electrical standards based on quantum effects

63
Electrical Standards based on quantum effects Beat Jeckelmann

Upload: others

Post on 21-Jan-2022

2 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: Electrical Standards based on quantum effects

Electrical Standards based on quantum effects Beat Jeckelmann

Page 2: Electrical Standards based on quantum effects

Outline

Introduction

Electrical units in the SI today and in the future

Part I: Josephson voltage standards and applications

Part II: Quantum Hall resistance standards and applications

Varenna 2016 / El. Standards I 2

Page 3: Electrical Standards based on quantum effects

The SI today

Stability?

„practical“

sub-system

Varenna 2016 / El. Standards I 3

Page 4: Electrical Standards based on quantum effects

The ampere definition

Varenna 2016 / El. Standards I 4

F

I = 1 A

I = 1 A

r = 1 m

l = 1 m

m

N 102 7

l

F

r

I

l

F

2

2

0

2

7

20A

N 1042

l

r

I

F

“The ampere is that constant current

which, if maintained in two straight parallel

conductors of infinite length, of negligible

circular cross-section, and placed 1 metre

apart in vacuum, would produce between

these conductors a force equal to 2 ×10−7

Newton per metre of length.”

Ampère’s law for the idealized case:

With the ampere definition and

equating mechanical and electrical

power, one obtains for the vacuum

permeability:

Page 5: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Electrical units in the SI

V I

R

IRV Ohm‘s law:

Electrical units:

Two realisations in terms of mechanical

units necessary

Today:

Ohm: calculable capacitor (10-8)

Watt: watt balance (10-8)

2

70

A

N104

Link to mechanical units

Ampere definition introduces dimension „A“

and fixes the value for µ0:

5

Page 6: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

The SI realisation of the ohm: the calculable capacitor

Thompson-Lampard Theorem (1956):

exp(C1

'

0

) exp(C2

'

0

)1

C' 0 ln(2)

1.95pFm1

Cross-capacitance identical:

6

Page 7: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Measurements:

∆L = 5 - 50 cm

∆C = 0.1 - 1 pF

u: several parts in 108

Calculable capacitor: Practical Realisations

Running projects

NMIA, BIPM, NRC, LNE

u < 10-8

7

Page 8: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

CODATA 2014:

NPL-88: u = 5.4 x 10-8

NIST-97: u = 2.4 x 10-8

NMI-97: u = 4.4 x 10-8

NIM-95: u = 1.3 x 10-7

LNE-01: u = 5.3 x 10-8

New Projects:

BIPM: u 10-8

expected 2016

Link from the calculable capacitor

to the ohm

8

Page 9: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Realization of the ohm before 1990

Complicated electro-mechanical

experiments needed to realize the

ohm

Artifacts were used to maintain the

unit:

drift in time

differences of up to several ppm

from country to country

9

Page 10: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Electrical quantum standards

Quantum mechanical effects allow the realization of highly reproducible electrical standards:

B. Josephson predicts quantized

voltage steps in superconductors (1962)

voltage standard

K. Von Klitzing discovers the quantum

Hall effect in 1980 Resistance standard

10

Page 11: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Electrical standards based on fundamental constants C

urr

en

t[m

A]

0 .1

0 .2

Volt age [ mV]

2 3

JJ

fK

ifi

e

hU J

2

Josephson effect

KJ: Josephson constant

Weakly coupled superconductors

16

12

8

4

0

RH

(kW

)

108642

B (T)

6

4

2

0

Rxx (kW

)i = 2

3

4 i

R

ei

hR K

2H

Quantum Hall effect

RK: von Klitzing constant

2D electron gas in high

magnetic field

11

Page 12: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Practical electrical units

To make best use of the good reproducibility and worldwide availability of

the quantum standards, the CIPM introduced conventional values for the

Josephson- and von Klitzing constants as of January 1, 1990.

KJ-90 = 483 597.9 GHz/ V rel. uncertainty in the SI : 0.4 ppm

RK-90 = 25 812.807 W 0.2 ppm

(now: 0.1 ppm)

Worldwide uniformity and improvement of electrical calibrations as a

consequence of the conventional units.

The uncertainty of the constants does only apply if electrical units are linked

with mechanical units.

