brooklyn, new york remedial investigation report · brooklyn, new york remedial investigation...

DOMINO SUGAR SITE E

317-329 KENT AVENUE BROOKLYN, NEW YORK

Remedial Investigation Report

NYC VCP Site Number: 15CVCP002K

Prepared for:

Two Trees Management, LLC

45 Main Street, Suite 602

Brooklyn, NY 11201

Prepared by:

EEBB CC

1808 Middle Country Road

Ridge, NY 11961

September 2014

Environmental Business Consultants

REMEDIAL INVESTIGATION REPORT

TABLE OF CONTENTS

LIST OF ACRONYMS

CERTIFICATION

EXECUTIVE SUMMARY ...................................................................................................... i

REMEDIAL INVESTIGATION REPORT ............................................................................ 1

1.0 SITE BACKGROUND............................................................................................... 1

1.1 Site Location and Current Usage ............................................................................ 1

1.2 Proposed Redevelopment Plan ............................................................................... 1

1.3 Description of Surrounding Property...................................................................... 3

2.0 SITE HISTORY.......................................................................................................... 5

2.1 Past Uses and Ownership........................................................................................ 5

2.1.1 Phase I Environmental Site Assessment Report (EHI, 2004) ......................... 5

2.1.2 Phase I Environmental Site Assessment Report (Emteque LLC, 2012).......... 5

2.2 Previous Investigations ........................................................................................... 7

2.2.1 Phase III Environmental Site Assessment (Nova, 2004) ........................................ 7

2.2.2 Subsurface (Phase II) Investigation (AKRF, 2009) ................................................ 8

2.3 Site Inspection......................................................................................................... 8

2.4 Areas of Concern .................................................................................................... 9

3.0 PROJECT MANAGEMENT.................................................................................... 10

3.1 Project Organization ............................................................................................. 10

3.2 Health and Safety.................................................................................................. 10

3.3 Materials Management.......................................................................................... 10

4.0 REMEDIAL INVESTIGATION ACTIVITIES....................................................... 11

4.1 Geophysical Investigation..................................................................................... 11

4.2 Borings and Monitoring Wells.............................................................................. 11

4.3 Sample Collection and Chemical Analysis........................................................... 12

5.0 ENVIRONMENTAL EVALUATION..................................................................... 17

5.1 Geological and Hydrogeological Conditions........................................................ 17

5.2 Soil Chemistry ...................................................................................................... 17

REMEDIAL INVESTIGATION REPORT

TABLE OF CONTENTS

5.3 Groundwater Chemistry........................................................................................ 18

5.5 Prior Activity ........................................................................................................ 19

5.6 Impediments to Remedial Action ......................................................................... 19

TABLES Table 1 - Construction Details for Soil Borings Table 2 - Soil Analytical Results (VOCs) Table 3 - Soil Analytical Results (SVOCs) Table 4 - Soil Analytical Results (Pesticides/PCBs) Table 5 - Soil Analytical Results (Metals) Table 6 - Groundwater Analytical Results (VOCs) Table 7 - Groundwater Analytical Results (SVOCs) Table 8 - Groundwater Analytical Results (Pesticides/PCBs) Table 9 - Groundwater Analytical Results (Total Metals) Table 10 - Groundwater Analytical Results (Dissolved Metals) Table 11 - Soil Gas Analytical Results (VOCs)

FIGURES Figure 1 - Site Location Map Figure 2 - Site Boundary Map Figure 3 - Redevelopment Plan Figure 4 - Surrounding Land Use Figure 5 - Site Sampling Locations Figure 6 - Soil Exceedences Map Figure 7 - Groundwater Exceedences Map Figure 8 - Soil Vapor Detections

ATTACHMENTS Attachment A - Soil Boring Logs Attachment B - Groundwater Sampling Logs Attachment C - Soil Gas Sampling Logs Attachment D - Laboratory Reports in Digital Format Attachment E - EHI 2004 Phase I Report Attachment F - Emteque 2012 Phase I Report Attachment G - Nova 2004 Phase III Report Attachment H - AKRF 2009 Phase II Report

LIST OF ACRONYMS Acronym Definition

AOC Area of Concern

CAMP Community Air Monitoring Plan

COC Contaminant of Concern

CPP Citizen Participation Plan

CSM Conceptual Site Model

DER-10 New York State Department of Environmental Conservation Technical Guide 10

FID Flame Ionization Detector

GPS Global Positioning System

HASP Health and Safety Plan

HAZWOPER Hazardous Waste Operations and Emergency Response

IRM Interim Remedial Measure

NAPL Non-aqueous Phase Liquid

NYC VCP New York City Voluntary Cleanup Program

NYC DOHMH New York City Department of Health and Mental Hygiene

NYC OER New York City Office of Environmental Remediation

NYS DOH ELAP

New York State Department of Health Environmental Laboratory Accreditation Program

OSHA Occupational Safety and Health Administration

PID Photo-ionization Detector

QEP Qualified Environmental Professional

RI Remedial Investigation

RIR Remedial Investigation Report

SCO Soil Cleanup Objective

SPEED Searchable Property Environmental Electronic Database

CERTIFICATION I, Kevin Brussee, am a Qualified Environmental Professional, as defined in RCNY § 43-1402(ar). I have primary

direct responsibility for implementation of the Remedial Investigation for the Domino Sugar Site E Redevelopment

Project located at 317 to 329 Kent Avenue, Brooklyn, NY, (NYC VCP Site No. 15CVCP002K). I am responsible

for the content of this Remedial Investigation Report (RIR), have reviewed its contents and certify that this RIR is

accurate to the best of my knowledge and contains all available environmental information and data regarding the

property.

