.635.047.897.917.907.847.817.837.927.897.917.923.50131.20.12
265.475.545.515.445.415.455.565.535.515.465.385.425.395.365.385.275.355.315.015.155.087.427.407.417.277.237.257.347.377.367.490.5316.91.51
275.925.975.955.845.745.845.875.795.832x5.725.725.725.665.575.625.695.65.655.045.135.097.547.537.547.437.407.427.357.377.367.540.68110.3
284.674.714.694.604.634.644.544.584.594.524.504.514.494.464.484.54.474.493.463.623.547.387.447.417.127.077.107.297.317.307.390.7569.82.53
295.875.845.865.865.755.825.95.865.865.515.645.585.645.735.695.784.635.215.195.375.287.587.637.617.397.357.377.517.547.537.58214.6032.00.96
304.854.884.874.604.674.714.694.684.694.614.674.644.574.564.574.574.574.573.843.903.877.587.607.597.547.547.547.547.547.547.530.42110.31.22
314.934.934.934.874.874.894.934.924.914.814.804.814.784.874.834.834.874.854.424.564.497.457.487.477.137.117.127.317.277.297.4375.275.22.28
325.625.645.635.605.565.605.635.635.625.575.575.575.485.485.485.515.495.504.804.984.897.807.847.827.797.777.787.857.847.857.884.11321.10.41
335.885.955.925.835.845.865.915.885.885.785.785.785.755.755.755.745.745.745.195.265.237.457.527.497.397.367.387.467.497.487.490.9958.70.89
346.166.176.176.156.136.156.146.096.136.096.096.096.056.056.056.066.096.085.205.425.317.787.837.817.757.727.747.817.827.827.790.2423.60.25
355.805.865.835.775.755.785.765.765.775.695.695.695.75.75.705.715.685.705.105.225.167.657.707.687.387.367.377.567.617.597.660.6822.30.99
365.265.245.255.255.215.245.215.175.215.25.205.205.175.175.175.225.135.184.424.474.457.627.667.647.497.417.457.597.607.607.630.4594.81.26
375.405.525.465.495.525.495.535.545.525.325.325.325.365.365.365.415.415.414.854.904.887.457.517.487.107.147.127.357.447.407.483.0068.11.82
385.385.65.495.505.535.515.485.455.485.355.355.355.45.45.404.455.424.944.644.734.697.477.527.507.217.187.207.407.427.417.440.44306.41.64
394.914.834.874.764.644.764.784.634.724.674.674.674.644.644.644.685.645.163.994.104.057.377.397.387.117.157.137.307.377.347.412.84212.22.30
406.005.965.986.005.955.986.025.975.995.835.835.834.894.894.895.915.855.885.185.175.187.887.927.907.787.897.847.907.897.907.8911.30130.00.22
415.305.325.315.385.395.365.405.375.385.255.255.255.35.35.305.315.225.274.434.624.537.657.697.677.507.557.537.677.677.677.650.5218.61.06
424.744.774.764.694.614.694.704.584.663x4.544.544.544.484.484.484.54.494.503.583.643.617.037.027.037.067.167.117.037.077.057.322.5178.6
435.285.395.345.355.315.335.335.305.325.175.175.175.245.245.245.285.195.244.264.574.427.717.747.737.667.537.607.707.657.687.7768.5026.60.89
445.765.675.725.755.685.725.795.715.745.515.515.515.535.535.535.585.615.604.895.034.967.647.647.647.437.417.427.607.547.577.612.7014.91.01
455.975.95.945.985.965.966.005.975.985.815.815.815.835.835.835.825.875.855.085.205.147.797.827.817.617.707.667.817.757.787.760.58274.60.48
465.465.385.425.435.405.425.455.335.405.385.385.385.255.255.255.265.35.284.344.474.417.717.737.727.587.497.547.697.677.687.70.3961.20.98
475.695.635.665.65.515.595.615.485.565.515.515.515.425.425.425.425.485.454.694.704.707.537.577.557.517.407.467.517.517.517.563.7855.00.99
485.735.565.655.785.665.705.825.715.745.525.525.525.555.555.555.65.635.624.834.734.787.737.767.757.717.737.727.747.757.757.731.8994.40.51
495.205.205.205.205.185.195.115.115.145.095.095.095.075.075.074.995.015.004.324.384.357.587.577.587.577.527.557.567.547.557.561.19130.01.07
504.554.64.585.584.494.884.544.434.624.384.384.384.364.364.364.444.554.503.733.843.797.087.067.077.327.357.347.037.027.037.086.0832.31.93
516.006.046.026.015.945.995.995.985.995.835.835.835.835.835.835.925.995.965.105.265.187.707.747.727.637.617.627.77.667.687.63122.1057.10.47
526.326.656.496.156.176.276.66.246.372x6.46.406.406.356.356.356.376.546.465.926.005.967.557.587.577.297.337.317.57.497.507.560.64129.9
534.974.984.985.024.954.984.954.864.934.874.874.874.854.854.854.814.74.764.024.144.087.337.317.327.327.277.307.47.367.387.350.1826.61.80
544.604.604.604.554.484.544.494.364.462x4.374.374.374.344.344.344.324.324.325.543.804.677.057.027.047.417.457.437.077.217.147.1541.1321.21.64
554.244.304.274.294.084.214.174.044.144.044.044.043.993.993.994.13.954.033.443.483.467.317.247.287.167.207.187.347.307.327.3959.1338.52.56
564.324.384.354.384.304.344.354.224.304.234.234.234.174.174.174.174.174.173.473.543.517.027.037.037.027.137.087.047.067.057.1162.2531.12.89
575.285.245.265.255.085.205.255.145.203x5.085.085.085.155.155.155.125.055.094.333.493.917.297.177.237.147.097.127.377.247.317.3889.2118.5
585.045.025.034.924.844.934.954.864.914.764.764.764.674.674.674.744.684.714.114.194.157.177.127.157.007.017.017.157.147.157.2212.5944.22.49
596.066.086.075.995.865.976.055.986.005.875.875.875.835.835.835.835.945.895.225.405.317.487.467.477.337.437.387.457.447.457.4274.342.40.71
605.154.714.934.624.524.694.654.504.612x4.454.454.454.414.414.414.434.484.463.643.743.697.407.397.407.407.437.427.357.317.337.440.5228.3
614.694.694.694.664.524.624.664.524.602x4.434.434.434.514.514.515.574.465.023.773.853.817.057.147.107.077.107.097.347.327.337.15374.709.2
626.836.836.836.776.496.706.846.646.736.76.706.706.676.676.676.616.656.635.936.136.037.747.777.767.087.067.077.727.717.727.73679.6013.3
636.036.256.146.226.126.166.236.116.176.146.146.146.016.016.016.096.126.115.515.535.527.477.497.487.257.257.257.327.407.367.440.8510.30.75
Mean5.415.435.425.385.335.385.385.335.365.265.305.285.235.245.235.295.265.284.584.614.597.577.567.407.417.407.527.537.537.570.543372.63
STDEV0.560.570.550.560.550.600.590.580.220.220.590.590.580.580.610.570.610.630.620.230.230.220.220.220.220.220.22
115.83
225.45
335.34
445.13
554.87
665.20
775.23
885.34
995.71
10104.71
11115.23
12124.39
13135.80
14154.50
15165.38
16176.11
17185.85
18195.70
19205.49
20215.31
21224.54
22234.79
23245.49
24255.65
25266.19
26275.42
27285.72
29305.58
30314.64
31324.81
32335.57
33356.09
34365.69
35375.20
36385.32
37395.35
38404.67
39415.83
40425.25
41445.17
42455.51
43465.81
45485.51
46495.52
47505.09
48525.83
49544.87
50554.37
51564.04
52605.87
53646.14
115.835.81
225.455.68
335.345.35
445.135.30
554.875.04
665.205.21
775.235.40
885.345.52
995.715.80
10104.715.16
11115.235.33
12124.394.54
13135.805.98
14154.504.69
15165.384.93
16176.116.33
17185.856.03
18195.705.89
19205.495.49
20215.315.50
21224.544.61
22234.794.80
23245.495.57
24255.655.71
25266.196.28
26275.425.51
27285.725.95
28305.585.86
29314.644.87
30324.814.93
31335.575.63
32356.096.17
33365.695.83
34375.205.25
35385.325.46
36395.355.49
37404.674.87
38415.835.98
39425.255.31
40445.175.34
41455.515.72
42465.815.94
43485.515.66
44495.525.65
45505.095.20
46525.836.02
47544.874.98
48554.374.60
49564.044.27
50605.876.07
51646.146.14
51 samples
Water pHSalt pHBuffer pHLime Requirement Comparisons on all Methods in tons ECCE/acre
AllenOjegaHenryAllenOjegaHenryHenryModified A-E (1)Modified A-E (2)Henry'sAL/OjAllen'sOjega's
2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2:1 Salt pH1-1 Salt pHAdjusted Salt pHA-E buffer pHA-E Buffer pHA-E Buffer pHA-E(m)Moore-SikoraAllen 2-1Ojega 2-1Ojega 1-1Orig. A-E 2-1Orig. A-E 1-12-1 LR1-1 LR2-1 LR1-1 LRMoore-Sikora 2-1Moore-Sikora 1-1UGA 2-1John's form. 2-1UGA 1-1John's form. 1-1Georgia Data 1-1IncubationsTitrationsTitrationsTitrations
116.055.905.995.835.835.675.185.295.787.557.517.657.587.550.980.931.120.570.641.161.301.301.450.720.810.360.400.400.470.350.600.770.770.84
226.015.955.835.455.455.494.864.965.467.657.667.787.727.720.720.810.950.390.450.981.111.091.230.510.580.310.690.360.470.240.460.510.510.62
