This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/17/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsAdvanced Sport 300 MG
N/AMatrix: Edible
Certificateof Analysis
Sample:DA00506007-001Harvest/Lot ID: 100619
Seed to Sale #N?ABatch Date :N/A
Batch#: N/ASample Size Received: 30 mg
Retail Product Size: 0.507Ordered : 05/04/20Sampled : 05/04/20
Completed: 05/17/20 Expires: 05/17/21Sampling Method: SOP Client Method
May 17, 2020 | Organic scientific llc7300 n waterway dr. MiamiFl, Usa 33143
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.074%THC/Capsule :0.375 mg
Total CBD
1.987%CBD/Capsule :10.074 mg
Total Cannabinoids
2.225%Total Cannabinoids/Capsule:11.281 mg
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.113% ND 0.036% ND ND 0.015% ND ND 1.987% 0.074% ND
1.130mg/g ND
0.360mg/g ND ND
0.150mg/g ND ND
19.870mg/g
0.740mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :1224 1.5953g 05/06/20 11:05:38 574
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 05/07/20 10:29:25Analytical Batch -DA012211POT Instrument Used : DA-LC-003 Batch Date : 05/06/20 09:01:09
Reagent Dilution Consums. ID
031820.R16 400 280670723914C4-914AK929C6-929H76262-590
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSED
Analyzed By Weight Extraction date LOD(ppm) Extracted By584 1g 05/07/20 584
Analysis Method -SOP.T.40.013 Batch Date : 05/07/20 09:27:53Analytical Batch -DA012254FIL Reviewed On - 05/07/20 10:24:14Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/17/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsAdvanced Sport 300 MG
N/AMatrix : Edible
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00506007-001Harvest/LOT ID: 100619Batch# : N/ASampled : 05/04/20Ordered : 05/04/20
Sample Size Received : 30 mgCompleted : 05/17/20Expires: 05/17/21Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDCYPERMETHRIN 0.05 ppm 1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMETHYL PARATHION 0.005 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRIN I 0.01 ppm 1 NDPYRETHRIN II 0.01 ppm 1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPINOSAD (SPINOSYN A) 0.01 ppm 3 NDSPINOSAD (SPINOSYN D) 0.01 ppm 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0 PPM 20 ND
TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 0.9915g 05/06/20 03:05:05 1082
Analysis Method - SOP.T.30.065, SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch - DA012188PES Reviewed On- 05/07/20 10:24:14Instrument Used : DA-LCMS-001_DER (PES)Batch Date : 05/05/20 12:48:04
Reagent Dilution Consums. ID041420.10 10 280678841050420.R29 76262-590050420.R30050420.R31041720.03
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/17/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsAdvanced Sport 300 MG
N/AMatrix : Edible
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00506007-001Harvest/LOT ID: 100619Batch# : N/ASampled : 05/04/20Ordered : 05/04/20
Sample Size Received : 30 mgCompleted : 05/17/20Expires: 05/17/21Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 5 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONE 75 ppm 5000 PASS ND
ACETONITRILE 6 ppm 410 PASS ND
BENZENE 0.1 ppm 2 PASS ND
BUTANES (N-BUTANE) 500 ppm 2000 PASS ND
CHLOROFORM 0.2 ppm 60 PASS ND
DICHLOROMETHANE 12.5 ppm 600 PASS ND
ETHANOL 500 ppm 5000 PASS ND
ETHYL ACETATE 40 ppm 5000 PASS ND
ETHYL ETHER 50 ppm 5000 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
HEPTANE 500 ppm 5000 PASS ND
METHANOL 25 ppm 3000 PASS ND
N-HEXANE 25 ppm 290 PASS ND
PENTANES (N-PENTANE) 75 ppm 5000 PASS ND
PROPANE 500 ppm 2100 PASS ND
TOLUENE 15 ppm 890 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
TRICHLOROETHYLENE 2.5 ppm 80 PASS ND
XYLENES-M (1,3-DIMETHYLBENZENE)
13.5 ppm 2170 PASS ND
XYLENES-M&P (1,3&1,4-DIMETHYLBENZENE)
27 ppm 2170 PASS ND
XYLENES-O (1,2-DIMETHYLBENZENE)
13.5 ppm 2170 PASS ND
XYLENES-P (1,4-DIMETHYLBENZENE)
13.5 ppm 2170 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0262g 05/08/20 07:05:02 850
Analysis Method -SOP.T.40.032Analytical Batch -DA012298SOL Reviewed On - 05/11/20 13:24:02Instrument Used : DA-GCMS-002Batch Date : 05/08/20 18:49:25
Reagent Dilution Consums. ID
1 00279984161291-124154107
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
05/17/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsAdvanced Sport 300 MG
N/AMatrix : Edible
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00506007-001Harvest/LOT ID: 100619Batch# : N/ASampled : 05/04/20Ordered : 05/04/20
Sample Size Received : 30 mgCompleted : 05/17/20Expires: 05/17/21Sample Method : SOP Client Method
Page 4 of 4
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA012189 | Reviewed On - 05/16/20 01:27:34Instrument Used : DA-LCMS-001_DER (MYC)Batch Date : 05/05/20 12:49:16
Analyzed by Weight Extraction date Extracted By585 1g 05/06/20 03:05:29 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043 / SOP.T.40.045Analytical Batch -DA012236MIC | Reviewed On - 05/11/20 08:15:20Instrument Used : (Micro) 25-27C IncubatorBatch Date : 05/07/20 08:28:03
Analyzed by Weight Extraction date Extracted By513 0.9196g NA NA
Reagent Dilution Consums. ID
022520.09 4603475C
914C4-914AK
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID050620.R01030920.01050520.R01050520.R02050520.R05050520.R04
050520.R03042720.R36
100 106557-04-091619
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 1.5CADMIUM 0.02 PPM ND 0.5LEAD 0.05 PPM ND 0.5MERCURY 0.02 PPM ND 3
Analyzed by Weight Extraction date Extracted By53 0.2514g 05/06/20 09:05:06 1022
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA012217HEA | Reviewed On - 05/07/20 08:47:39Instrument Used : DA-ICPMS-001Batch Date : 05/06/20 09:12:55
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.