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  • 7/29/2019 CPR Systems | CARL Labs Paint Adhesion Testing

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    CARL Testing Outline of Surface Cleaning Investigation

    30 Test Panels 5 X 8

    30 Steel

    Grease & Oil Applied to Each Panel: per standardized method

    using Pennzoil 705 white grease and Mystic JT-8 SAE 10W/40

    heavy duty motor oil

    3 Cleaning Processes Utilized to Clean the Pre-Soiled Panels: Tophalf of panels received light wipe with cotton/pulp fiber towel;

    bottom half received cleaning by one of following:

    1) Alkaline Wipe (2.3% solution at room temperature)

    2) Solvent Wipe (xylene at room temperature)

    3) Podell Cleaning System (2000 psi power spray at 160F)

    5 Different Paint Types Applied1) Water-Based Epoxy

    2) VOC-Based Enamel

    3) VOC-Based Epoxy (Two Part Chemistry)

    4) VOC-Based Urethane (Two Part Chemistry)

    5) Epoxy Powder Coating

    Adhesion Test Performed On All Panels per ASTM-3359

    Higher grade of adhesion for various coatings would

    indicate that a particular cleaning type offers better

    cleaning characteristics compared to others

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    Steel

    Oil & Grease

    Contaminate

    Water Based Epoxy

    Single Component

    Solvent Wipe Alkaline Wipe G. Podell Clean

    Lightly Dirty

    rag wipe

    Steel

    Oil & Grease

    Contaminant

    Enamel

    Steel

    Oil & Grease

    Contaminant

    Solvent Based

    Epoxy Two Component

    Steel

    Oil & Grease

    Contaminant

    Urethane

    Two Component

    Number

    Of Samples

    6

    6

    6

    6

    Podell CPR/CARL Test Sample Preparation

    and Sample Description

    Steel

    Oil & GreaseContaminant

    Powder Coating

    6

    Top Half of Coupon

    Bottom Half of Coupon

    Lightly Dirty

    rag wipe

    Lightly Dirty

    rag wipe

    30

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    Contaminated (soiled) metal panels according

    to ASTM process (dwell time 24 hrs.)

    Cleaned, metal panels racked for drying (dwell

    time 24 hrs.) prior to application of paint

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    Paint application to each metal panel. The paint was

    applied to the lightly cleaned top half and to the more

    aggressively cleaned bottom half. Paint applied via

    metered draw bar. Set of two panels per each paintsystem, one received 3 wet mils and the other received 6

    wet mils.

    Staging of painted metal panels (drying dwell

    time 7 days) prior to adhesion testing

    Draw

    Bar

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    Array of painted metal panels after

    performing the ASTM-3359 adhesion test

    Angled cutting edges makes thecross-hatch marks on the painted

    paint. A special adhesion testing

    tape is used to test paints

    adhesion to the panel

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    Adhesion Quality Scoring

    5 B - Best Quality

    2 to 3 B - low Quality

    0 to 1 B Very Poor Quality

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    PC # T C M T C T D T T V T T V PC # T C M T C T D T T V T T V PC # T C M T C T D T T V T T V

