chapter 2: part i process, product design, process ......learning outcomes after studying this...

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CHAPTER 2: Part I Process, Product Design, Process Creation & Sustainability (Intro.)

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Page 1: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Intro to PD - 1

CHAPTER 2: Part I Process, Product Design,

Process Creation & Sustainability (Intro.)

Page 2: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process engineers.

• Be able to describe the life cycle of a chemical process and identify the

activities associated with it.

• Have an appreciation of the key steps in carrying out a product/process design.

• Be knowledgeable about the kinds of design decisions that challenge product and process design teams.

• Be familiar with the key roles of a chemical/process engineer.

• Be aware of the various techniques and steps involve during process creation.

Page 3: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Introduction & definition of concepts

• Product centric process design • Chemical product design

• Sustainable process design

Page 4: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Chemical process design

Process Flowsheet?

Raw material Products

Operating condition?

Equipment parameters?

Chemical process design involves the determination of the process flowsheet and the corresponding condition of

operation and equipment design that converts the selected raw materials to the desired products

Page 5: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Are our products & processes sustainable?

Only 25 wt. % of what goes into the pipe comes out as goods and services – scope for significant improvements (Adapted from Driolli, 2005)

Natural Resources

Goods and Services

Pollution, Waste and Environmental Disturbances

Need for significant improvement

Note: Without signficant improvements, our products-processes are not sustainable

Page 6: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Sustainable chemical process design

6

As a new definition of process design

Chemical Product Chemical Process ?? Raw Material

Chemical process design is about finding a sustainable process that can convert the raw materials to the desired

chemical products

Sustainable in terms of economic, low environmental impact, low waste, efficient operation, correct raw material, …..

Page 7: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Raw material, solvents, water, power, steam, …

Products, solvents, water, power, steam, unconverted materials, …

Chemical Process

time

D

eman

d

R

eser

ve

Sustainability of total system and sub-systems

Sustainability limit

Concept of sustainability 1 (Prolong the life of the process)

Page 8: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

• Boundary: process and its connections

• Compared to a base-case design and generate alternatives that improve the following

• Operability, energy consumption, waste reduction, environmental impact, safety, cost, ….

• Sustainability metrics (as defined by IChemE): 49 Environmental (resource usage; emissions, effluents, waste), economic (profit, value, tax; investments), societal (workplace, society)

Raw material, solvents, water, power, steam, …

Products, solvents, water, power, steam, unconverted materials, …

Chemical Process

Concept of Sustainability 2 (Measure of sustainability)

Page 9: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

• Improve the following:

• Operability, energy consumption, waste reduction, environmental impact, safety, cost, ….

• Sustainability metrics (as defined by IChemE)

Raw material, solvents, water, power, steam, …

Products, solvents, water, power, steam, unconverted materials, …

Chemical Process

Apply a systematic analysis of the mass and energy paths within the process to determine a set of mass and energy indicators that will help to define attainable targets for improvement;

generate alternatives that meet these targets through a “reverse” approach

(How to achieve sustainability?)

Concept of Sustainability 3

Page 10: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

“The sustainability of an industrial process can be evaluated using a set of three-dimensional (3D) indicators that represent all three dimensions of sustainability:  economic, environmental, and societal”

Sustainability Metrics defines by IChemE

Page 11: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

• Process Design – whose job?

• Design project in the context of a chemical process engineer’s role

• Process Design Definition

• Process Design Procedure

• Process Design Activities

• Process Life Cycle

• Levels of Design Accuracy

Introduction to Process Design Job

Page 12: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

One day in a job interview…...

What is your field of study? Chemical-polymer

Engineering!

Then, our chemistry lab might be the best place for you ? Oh no!

Not again...

The manager

The fresh grad

Page 13: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Chemical/Process Engineering

..is the field of study that involves the process of converting resources into value-added (VA) products

Page 14: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

What a Chemical Process Engineer* Does for a Living

1. Process Development

2. Process Design

3. Construction

4. Manufacturing

5. Technical Sales

6. Research

*A person whose job is related to the process of transforming materials into value-added products

Page 15: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

1. Process Development

• Design • Construction • Operation - testing - reaction & catalyst - process conditions - process control scheme - materials of construction

Pilot Plant (10 kg/hr) Chemical

Lab (10g)

Commercial Scale

(100 tonne/hr)

Page 16: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

2. Process Design

Process Parameters: • production rate • process conditions (T, P) • type of vessels • control systems • safety & pollution control system

Chemical Engineers Jobs’:

INPUT Process Flowsheet: • equipment & streams P & I Diagram Equipment Specifications • size • dimension • materials of construction • min/max capacity

OUTPUT

Page 17: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

3. Construction - “Moment of Truth”

Chemical Engineers Jobs’:

• Ascertain that equipment operates correctly?

• Are involved in plant commissioning (start up)

• Identify any problems with process and equipment

• Specify redesign requirements (as required)

Page 18: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

4. Commercial Production

Chemical Engineer

Troubleshooting Supervision Quality Control Debottlenecking

Energy Conservation Raw material conservation Pollution control Process control

Routine Operation

Process Improvement

Page 19: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

5. Technical Sales (or Sales Engineer)

Chemical Engineer Jobs’:

• Provide process and product recommendations

• Provide advice on development of new process & products

• “Networking” with experts from other fields in solving

process/equipment problems to meet customer needs

Page 20: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

6. Research

Chemical engineers Jobs’:

• Cooperate with chemist, scientists and

engineers from other fields to produce

new products.

• Develop new processing techniques.

• Improve & optimise process

operations.

• Design new equipment or improve the

existing ones.