335.595.465.455.345.345.264.574.655.177.757.717.837.777.790.780.900.990.370.390.530.550.580.610.460.480.280.630.320.440.213.210.830.830.83
445.525.435.325.135.135.114.584.655.187.567.567.657.617.591.391.471.640.780.851.451.571.611.750.931.010.451.140.530.800.860.670.670.92
555.215.045.024.874.874.814.214.194.817.587.557.707.637.601.571.701.920.750.811.321.431.481.611.011.090.511.380.701.160.391.201.021.021.03
665.425.305.235.205.205.054.444.465.047.637.617.677.647.631.241.361.490.780.831.041.111.161.240.880.930.491.310.681.100.341.020.800.800.77
775.655.475.505.235.234.654.544.565.147.457.387.537.457.431.701.902.251.011.341.582.091.762.251.221.610.541.470.620.970.443.081.201.201.41
885.905.765.665.345.345.264.724.755.327.687.617.687.647.610.801.071.350.650.741.481.691.651.880.790.900.411.000.550.820.360.711.061.061.26
996.045.965.825.715.715.654.985.015.587.697.657.807.727.760.630.831.020.330.380.560.630.630.710.400.450.320.690.390.510.270.650.750.750.84
10105.435.335.244.714.715.014.524.525.127.737.707.787.747.780.901.031.150.540.570.830.880.930.990.520.560.290.560.340.490.220.680.690.690.69
11116.056.015.625.235.235.284.594.665.197.697.617.767.697.690.591.071.230.530.541.141.171.271.300.700.710.380.930.510.760.310.590.270.270.32
12125.414.754.674.394.394.883.943.934.547.137.147.187.167.103.583.646.522.422.182.652.392.712.782.652.391.465.821.733.871.292.743.093.093.66
13136.566.666.305.805.805.915.375.435.977.827.737.817.777.78-0.170.260.190.260.280.580.630.650.710.290.320.220.350.280.270.140.540.050.050.33
14155.034.874.764.504.504.503.923.984.527.597.517.687.597.591.632.002.140.911.240.851.670.911.871.791.230.561.550.831.470.590.921.201.201.33
15165.235.255.055.385.384.794.274.244.877.597.527.557.537.541.441.791.951.180.191.600.491.810.571.081.250.631.820.681.130.461.901.071.071.35
16176.626.546.426.116.116.195.675.766.277.687.657.797.727.75-0.070.220.290.120.440.300.540.350.600.250.220.210.190.250.110.140.440.320.320.51
17186.326.256.155.855.855.835.435.546.037.737.667.727.697.740.300.480.730.340.470.421.040.471.160.310.410.260.410.300.250.190.400.520.520.67
18196.196.142.935.705.705.715.105.175.707.767.657.737.697.750.360.740.820.401.210.871.870.982.080.380.440.441.090.370.450.221.590.420.420.41
19205.795.705.615.495.495.374.884.865.487.537.447.457.447.431.241.581.791.131.161.751.801.952.000.511.240.782.381.011.820.550.911.201.201.21
20215.735.595.595.315.315.264.774.775.377.427.377.507.437.401.661.902.431.021.571.591.681.771.631.161.370.531.470.640.990.441.180.820.821.50
21225.255.294.984.544.544.413.913.944.517.587.537.507.517.411.421.801.921.451.311.552.121.612.251.721.850.862.730.781.360.621.780.900.901.07
22235.465.375.104.794.794.634.224.164.827.637.477.547.517.511.201.702.101.240.552.010.672.230.741.611.410.641.830.711.200.551.700.820.821.01
23245.945.865.715.495.495.364.844.835.447.757.667.757.717.770.570.891.020.480.540.591.020.661.140.960.510.350.810.350.470.530.610.580.580.86
24255.585.495.565.655.655.625.055.025.657.627.537.717.627.661.161.381.670.510.080.960.141.070.160.410.650.410.910.330.420.220.461.121.120.65
25266.716.576.516.196.196.235.695.746.297.897.797.907.857.91-0.040.000.000.071.280.121.620.131.800.230.080.130.090.130.050.260.160.080.080.14
26275.595.485.555.425.425.385.215.215.817.337.367.417.397.362.051.882.121.190.871.511.101.681.230.191.400.451.000.620.850.080.671.151.151.09
27286.085.866.095.725.725.625.233.695.837.547.457.547.497.361.050.921.290.641.771.622.711.822.730.891.200.380.781.784.010.320.590.570.571.27
28306.015.975.995.585.585.695.475.526.077.547.537.617.577.530.920.891.020.601.190.961.341.091.391.070.850.370.580.370.351.120.540.910.911.09
29315.205.124.854.644.644.574.013.884.617.487.527.597.567.541.891.921.971.091.431.222.361.382.651.261.340.611.730.611.000.251.151.251.251.32
30325.635.305.314.814.814.834.644.715.247.467.457.477.467.291.821.851.931.390.372.280.452.580.501.191.900.782.410.881.510.680.981.021.021.02
31335.695.615.675.575.575.485.065.015.667.807.737.827.787.850.570.720.920.330.870.411.060.461.191.320.320.270.560.230.270.580.240.660.660.74
32356.696.646.416.096.096.055.445.406.047.807.737.817.777.82-0.170.120.230.180.570.251.110.291.240.490.220.240.370.240.230.240.590.020.020.26
33366.126.036.025.695.695.705.285.475.887.657.587.687.637.590.640.800.970.510.850.991.301.111.450.290.730.370.720.470.500.151.050.580.580.63
34375.765.735.545.205.205.174.665.335.267.637.577.647.617.600.951.261.420.831.131.261.921.402.130.950.960.631.790.400.450.321.420.410.410.71
35385.415.275.425.325.325.365.095.305.697.367.317.487.407.402.182.182.291.081.081.821.722.031.910.841.320.611.590.881.340.351.251.781.781.15
36395.605.425.545.355.355.404.904.495.507.377.357.507.427.412.001.912.141.031.761.642.471.822.621.231.260.862.720.580.900.620.711.171.171.11
37405.315.185.034.674.674.644.244.264.847.527.417.387.407.341.702.202.391.640.262.300.432.600.501.561.891.043.590.991.830.681.461.101.101.28
38416.486.386.215.835.834.895.155.215.757.897.797.907.857.900.060.270.350.130.740.221.070.251.180.870.280.250.570.160.160.110.390.070.070.22
39425.635.415.435.255.255.304.754.795.357.627.597.677.637.671.211.301.420.742.921.062.661.182.680.230.740.380.910.390.530.280.850.820.820.67
40445.855.755.575.175.175.244.674.715.277.687.657.737.697.680.811.011.250.610.710.891.150.991.282.100.750.451.130.370.510.300.550.530.530.72
41456.005.675.735.515.515.535.105.115.707.557.557.647.607.571.221.171.390.630.311.010.541.130.610.570.850.330.700.350.440.390.220.650.650.93
42466.416.126.055.815.815.835.255.325.857.757.717.817.767.780.390.520.720.270.640.481.070.541.190.600.350.260.460.210.210.160.480.360.360.36
43485.915.755.675.515.515.424.774.785.377.567.537.557.547.511.121.261.450.820.500.990.551.110.610.581.040.541.410.490.710.383.290.620.620.96
44495.815.735.765.525.525.555.235.265.837.737.667.757.707.750.700.861.970.471.050.511.120.581.250.900.500.260.490.260.280.130.871.051.050.51
45505.655.575.455.095.095.074.524.475.127.597.527.587.557.551.191.491.641.002.911.072.081.192.000.601.110.611.740.570.890.411.251.231.231.20
46525.835.835.835.835.345.355.947.587.727.657.681.011.210.350.210.470.330.540.381.210.500.350.660.330.360.200.260.640.64
47545.274.874.874.854.214.264.817.417.327.377.382.002.251.733.021.801.782.021.721.291.650.682.000.681.130.413.531.801.80
48554.944.374.374.343.893.774.497.217.047.127.143.053.242.772.273.282.563.402.471.782.691.113.890.931.694.442.832.83
49564.704.044.043.993.653.684.257.467.287.377.322.252.532.273.052.562.892.452.792.692.131.234.451.352.750.772.062.322.32
50606.055.875.875.835.415.466.017.357.477.417.451.162.290.611.870.711.810.811.760.980.870.400.800.330.310.250.630.760.76
51646.506.146.146.015.615.686.217.367.487.427.360.001.210.521.020.751.020.861.130.280.810.330.480.390.270.201.051.051.05
5.815.695.545.355.355.304.824.825.427.617.567.657.607.601.061.241.500.740.931.121.321.241.440.870.920.481.270.550.860.381.040.820.820.92
All Results
Water pHSalt pHBuffer pHLime Requirement Comparisons on all Methods in tons ECCE/acre
AllenOjegaHenryAllenOjegaHenryHenryModified A-E (1)Modified A-E (2)Henry'sAL/OjAllen'sOjega's
2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2:1 Salt pH1-1 Salt pHAdjusted Salt pHA-E buffer pHA-E Buffer pHA-E Buffer pHA-E(m)Moore-SikoraAllen 2-1Ojega 2-1Ojega 1-1Orig. A-E 2-1Orig. A-E 1-12-1 LR1-1 LR2-1 LR1-1 LRMoore-Sikora 2-1Moore-Sikora 1-1UGA 2-1John's form. 2-1UGA 1-1John's form. 1-1Georgia Data 1-1IncubationsTitrationsTitrationsTitrations
