do concrete materials specifications address real performance? david a. lange university of illinois...

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ILLIN OIS U niversity ofIllinoisat U rbana -Cham paign ILLIN OIS U niversity ofIllinoisat U rbana -Cham paign Do Concrete Materials Specifications Address Real Performance? David A. Lange University of Illinois at Urbana- Champaign

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ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Do Concrete Materials Specifications Address Real Performance?

David A. LangeUniversity of Illinois at Urbana-Champaign

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

How do you spec concrete?

1930 “6 bag mix”

1970 “f’c = 3500 psi, 5 in slump” And add some air entrainer

2010 ?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Is concrete that simple? How simple are your expectations?

Are we worried only about strength? What about …

Long-term durability Crack-free surfaces Perfect consolidation in conjested forms

These cause more concrete to be replaced than structural failure!

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Seeking the Holy Grail

Admixtures developed in 1970’s open the door to lower w/c and high strength

Feasible high strength concrete moved from 6000 psi to 16,000 psi

Feasible w/c moved from 0.50 to 0.30 Everybody loves high strength!

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

But there are trade-offs…

Low w/c high autogenous shrinkage High paste content greater vol change High E high stress for given strain High strength more brittle

…greater problems with cracking!

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

For example: Early slab cracks

Early age pavement cracking is a persistent problem Runway at Willard

Airport (7/21/98) Early cracking within

18 hrs and additional cracking at 3-8 days

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Concrete IS complex

Properties change with time Microstructure changes with time Volume changes with time Self imposed stresses occur Plus, you are placing it in the field under

variable weather conditions There are a million ways to make

concrete for your desired workability, early strength, long-term performance

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Overview

Volume stability Internal RH and drying shrinkage Restrained stress Case: Airport slab curling Case: SCC segregation

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Chemical shrinkage

Volume stability

Volume Change

Thermal Shrinkage Creep

External Influences

Autogenous shrinkage

External drying shrinkage Basic creep Drying creepHeat release

from hydration

Cement hydration

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Chemical shrinkage

Ref: PCA, Design & Control of Concrete Mixtures

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Self-dessication

solid

water

air (water vapor)

Jensen & Hansen, 2001

Autogenousshrinkage

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Chemical shrinkage drives autogenous shrinkage

Ref: Barcelo, 2000

Note: The knee pt took place at only = 4%

The diversion of chemical and autogenous shrinkage defines “set”

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Measuring autogenous shrinkage

Sometimes the easiest solution is also the best…

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Autogenous shrinkage

-250

-200

-150

-100

-50

0

50

0 20 40 60 80 100

Age (d)

Autogenous Shrinkage (10

-6 m/m)

OPC1, w/c = 0.40SCC1, w/c = 0.39SCC2, w/c = 0.33SCC3, w/c = 0.41SCC4, w/c = 0.32HPC1, w/c = 0.25SCC2-2SCC2-slag

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Concern is primarily low w/c

0.50 0.50 w/cw/c

0.30 0.30 w/cw/c

Cement grains initially separated

by water

Initial set locks in paste structure

“Extra” water remains in small

pores even at =1

Pores to 50 nm emptied

Pore fluid pressure reduced as smaller pores are emptied

Autogenous Autogenous shrinkageshrinkage

Increasing degree of hydration

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Internal RH & Internal Drying

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Mechanism of shrinkage

Shrinkage dominated by capillary surface tension mechanism

As water leaves pore system, curved menisci develop, creating reduction in RH and “vacuum” (underpressure) within the pore fluid

Hydration product

Hydration product

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Physical source of stress

p”sy

S S

" ' 2y yF p p sΣ = + +

Water surface

1m

Pc

Vapor Diffusion

We can quantify the stress using measured internal RH using Kelvin Laplace equation

ln( )"

'

RH RTp

v− =−

p” = vapor pressure = pore fluid pressureR = universal gas constantT = temperature in kelvinsv’ = molar volume of water

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Measuring internal RH

Old way: New embedded sensors:

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Reduced RH drives shrinkageSCC4, w/c = 0.34

-100

-90

-80

-70

-60

-50

-40

-30

-20

-10

0

0 10 20 30 40 50 60 70 80

Age (d)

97.5

98.0

98.5

99.0

99.5

100.0

Autogenous Shrinkage

Relative Humidity

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Modeling RH & Stress

⎟⎟⎠

⎞⎜⎜⎝

⎛−⎟

⎟⎠

⎞⎜⎜⎝

⎛⎟⎠

⎞⎜⎝

⎛−−−=0

3

3

1

3

1

98.01(75.01

'