    11 GPHPP S SW-VE 5 B 5 B 41 A W R T S SW-VE 0 B 0 B 71 X W S SW-VE 3 B 3 B

    12 GPHPP S SW-VE 5 B 5 B 42 A W R T S SW-VE 0 B 0 B 72 X W S SW-VE 3 B 3 B

    13 GPHPP S SW-WE 5 B 5 B 43 A W R T S SW-WE 0 B 0 B 73 X W S SW-WE 0 B 0 B

    14 GPHPP S SW-WE 5 B 5 B 44 A W R T S SW-WE 0 B 0 B 74 X W S SW-WE 0 B 0 B

    15 GPHPP S V-VE 5 B 5 B 45 A W R T S V-VE 0 B 0 B 75 X W S V-VE 5 B 5 B

    16 GPHPP S V-VE 5 B 5 B 46 A W R T S V-VE 0 B 0 B 76 X W S V-VE 5 B 5 B

    17 GPHPP S U 5 B 5 B 47 A W R T S U 0 B 0 B 77 X W S U 0 B 0 B

    18 GPHPP S U 5 B 4 B 48 A W R T S U 0 B 0 B 78 X W S U 0 B 0 B

    19 GPHPP S P C 5 B 5 B 49 A W R T S P C 3 B 2 B 79 X W S P C 5 B 5 B

    20 GPHPP S P C 5 B 5 B 50 A W R T S P C 5 B 5 B 80 X W S P C 5 B 5 B

    21 GPHPP G SW-VE 0 B 1 B 51 A W R T G SW-VE 1 B 1 B 81 X W G SW-VE 4 B 4 B

    22 GPHPP G SW-VE 4 B 4 B 52 A W R T G SW-VE 2 B 1 B 82 X W G SW-VE 4 B 4 B

    23 GPHPP G SW-WE 5 B 3 B 53 A W R T G SW-WE 0 B 0 B 83 X W G SW-WE 0 B 0 B

    24 GPHPP G SW-WE 4 B 3 B 54 A W R T G SW-WE 0 B 0 B 84 X W G SW-WE 1 B 4 B

    25 GPHPP G V-VE 5 B 5 B 55 A W R T G V-VE 2 B 0 B 85 X W G V-VE 5 B 5 B

    26 GPHPP G V-VE 5 B 5 B 56 A W R T G V-VE 2 B 2 B 86 X W G V-VE 5 B 5 B

    27 GPHPP G U 0 B 0 B 57 A W R T G U 0 B 0 B 87 X W G U 0 B 0 B

    28 GPHPP G U 0 B 0 B 58 A W R T G U 0 B 0 B 88 X W G U 1 B 2 B

    29 GPHPP G P C 5 B 5 B 59 A W R T G P C 5 B 5 B 89 X W G P C 5 B 5 B

    30 GPHPP G P C 5 B 5 B 60 A W R T G P C 2 B 4 B 90 X W G P C 5 B 5 B

    Rating 1st 2nd Ttl Wtd Sc. Rating 1st 2nd Ttl Wtd Sc. Rating 1st 2nd Ttl Wtd Sc.

    5 B 15 13 28 140 5 B 2 2 4 20 5 B 8 8 16 80

    4 B 2 2 4 16 4 B 0 2 2 8 4 B 2 3 5 20

    3 B 0 2 2 6 3 B 1 1 2 6 3 B 2 2 4 12

    2 B 0 0 0 0 2 B 4 0 4 8 2 B 0 1 1 2

    1 B 0 1 1 1 1 B 1 2 3 3 1 B 2 0 2 2

    0 B 3 2 5 0 0 B 12 13 25 0 0 B 6 6 12 0

    Totals 20 20 40 163 Totals 20 20 40 45 Totals 20 20 40 116

    T C Type of Cleaning Galvanized Steel is excluded from this summary

    M T Metal Type because little adhesion was demonstrated on it.

    C T D Coating-Type Designation

    T T V Tape Test Value per ASTM-3359 Powder Coat was least effective with RT-Alkaline

    GPHPP G. Podell Hi Pressure Phosphate wipe, as was every thing else; Rag-Wipe excepted.

    A W R T Alkaline Wipe - Room Temperature

    X W Xylene Wipe - Room Temperature Order of cleaner effectiveness:

    S Steel GPHPP 163

    G GalvanilX W 116

    SW-VE Sherwin-Williams VOC Enamel A W R T 45

    SW-WE Sherwin-Williams Water/Epoxy

    V-VE Valspar VOC/Epoxy

    U Urethane

    P C Powder Coat

    Total Adhesion Values Summed

    T. G. Podell CPR System 163Xylene Wipe 116

    Alkaline Wipe 45

    Test Generated Data

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    Executive Summary of Test Results

    Steel: Podell CPR cleaning provided very good adhesion

    values for all of the coating types.

    Alkaline wipe cleaning provided poor adhesion values

    for all coating types with the exception of the powder

    coating which appeared to adhere well to the steel

    substrate.

    Xylene wipe cleaning provided good adhesion values

    for the VOC epoxy and the Powder Coating types.However, the other coating types did not adhere well

    to the xylene wiped steel substrate