16.055.905.995.835.775.675.185.295.787.557.517.657.587.550.980.931.120.570.641.161.301.301.450.720.810.360.400.400.470.350.600.770.770.84
26.015.955.835.455.575.494.864.965.467.657.667.787.727.720.720.810.950.390.450.981.111.091.230.510.580.310.690.360.470.240.460.510.510.62
35.595.465.455.345.335.264.574.655.177.757.717.837.777.790.780.900.990.370.390.530.550.580.610.460.480.280.630.320.440.213.210.830.830.83
45.525.435.325.135.245.114.584.655.187.567.567.657.617.591.391.471.640.780.851.451.571.611.750.931.010.451.140.530.800.860.670.670.92
55.215.045.024.874.974.814.214.194.817.587.557.707.637.601.571.701.920.750.811.321.431.481.611.011.090.511.380.701.160.391.201.021.021.03
65.425.305.235.205.195.054.444.465.047.637.617.677.647.631.241.361.490.780.831.041.111.161.240.880.930.491.310.681.100.341.020.800.800.77
75.655.475.505.235.374.654.544.565.147.457.387.537.457.431.701.902.251.011.341.582.091.762.251.221.610.541.470.620.970.443.081.201.201.41
85.905.765.665.345.435.264.724.755.327.687.617.687.647.610.801.071.350.650.741.481.691.651.880.790.900.411.000.550.820.360.711.061.061.26
96.045.965.825.715.755.654.985.015.587.697.657.807.727.760.630.831.020.330.380.560.630.630.710.400.450.320.690.390.510.270.650.750.750.84
105.435.335.244.715.345.014.524.525.127.737.707.787.747.780.901.031.150.540.570.830.880.930.990.520.560.290.560.340.490.220.680.690.690.69
116.056.015.625.235.325.284.594.665.197.697.617.767.697.690.591.071.230.530.541.141.171.271.300.700.710.380.930.510.760.310.590.270.270.32
125.414.754.674.394.504.883.943.934.547.137.147.187.167.103.583.646.522.422.182.652.392.712.782.652.391.465.821.733.871.292.743.093.093.66
136.566.666.305.805.935.915.375.435.977.827.737.817.777.78-0.170.260.190.260.280.580.630.650.710.290.320.220.350.280.270.140.540.050.050.33
155.034.874.764.504.624.503.923.984.527.597.517.687.597.591.632.002.140.911.240.851.670.911.871.791.230.561.550.831.470.590.921.201.201.33
165.235.255.055.384.904.794.274.244.877.597.527.557.537.541.441.791.951.180.191.600.491.810.571.081.250.631.820.681.130.461.901.071.071.35
176.626.546.426.116.266.195.675.766.277.687.657.797.727.75-0.070.220.290.120.440.300.540.350.600.250.220.210.190.250.110.140.440.320.320.51
186.326.256.155.855.975.835.435.546.037.737.667.727.697.740.300.480.730.340.470.421.040.471.160.310.410.260.410.300.250.190.400.520.520.67
196.196.142.935.705.845.715.105.175.707.767.657.737.697.750.360.740.820.401.210.871.870.982.080.380.440.441.090.370.450.221.590.420.420.41
205.795.705.615.495.455.374.884.865.487.537.447.457.447.431.241.581.791.131.161.751.801.952.000.511.240.782.381.011.820.550.911.201.201.21
215.735.595.595.315.405.264.774.775.377.427.377.507.437.401.661.902.431.021.571.591.681.771.631.161.370.531.470.640.990.441.180.820.821.50
225.255.294.984.544.574.413.913.944.517.587.537.507.517.411.421.801.921.451.311.552.121.612.251.721.850.862.730.781.360.621.780.900.901.07
235.465.375.104.794.764.634.224.164.827.637.477.547.517.511.201.702.101.240.552.010.672.230.741.611.410.641.830.711.200.551.700.820.821.01
245.945.865.715.495.515.364.844.835.447.757.667.757.717.770.570.891.020.480.540.591.020.661.140.960.510.350.810.350.470.530.610.580.580.86
255.585.495.565.655.715.625.055.025.657.627.537.717.627.661.161.381.670.510.080.960.141.070.160.410.650.410.910.330.420.220.461.121.120.65
266.716.576.516.195.956.235.695.746.297.897.797.907.857.91-0.040.000.000.071.280.121.620.131.800.230.080.130.090.130.050.260.160.080.080.14
275.595.485.555.425.455.385.215.215.817.337.367.417.397.362.051.882.121.190.871.511.101.681.230.191.400.451.000.620.850.080.671.151.151.09
286.085.866.095.725.845.625.233.695.837.547.457.547.497.361.050.921.290.641.771.622.711.822.730.891.200.380.781.784.010.320.590.570.571.27
295.224.904.884.514.644.483.713.754.317.387.377.417.397.302.432.482.971.650.702.531.122.711.901.792.101.707.131.473.080.292.502.503.75
306.015.975.995.585.825.695.475.526.077.547.537.617.577.530.920.891.020.601.190.961.341.091.391.070.850.370.580.370.351.120.540.910.911.09
315.205.124.854.644.714.574.013.884.617.487.527.597.567.541.891.921.971.091.431.222.361.382.651.261.340.611.730.611.000.251.151.251.251.32
325.635.305.314.814.894.834.644.715.247.467.457.477.467.291.821.851.931.390.372.280.452.580.501.191.900.782.410.881.510.680.981.021.021.02
335.695.615.675.575.605.485.065.015.667.807.737.827.787.850.570.720.920.330.870.411.060.461.191.320.320.270.560.230.270.580.240.660.660.74
346.025.975.885.785.865.755.295.045.897.447.467.497.477.481.121.191.400.740.230.890.311.010.360.220.890.360.690.280.340.180.940.620.620.69
356.696.646.416.096.156.055.445.406.047.807.737.817.777.82-0.170.120.230.180.570.251.110.291.240.490.220.240.370.240.230.240.590.020.020.26
366.126.036.025.695.785.705.285.475.887.657.587.687.637.590.640.800.970.510.850.991.301.111.450.290.730.370.720.470.500.151.050.580.580.63
375.765.735.545.205.245.174.665.335.267.637.577.647.617.600.951.261.420.831.131.261.921.402.130.950.960.631.790.400.450.321.420.410.410.71
385.415.275.425.325.495.365.095.305.697.367.317.487.407.402.182.182.291.081.081.821.722.031.910.841.320.611.590.881.340.351.251.781.781.15
395.605.425.545.355.515.404.904.495.507.377.357.507.427.412.001.912.141.031.761.642.471.822.621.231.260.862.720.580.900.620.711.171.171.11
405.315.185.034.674.764.644.244.264.847.527.417.387.407.341.702.202.391.640.262.300.432.600.501.561.891.043.590.991.830.681.461.101.101.28
416.486.386.215.835.984.895.155.215.757.897.797.907.857.900.060.270.350.130.740.221.070.251.180.870.280.250.570.160.160.110.390.070.070.22
425.635.415.435.255.365.304.754.795.357.627.597.677.637.671.211.301.420.742.921.062.661.182.680.230.740.380.910.390.530.280.850.820.820.67
434.724.394.804.544.694.483.763.724.366.046.357.036.697.059.196.687.792.670.637.320.937.981.040.902.843.8526.532.185.341.9912.158.898.899.87
445.855.755.575.175.335.244.674.715.277.687.657.737.697.680.811.011.250.610.710.891.150.991.282.100.750.451.130.370.510.300.550.530.530.72
456.005.675.735.515.725.535.105.115.707.557.557.647.607.571.221.171.390.630.311.010.541.130.610.570.850.330.700.350.440.390.220.650.650.93
466.416.126.055.815.965.835.255.325.857.757.717.817.767.780.390.520.720.270.640.481.070.541.190.600.350.260.460.210.210.160.480.360.360.36
475.535.485.375.385.425.254.614.715.217.697.657.727.697.680.951.141.250.590.950.981.151.091.280.460.730.390.970.300.400.640.640.60
485.915.755.675.515.595.424.774.785.377.567.537.557.547.511.121.261.450.820.500.990.551.110.610.581.040.541.410.490.710.383.290.620.620.96
495.815.735.765.525.705.555.235.265.837.737.667.757.707.750.700.861.970.471.050.511.120.581.250.900.500.260.490.260.280.130.871.051.050.51
505.655.575.455.095.195.074.524.475.127.597.527.587.557.551.191.491.641.002.911.072.081.192.000.601.110.611.740.570.890.411.251.231.231.20
514.914.384.884.363.973.924.577.227.077.157.033.053.292.690.441.930.601.990.671.303.051.274.731.784.051.094.344.34
525.835.835.995.835.345.355.947.587.727.657.681.011.210.350.210.470.330.540.381.210.500.350.660.330.360.200.260.640.64
536.816.406.276.356.036.637.527.577.547.50-1.061.020.021.810.081.870.082.120.020.240.470.560.450.45
545.274.874.984.854.214.264.817.417.327.377.382.002.251.733.021.801.782.021.721.291.650.682.000.681.130.413.531.801.80
554.944.374.544.343.893.774.497.217.047.127.143.053.242.772.273.282.563.402.471.782.691.113.890.931.694.442.832.83
564.704.044.213.993.653.684.257.467.287.377.322.252.532.273.052.562.892.452.792.692.131.234.451.352.750.772.062.322.32