)ln(

kk

RH

v

RTRHaHTHTε

⎟⎟⎠

⎞⎜⎜⎝

⎛−⎟

⎟⎠

⎞⎜⎜⎝

⎛⎟⎠

⎞⎜⎝

⎛−−−=0

3

3

1

3

1

98.01(75.01

'

)ln(

kk

RH

v

RTRHHTε

0.0E+00

1.0E-04

2.0E-04

3.0E-04

4.0E-04

0 7 14 21 28 35 42 49 56

Time (day)

Drying Shrinkage (in./in./) Measured

Theoretical

Fitted

Add a fitting parameter

NOTE: The fitting parameter is associated with creep in the nanostructure

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Long term autogenous shrinkage

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

External drying stresses

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

RH as function of time & depth

Different depths from drying surface in 3”x3” concrete prism exposed to 50% RH and 23o C

3" x 3" Concrete Prism, 0.50 w/c

60

65

70

75

80

85

90

95

100

0 2 4 6 8 10 12 14

Time Days

Internal RH (%)

1/2"

1/4"

3/4"

Depth from drying surface

Specimen demolded at 1 d

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

External restraint stress superposed

ft

+ +-

Free shrinkage drying stresses

++

Overall stress gradient in restrained cement materials

+

Applied restraint stress

T=0

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Time to fracture (under full restraint) related to gradient severity

0

1

2

3

4

5

6

0 10 20 30 40 50 60 70

Specimen Width (mm)

Stress (MPa)

A-44A-44 AverageB-44B-44 AverageC-44C-44 AverageD-44D-44 Average4141 Average3838 Average3232 Average

Failed at 7.9 days

Failed at 3.3 days

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Shrinkage problems

Uniform shrinkage cracking under restraint

Shrinkage Gradients Tensile stresses on top surface Curling behavior of slabs, and cracking u

nder wheel loading

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Evidence of surface drying damage

Hwang & Young ’84

Bisshop ‘02

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Restrained stresses

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Applying restraint

LVDT Extensometer

Load cell

Actuator

3 in (76 mm)

3 in (76 mm)

Feedback Control

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Typical Restrained Test Data

Creep

Cumulative Shrinkage + Creep

-c tot sh =

c

c ttJ =)',(

( )1

n

tot el ii

ε ε=

= ∑

( )cel

E t

=

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

A versatile test method

Assess early cracking tendencies

0.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.0

0 2 4 6 8 10

Age (d)

Stress-Strength RatioOPC1, w/c = 0.40

SCC1, w/c = 0.39

SCC2, w/c = 0.33

SCC3, w/c = 0.41

SCC4, w/c = 0.34

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Chemical shrinkage

Volume stability

Volume Change

Thermal Shrinkage Creep

External Influences

Autogenous shrinkage

External drying shrinkage Basic creep Drying creepHeat release

from hydration

Cement hydration

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Now we are ready for structural modeling!

All this work defines “material models” that capture… Autogenous shrinkage Drying shrinkage Creep Thermal deformation Interdependence of creep & shrinkage

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Case: Airfield slabs

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Curling of Slab on Ground

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

HIGH STRESS

SLAB CURLINGP

NAPTF slab cracking

Material (I) Material (II)

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

¼ modeling using symmetric boundary conditions

NAPTF single slab

1. 20-node solid elements for slab2. Non-linear springs for base contact

2250 mm

2250 mm

275 mm.

Finite Element Model

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Loadings

Age(day)

14 28 42 56 7075

80

85

90

95

100

105

262.5mm

25mm

137.5mm

Temperature Internal RH

Age(day)

14 28 42 56 7018

20

22

24

26

28

30

32262.5mm25mm

137.5mm

Number are sensor locations (Depth from top surfaces of the slab)

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

DeformationX

ZY

Deformation

Displacement in z-axis(Bottom View)

Ground Contacted

Ground Contacts

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Maximum Principle Stress

Stress Distribution

Age = 68 days

1.61 MPa (234 psi)

X

ZY

What will happen when wheel loads are applied ?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Clip Gauge Setup

Lift-off Displacement

Age(day)

14 28 42 56 70

0

1

2

3

4

MeasuredModel prediction

Lift-off Displacement

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Analysis of stresses

σmax = 77 psi

Curling Only Curling + Wheel loading

σmax = 472 psi σmax = 558 psi

No Curling

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Case: Self Consolidating Concrete

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Several issues

Do SCC mixtures tend toward higher shrinkage?