12

Page 13: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Quantum effects and „Practical“ electrical units

Ω 812.807 2590K R

V I

R

h

e2

h

2 ef e f

QHE

SETJosephson

1-90J V GHz 597.9 483K

13

Page 14: Electrical Standards based on quantum effects

Electrical units in th «new» SI

Varenna 2016 / El. Standards I 16

h and e have fixed values (defining

constants)

RK (h/e2) and KJ (2e/h) are fixed

Quantum Hall and Josephson

standards realize the ohm and the

volt in the new SI directly (assuming

that the QHE and JV relations are

correct!)

0 has to be measured

Page 15: Electrical Standards based on quantum effects

Validity of RK and KJ relations

Varenna 2016 / El. Standards I 17

-120 -100 -80 -60 -40 -20 0 20 40

(h - hCODATA-14)/hCODATA 109

Avogadro, IAC-15

Avogadro, IAC-11

watt balance, NIST 15

watt balance, NIST 16

watt balance, NRC 15

Watt balance results rely on

QHE and JV relations

Watt balance - Avogadro

< ~ 10-8

Determination of the Planck constant

Page 16: Electrical Standards based on quantum effects

Realization of electrical units

Varenna 2016 / El. Standards I 18

h

Cs

s

V Ω A

F H

W

Cs clock

JAVS

e

QHR

Sampling,

resonant

bridges

Sampling,

AC/DC

transfer

AC voltage

AC current

SET

Page 17: Electrical Standards based on quantum effects

Outline

Varenna 2016 / El. Standards I 19

Introduction

Electrical units in the SI today

Part I: Josephson effect

DC and AC Josephson effects

Different types of Josephson junctions

Hysteretic Josephson Arrays and their applications

Programmable arrays

Pulsed driven arrays

Page 18: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Electrons in a superconductor Cooper pairing mechanism

ions

2nd electron

attracted by

charge density

Region of pos. charge

persists

passage

of electron

• Conduction electrons pair up

through exchange of “virtual”

phonons

• Interaction is isotropic

• Macroscopic wave function

describes entire electronic

system

densitypair cooper

n

ei

+ + + + + + + +

++++++++

+

+ +

+

+ + + + + +

++++++

+

+ + +

+

++ + + +

20

Page 19: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

DC Josephson effect

Insulating layer super

conductor

Y1,1 Y2,2

Quantum states in superconductor

described by Schrödinger equation:

Ei

dt

d

Two weakly coupled

superconductors:

Phase coherent transfer of Cooper

pairs

1222

2111

KEi

dt

d

KEi

dt

d

21

Page 20: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

DC Josephson effect (2)

I

V = 0

S1 S2

A small supercurrent flows through

the weak link with a corresponding

phase shift:

) ) sinsin 12 cc III

Ic: critical current of the weak link

22

Page 21: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

AC Josephson effect

I

V > 0

S1 S2

With )teVEE 221 Schrödinger eq. also gives:

)dt

d

etV

2

DC external current I > Ic

• Direct voltage across junction

• Oscillating supercurrent flows with

frequency f

Vh

efJ

2

f

Voltage driven oscillator JJ ffe

hV 0

2Mean voltage:

23

Page 22: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Josephson Voltage Standard

Microwave irradiation, frequency f, applied to junction:

Cooper pair current synchronizes with f and its harmonics

Direct voltage appears at the terminals

fe

hnV

2

• Relationship independent of

Temperature, material, polarization current…

• Tested at a level of 3 10-19

V1 ~ 145 V @ 70 GHz

V < 2.5 mV (gap energy in Nb)

24

Page 23: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Universality Tests J-S. Tsai et al.,PRL, 51, 316 (1983)

• Test of the material independence

of the Josephson relationship

• Two different superconductors

(Nb, In) and different weak links

No difference of the Josephson voltages (when biased with the same

microwave frequency on the same step) at the level of 1 10-16

Most precise test (A. K. Jain et al, PRL 58 (1987)): 3 10-19

Extremely sensitive method

)

21

211

LLLL

dtVVL

I

s

s

I1

I2

I s

V1

V2

Ls

L1

L2

h

25

Page 24: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Real Josephson junction