574.934.234.344.173.683.674.287.027.037.027.053.813.953.051.842.892.122.772.362.132.971.254.561.072.030.774.594.124.12
585.855.085.205.154.584.535.186.967.237.107.312.376.463.522.406.062.806.753.002.171.660.993.381.162.231.243.004.324.32
595.164.764.934.674.284.274.887.047.157.097.153.423.892.140.832.490.972.791.101.742.401.888.760.310.451.222.973.583.58
606.055.875.975.835.415.466.017.357.477.417.451.162.290.611.870.711.810.811.760.980.870.400.800.330.310.250.630.760.76
615.124.454.694.413.843.844.447.027.407.217.333.504.333.142.683.042.713.442.761.442.072.3011.602.315.891.726.996.99
625.214.434.624.513.973.924.577.317.107.207.332.403.255.06-0.175.12-0.645.48-0.781.871.983.8327.332.647.199.389.38
636.806.706.706.676.136.226.737.727.767.747.72-0.670.77-0.380.66-1.450.94-1.821.07-1.04-0.200.07-0.300.06-0.13-0.280.370.37
646.506.146.166.015.615.686.217.367.487.427.360.001.210.521.020.751.020.861.130.280.810.330.480.390.270.201.051.051.05
5.785.655.525.335.415.284.744.725.347.577.537.567.527.531.061.351.061.051.461.341.591.461.191.130.702.650.681.220.481.441.051.011.15
1.06
UGA Method
University of Georgia 2-1 MethodUniversity of Georgia 1-1 MethodUGA Method on Sample sent to Georgia
EquivDr. Young's Formulaweighed soilEquivour formulaGeorgia
pH1pH2Water pHLBCLime (lbs/acreJohn's formulaLBCLime (lbs/acre)Lime(tons/acre)pH1pH2Equiv. Water pHLBCLime (tons/acreJohn's Formulasoil wt (g)LBCLime(tons/acre)John's FormulapH1pH2soil wt(g)Water pHLBCLR(tons/acre)Data
TitrationsTitrations
15.316.885.913010.360.400.00030117170.365.296.0085.893310.400.4783230.390.450.775.306.1225.55.902900.350.350.77
24.847.395.441850.310.400.00018546150.314.965.9685.562350.360.4782290.350.460.514.946.5122.95.541700.260.270.51
34.607.845.201460.280.380.00014595540.284.656.018.75.251730.320.448.71550.290.390.984.716.7823.35.311260.230.230.98
44.636.605.232400.450.660.00023998970.454.655.477.15.252870.530.807.13150.580.900.670.67
54.276.334.872290.510.800.000229410230.514.194.977.44.793010.701.167.43180.731.251.024.225.6421.54.821990.450.461.02
64.396.414.992340.490.760.00023409870.494.465.177.55.063310.681.107.53450.701.160.804.585.9723.05.181900.370.370.80
74.586.255.182830.540.830.000283010870.544.565.308.15.163170.620.978.13060.590.931.204.565.6324.35.162350.460.461.20
84.756.775.352340.410.580.00023408190.414.755.507.65.353130.550.827.63220.560.851.064.835.9722.75.432350.390.401.06
95.067.165.662250.320.400.00022516480.325.015.918.15.612610.390.518.12520.380.490.755.056.3521.45.652180.320.320.75
105.237.305.832280.290.330.00022835800.294.525.878.55.121740.340.498.51600.320.440.694.576.6721.35.171360.260.270.69
114.726.915.322160.380.540.00021587680.384.665.518.15.262760.510.768.12670.490.730.274.616.1025.25.211620.310.310.27
123.934.764.535691.463.080.000569529271.463.934.288.14.536711.733.878.16471.663.683.094.084.5418.44.687251.761.763.09
135.417.756.012020.220.210.00020204400.225.436.327.56.032640.280.277.52750.290.290.485.467.2222.16.061560.160.160.48
144.045.0521.34.642830.700.70
154.026.124.622250.560.900.000225111160.563.984.697.94.583310.831.477.93270.821.451.201.20
164.305.944.902880.631.030.000288212680.634.245.027.64.843010.681.137.63100.701.171.074.285.4620.74.882500.560.561.07
175.717.516.312630.210.110.00026264150.215.766.467.66.363360.250.117.63450.260.110.325.817.0120.26.412510.170.180.32
185.457.386.052450.260.240.00024495140.265.546.308.26.143090.300.258.22950.280.240.525.446.7621.96.042100.220.220.52
194.856.615.452690.440.620.00026868860.445.176.018.25.772800.370.458.22660.350.430.425.276.6322.75.871980.240.240.42
204.815.835.414630.781.290.000463415660.784.865.246.95.466181.011.826.97001.152.171.204.915.6220.15.514280.680.681.20
213.946.214.542080.530.850.000208210660.534.775.417.85.373670.640.997.83680.640.990.824.905.7923.95.502880.460.460.82
224.205.474.803720.861.510.000372217120.863.944.717.44.543050.781.367.43220.821.450.903.944.9423.54.542580.660.660.90
234.205.914.802760.641.040.000276412710.644.164.937.84.763050.711.207.83060.721.210.824.035.1121.64.632600.640.640.82
244.817.095.412070.350.470.00020737010.354.835.958.35.432100.350.478.31970.330.440.584.215.2622.14.812610.600.600.58
255.136.725.732970.410.520.00029738150.415.026.077.85.622240.330.427.82240.330.421.124.906.6321.35.501650.260.271.12
265.748.546.341690.130.050.00016882570.135.747.149.26.341680.130.059.21430.110.050.085.086.4220.65.682190.310.310.08
275.286.555.883720.450.550.00037229080.455.215.707.25.814790.620.857.25200.670.951.155.777.9623.56.371180.090.091.15
285.286.805.883110.380.440.00031107590.383.694.307.44.293851.082.057.44071.142.200.575.296.2020.05.893340.410.410.57
293.704.484.306061.703.740.000606033931.703.754.197.34.355341.473.087.35711.573.372.505.316.3220.85.912910.350.352.50
305.576.766.173970.370.320.00039727390.375.526.147.16.123790.370.357.14170.410.390.913.764.3520.74.364981.361.360.91
314.015.954.612440.610.990.000243612130.613.884.898.84.482330.611.008.82070.540.871.255.626.4721.26.223370.300.301.25
324.665.775.264260.781.310.000425815670.784.715.196.25.314890.881.516.26171.102.081.024.054.9226.54.652640.650.651.02
335.107.515.701960.270.320.00019615490.275.016.538.15.611550.230.278.11490.220.260.664.745.4717.65.344690.830.830.66
345.356.885.953090.360.390.00030897110.365.046.288.25.641890.280.348.21810.260.320.625.157.0121.85.751490.200.200.62
355.487.486.082360.240.210.00023634820.245.406.478.362200.240.238.32070.230.220.025.306.5024.35.902080.250.260.02
365.356.825.953220.370.410.00032157400.375.475.987.36.074610.470.507.34930.510.550.585.537.0923.66.131640.160.160.58
374.606.025.203330.631.000.000332912650.635.336.027.35.933400.400.457.33640.430.490.415.406.2322.86.003210.350.350.41
385.096.195.694300.610.870.000429712120.615.305.626.45.97340.881.346.48961.081.791.784.755.9521.55.352360.410.421.78
394.885.775.485310.861.450.000531117210.864.495.316.85.092870.580.906.83290.661.071.175.035.6019.95.635360.790.801.17
404.285.294.884681.041.940.000468020781.044.264.797.44.864430.991.837.44681.051.961.104.335.1021.34.933680.800.801.10
414.238.594.831080.250.350.00010844920.255.217.168.35.811200.160.168.31130.150.150.075.287.9622.45.881010.120.130.07
424.786.905.382230.380.530.00022307670.384.795.838.15.392260.390.538.12180.370.510.824.866.2820.75.462080.340.340.82
433.734.074.3313903.8512.730.001390277023.853.724.027.24.327832.185.347.28502.366.028.893.874.1920.44.479302.452.458.89
444.666.615.262420.450.650.00024248920.454.715.857.75.312060.370.517.72090.370.520.534.756.1420.85.352100.370.370.53
455.137.075.732440.330.400.00024366680.335.116.036.25.712550.350.446.23220.450.580.655.125.9919.15.723650.510.510.65
465.327.485.922190.260.270.00021885160.265.326.647.65.921780.210.217.61830.220.220.365.377.0721.15.971700.190.190.36
474.636.875.232110.390.560.00021107890.394.716.127.15.311670.300.407.11830.330.450.640.64
484.896.305.493350.540.790.000335210790.544.785.618.35.382830.490.718.32660.460.660.624.935.9422.35.532690.420.430.62
495.287.465.882170.260.280.00021685290.265.266.398.35.862080.260.288.31960.240.261.055.507.3620.06.101630.160.161.05
504.466.035.063010.610.980.000301112280.614.475.317.55.072800.570.897.52910.590.931.234.595.7320.25.192640.500.501.23
513.954.904.554981.272.540.000497525371.273.924.266.14.526911.784.056.18852.285.804.344.084.6218.24.686231.511.544.34
525.376.915.973070.350.370.00030696940.355.356.168.45.952900.330.368.42700.310.330.645.486.7320.06.082430.250.250.64
53
