designing robust parameters for injection-compression ... · light-guided plate; regression model....
TRANSCRIPT
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 93
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
Designing Robust Parameters for
Injection-compression Molding Light-guided Plates
Based on Desirability Function and Regression Model Tsung-Yen Lin
Fu Chun Shin Machinery Manufacture Co., LTD Tainan, Taiwan
Ming-Shyan Huang*
Department of Mechanical and Automation Engineering, National Kaohsiung First University of Science and Technology,
Kaohsiung, Taiwan
e-mail: [email protected]
*Corresponding author
Abstract-- This work describes a robust injection
compression molding parameter design method that uses linear
regression model and desirability function to reduce the effect of
environmental noise on injection molded parts quality. The
design objective was to achieve a uniform geometry and
dimensions of light-guided plate (LGP) after injection molding.
In this study, an experimental 2.5-inch LGP injection
compression molding was performed to test the feasibility of the
desirability function, regarding its construction of a composite
quality indicator that represents the quality-loss function of
multiple qualities. Firstly, the experimental design and ANOVA
methods were employed to select parameters that affect part
qualities and adjustment factors. Secondly, a two-level,
statistically-designed experiment using least squared error
method was performed to generate a regression model between
part quality and adjustment factors. The mathematical model
was then used to optimize process parameters. The experimental
findings show that the robust process parameters generated by
the proposed method yield a better uniform production quality
than the initial and thus improved and uniform production
quality, which validates its feasibility.
Index Term-- Desirability function; injection molding;
light-guided plate; regression model.
I. INTRODUCTION
A light-guided plate (LGP) is a key component of
backlight modules in liquid crystal displays that directs light
propagation to enhance luminance and uniformity. The
replication effect of the microstructures distributing on the
surface of LGPs determines the optical performance. For
v-grooves microstructures, the depth of the melt filling has a
strong correlation with the luminance of LGPs [1]. Although
injection molding (IM) is one of the most common processes
for manufacturing microfeatured parts, it has some inherent
problems [2-4]. The primary difficulty is that molten polymers
in a tiny cavity instanteously freeze once they touch the
relatively cooler cavity wall. Increasing the plastic
temperature, mold temperature, injection speed, and packing
pressure may enhance the luminance performance of an LGP
[5, 6] However, residual stress exists in LGPs, and the
uniformity of the microfeatures remains a problem with IM.
Injection compression molding (ICM) was developed to solve
these problems [7].
ICM introduces a compression action into the filling
process. With a reliance on pressure transmitted from the glue
sprue, pressure is also imposed by a compression action from
the mold wall. This process has many advantages, including
even packing, less molding pressure, less residual stress, less
molecular orientation, less uneven shrinkage, less density
variation, less warpage, and better dimensional accuracy than
found with the IM process. On the basis of these advantages,
ICM is typically used to fabricate parts requiring a high
accuracy and no residual stress, such as LPGs. For instance,
Wu and Su [8] who used ICM to reduce the shrinkage of
LGPs, found that the mold and barrel temperatures and
injection speed were the key parameters for enhancing the
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 94
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
accuracy of the optical components and eliminating shrinkage.
Shen et al. [9] applied ICM to mold 2-inch LGPs. Their
investigation demonstrated that the replication effects of
microstructures were improved with increasing plastic
temperature and were dependent on the proper compression
distance and speed.
Traditionally, parameter setting for injection compression
molding relied on statistical analyses and experimentation,
computer-aided simulations, or operator experience [10, 11].
However, if the setting for producing molded parts approaches
the specification limits, the process is easily affected by
environmental variation, which reduces the yield rate. In such
a case, the parameters are inadequate, and the process is not
robust. Other methods such as fuzzy theory and artificial
neural network (ANN) that have been proposed to address
such problems generally require substantial data [12-14]. For
instance, ANN is an empirical modeling technique that
mimics the nature of biological neural network systems and
possesses the ability to learn using learning algorithms such as
back propagation. An accurate representation of the process
can be obtained by training the network using just
experimental data, without precise understanding and
development of a rigorous mathematical model. Because of
the aforementioned benefits, various applications of ANN
have been reported for controlling the injection molding
process [15, 16].
The Taguchi method and response surface method have
been developed to target a single quality by designing
experiments to optimize process parameters [17-20]. However,
the Taguchi method of experimentally searching for optimal
process parameters is confined to the design ranges of factor
levels. The response surface method has no such limitation
despite its more complex experimental design.
