certificate of analysis · 2021. 7. 31. · email: ordered :sam@getfluent.com sample :...
TRANSCRIPT
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
07/30/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOG Kush WF 3.5g
OG KushMatrix: Flower
Certificateof Analysis
Sample:DA10727001-004Harvest/Lot ID: 0552 1637 0663 4642
Cultivation Facility: Tampa CultivationProcessing Facility : Tampa Processing
Seed to Sale# 0552 1637 0663 4642Batch Date: 07/16/21
Batch#: 3709 2701 6242 8437Sample Size Received: 31.5 gram
Total Weight/Volume: 828 unitsRetail Product Size: 3.5 gram
Ordered : 07/26/21sampled : 07/26/21
Completed: 07/30/21Sampling Method: SOP.T.20.010
Jul 30, 2021 | FLUENT82 NE 26th streetMiami, FL, 33137, US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolvents
NOT TESTED
FilthPASSED
Water ActivityPASSED
MoisturePASSED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
19.324%TOTAL THC/Container :676.340mg
Total CBD
0.069%TOTAL CBD/Container :2.422 mg
Total Cannabinoids
23.559%Total Cannabinoids/Container:824.565 mg
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
% ND 0.0790 1.3310 0.1540 ND ND ND 0.4510 <0.010 0.0240 21.5200
mg/g ND 0.7900 13.3100 1.5400 ND ND ND 4.5100 <0.010 0.2400 215.2000
LOD 0.0010 0.0010 0.0010 0.0010 0.0001 0.0010 0.0010 0.0001 0.0010 0.0010 0.0010
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 0.2093g 07/27/21 11:07:06 1823Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 07/28/21 12:12:28 Batch Date : 07/27/21 10:03:08Analytical Batch -DA029147POT Instrument Used : DA-LC-001 Running On : 07/28/21 11:37:56
Reagent Dilution Consums. ID
072321.R29 400 CE0123070621.21 287035261072321.R27 11945-019CD-019C
914C4-914AK929C6-929H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By457 NA NA NAAnalyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 07/27/21 12:15:44Analytical Batch -DA029159FIL Reviewed On - 07/27/21 14:14:40Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 457 NA NA 0.01 aw 0.65aw 0.545aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 07/27/21 11:42:10Analytical Batch -DA029155WAT Reviewed On - 07/27/21 16:30:58Instrument Used : DA-028 Rotronic Hygropalm
Moisture PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultMOISTURE CONTENT 457 NA NA 1 % 15% 13.240%
Analysis Method -MoistureAnalysis SOP.T.40.011 Batch Date : 07/27/21 11:26:29Analytical Batch -DA029153MOI Reviewed On - 07/27/21 16:34:36Instrument Used : DA-003 Moisture Analyzer
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
07/30/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOG Kush WF 3.5g
OG KushMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10727001-004Harvest/LOT ID: 0552 1637 0663 4642Batch# : 3709 27016242 8437Sampled : 07/26/21Ordered : 07/26/21
Sample Size Received : 31.5 gramTotal Weight/Volume : 828 unitsCompleted : 07/30/21Expires: 07/30/22Sample Method : SOP.T.20.010
Page 2 of 4
Terpenes TESTEDTerpenes LOD(%) mg/g % Result (%)
TOTAL TERPINEOL 0.007 0.569 0.056CAMPHENE 0.007 ND NDBETA-MYRCENE 0.007 2.578 0.257ALPHA-PHELLANDRENE
0.007 1.146 0.114
3-CARENE 0.007 0.421 0.042OCIMENE 0.007 ND NDEUCALYPTOL 0.007 ND NDLINALOOL 0.007 ND NDFENCHONE 0.007 ND NDISOPULEGOL 0.007 ND NDISOBORNEOL 0.007 ND NDHEXAHYDROTHYMOL
0.007 ND ND
NEROL 0.007 ND NDGERANYL ACETATE 0.007 ND NDBETA-CARYOPHYLLENE
0.007 1.251 0.125
VALENCENE 0.007 ND NDCIS-NEROLIDOL 0.007 0.273 0.027CARYOPHYLLENEOXIDE
0.007 ND ND
CEDROL 0.007 ND NDFARNESENE 0.007 0.966 0.096ALPHA-BISABOLOL 0.007 ND NDALPHA-PINENE 0.007 0.609 0.060SABINENE 0.007 ND NDBETA-PINENE 0.007 0.777 0.077ALPHA-TERPINENE 0.007 0.386 0.038LIMONENE 0.007 ND NDGAMMA-TERPINENE
0.007 < 0.2 < 0.020
TERPINOLENE 0.007 7.588 0.758SABINENEHYDRATE
0.007 ND ND
FENCHYL ALCOHOL 0.007 ND NDCAMPHOR 0.013 ND ND
Terpenes LOD(%) mg/g % Result (%)
BORNEOL 0.013 ND NDGERANIOL 0.007 ND NDPULEGONE 0.007 ND NDALPHA-CEDRENE 0.007 ND NDALPHA-HUMULENE 0.007 0.310 0.031TRANS-NEROLIDOL 0.007 ND NDGUAIOL 0.007 ND ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1082 1.0182g 07/27/21 12:07:36 2651
Analysis Method -SOP.T.40.090Analytical Batch -DA029138TER Reviewed On - 07/29/21 18:27:43Instrument Used : DA-GCMS-004Running On : 07/27/21 16:41:39Batch Date : 07/27/21 09:51:09
Reagent Dilution Consums. ID
061821.09 10 CE0123R1AB5972012499402
Terpenoid profile screening is performed using GC-MS/MS TQ-8040 with LiquidInjection (Gas Chromatography – Mass Spectrometer Triple Quad) which canscreen 37 terpenes using Method SOP.T.40.090 Terpenoid Analysis Via GC-MS/MS.