Qualified Environmental Professional Date Signature

DOMINO SUGAR SITE E 317-329 Kent Avenue, Brooklyn, NY Remedial Investigation Report

i Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

EXECUTIVE SUMMARY The Remedial Investigation Report (RIR) provides sufficient information for establishment of

remedial action objectives, evaluation of remedial action alternatives, and selection of a remedy

pursuant to RCNY§ 43-1407(f). The remedial investigation (RI) described in this document is

consistent with applicable guidance.

Site Location and Current Usage

Domino Sugar Site E is located at 317 to 329 Kent Avenue in the Williamsburg-South Side

section of Brooklyn, New York, and is currently identified as a portion of Block 2428, Lot 1 on

the New York City Tax Map. Figure 1 shows the Site location. Lot 1 is a 57,600 ft2 lot located

on the east side of Kent Avenue between South 3rd Street to the north and South 4th Street to the

south. Site E has been undeveloped and utilized for parking for employees of the Domino Sugar

Company and other sugar refinery companies since the 1940's. The former parking lot is

currently being utilized as The Brooklyn Bike Park, a recreational bicycle track.

Site A is currently bordered by South 3rd Street to the north, South 4th Street to the south,

several residential apartment buildings and a scrap metal facility to the east and Kent Avenue to

the west. Site A is an rectangular shaped lot consisting of 180 ft of street frontage on Kent

Avenue and 320 ft of street frontage on both South 3rd Street and South 4th Street, for a total of

approximately 57,600 ft2. A map of the site boundary is shown on Figure 2.

Summary of Proposed Redevelopment Plan

Redevelopment of the former Domino Sugar properties (Block 2414, Lot 1 and Block 2428, Lot

1) will include four new mixed-use buildings (Sites A, B, D, E), adaptively reuse the existing

landmarked Refinery building (Site F), create a one acre inland green space to be called Domino

Square (Site C) and develop a new waterfront park.

The proposed future use of Site E will consist of a new 15-story mixed-use building with 5 cellar

levels. The new building will have a total floor area of approximately 774,003 ft2, consisting of

approximately 20,612 ft2 of retail space, a 178,718 ft2 parking facility, and 114,369 ft2 of

community facility uses. This building would rise to a maximum height of approximately 435

feet.


ii Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

The lowest cellar level (C5) will occupy the majority of the Site E footprint, with the exception

of areas in the northwest and southwest corners. Cellar level C5 will consist of three separate

community facility areas that will be used as a soccer field, gymnasium, and an aquatic center.

Cellar level C5 will also have four elevator pits, and five stairwells. The next lowest cellar level

(C4) will consist of a locker room for the community facilities on C5, and an additional

recreation space for the community facility. Cellar level C3 will consist of a storage room and

office space for the community facilities, and several large mechanical rooms. Cellar levels C2

and C1 will consist of an underground parking garage, but will also contain the the electrical

room, telecom room, plumbing room, gas meter room, water and sewer room, fire protection

room, two compactor rooms, bike storage room, men's and women's lockers and lunch room, the

building supers' office, workshop and storage room.

The building's first floor will consist of three retail spaces on the west end of the building, the

building's residential lobby, and additional parking. The second floor will have apartments along

the west end of the building, additional ground level retail spaces along the eastern end of South

3rd Street and South 4th Street, and additional parking spaces within the middle of the building.

The third floor will consist of residential apartments along Kent Avenue, South 3rd Street and

South 4th Street, and parking within the center of the building. After the 3rd floor, the building

divides into two separate towers. The two residential towers rise from the 4th floor to the 12th

floor before joining again at the 13th floor. The 4th through 15th floors consist solely of

residential apartments.

Assuming an excavation depth of approximately 52 ft for the entire 57,600 ft2 lot for

construction of the new building's five cellar levels, a total of approximately 111,000 cubic yards

(166,400 tons) of soil will require excavation. Layout of the proposed site development is

presented in Figure 3. The current zoning designation is C6-2. The proposed use is consistent

with existing zoning for the property.

Summary of Past Uses of Site and Areas of Concern

Historic Sanborn maps were reviewed to determine the historic use of Site E. The Sanborn maps

indicate Site that prior to 1887, Site was primarily developed with multiple 3-story row houses

along South 3rd Street and South 4th Street. However, the northwest corner of Site E was


iii Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

developed with a 9-story industrial building identified as the kiln and filter house for the

Havemeyer & Elder Sugar Refinery located across Kent Avenue. The building contained

numerous coal fired boilers and two large smoke stacks.

By 1904 Sanborn map, the sugar refinery operation had expanded to several of the lots along

South 4th Street. The sugar refinery facility operated under the name American Sugar Refinery.

