dlc report
TRANSCRIPT
The Frictional Effects of Diamond-Like-Carbon Deposited on a Substrate via Plasma Enhanced Chemical Vapor Deposition
ContentsTable of Contributions......................................................................................................................1
Introduction and Literature Review...........................................................................................2
DLC History.......................................................................................................................................2
DLC Chemical Properties:........................................................................................................ 4DLC Characteristics......................................................................................................................5
DLC Coating Processes.............................................................................................................7
DLC Applications.........................................................................................................................10
Testing Method Selection............................................................................................................12
Alternative Testing Methods.......................................................................................................13
Ball-on-Flat (Heimberg et al, 2001)...................................................................................13
Laboratory Bench Rig (Gangopadhyay et al, 2011).................................................14
Motored Valvetrain Rig for Friction Evaluations (Gangopadhyay et al, 2011).............................................................................................................................................................. 15
Twin-Disc Testing Rig (Löhr, 2006)...................................................................................16
Methodology....................................................................................................................................... 17
Calculations and Results............................................................................................................. 21
Calculations....................................................................................................................................21
Results:.............................................................................................................................................26
Discussion............................................................................................................................................33
MDF.................................................................................................................................................... 33
Metal Sheet.................................................................................................................................... 35
Comparison.................................................................................................................................... 36
Conclusions and the future of DLC Coating......................................................................38
Project Management - Critical Assessment.......................................................................40
Table of Contributions
Member ContributionAli Maasoumian - Background research on friction
- Literature review over DLC chemical properties- Research over DLC characteristics- Research over DLC applications- Testing set up and optimization
Amandeep Mankoo - Background research on friction- Testing and setup- Research over improvements on current methods- Introduction and conclusion
Joseph Mendonca - Background research on DLC history- Literature review over DLC coating methods- Testing setup and optimization- Report formatting
Mohammed Miah - Background research on testing methods- Testing and data collection- Methodology- Research on DLC future applications- Conclusion and discussions
Nakul Shah - Testing setup assessment- Testing- Data collection and calculations- Data analysis- Discussion
1
Introduction and Literature Review
The optimization of a system is a key aspect in the field of Engineering, with
continuous improvements always being made to combat efficiency, a key component
of energy loss being friction. Many of today’s methods of overcoming frictional losses
are expensive, therefore a cost-effective method of reducing frictional losses is
investigated.
Diamond-like carbon (DLC) coating is a process in which a thin film of diamond-like
carbon is deposited on a substrate in order to improve the physical and chemical
resistance of the base material. This report examines the effect that DLC coating has
on the static and dynamic friction when applied to an industrial adhesive tape, this is
done in an attempt to assess its feasibility, with the overall aim being a
commercialised friction-reducing sticky tape, which can be stuck to a variety of
surfaces. Applications may include the underside of skis and sliding drawers in
domestic or industrial furniture.
DLC HistoryHard amorphous carbon films were first mentioned by Schmellenmeier (1953). In his
investigation, the influence of an ionized acetylene atmosphere on the surfaces of
tungsten-cobalt alloys was investigated using a glow discharge system which is a
plasma formed by the passing of an electric current through a hydrocarbon
atmosphere. The aim of the experiment was to observe if tungsten carbide hard
metal surface layers could be produced. However, it was noticed that a hard
amorphous carbon film was deposited on the cathode of the direct current (DC) glow
discharge system. In a further study performed by Schmellenmeier (1956), it was
found that some of these micrometer thick layers had ‘structure-less’ regions but
others were formed of crystallites; which was identified as diamond by x-ray
diffraction.
The term ‘diamond like carbon’ was first used by Aisenberg and Chabot (1971). The
investigation focused on an ion beam deposition technique, which is the process of
applying a material to a substrate by using ion beams. The ion beam used consisted
on carbon and argon gas and when applied to the substrate, thin carbon films were
deposited on the graphite electrodes. An investigation into the properties of these
films was done and it was found that the coatings had favorable scratch and
chemical resistance as well as electronic insulation whilst being optically transparent.
2
Around this period, other studies into the properties of these amorphous carbon films
were published. Spencer et al (1976) used x-ray diffraction and transmission electron
microscopy to study the structure of these films. The findings supported the research
done by Aisenberg and Chabot as it showed the same crystalline structure but
furthered the understanding by classing these crystalline compositions as either large
or small.
Since the mid 1970s, there have been constant advancements in deposition methods
and the characteristics of these films were characterized in detail. Weissmantel et al
(1977, 1979) reported on 2 different methods for the preparation of DLC coating. The
first is the dual beam technique through which a carbon target was bombarded with
argon ions and the carbon film produced from this was simultaneously bombarded by
a second ion source. The film produced was hard and described as ‘amorphous with
crystallites in the regions exposed to the highest ion densities.’
The second method comprised of using DC hot cathode ionization to generate
hydrocarbon ions in a benzene atmosphere, which bond to a substrate that has a
negative charge bias. The films produced were hard, partially optically transparent
and electrically insulating. Weissmantel and co workers described the material
structure as a mixture of nano-crystalline components consisting of graphite and
diamond like elements.
In the early 1980’s, a new quality that DLC films possess had been discovered. Enke,
Dimigen et al (1980) reported on the friction properties of DLC coatings against steel.
It was found that in contrast to graphite, the DLC films had noticeably lower friction
coefficients, especially under conditions of low humidity.
In the early 1990s work had commenced on manipulating the deposition processes in
order to optimize the properties of the coatings. Martinu et al (1992) worked to
increase the effectiveness of the radio frequency (r.f.) process. This was achieved by
running the process whilst simultaneously operating microwave radiation. The
addition of microwaves increases the ion fluxes on the substrate, which in turn
increases the deposition rate and increases the hardness by reducing the hydrogen
content present in the deposited film.
3
Figure 1: Graph to show the number of publications on DLC between 1970 and 2012
The combination of lower friction and increased hardness and wear resistance has
led to an increase in the number of research groups working with DLC coating
technologies. Figure 1, above, displays this increase in DLC based research
publications since 1970.
DLC Chemical Properties:Diamond Like Carbon (DLC) coating is done through a process of fusion where
carbon atoms are coated over other materials. Typically the carbon layers consist of
two different atomic configurations of sp2 and sp3 with 30-50% sp2 (Graphite) and
50-70% sp3 (Diamond) compositions respectively, as described by Wallwork (2010).
The reasoning behind this is as DLC coating is done through rapid fusion, there is not
sufficient time for crystalline sp3 diamonds to be formed in the initially coated atoms;
hence the first layers consist of sp2 (Graphite) configuration over which the
crystalline structure sp3 (Diamond) configuration will be formed.