Cooper pair current

I = Ic sin

I = C dV/dt

I = V/R

R

C

I = I0 + I1 sin t ) )

dt

tdVC

R

tVItII c sinsin10

) ) dtdetV 2

With Josephson relation

)tiidt

d

dt

dc W sinsin 102

2

differential equation of a driven damped

oscillator

CRIh

ecc

22

c (McCumber parameter) describes damping of the Josephson oscillator

(c )1/2 quality factor LCR resonator (Josephson junction: role of L)

Chaotic properties; stable operation only in limited parameter space

26

Page 25: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

I-V Characteristics

Weakly damped

Nb-Al2O3-Nb Josephson

junction without microwave

power

V

I

2.5 mV

0.4 mA

27

Page 26: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

I-V Characteristics with microwave power (f = 70 GHz)

Weakly damped junction

c > 100

• Voltage steps at zero current

(“zero crossing” steps)

• Hysteretic

0.2

0.1

Voltage (mV)

0 1 2 3

Current (mA)

Highly damped junction

c < 1

• Different current for every

voltage step 0.1

0.2

Voltage(mV)

0

Current(mA)

1 2

28

Page 27: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Junction Arrays Idea: Increase the voltage by cascading an array of junctions in series

• Early days: not possible to produce overdamped arrays with sufficient

uniformity for polarization of the entire array on the same voltage step

Solution: Levinsen (1977) proposes zero-crossing steps (c > 100)

(SIS junctions: superconductor-insulator-superconductor)

• 1985, first 1 V array: Niemeyer, Hamilton, Kautz, NIST

• 1987, 10 V array, NIST, 14’484 junctions, ~ 150’000 voltage steps

Limited parameter space available

• External frequency has to be well above resonant frequency of the junctions,

to prevent chaotic behaviour (70 GHz)

• Current step width > induced current noise

• Dependence of non-chaotic regime on microwave power

29

Page 28: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Junction Arrays (2)

Problems to be solved:

• Homogeneous distribution of microwave power to all junctions

• Fabrication of large junction arrays with little variation in parameters

ground plane

junctions

dielectric

Microstrip line

Impedance 2 to 5 W

very low attenuation

30

Page 29: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

SIS Arrays

(superconductor-insulator-superconductor)

NIST design (similar to PTB

design):

• 20’000 junctions

• Nb/ Al2O3/ Nb technology

• Vmax = 10 V

75 GHzin

dc contact

Resistive termination

Disadvantage of SIS arrays: steps unstable and difficult to select

31

Page 30: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Measurement system

Filter FilterBiasElectronics

Frequencysynthesizer

UTC10 MHz

DUT

Nanovoltmeter

4.2 K

array

32

Page 31: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Josephson Array Standard

10 V systems commercially available

• Hypres (USA): NIST array technology

• SupraCon (Germany): PTB array technology

33

Page 32: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Comparison of JAVS

BIPM key comparison

Direct comparison of 10 V JAVS

against BIPM transportable

standard

Agreement to a few parts in 1010

34

Page 33: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

JAVS Application

Linearity check of a high-

end DVM

Agilent 3458 A

10 V range

-2

-1

0

1

2

non-lin

earity

(

V)

1050-5-10

VJAVS (V)

-10

-5

0

5

VD

VM

- V

JA

VS (

V)

gain error: 0.87(1) ppm

0.15 ppm (rel. 10 V)

35

Page 34: Electrical Standards based on quantum effects

Josephson Standard for AC voltages

Varenna 2016 / El. Standards I

36

Pulse driven JVS:

Best AC source available

Suitable for impedance

measurements

Programmable JVS:

• How to deal with transients?

PJVS AC-JVS n(t) f(t)

Page 35: Electrical Standards based on quantum effects

Josephson Standard for AC voltages

Varenna 2016 / El. Standards I

37

Page 36: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Programmable Josephson Arrays (PJVS)

+V1

-V1

Current

Advances in nanotechnologies:

• Several thousand non-hysteretic junctions with same characteristics can

be made

Overdamped junctions

• SNS junctions

(superconductor/ normal metal/

superconductor)

• SINIS junctions

(supercond./insulator/normal/

insulator/supercond.)

• Externally shunted SIS

junctions

Advantage: voltage steps can be selected precisely (by choice of bias

current) and very rapidly.