It consisted of a 7-story industrial building at 29 to 35 South 4th Street that housed 16 electrical

engines, a 2-story building at 38-40 South 3rd Street that was utilized for coal storage, a 2 and 4-

story building at 42-44 South 3rd Street that housed numerous boilers, and a 10-story industrial

building at 317-323 Kent Avenue that consisted of 14 boilers, and was utilized as the kiln and

filter house. Several of the 3-story row houses along South 4th Street were also utilized by

American Sugar Refinery for pattern storage. A small lot at 325 Kent Avenue was developed

with three 3-story buildings identified as the facility's plating room, paints, and saw-dust house.

By 1918, the American Sugar Refining Company of NY utilized nearly the entire footprint of

Site E, with the exception of a 3-story apartment building w/first floor store on the corner of

South 4th Street and Kent Avenue (329 Kent Avenue). The 1918 Sanborn map labels Site E as

several distinct sections with letters according to the use of the buildings by the American Sugar

Refining Company of NY.

Section G - Consists of two buildings and an open space area - 1) 317 - 323 Kent Avenue

- A 9-story building with a basement that was used as the kiln and filter house, 2) 32-36

South 3rd Street - labeled as the old boiler house, and as vacant and partly removed, and

3) 38-40 South 3rd Street - a coal yard.

Section Q - Consists of three buildings 1) 46-54 South 3rth Street - A 68ft high building

consisting of six large syrup tanks, 2) 42-44 South 3rd Street - a 2-story building used for

storage of bone black and 3) 49 South 4th Street - a 1-story building labeled as a filling

house.

Section P - Developed with two adjacent seven story buildings. The building at 37-49

South 4th Street was labeled as the filter house, and the building at 29-35 South 4th Street

was labeled as the filler house.

Section T - Developed with a former 3-story residential building labeled as the pattern

shop, and an open lot likely used for parking.


iv Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

By 1935, most of the industrial buildings are vacant, and by 1947, the majority of the

buildings on Site E were demolished. The remaining two 3-story buildings on the corner of

South 4th Street and Kent Avenue (327 and 329 Kent Avenue) were demolished by 1977.

The AOCs identified for Site E include:

1. Historic fill layer is present at the Site from grade to depths as great as 15 feet below

grade;

2. The past use of a portion of Site E as a plating facility; and

3. Areas of the Site that were formerly developed with industrial buildings that house large

scale electric generators and boilers for the sugar refinery.

Summary of the Work Performed under the Remedial Investigation

EBC performed the following scope of work within Site E in April of 2014:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,

buildings, etc.);

2. Installed six soil borings within Site E, and collected twelve soil samples for chemical

analysis from the soil borings to evaluate soil quality; and

3. Installed two groundwater monitoring wells within Site E and collected two groundwater

samples from the two monitoring wells, and collected one groundwater sample from an

existing geotechnical monitoring well to evaluate groundwater quality; and

4. Installed five soil vapor probes across the Site and collected five soil vapor samples for

chemical analysis.

Summary of Environmental Findings

1. The elevation of Site E is approximately 34 feet on the eastern end, and approximately 21

feet along Kent Avenue.

2. Depth to groundwater varies across Site E from approximately 34 feet on the eastern end,

to approximately 22 feet along Kent Avenue.

3. Depth to bedrock is at the Site is greater than 100 feet.

4. The stratigraphy of Site E, from the surface down, consists of a layer of historic fill

material that varies from 2 to approximately 15ft, underlain by a medium silty brown

sand with gravel.


v Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

5. Soil/fill samples collected during the 2014 EBC RI, 2004 Nova Phase III, and 2008

AKRF Phase II showed no VOCs above Unrestricted Use SCOs with the exception of

acetone (68 micrograms per kilogram [µg/Kg]). Naphthalene (maximum [max] of 430

µg/Kg) was detected in multiple soil samples below Unrestricted Use SCOs. Eight

SVOCs including benz(a)anthracene (max of 23,000 μg/Kg), benzo(a)pyrene (max of

20,000 μg/Kg), benzo(b)fluoranthene (max of 20,000 μg/Kg), benzo(k)fluoranthene (max

of 20,000 μg/Kg), chrysene (max of 19,000 μg/Kg), dibenz(a,h)anthracene (max of 8,600

μg/Kg), indeno(1,2,3-cd)pyrene (max of 18,000) and phenanthrene (max of 160,000

μg/Kg) were detected above Unrestricted Use and Restricted Residential Use SCOs

within soil samples retained from the historic fill layer. Several metals including arsenic

(137 mg/Kg), cadmium (8.19 mg/kg), copper (max of 185 mg/Kg), lead (max of 446

mg/Kg), mercury (max of 0.55 mg/Kg), nickel (39.6 mg/Kg), and zinc (max of 1,480

mg/Kg) were detected above Unrestricted Use SCOs. Of these metals, arsenic, cadmium

and lead also exceeded Restricted Residential Use SCOs within soil samples collected

from the historic fill layer. PCB-1254 (210 µg/Kg) was detected within one shallow soil

sample at a concentration above Unrestricted Use SCOs and within one shallow soil

sample and PCB-1260 (maximum of 25 µg/Kg) was detected within two shallow soil

samples at a concentration below Unrestricted Use SCOs. The pesticides 4,4'-DDD (max

of 15 µg/Kg) and 4,4'-DDT (max of 13 µg/Kg) were detected within two shallow soil

samples at a concentration above Unrestricted Use SCOs. Neither the pesticides nor

PCBs were detected within any of the deeper soil samples retained from the same soil

boring locations. Overall, the findings were consistent with observations for historical fill

sites in areas throughout NYC.

6. Groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II

showed no detectable concentrations of pesticides or PCBs. The chlorinated VOCs cis-

1,2-dichlorothene (maximum of 5.56 µg/L), tetrachloroethene (maximum of 5.7 µg/L),

and trichloroethene (maximum of 27 µg/L) were detected within the groundwater

samples collected by AKRF in 2008 and EBC in 2014 above GQS. The following VOCs

were detected in one or more of the groundwater samples at concentrations below GQS:

1,1-dichloroethene (1.7 µg/L), acetone (maximum of 2.7 µg/L), carbon disulfide (0.90

µg/L), chloroform (1.5 µg/L), and methylene chloride (0.38 µg/L). SVOCs detected


vi Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

above GQS included benzo(a)anthracene (max of 0.49 µg/L), benzo(b)fluoranthene (max

of 0.48 µg/L), benzo(k)fluoranthene (0.08 µg/L), bis(2-ethylhexyl)phthalate (max of 42

µg/L), chrysene (max. of 0.49 µg/L), and indeno(1,2,3-cd)pyrene (3.7 µg/L) in one or

more of the three groundwater samples collected by EBC in 2014 and the groundwater

sample collected by AKRF in 2008. Dissolved metals present in groundwater at levels

above GQS included iron, lead, magnesium, manganese, selenium and sodium. The

presence of some of these metals in groundwater, specifically those that are common

salinity indicators, can be attributed to the proximity to the East River and the intrusion of

road salting.

7. Soil vapor samples collected during the 2014 EBC RI indicated petroleum related VOCs

and chlorinated VOCs were present at low concentrations. Petroleum-related VOCs

(BTEX) were detected at a maximum concentration of 141.43 μg/m3. Overall the highest

reported concentrations was for acetone (maximum of 7693 μg/m3). Trichloroethylene

(TCE) was detected in three of the five soil vapor samples at a concentration ranging

from 241 to 61.2 μg/m3. The New York State Department of Health (NYSDOH) Final

Guidance on Soil Vapor Intrusion (October 2006) notes mitigation is the recommended

action for a TCE concentrations above 250 μg/m3 in soil gas.Tetrachloroethylene (PCE)

was detected in all five soil vapor samples, and ranged in concentration from 2.03 to 28.3

μg/m3. Carbon tetrachloride was detected within three of the five soil vapor samples at a

maximum concentration of 0.566 μg/m3, and 1,1,1-trichloethylene (TCA) was detected in

three of the five soil vapor samples at a maximum concentration of 3.54 μg/m3. The PCE,

carbon tetrachloride and TCA concentrations are below the monitoring level ranges

established within the NYSDOH Final Guidance on Soil Vapor Intrusion.


1

EEBB CC Environmental Business Consultants 1808 Middle Country Road

Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

REMEDIAL INVESTIGATION REPORT 1.0 SITE BACKGROUND

Two Trees Management LLC has applied to enroll in the New York City Voluntary Cleanup

Program (NYC VCP) to investigate and remediate a 1.32-acre Site located at 317 to 329 Kent

Avenue in the Williamsburg-South Side section of Brooklyn, New York. Site E will be

redeveloped with a 15-story mixed use building that will have 5 cellar levels for community

facility space and parking. The portion of the RI work conducted on Site E was performed

between April 2, 2014, and May 8, 2014. This RIR summarizes the nature and extent of

contamination and provides sufficient information for establishment of remedial action

objectives, evaluation of remedial action alternatives, and selection of a remedy that is protective

of human health and the environment consistent with the use of the property pursuant to RCNY§

43-1407(f).

1.1 Site Location and Current Usage

Domino Sugar Site E is located at 317 to 329 Kent Avenue in the Williamsburg-South Side

section of Brooklyn, New York, and is currently identified as a portion of Block 2428, Lot 1 on

the New York City Tax Map. Figure 1 shows the Site location. Lot 1 is a 57,600 ft2 lot located

on the east side of Kent Avenue between South 3rd Street to the north and South 4th Street to the

south. Site E has been undeveloped and utilized for parking for employees of the Domino Sugar

Company and other sugar refinery companies since the 1940's. The former parking lot is

currently being utilized as The Brooklyn Bike Park, a recreational bicycle track.

Site A is currently bordered by South 3rd Street to the north, South 4th Street to the south,

several residential apartment buildings and a scrap metal facility to the east and Kent Avenue to

the west. Site A is an rectangular shaped lot consisting of 180 ft of street frontage on Kent

Avenue and 320 ft of street frontage on both South 3rd Street and South 4th Street, for a total of

approximately 57,600 ft2.A map of the site boundary is shown on Figure 2.

1.2 Proposed Redevelopment Plan

Redevelopment of the former Domino Sugar properties (Block 2414, Lot 1 and Block 2428, Lot

1) will include four new mixed-use buildings (Sites A, B, D, E), adaptively reuse the existing


2 Environmental Business Consultants


Phone 631.504.6000 Fax 631.924.2870

landmarked Refinery building (Site F), create a one acre inland green space to be called Domino

Square (Site C) and develop a new waterfront park.