Figure 2: Different Carbon states configurations
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The sp2 configuration in graphite has more softening effects while the crystalline sp3
diamond like configuration makes the material harder. Moreover, when DLC coating
is done over metals such as Titanium, Iron or Steel, the first layer will form carbide
with the metal on which other layers of DLC will form. The formation of carbide has
great effects on making the metal resistant against wear and oxidation.
Furthermore, the sp3 DLC is very resistant to abrasive and adhesive wear which
makes it extremely suitable for applications with high contact pressure, both rolling
and sliding. Added to this, DLC coating makes materials to act as insulators with high
values of resistivity. However, if the DLC is done through cobblestone, the electrons
mat get passed through a mechanism called hoping conductivity of electrons by
quantum mechanical tunneling. This can be used to make the material act as a semi-
conductor.
DLC CharacteristicsAs stated in the previous section, with a large fraction of diamond like sp3 configured
carbons, DLC exhibits many properties associated with diamond such as high values
of hardness and chemical inertness. The former property however is also associated
with the coating process used. This is due the introduction of Hydrogen in some
5
Figure 3: sp3 configuration Figure 4: sp2 configuration
Figure 5: Nanostructure of DLC films
Figure 6: Radial distribution function for DLC
methods of DLC coating for adhesion purposes. DLC coated materials with Hydrogen
yield for lower values of hardness ranging from 15 to 20 GPa according to Weia et al
(1999). In contrast un-Hydrogenated DLC coatings give higher values of hardness
and residual stress compared to Hydrogenated coatings (Residual stress is the
internal stress locked in a material even when it is not under external forces. It is the
result of equilibrium after the material has gone under plastic deformation). In despite
of the obvious benefits of un-Hydrogenated DLC coating, low adhesion factor, which
makes them easily delaminate from a substrate makes is its crucial downside in
comparison with Hydrogenated DLC coating.
In addition to high values of hardness, the smoothness of DLC coating and its tri-
biological properties make it extremely resistant to wear. Furthermore, DLC has very
low value for coefficient of friction (0.04-0.08), which is its prominent feature for use
in industrial applications. Due to its high resistance to abrasive and adhesive wear,
DLC is suitable for applications with extreme contact pressure on both sliding and
rolling surfaces. Furthermore, due to small electron affinity, DLC has high electrical
conductivity, which makes them ideal for different application in electrical industries
as well. However, some DLC coated materials can act as semiconductors through
the mechanism of hoping conductivity Boardman et al (2008). In these materials,
electrons can move by quantum mechanical tunneling, which turns them into
semiconductors.
Added to all this, DLC coating is transparent under infrared light as it follows the
properties of Diamond. It is also biologically inert in contact with other substances.
Further enhancement of the mechanical properties of DLC can be done through
multilayer structure, although complexity and expense may also come into effect. The
following table includes some characteristics and properties of DLC coating.
6
Table 1: DLC characteristics and properties
DLC Coating Processes There are two main categories regarding current DLC coating methods. The first is
known as plasma enhanced chemical vapor deposition (CVD). CVD is the process
through which a substrate is exposed to one or more precursors, which are
compounds that participate in a chemical reaction that produces another compound.
These precursors react and/or decompose on the substrate surface to produce a
desired deposit. The most used format of CVD is plasma enhanced chemical vapor
deposition (PECVD). PECVD is where plasma is introduced to enhance the chemical
reaction rates of the precursors. This allows deposition to occur at much lower
operating temperatures which broadens its usage as the these conditions are
suitable for organic substrates which cannot stand the high temperatures usually
associated with CVD processes. Figure 7 indicates the basic layout of a PECVD
chamber. It can be seen that the plasma fill the chamber as the electric current
passes from the top electrode to the bottom where a substrate is positioned.
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Composition Typical 30-50% sp2 (Graphitic) Bond / 50-70% sp3 (Diamond) bond. Variable with process
Hardness Microhardness 10-40GPa
Sliding wear rate 5.1E -07mm/Nm2
Coefficient of friction 0.04-0.08 Dependant on substrate surface condition
improved with polished surface
Color Black
Biocompatibility Non Toxic, Non Cyto-Toxic, Non-Gene toxic, Non-
Carcinotoxic
Max operating temperature
400-500oC
Electrical resistance 400-800Wm2/k (1010ΩCm)
Chemical stability Stable in Acids, Alkalis, Solvents and Gas
Figure 7: Schematic of PECVD Chamber
A study was undergone by N. Cuong et al (2003) to investigate DLC films deposited
on polymers by PECVD. The team used a polycarbonate (PC) substrate, which is
thermally stable up to around 190°C. PC has low hardness and demonstrates poor
chemical and physical resistance. N. Cuong et al were able to overcome these poor
qualities by applying an amorphous carbon film to the surface of the polycarbonate.
The PC sample was cleaned with ethanol and dried in a vacuum desiccator. It is then
placed on the lower plate electrode that is cooled by water. This prevents the
substrate exceeding temperatures of 80°C. As a pre-deposition process, the
substrate was bombarded with argon plasma to remove any remaining
contaminations. The deposition process was then undergone with an approximate
deposition rate of 8nm/min. The films produced on the PC substrate were friction
tested using a ball on disk method, which found that hydrogenated carbon films
deposited had a friction coefficient as low as 0.3 as compared to a coefficient of 0.7
of the PC surface. Further work was also done to test resistance against organic
solvents. A drop of acetone was applied to the coating and to the PC surface for a
few seconds. After inspection, it was observed that the untreated surface had been
altered by the reaction whereas the DLC coating was not corroded.
The second categorical method is physical vapor deposition (PVD). This category
describes a variety of methods that use vacuum deposition to deposit thin films by
condensing a vaporized form of the desired coating material. There are several types
of physical vapor deposition such as sputter deposition, which utilizes a glow plasma
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discharge to eject material from a target which bonds onto a given substrate.
However, the most widely used method of PVD is cathodic arc deposition. This is
where a high-powered electric ‘arc’ is discharged at a cathode material, which blasts
away some material into highly ionized vapor, which can be deposited onto a
substrate. Figure 8 below illustrates this process.
Figure 8: Schematic of cathodic
Takikawa and Tanoue (2007) produced a review of the cathodic arc process. They
specify several different types of arcs that can be used such as a steered arc, which
is most commonly used in industry. A magnetic field is applied on the cathode
surface. This is done in order to avoid overheating of the cathode by keeping it at a
single location and it maintains uniform erosion. The paper highlights the problem
with all different arc types associated with this method; which is the formation of
‘macrodroplets’ that are a secondary emission from the cathode spot. The drops
connect to the film in the preparation and roughen its surface, which therefore
increase the coefficient of friction of the film. As a result of this, any applications of
DLC that utilize the low friction aspect of the material will require the use of CVD
rather than PVD but either method can be used if the application of the film is for
physical and chemical resistance.
