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Dash, J., J. Freeman, and B. Zimmermann, Cold Fusion Research - Low Energy Nuclear Reactions. 2003, Portland State University: Porland, OR. Slide 1 Cold Fusion Research Low Energy Nuclear Reactions Dr. John Dash, Mentor Portland State University Jeremy Freeman Mountain View High School Ben Zimmerman Wilson High School

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Page 1: Cold Fusion Research - LENR-CANR.orglenr-canr.org/acrobat/DashJcoldfusion.pdf · process was only theoretically possible in stars and large Tokamak reactors. ... 0.2 0.25 0.3 0.35

Dash, J., J. Freeman, and B. Zimmermann, Cold Fusion Research - Low Energy Nuclear Reactions. 2003, Portland State University: Porland, OR.

Slide 1

Cold Fusion ResearchLow Energy Nuclear ReactionsDr. John Dash, MentorPortland State University

Jeremy FreemanMountain View High School

Ben ZimmermanWilson High School

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Slide 2

IntroductionMarch 23, 1989. Electrochemists B. Stanley Pons and Martin Fleischmann shock the world by announcing their discovery of cold fusion.

Pons (left) and Fleischmann

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Slide 3

PossibilitiesThe original idea, that Deuterium could fuse in a small cell at room temperature, went against common knowledge.The D-D fusion process was only theoretically possible in stars and large Tokamakreactors.The startling results reported provided hope for a new source of energy.

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Slide 4

The Skeptical Revolution

Many, but not all, attempts to replicate the Fleischmann/Pons experiment return null results.Severe criticism of the topic appears in the scientific community soon after the 1989 announcement, often referring to the entire field as a “Pathological Science.”Cold fusion falls from the media spotlight.

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Slide 5

A Decade of ResearchDespite the poor reproducibility of the effect and the opposition of cold fusion skeptics, many researchers continue to pursue their interest in the subject.As a result of continuing research, a very large amount of evidence in support of cold fusion has been collected. This evidence includes excess heat, nuclear by-products, and nuclear transmutation.

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Slide 6

Our Apprenticeship

From Left:

Ben, Conrado Salas Cano, Dr. Dash and Jeremy

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Slide 7

Specific Aims Reproducibility – Construction of two identical experimental cells, with the goal of achieving positive experimental results for bothTo create a working demonstration of the cold fusion phenomenonTo reach approximately one Watt of excess heat energyTo examine electrodes for evidence of micro-chemical changes.

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Slide 8

Materials and Methods

The three cells, midway through the experiments

CB JC

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Slide 9

Cell Design

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Slide 10

The Purpose of Palladium

Palladium is known to absorb up to 900 times its volume of hydrogen.

Deuterium ions are attracted to the palladium cathode and occupy interstitial positions in the crystal lattice.

Palladium atomDeuterium atom

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Slide 11

Electrical Circuit Diagram

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Slide 12

First Experimental Setup

All three cells are placed in insulating cups within the box

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Slide 13

J Cell Polarity Reversal

On the 17th of July, midway through the experiments, the J experimental cell’s polarity was reversed, then restored, causing the formation of a greater surface area on the Palladium cathode.

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Slide 14

First Setup Results22 July Power Inputs

4.8

5

5.2

5.4

5.6

5.8

6

0 50 100 150 200 250 300 350 400Accumulated Run Time (minutes)

Control J Cell B Cell

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Slide 15

First Setup Results22 July Average Temperatures

50

51

52

53

54

55

56

57

58

59

60

300 320 340 360 380 400

Accumulated Run T ime (minutes)

Control J Cell B Cell

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Slide 16

* This term is only applicable during early experiments

Power In Power Out

Steady State

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Slide 17

Excess Heat Equation

The amount of excess heat produced by the experimental cells was found by comparison with our control cell, which was designed and assumed to produce none.

dHdt

dHdt

V I T TT T

V IdH

dtexcess D O

DD ambient

H ambientH

H O= − ⋅ +−−

⋅ −2 2( )

Power In Power OutExcess Heat Power Out Power In

== −

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Slide 18

First Setup Results22 July Excess Heat

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1

300 320 340 360 380 400Accumulated Run Time (minutes)

J Cell B Cell

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Slide 19

Second Experimental SetupA SEEBECK Envelope Calorimeter was utilized for a second set of experimental data on the same three cells.

This machine (lower green box) contains 100 thermocouples per square inch, which provide a total box output data set.