The proposed future use of Site E will consist of a new 15-story mixed-use building with 5 cellar

levels. The new building will have a total floor area of approximately 774,003 ft2, consisting of

approximately 20,612 ft2 of retail space, a 178,718 ft2 parking facility, and 114,369 ft2 of

community facility uses. This building would rise to a maximum height of approximately 435

feet.

The lowest cellar level (C5) will occupy the majority of the Site E footprint, with the exception

of areas in the northwest and southwest corners. Cellar level C5 will consist of three separate

community facility areas that will be used as a soccer field, gymnasium, and an aquatic center.

Cellar level C5 will also have four elevator pits, and five stairwells. The next lowest cellar level

(C4) will consist of a locker room for the community facilities on C5, and an additional

recreation space for the community facility. Cellar level C3 will consist of a storage room and

office space for the community facilities, and several large mechanical rooms. Cellar levels C2

and C1 will consist of an underground parking garage, but will also contain the the electrical

room, telecom room, plumbing room, gas meter room, water and sewer room, fire protection

room, two compactor rooms, bike storage room, men's and women's lockers and lunch room, the

building supers' office, workshop and storage room.

The building's first floor will consist of three retail spaces on the west end of the building, the

building's residential lobby, and additional parking. The second floor will have apartments along

the west end of the building, additional ground level retail spaces along the eastern end of South

3rd Street and South 4th Street, and additional parking spaces within the middle of the building.

The third floor will consist of residential apartments along Kent Avenue, South 3rd Street and

South 4th Street, and parking within the center of the building. After the 3rd floor, the building

divides into two separate towers. The two residential towers rise from the 4th floor to the 12th

floor before joining again at the 13th floor. The 4th through 15th floors consist solely of

residential apartments.




Phone 631.504.6000 Fax 631.924.2870

Assuming an excavation depth of approximately 52 ft for the entire 57,600 ft2 lot for

construction of the new building's five cellar levels, a total of approximately 111,000 cubic yards

(166,400 tons) of soil will require excavation. Layout of the proposed site development is

presented in Figure 3. The current zoning designation is C6-2. The proposed use is consistent

with existing zoning for the property.

Layout of the proposed site development is presented in Figure 3. The current zoning designation

is C6-2. The proposed use is consistent with existing zoning for the property.

1.3 Description of Surrounding Property

The area immediately surrounding Site E consists of the former Domino Sugar facility buildings

to west, and industrial buildings to the north, south and east. Figure 4 shows the surrounding land

usage of the adjacent properties listed below as well as additional properties located up to 500

feet away from the Site. No hospitals, schools or daycare facilities are located within a 250 ft

radius of the Site.

Surrounding Property Usage

Direction Property Description

North – Opposite side of South 3rd Street

Block 2415, Lot 1 - 315 Kent Avenue Developed with a 1-story industrial/manufacturing building

Block 2415, Lot 7501 - 29 South 3rd Street Developed a new 4-story, 26-unit residential apartment building.

Block 2415, Lot 38 - 37 South 3rd Street Developed a 4-story, 8-unit residential apartment building, with first floor retail space.

Block 2415, Lots 36 and 37 - 41 and 43 South 3rd Street Two small undeveloped lots

South – Opposite side of South 4th Street

Block 2441, Lot 8 - 331 Kent Avenue Developed with a 2-story commercial/office building consisting of 3 commercial spaces and one residential unit.

Block 2441, Lot 12 - 34 South 4th Street Developed with a 1-1/2-story industrial/manufacturing building constructed in 1996.

Block 2441, Lot 15 - 48 South 4th Street Developed with former 2-1/2 story industrial/manufacturing building converted into residential apartments.




Phone 631.504.6000 Fax 631.924.2870

Block 2441, Lot 21 - 47 South 5th Street Developed with a small one-story industrial/manufacturing building converted into a bar/restaurant.

East – Adjacent Property

Block 2428, Lot 24 - 56 South 3rd Street Developed with a new 4-story residential/apartment building. Block 2428, Lot 30 - 55 South 4th Street Developed with a one industrial/manufacturing building utilized for scrap metal sorting/storage. Block 2428, Lots 36 and 27 - 376 and 378 Wythe Avenue Two thin lots developed with multi-family walk-ups with rear yards.

West –

Block 2414, Lot 1 (SITE C) - 314 Kent Avenue Former industrial buildings associated with the Domino Sugar Factory.




Phone 631.504.6000 Fax 631.924.2870

2.0 SITE HISTORY

2.1 Past Uses and Ownership

Two Phase I Environmental Site Assessment (ESA) Reports have been completed for Sites A, B,

C, D, E and F. Both reports are summarized below.

2.1.1 Phase I Environmental Site Assessment Report (EHI, 2004)

A Phase I Environmental Site Assessment Report was completed by Environmental Health

Investigations, Inc. in 2004, for Sites A, B, C, D, E, and F. A copy of the Phase I Report is

attached in Attachment E. The Phase I Environmental Site Assessment Report identified the

vacant lot as parking for Domino Sugar employees, but did not thoroughly investigate the Site E

history prior to use as parking. The Phase I Report did not reveal any on-Site Recognized

Environmental Conditions in connection with Site E.