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DLC ApplicationsDLC coating has been associated to make improvements in many applications due to
its profound characteristics which can imply vast developments in fields associated
with high friction and wear, as well as chemical inertness.
Figure 9: Comparison of performance of uncoated, titanium nitride coated and DLC coated drills during stainless steel machining
One of the most prominent applications of DLC coating is in high speed steel
machining and drilling. In recent uses of DLC coating in steel machining it has been
noted that that when DLC coated machines and drills were performed in comparison
with other coated and uncoated machines, they produced fourfold increase in tool’s
life and durability as investigated by Boardman et al (2008). Figure 9 illustrates the
obtained results for Comparison of performance for uncoated, titanium nitride coated
and DLC (~5% Titanium) coated drills during stainless steel machining.
Furthermore, Monaghan et al (1994) performed an investigation and found that
Diamond coatings of machinery tools are the best performing coatings in terms of
performance and durability for Aluminium and Cupper alloys as they provide the least
surface roughness and material waste. However, due to high coating costs of
Diamond, DLC coatings provide the best cost for performance value. Added to all
this, DLC coating provides significantly longer lifetime and durability as well as
chemical inertness under high temperature and friction.
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Moreover, DLC coating of metallic saws for use in bone cutting results in twice the
tool’s lifetime over alternative methods; but even more importantly it resulted in low
frictional heating and higher quality of cut and bone necrosis (killing of bone tissue)
which results for the new tissue to take cut area easily and reduced healing period
according to Makino (2009).
Another vast application of DLC coatings can be found in Engines and mechanical
components. In engine applications, DLC coating of different engine components
which are exposed to high friction and wear such as pistons, piston rings and pins,
connecting rods, valves, camshaft and followers, rockers, gear and bearings have
shown significant improvements in performance gain and durability as well as fuel
efficiency. According to a study by Wei et al (1999), DLC coating of the cams and
bearings of a 500cc formula motorbike engine resulted in 8 break horsepower gain
over the uncoated engine.
Figure 10: DLC coated cam, rocker, piston, rods and bearings
Additionally, DLC coating of the interior layer for pipes with DLC films has shown to
provide excellent hardness as well as vastly reduced coefficient of friction and wear
rate as shown by the table below (Figure 11). Application of these pipes can be found
in industries such as oil and gas, tribological and corrosion performance oriented
improvements in pump barrels, downhole pipes etc. (Kobe Steel Ltd, 2010).
Figure 11: Wear rate and coefficient of friction of DLC coated and uncoated pipes
11
Testing Method SelectionA set of criteria was constructed to provide a list of various testing methods that
would help determine the feasibility of DLC coated tape, these criteria can be
summarized as follows:
How resource intensive is the testing method?
This is significant as the pool of resources for this project is limited and any cost that
exceeds this limit would leave the project incomplete. In terms of resources this
encompasses financial budget and raw materials.
How valid is the testing method?
If this isn’t taken into consideration there is a high possibility that the project will be
moot and not provide any significant insight into the feasibility of DLC coated
adhesive tape, thus this should be the first question that is asked before any method
can be considered.
How accurate is the testing method?
This is different from validity as it indicates essentially how close the values
interpreted from the results are to the actual values, this is important in its own right
as the data obtained from an accurate testing method can be transferred and applied
in various other applications as true values.
How easily can the method be performed?
This refers to the skill cap required to perform the chosen method, this can refer to
any specialist tools that may be required to perform a certain method, whether
specific facilities are needed for the performed experiment.
With these questions taken into consideration a specific set of Design Criteria can be
obtained, a Minimalistic approach has to be taken in the selection process as the
physical resources available for the project are limited, this however cannot come at
the cost of legitimate data that is valid to draw conclusions from. The data itself does
not have to be to high level of precision and accuracy, this is because to test the
feasibility of DLC tape, the coatings only have to perform relative to other DLC
coatings of different thicknesses. The project is also short term and therefore the test
has to be relatively simple to perform thus allowing ample time for data analysis and
drawing conclusive evidence of the feasibility of DLC coated adhesive tape.
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Alternative Testing Methods
Ball-on-Flat (Heimberg et al, 2001)Heimberg et al (2001) performed reciprocating ball-on-flat friction tests, utilising a
tribometer. An investigation was carried out into the effect of time and speed on
super-low friction behaviour of DLC coatings. The experiment was designed to
achieve friction coefficients down to 0.001 at atmospheric pressure in dry nitrogen,
with the friction behaviour explained in terms of gas adsorption. The coatings were
prepared by low temperature, plasma assisted chemical vapour deposition to 1µm
thickness on sapphire and steel balls, and on steel flats. The ball was loaded against
the flat to 9.8N. Each track was initially run-in for 1000 cycles at constant sliding
speeds, in order to find an average value for the friction coefficient.
The aim of this experiment was to achieve super-low friction, and therefore carried
out to a high degree of accuracy. Friction coefficients as low as 0.007 were obtained
at high speeds, which were slightly higher than expected. This was due to the
interaction time between the surfaces. At shorter test times the average friction
coefficient decreased to 0.003. This particular method takes a relatively time-
consuming approach to calculate the friction coefficient. Due to this, a more time-
effective method to calculate the average friction coefficient was developed. The
same method of applying the DLC coating, PCVD, was also used. However in the
ball-on-flat experiment, the coating was applied onto metal, whereas we are applying
the coating to tape. A different coating thickness was also used for the ball-on-flat
experiment.
Figure 12: Ball-on-Flat
Pin-on-Disc
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Kano and Yoshida (2010) carried out pin-on-disc tests, in which ultra-low friction of
DLC coating with lubricant was investigated. Both reciprocating and rotating sliding
tests were conducted. The experiment was designed to investigate the theory that
reducing the mechanical friction in an engine would improve the fuel economy, and
the effect that this method would have on the friction between the cam and follower
of an engine. Three types of coating were applied to each surface, with and without
lubrication, in order to find the best combination for optimal friction coefficient. While
it was vital to the proposed experiment, this procedure requires extra machinery and
funding as well as copious amounts of time. The results showed that the ta-C(T)
coating, coupled with the oleic acid lubrication, provided the lowest friction coefficient.
When considering the practical applications of the DLC coated sticky tape, lubrication
can be factored out as it is irrelevant.