544.235.814.832990.681.130.000299213580.684.265.038.24.863050.681.138.22910.651.071.804.305.5920.54.902300.510.511.80
553.874.994.474221.112.120.000422022201.113.774.467.54.373400.931.697.53550.971.782.832.83
563.554.684.154181.232.430.000418324681.233.684.176.94.284791.352.756.95431.533.252.323.764.6319.34.363641.001.002.32
573.644.724.244381.252.480.000437625031.253.674.297.94.273791.072.037.93751.062.004.123.694.5720.04.293450.970.974.12
584.575.495.175140.991.810.000513819830.994.534.937.25.135871.162.237.26371.262.504.324.715.0620.55.318471.521.524.32
594.234.804.838291.884.450.000829237651.884.275.9574.871400.310.4571560.350.513.584.414.8219.95.017341.541.543.58
605.376.705.973550.400.440.00035548030.405.466.217.66.063130.330.317.63220.330.330.765.566.4720.06.163330.310.320.76
613.874.414.478752.305.850.000875346042.303.844.116.84.448702.315.896.810002.667.246.996.99
623.994.304.5915253.8313.000.001524776543.833.924.156.74.5210212.647.196.711913.079.119.389.38
636.228.136.822470.07-0.170.00024751390.076.227.407.16.821990.06-0.137.12190.06-0.150.374.014.3620.64.618422.100.37
645.606.886.203690.330.260.00036936650.335.686.186.96.284700.390.276.95320.440.311.055.786.6520.06.383490.250.251.05
4.736.395.330.701.390.704.725.557.615.32351.740.671.207.61373.360.711.341.494.805.955.40312.230.580.551.49
Incubations
2-1 Water pHSalt pHequivalentRate of Ca(OH)2 added in mg100/74Lime Buffer CapacityLime Requirement( tons ECCE/acre)
00.511.500.511.5H2O pH0.511.50.511.50.511.5MeanTitrations
16.746.997.237.556.006.236.496.686.6020.741.562.21.35135135141218114312360.610.570.620.600.77
26.687.117.357.685.876.216.416.686.4715.531.146.61.35135135146187787780.390.490.490.460.51
36.046.146.256.575.195.285.395.755.7920.641.161.71.35135135143087277814884.043.641.953.210.98
45.656.056.376.855.515.866.166.676.1122.745.568.21.35135135148789467950.870.940.790.860.67
55.876.547.097.244.765.305.756.175.3625.551.176.61.35135135146396977341.111.211.281.201.02
66.316.627.027.315.225.725.976.255.8223.346.669.91.35135135146308409170.811.071.171.020.80
75.946.006.126.205.685.825.965.996.2834.869.5104.31.35135135143356335645462.752.753.733.081.20
86.537.227.587.855.746.256.626.966.3431.162.193.21.351351351482395410330.630.730.780.711.06
97.337.647.898.145.565.926.576.696.1620.841.662.41.35135135147815577470.730.520.700.650.75
106.296.877.527.725.045.596.036.415.6417.034.151.11.35135135144194655040.610.680.740.680.69
116.636.716.776.935.375.655.765.865.977.915.723.61.35135135143795446500.430.620.730.590.27
125.696.437.187.494.995.646.466.845.5989.1178.1267.21.35135135141852163719522.802.472.952.743.09
137.157.107.077.455.996.086.186.426.598.216.424.61.3513513514123111667730.630.590.390.540.48
155.316.236.917.484.355.406.677.084.9532.765.598.21.35135135144213824860.910.821.050.921.20
165.946.346.577.074.875.215.636.235.4733.366.599.81.3513513514132211839922.151.931.621.901.07
177.217.227.357.476.166.286.436.576.7612.525.037.51.35135135141407125012350.480.430.420.440.32
187.077.117.247.556.116.326.526.846.7116.633.249.81.3513513514106910959220.420.430.360.400.52
196.896.997.027.155.735.805.875.916.3310.120.330.41.35135135141955195522811.511.511.761.590.42
206.867.117.287.475.796.116.416.736.3929.859.689.41.35135135141258129812850.890.920.910.911.20
216.516.767.057.385.726.026.406.796.3237.074.1111.11.35135135141668147214031.301.151.091.180.82
225.595.976.456.564.614.995.455.655.2126.452.979.31.351351351494085110311.781.611.951.780.90
236.326.486.757.045.405.555.966.266.0025.050.075.11.35135135142254120811802.481.331.301.700.82
246.757.027.167.825.465.956.287.226.0621.242.363.51.35135135145846974870.610.730.510.610.58
257.037.147.467.816.176.247.077.256.7716.031.947.91.351351351430824795991.020.160.200.461.12
266.777.017.297.475.455.906.016.306.053.67.210.81.35135135141081741720.110.180.180.160.08
276.817.037.157.376.146.366.556.646.7426.953.780.61.35135135141650177121780.590.640.780.671.15
286.897.307.517.825.976.436.696.986.5731.262.593.71.3513513514918117312540.490.620.660.590.57
295.035.115.305.434.384.814.945.214.9892.6185.2277.71.35135135142909446845226.179.479.592.50
306.867.147.748.045.676.216.837.286.2726.853.680.31.35135135146706246740.560.520.560.540.91
315.586.257.017.614.205.096.066.674.8032.565.097.51.35135135144934725331.131.091.231.151.25
326.566.836.956.906.126.346.366.426.7225.150.275.31.35135135141542282833930.591.071.290.981.02
336.647.037.337.835.976.166.286.366.5718.236.354.51.35135135144304964490.230.260.240.240.66
346.697.167.197.266.196.266.446.536.7917.033.950.91.35135135143818269525461.180.840.790.940.62
356.887.197.167.265.425.996.417.066.026.513.019.41.35135135145844875710.630.530.620.590.02
367.427.497.607.746.126.186.296.396.7215.531.146.61.35135135143499247023331.330.940.891.050.58
376.086.666.906.955.545.695.906.006.1417.534.952.41.35135135141574131115401.511.261.481.420.41
387.207.267.527.676.276.306.706.936.8728.356.785.01.351351351412760178017402.930.410.401.251.78
397.247.337.457.576.196.356.516.676.7927.354.681.91.35135135142306230623060.710.710.710.711.17
405.996.336.846.995.265.576.166.335.8631.663.294.81.3513513514137794911971.711.181.481.461.10
416.746.957.047.355.575.765.836.236.175.310.616.01.35135135143795533270.350.510.300.390.07
426.736.916.987.325.555.885.956.336.1516.733.350.01.351351351468211258660.651.070.820.850.82
435.075.557.068.203.854.366.257.474.45280.9561.7842.61.351351351474423163314519.728.388.3412.158.89
447.107.197.387.675.886.156.376.776.4817.735.453.01.35135135148859758050.550.600.500.550.53
457.137.667.817.956.246.826.967.076.8423.046.069.01.351351351453686411240.140.220.290.220.65
466.987.127.287.435.735.926.116.356.339.118.227.31.35135135146476475950.500.500.460.480.36
486.606.716.897.065.355.435.595.865.9523.847.671.31.35135135144017267818904.623.082.173.290.62
496.586.657.097.405.425.546.086.466.0212.525.137.61.351351351414115134891.520.550.530.871.05
506.706.967.187.395.545.876.106.486.1429.559.088.51.35135135141207142312721.161.371.221.251.23
514.885.105.705.744.584.675.185.645.18107.0214.0321.01.3513513514160664820409230.859.257.864.34
527.207.577.767.786.076.506.836.936.6715.731.447.11.35135135144945597410.210.240.320.260.64
545.515.576.606.664.444.655.695.805.0444.488.8133.11.3513513514285696013235.881.982.733.531.80
555.445.996.256.754.244.755.195.614.8469.8139.6209.41.35135135141849198520654.184.494.674.442.83
565.136.186.827.314.135.175.876.514.7357.3114.6171.91.35135135147458909761.762.112.312.062.32
575.865.096.357.213.884.745.306.274.48101.6203.2304.81.35135135141596193417234.185.074.514.594.12
586.066.737.227.545.195.886.496.875.79106.6213.1319.71.35135135142087221625722.732.903.373.004.32
595.375.886.967.564.405.156.346.935.0088.4176.7265.11.35135135141592123114163.342.592.972.973.58
606.756.927.207.325.706.136.356.466.3018.737.456.11.35135135145887789980.470.620.800.630.76
614.985.905.475.734.304.414.634.704.90172.4344.7517.11.351351351421175141171747046.5931.0638.436.99
637.858.138.238.306.947.257.337.377.549.218.527.71.3513513514402639870-0.18-0.28-0.38-0.280.37
647.127.267.437.566.136.256.406.586.7328.156.384.41.35135135143168281625351.171.040.941.051.05
1.441.37
KCl
Sample #AlMn
10.3785.10
20.7741.54
37.9574.73
42.4432.73
517.464.69
64.809.74
78.4616.86
81.9718.82
90.6739.42
106.6415.37
112.8129.68
12111.20212.90
138.1529.20
1442.8044.57
1515.8081.88
160.5324.07
171.0418.45
181.1144.27
195.07105.60
201.4662.38
2131.6216.40
2212.7360.24
232.1249.58
243.50131.20
250.5316.89
260.68110.30
270.7569.77
