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Creep and Tensile Properties of Direct Metal Laser Sintered (DMLS) Inconel 738LC Coupons and Comparison to Cast Properties Jason Wilkes, Ph.D. Kevin Hoopes Jon Helfand © Southwest Research Institute 2012 1

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Page 1: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Creep and Tensile Properties of Direct Metal Laser Sintered

(DMLS) Inconel 738LC Coupons and Comparison to

Cast PropertiesJason Wilkes, Ph.D.

Kevin HoopesJon Helfand

© Southwest Research Institute 2012 1

Page 2: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

sCO2 cycle promises more compact turbomachinery than supercritical steam or helium cycles

2

Adapted from Dostal (2004)

5 mSteam turbine: 55 stages / 250 MW

Mitsubishi Heavy Industries (with casing)

Helium turbine: 17 stages / 333 MW (167 MWe)X.L. Yan, L.M. Lidsky (MIT) (without casing)

sCO2 turbine: 4 stages / 450 MW (300 MWe)(without casing)

Note: Compressors are comparable in size

1 m

Source: Wright (2011)

Page 3: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

A 10MW 275 bar 705°C compact integrally geared radial inflow turbine was designed under DOE-EERE 7114

© Southwest Research Institute 2012 3

First Stage• Diameter ~ 230 mm• Speed ~ 18000 rpm• Power ~ 3.5 MW

Page 4: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Whoever said that compact turbomachinery was a good thing never machined a single piece shrouded impeller from Inconel 740

© Southwest Research Institute 2012 4

Quoted Estimate• 500 hrs. on the

machine• $100/tool *500 tools• NRE $10k/wheel

~100,000 USD

Page 5: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

How else can a high temperature closed sCO2 impeller be fabricated?

5 axis edm – Very expensive Cast Alloy – Received several no-quotes DMLS?

© Southwest Research Institute 2012 5

Page 6: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

DMLS, SLM, AM Process Overview

Page 7: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Published data are scarce Stationary and rotating parts have

been “printed” Published application of DMLS to

rotating parts limited to development test rigs• 100,000 rpm 1380 °F Inconel GT

wheel (Inconel 718)• Authors’ experience with

microturbomachine closed impellers and turbines

− Overspeed test successful at 1140 ft/s− Overspeed test to failure at 1403 ft/s

DMLS in Turbomachinery

Flow Straightener for Helicopter Engine (Killian 2013)

100 krpm GT wheel (Killian 2013)

How does a superalloy manufactured additively compare to cast or forged superalloys?

Page 8: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

A total of 24 samples were printed

© Southwest Research Institute 2012 9

14 XY samples 10 Z samples

Page 9: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Points were selected to allow for a direct comparison to cast Inconel 738 properties and additionally design stresses at elevated temperatures

© Southwest Research Institute 2012 11

Page 10: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Raw data shows that creeps faster in the XY orientation than in the Z orientation, and that DMLS creep strength is inferior to cast creep strength

© Southwest Research Institute 2012 12

10 -1 10 0 10 1 10 2 10 3 10 4

Time (hours)

50

55

60

65

70

75

80

85

90

95

Stre

ss (k

si)

Rupture Time vs. Stress for Inconel 738

C738 - 0.2%

C738 - 1%

C738 - Rupture

P738LCX Y

- .2%

P738LCX Y

- 1%

P738LCX Y

- Rupture

P738LCZ

- .2%

P738LCZ

- 1%

P738LCZ

- Rupture

.2% XY Rupture

1%

ZXYRupture

ZXY 1%

1300°F/ 705°C

1450°F/ 788°C

Page 11: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

© Southwest Research Institute 2012 13

38 40 42 44 46 48 50 52 54 56

LMP=T*(20+log(t))/1000

0

10

20

30

40

50

60

70

80

90

100R

uptu

re S

tress

(ksi

)Conventional Rupture LMP

C738

C738LC

P738LCX Y

P738LCZ

Page 12: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

© Southwest Research Institute 2012 14

38 40 42 44 46 48 50 52 54

LMP =T*(20+log(t/ ))/1000

0

10

20

30

40

50

60

70

80

90

100St

ress

(ksi

)Strain Based LMP

C738

P738LCX Y

P738LCZ

P738LCXY,Rickenbacher

P738LCZ,Rickenbacher

Page 13: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

© Southwest Research Institute 2012 15

1100 1150 1200 1250 1300 1350 1400

Temperature ° F

-10

0

10

20

30

40

50

60

70

80

90St

ress

(ksi

)allow

at 0.2% Strain versus Design Temperature

C738

P738LCX Y

P738LCZ

P738LCXY,Rickenbacher

P738LCZ,Rickenbacher

Page 14: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

© Southwest Research Institute 2012 16

1100 1150 1200 1250 1300 1350 1400

Temperature ° F

0

10

20

30

40

50

60

70

80

Stre

ss (k

si)

allow at .67 Rupture versus Design Temperature

C738

C738LC

P738LCX Y

P738LCZ

Page 15: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Tensile and Yield properties in the two orientations were generally similar

600C• 20% ↓ yield• 20% ↑ UTS

700C• 5% ↓ yield• 10% ↓ UTS

© Southwest Research Institute 2012 17

0 200 400 600 800 1000 1200 1400 1600 1800

Temperature [F]

50

75

100

125

150

175

200

Stre

ss [k

si]

P738LCX Y

t

P738LCX Y

y

P738LCZ

t

P738LCZ

y

C738 t

C738 y

Page 16: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Per plastic collapse analysis, the impeller should survive 100,000 hrs. without failing due to creep.

© Southwest Research Institute 2012 18

Page 17: Creep and Tensile Properties of Direct Metal Laser ...sco2symposium.com/papers2018/materials/168_pres.pdf · Rupture Time vs. Stress for Inconel 738 C738 - 0.2% C738 - 1% C738 - Rupture

Conclusions

Z Orientation• Allowable stress for 100,000 hr service life at

700°C is 5-10% lower than cast Inconel 738LC XY Orientation

• Allowable stress for 100,000 hr service life at 700°C is 51% lower than cast Inconel 738LC

Allowable stresses are still sufficient to build the designed impeller and survive creep.

© Southwest Research Institute 2012 19