Figure 13. Pin-on-Disc Sliding Test
Laboratory Bench Rig (Gangopadhyay et al, 2011)The test utilised a Plint TE77 test rig. An uncoated, reciprocating polished cylinder
was loaded against a coated steel flat, with test duration of one hour, conducting
tests with and without lubrication. The aim for this experiment was to understand the
interactions of lubrication additives with DLC coating. As stated previously, the use of
lubrication is irrelevant for the adhesive tape tests. While the method of polishing to
decrease surface roughness is useful in obtaining the desired results, it is difficult
and time-consuming to polish the tape and therefore this process will not be carried
out. However, wiping the tape with disinfectant after each test run will be necessary
as it is a quick process and allows for smoother contact between surfaces. The
14
cylinder was loaded to the flat at 240N, whereas the sliding test will not require any
load, allowing for a simpler method. Results for this testing method showed that the
friction coefficient decreased with time. This contradicted the ball-on-flat method, due
to the use of lubricants. Results also showed that unlubricated tests had a lower
friction coefficient overall. A rise in oil temperature also gave higher friction
coefficients. However the surface roughness did not have much effect on the friction
coefficient, with no visible wear observed on either contact surface.
Figure 14. Plint PE77 Test Rig (Gangopadhyay et al, 2011)
Motored Valvetrain Rig for Friction Evaluations (Gangopadhyay et al, 2011)A rig was constructed in order to represent an actual engine. This method of testing
the effect of lubricants on DLC coatings is highly expensive due to the technology
applied and materials used. Aside from conducting lubrication tests, the rig was run
at various speeds in order to evaluate friction torque, resulting in lengthy tests.
Results showed that the friction torque decreased with increasing engine speed,
suggesting the system operates in a mixed lubrication regime. The polished buckets
showed substantial friction reduction at all speed, confirming the importance of
surface roughness. The unlubricated DLC coating test showed significant reduction
in friction coefficient compared to the steel-steel pairing, due to the formation of a
transfer layer. The friction coefficient was slightly higher with oil than without, and the
wear was higher with DLC coating than without, in lubrication tests.
15
Figure 15. Motored Valvetrain Rig (Gangopadhyay et al, 2011)
Twin-Disc Testing Rig (Löhr, 2006)Wear tests were carried out on different DLC coatings under lubricated and dry slip-
rolling friction in a twin-disc testing rig. The analysis of acoustic emission (AE)
provided an easy and comfortable tool for monitoring the wear life of DLC coatings.
Steel samples with a thin DLC coating were tested under both lubricated and dry slip-
rolling friction in an Amsler-type twin-disc wear tester. Two disc specimens formed
the test setup, rolling against each other with a slip of approximately 10%. A pressure
of up to 2.3GPa was observed in the centre of the contact area. A steel bearing
served as the substrate of the DLC coating as well as the material of the counter
body. Only the cylindrical specimen was coated with an interlayer and a DLC-coating
using AE.
The experimental setup is simpler than other testing methods, as it uses two discs,
one of which is coated. The main difference is that it incorporates a sensor, which
measures the acoustic emissions. Acoustic emissions such as this are related to the
irreversible changes that a material undergoes in its internal structure.
16
Figure 16: Twin Disc Wear Tester (Löhr, 2006)
Depending on the intended application, testing methods for DLC coating will differ. A
test was carried out to investigate the effect that DLC coating has on the frictional
properties of orthodontic wires. Two types of wire (nickel-titanium and stainless steel)
were coated with DLC. Three types of brackets, a conventional stainless steel
bracket and two self-ligating brackets, were used for measuring static friction. DLC
layers were observed by three-dimensional scanning electron microscopy (3D-SEM),
and the surface roughness was measured. Frictional forces and surface roughness
were compared by the Kruskal-Wallis and Mann Whitney U-tests.
This method is carried out on a relatively small scale due to the intended application.
Two materials were used for coating. Our experiment involved the use of steel and
MDF as the counter surface for the DLC coating. (Muguruma et al, 2011)
MethodologyAs mentioned prior the testing method is required to meet a few specifications before
it can be considered as the chosen method. A factor to take into consideration is that
the data analyzed is relative, this means that systematic errors that maintain a
constant effect on all results are irrelevant, as this will not affect the result’s worth as
they are still valid for the purpose of this investigation.
The chosen testing method involves a metal block of dimensions
79mmx50mmx20mm and weight 623 grams placed on a ramp that can be adjusted
17
in slope angle at a range of intervals until points of both static and dynamic friction
can be observed.
The metal block will have tape attached to its long faces with different thicknesses of
DLC coating, all of which will be tested and compared to one another. The ramp had
to be built using two separate panels of MDF, both of dimensions
800mmx27mmx12mm attached together using a flexible metal hinge, the hinge
allowed for the ramp itself to be adjustable. For the first set of testing, a separate
wooden block was used as a slider to achieve fixed variation in slope angle. This
method however only allowed for a very small range of different slope angles and
also lacked the level of precision that was necessary when adjusting the slope angle,
also it required manual movement increasing the effect of human error on the results
and thus making the results less reliable.
Thus a new method of adjusting the slope angle would be required, instead of using
a wooden block as a manual sliding mechanism, a scissor lift of appropriate
dimensions was used instead, this piece of equipment provided a much larger range
of heights while providing precise height adjustment thereby allowing for more
accurate observations.
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Figure 18: The different thicknesses of DLC coated tape with no coating on the left 0.8 microns in the middle with 1.2 microns on the right
Figure 20: Wooden block used as slider
Figure 17: Metal block
Figure 19: Constructed Incline Plane
The MDF surface would also need to be taken into consideration as it was providing
inconsistent results as well as the observation points exceeding the large range of
the scissor lift, this meant that a surface with a lower coefficient of friction was
necessary so that the observation points occur at smaller angles that the scissor lift
can reach, to achieve this a metal sheet was attached to the MDF surface and was
tested following the same parameters as the MDF surface.
With the metal block placed at a fixed point on the ramp, the ramp was moved
steadily through a range of increased slope angles whilst being stopped at regular
intervals. At these intervals energy was applied to the system in the form of a simple
tap to the testing rig at a fixed location, after the tap the metal block would be
observed to see if it had reached a certain point, the points that require observing are
when static friction occurs and when dynamic friction occurs.
