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Engineering NDT Advance dNDE Pressure Equipment Integrity Management Lab Analys is Development of NDT Inspection Development of NDT Inspection Techniques For Heavy Wall Techniques For Heavy Wall Stainless Steel Piping Stainless Steel Piping Presented by: Larry Bartley - Canspec Group Inc. Plant Services Coordinator Presented to National Pressure Equipment Conference National Pressure Equipment Conference February 9 – 11, 2005

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Page 1: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

AdvancedNDE Pressure

Equipment Integrity

Management

Lab Analysi

s

Development of NDT Inspection Development of NDT Inspection Techniques For Heavy Wall Stainless Techniques For Heavy Wall Stainless

Steel PipingSteel Piping

Presented by:

Larry Bartley - Canspec Group Inc. Plant Services Coordinator

Presented to

National Pressure Equipment ConferenceNational Pressure Equipment ConferenceFebruary 9 – 11, 2005

Page 2: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Acknowledgements

• Brian BeresfordCanspec Group Inc.

• David MackintoshCanspec Group Inc.

• Wayne SmithOxy Vinyls, Canada

• Hang ZhengCanspec Group Inc.

• Gary Kroner Carbon Steel Inspection

Page 3: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Overview

• Introduction• Detection method• Probe development• Test standard • Inspection of the test pipes• Analysis technique• Conclusions

Page 4: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Introduction• Canspec developed a nondestructive

examination method for SA-312 TP 316L SS pipes:– NPS 3 in. diameter (0.121 in. wall thickness) and– NPS 6 in. diameter (0.146 in. wall thickness).

• Examine pipes while in operation• Pipes in horizontal position• Pipes had been used to carry liquid vinyl

chloride monomer (VCM) at 150 psig and approximately 17C since 1996.

• Pipes were known to have corrosion pits on the internal surface.

Page 5: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Corrosion mechanism• Water condensates containing chlorides tended

to gather at the bottom of the pipe, causing pitting on the internal surface.

• Inside the pits, water and high concentrations of chloride ions collected.

• Corrosion rate inside pits increased, eventually caused a large cavity inside the pipe wall. 

Page 6: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Sample

NPS 3 in. diameter test piece

Page 7: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Choice of NDE Method• Factors in decision: material, size of pipes, type

of defects• Eddy current was considered to be the best

choice.• Eddy current has good sensitivity to corrosion

pits on the pipe internal surface while scanning from the outside.

• Eddy current allows a fast and efficient inspection of the pipes while the plant is in operation.

Page 8: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Probe Development• Probe consisted of a differential coil embedded

in a hand-held housing.• Two stainless steel bars maintained constant

clearance between the coils and the pipe surface and provided wear resistance

• Probe is hand-held for easy scanning along the pipe surface.

Page 9: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Test Standard • A section of the test pipe (NPS 3 in.) was

longitudinally split in half and one half was made to be a test standard piece.

• Defects: four 3/64 in. (0.047 in.) diameter drilled

holes of depths 100%, 75%, 50% and 20% wall.• Natural corrosion pit about 0.05 in. diameter, 0.032

in. deep (26% wall loss)• Tests indicated good sensitivity to the shallowest

hole (20% wall loss).• The calibrated test system could detect and size

the natural pit.

Page 10: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

View of Test Standard

Page 11: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Permeability variation• A simulated permeability variation was also added

to the test standard piece.• Objective: to set the system to differentiate

irrelevant indications due to permeability variations.

Page 12: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Inspection Results —Flaws detected:

1) Through-wall pinhole

2) Inside diameter indication, 90% wall-loss pit.

3) Inside diameter indication, 20% wall-loss pit.

(All above defects located at the bottom of the pipe.)

Page 13: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Eddy Current Data from the 90% pit

Page 14: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Visual Verification

• Pipe was longitudinally split in half, and internal surface was cleaned by wire brush.

• Small diameter pits could be seen at locations predicted by eddy current examination.

Page 15: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Results from the Pit Called at 90%

• Metallographic examination revealed a 1 mm diameter opening on the pipe internal surface.

• Inside the pipe wall, the pit broadened to an area of 3.5 × 5 mm.

• Wall loss was physically measured to be 90%.

Page 16: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

View of the 90% pit from the internal surface

Page 17: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Scanning electron microscope (SEM) image of the cross section of the 90% pit.

Page 18: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Scanning electron microscope (SEM) image of the 90% pit.Scanning electron microscope (SEM) image of the 90% pit.

Page 19: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

• Diameter 0.04 in., depth 0.020 in. (17% wall loss).

• Results verified that the system met the required sensitivity to 25% wall loss.

Results from the Shallow Pit

Page 20: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

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Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Inspection of the Test Pipes (cont’d)

• The second indication was a 0.04 in. diameter, 0.020 in. deep pit which accounted for a 17% wall loss. More importantly, the system could detect a pit where the wall loss was as small as 17%, which met the required 25% wall loss criteria.

View of the 20% pit from the internal surface

Page 21: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

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Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Analysis Technique

• An inspection and analysis procedure was developed specifically for the pipes to be inspected.

• The procedure detailed the equipment required, the calibration standard, the operation parameters and procedure.

• Methods of identifying irrelevant indications were specifically addressed.

Data Analysis

Page 22: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Analysis Technique (Cont’d)

• ASME standard

100%

60%

20%

Page 23: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Analysis Technique (Cont’d)

• Permeability Mix

100%Standard Perm

Test Pipe

Page 24: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Analysis Technique (Cont’d)

• Defect in test pipe 17% wall loss

Page 25: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

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Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Continued NDE• Inspection of another NPS 3 in.-diameter pipe in

the plant showed an indication different from pit-like indication.

• Subsequent metallographic examination of this area revealed longitudinally-oriented crack-like defects associated with corrosion.

• The defects were up 0.025 in. deep inside the pipe, which accounted for a 20% wall loss.

Page 26: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Analysis Technique (cont’d)

Page 27: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Conclusions

Pitting was caused by chloride corrosion as a result of moisture in the liquid VCM in the pipe.

The wall loss measured from the cross section of the pit was 90%, which confirmed the eddy current inspection results. 

The inspection system can detect pits larger than 20% wall loss, which meets the 25% wall loss criteria required by the customer.

Page 28: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

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Advanced NDE Pressure

Equipment Integrity

Management

Lab Analysis

Conclusions

The system can give a reasonably good estimation of the amount of wall loss and the size of a pit within its resolution ranges.

The system can also detect crack-like defects associated with corrosion.

The system has the ability to eliminate false indications caused by permeability variations.

Page 29: Engineering NDT Advanced NDE Pressure Equipment Integrity Management Lab Analysis Development of NDT Inspection Techniques For Heavy Wall Stainless Steel

Engineering

NDT

AdvancedNDE Pressure

Equipment Integrity

Management

Lab Analysi

s

Thank You

(www.canspec.com)