In practice, seeking the ideal process parameters and
focusing on multi-quality characteristics is difficult but
generally necessary. When studying multi-quality
characteristics, i.e., numerous correlated quality characteristics,
experimental data may be contradictory and data analysis may
be difficult. Principal component analysis (PCA) can convert
data for multi-quality characteristics into several independent
quality indicators. Some of these indicators can then be
selected to construct a composite quality indicator that
represents the mathematical function of the required
multi-quality characteristics. However, if any of the multiple
principal components have eigenvalues exceeding one being
selected, the feasible solution generated by PCA may not
satisfy each quality indicator. To resolve this problem, Liao
[21] proposed the weighted principal component (WPC)
method of estimating quality by the accountability proportion
of PCA. Another approach, suggested by Derringer and Suich,
is the desirability function (DF), which redefines composite
quality [22]. The desirability function approach is one of the
most widely used methods for solving the multi-quality
characteristics problem, first introduced by Harrington [23].
This technique involves estimating each of the characteristics
with response surface functions and then using a
transformation routine to simplify the problem into a single
measure of performance. A number of researchers have
suggested improvements to the desirability function approach
over the past four decades [24]. This work used the DF
method of generating composite quality indicators. A
regression-model based searching method was then used to set
the robust injection molding parameters proposed by Huang
and Lin [25]. This method first uses DOE and ANOVA
methods to select the main parameters affecting parts quality
as adjustment factors. A two-level statistically designed
experiment using least squared error method is then performed
to generate a regression model between parts quality and
adjustment factors. Based on this mathematical model, this
study employed the steepest decent method to optimize
process parameters. A 2.5-inch injection-compression molding
experiment were then performed to verify model performance.
II. DESIGN OF ROBUST PARAMETERS
Figure 1 shows the proposed robust parameter searching
method, which includes the following three phases: (1) setting
the composite quality indicator, (2) executing full factorial
experiments, and (3) searching for robust process parameters.
The three phases are discussed in detail below.
A. Phase 1 – Setting the Composite Quality Indicator
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 95
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
Data containing information about multi-quality
characteristics were first collected and normalized to generate
dimensionless values, each of which is between 0 and 1. If the
quality requirements differ, the corresponding normalization
may differ as well: (1) larger-the-better - the target value of
quality objectives is uncertain but was expected to be large, (2)
smaller-the-better - the target value of quality objectives was
uncertain and was expected to eventually be small, and (3)
target-the-best – the target values of quality objectives were
certain and were expected to be achieved.
Second, the DF was used in this phase to convert
observed data into a composite quality indicator, which
represents a mathematical model of multi-quality
characteristics. The desirability function method proposed by
Derringer and Suich [22] suggests that the composite quality
indicator can be defined as
n
i
n1
idDF1
/ (1)
where, ‘n’ denotes the number of quality characteristics; the
DF value becomes zero if one of the di is zero. It becomes one
only if all instances of di are one. The di represents the
desirability value of the ith
quality characteristic defined by
Derringer and Suich[22]
as follows:
USLii
USLiiLSLi
t
LSLiUSLi
LSLii
LSLii
i
xx
xxxxx
xx
xx
d
,
,,
,,
,
,
1
0
(2)
where ix represents the mean value of the ith
quality
characteristics; USLix , and LSLix , are the upper
specification limit and lower specification limit of the ith
quality characteristics, respectively. The value t is the
relaxation factor, and its value is set between 0 and 10.
Adjustment factors are selected according to the
contribution percentage of experimental factors to the
composite quality indicator , which is determined by
ANOVA method. The adjustment factors have two distinct
characteristics: (1) a change in adjustment factors caused by
environmental interference substantially affects parts quality.
If the adjustment factors are controlled, the required product
quality is assured. By varying adjustment factors, this research
discovered a process window that enables adjustment of
selected factors within the window so that molded parts meet
their quality specifications. (2) If the process parameters
within the process window obtain parts with insufficient
quality, the range is further adjusted until quality requirements
are met.
In this phase, the composite quality indicator is
generated using many quality indicators with different
adjustment factors. However, this work examines only the
three most important adjustment factors. The factors are used
again in phases 2 and 3 to optimize the process parameters.
The steps in phase 1 can be summarized as: (1) normalize the
measurements - after performing the suggested Taguchi design
experiment, normalize the observations of each quality. (2)
Determine - by using DF for the above normalized
observations, the composite quality DF can be generated using
Eq. (1). (3) Select the three most significant adjustment factors
- adjustment factors are selected according to their
proportional contribution to the composite quality indicator as
revealed by ANOVA analysis. These adjustment factors were
then used as the experimental factors in the 2K full factorial
experiments in phase 2, where K is less than 3 considering
experimental cost.