How will segregation influence stresses?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

We can expect problems

Typical SCC has lower aggregate content, higher FA/CA ratio, and lower w/cm ratio

0.0

0.5

1.0

1.5

2.0

2.5

50 55 60 65 70 75 80 85 90 95 100

AGGREGATE CONTENT (%)

FA/CA RATIO

SCC Database

Mixtures studied

SCC4

OPC1

SCC3 SCC2

SCC1

Typical non-SCC

materials, according to

ACI mixture

proportioning method

FA

/CA

Rat

io

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Problems can arise

-180

-160

-140

-120

-100

-80

-60

-40

-20

0

20

0 5 10 15 20 25 30

Age (d)

Autogenous Shrinkage (10

-6 m/m)

OPC1, w/c = 0.40

SCC1, w/c = 0.39

SCC2, w/c = 0.33

SCC3, w/c = 0.41

SCC4, w/c = 0.32

Typical Concrete – “Safe Zone” ?

0.39, 37%

0.34, 34%

0.41, 33%

0.40, 32%

0.33, 40%

w/b, paste%

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Role of paste content and w/c ratio

0.39, 37%

0.34, 34%

0.41, 33%

0.40, 32%

0.33, 40%

w/c, Paste%

-1000

-900

-800

-700

-600

-500

-400

-300

-200

-100

0

0 5 10 15 20 25 30

Age (days)

Free Shrinkage (x10

-6)

OPC1, w/c = 0.40

SCC1, w/c = 0.39

SCC2, w/c = 0.33

SCC3, w/c = 0.41

SCC5, w/c = 0.34

Typical Concrete – “Safe Zone” ?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Acceptance Criteria: w/c ratio Tazawa et al found that 0.30

was an acceptable threshold In our study, 0.34 keeps total

shrinkage at reasonable levels 0.42 eliminates autogenous

shrinkage Application specific limits

High Restraint: 0.42 Med Restraint: 0.34 Low Restraint: w/c based on

strength or cost

0

100

200

300

400

500

600

700

800

900

0.30 0.32 0.34 0.36 0.38 0.40 0.42

w/cm

Autogenous Shrinkage Strain (x10

-6)

Autogenous Shrinkage (28d)

Total Shrinkage (28d)

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

0

100

200

300

400

500

600

700

800

900

30% 32% 34% 36% 38% 40% 42%

Paste Content by Volume

Autogenous Shrinkage Strain (x10

-6)

Autogenous Shrinkage (28d)

Total Shrinkage (28d)

Acceptance Criteria: Paste Content

IDOT max cement factor is 7.05 cwt/yd3 At 705 lb/yd3, 0.40 w/c = 32% paste Below 32%, SCC has questionable

fresh properties Is 34% a reasonable compromise? Application specific limits

High Restraint: 25-30% Med Restraint: 30-35% Low Restraint: Based on cost

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Segregation

SCC may segregate during placement Static or Dynamic

How does this impact hardened performance?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Consider static segregation

Specimen 8” x 8” x 20” prism

8 equal layers Each layer

assigned:CA%, E and sh

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Experiment Cast vertically to produce a

segregated cross section

Laid flat to measure deflection caused by autogenous shrinkage of segregated layer

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Results

0.000

0.001

0.002

0.003

0.004

0.005

0.006

0.007

0.008

0 2 4 6 8 10 12 14 16

Concrete Age (d)

Deflection (in)

Measured Deflection

FEM Calculated Deflection

Def

lect

ion

(i

n)

Concrete Age (d)

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Model validation

Now run model under restrained conditions to assess STRESS

Model confirms we have reasonable rules for segregation limits

HVSI = 0 or 1 is OK HVSI = 2 or 3 is BAD

0

50

100

150

200

250

300

350

400

450

0 1 2 3

HVSI Rating

Max Stress Developed (psi)

SCC1 SCC2

SCC3 SCC4

HVSI Rating

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Back to Specifications…

What is the “real performance” we need to ensure? More that strength

Spec writers need to assert more control Example: IDOT -- SCC will have limits on

segregation, min. aggregate content, min. w/c

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Specing “real performance”

How do you impose long-term requirements using short-term properties?

How do you impose limitation on long term cracking when factors are so extensive, including environment and loadings “beyond control of material supplier”?

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Performance vs. Prescription

Can Performance Based Specs do the whole job? Prescriptions…

Min. and max w/c Min. aggregate content Aggregate gradation limits

Performance requirements… Max. drying shrinkage, maybe autogenous shrinkage Permeability (RCPT ?)

ILLINOIS

University of Illinois at Urbana -Champaign

ILLINOISUniversity of Illinois at Urbana -Champaign

Last thoughts

“Times they are a’changing…” We have higher expectations We have new tools, new knowledge We are ever pushing the boundaries of

past experience