This method of testing, as the analysis is relative, requires consistency in the defined
points (Datum points) in order to yield valid results since the results are only
compared to each other. With this taken into account the point of static friction has
been quantified for this experiment as the point when the metal block moves a
considerable distance and then stops, a considerable distance in this case is
approximately half the length of the block. The point of dynamic friction is much
19
Figure 21: Scissor lift as used in experiment
Figure 22: Metal hinge used for the ramp
Figure 23: Sheet Metal used as surface
Figure 25: Diagram representing the use of similar triangles to calculate the angle
easier to quantify and observe, as it is the point that the metal block begins moving
freely without stopping, in essence friction has been overcome.
When it comes to measuring the actual results, the desired information is the incline
plane angle with the horizontal, however measuring this angle manually inputs a lot
of human error, to avoid this basic trigonometry is used to calculate the angle
instead, to further reduce human error the elevated height is only measured from a
predetermined datum point that is constant throughout the experiment. The reason
that measuring the length is unnecessary is because the triangles are similar,
therefore the angle will remain constant, this helps reduce human error by reducing
the number of manual measurements that need to be taken thus making it more
effective in providing valid data.
A Metal Block
B Scissor Lift
20
G DC
A
F
E
B
Figure 24: Datum point for height measurements
Figure 26: Experimental rig set up
C Wooden Ramp
D Metal Sheet
E Dial
F Metal Hinge
G Datum Point
Calculations and Results
CalculationsThe aim of this experiment is to obtain the friction coefficient values for the different
surface types. This was achieved by using calculations for an inclined plane, such as
the weight components. Figure 27 shows how the experiment was modelled
mathematically for the analysis. Table 3 shows the definition of the notation from the
model.
Figure 27: Mathematical
Notation Definition (unit)
m Mass (kg)
mg Weight (N)
mgcosθ = N Normal/Reaction forces (N)
Mgsinθ Driving force (N)
f Frictional force
θ Plane angle (degrees)
In the
experiment, the values that were obtained are the ‘adjacent’ and ‘opposite’ distances
of the right angle triangle. As mentioned in the methodology the adjacent distant was
21
Table 2: Experimental rig components
Table 3: Notations and definitions of mathematical model
kept constant at 400mm in order to reduce the factor of error in the obtained data.
Table 4 shows the values obtained from the experiment for an MDF surface, and
table 5 shows the values obtained from a steel plate surface.
Table 4: Experimental values of MDF
Using the trigonometric function ‘tan’, where tan (θ )= oppositeadjacent , the plane angle can
be calculated, as shown in table 3 to 2 . The excel formula used is:
=DEGREES(ATAN(Opposite/Adjacent)). Excel does its trigonometric calculations in
radians, whereas the angles was preferred in degrees.
22
Table 5: Experimental values of Steel Plate
MDF
Static Dynamic
A
(mm)
O
(mm)
A
(mm)
O
(mm)
metal 400 77 400 140
400 73 400 127
400 71 400 126
400 72 400 140
400 70 400 113
thin 400 84 400 91.5
400 85.5 400 90
400 88.5 400 89.5
400 88 400 89
400 88.5 400 90
thick 400 80.5 400 86
400 81 400 83
400 79 400 85
400 80 400 83
400 78 400 82
Steel Plate
Static Dynamic
A
(mm)
O
(mm)
A
(mm)
O
(mm)
tape 400 90 400 101
400 92 400 101
400 95 400 100
400 90 400 107
400 91 400 103
thin 400 86 400 96
400 84 400 96
400 85 400 95
400 85 400 95
400 86 400 96
thick 400 80 400 90
400 79 400 92
400 77 400 93
400 79 400 92
400 80 400 93
The next parameter that needs to be calculated is the driving force. The driving force
is the component of the metal blocks weight that is dragging the block down the
slope. The mass of the block is a constant value that is weighed to be 0.623kg. Using
this mass value, and the value of constant gravitational acceleration, the weight of
the steel block can be calculated using a simplified Newton’s second LawF=ma
where F is the force, m is the mass and a is the acceleration . This makes the weight
of the steel block 6.11163 N. This force is pulling the block downwards, perpendicular
to the floor, not the inclined slope as this is an effect of gravity which pulls objects
towards the earths centre. The driving force is the force vector that is parallel to the
inclined slope. This is calculated via simple trigonometry by multiplying the weight of
the block by the sine of the plane angle:mgsin (θ). This parameter is very important
when comparing static and dynamic friction. The driving force for a static friction test
theoretically is also equal to the frictional resistance force applied by the two
surfaces, to stop the block from slipping down the slope. As the angle is increased
23
Table 6: Plane angle for all tests
MDF Metal Plate
static dynamic static dynamic
Ө
(degrees)
Ө
(degrees)
Ө
(degrees)
Ө
(degrees)
Metal/Tape 10.90 19.29 12.68 14.17
10.34 17.61 12.95 14.17
10.07 17.48 13.36 14.04
10.20 19.29 12.68 14.98
9.93 15.77 12.82 14.44
thin 11.86 12.88 12.13 13.50
12.07 12.68 11.86 13.50
12.48 12.61 12.00 13.36
12.41 12.54 12.00 13.36
12.48 12.68 12.13 13.50
thick 11.38 12.13 11.31 12.68
11.45 11.72 11.17 12.95
11.17 12.00 10.90 13.09
11.31 11.72 11.17 12.95
11.03 11.59 11.31 13.09
gradually, so is the driving force component. The angle is increased until it is
observed that the block reached the static point of friction as defined in the
methodology section, which for the purpose of this testing is more convenient. This
demonstrates that the driving force has now equalled or ever so slightly surpassed
the frictional resistance value. This value is very important when working out the
friction coefficient µ. For the dynamic tests, the static frictional resistance is used
because theoretically, this value is constant for the same two frictional surfaces. The
Driving force is shown in table 5, to 2d.p.
The other component that the weight of the block produces is the force that the block
presses perpendicular to the inclined plane. This force keeps the block planted on to
the inclined surface. According to Newton’s third law of motion, the inclined plane is
applying an equal force back onto the block. This force is known as the reaction
force. This can be calculated by using simple trigonometry again and with the same
formula as the driving force, except a cosine function is used:mgcos(θ). This is useful
as it has a direct link to the calculation of the coefficient of friction. This is also shown
in table 7.
