din deutsches institut für normung e. v. 1 © 2005 din deutsches institut für normung e. v. wp 6...
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DIN Deutsches Institut für Normung e. V.
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WP 6
Harmonization Work for Standards
Norbert Siegel DIN Deutsches Institut für NormungR&D Phase Standardization Department
Athens Project Meeting May 16th, 2009
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Contents
• introduction
• work package 6.1
• work package 6.2
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DIN Deutsches Institut für Normung e. V.
DIN German Institute for Standardization
DIN is a registered non-profit association supported by the private sector.
On the basis of a contractual agreement with the Federal Republic of Germany,
DIN is the responsible German standards body in European and international
standards work.
Source: DIN Annual Report 2006
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R & D Phase Standardization
2007 EU Vice President
Günter Verheugen
• “Standardization is a link between inventions
and wide industrial usage“
• “Standards are not enough used for the transfer
of R&D results at the time being.”
DIN Deutsches Institut für Normung e. V.
Example: Nanotechnology
Measurement and test standards (including terminology)
Terminological definitions facilitate communication and cooperation in nanotechnology and nanotechnology research
Agreements on new methods of measurement and testing are essential for scientific progress in nanotechnology research
Quality and safety standards
A means to protect users and consumers and raise acceptance levels, with a positive impact on market growth and a desirable knock-on effect for research
The role of standards in research
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Work package
6.1 Survey on existing standards in relevant peripheric areas
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31 pages report:
Standards and standardization for nanotechnologies and related fields
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NSBs and international standardization
National
European
Inter-national
BSI AFNOR CNI …
Sectors
engineering
construction
services
IT
aviation
optics
fine mechanics
...
electrotechnics
electronics
telecommunication
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Standardization Bodies Nanotechnologies 1
ISO TC 229 Nanotechnologies
IEC TC 113 Nanotechnology:Standardization for electrical and electronicsproducts and systems
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Standardization Bodies Nanotechnologies 2
CEN TC 352 Nanotechnologies
DIN NA 062-08-17 AA Nanotechnologien
Other national mirror committees:BSI, AFNOR, NBN, NEN, DS, UNI...
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Non-formal Standardization
• ASTM Committee E 56 Nanotechnology
• IEEE (Test methods for CNT)
• SEMI (Nanoimprint lithography)
• OECD Working Party on Manufactured Nanomaterials
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Main results updated
for Athens demonstration course lecture
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Work package
6.2 Analysis of parameters and measuring techniques relevant for standardization
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Work package 6 -
questions to ask
a What parameter or measuring technique is relevant ?
b Whom does it concern ?
c Who could cooperate ?
d What mean of standardization is adequate ?
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Step 1:
Needs for standardization seen in the project
"uncensored" list of the needs seen by the different project partners
co-operation with WP 2
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Naples University
developed non standard methods for the structural analysis
measurement protocols and/or strategies and software programs which allow users of X-ray diffraction equipment for a correct and complete interpretation of diffraction data from standard SAXS-WAXS measurements
Sample preparation for
TEM
AFM
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Research Institute on Membrane Technology, ITM-CNR:
theoretical preparation of bulk and interface models of dense amorphous polymeric materials
experimental stabilisation of ‘universal’ criteria for membrane preparation and measurement treatment
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Bulgarian Academy of Sciences -
Central Laboratory Physico-Chemical Mechanics
standardize their rheological tools (procedures) for control of the dispersity and the superstructure of nanocomposites. Reference polymer nanomaterials with well defined viscosity would be desirable
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University of Rostock,
Institute of Physics, Polymer Physics
A standard procedure for determination of rigid amorphous fraction should be standardized.
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National Technical University of Athens
need of standard reference materials (polymer nanomaterials) with well characterized morphology (spatial distribution of nanoparticles) and chemistry (polymer filler interactions) to quantify the response by their experimental techniques in terms of these parameters.
