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IntroductionIntroduction toto new FT/IR new FT/IR
microscopemicroscope
IrtronIrtron IRT-3000 IRT-3000
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The The requirementsrequirements forfor FT/IR FT/IR
HardwareHardware
SoftwareSoftware
ApplicationApplication
AbleAble toto acquireacquireaccurate accurate spectraspectra
Easy Easy toto useuse
DevelopmentDevelopment of ofanalysisanalysis methodsmethods
SFE-FT/IR,EG-ATRSFE-FT/IR,EG-ATR
SpectraSpectra Manager II Manager II
FT/IR-4000,6000FT/IR-4000,6000Irtron New
IR Profile SystemNew
Smart Tech
NewNew
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DevelopmentDevelopment ConceptConcept
New IR microscope New IR microscope isis developeddeveloped under under
the the followingfollowing conceptconcept
A A fullyfully automatedautomated system system
Improvement of the Improvement of the operativenessoperativeness
CostCost reductionreduction
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New New featuresfeatures of of IrtronIrtron
Up Up toto 2 2 detectorsdetectors availableavailable
CCD camera CCD camera observationobservation
Up Up toto 4 4 objectivesobjectives withwith revolver revolver
Auto apertureAuto aperture
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OpticalOptical System of System of IrtronIrtron
Direct through optics
:Eye piece
(option)
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Direct through optics
:Eye piece
(option)
Up to 2detectorsavailable
Observation :CCD cameraas standard
Cassegrainianobjective
Autoaperture as
standard
Manual samplestage
IrtronIrtron hardware hardware featuresfeatures
Up to 4objectives
available withrevolver
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System System configurationconfiguration
ObjectivesObjectives x10, x16 or x32 x10, x16 or x32 CassegrainianCassegrainian objectiveobjective, , stdstd..
ATR ATR CassegrainianCassegrainian objectivesobjectives ( (optionoption))
AuAu opticsoptics ( (optionoption))
DetectorsDetectorsmid band MCT with Nmid band MCT with N22 Dewar (15hr, std.) Dewar (15hr, std.)
narrow / narrow / widewide band MCT ( band MCT (optionoption))
DLATGS, DLATGS, InSbInSb ( (optionoption))
Auto aperture ( x, y, Auto aperture ( x, y, ) ), , stdstd..
StagesStagesManual Manual typetype, , stdstd..
Auto X-Y-Z type (Auto X-Y-Z type (optionoption : IR : IR ProfileProfile))
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DialogDialog forfor aperture aperture settingsetting
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One One pointpoint micro-measurementmicro-measurementMeasured result of IR microscope
Sample:stein on metal plate
Size : 30 x 25 um
30 x 25 um
It became clear for this stain to be the oil-based ink from the IR spectrum(reflection method).
Result of Peak PickingNo. Position Intensity No. Position Intensity 1: 1713.44 0.5256 2: 1339.32 0.2283 3: 1239.04 0.6006 4: 1092.48 0.2283 5: 1016.30 0.4605 6: 870.70 0.4195 7: 719.32 0.8514
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S/N ratio (IRT-3000)
Measurement Condition
FTIR : FTIR-4200
Objective : x16
Method : Transmission
Measurement area : 100x100
mm
Scan times : 180 times (2 min)
IRT-3000
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PolystyrenePolystyrene SpectraSpectra usingusingdifferentdifferent detectorsdetectors
Wavenumber[cm-1]
Wavenumber[cm-1]
Abs
AbsSize : 50 x 50 um
Accumulation: 540
Size : 10 x 10 um
Accumulation: 50
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Autostage
Mapping
Autofocus
Easy operation
IR ProfileSystem
Auto
validationReliability
Stresssensor
ATR Mapping
"IR "IR ProfileProfile System" System" supportingsupporting IrtronIrtron
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DialogsDialogs of IR of IR ProfileProfile System System
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Position Position adjustmentadjustment
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DialogDialog forfor mappingmappingmeasurementmeasurement settingsetting
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Multi Multi pointpoint measurementmeasurement
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ATR ATR MappingMapping OutlineOutline
Stress sensor
ATR Cassegrainian
X-Y-Z Auto stage
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New ATR New ATR CassegrainianCassegrainianobjectivesobjectives
TipTip shapedshaped ATR ATR prismprism : 0.7 mm : 0.7 mm
ATR-JCZATR-JCZ
ZnSeZnSe
ATR-JCGATR-JCG
Ge Ge
ATR-JCDATR-JCD
DiamondDiamond
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SummarySummary II. . IrtronIrtron
DetectorsDetectorsup up toto 2 2 detectorsdetectors availableavailable
ObservationObservation
CCD camera CCD camera asas standard standard
ObjectiveObjective
X 10, x16 or x32 Cassegrainian objectiveX 10, x16 or x32 Cassegrainian objective
Up to 4 objectives Up to 4 objectives withwith revolver revolver
Auto aperture Auto aperture asas standard standard
ManualManual samplesample stage stage
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SummarySummary IIII. IR . IR ProfileProfile
Auto X-Y-Z stage Auto X-Y-Z stage withwith software software
Auto Auto focusfocus
Multi point auto measurementMulti point auto measurement
Mapping and line analysisMapping and line analysis
ATR Mapping ATR Mapping withwith stress stress sensorsensorATR ATR CassegrainianCassegrainian ( ( optionoption ) ) willwill bebe requiredrequired