2.1.2 Phase I Environmental Site Assessment Report (Emteque LLC, 2012)

A Phase I Environmental Site Assessment Report was completed by Emteque LLC in 2012, for

Sites A, B, C, D, E, and F. A copy of the Phase I Report is attached in Attachment F. Historic

Sanborn maps provided within the report were reviewed to determine the following historic use

of Site E:

1887 Sanborn Map - The 1887 Sanborn map indicates Site E formerly consisted of multiple

20 or 25ft wide lots along South 3rd Street and South 4th Street that were developed with 3

story houses. The northwest corner of Site E was developed with a 9-story building used as

the kiln and filter house for the Havemeyer & Elder Sugar Refinery. The building contained

numerous coal fired boilers and two large smoke stacks.

1904 Sanborn Map - The 1904 Sanborn map indicates the sugar refinery operation

expanded to several of the lots along South 4th Street. The facility was now operated under

the name American Sugar Refinery. It consisted of a 7-story building at 29 to 35 South 4th

Street that housed 16 engines, a 2-story building at 38-40 South 3rd Street that was utilized

for coal storage, a 2 and 4-story building at 42-44 South 3rd Street that housed numerous

boilers, and a 10-story building at 317-323 Kent Avenue that consisted of 14 boilers, and was

utilized as the kiln and filter house. Several of the 3-story houses at 37, 39 and 41 South 4th




Phone 631.504.6000 Fax 631.924.2870

Street are labeled as pattern storage. A small lot at 325 Kent Avenue is developed with three

buildings labeled as a plating room, paints, and saw-dust house.

1918 Sanborn Map - The 1918 Sanborn map indicates the American Sugar Refining

Company of NY utilized nearly the entire footprint of Site E, with the exception of a 3-story

apartment building w/first floor store on the corner of South 4th Streetn and Kent Avenue

(329 Kent Avenue). Site E is shown as being developed with the following:

o Section G - Consists of two buildings and an open space area - 1) 317 - 323 Kent

Avenue - A 9-story building with a basement that was used as the kiln and filter

house, 2) 32-36 South 3rd Street - labeled as the old boiler house, and as vacant and

partly removed, and 3) 38-40 South 3rd Street - a coal yard.

o Section Q - Consists of three buildings 1) 46-54 South 3rth Street - A 68ft high

building consisting of six large syrup tanks, 2) 42-44 South 3rd Street - a 2-story

building used for storage of bone black and 3) 49 South 4th Street - a 1-story building

labeled as a filling house.

o Section P - Developed with two adjacent seven story buildings. The building at 37-49

South 4th Street was labeled as the filter house, and the building at 29-35 South 4th

Street was labeled as the filler house.

o Section T - Developed with a former 3-story residential building labeled as the

pattern shop, and an open lot likely used for parking.

1935 Sanborn Map - The 1935 Sanborn map appears to label most buildings as the same as

those depicted on the 1918 Sanborn map, but most buildings are labeled as vacant.

1947, 1950 and 1965 Sanborn Maps - The 1947, 1950 and 1965 Sanborn maps depict the

majority of Site E as being undeveloped with the exception of two 3-story buildings on the

corner of South 4th Street and Kent Avenue (327 and 329 Kent Avenue).

1977-2007 Sanborn Maps - All Sanborn maps from 1977 to 2007 depict the entire footprint

of Site E as undeveloped.




Phone 631.504.6000 Fax 631.924.2870

The Emteque LLC Phase I Environmental Site Assessment Report identified multiple recognized

environmental conditions in connection with Lot 1. However, only one is believed to be

associated with Site E:

Historic / Urban fill (Site A) - Emteque LLC stated previous environmental investigations

have identified soil and groundwater contamination attributed to previous filling of the

property prior to development. Emteque LLC recommended additional sampling of soil and

groundwater to fully characterize the site to aid in the development and implementation both

engineering and institutional controls. Additionally, further characterization of the site soil

will be required prior to its off-site disposal.

2.2 Previous Investigations

EBC was provided digital copies of previous investigations performed at the Site. A summary of

each is provided below.

2.2.1 Phase III Environmental Site Assessment (Nova, 2004)

A Phase III Environmental Site Assessment was performed at Site E, as well as the remainder of

the Domino Sugar property (Sites A, B, C, D and F) by Nova Consulting & Engineering, LLC

(Nova) in June of 2004. The Phase III Environmental Site Assessment included the installation

of five evenly spaced soil borings across Site E. From each of the five soil borings, Nova

retained soil samples in 4 ft intervals from 0-4 feet below grade to 16 to 20 feet below grade or

refusal.

Each of the soil samples were submitted for laboratory analysis of VOCs, and SVOCs, and the

soil samples retained from soil borings B-4 and B-5 were also submitted for laboratory analysis

of RCRA metals. The laboratory results are compared to NYSDEC Unrestricted Use Soil

Cleanup Objectives (UUSCOs) and Restricted Residential Use Soil Cleanup Objectives

(RRSCOs) as presented in 6NYCRR Part 375-6.8 and CP51 on Tables 2a, 3a, and 5. Figure 6

shows the location and posts the values for soil that exceeds UUSCOs and RRSCOs. A copy of

the report is included in Attachment G.