B. Phase 2 – Executing Full Factorial Experiments
As mentioned above, environmental noise may degrade
the quality of injection molded parts. For quality
characteristics to meet quality specification limits, the process
window must be robust and allow varying adjustment factors.
By varying the adjustment factors caused by environmental
interference and by performing the 2K full factorial
experiments, a robust process window can be identified. The
experimental runs were designed to combine the extreme
points of a three-dimension process window. If a defect occurs
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 96
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
at extreme points in the process window, a better region can be
found by using the steepest decent method to relocate the
parameter settings.
The steps of phase 2 are: (1) design the 2K
full factorial
experiments - the experiments were designed according to the
number and the possible ranges of adjustment factors. The
initial central point for 2K
full factorial experiment was
obtained by referring to the optimal parameter setting of DOE
suggested in phase 1. (2) Obtain the new new by using PCA
for observation after normalization - the new quality indicators
new are obtained. (3) Check robustness - if all the new
for
running 2K
full factorial experiments meet the quality
specification levels, this means that the set-points of the
process parameters of this experimental group could be robust
for the new. However, if the robustness confirmation fails at
this point, the next step is to repeat phase 3 and search for
another set of process parameters by employing the regression
model-based robust parameter search method.
C. Phase 3 – Searching for Robust Process Parameters [25]
After establishing a regression model based on the
relationship between the process parameters and quality
observations, the steepest decent method was used to
determine the distance and direction to the target. For any
given quality observation, y and k number of process
parameters were assumed to significantly affect quality, such
as k21 ,x,,xx . The sample data of full factorial experiment
in the previous phase could be used to fit the regression model.
Therefore, the following matrix can be used to obtain the data
sample that fits the model:
εXβY
(3)
n
2
1
y
y
y
Y ;
nkn2n1
2k2221
11211
xxx1
xxx1
xxx1
k
X ;
k
1
0
β (4)
where Y represents the vector of observation, which may be
DFnew
or wnew
here; X represents the matrix of experimental
runs; xnk represents the kth
process parameter in the
experimental run ‘n’. β represents the vector of estimated
coefficients of the regression model, and ε represents the
random error vector.
The β vector can be estimated by the least squared error
method as follows:
YX'XX'β1
2
1
(5)
The composite equation of the relationship between the
process parameters and the product quality can then be
determined. Additionally, Y and matrix X in Eq. (8) must be
converted into Eq. (9) to get coefficient β in the regression
model.
The steps of phase 3 are as follows: Step 1: establish the
regression model – Eq. (7) represents the relationship between
process parameters and parts quality. The Y and X in Eq. (8)
can also be substituted into the following equations:
8
2
1
y
y
y
Y ;
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 97
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
11111111
11111111
11111111
11111111
11111111
11111111
11111111
11111111
X (6)
The X matrix contains the values 1 and -1, which represent the
upper and lower levels of each control factor, respectively.
The second, third, and fourth columns represent control factor
levels x1, x2, and x3, respectively. The fifth, sixth, and seventh
columns represent interaction effect levels x1 to x2, x1 to x3,
and x2 to x3, respectively. The eighth column indicates the
interaction effect among x1, x2, and x3. Entering vector Y and
matrix X into Eq. (9) obtains the coefficient vector of the
regression model, β. Step 2: estimate the responses for all
possible treatments in the varying ranges. The set-point of the
process parameters (or the predicted points of the robust
molding parameters) and the least resolution of machine
control are used as the basis for arranging all possible
treatments in the varying ranges. For example, if there are
three adjustment factors and if the upper and lower limits are
five times the least resolution of the injection molding
machine, the number of treatments is 5K. Step 3: determine
whether or not the inference process should be continued - this
step determines whether or not the inference of the robust
molding parameters should continue. By substituting all
treatments to construct coefficient vectors of the regression
model and to generate predicted values, stopping the inference
process has two conditions: either all predicted values meet
the quality specifications or only some predicted values do. In
the latter case, the set-point should be selected in the inference
process before proceeding to step 4. In the former case, phase
2 is performed to test robustness. Step 4: Infer the next robust
molding parameter - set the search direction by using steepest
decent method. The forward distance relies on the least
resolution of the machine control. Return to step 2.