MDF Metal Plate
Driving
Force
Reaction
Force
Driving
Force
Reaction
Force
Metal/Tape 1.16 5.96 1.34 5.93
1.10 5.96 1.37 5.93
1.07 5.95 1.41 5.93
1.08 5.96 1.34 5.90
1.05 5.96 1.36 5.92
thin 1.26 5.98 1.28 5.94
1.28 5.98 1.26 5.94
1.32 5.98 1.27 5.95
1.31 5.98 1.27 5.95
1.32 5.98 1.28 5.94
thick 1.21 5.99 1.20 5.96
1.21 6.00 1.18 5.96
1.18 6.00 1.16 5.95
1.20 6.00 1.18 5.96
1.17 5.99 1.20 5.95
24Table 7: Weight components
The friction coefficient is calculated using the formula:FR=μ× R, where FR is the
frictional resistance, µ is the coefficient of friction, and R is the reaction force exerted
by the inclined plane. It is this parameter that we expect to minimize using the DLC
coating. This means that less force is required to move the object down the inclined
slope. As mentioned previously, the frictional resistance for dynamic tests will be the
same as the static tests, as that is the maximum friction experienced. Table 8 shows
these values, and table 9 shows the average of the 5 repetitions for each test.
Table 8: Friction coefficients for all tests
The Metal Block
25
Table 9: Averages of all tests
MDF Metal Plate
Static Dynamic Static Dynamic
µ µ µ µ
metal 0.1925 0.200273 0.225 0.226402
0.1825 0.188367 0.23 0.231183
0.1775 0.183234
0.237
5 0.238184
0.18 0.18769 0.225 0.22723
0.175 0.179127
0.227
5 0.229068
thin 0.21 0.210826 0.215 0.216166
0.21375 0.214254 0.21 0.211353
0.22125 0.221367
0.212
5 0.213641
0.22 0.220116
0.212
5 0.213641
0.22125 0.221426 0.215 0.216166
thick 0.20125 0.201803 0.20 0.201019
0.2025 0.202699
0.197
5 0.198816
0.1975 0.198084
0.192
5 0.194071
0.2 0.200294
0.197
5 0.198816
0.195 0.195375 0.2 0.201347
MDF Metal plate
static dynamic static dynamic
metal 0.1815 0.187738 - -
tape - - 0.229 0.230413
thin 0.21725 0.217598 0.213 0.214193
thick 0.19925 0.199651 0.1975 0.198814
Results :
1 2 3 4 50.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
Data trend of static tests with MDF
metalthinthick
test number
coef
fici
ent
of fr
icti
on
Figure 28: Data for each repetition of the experiment for static friction using MDF
26
L
D
H
D = 20 mmL = 78 mmH = 51 mmArea = 0.00156 m2
Mass/Weight = 0.623kg/6.11163NThe Area is defined as the surface area for one of the surfaces that will be making contact with the inclined plane for the purpose of testing, therefore this means that these faces will be the ones that are DLC coated as well.
1 2 3 4 50.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
Data trend of Dynamic tests with MDF
metalthinthick
test number
coef
fici
ent
of fr
icti
on
Figure 29: Data for each repetition of the experiment for dynamic friction using MDF
metal thin thick0.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
Data trend of static tests with metal, thin and thick, on MDF
test1test2test3test4test5average
Testing element
coef
fici
ent
of fr
icti
on
Figure 30: Comparison of data spread for each testing element and the averages, for
static tests on MDF
27
metal thin thick0.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
Data trend of Dynamic tests with metal, thin and thick, on MDF
test1test2test3test4test5average
Testing Element
coef
fici
ent
of fr
icti
on
Figure 31: Comparison of data spread for each testing element and the averages, for
dynamic tests on MDF
1 2 3 4 50.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
0.24
0.25
Data trend of static tests with Metal plate
Tapethinthick
test number
coef
fici
ent
of fr
icti
on
Figure 32: Data for each repetition of the experiment for static friction using Metal
plate
28
1 2 3 4 50.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
0.24
0.25
Data trend of Dynamic tests with Metal plate
tapethinthick
test number
coef
fici
ent
of fr
icti
on
Figure 33: Data for each repetition of the experiment for dynamic friction using Metal
plate
tape thin thick0.150.160.170.180.19
0.20.210.220.230.240.25
Data trend of static tests with metal, thin and thick, on Metal plate
test1test2test3test4test5average
Testing element
coef
fici
ent
of fr
icti
on
Figure 34: Comparison of data spread for each testing element and the averages, for
static tests on Metal plate
29
tape thin thick0.15
0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
0.24
0.25
Data trend of dynamic tests with metal, thin and thick, on Metal plate
test1test2test3test4test5average
Testing element
coef
fici
ent
of fr
icti
on
Figure 35: Comparison of data spread for each testing element and the averages, for
dynamic tests on Metal plate
metal thin thick0.16
0.17
0.18
0.19
0.2
0.21
0.22
0.23
Average µ for MDF
staticdynamic
Testing element
Coef
fici
ent
of F
rict
ion
Figure 36: Comparison of averages of static and dynamic tests, for all testing
elements on MDF
30
tape thin thick0.18
0.19
0.2
0.21
0.22
0.23
0.24
Average µ for Metal Plate
staticdynamic
Testing element
Coef
fici
ent
of F
rict
ion
Figure 37: Comparison of averages of static and dynamic tests, for all testing
elements on Metal plate
MDF Metal plate0.21
0.211
0.212
0.213
0.214
0.215
0.216
0.217
0.218
MDF vs metal plate Thin comparison
thin StaticThin Dynamic
Testing Surface
Coef
fici
ent
of F
rict
ion
Figure 38: Comparison between static and dynamic values for both testing surfaces,
for the thin testing element
31
MDF Metal plate0.196
0.1965
0.197
0.1975
0.198
0.1985
0.199
0.1995
0.2
MDF vs metal plate Thick comparison
thin StaticThin Dynamic
Testing Surface
Coef
fici
ent
of F
rict
ion
Figure 39: Comparison between static and dynamic values for both testing surfaces,
for the thick testing element
1 2 3 4 50.204
0.206
0.208
0.21
0.212
0.214
0.216
0.218
0.22
0.222
0.224
MDF vs Metal in thin static and dynamic
static MDFdynamic MDFstatic Metaldynamic Metal
Test Number
Coef
fici
ent
of F
rict
ion
Figure 40: Comparison of all test values for thin element
32
1 2 3 4 50.186
0.188
0.19
0.192
0.194
0.196
0.198
0.2
0.202
0.204
MDF vs Metal in thick static and dynamic
static MDFdynamic MDFstatic Metaldynamic Metal
Test Number
Coef
fici
ent
of F
rict
ion
Figure 41: Comparison of all test values for thick element
Discussion
MDFFigures 28 and 29 display a comparison of the experiments. For different testing
elements, it is noticeable that for both the static and the dynamic tests the metal
surface has the lowest coefficient of friction throughout all 5 repetitions. This deviates
from our expectations, as we expect the metal to demonstrate a higher frictional
coefficient than the DLC films. These anomalous results could be attributed to the
actual surface of the metal block that made direct contact with the inclined plane.
