developed methods
TRANSCRIPT
Separation of antivirals using organic solvents blending technique
Ledipasvir in mixture with Copovidone 1- Sofosbuvir 2- Ledipasvir copovidone
3- Naphthalene (internal standard)
Gradient elution:
1-Paracetamol2-Phenylephrine HCl3-Guaifensine4-Methyl paraben sodium5-Propyl paraben sodium
qualificative and quantitative analytical method for analysis of preservative in co-trimoxazole suspension via gradient elution:
1-Sodium benzoate2-Methyl paraben sodium3-Propyl paraben sodium
Gradient method for rapid washing out interference of doxycycline after elution of principle peak:
1-EDTA disodium
Isocratic elution method for separation of Oxybutinin HCl and preservatives is syrup:
1- Methyl paraben sodium2- propyl paraben sodium 3- Oxybutinin HCl
1- Pseudoephedrine HCl2- Chlorpheniramine maleate
on C8 packing
Separation of butylated hydroxyl-touene from ointment bas after ectraction:
1- Butylated hydroxyl toluene
1- Amprolium
Separation of B1, B6 by ion pairing
1- Pyridoxine HCl2- Thiamine HCl
Separation of Critical pair 1, 2 with resolution Rs = 3 and K for the last peak = 8 by isocratic method
1- Lidocaine HCl2- Methyl paraben3- Triamcinolone acetonide4- Propyl paraben
1-Methoxaline2-Chlorochresol
Vitamine B12 ampoul and propyl paraben as preservative
1- Cyanocobalamine2- Propyl paraben
1-Caffeine2-Clorpheniramine maleate3-Dextromethorphane
GC method
1- n-butanol2-propylene glycol
GC method
Separation done by ion pairing technique and its effect on folic acid molecules:
1- Folic acid 2- Cyanocobalamine
1- Cyanocobalamine2- Folic acid
C8 packing with 10um particle size
C18 packing with 5 um particle size
Separation of 1,2 princple peaks on C8 packing with 10um particle size and reversed elution sequence of the same two peaks by the same mobile phase on C18 packing with 5um particle size
1- Amprolium2- Ethopabate
Qualification and quantification method for analysis of preservatives in Phyto extracts
1- Potassium sorbate 2- sodium benzoate 3- Methyl paraben sodium
Thyme extractGuava extract
Fennel extract
Eucalyptus extract