III. EVALUATION OF 2.5-INCH LGP INJECTION
COMPRESSION MOLDING
A. Experimental Setup
This study analyzed the injection compression of a
2.5-inch LGP, which is characterized by V-shaped
micro-structure. The objective of the experiment was to
replicate these micro-structures. Figure 2 shows that the
light-guided plates was 55 mm long, 41 mm wide, and 0.7 mm
thick. The V-shaped micro-structure had a depth of 15 μm, a
width of 52 μm, and an included angle of 120°. The LGP
stamper was clipped to the core of the mold and was filled by
a fan gate. The mold design was single cavity with two
cooling channels. The molding material was PMMA (Japan),
and the molding machine was a FANUC ROBOSHOT α-30iA.
Injection compression molding technology was used to
experimentally increase the replication ability of the
micro-structure. The eight experimental parameters included
filling speed, melt temperature, mold temperature,
compression distance, compression speed, holding pressure,
holding time and cooling time, and the Taguchi’s L18
orthogonal array was used for verification. Table 1 shows the
combinations of the eight parameters in the L18 orthogonal
array and measured observations. Three samples were
obtained in each experimental run. Figure 3 shows the points
of the molded micro-structure of LGP that were measured by a
3D profiler. The two observed objectives were based on the
average and range value of micro-structure height of the nine
measured points. The measured points were fixed in the same
micro-structure by making clips, and the average range and
maximum deviation in range were larger than 13.5 m and
smaller than 0.41 m, respectively, which was in accordance
with industrial specifications.
B. Taguchi Analysis
Table 2 shows the L18 experimental results of 2.5-inch
LGP injection compression molding, including the average
normalized values of average/range of nine-point heights and
the composite quality indicator DF. Of these eighteen
combinations of Taguchi orthogonal array, the best
combination was that in Exp. No. 3. Table 3 shows the
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 98
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
ANOVA results for these DF values. Since the results showed
that compression distance, compression speed, and cooling
time significantly affected the DF values, these three factors
were selected for adjustment.
Tables 4(a) and 4(b) show the results of the full factorial
experiment for the first two inferences of robust parameters. In
the two failed tests in the full factorial experiment, the set
points were compression distances of 5.0 mm and 3.9 mm,
compression speeds of 100% and 98%, and cooling times of
45 s and 44.5 s. The DF values in the tables did not meet all
robustness criteria in this phase. Thus, the search was repeated
until a set-point that met the robustness criteria was found (see
Table 4(c)).
C. Verification
The additional verification was performed to test the
robustness of the optimal process parameters found by the DF
method. The two set points, the initial central point of Table
4(a) and the robust central point of Table 4(c), were used to
inject fifty molds as measurement samples, i.e., the initial
setting of robust process parameters were compression
distance of 5 mm, compression speed of 100%, and cooling
time of 45 s. The robust process parameters were compression
distance of 4.8 mm, compression speed of 99.6%, and cooling
time of 45.4 s. results of robustness testing. Figures 4(a) and
4(b) show the normal distribution of quality characteristics in
terms of probability density function. The dashed and solid
lines indicate the initial setting of process parameters and the
robust setting of process parameters, respectively. In this case
study, the initial setting of process parameters obtained almost
unqualified LGP for the average 9-point micro-structure
height, and eighteen of fifty parts were unqualified within the
range (Table 5). In contrast, the performance of the proposed
method for optimizing process parameters generated 100%
qualified products. Thus, the average value and standard
deviation of part qualities were substantially improved by the
proposed method.
IV. CONLCUSION
This work proposed a robust parameter searching
method that not only identifies the set-point of robust
parameters of an injection molding process for multi-quality
characteristics, but also meets the requirements of
multi-quality characteristics of molded parts. A light-guided
plate experiment was performed to examine this method. The
proposed search method was based on a DF method that can
successfully construct a composite quality indicator, which
represents the mathematical model of multi-quality
characteristics and a regression model-based search method
that can reflect variables to adjust search distance and
direction.
The proposed method has five major advantages:
1) The operator is not required to use complex experimental
designs.
2) The regression model for describing the mathematical
relationship between part quality and process parameters is
simple and the inference of robust process parameters is
efficient.
3) The ratio of products disqualified due to unstable
machines and non-uniform materials is decreased, and the
effectiveness of the molding process is improved.
4) The treatment applied in the full-factorial experiments can
be confirmed to ensure that the molding process is robust.
5) The search for robust parameters is not restricted to the
designed levels of controlled factors.
In summary, the experimental results indicate that the
proposed method effectively solves the problem of
multi-quality characteristics, significantly improves the
stability of the molding process, and increases yield.