28214.6031.95
290.42110.30
3075.275.23
314.11321.10
320.9958.71
330.2423.56
340.6822.33
350.4594.78
363.0068.07
370.44306.40
382.84212.20
3911.30130.00
400.5218.56
412.5178.64
42768.5026.58
432.7014.90
440.58274.60
450.3961.24
463.7854.98
471.8994.37
481.19130.00
496.0832.25
50122.1057.06
510.64129.90
520.1826.55
5341.1321.18
5459.1338.54
5562.2531.09
5689.2118.49
5712.5944.21
5874.342.43
590.5228.26
60374.709.22
61679.6013.27
620.8510.30
630.5472.63
10.93
20.81
30.90
41.47
51.70
61.36
71.90
81.07
90.83
101.03
111.07
123.64
130.26
152.00
161.79
170.22
180.48
190.74
201.58
211.90
221.80
231.70
240.89
251.38
260.00
271.88
280.92
300.89
311.92
321.85
330.72
350.12
360.80
371.26
382.18
391.91
402.20
410.27
421.30
441.01
451.17
460.52
481.26
490.86
501.49
521.01
542.00
553.05
562.25
601.16
640.00
B.Sat
OjegaFinch
CaMgKNaCECExc. acidity% B. Saturation% B.UnsatCaMgKNaCECExch AcidityB. Saturation% B.Unsat
13.631.020.090.1110.185.3352.447.645.901.000.490.048.661.2385.814.2
21.880.560.170.096.23.5056.543.552.380.500.120.024.161.1472.627.4
30.750.270.080.123.722.5067.232.800.740.170.050.032.271.2843.656.4
42.380.880.130.094.020.5413.486.573.100.830.10.0361.9467.732.3
51.000.330.310.124.22.4458.141.901.260.300.50.024.462.3846.653.4
61.630.500.190.096.293.8861.738.311.920.430.260.034.832.1954.745.3
72.132.500.380.1612.397.2258.341.733.152.170.310.1311.415.6550.549.5
83.131.690.290.129.84.5746.653.374.351.580.260.58.161.4782.018.0
92.630.350.280.117.063.6952.347.732.950.250.210.094.210.7183.116.9
101.130.270.130.094.412.7963.336.731.340.200.170.042.831.0861.838.2
111.380.480.130.116.754.6568.931.112.150.420.130.184.081.2070.629.4
122.501.250.190.1016.0311.9974.825.203.551.420.180.113.828.5738.062.0
132.500.540.090.106.813.5852.647.433.650.420.080.074.580.3692.17.9
14
151.500.460.120.127.074.8768.931.121.550.330.150.0752.9042.058.0
161.500.380.130.127.915.7873.126.934.700.250.080.064.58-0.51111.1-11.1
174.250.710.470.1210.65.0547.652.364.800.750.460.037.661.6278.921.1
183.750.770.250.1110.595.7153.946.083.300.750.210.096.412.0667.932.1
192.500.420.140.116.993.8254.645.353.800.420.10.074.50.1197.62.4
203.880.810.290.1110.044.9549.350.706.350.830.310.087.750.1897.72.3
214.631.460.220.1216.039.6059.940.111.101.670.280.1114.0810.9222.477.6
221.000.350.080.126.555.0076.323.662.600.300.10.044.11.0674.125.9
231.880.560.130.159.326.6070.829.181.940.330.10.095.53.0444.755.3
241.380.330.100.125.323.3963.736.282.650.370.170.044.41.1773.426.6
251.750.210.240.137.304.9768.131.922.760.330.330.084.410.9179.420.6
262.250.330.210.114.761.8639.160.927.400.270.350.032.8-5.25287.5-187.5
274.131.270.440.1215.499.5361.538.4817.801.670.560.1911.33-8.89178.5-78.5
282.004.100.250.1125.9619.5075.124.883.004.500.310.1321.4913.5536.963.1
292.004.500.170.2214.787.8953.446.628.503.670.210.1713.160.6195.44.6
304.501.020.290.1012.446.5352.547.510.751.170.330.1107.6523.576.5
311.500.400.080.107.155.0770.929.096.000.420.10.056-0.57109.5-9.5
323.133.750.120.3717.149.7757.043.001.163.670.150.4115.4910.1034.865.2
331.750.380.130.095.272.9255.444.593.150.300.170.033.03-0.62120.5-20.5
343.131.000.290.1012.968.4465.134.882.401.000.230.069.415.7239.260.8
352.380.540.190.106.152.9447.852.207.250.470.180.034.86-3.07163.2-63.2
365.000.961.900.1211.223.2428.971.123.751.000.180.0811.416.4043.956.1
372.750.920.100.107.433.5647.952.096.000.920.151.837.5-1.40118.7-18.7
384.251.540.230.1214.818.6758.541.467.001.580.230.114.325.4162.237.8
393.751.080.370.2711.476.0052.347.697.551.250.330.1813.914.6066.933.1
402.881.330.200.118.854.3348.951.074.651.500.210.0892.5671.628.4
411.000.250.110.082.140.7032.767.291.180.230.210.021.770.1392.77.3
422.500.540.210.106.192.8445.954.123.580.530.380.035.090.5788.811.2
4312.506.250.370.3233.1913.7541.458.579.505.670.310.2834.9919.2345.055.0
442.380.600.140.136.253.0048.052.003.020.570.170.035.41.6170.229.8
453.131.600.140.149.874.8649.250.764.801.830.130.1114.087.2148.851.2
462.630.790.170.136.162.4439.660.393.160.670.240.056.262.1465.834.2
471.250.310.070.104.733.0063.436.581.760.270.090.033.771.6257.043.0
482.380.830.200.108.224.7157.342.704.000.750.180.058.333.3559.840.2
491.750.310.110.094.502.2449.850.221.320.270.140.033.731.9747.252.8
502.130.630.230.136.613.4952.847.201.860.600.450.047.34.3540.459.6
512.751.130.170.1314.2310.0570.629.374.001.670.180.0718.3312.4132.367.7
522.000.520.190.126.453.6256.143.882.200.500.150.055.832.9349.750.3
5332.501.600.470.1627.08-7.65-28.2128.2516.001.830.490.1330.6512.2060.239.8
540.750.170.040.138.487.3987.112.851.600.250.090.056.584.5930.269.8
551.000.230.080.1511.9410.4887.812.231.900.330.120.0711.338.9121.478.6
562.250.750.130.1516.2813.0079.920.153.100.830.170.098.754.5647.952.1
571.500.580.150.1711.699.2979.520.532.050.670.210.1413.5810.5122.677.4
583.005.830.330.3332.0222.5370.429.6419.804.330.360.377.66-17.20324.5-224.5
594.001.800.510.0815.939.5459.940.116.900.400.560.2323.6515.5634.265.8
606.040.880.150.0911.654.4938.561.466.200.160.260.19114.1961.938.1
617.501.520.150.1018.048.7748.651.395.501.580.120.2122.7415.3332.667.4
621.500.330.370.1428.1825.8491.78.3010.503.000.410.7240.8226.1935.864.2
6322.501.790.091.0016.92-8.46-50.0150.0011.401.750.130.2622.078.5361.438.6
647.502.900.360.0912.691.8414.585.505.202.420.360.1316.588.4748.951.1
Normality Calc.
Ca(OH)2 NORMAILITY CALCULATOR
Volume of KHC8H4O45.00ml
Formula weight of KHC8H4O4204.23g/mol
Volume of Ca(OH)2 consumed in titration5.60ml
Moles of KHC8K4O40.0002448moles
Equivalents of KHC8H4O40.0002448eq
Normality of Ca(OH)20.04372N
Normality of Ca(OH)20.0437N
Weekly
Normality ReadingsMeanNormaility
4/28/083.86
5.4
6.905.390.0440
5/8/085.2
4.87
4.965.010.0471
5/15/085.45
5.55
5.555.520.0444
5/21/085.55
5.55
5.455.520.0444
5/28/085.55
5.6
5.555.570.0444
6/5/085.55
5.55
5.65.570.0444
6/12/085.6
5.55
5.555.570.0444
Ca(OH)2 rates
Rates for soils in mlRates for soils in mg
soil idallen ojega mlmeq of Ca(OH)2 per 10 gml of 0.0437 N Ca(OH)2 per 100 g soil00.511.5
14.830.11205625.6421052632012.825.638.5207.3
23.620.08398419.218306636209.619.228.8
34.790.11112825.4297482838012.725.438.1
45.300.1229628.1372997712014.128.142.2
55.950.1380431.5881006865015.831.647.4
65.430.12597628.8274599542014.428.843.2
78.100.1879243.0022883295021.543.064.5
87.240.16796838.4366132723019.238.457.7
94.850.1125225.7482837529012.925.738.6
103.970.09210421.0764302059010.521.131.6
111.830.0424569.715331807804.99.714.6
1220.750.4814110.1601830664055.1110.2165.2
131.910.04431210.140045766605.110.115.2
142.880.06681615.289702517207.615.322.9
157.630.17701640.5070938215020.340.560.8
167.750.179841.1441647597020.641.161.7
172.910.06751215.448970251707.715.423.2
183.870.08978420.5455377574010.320.530.8
192.360.05475212.529061784906.312.518.8
206.940.16100836.8439359268018.436.855.3
218.630.20021645.8160183066022.945.868.7
226.160.14291232.7029748284016.432.749.1
235.830.13525630.9510297483015.531.046.4
244.930.11437626.1729977117013.126.239.3
253.720.08630419.749199084709.919.729.6
260.840.0194884.459496567502.24.56.7
276.260.14523233.2338672769016.633.249.9
287.280.16889638.6489702517019.338.658.0
2921.570.500424114.5135011442057.3114.5171.8
306.240.14476833.1276887872016.633.149.7
317.570.17562440.1885583524020.140.260.3
325.850.1357231.057208238015.531.146.6
334.230.09813622.4567505721011.222.533.7
343.950.0916420.9702517162010.521.031.5
351.510.0350328.016475972504.08.012.0
363.620.08398419.218306636209.619.228.8
374.070.09442421.6073226545010.821.632.4
386.600.1531235.0389016018017.535.052.6