The work on these items will show which techniques and test procedures are appropriate for standardization.
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Romanian Academy, P.Poni Institute of Macromolecular Chemistry
Department of Physical Chemistry of Polymers
for mechanical properties of the films a reference material would be desirable
standard for measurements of zeta potential in aqueous and non-aqueous dispersions
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Sopra-S.A.
always a need for new standards, procedures, terminology and materials.
the topology of the surface, at the nano-micro size should be standardized for roughness, BRDF, PSD. Reference materials would be useful for most of the available techniques of today and tomorrow as for surface porosimetry.
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Charles University in Prague, Faculty of Mathematics and Physics
Department of Macromolecular Physics
To tackle individual problems, rather specialized scientific and often new solutions are needed, which cannot be standardized. Regarding test methods, they do not see a need for standards. but a nomenclature for nanostructures and nanoparticles would be helpful. (Note: There are activities at ISO level.
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GVS S.p.A:
40069 Zola Predosa (Bologna)
GVS proposes to standardize all test procedures regarding filtration media used in GVS
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NanoBioMatters Ltd., Spain
NanoBioMatters uses a great deal of test and measuring methods, like particle size distribution measurements (laser diffraction), thermal analysis (TGA, DSC), spectroscopic analysis (FTIR, UV-vis), oxygen and vapour transmission rate measurements, optical and electron microscopy (SEM, TEM), colorimetry, X-ray diffractometry, humidity measurements, antimicrobial tests, migration tests, and compostability.
NanoBioMatters thinks, that all test procedures used should be standardized.
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Step 2:
What actions already started could be taken as a basis for standardization activities?
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What measuring method
is used by several NaPolyNet partners?
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Differential scanning calorimetry -
common test method in the project
Research for calibration of DSC is done at Scite and Rostock University.
Romanian Academy, National Technical University of Athens and Charles University and NanoBioMatters are using the method.
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Discussion meeting at SciTe Leuven,
March 11th, 2009
Prof. Vincent Mathot, SciTe and Katholieke Universiteit Leuven
Dr. Geert Vanden Poel, DSM Resolve, The Netherlands
Dr. Albert Sargsyan, DSM Resolve, The Netherlands
Mr. Thijs Pijpers, ScTe and K.U. Leuven, Belgium
Dr. Yvo Leest, SciTe and K.U. Leuven, Belgium
Mr. Norbert Siegel, DIN Deutsches Institut für Normung, Germany
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"Towards a Recommendation for Temperature Calibration of Fast-Scan Calorimeters"
The works of SciTe and DSM Resolve form a very valuable basis. Further investigations should be performed and attempts to get involved a few other researchers should be done to substantiate results. A draft recommendation for temperature calibration of Fast-Scan Calorimeters should then be elaborated, which could form the basis for a specification or standard.
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NaPolyNet Research Group Calibrants FSC
Concerning the calibrants to be scrutinized: these should preferably have an onset or peak maximum temperature which:
• suits all calorimeters, meaning for the whole range of scan rates;
• should be usable in both heating and cooling;
• do not show any supercooling phenomena.
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Invitation to other DSC experts to join
SciTe, the Netherlands / K.U.Leuven, Belgium
Universität Rostock, Germany
Vrije Universiteit Brussel
Tallinn University of Technology, Estonia
Virginia Polytechnic Institute and State University, U.S.A.
DSM Resolve, the Netherlands
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Ask NaPolyNet partners using DSC
to test calibration method
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Other activities:
Jean-Louis Stehle, SOPRA S.A.
CO-NANOMET effort
group of thin films and structured surfaces lead by professor Richard Leach of NPL (UK)
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Norbert Siegel
R & D Phase Standardization
e-mail: [email protected]
DIN German Institute for Standardization
Burggrafenstr. 610787 Berlin
GERMANY
http://www.din.dephone: +49 30/2601-2343fax: +49 30/2601-42343
Thanks for your attention!