REFERENCES
[1] Lin, T.H.; Isayev, A.I.; Mehranpour, M. Luminance of
injection-molded V-groove light guide plates. Polym. Eng. Sci. 2008,
48, 1615-1623.
[2] Xu, G.; Yu, L.; Lee, J.; Koelling, K.W. Experimental and numerical
studies of injection molding with microfeatures, Polym. Eng. Sci. 2005,
45, 866-875.
[3] Sha, B.; Dimov, S.; Griffiths, C.; Packianather, M.S. Investigation of
micro-injection moulding: Factors affecting the replication quality, J.
Mater. Process. Technol. 2007, 183, 284-296.
[4] Giboz, J.; Copponnex, T.; Mélé, P. Microinjection molding of
thermoplastic polymers: Morphological comparison with conventional
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 99
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
injection molding, Micromech. Microeng. 2009, 19, 025023-025035.
[5] Yao, D.; Chen, S.C.; Kim, B. Rapid thermal cycling of injection
molds: An overview on technical approaches and applications, Adv.
Polym. Technol. 2008, 27, 233-255.
[6] Yokoi, H.; Han, X.; Takahashi, T.; Kim, W.K. Effects of molding
conditions on transcription molding of microscale prism patterns
using ultra-high-speed injection molding, Polym. Eng. Sci. 2006, 46,
1590-1597.
[7] Huang, M.-S.; Chung, C.F. Injection molding and injection
compression molding of thin-walled light-guided plates with
v-grooved microfeatures, J. Applied. Polym. Sci. 2011, 121,
1151-1159.
[8] Wu, C.H.; Su, Y.L. Optimization of wedge-shaped parts for injection
molding and injection compression molding, Int. Commun. Heat Mass
Transf. 2003, 30, 215-224.
[9] Shen, Y.K.; Chang, H.J.; Hung, L.H. Analysis of the replication
properties of lightguiding plate for micro injection compression
molding, Key Eng. Mater. 2007, 329, 643-648.
[10] Nirkhe, C.P.; Barry, C.M.F. Comparison of approaches for optimizing
molding parameters, Annual Technical Conference - ANTEC,
Conference Proceedings, Nashville, TN, 2003, 3534-3538.
[11] Bozzelli, J.W. Injection molding process optimization and
documentation, Annual Technical Conference - ANTEC, Conference
Proceedings, Nashville, TN, 2003, 534-538.
[12] Vagelatos, G.A.; Rigatos, G.G.; Tzafestas, S.G. Incremental fuzzy
supervisory controller design for optimizing the injection molding
process, Expert Syst. Appl. 2001, 20, 207-216.
[13] Sadeghi, B.H.M. BP-neural network predictor model for plastic
injection molding process, J. Mater. Process. Technol. 2000, 103,
411-416.
[14] Lau, H.C.W.; Ning, A.; Pun, K.F.; Chin, K.S. Neural networks for the
dimensional control of molded parts based on a reverse process model,
J. Mater. Process. Technol. 2001, 117, 89-96.
[15] Schnerr, O.; Michaeli, W. Neural networks for quality prediction and
closed-loop quality control in automotive industry, Annual Technical
Conference - ANTEC, Conference Proceedings, Atlanta, GA, 1998,
660-664.
[16] Sun, X.; Turng, L.-S. Artificial neural network-based supercritical
fluid dosage control for microcellular injection molding, Adv. Polym.
Technol. 2012, 31, 7-19.
[17] Goupy, J. What kind of experimental design for finding and checking
robustness of analytical methods? Anal Chim. Acta 2005, 544,
184-190.
[18] Dowlatshahi, S. An application of design of experiments for
optimization of plastic injection molding processes, J. Manuf. Technol.
Manage. 2004, 15, 445-454.
[19] Viana, J.C.; Kearney, P.; Cunha, A.M. Improving impact strength of
injection molded plates through molding conditions optimization: A
design of experiments approach, Annual Technical Conference -
ANTEC, Conference Proceedings, Atlanta, GA, 1998, 646-650.
[20] Liu, C.; Manzione, L.T. Process studies in precision injection molding.
I: process parameters and precision, Polym. Eng. Sci. 1996, 36, 1-9.
[21] Liao, H.C. Study of laminated object manufacturing with separately
applied heating and pressing, Int. J. Adv. Manuf. Technol. 2006, 27,
720-725.