This MDF surface, after repeat testing, may have formed slip lines that are parallel
with the motion of the block, hence increasing the size of the plane angle that the
points of static/dynamic friction occur. This is because the surface finish is not taken
into consideration when calculating the value for the coefficient of friction, therefore
the minimal contact on the MDF board caused by the slip lines reduce the friction.
This factor becomes even more valid when taking into account that the DLC coated
tape overlapped the metal surface. This means that for the DLC friction tests, the slip
lines were not a present factor as the surface dimensions were different and
therefore could not be utilized in a similar manner as when the bare metal surface
was used.
33
The MDF board is made from bonding multiple wood fibres together using an
adhesive, thus the testing surface was not ideal since it is not uniform throughout the
wooden surface. Therefore each test had to start at the exact same position on the
MDF board; otherwise it would not have been an accurate test. However this method
of controlling variables produces the issue of repetitive wear on the relevant surfaces.
Subsequently after each test, the position used as the initial starting position would
receive some wear, thus making that particular location smoother than before
causing a systematic error that will have a significant effect on further testing.
Another by-product of repetitive use is physical erosion of the DLC coating, which
makes the film surface rougher and thus increases friction. We see this in action for
the thin element especially; which demonstrated surface damage after the first few
tests. This does plateau after test 3, suggesting that the wear and tear on the
elements was only done to the weak bonded regions as the material that had not
been worn away was intact, this however could be a factor of the irregularities on
both the finish of the metal block and the surface of the inclined plane.
The results displayed by figures 28 and 29, show that all three elements had very
similar friction coefficients after the first test, as none of the previously mentioned
biases were in play, therefore that set of results are the most reliable. From here, the
difference between the coatings increase as the aforementioned biases begin to take
effect; increasing systematically after every test. Despite this, the results followed the
expected trend, in that the thicker DLC element experiences less friction than the thin
equivalent. This is the natural assumption as a thicker DLC coating means that the
properties of the DLC substrate are more prominent, due to the fact that they are less
influenced by the metal surface underneath.
Figures 30 and 31 show how the data is spread for the respective testing elements,
and the average trend for each element. These graphs show how widely distributed
the data is for the static and dynamic tests. We can see that the results for the static
and dynamic friction have very little difference in terms of range between various
results, suggesting that both of the respective friction coefficients are similar. Also the
similarities between the results make it seem as if they are consistent repetitions,
except for one point in the metal element testing set that occurs at a significant
distance above its relative test values, seeming to deviate away from the rest. This
anomalous result could very well be deduced from human error as the plain metal
surface was the first set of tests performed and therefore the testing procedure was
not well versed at this point. Figures 28 and 29 share the same evidence in terms of
34
the comparison between the dynamic and static values. Although it does look like an
outlier, it there is a valid explanation for its presence. We also see the previously
mentioned anomaly of the metal element producing a much lower friction coefficient
in comparison to the other two elements
Metal SheetThe data obtained from the tests which implemented the metal sheet (graphed and
shown in figures 32-35) are much more promising than the MDF results. Figures 32
and 33 show the data trends for the three testing elements; uncoated tape, thin DLC
coating, and thick DLC coating. In these tests, plain adhesive tape was used as a
testing element instead of the metal surfacing.
The first reason for applying the tape is that it has a much more uniform surface in
comparison to the metal surface. This means that there are less parameters that
could potentially affect the results. Another reason for using the tape is because the
metal sides used for testing were already used for the DLC coating strips. The tape
was the same tape that was used as the adhesive for the DLC coatings, therefore the
comparison was more consistent. If the metal surface was required to be used, the
DLC coatings would have to be removed, and the surface would have to be polished
to remove any adhesive stuck onto the metal. This process could greatly deter the
results of the experiment.
The figures 32 and 33 show exactly what would be expected from the experiments
for each test. The figures show that the highest resistance to motion is the plain tape
surface, next is the thin coating, and finally the thick coating. This observation is
consistent with every repetition of the test, as well as the static and dynamic tests.
The variation from the average test values is not significant, confirming the reliability
of the results. There is a slight abnormality in tape results for the third test, where the
friction coefficient is noticeably higher than the rest of the results. This is in fact
expected, because during the test we realised that the tape accumulated some
contamination, which needed to be removed before any other tests continued. After
removing this small abnormality the results show a much more consistent trend. By
using the metal sheet, we removed the effect of compression on the fibres on the
MDF. The effects of this change are shown in the figures, as the data trend for all
friction tests does not decrease, staying more parallel to the horizontal axis.
35
Figures 34 and 35 show how the data is spread for each testing element, as well as
how each element compares with the other. Both graphs show practically identical
graphs, meaning that the differences between the static and dynamic friction
coefficients are miniscule. For each testing element, we see that there is extremely
small deviation from each result, thus demonstrating the reliability of these
experiments. The trends of averages for each element are very satisfying. It shows
that as the DLC coating gets thicker, the friction of the surface reduces too. This is
represented with a linear looking line on the graph. This is exactly what we expect
from these tests and shows that choosing the tape did in fact deliver more concise
results.
Comparison Figure 36 and 37 show the comparison of the averages of static and dynamic
coefficients of friction, for each testing element and testing surface. Straight away, we
see that there is a concern with the metal results on the MDF, and this issue has
been discussed above. The metal plate graph shows a more comforting negative
correlation as the DLC coating increases. A notable observation would be that for all
test averages, the static friction is always lower than the dynamic coefficient of
friction. This is a desirable result, duly because of the definitions of static and
dynamic frictions the static friction is always lower than dynamic friction. For the MDF
metal test, the dynamic is substantially higher than the static. This could be because
of non-uniformity of both the MDF and the metal surface. This means that a greater
driving force is required to overcome many contacts of the grooves on both surfaces,
that keep 'hooking' onto each other, stopping the steady flow to characterise the
result as dynamic.
Figures 38 and 39 display a comparison of the different testing surfaces with both
static and dynamic, with respect to the thin and thick DLC coatings. It is seen
immediately that the MDF has a much higher coefficient of friction compared to metal
plate. This is mostly because of the high friction surface of the MDF where the
surface is not uniform and it is comprised of fibers instead of a smooth one piece
surface. The other noticeable fact is that the difference of static and dynamic for both
coatings, is much larger with the metal plate than the MDF wood. A reason for this
could be because the metal surface or the coating was not cleaned properly, thus
leaving contaminants, making it much harder for the block to slide down the inclined
plane, increasing the result for dynamic tests. Even with this difference, when
36
comparing numerically, the difference is practically non effective, as the difference is
in the thousandths.
