Supplementary File
Synthesis, Characterization and Antimicrobial Studies of Novel Series of 2,4-
bis(hydrazino)-6-substituted-1,3,5-Triazine and Their Schiff Base Derivatives
Hessa H. Al-Rasheed, Essam N. Sholkamy, Monirah Al Alshaikh, Mohammed R. H. Siddiqui , Ahmed S. Al-Obaidi and Ayman El-Faham*
Table of content
Figure S1: 1H NMR and 13 C NMR for 4a
Figure S2: 1H NMR and 13 C NMR for 4b
Figure S3: 1H NMR and 13 C NMR for 4c
Figure S4: 1H NMR and 13 C NMR for 4d
Figure S5: 1H NMR and 13 C NMR for 4e
Figure S6: 1H NMR and 13 C NMR for 4f
Figure S7: 1H NMR and 13 C NMR for 4g
Figure S8: 1H NMR and 13 C NMR for 4h
Figure S9: 1H NMR and 13 C NMR for 4i
Figure S10: 1H NMR and 13 C NMR for 4j
Figure S11: 1H NMR and 13 C NMR for 4k
Figure S12: 1H NMR and 13 C NMR for 4l
Figure S13: 1H NMR and 13 C NMR for 4m
Figure S14: 1H NMR and 13 C NMR for 5a
Figure S15: 1H NMR and 13 C NMR for 5b
Figure S16: 1H NMR for 5c
Figure S17: 1H NMR and 13 C NMR for 5d
Figure S18: 1H NMR and 13 C NMR for 5e
Figure S19: 1H NMR and 13 C NMR for 5f
Figure S20: 1H NMR and 13 C NMR for 5g
Figure S21: 1H NMR and 13 C NMR for 5h
Figure S22: 1H NMR and 13 C NMR for 5i
Figure S23: 1H NMR and 13 C NMR for 6a
Figure S24: LC-MS for 6a
Figure S25: 1H NMR and 13 C NMR for 6b
Figure S26: 1H NMR and 13 C NMR for 6c
Figure S27: 1H NMR and 13 C NMR for 6d
Figure S28: 1H NMR and 13 C NMR for 6e
Figure S29: 1H NMR and 13 C NMR for 6f
Figure S30: 1H NMR and 13 C NMR for 6g
Figure S31: 1H NMR and 13 C NMR for 6h
Figure S32: 1H NMR and 13 C NMR for 6i
Figure S33: 1H NMR and 13 C NMR for 7a
Figure S34: 1H NMR and 13 C NMR for 7b
Figure S35: 1H NMR and 13 C NMR for 7c
Figure S36: 1H NMR for 7d
Figure S37: 1H NMR and 13 C NMR for 7e
Figure S38: 1H NMR and 13 C NMR for 7f
Figure S39: 1H NMR and 13 C NMR for 7g
Figure S40: 1H NMR and 13 C NMR for 7h
Figure S41: 1H NMR and 13 C NMR for 7i
Figure S42: LC-MS for 7i
Figure S43: 1H NMR and 13 C NMR for 8a
Figure S44: 1H NMR and 13 C NMR for 8b
Figure S45: 1H NMR and 13 C NMR for 8c
Figure S46: 1H NMR and 13 C NMR for 8d
Figure S47: 1H NMR and 13 C NMR for 8e
Figure S48: 1H NMR and 13 C NMR for 8f
Figure S49: 1H NMR and 13 C NMR for 8g
Figure S50: LC-MS for 7a
Figure S51: LC-MS for 7d
Figure S52: LC-MS for 7f
Figure S1: Supplementary spectrum for compound 4a (1H and 13C)
Figure S2: Supplementary spectrum for compound 4b (1H and 13C)
Figure S3: Supplementary spectrum for compound 4c (1H and 13C)
Figure S4: Supplementary spectrum for compound 4d (1H and 13C)
Figure S5: Supplementary spectrum for compound 4e (1H and 13C)
Figure S6: Supplementary spectrum for compound 4f (1H and 13C)
Figure S7: Supplementary spectrum for compound 4g (1H and 13C)
Figure S8: Supplementary spectrum for compound 4h (1H and 13C)
Figure S9: Supplementary spectrum for compound 4i (1H and 13C)
Figure S10: Supplementary spectrum for compound 4j (1H and 13C)
Figure S11: Supplementary spectrum for compound 4k (1H and 13C)
Figure S12: Supplementary spectrum for compound 4l (1H and 13C)
Figure S13: Supplementary spectrum for compound 4m (1H and 13C)
Figure S14: Supplementary spectrum for compound 5a (1H and 13C)
Figure S15: Supplementary spectrum for compound 5b (1H and 13C)
Figure S16: Supplementary spectrum for compound 5c (1H NMR)
Figure S17: Supplementary spectrum for compound 5d (1H and 13C)
Figure S18: Supplementary spectrum for compound 5e (1H and 13C)
Figure S19: Supplementary spectrum for compound 5f (1H and 13C)
Figure S20: Supplementary spectrum for compound 5g (1H and 13C)
Figure S21: Supplementary spectrum for compound 5h (1H and 13C)
Figure S22: Supplementary spectrum for compound 5i (1H and 13C)
Figure S23: Supplementary spectrum for compound 6a (1H and 13C)
Figure S24: LC-MS for compound 6a
Figure S25: Supplementary spectrum for compound 6b (1H and 13C)
Figure S26: Supplementary spectrum for compound 6c (1H and 13C)
Figure S27: Supplementary spectrum for compound 6d (1H and 13C)
Figure S28: Supplementary spectrum for compound 6e (1H and 13C)
Figure S29: Supplementary spectrum for compound 6f (1H and 13C)
Figure S30: Supplementary spectrum for compound 6g (1H and 13C)
Figure S31: Supplementary spectrum for compound 6h (1H and 13C)
Figure S32: Supplementary spectrum for compound 6i (1H and 13C)
Figure S33: Supplementary spectrum for compound 7a (1H and 13C)
Figure S34: Supplementary spectrum for compound 7b (1H and 13C)
Figure S35: Supplementary spectrum for compound 7c (1H and 13C)
Figure S36: Supplementary spectrum for compound 7d (1H NMR)
Figure S37: Supplementary spectrum for compound 7e (1H and 13C)
Figure S38: Supplementary spectrum for compound 7f (1H and 13C)
Figure S39: Supplementary spectrum for compound 7g (1H and 13C)
Figure S40: Supplementary spectrum for compound 7h (1H and 13C)
Figure S41: Supplementary spectrum for compound 7i (1H and 13C)
Figure S42: LC-MS for compound 7i
Figure S43: Supplementary spectrum for compound 8a (1H and 13C)
Figure S44: Supplementary spectrum for compound 8b (1H and 13C)
Figure S45: Supplementary spectrum for compound 8c (1H and 13C)
Figure S46: Supplementary spectrum for compound 8d (1H and 13C)
Figure S47: Supplementary spectrum for compound 8e (1H and 13C)
Figure S48: Supplementary spectrum for compound 8f (1H and 13C)
Figure S49: Supplementary spectrum for compound 8g (1H and 13C)
Figure S50: LC-MS for 7a
Figure S51: LC-MS for 7d
Figure S51: LC-MS for 7f