[22] Derringer, G.; Suich, R. Simultaneous optimization of several
response variables, J. Qual. Technol. 1980, 12, 214-219.
[23] Harrington, E.C. The desirability function, Ind. Qual. Control, 1965,
21, 494-498.
[24] Goethals, P.L.; Cho, B.R. Extending the desirability function to
account for variability measures in univariate and multivariate
response experiments, Comput. Ind. Eng. 2012, 62, 457-468.
[25] Huang, M.-S.; Lin, T.Y. Simulation of a regression-model & PCA
based searching method developed for setting the robust injection
molding parameters of multi-quality characteristics, Int. J. Heat Mass
Transf. 2008, 51, 5828-5837.
[26]
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 100
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
Fig. 1. Flowchart of the robust parameter searching method for multi-quality characteristics.
Yes
Get the optimal setting and
normalize the observations from
Taguchi D.O.E.
Get and choose adjustment
factors by ANOVA analysis
Construct the 23 full factorial
experiments
Get new
Satisfy
robustness?
No
Buildup regression model
Estimate the response for all
possible treatments in their
varying range
Inferring next robust process
parameters
Stop the inference
process?
No
Phase 1
Phase 2
Phase 3
Finish Yes
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 101
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
(a)
(b)
Fig. 2. 2.5-inch LGP molding: (a) geometry of the injection compression mold; (b) micro-structure of the LGP stamper for injection compression molding
(Materials: Beryllium copper alloy).
55 mm
41 mm
8 mm
Fan gate
Round sprue
Cooling
channels
0.0
15 m
m
120°
0.052 mm
0.7 mm
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 102
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
Unit: mm
Fig. 3. Measuring positions of 2.5-inch LGP microstructures.
Averaged LGP’s 9-point micro-structure height (m) (a)
0
10
20
30
40
50
60
12.60 12.80 13.00 13.20 13.40 13.60 13.80
0
10
20
30
40
50
60
12.60 12.80 13.00 13.20 13.40 13.60 13.80
Lower Specification Limit: 13.50 m
NG Good Robust setting
Initial setting
Mean StDev N
13.62 0.008 50
12.71 0.010 50
Fre
quen
cy
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 103
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
Range of LGP’s 9-point micro-structure height (m)
(b)
Fig. 4. Heights of 2.5-inch LGP 9-point micro-structures: (a) average, (b) range.
0
5
10
15
20
0.28 0.3 0.32 0.34 0.36 0.38 0.4 0.42 0.44 0.46 0.48
Robust setting
Initial setting
Mean StDev N
0.38 0.024 50
0.40 0.024 50
Upper Specification Limit: 0.41 m
Good NG
Fre
quen
cy
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 104
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
TABLE I
The L18 (21×37) experiment for 2.5-inch LGP injection compression molding
Control factors Observations (gray digits).
Exp.
No. Filling
speed
(mm/s)
Melt
temp.
(oC)
Mold
temp.
(oC)
Compress.
distance
(mm)
Compress.
speed
(%)
Holding
pressure
(kgf/cm2)
Holding
time
(s)
Cooling
time
(s)
Avg.
9-point
heights1
(μm)
Avg.
9-point
heights2
(μm)
Avg.
9-point
heights3
(μm)
Range
9-point
heights1
(μm)
Range
9-point
heights2
(μm)
Range
9-point
heights3
(μm)
1 50 240 70 3 80 700 3 35 12.72 12.71 12.71 0.42 0.36 0.41
2 50 240 80 4 90 800 4 40 13.18 13.19 13.19 0.54 0.50 0.46
3 50 240 90 5 100 900 5 45 13.55 13.59 13.54 0.49 0.36 0.35
4 50 250 70 3 90 800 5 45 13.09 13.10 13.12 0.48 0.42 0.44
5 50 250 80 4 100 900 3 35 13.50 13.45 13.45 0.55 0.41 0.38
6 50 250 90 5 80 700 4 40 13.61 13.62 13.62 0.46 0.45 0.45
7 50 260 70 4 80 900 4 45 13.26 13.26 13.26 0.43 0.31 0.34
8 50 260 80 5 90 700 5 35 13.48 13.45 13.50 0.48 0.43 0.55
9 50 260 90 3 100 800 3 40 13.45 13.50 13.51 0.49 0.43 0.32
10 55 240 70 5 100 800 4 35 13.20 13.16 13.18 0.34 0.38 0.39
11 55 240 80 3 80 900 5 40 13.19 13.20 13.18 0.47 0.50 0.43
12 55 240 90 4 90 700 3 45 13.45 13.46 13.45 0.44 0.58 0.37
13 55 250 70 4 100 700 5 40 13.34 13.36 13.34 0.46 0.45 0.42
14 55 250 80 5 80 800 3 45 13.52 13.47 13.53 0.49 0.35 0.46
15 55 250 90 3 90 900 4 35 13.58 13.61 13.62 0.50 0.49 0.49
16 55 260 70 5 90 900 3 40 13.47 13.46 13.45 0.47 0.41 0.49
17 55 260 80 3 100 700 4 45 13.47 13.48 13.45 0.42 0.44 0.40
18 55 260 90 4 80 800 5 35 13.61 13.68 13.66 0.56 0.49 0.53 1, 2, 3
mean sample 1, 2, and 3 at the same run, respectively.
