cover page - organic analysis data package semivolatile

K2005164Naval Facilities Engineering Command Haw

JP-8

Semivolatile Range Organics by GC/FID

Cover Page - Organic Analysis Data Package

Client:

Project:

Service Request:

Date

Collected

Date

ReceivedLab CodeSample Name

ALS Group USA, Corp. dba ALS Environmental

K2005164-001 06/18/2020 06/20/202020-06644(360-011)

K2005164-002 06/18/2020 06/20/202020-06645(360-001)

KWG2001792-1 06/18/2020 06/20/202020-06644(360-011)MS

Cover Page - Organic 1of1Page

RR214104SuperSet Reference:u:\Stealth\Crystal.rpt\FormSSum.rpt

Analytical Results

Naval Facilities Engineering Command Haw K2005164

K2005164-001

ug/L

NA

20-06644(360-011)

06/18/2020

06/20/2020

JP-8

Water

Client:

Project:

Sample Matrix:

Service Request:

Date Collected:

Date Received:


Units:

Basis:

Sample Name:


Lab Code:

Level: LowExtraction Method:

Analysis Method:

EPA 3510C

8015C

NoteMDLMRLQResultAnalyte Name

Extraction

Lot

Date

Analyzed

Date

Extracted

Dilution

Factor

53 06/25/201 KWG200179206/25/2053Z91JP-8 (C8 - C18)

53 06/25/201 KWG200179206/25/2012J19C10 - C25 DRO

Surrogate Name %Rec

Control

Limits NoteDate

Analyzed

55-133 Acceptableo-Terphenyl 06/25/2098

Comments:

1of1Page16:17:3606/26/2020Printed: Form 1A - Organic

Merged SuperSet Reference: RR214104u:\Stealth\Crystal.rpt\Form1mNew.rpt

Analytical Results


K2005164-002

ug/L

NA

20-06645(360-001)

06/18/2020

06/20/2020

JP-8

Water

Client:

Project:

Sample Matrix:

Service Request:

Date Collected:

Date Received:


Units:

Basis:

Sample Name:


Lab Code:


Analysis Method:

EPA 3510C

8015C


Extraction

Lot

Date

Analyzed

Date

Extracted

Dilution

Factor

53 06/25/201 KWG200179206/25/2053UNDJP-8 (C8 - C18)

53 06/25/201 KWG200179206/25/2012J13C10 - C25 DRO

Surrogate Name %Rec

Control

Limits NoteDate

Analyzed


Comments:



Analytical Results


KWG2001792-4

ug/L

NA

Method Blank

NA

NA

JP-8

Water

Client:

Project:

Sample Matrix:

Service Request:

Date Collected:

Date Received:


Units:

Basis:

Sample Name:


Lab Code:


Analysis Method:

EPA 3510C

8015C


Extraction

Lot

Date

Analyzed

Date

Extracted

Dilution

Factor

50 06/25/201 KWG200179206/25/2050UNDJP-8 (C8 - C18)

50 06/25/201 KWG200179206/25/2011J15C10 - C25 DRO

Surrogate Name %Rec

Control

Limits NoteDate

Analyzed


Comments:




Extraction Method:

QA/QC Report

Surrogate Recovery Summary


Low

Water

JP-8

Client:

Project:

Sample Matrix:

Service Request:

Units:

Level:

Sample Name Lab Code


EPA 3510C

Analysis Method: 8015C

Sur1

Percent

K2005164-00120-06644(360-011) 98

K2005164-00220-06645(360-001) 84

KWG2001792-4Method Blank 94

KWG2001792-120-06644(360-011)MS 83

KWG2001792-2Lab Control Sample 84

KWG2001792-3Duplicate Lab Control Sample 81

Form 2A - OrganicPrinted: 06/26/2020 16:17:48 1 of 1

Surrogate Recovery Control Limits (%)

55-133o-Terphenyl

Results flagged with an asterisk (*) indicate values outside control criteria.

Page

Results flagged with a pound (#) indicate the control criteria is not applicable.