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Slide 20

Second Setup ResultsJuly 28 (C) - 29 (J) - 30 (B) Power Inputs

4.5

5

5.5

6

6.5

7

0 50 100 150 200 250 300

Accumulated Run Time (Minutes)

Pow

er In

put (

Wat

ts)

Control J Cell B Cell

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Slide 21

Second Setup ResultsJuly 28 (C) - 29 (J) - 30 (B) Temperature Evolution

2527293133353739414345

0 50 100 150 200 250 300

Accumulated Run Time (Minutes)

Tem

pera

ture

(C)

Control J Cell B Cell

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Slide 22

Second Setup ResultsSteady State Excess heat

0

0.05

0.1

0.15

0.2

0.25

0.3

0.35

0.4

0.45

0.5

270 275 280 285 290 295 300

Accumulated Run Time (minutes)

Hea

t Ene

rgy

(wat

ts)

J Cell B Cell

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Slide 23

Third Experimental Setup

Our mobile, open-air demonstration cart

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Slide 24

B Cell Polarity Reversal

On the 7th of August the B Cell’s polarity was reversed and then restored, resulting in the formation of a larger surface area on the palladium cathode.

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Slide 25

Third Setup Results6 August Excess Heat

0.00

0.20

0.40

0.60

0.80

1.00

1.20

1.40

1.60

1.80

2.00

0 50 100 150 200 250 300 350

Accumulated Run Time (min)

Hea

t Ene

rgy

(wat

ts)

J Cell B Cell

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Slide 26

Third Setup Results8 August I.R. Excess Heat

0.00

0.20

0.40

0.60

0.80

1.00

1.20

1.40

1.60

1.80

2.00

0 50 100 150 200 250 300 350 400

Accumulated Run Time (Minutes)

J Cell B Cell

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Slide 27

Scanning Electron Microscope

SEM and EDX Characterization

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Slide 28

Palladium Before Electrolysis

A

B

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Slide 29

Palladium Before EDX Spectra

A

B

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Slide 30

Palladium ImpuritiesExisting impurities on the palladium sample consisted mostly of carbon and oxygen. There were small amounts of other elements, but no significant contamination. No silver or cadmium was present.

Characterization data from a nearly identical experiment* is presented to show micro-chemical changes in composition after electrolysis.

*Conrado Salas Cano’s Master’s thesis

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Slide 31

Conrado Salas Cano’s D2O Palladium Cathode

Before

After

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Slide 32

Before Electrolysis ComparisonIn numberof atoms

In mass σin mass

41.93% 10.56% 0.20%

20.69% 6.94% 0.48%

0.07% 0.04% 0.06%

1.09% 1.45% 0.24%

36.09% 80.51% 0.85%

0.00% 0.00% 0.70%

0.00% 0.00% 0.42%

0.13% 0.51% 0.20%

C

O

S

Cu

Pd

Ag

Cd

Pt

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Slide 33

Pd Cathode After Electrolysis

In number of atoms In mass σin mass

12.87% 3.21% 0.07%

47.04% 15.59% 0.20%

4.55% 3.02% 0.04%

0.71% 0.94% 0.09%

33.14% 73.04% 0.31%

1.43% 3.19% 0.25%

0.00% 0.00% 0.19%

0.26% 1.03% 0.08%

C

O

S

Cu

Pd

Ag

Cd

Pt

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Slide 34

In numberof atoms

In mass

σin

mass

0.00% 0.00% 0.30%

12.68% 2.29% 0.41%

2.03% 0.73% 0.07%

11.50% 8.22% 1.02%

57.23% 68.5% 1.33%

16.43% 19.9% 0.81%

0.00% 0.00% 0.65%

0.13% 0.29% 0.13%

Spectrum and SEMQuant from spot #2

C

O

S

Cu

Pd

Ag

Cd

Pt

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Slide 35

Theoretical ExplanationThe Trapped Neutron Catalyzed Fusion Model can

provide an explanation for excess heat and nuclear transmutation based on the capture of thermal neutrons.

An explanation for the presence of silver after electrolysis is shown below:

Obtained from H. Kozima’s Discovery of the Cold Fusion Phenomenon, 1998 Ohtake Shuppan, Inc.

The natural abundance of Pd 108 is 27% and Pd 109 has a decay time of 13.6 hours.

n+ = +46108

46109 615Pd Pd MeV.

46109

47109 1166Pd Ag MeV= + + +−e eν .

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Slide 36

Summary & ConclusionsConsistently produced excess heat exists for reproducible cell types

Possible formation of unexpected elements after electrolysis points to nuclear reactions

Although several theories have been put forth, the driving mechanism responsible for cold fusion still remains largely a mystery.

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Slide 37

Key Apprenticeship Learning

Advanced, analytical laboratory skills developmentIntroductory familiarity with SEM, EDS, Calorimeters, and computer programsInstant immersion into a higher academic settingA fuller understanding of the scientific community

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Slide 38

AcknowledgementsDr. John Dash, MentorProfessor Hideo Kozima, Co-mentorDr. Jon Warner, Co-mentorConrado Salas Cano, Co-mentorApprenticeships in Science and Engineering program, with funding provided by the Academy of Applied Science’s REAP Program and the Engineering and Technology Industry CouncilBen and Jeremy’s Parents

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Slide 39

Questions and Comments