TABLE II
The composite quality indicators DF generated by DF method in the L18 experiment of 2.5-inch LGP injection compression molding
Exp. No. Average normalized averaged
nine-point heights
Average normalized range of
nine-point heights DF
1 0.004 0.68 0.05
2 0.487 0.30 0.38
3 0.876 0.67 0.76*
4 0.403 0.49 0.45
5 0.779 0.49 0.62
6 0.928 0.47 0.66
7 0.563 0.81 0.68
8 0.789 0.35 0.52
9 0.795 0.62 0.70
10 0.482 0.78 0.61
11 0.488 0.42 0.45
12 0.762 0.43 0.57
13 0.652 0.51 0.57
14 0.818 0.54 0.67
15 0.915 0.32 0.54
16 0.770 0.46 0.59
17 0.774 0.59 0.68
18 0.969 0.20 0.44
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 105
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
TABLE III
The ANOVA analysis of the composite quality indicator DF in 2.5-inch LGP injection compression molding
SV DOF SS MS F PSS CP (%)
Filling speed 1 0.01
Melt temp. 2 0.06 0.03 2.49 0.04 7.86 Mold temp. 2 0.04 0.02 1.83 0.02 4.40 Compression distance 2 0.08 0.04 3.19 0.05 11.57 Compression speed 2 0.10 0.05 4.25 0.08 17.17 Holding pressure 2 0.03
Holding time 2 0.01
Cooling time 2 0.09 0.04 3.67 0.06 14.10 Error 2 0.01
Pooled error (7) (0.08) (0.01) 0.20 44.90 Total 17 0.45 0.16 100.00
SV, source of variation; DOF, degrees of freedom; SS, sum of squares; MS, mean square; PSS, pure of sum squares; CP,
contribution percentage; F1,7,0.01=12.25, F2,7,0.01=9.55.
TABLE IV
Full-factorial experiment and principal component analysis in 2.5-inch LGP injection compression molding
(a) The first inference of robust parameters by the proposed method.
Initial central point Average
normalized
averaged
nine-point heights
Average
normalized
range of
nine-point
heights
DF
Exp.
No.
Compression
distance
5 mm
Compression speed
100%
Cooling time
45 s 0.90 0.68 0.78
1 +0.5 +1% +0.5 0.91 0.70 0.80
2 -0.5 +1% +0.5 0.67 0.28 0.44
3 +0.5 -1% +0.5 0.88 0.21 0.43
4 -0.5 -1% +0.5 0.85 0.20 0.41
5 +0.5 +1% -0.5 0.97 0.88 0.92
6 -0.5 +1% -0.5 0.94 0.67 0.79
7 +0.5 -1% -0.5 0.97 0.67 0.80
8 -0.5 -1% -0.5 0.70 0.37 0.51
Normalized lower specification limit ≧0.81 ≧0.63 ≧0.71
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 106
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
(b) The second inference of robust parameters by the proposed method
Initial central point Average
normalized
averaged
nine-point heights
Average
normalized
range of
nine-point
heights
DF
Exp.
No.
Compression
distance
3.9 mm
Compression speed
98%
Cooling time
44.5 s 0.82 0.64 0.73
1 +0.5 +1% +0.5 0.49 0.30 0.38
2 -0.5 +1% +0.5 0.93 0.47 0.66
3 +0.5 -1% +0.5 0.80 0.59 0.69
4 -0.5 -1% +0.5 0.92 0.60 0.75
5 +0.5 +1% -0.5 0.78 0.43 0.58
6 -0.5 +1% -0.5 0.92 0.56 0.72
7 +0.5 -1% -0.5 0.80 0.62 0.70
8 -0.5 -1% -0.5 0.87 0.65 0.76
Normalized lower specification limit ≧0.81 ≧0.63 ≧0.71
(c) The third inference of robust parameters by the proposed method
Initial central point Average
normalized
averaged
nine-point heights
Average
normalized
range of
nine-point
heights
DF
Exp.