) ) fe

htntV

2

38

Page 37: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Programmable Arrays (2)

V1 2V1 4V1 8V1

Output voltage

Computer controlled bias sources

frf

• Array is divided into segments (binary sequence)

• Each segment controlled by its own bias source

• Steps –V1, 0 and +V1 in each segment selected

D/A converter with fundamental accuracy (Hamilton 1995)

39

Page 38: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

SNS array (NIST, 1997)

-20 -10 0 10 20

0.2

0.1

0.0

-0.1

-0.2

Current (mA)

Cell 5: 4096 junctionsT = 4.2 Kf = 16 GHz

+V1

-V1

0

Nb /PdAu / Nb technology

1 V array; f = 16 GHz

• 32’768 junctions

• 33 µV/junction

• LSB (128 junctions) : 4.23 mV

junctions

40

Page 39: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

10 V SINIS Array PTB

• Series array consisting of 69 120 SINIS Josephson junctions

• Step at 10 V (step width: 200 µA)

J. Kohlmann et al., IEEE Trans. Instrum. Meas. 50 (2001) 192-194.

41

Page 40: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Waveform Synthesis

Synthesized sine wave with a 13 bit PTB

Josephson array: V = 1.2 Vpp, f = 400 Hz

ts tr

s

rrms

Nt

t

6

16

Uncertainty

N = 64

ts = 39 s

tr = 250 ns

R. Behr et al, IEEE IM 54, 2005

42

Page 41: Electrical Standards based on quantum effects

Suppression of transients: Sampling and signal reconstruction

Varenna 2016 / El. Standards I 43

Accurate synchronization possible to remove data points

during the transients

Digitizer digital filter remove 50 points for each transition

limits the frequency

Average value

Page 42: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Applications

The Quantum Voltmeter

V

FilterBiassources

f = 70 GHz

Computer

Nanovolt-meter

Programmablearray

44

Page 43: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Josephson Potentiometer

IVX

Vs

fJ

JAVS 1RX

RsJAVS 2

Comparison of resistance standards

s

s

x

x

Js

Jx

s

x

V

V

V

V

n

n

VV

VV

R

R1

2

1

2

1

PTB, R. Behr et al., IEEE IM 52, 521 (2003)

10 kW in terms of the QHR (12.9 kW) to 3 parts in 109

45

Page 44: Electrical Standards based on quantum effects

Josephson Locked Synthesizer (JoLoS)

Varenna 2016 / El. Standards I 46

0

PJVS

out fV V

Page 45: Electrical Standards based on quantum effects

JoLoS: Data acquisiton and signal reconstruction

Varenna 2016 / El. Standards I 47

VPJVS: Fundamental of the DFT of the theoretical (KJ-90) waveform (calculated)

ASYN: Fundamental of the DFT of the synthesizer waveform (measured)

APJVS: Fundamental of the DFT of the reconstructed waveform (measured)

Page 46: Electrical Standards based on quantum effects

JoLoS Application: Thermal transfer measurements

Varenna 2016 / El. Standards I 48

A. Rüfenacht et al., IEEE Trans. Instrum. Meas. 60-8, 2372-2377 (2011).

Page 47: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Pulse driven Josephson arrays

Due to undefined transitions between steps:

applications of binary programmable arrays are limited to < 1 kHz

Different approach:

Change frequency in time instead of number of junctions

) )(2

tfe

hNtV

Problem: Sine-wave excitation: step amplitude decreases with

frequency

Solution (Benz and Hamilton, 1995):

Replace sine wave with pulse excitation; in this case, step amplitude

is independent of pulse repetition frequencies (simulations) for f < fc

49

Page 48: Electrical Standards based on quantum effects

Pulse driven Josephson arrays (2)

Varenna 2016 / El. Standards I 50

Single large array with N junctions distributed along a wide bandwidth

transmission line

A pulse train at frequency f generates an average voltage:

fe

hNV

2

H. Worsham, J.X. Przybysz, S. Benz, and C. Hamilton, NIST & Westinghouse, 1995

Page 49: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Pulse driven Josephson arrays (3)

Generation of complex wave forms by modulating the pulse train

with a digital word generator

51 Courtesy S. Benz, NIST

Page 50: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Bipolar operation

+I1

-I1

n =1

n =-1

V

(Benz et al., 1998)

Combination of pulse train

and sine wave bias

Resistively shunted

JJ, driven by microwave,

frequency f )