396.360.14755233.7647597254016.933.850.6
407.360.17075239.0736842105019.539.158.6
411.240.0287686.583066361603.36.69.9
423.880.09001620.5986270023010.320.630.9
4365.441.518208347.41601830660173.7347.4521.1
444.120.09558421.8727688787010.921.932.8
455.360.12435228.4558352403014.228.542.7
462.120.04918411.254919908505.611.316.9
473.430.07957618.20961098409.118.227.3
485.540.12852829.4114416476014.729.444.1
492.920.06774415.502059496607.815.523.3
506.870.15938436.4723112128018.236.554.7
5124.930.578376132.3514874142066.2132.4198.5
523.660.08491219.430663615609.719.429.1
532.600.0603213.803203661306.913.820.7
5410.340.23988854.8942791762027.454.982.3
5516.260.37723286.3231121281043.286.3129.5
5613.350.3097270.8741418764035.470.9106.3
5723.670.549144125.6622425629062.8125.7188.5
5824.830.576056131.8205949657065.9131.8197.7
5920.590.477688109.3107551487054.7109.3164.0
604.360.10115223.1469107551011.623.134.7
6140.160.931712213.20640732270106.6213.2319.8
6253.931.251176286.31029748280143.2286.3429.5
632.150.0498811.41418764305.711.417.1
646.600.1531234.8017.434.852.2Total
1549.73099.34649.09298.0
Rates
weight of soil (g)00.511.5
120.00.02.65.17.7
3500.00.81.52.3
480.00.20.30.5
7300.01.12.13.2
5200.01.53.04.5
27500.06.813.520.3
29200.02.95.88.7
40500.010.020.030.0
4780.00.71.52.2
511000.025.551.076.5
5380.02.14.26.4
54200.05.410.816.2
61200.06.112.218.3
6280.02.55.07.4
1012.825.638.5
301.53.04.5
402.04.06.0
703.57.010.5
1507.515.022.5
27013.527.040.5
29014.529.043.5
40020.040.060.0
4709.118.227.3
51025.551.076.5
53026.553.079.5
54027.054.081.0
61030.561.091.5
62031.062.093.0
Water vs Salt pH
Water pH 2-1Adjusted Salt pH
Stir 4x and ReadMeanShake and ReadMeanSalt pHMeanWater pH
15.785.725.355.755.865.815.135.225.185.815.84
25.505.525.505.75.665.684.814.914.865.495.52
35.335.35.335.35.45.354.534.604.575.205.23
45.225.195.225.265.345.304.554.614.585.215.24
54.934.954.935.035.055.044.194.234.214.844.87
65.255.105.255.255.165.214.424.464.445.075.10
75.425.295.425.425.385.404.514.574.545.175.20
85.415.365.415.535.55.524.74.744.725.355.38
95.775.675.775.825.785.804.945.024.985.615.64
105.745.135.745.175.155.164.484.564.525.155.18
115.305.335.305.45.265.334.624.564.595.225.25
124.494.484.494.54.584.543.963.913.944.574.60
135.925.885.926.025.935.985.385.365.376.006.03
144.554.624.554.634.744.693.953.883.924.554.58
154.824.954.824.845.014.934.324.224.274.904.93
166.236.216.236.286.376.335.685.655.676.306.33
175.985.915.986.036.036.035.45.455.436.066.09
185.785.855.785.95.885.895.135.065.105.735.76
195.415.455.415.515.475.494.914.844.885.515.54
205.335.375.335.435.535.484.734.814.775.405.43
214.514.584.514.564.664.613.883.943.914.544.57
224.704.784.704.744.864.804.24.244.224.854.88
235.485.485.485.555.595.574.854.824.845.475.50
245.685.735.685.685.735.715.085.025.055.685.71
255.316.265.316.266.36.285.645.735.696.326.35
265.445.415.445.475.545.515.175.255.215.845.87
275.845.745.845.925.975.955.215.255.235.865.89
284.604.634.604.674.714.693.663.763.714.344.37
295.865.755.865.875.845.865.425.525.476.106.13
304.604.674.604.854.884.873.974.054.014.644.67
314.874.874.874.934.934.934.624.654.645.275.30
325.605.565.605.625.645.635.035.085.065.695.72
335.835.845.835.885.955.925.255.335.295.925.95
346.156.136.156.166.176.175.425.455.446.076.10
355.775.755.775.85.865.835.275.285.285.915.94
365.255.215.255.265.245.254.624.694.665.295.32
375.495.525.495.45.525.465.085.105.095.725.75
385.505.535.505.385.65.494.894.904.905.535.56
394.764.644.764.914.834.874.214.264.244.874.90
406.005.956.0065.965.985.225.075.155.785.81
415.385.395.385.35.325.314.784.724.755.385.41
424.694.614.694.744.774.763.723.803.764.394.42
435.355.315.355.285.395.344.654.684.675.305.33
445.755.685.755.765.675.725.115.085.105.735.76
455.985.965.985.975.95.945.245.265.255.885.91
465.435.405.435.465.385.424.614.604.615.245.27
475.65.515.605.695.635.664.724.824.775.405.43
485.785.665.785.735.565.655.175.285.235.865.89
495.205.185.205.25.25.204.514.524.525.155.18
505.584.495.584.554.64.583.993.943.974.604.63
516.015.946.0166.046.025.35.385.345.976.00
526.156.176.156.326.336.336.075.986.036.666.69
535.024.955.024.974.984.984.214.214.214.844.87
544.554.484.554.64.64.603.93.883.894.524.55
554.294.084.294.244.34.273.663.633.654.284.31
564.384.304.384.324.384.353.683.673.684.314.34
575.255.085.255.285.245.264.554.604.585.215.24
584.924.844.925.045.025.034.244.324.284.914.94
595.995.865.996.065.996.035.375.455.416.046.07
604.624.524.625.154.714.933.823.863.844.474.50
614.664.524.664.694.694.693.953.983.974.604.63
626.776.496.776.836.786.816.136.136.136.766.79
636.226.126.226.036.256.145.585.645.616.246.27
5.385.335.385.385.425.424.734.754.745.395.42
difference0.640.67
2:1 Salt pH I've done
123Mean
15.135.225.195.315.285.23
24.814.914.814.844.894.85
34.534.64.684.604.604.60
44.554.614.594.634.704.62
54.194.234.214.274.344.25
64.424.464.44.394.504.43
74.514.574.54.584.624.56
84.74.744.664.754.824.73
94.945.024.875.065.054.99
104.484.564.995.234.624.78
114.624.564.624.724.704.64
123.963.914.643.934.024.09
135.385.365.335.414.455.19
14
153.953.883.934.024.063.97
164.324.224.184.304.334.27
175.685.655.595.715.675.66
185.45.455.45.455.485.44
195.135.064.854.854.934.96
204.914.844.774.814.924.85
214.734.814.693.944.754.58
223.883.943.924.203.953.98
234.24.244.114.204.214.19
244.854.824.754.814.864.82
255.085.025.025.135.135.08
265.645.735.585.745.705.68
275.175.255.175.285.275.23
285.215.255.125.285.255.22
293.663.763.613.703.723.69
305.425.525.425.575.565.50
313.974.054.084.014.044.03
324.624.654.64.664.644.63
335.035.085.045.105.125.07
345.255.335.25.355.285.28
355.425.455.335.485.485.43
365.275.285.265.355.325.30
374.624.694.534.604.594.61
385.085.14.995.095.135.08
394.894.94.814.884.914.88
404.214.264.074.284.254.21
415.225.075.214.235.214.99
424.784.724.724.784.754.75
433.723.83.683.733.783.74
444.654.684.534.664.684.64
455.115.085.15.135.185.12
465.245.265.225.325.355.28
474.614.64.644.634.864.67
484.724.824.764.894.824.80
495.175.285.25.285.275.24
504.514.524.434.464.484.48
513.993.943.83.953.953.93
525.35.385.315.375.395.35
536.075.985.996.01
544.214.214.154.234.254.21
553.93.883.83.873.883.87
563.663.633.63.553.593.61
573.683.673.573.643.643.64
584.554.64.524.574.514.55
594.244.324.194.234.214.24
605.375.455.315.375.345.37
613.823.863.723.873.843.82
623.953.983.883.993.953.95
636.136.136.036.225.776.06
645.585.645.485.605.625.58
4.734.734.704.734.734.74
Base saturation
Base Saturation(ojega)Soil pH
R0010.525.67
R0020.565.49
R0030.675.26
R0040.135.11
R0050.584.81
R0060.625.05
R0070.584.65
R0080.475.26
R0090.525.65
R0100.635.01
R0110.695.28
R0120.754.88
R0130.535.91
R0140.694.50
R0150.734.79
R0160.486.19
R0170.545.83
R0180.555.71
R0190.495.37
R0200.605.26
R0210.764.41
R0220.714.63
R0230.645.36
R0240.685.62
R0250.396.23
R0260.625.38
R027 *0.755.62
R0280.534.48
R0290.525.69
R0300.714.57
R0310.574.83
R0320.555.48
R0330.655.75
R0340.486.05
R0350.295.70
R0360.485.17
R0370.595.36
R0380.525.40
R0390.494.64
R0400.334.89
R0410.465.30
R042 *0.414.48
R0430.485.24
R0440.495.53
R0450.405.83
R0460.635.25
R0470.575.42
R0480.505.55
R0490.535.07
R0500.714.36
R0510.565.83
R052 *
R0530.874.85
R054 *0.884.34
R0550.803.99
R0560.794.17
R057 *0.705.15
R0580.604.67
R0590.395.83
R060 *0.494.41
R0610.924.51
R062
R0630.146.01
Base saturation
1:1 H2O pH
Base Saturation
Base saturation vs 2;1 Water pH
SAS Input
Number of Means 2 3 4 5
Critical Range .3397 .3576 .3695 .3784
Means with the same letter are not significantly different.