Phone 631.504.6000 Fax 631.924.2870

2.2.2 Subsurface (Phase II) Investigation (AKRF, 2009)

A Subsurface (Phase II) Investigation was performed across Lot 1, and Block 2428, Lot 1 by

AKRF, Inc. (AKRF) in February of 2009. The Subsurface (Phase II) Investigation was

conducted to determine whether current or former on- or off-site activities have adversely

affected the subject property. AKRF’s Subsurface (Phase II) Investigation included the following

work on Site E:

Installation of two soil borings (SB-12 and SB-13) to collect a shallow soil sample (0-2ft)

and a deep soil sample from both soil borings (16-18ft and 27-29ft) for laboratory

analysis.

Conversion of soil boring SB-13 into a monitoring well and the collection of one

groundwater sample from the monitoring well.

Each of the four soil samples were submitted for laboratory analysis of VOCs, SVOCs,

pesticides/PCBs and metals. The laboratory results are compared to 6NYCRR Part 375-6.8 and

CP51 as presented in Tables 2a, 3a, 4, and 5. Figure 6 shows the location and posts the values for

soil that exceeds UUSCOs and RRSCOs.

Groundwater sample SB-13 was submitted for laboratory analysis of VOCs, SVOCs,

pesticides/PCBs, total metals and dissolved metals. The laboratory results are summarized on

Tables 6 through 10, and compared to New York State 6NYCRR Part 703.5 Class GA

Groundwater Quality Standards (GQS). Figure 7 shows the location and posts the values for

groundwater that exceed GQS. A copy of the report is included in Attachment H.

2.3 Site Inspection

Mr. Dominick Mosca of EBC performed a site inspection on Thursday, April 2, 2014, beginning

at approximately 7:00 am. The reconnaissance included a visual inspection of Site E, roadways,

and sidewalks surrounding Site E, and the exterior of adjacent properties. At the time of the

inspection, Site E was undeveloped, but was utilized as a bicycle park. The Site was uncapped,

and the exposed soil cover has shaped to construct roadways/pathways for bicycles. An 8-foot

high chain link fence was constructed around the perimeter of the Site and gates on South 3rd

Street, South 4th Street and Kent Avenue provided access. A small trailer was set up near the

gate on Kent Avenue, which was utilized for bicycle rentals and access to the bicycle park.




Phone 631.504.6000 Fax 631.924.2870

No storm drains, aboveground storage tanks, or any hazardous chemicals were observed in Site E

during the Site inspection.

2.4 Areas of Concern

The AOCs identified for Site E include:

1. Historic fill layer is present at the Site from grade to depths as great as 15 feet below

grade;

2. The past use of a portion of Site E as a plating facility; and

3. Areas of the Site that were formerly developed with industrial buildings that house large

scale electric generators and boilers for the sugar refinery.




Phone 631.504.6000 Fax 631.924.2870

3.0 PROJECT MANAGEMENT

3.1 Project Organization

The Qualified Environmental Profession (QEP) responsible for preparation of this RIR is Kevin

Brussee.

3.2 Health and Safety

All work described in this RIR was performed in full compliance with applicable laws and

regulations, including Site and OSHA worker safety requirements and HAZWOPER

requirements.

3.3 Materials Management

All material encountered during the RI was managed in accordance with applicable laws and

regulations.




Phone 631.504.6000 Fax 631.924.2870

4.0 REMEDIAL INVESTIGATION ACTIVITIES

EBC performed the following scope of work within Site E in April of 2014:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,

buildings, etc.);

2. Installed six soil borings within Site E, and collected twelve soil samples for chemical

analysis from the soil borings to evaluate soil quality; and

3. Installed two groundwater monitoring wells within Site E and collected two groundwater

samples from the two monitoring wells, and collected one groundwater sample from an

existing geotechnical monitoring well to evaluate groundwater quality; and

4. Installed five soil vapor probes across the Site and collected five soil vapor samples for

chemical analysis.

4.1 Geophysical Investigation

A geophysical investigation was not performed as a part of this assessment.

4.2 Borings and Monitoring Wells

Drilling and Soil Logging

On April 2, 2014, and April 8, 2014, six soil borings (SB1, SB2 and SB4 through SB7) were

performed in the approximate locations shown on Figure 5. Refusal was repeatedly encountered

at very shallow depths at soil boring SB3, and was therefore not completed. The location of the

six completed soil borings were chosen to gain representative soil quality information across Site

E. For each of the six soil borings, soil samples were collected continuously from grade to

refusal using a five-foot steel macro-core sampler with acetate liners and Geoprobe direct-push

equipment. Soil recovered from each of the soil borings was field screened for the presence of

VOCs with a photo-ionization detector (PID) and visually inspected for evidence of

contamination. No PID readings above background concentrations were obtained from any of the

soil borings.

One soil sample was retained from each boring representing the interval 0 to 2 feet below grade

and one soil sample was retained from each of the soil borings from the 2ft interval immediately

above the refusal depth. Therefore, soil samples were retained from the interval 15 to 17 feet




Phone 631.504.6000 Fax 631.924.2870

below grade for soil borings SB4, SB6, and SB7, the interval 14 to 16 feet below grade for soil

boring SB5, and 29 to 31 feet below grade for soil borings SB1 and SB2.