Page 21: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

What a Chemical Process Engineer* Does for a Living

1. Process Development

2. Process Design: to be discussed?

3. Construction

4. Manufacturing

5. Technical Sales

6. Research

*A person whose job is related to the process of transforming materials into value-added products

Page 22: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Discussion Sessions: Process Design Issues

Discuss among your group members:

• What is a good definition for Process Design? • What are the basic prerequisites? • What do you think are the key steps involved in Process Design? • What initial key information do you think would be needed?

Page 23: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

A design project

• Survey/feasibility studies

• Project team

• Project structure/planning (milestone)

• Process and Product Design

Desired Products

PROCESS ?

Raw materials?

Process Structure

Page 24: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Class of Chemical Products

• Thousands of chemical products are manufactured.

• 3M company (formerly known Minnesota Mining & Manufacturing Company) – developed over 60 000 chemical products since 1904.

• Thus, chemical products roughly classified as; Basic chemical products, Industrial products and Consumer products.

• Basic chemical products:

- manufactured from natural resources such as commodity chemicals (ethylene, acetone, vinyl chloride) , specialty chemicals (difluoroethylene, ethylene glycol monomethyl, diethyl ketone), biomaterials (pharmaceuticals, tissue implants), polymeric materials (ethylene copolymer, polyvinyl chloride (PVC), polystyrene).

- Categories as well-defined molecules/mixture of molecules.

- Not sold directly to the consumer.

Page 25: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Class of Chemical Products

• Industrial products:

- Begins with basic chemical products.

- Such as: films, fibers (woven, nonwoven), paper, creams, pastes (cements, glues, adhesives)

• Consumer products:

- Manufactured from basic chemicals and industrial chemical products.

- Such as: dialysis devices, hand warmers, ink-jet cartriges, transparencies for

overhead projector, drug delivery patches, fuel cells, cosmetics, detergents.

- Sold directly to customer.

Page 26: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Manufacture of Chemical Products

Natural

Resources

Basic

Chemical

Products

Industrial

Products

Manufacturing

Process

Manufacturing

Process

Manufacturing

Process

Basic Chemical

Products

(Commodity and

Specialty Chemicals,

Biomaterials,

Polymeric Material)

Industrial Products

( Films, Fibers, Paper,..)

Customer Products

(Paper bag, Dialysis

Devices, Post-it Notes,

Transparencies, Drug

delivery Patches,

Cosmetics,..)

Manufacturing

Process

Manufacturing

Process

Manufacturing

Process

Manufacturing

Process

Manufacturing

Process

Manufacturing

Process

Page 27: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Methane

Ammonia

Methanol

Ethylene

Oxide

Chloralkali

Plant

Ethane

Propane

Ammonia

MTBE

Urea

Formadehyde

Ammonia Urea

Ammonium Nitrate

Ammonium

Phosphate Polyvinyl Chloride

Titanium Dioxide

Silicones

Polyethylene LDPE

Glycol

Surfactant

Polypropylene

Acrylics

Acrylonitrile

Caprolactam Terephthalic

Acid Polystyrene

ABS, SAN

MTBE

Unsaturated Esters

Butane

Benzene

Type of Process: Fractionated of Raw Natural Gas

Middle Distillates

Basic Chemical Products

Page 28: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

What is a Process/ Product Design?

A project/endeavor/task to determine the structure of a process to produce a product in the way that is economical, safe, and environmentally friendly.

Among other things, a project would involve management, planning, assessment and evaluation

Page 29: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Process Design in Top Management Level

Board of Director (BOD)1

(ideas, project scope)

What Product? Project “Green Light” Budgetary Requirements New Routes/Off-the Shelf Problems?

Executive Committee2

(feedback, feasibility studies, market survey)

Discussions/interviews with • Authority • Plant managers • Management team • Community

Decisions/Activities

Planning/Organisational Design

• Project Structure/Team • Project Milestone/Planning • Process/Product Design

1Client (Prospective owner), Project Manager, Investor 2Project Manager, CMT, Contractor, Authority

Page 30: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

(Seider et al., 2004)

Figure: Process Life Cycle– A Bird’s Eye View

Steps in Development of Process/Product Design

Page 31: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Process Design – Basic Components at Project Team Level

• Steps in the design of a chemical process: 1. Project Conception

2. Process Synthesis/Creation

3. Equipment Design

4. Economic Analysis

5. Optimisation

(Ulrich, 1984)

Page 32: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Process Design – Process Synthesis/Creation

Process Simulation

parameter

optimisation

Optimised Design

Material and Energy Balances

(manual & simulation)

Process Synthesis/

Flowsheeting

Process

Modelling/Analysis

(Manan, 2001)

structural optimisation

Page 33: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Process Creation (details)

• Product design team identifies needs and generate ideas for new product that meets customer requirement.

• Brainstorming sessions for alternatives

• Select promising alternatives for further research and development

• Base on the principles of thermodynamics, chemical kinetics, heat & mass transfer etc

Create & Access Primitive Problem

From lab or established database e.g. Knovel website, NIST (National Institute of Standard & Technology) chemical webpage, patents, research journals & etc.

Page 34: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Process Creation and Detailed Design

Page 35: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Final Design & Operation

Page 36: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Construction and Operation

Layout and

3-D Modelling

Construction

Startup and

Commissioning

Plant Operation

Debottlenecking

Decommisioning

Page 37: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

Some common terminology

• Process flow diagram (PFD) / process flowsheet – “interconnections of the individual process operations (e.g. drying, mixing, etc.) together with the quantitative variables (e.g. P, T, flowrates and composition)”

Page 38: CHAPTER 2: Part I Process, Product Design, Process ......Learning Outcomes After studying this topic, participants should: • Recognise the significance of design project for chemical/process

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