Figures 40 and 41 show how the coefficient of friction varies with the static and
dynamic tests for the two testing surfaces, with respect to the DLC coating thickness.
It is show in both graphs that for most of the tests, the MDF has a higher coefficient
of friction than the metal plate, but there are two tests (test 1 for thin, and test 5 for
thick) where the metal plate has a higher static and dynamic coefficient of frictions.
These could be abnormalities, although the differences are excusable, as they would
not have any practical difference to the experiments. Figure 14 shows that as the
tests progress, the coefficient of friction increases for the static and dynamic MDF.
The reason has been mentioned previously, where the coating on the adhesive
would get scratched after each test, thus increasing its resistance to surface slip. We
see that every other trend on both graphs has some oscillations but numerically, they
are all stable towards an average figure that doesn't deviate away from all the
results. This shows the consistency and reliability of the results obtained from the
experiment.
Other conditions could have an impact on the results of the experiments, such as the
humidity and the temperature of the room. The humidity would affect the MDF, and
the resistance of micro condensation on the steel and the testing elements. The
temperature would mostly have an effect on the metal block, as it would increase the
surface area, thus spreading or concentrating the force and resistance over the area.
This could have an effect on the pressure exerted by the weight of the block, as it is
inversely proportional to area.
37
Conclusions and the future of DLC Coating
The main objective of this investigation was to discover how feasible DLC coated
adhesive tape is as a low friction material. The idea behind it being that the DLC tape
can be conveniently placed on various different surfaces and help enhance some
sort of feature using its valuable properties, an example being the inside of a chest of
drawers to help the drawers to be extracted smoothly.
With this in mind the testing showed, although with the anomaly of the metal block
itself, that the DLC coating possessed superior properties in terms of being a low
friction material. This can be concluded from the relatively much lower coefficients of
friction obtained from the DLC coated materials, this claim can be supported further
by the thicker DLC coating showing more promise than the thinner coating, therefore
a positive relationship exists between the thickness of the DLC coating and the
coefficient of friction.
However there is still a lot left desired from how the testing method that was
performed. A key benefit of this method was its simplicity, however this criteria was
so critical due to the time constraint that it came at the cost of a truly accurate and
precise testing method. A key drain in the precision was the means of applying
energy to the system, this force was generated by a human element and
subsequently is prone to human error. In hindsight, this step of the experiment could
have been automated using a small electric fan of some sort that applies a
continuous subtle force, this would have reduced the time significantly between
intervals and allowed for more accurate results that in turn would provide clearer
evidence. Another source of error was the manual increase of the plane angle. This
could have been automated as well, but more importantly the plane angle was not
sensitive enough to the rotation of the dial, and as a result significantly reduced the
precision of the recorded data.
Other researchers previously performed similar testing that shared the same premise
albeit with one key difference. This difference was that not only the DLC coating
applied was applied, but various different lubricants were tested on top of the coating
as well, this was in an attempt to find the best combination that provides the most
useful properties. The reason this statement is relevant is because these lubricants
could in effect enhance the feasibility of DLC coated tape, thus a more in depth study
that involved unlubricated and lubricated DLC tape could enhance the conclusions
drawn from this experiment.
38
Not only was the precision of the test lacking but the test ranged between too few
materials and therefore a further in depth study will be required to truly assess the
feasibility of DLC coated tape. A material that would help increase the depth of the
study is Teflon, a material commonly used for its low friction properties which seems
an obvious choice for further comparative testing. This would provide an interesting
perspective on the future of DLC coating applications, as proof of DLC coatings
properties being superior then popularly used materials used in industry speaks
volumes about other possible uses of DLC coating. The current applications of DLC
coatings have been discussed in previous sections, these applications being
prevalent in many areas especially the medical and automotive industry.
However all these uses are involved heavily in the industrial sector where it has been
recognised as highly valuable to informed minds, and an area it will continue to
expand its presence. This insinuates that there is still a lot of possibilities for DLC to
grow, one of these possibilities being in the tertiary sector, this is especially so for the
DLC coated tape, as the ability to conveniently reduce the friction of a surface
implicates many possible uses that have yet to be delved into, thus making it a very
interesting prospect.
As promising as the future of DLC is, there are still some issues that need to be
addressed before it can be fully utilized. One of these issues is the possible
thicknesses of the coatings, currently these are approximated at 2 micrometres.
Naturally this is a big obstacle as the properties of the DLC coated tape are directly
related to the thickness of the coating, at this point in time there is research being put
into reducing these internal stresses, thus implicating thicker coatings in the future.
Overall the future of DLC coated tape seems very positive, there is a lot of room left
for DLC coatings to develop yet it is already being heavily utilized in industry, if this
success translates to the tertiary sector then the tape will become even more
relevant as a temporary coating of DLC from a worn away DLC film or allowing the
coating of a less conventional object.
39
Project Management - Critical Assessment
Task NameStart Date End Date
Research 12/01/15 30/01/15Future Applications 12/01/15 30/01/15History of DLC Coating 12/01/15 16/01/15Alternative Testing Methods 14/01/15 21/01/15Physical Attributes 19/01/15 23/01/15Chemical Compositions 19/01/15 21/01/15Overall Friction Research 28/01/15 30/01/15
Testing 02/02/15 20/02/15Experimental Setup 02/02/15 03/02/15MDF Testing 03/02/15 06/02/15Metal Plate Testing 09/02/15 13/02/15Further Tests to exclude Anomalies 16/02/15 18/02/15Data Processing 19/02/15 20/02/15
Report Writing 23/02/15 06/03/15Introduction 23/02/15 25/02/15Literature Review 23/02/15 27/02/15Methodology 23/02/15 25/02/15Results 23/02/15 24/02/15Discussion and Conclusion 02/03/15 06/03/15Project Management 02/03/15 03/03/15
Table 10: Project time management
Overall the project ran smoothly, there was a week delay in acquiring a lab to
perform our experiment. However this was counteracted by the extra background
research performed during this week, which subsequently reduced the time taken to
write up the literature review. The tasks could have been delegated better, a method
of this would be to give members more tasks, but in smaller sections so that the team
could perform the write up in a more synchronized approach. With that said the lag
that occurred between tasks due to this was almost negligible, this is because the
plan was designed to leave excess time for the final formatting of the report as a
countermeasure for any possible uncertainties.
If this project was repeated, even though the task was set over a brief period,
perhaps an extra week could have been utilised to obtain the means to perform a
well-controlled experiment. Such components include the humidity and temperature,
which had a definite impact on the obtained results. Following this extra time would
be needed to make the recommendations mentioned in the conclusion section.
40
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