J

T

JJK

dttV1

0

0

Microwave bias

Synchronized

current bias

Quantized JJ

pulse

52

Page 51: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Bipolar pulse control

Fast switching

• Sampling frequency fs

• Code levels I1

2 ;2 mmff s

JK

f

qp

qpV

p: number of “1”

q: number of “0”

Specific frequency and phase

relationships between sampling

and drive frequencies required

53

Page 52: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Digital waveform synthesis

Ibias

Vout

–V

Time

+V

• Timing and polarity of the

modulation signal precisely

determine the voltage

waveform

• Peak to peak voltage:

J

spp

K

fNmV max

Number of junctions

54

Page 53: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Josephson Array Pulse Quantizer

RMS value of output determined by:

• Digital code, sampling frequency and number of junctions

Exact quantization if:

• Correct synchronisation of code and hf-drive, switching time << 1/f

• Transmission path to every junction independent of frequency from

dc to about 18 GHz

55

Page 54: Electrical Standards based on quantum effects

AC-JVS: Results

Varenna 2016 / El. Standards I 56 N. Flowers-Jacobs et al. IEEE Trans. Appl. Supercond., 2016.

Courtesy S. Benz, NIST

Page 55: Electrical Standards based on quantum effects

Comparison PJVS – AC-JVS

Varenna 2016 / El. Standards I 57

VSL, Delft

Page 56: Electrical Standards based on quantum effects

Comparison PJVS – AC-JVS (2)

Varenna 2016 / El. Standards I 58

B.Jeanneret et al., Metrologia 48, pp.311-316 (2011).

Page 57: Electrical Standards based on quantum effects

Application AC-JVS: Josephson Impedance Bridge

Varenna 2016 / El. Standards I 59

Present situation

Future with JB-FDB

Quad Bridge

10:1 Bridge

u = 10-9

Courtesy L. Palafox, PTB

Page 58: Electrical Standards based on quantum effects

Josephson Impedance Bridge

Varenna 2016 / El. Standards I 60

Future with JB-FDB Fully automated

Bandwidth 50 Hz – 50 kHz (10X)

Accuracy: 10-8 @ 1 kHz

JB-FDB

10:1 Bridge

Fully manual

Bandwidth 50 Hz – 5 kHz

Accuracy: 10-8 @ 1 kHz

Page 59: Electrical Standards based on quantum effects

The Josephson Bridge: Comparison R-R

Varenna 2016 / El. Standards I 61

Use as reference

12.9 kW thermostated

resistors

Range: 1 kHz to 20 kHz

Agreement < 0.1 ppm

F. Overney et al., Metrologia (2016).

Page 60: Electrical Standards based on quantum effects

Range JVS applications

Varenna 2016 / El. Standards I 62

DC

Electrical power

Temperature/ Resistance bridges

Johnson Noise Thermometry

1 10 100 1k 10k 100k 1M

10m

100m

1

10

Am

plitu

de

/ V

Frequency / Hz

•ADCs

•Thermal converters

Dyn

am

ic m

easu

rem

en

ts

Impedance bridges

Page 61: Electrical Standards based on quantum effects

Range JVS applications

Varenna 2016 / El. Standards I 63

DC

Electrical power

Temperature/ Resistance bridges

Johnson Noise Thermometry

1 10 100 1k 10k 100k 1M

10m

100m

1

10

Am

plitu

de

/ V

Frequency / Hz

ADCs

Thermal converters

Dyn

am

ic m

easu

rem

en

ts

Pulse driven arrays

Binary arrays

Impedance bridges

Page 62: Electrical Standards based on quantum effects

Varenna 2016 / El. Standards I

Summary Part I

Josephson Array voltage standards well established as

primary standards for DC voltage in the range -10 V to 10 V

I. Reproducibility: parts in 109

II. Two orders of magnitude better than realisation of the volt in

the SI

Programmable standards well established

I. Low frequency arbitrary waveforms up to 10 V better power

standards

II. Arbitrary waveforms DC to 1 MHz, with pulsed driven arrays;

voltage up to 2 V improved low voltage AC/DC transfer

impedance comparisons in the whole

complex plane

64

Page 63: Electrical Standards based on quantum effects

Thank you very much for your attention