No.
Compression
distance
4.8 mm
Compression speed
99.6%
Cooling time
45.4 s 0.93 0.70 0.81
1 +0.5 +1% +0.5 0.88 0.64 0.75
2 -0.5 +1% +0.5 0.88 0.78 0.83
3 +0.5 -1% +0.5 0.89 0.65 0.76
4 -0.5 -1% +0.5 0.96 0.83 0.89
5 +0.5 +1% -0.5 0.88 0.67 0.77
6 -0.5 +1% -0.5 0.98 0.77 0.86
7 +0.5 -1% -0.5 0.98 0.70 0.83
8 -0.5 -1% -0.5 1.03 0.88 0.95
Normalized lower specification limit ≧0.81 ≧0.63 ≧0.71
International Journal of Engineering & Technology IJET-IJENS Vol:14 No:01 107
146601-4949-IJET-IJENS © February 2014 IJENS I J E N S
TABLE V Robustness quality of 2.5-inch LGP injection compression molding obtained using the proposed method
The initial setting The robust setting
Exp.
No.
Average
nine-point
heights
(μm)
Range of
nine-point
heights
(μm)
Exp.
No
Average
nine-point
heights
(μm)
Range of
nine-point
heights
(μm)
Exp.
No.
Average
nine-point
heights
(μm)
Range of
nine-point
heights
(μm)
Exp.
No
Average
nine-point
heights
(μm)
Range of
nine-point
heights
(μm)
1 (12.71) 0.36 26 (12.71) (0.44) 1 13.62 0.39 26 13.63 0.41 2 (12.72) 0.35 27 (12.70) 0.40 2 13.62 0.39 27 13.62 0.39 3 (12.72) 0.40 28 (12.70) 0.38 3 13.61 0.34 28 13.64 0.39 4 (12.70) 0.40 29 (12.72) (0.43) 4 13.61 0.38 29 13.63 0.35 5 (12.70) 0.40 30 (12.70) 0.39 5 13.61 0.36 30 13.60 0.33 6 (12.70) (0.44) 31 (12.73) 0.39 6 13.63 0.38 31 13.62 0.38 7 (12.69) (0.43) 32 (12.70) (0.43) 7 13.62 0.42 32 13.64 0.36 8 (12.72) (0.43) 33 (12.69) 0.36 8 13.63 0.39 33 13.63 0.40 9 (12.71) 0.40 34 (12.71) 0.38 9 13.62 0.37 34 13.62 0.38
10 (12.71) 0.34 35 (12.73) 0.40 10 13.63 0.41 35 13.62 0.36 11 (12.72) (0.42) 36 (12.71) 0.36 11 13.63 0.39 36 13.62 0.38 12 (12.70) 0.37 37 (12.70) (0.42) 12 13.62 0.39 37 13.60 0.35 13 (12.72) 0.39 38 (12.73) 0.38 13 13.61 0.39 38 13.62 0.37 14 (12.73) (0.41) 39 (12.71) (0.42) 14 13.62 0.36 39 13.62 0.33 15 (12.72) 0.37 40 (12.70) (0.41) 15 13.63 0.39 40 13.63 0.40 16 (12.71) 0.39 41 (12.72) 0.39 16 13.62 0.34 41 13.63 0.37 17 (12.72) 0.40 42 (12.72) 0.36 17 13.62 0.41 42 13.62 0.37 18 (12.72) 0.40 43 (12.73) 0.39 18 13.62 0.33 43 13.61 0.33 19 (12.70) 0.39 44 (12.71) (0.42) 19 13.62 0.39 44 13.61 0.37 20 (12.70) (0.41) 45 (12.71) 0.38 20 13.62 0.39 45 13.63 0.37 21 (12.71) (0.42) 46 (12.71) (0.41) 21 13.63 0.40 46 13.62 0.38 22 (12.72) 0.38 47 (12.70) 0.38 22 13.62 0.39 47 13.63 0.38 23 (12.71) (0.41) 48 (12.71) (0.43) 23 13.62 0.37 48 13.62 0.35 24 (12.72) 0.38 49 (12.71) (0.42) 24 13.63 0.39 49 13.62 0.33 25 (12.71) 0.37 50 (12.72) 0.40 25 13.62 0.35 50 13.62 0.41