Duncan Grouping Mean N Method
A 1.3563 56 A_E2
A
B A 1.2382 56 A_E1
B A
B A 1.2298 56 CAOH
B A
B A 0.9955 56 M_S
B
B 0.9311 56 A_E
A-E2A-E1CA(OH)2M-SA-E
1.32631.23821.22980.99550.9311
Duncan Grouping Mean N Method
A-E 2A-E 1Ca(OH)2M-SA-E
A 1.35625 56 A_E21.361.241.2310.93
A
A 1.23821 56 A_E1
A
A 1.22982 56 CAOH
B 0.99554 56 M_S
B
B 0.93107 56 A_E
SAS Input
CaCO3 tons/Ac
Buffer Methods
Lime Requirement vs Buffer methods on Tukey Test
All samples 51
Buffer Methods
Lime Requirement
LR vs Buffer Methods
Corr. Matrix
Water pHSalt pHBuffer pHLime Requirement Comparisons on all Methods in tons ECCE/acreCation Exchange Capacity and Base Saturation
AllenOjegaHenryAdjusted Salt pHAdjusted Salt pHAllenOjegaHenryHenryModified A-E (1)Modified A-E (2)Henry'sAL/OjAllen'sOjega'sOjegaFinchCaCl2-AluminumKCl-Aluminum
2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2-1 Water pH1-1 Water pH2:1 Salt pH1-1 Salt pHpH 2-1pH 1-1A-E buffer pHA-E Buffer pHA-E Buffer pHA-E(m)Moore-SikoraAllen 2-1Ojega 2-1Ojega 1-1Orig. A-E 2-1Orig. A-E 1-12-1 LR1-1 LR2-1 LR1-1 LRMoore-Sikora 2-1Moore-Sikora 1-1UGA 2-1John's form. 2-1UGA 1-1John's form. 1-1Georgia Data 1-1IncubationsTitrationsTitrationsTitrationsInc/Titr meanMechanical Analysis ResultsCaMgKNaCECExc. acidity% B. Saturation% B.UnsatCaMgKNaCECExch AcidityB. Saturation% B.UnsatAlMnAlMn
16.055.905.995.835.815.835.986.546.587.147.557.517.657.287.550.980.931.120.570.641.161.301.301.450.720.810.450.530.370.320.350.420.770.770.840.60Texure% Clay% Silt% Sand3.631.020.090.1110.185.3352.447.645.901.000.490.048.661.2385.814.232.626.140.3785.10
26.015.955.835.455.685.455.556.166.156.767.657.667.787.467.720.720.810.950.390.450.981.111.091.230.510.580.410.570.390.410.240.360.510.510.620.44Loam21.427.251.41.880.560.170.096.23.5056.543.552.380.500.120.024.161.1472.627.45.022.140.7741.54
35.595.465.455.345.355.345.316.055.916.657.757.717.837.767.790.780.900.990.370.390.530.550.580.610.460.480.310.420.320.370.210.820.830.830.830.82Sandy Loam7.533.159.40.750.270.080.123.722.5067.232.800.740.170.050.032.271.2843.656.4153.209.887.9574.73
45.525.435.325.135.305.135.355.845.956.447.567.567.657.367.591.391.471.640.780.851.451.571.611.750.931.010.470.690.540.630.670.670.670.920.67Sandy loam9.229.061.82.380.880.130.094.020.5413.486.573.100.830.10.0361.9467.732.3368.802.382.4432.73
55.215.045.024.875.044.874.935.585.536.187.587.557.707.477.601.571.701.920.750.811.321.431.481.611.011.090.560.900.670.860.390.771.021.021.030.89Loam20.536.942.61.000.330.310.124.22.4458.141.901.260.300.50.024.462.3846.653.4142.200.8617.464.69
65.425.305.235.205.215.205.185.915.786.517.637.617.677.567.631.241.361.490.780.831.041.111.161.240.880.930.530.810.690.840.340.640.800.800.770.72Loam10.536.153.41.630.500.190.096.293.8861.738.311.920.430.260.034.832.1954.745.3152.901.034.809.74
75.655.475.505.235.405.235.245.945.846.547.457.387.537.267.431.701.902.251.011.341.582.091.762.251.221.610.881.540.700.850.441.291.201.201.411.24Loam Sand8.211.580.32.132.500.380.1612.397.2258.341.733.152.170.310.1311.415.6550.549.5123.800.528.4616.86
85.905.765.665.345.525.345.436.056.036.657.687.617.687.267.610.801.071.350.650.741.481.691.651.880.790.900.530.780.560.640.360.661.061.061.260.86Sandy Clay Loam26.524.848.73.131.690.290.129.84.5746.653.374.351.580.260.58.161.4782.018.07.600.781.9718.82
96.045.965.825.715.805.715.746.426.347.027.697.657.807.667.760.630.831.020.330.380.560.630.630.710.400.450.440.580.410.420.270.430.750.750.840.59Sandy Loam14.617.368.12.630.350.280.117.063.6952.347.732.950.250.210.094.210.7183.116.9109.503.480.6739.42
105.435.335.244.715.164.715.745.426.346.027.737.707.787.657.780.901.031.150.540.570.830.880.930.990.520.560.390.500.350.420.220.450.690.690.690.57Sandy Clay Loam10.623.965.51.130.270.130.094.412.7963.336.731.340.200.170.042.831.0861.838.283.992.306.6415.37
116.056.015.625.235.335.235.395.945.996.547.697.617.767.497.690.591.071.230.530.541.141.171.271.300.700.710.470.680.480.560.310.240.270.270.320.26Sandy Loam19.615.564.91.380.480.130.116.754.6568.931.112.150.420.130.184.081.2070.629.4469.804.872.8129.68
125.414.754.674.394.544.394.695.105.295.707.137.147.187.107.103.583.646.522.422.182.652.392.712.782.652.392.245.681.822.411.292.343.093.093.662.71Sandy Loam9.015.076.02.501.250.190.1016.0311.9974.825.203.551.420.180.113.828.5738.062.015.0915.89111.20212.90
136.566.666.305.805.985.806.116.516.717.117.827.737.817.577.78-0.170.260.190.260.280.580.630.650.710.290.320.250.240.280.210.140.200.050.050.330.12Loam25.736.238.12.500.540.090.106.813.5852.647.433.650.420.080.074.580.3692.17.9237.604.018.1529.20
145.034.874.764.504.694.504.725.215.325.817.597.517.687.707.591.632.002.140.911.240.851.670.911.871.791.230.831.450.891.170.590.731.201.201.330.97Sandy Loam9.710.779.61.500.460.120.127.074.8768.931.121.550.330.150.0752.9042.058.0156.104.1942.8044.57
155.235.255.055.384.935.385.006.095.606.697.597.527.557.397.541.441.791.951.180.191.600.491.810.571.081.250.861.510.690.880.460.981.071.071.351.03Sandy Loam14.536.149.41.500.380.130.127.915.7873.126.934.700.250.080.064.58-0.51111.1-11.1642.2019.1015.8081.88
166.626.546.426.116.336.116.416.827.017.427.687.657.797.447.75-0.070.220.290.120.440.300.540.350.600.250.220.250.130.250.080.140.220.320.320.510.27Sandy Loam12.534.652.94.250.710.470.1210.65.0547.652.364.800.750.460.037.661.6278.921.1308.003.530.5324.07
176.326.256.155.856.035.856.156.566.757.167.737.667.727.667.740.300.480.730.340.470.421.040.471.160.310.410.340.330.310.200.190.290.520.520.670.41Sandy Clay Loam10.516.173.43.750.770.250.1110.595.7153.946.083.300.750.210.096.412.0667.932.113.171.761.0418.45
186.196.142.935.705.895.705.576.416.177.017.767.657.737.417.750.360.740.820.401.210.871.870.982.080.380.440.440.610.380.360.220.300.420.420.410.36Sandy Loam10.511.378.22.500.420.140.116.993.8254.645.353.800.420.10.074.50.1197.62.46.023.521.1144.27
195.795.705.615.495.495.495.556.206.156.807.537.447.457.147.431.241.581.791.131.161.751.801.952.000.511.240.841.420.520.560.550.631.201.201.210.92Sandy Loam10.912.576.63.880.810.290.1110.044.9549.350.706.350.830.310.087.750.1897.72.38.758.915.07105.60
205.735.595.595.315.505.315.066.025.666.627.427.377.507.227.401.661.902.431.021.571.591.681.771.631.161.370.520.810.620.690.440.830.820.821.500.82Sandy Loam11.224.864.04.631.460.220.1216.039.6059.940.111.101.670.280.1114.0810.9222.477.63.191.851.4662.38
215.255.294.984.544.614.544.625.255.225.857.587.537.507.467.411.421.801.921.451.311.552.121.612.251.721.850.811.430.761.010.620.970.900.901.070.93Loam24.927.547.61.000.350.080.126.555.0076.323.662.600.300.10.044.11.0674.125.913.392.4031.6216.40
225.465.375.104.794.804.794.895.505.496.107.637.477.547.267.511.201.702.101.240.552.010.672.230.741.611.410.560.900.710.920.550.690.820.821.010.76Loam16.635.949.51.880.560.130.159.326.6070.829.181.940.330.10.095.53.0444.755.367.724.0412.7360.24
235.945.865.715.495.575.495.536.206.136.807.757.667.757.707.770.570.891.020.480.540.591.020.661.140.960.510.430.600.360.400.530.430.580.580.860.50Sandy Loam12.314.273.51.380.