Total (%) 1.687
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
07/30/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOG Kush WF 3.5g
OG KushMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10727001-004Harvest/LOT ID: 0552 1637 0663 4642Batch# : 3709 27016242 8437Sampled : 07/26/21Ordered : 07/26/21
Sample Size Received : 31.5 gramTotal Weight/Volume : 828 unitsCompleted : 07/30/21Expires: 07/30/22Sample Method : SOP.T.20.010
Page 3 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.1 NDACEPHATE 0.01 ppm 0.1 NDACEQUINOCYL 0.01 ppm 0.1 NDACETAMIPRID 0.01 ppm 0.1 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 0.1 NDBIFENAZATE 0.01 ppm 0.1 NDBIFENTHRIN 0.01 ppm 0.1 NDBOSCALID 0.01 PPM 0.1 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 1 NDCHLORMEQUAT CHLORIDE 0.1 ppm 1 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.2 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZINON 0.01 ppm 0.1 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 0.1 NDFENHEXAMID 0.01 ppm 0.1 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 0.1 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 0.1 NDFLUDIOXONIL 0.01 ppm 0.1 NDHEXYTHIAZOX 0.01 ppm 0.1 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 0.4 NDKRESOXIM-METHYL 0.01 ppm 0.1 NDMALATHION 0.02 ppm 0.2 NDMETALAXYL 0.01 ppm 0.1 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 0.1 NDNALED 0.025 ppm 0.25 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.1 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.1 NDPROPICONAZOLE 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 0.5 NDPYRIDABEN 0.02 ppm 0.2 NDSPIROMESIFEN 0.01 ppm 0.1 NDSPIROTETRAMAT 0.01 ppm 0.1 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 0.1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 0.5 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.05 PPM 5 ND
TOTAL DIMETHOMORPH 0.02 PPM 0.2 NDTOTAL PERMETHRIN 0.01 ppm 0.1 NDTOTAL SPINETORAM 0.02 PPM 0.2 NDTOTAL SPINOSAD 0.01 ppm 0.1 NDTRIFLOXYSTROBIN 0.01 ppm 0.1 NDPENTACHLORONITROBENZENE (PCNB)*
0.01 PPM 0.15 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 0.7 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 0.5 NDCYPERMETHRIN * 0.01 PPM 0.5 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 , 1665 1.1331g 07/27/21 11:07:21 585 , 585Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.40.066, SOP.T.40.070 , SOP.T.30.065,SOP.T40.070Analytical Batch - DA029134PES , DA029148VOL Reviewed On- 07/27/21
14:14:40Instrument Used : DA-LCMS-003 (PES) , DA-GCMS-006Running On : 07/28/21 16:49:59 , 07/27/21 16:05:23 Batch Date : 07/27/21 09:40:53
Reagent Dilution Consums. ID063021.R44 25 6524407-03063021.R43071321.R06072121.R01092820.59
Pesticide screen is performed using LC-MS and/or GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060Sample Preparation for Pesticides Analysis via LCMSMS and GCMSMS.SOP.T40.065/SOP.T.40.066/SOP.T.40.070 Procedure for Pesticide Quantification Using LCMS and GCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
07/30/21
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsOG Kush WF 3.5g
OG KushMatrix : Flower
Certificate of Analysis PASSED
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10727001-004Harvest/LOT ID: 0552 1637 0663 4642Batch# : 3709 27016242 8437Sampled : 07/26/21Ordered : 07/26/21
Sample Size Received : 31.5 gramTotal Weight/Volume : 828 unitsCompleted : 07/30/21Expires: 07/30/22Sample Method : SOP.T.20.010
Page 4 of 4
Microbials PASSED
Analyte LOD Result Action Level (cfu/g)ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.TOTAL YEAST AND MOLD 10 1000 CFU 100000
Analysis Method -SOP.T.40.043 / SOP.T.40.044 / SOP.T.40.041Analytical Batch -DA029131MIC , DA029166TYM Batch Date : 07/27/21, 07/27/21Instrument Used : PathogenDx Scanner DA-111, Incubator (25-27C) DA-096Running On :
Analyzed by Weight Extraction date Extracted By1829, 1829 1.1402g 07/27/21 1829, 1829
Reagent060421.06071921.R36021921.37071021.R03Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing. Pour-plating is used for quantitation and confirmation, Total Yeast and Mold hasan action limit of 100,000 CFU.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA029135MYC | Reviewed On - 07/29/21 11:46:51Instrument Used : DA-LCMS-003 (MYC)Running On : 07/28/21 16:50:14Batch Date : 07/27/21 09:43:11
Analyzed by Weight Extraction date Extracted By585 g 07/27/21 01:07:56 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID071621.R04070221.R54070221.R56070221.R57072621.R08071921.R08
072621.R06072621.R07071421.R52071421.R51030420.08050121.01
100 3146-870-00811989-024CC-024
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 0.2CADMIUM 0.02 PPM ND 0.2MERCURY 0.02 PPM ND 0.2LEAD 0.05 PPM ND 0.5
Analyzed by Weight Extraction date Extracted By53 0.2789g 07/27/21 12:07:59 1879
Analysis Method -SOP.T.40.050, SOP.T.30.052, SOP.T.30.053, SOP.T.40.051Analytical Batch -DA029133HEA | Reviewed On - 07/28/21 08:15:27Instrument Used : DA-ICPMS-003Running On : 07/28/21 08:12:56Batch Date : 07/27/21 09:27:43
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) using Method SOP.T.30.052, SOP.T.30.053 Sample Preparation for Heavy MetalsAnalysis via ICP-MS and SOP.T.40.050, SOP.T.40.051 Heavy Metals Analysis via ICP-MS.