RR214104SuperSet Reference:

Sur1 =

u:\Stealth\Crystal.rpt\Form2.rpt

Matrix Spike Summary

Sample

Result %Rec

Matrix Spike

%Rec

Limits

QA/QC Report

06/25/2020

Naval Facilities Engineering Command Haw

20-06644(360-011)

K2005164-001

K2005164

ug/L

NA

Water

Low

JP-8

Client:

Project:

Sample Matrix:

Service Request:

Date Extracted:

Date Analyzed:

Sample Name:

Lab Code:

Extraction Method:

Units:

Basis:

Level:

Extraction Lot:

Analyte Name Result


06/25/2020

EPA 3510C



KWG2001792

KWG2001792-1

20-06644(360-011)MS

Spike

Amount

70-13091JP-8 (C8 - C18) 3300 732480

Form 3A - OrganicPrinted: 06/26/2020 16:17:52 Page 1 of 1


Results flagged with a pound (#) indicate the control criteria is not applicable.


Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.

u:\Stealth\Crystal.rpt\Form3MS.rpt

Lab Control Spike/Duplicate Lab Control Spike Summary

%Rec

Lab Control Spike

%Rec

Limits

Duplicate Lab Control Spike

%Rec RPD

RPD

Limit

QA/QC Report

Duplicate Lab Control Sample

KWG2001792-3


8015C

ug/L

NA

Lab Control Sample

KWG2001792-2


KWG2001792

Water

Low

JP-8

Client:

Project:

Sample Matrix:

Service Request:

Extraction Method:

Analysis Method:

Units:

Basis:

Level:

Extraction Lot:

Analyte Name Result Result


Date Extracted:

Date Analyzed:

06/25/2020

06/25/2020

EPA 3510C

Spike

Amount

Spike

Amount

70-1303200 71 30JP-8 (C8 - C18) 3200 73 32340 2280

Form 3C - OrganicPrinted: 06/26/2020 16:17:56 Page 1 of 1



Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.

u:\Stealth\Crystal.rpt\Form3DLC.rpt


Instrument ID:

File ID: Lab Code:

Sample Name:

Time Analyzed:

Date Analyzed:

Date Extracted:

Service Request:

Sample Matrix:

Project:

Client:

J:\GC21\DATA\062420F-DRO\0624F189.D

20:07

06/25/2020

GC21

Water

Method Blank

KWG2001792-4

06/25/2020


Method Blank Summary

K2005164

JP-8

QA/QC Report


This Method Blank applies to the following analyses:

EPA 3510C

8015C KWG2001792

LowExtraction Method:

Analysis Method:

Level:

Extraction Lot:

Sample Name Lab Code File ID

Date

Analyzed

Time

Analyzed

K2005164-001 21:15J:\GC21\DATA\062420F-DRO\0624F192.D20-06644(360-011) 06/25/20

K2005164-002 21:37J:\GC21\DATA\062420F-DRO\0624F193.D20-06645(360-001) 06/25/20

Form 4A - Organic 1Printed: of 1Page16:18:0606/26/2020RR214104SuperSet Reference:u:\Stealth\Crystal.rpt\Form4mb.rpt


Instrument ID:

File ID: Lab Code:

Sample Name:

Time Analyzed:

Date Analyzed:

Date Extracted:

Service Request:

Sample Matrix:

Project:

Client:

J:\GC21\DATA\062420F-JP8\0624F189.D

20:07

06/25/2020

GC21

Water

Method Blank

KWG2001792-4

06/25/2020


Method Blank Summary

K2005164

JP-8

QA/QC Report


This Method Blank applies to the following analyses:

EPA 3510C

8015C KWG2001792

LowExtraction Method:

Analysis Method:

Level:

Extraction Lot:


Date

Analyzed

Time

Analyzed

KWG2001792-3 20:30J:\GC21\DATA\062420F-JP8\0624F190.DDuplicate Lab Control Sample 06/25/20

KWG2001792-2 20:52J:\GC21\DATA\062420F-JP8\0624F191.DLab Control Sample 06/25/20

K2005164-001 21:15J:\GC21\DATA\062420F-JP8\0624F192.D20-06644(360-011) 06/25/20

K2005164-002 21:37J:\GC21\DATA\062420F-JP8\0624F193.D20-06645(360-001) 06/25/20

KWG2001792-1 22:00J:\GC21\DATA\062420F-JP8\0624F194.D20-06644(360-011)MS 06/25/20

Form 4A - Organic 1Printed: of 1Page16:18:1506/26/2020RR214104SuperSet Reference:u:\Stealth\Crystal.rpt\Form4mb.rpt

06/25/2020


Instrument ID:

File ID: Lab Code:

Sample Name:

Time Analyzed:

Date Analyzed:

Date Extracted:

Service Request:

Sample Matrix:

Project:

Client:

J:\GC21\DATA\062420F-JP8\0624F191.D

Lab Control Sample Summary

GC21

KWG2001792-2

Lab Control Sample

20:52

06/25/2020

Water

JP-8

K2005164Naval Facilities Engineering Command Haw


QA/QC Report

This Lab Control Sample applies to the following analyses:

EPA 3510C

8015C

Low

KWG2001792

Extraction Method:

Analysis Method:

Level:

Extraction Lot:


Date

Analyzed

Time

Analyzed

KWG2001792-4 20:07J:\GC21\DATA\062420F-JP8\0624F189.DMethod Blank 06/25/20

KWG2001792-4 20:07J:\GC21\DATA\062420F-DRO\0624F189.DMethod Blank 06/25/20

K2005164-001 21:15J:\GC21\DATA\062420F-JP8\0624F192.D20-06644(360-011) 06/25/20

K2005164-001 21:15J:\GC21\DATA\062420F-DRO\0624F192.D20-06644(360-011) 06/25/20

K2005164-002 21:37J:\GC21\DATA\062420F-JP8\0624F193.D20-06645(360-001) 06/25/20

K2005164-002 21:37J:\GC21\DATA\062420F-DRO\0624F193.D20-06645(360-001) 06/25/20

KWG2001792-1 22:00J:\GC21\DATA\062420F-JP8\0624F194.D20-06644(360-011)MS 06/25/20

Form 4B - Organic 1of1PagePrinted: 06/26/2020 16:18:20SuperSet Reference: RR214104u:\Stealth\Crystal.rpt\Form4LCS.rpt

QA/QC Results

Initial Calibration Summary


JP-8

K2005164

06/24/2020


CAL16321

GC21

Client:

Project:

Calibration ID:

Instrument ID:

Service Request:


Calibration Date:

Column: ZB-1

Level ID File ID

J:\GC21\DATA\062420F\0624F132.DAJ:\GC21\DATA\062420F\0624F133.DBJ:\GC21\DATA\062420F\0624F134.DCJ:\GC21\DATA\062420F\0624F135.DDJ:\GC21\DATA\062420F\0624F136.DE

Level ID File ID

J:\GC21\DATA\062420F\0624F137.DFJ:\GC21\DATA\062420F\0624F138.DGJ:\GC21\DATA\062420F\0624F139.DH

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RFAnalyte Name

JP-8 (C8 - C18) 50 200 50020 20002220 2160 1820 1840 1700A B C D E

20000 500005000 1690 1620 1540F G H

o-Terphenyl 2.5 10 251.0 1002300 2460 2280 2210 2130A B C D E

250 2020F

Form 6A - Organic 2of1PagePrinted: 06/26/2020 16:18:24RR214104SuperSet Reference:


u:\Stealth\Crystal.rpt\Form6iNew.rpt

QA/QC Results



JP-8

K2005164

06/24/2020


CAL16321

GC21

Client:

Project:

Calibration ID:

Instrument ID:

Service Request:


Calibration Date:

Column: ZB-1

Analyte Name

Compound

Type Fit Type Eval.

Eval.

Result Q

Control

Criteria

Calibration Evaluation

JP-8 (C8 - C18) MS AverageRF % RSD 13.6 £ 20

o-Terphenyl SURR AverageRF % RSD 6.8 £ 20




QA/QC Results

Second Source Calibration Verification

External Standard

JP-8

Client:

Project:

Service Request:

Date Analyzed:

Analysis Method:

Calibration Type:

Calibration Date:

Calibration ID:

Units:



06/24/2020

06/25/2020


8015C

CAL16321

ppm

J:\GC21\DATA\062420F\0624F142.DFile ID: Column ID: ZB-1

Analyte Name Expected Result

Average

RF

SSV

RF %D %Drift Criteria Curve Fit

AverageRF± 20 %NA-14157018208601000JP-8 (C8 - C18)

1of1PagePrinted: 6/26/2020 16:18:30 Form 6B - Organic


SuperSet Reference:

† SPCC Compound ‡ CCC Compound

RR214104u:\Stealth\Crystal.rpt\Form6SS.rpt

QA/QC Results



JP-8

K2005164

10/21/2019


CAL16158

GC21

Client:

Project:

Calibration ID:

Instrument ID:

Service Request:


Calibration Date:

Column: ZB-1

Level ID File ID

J:\GC21\DATA\102119F\1021F105.DAJ:\GC21\DATA\102119F\1021F106.DBJ:\GC21\DATA\102119F\1021F107.DCJ:\GC21\DATA\102119F\1021F108.DDJ:\GC21\DATA\102119F\1021F112.DEJ:\GC21\DATA\102119F\1021F113.DFJ:\GC21\DATA\102119F\1021F114.DGJ:\GC21\DATA\102119F\1021F115.DHJ:\GC21\DATA\102119F\1021F116.DIJ:\GC21\DATA\102119F\1021F120.DJ

Level ID File ID

J:\GC21\DATA\102119F\1021F121.DKJ:\GC21\DATA\102119F\1021F122.DLJ:\GC21\DATA\102119F\1021F123.DMJ:\GC21\DATA\102119F\1021F124.DNJ:\GC21\DATA\102119F\1021F125.DOJ:\GC21\DATA\102119F\1021F126.DPJ:\GC21\DATA\102119F\1021F127.DQJ:\GC21\DATA\102419F\1024F120.DR

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RF

Level

ID Amt RFAnalyte Name

C10 - C25 DRO20 2050J

200 500 200050 50002000 1850 1930 1750 1690K L M N O

5000020000 1560 1590P Q

o-Terphenyl1.0 2100J

10 25 1002.5 2501990 1940 1920 1820 1710K L M N O




QA/QC Results



JP-8

K2005164

10/21/2019


CAL16158

GC21

Client:

Project:

Calibration ID:

Instrument ID:

Service Request:


Calibration Date:

Column: ZB-1

Analyte Name

Compound

Type Fit Type Eval.

Eval.

Result Q

Control

Criteria

Calibration Evaluation

C10 - C25 DRO MS AverageRF % RSD 10.3 £ 20

o-Terphenyl SURR AverageRF % RSD 7.1 £ 20




QA/QC Results

Second Source Calibration Verification

External Standard

JP-8

Client:

Project:

Service Request:

Date Analyzed:

Analysis Method:

Calibration Type:

Calibration Date:

Calibration ID:

Units:



10/21/2019

10/22/2019


8015C

CAL16158

ppm

J:\GC21\DATA\102119F\1021F118.DFile ID: Column ID: ZB-1

J:\GC21\DATA\102119F\1021F129.D

J:\GC21\DATA\102519F\1025F110.D

Analyte Name Expected Result

Average

RF

SSV

RF %D %Drift Criteria Curve Fit

AverageRF± 20 %NA-9164018009101000C10 - C25 DRO

1of1PagePrinted: 6/26/2020 16:18:40 Form 6B - Organic


SuperSet Reference:

† SPCC Compound ‡ CCC Compound

RR214104u:\Stealth\Crystal.rpt\Form6SS.rpt

QA/QC Results

Continuing Calibration Verification Summary

JP-8

External Standard

Client:

Project:

Service Request:

Date Analyzed:

Calibration Type:

Analysis Method:

Calibration Date:

Calibration ID:

Units:

Analysis Lot:



8015C

10/21/2019

CAL16158

KWG2001830

ppm


06/25/2020

J:\GC21\DATA\062420F-DRO\0624F185.DFile ID: ZB-1Column ID:

Curve FitCriteria%Drift%D

CCV

RF

Average

RFResultExpectedAnalyte Name

± 20NA-109001000C10 - C25 DRO 1800 AverageRF1630

± 20NA135750o-Terphenyl 1910 AverageRF2170

Printed: 6/26/2020 16:18:44 1of1PageForm 7 - Organic


SuperSet Reference: RR214104u:\Stealth\Crystal.rpt\Form7.rpt

QA/QC Results


JP-8

External Standard

Client:

Project:

Service Request:

Date Analyzed:

Calibration Type:

Analysis Method:

Calibration Date:

Calibration ID:

Units:

Analysis Lot:



8015C

06/24/2020

CAL16321

KWG2001831

ppm


06/25/2020

J:\GC21\DATA\062420F-JP8\0624F187.DFile ID: ZB-1Column ID:


CCV

RF

Average


± 20NA-118901000JP-8 (C8 - C18) 1820 AverageRF1630

± 20NA-64750o-Terphenyl 2230 AverageRF2110




QA/QC Results


JP-8

External Standard

Client:

Project:

Service Request:

Date Analyzed:

Calibration Type:

Analysis Method:

Calibration Date:

Calibration ID:

Units:

Analysis Lot:



8015C

10/21/2019

CAL16158

KWG2001830

ppm


06/25/2020

J:\GC21\DATA\062420F-DRO\0624F195.DFile ID: ZB-1Column ID:


CCV

RF

Average


± 20NA-89201000C10 - C25 DRO 1800 AverageRF1660

± 20NA155750o-Terphenyl 1910 AverageRF2200




QA/QC Results


JP-8

External Standard

Client:

Project:

Service Request:

Date Analyzed:

Calibration Type:

Analysis Method:

Calibration Date:

Calibration ID:

Units:

Analysis Lot:



8015C

06/24/2020

CAL16321

KWG2001831

ppm


06/25/2020

J:\GC21\DATA\062420F-JP8\0624F196.DFile ID: ZB-1Column ID:


CCV

RF

Average


± 20NA-79301000JP-8 (C8 - C18) 1820 AverageRF1700

± 20NA-24950o-Terphenyl 2230 AverageRF2200




QA/QC Results

Analysis Run Log

JP-8

Client:

Project:

Service Request:

Analysis Method: Analysis Lot:




8015C

File ID

Date

Analysis

Started

Start

Time

Date

Analysis

Finished

Finish

Time


KWG2001830

Q

GC21

ZB-1

Instrument ID:

Column:

KWG2001830-1 6/25/2020 19:00 6/25/2020 19:160624F185.D Continuing Calibration Verification

KWG2001830-2 6/25/2020 19:45 6/25/2020 20:010624F188.D Instrument Blank

KWG2001792-4 6/25/2020 20:07 6/25/2020 20:230624F189.D Method Blank

K2005164-001 6/25/2020 21:15 6/25/2020 21:310624F192.D 20-06644(360-011)

K2005164-002 6/25/2020 21:37 6/25/2020 21:530624F193.D 20-06645(360-001)



Form 8 - Organic 1of1PagePrinted: 06/26/2020 16:18:57

Results flagged with an asterisk (*) indicate the holding time was exceeded for the analysis

RR214104SuperSet Reference:u:\Stealth\Crystal.rpt\Form8.rpt

QA/QC Results

Analysis Run Log

JP-8

Client:

Project:

Service Request:

Analysis Method: Analysis Lot:




8015C

File ID

Date

Analysis

Started

Start

Time

Date

Analysis

Finished

Finish

Time


KWG2001831

Q

GC21

ZB-1

Instrument ID:

Column:



KWG2001792-4 6/25/2020 20:07 6/25/2020 20:230624F189.D Method Blank

KWG2001792-3 6/25/2020 20:30 6/25/2020 20:460624F190.D Duplicate Lab Control Sample

KWG2001792-2 6/25/2020 20:52 6/25/2020 21:080624F191.D Lab Control Sample

K2005164-001 6/25/2020 21:15 6/25/2020 21:310624F192.D 20-06644(360-011)

K2005164-002 6/25/2020 21:37 6/25/2020 21:530624F193.D 20-06645(360-001)

KWG2001792-1 6/25/2020 22:00 6/25/2020 22:160624F194.D 20-06644(360-011)MS





RR214104SuperSet Reference:u:\Stealth\Crystal.rpt\Form8.rpt

QA/QC Results

Extraction Prep Log



JP-8

K2005164

Final

Volume

KWG2001792

Water

Low

Client:

Project:

Sample Matrix:

Service Request:

Extraction Method: Extraction Lot:

Level:


Date

Received

Sample

Amount % Solids Note


Date Extracted: 06/25/2020

EPA 3510C


Date

Collected

K2005164-001 480mL 1ml NA06/20/2020-06644(360-011) 06/18/20

K2005164-002 480mL 1ml NA06/20/2020-06645(360-001) 06/18/20

KWG2001792-4 500mL 1ml NANAMethod Blank NA

KWG2001792-1 485mL 1ml NA06/20/2020-06644(360-011)MS 06/18/20

KWG2001792-2 500mL 1ml NANALab Control Sample NA

KWG2001792-3 500mL 1ml NANADuplicate Lab Control Sample NA



SuperSet Reference: RR214104u:\Stealth\Crystal.rpt\Form9L.rpt

cover page - organic analysis data package semivolatile

Documents