Soil boring details are provided in Table 1. Boring logs were prepared by a Qualified

Environmental Professional and are attached in Attachment A.

Groundwater Monitoring Well Construction

A temporary 1-inch diameter PVC monitoring well consisting of 10 feet of 0.010 slot screen was

installed at two locations (E-MW1 and E-MW3), set to intersect the water table. Monitoring well

E-MW1 was installed on the western end of the Site and required installation at a depth of

approximately 40 feet below grade due the higher elevation of the Site on the western end.

Monitoring well E-MW3 was installed on the eastern end of the Site at a depth of approximately

30 feet below grade due to the 13 ft difference elevation between the western and eastern ends of

the Site. Monitoring well E-MW2 was an existing 2-inch diameter monitoring well installed by

the geotechnical company at a depth of approximately 40 feet below grade. Monitoring well

sampling details are provided in Table 1. Monitoring well locations are shown in Figure 5.

Survey

Soil borings and wells were located to the nearest 0.10 foot with respect to two or more

permanent site features.

Water Level Measurement

Approximate groundwater level measurements were collected using a Solinst oil/water interface

meter to ensure the surface of the water table was within the screened section of the monitoring

well. No free product was observed within the three monitoring wells. Water level data is

included in Table 1.

4.3 Sample Collection and Chemical Analysis

Sampling performed as part of the field investigation was conducted for all Areas of Concern

and also considered other means for bias of sampling based on professional judgment, area

history, discolored soil, stressed vegetation, drainage patterns, field instrument measurements,

odor, or other field indicators. All media including soil and soil vapor have been sampled and

evaluated in the RIR. Discrete (grab) samples have been used for final delineation of the nature




Phone 631.504.6000 Fax 631.924.2870

and extent of contamination and to determine the impact of contaminants on public health and

the environment. The sampling performed and presented in this RIR provides sufficient basis for

evaluation of remedial action alternatives, establishment of a qualitative human health exposure

assessment, and selection of a final remedy.

Soil Sampling

Twelve soil samples were collected for chemical analysis during this RI. Data on soil sample

collection for chemical analyses, including dates of collection and sample depths, is reported in

Tables 2, 3, 4 and 5. Figure 5 shows the location of samples collected during this RI, and the soil

boring locations of the 2009 AKRF Phase II. Laboratories and analytical methods for soil

samples collected during the 2014 EBC RI are shown below.

The twelve soil samples were collected in pre-cleaned, laboratory supplied glassware, stored in a

cooler with ice and submitted for analysis to Phoenix Environmental Laboratories (Phoenix) of

587 East Middle Turnpike, Manchester, CT 06040, a New York State ELAP certified

environmental laboratory (ELAP Certification No. 11301). All six soil samples retained from the

interval 0 to 2 feet below grade were analyzed for the presence of volatile organic compounds

(VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method

8270, pesticides/PCBs by EPA Methods 8081/8082 and target analyte list (TAL) metals. IEach

of the six soil samples retained from the deeper interval were analyzed for VOCs by EPA

Method 8260, SVOCs by EPA Method 8270, and TAL metals. Since pesticides and PCBs were

detected above UUSCOs within the 0-2ft soil sample retained from soil boring SB6, the deeper

soil sample from the same soil boring was also analyzed for pesticides/PCBs by EPA Methods

8081/8082.

Groundwater Sampling

Three groundwater samples were collected from Site E. Two of the groundwater samples (MW1

and MW3) were collected from one-inch diameter PVC monitoring wells installed 5-feet below

the water table interface by EBC. The third groundwater sample (MW2) was collected from a 2-

inch diameter monitoring well installed by the geotechnical company. The three groundwater

samples were collected utilizing dedicated polyethylene tubing and a stainless steel check valve.

Groundwater samples were collected in pre-cleaned, laboratory supplied glassware, stored in a




Phone 631.504.6000 Fax 631.924.2870

cooler with ice and submitted to Phoenix for analysis of VOCs by EPA Method 8260, SVOCs by

EPA Method 8270, and both total and dissolved TAL metals. One of the groundwater samples

(MW3) was also analyzed for pesticides/PCBs by EPA Methods 8081/8082. Groundwater

sample collection data is reported in Tables 6 through 10. Sampling logs with information on

purging and sampling of groundwater monitoring wells is included in Attachment B. Figure 5

shows the location of each of the three monitoring wells sampled by EBC and the location in

which groundwater was sampled during the 2008 AKRF Phase II. Laboratories and analytical

methods for groundwater samples collected during the 2014 EBC RI are shown below.

Soil Vapor Sampling

Five soil vapor probes were installed within Site E and five soil vapor samples were collected for

chemical analysis during this RI. Soil vapor sampling locations are shown in Figure 5. Soil vapor

sample collection data is reported in Table 11. Soil vapor sampling logs are included in

Attachment C. Methodologies used for soil vapor assessment conform to the NYS DOH Final

Guidance on Soil Vapor Intrusion, October 2006.

The five soil vapor implants were installed using Geoprobe™ equipment and tooling. The vapor

implants that were installed were the Geoprobe™ Model AT86 series, which are constructed of a

6-inch length of double woven stainless steel wire. The implants were installed to at depths

ranging from 15 to 25 feet below grade. Each implant was attached to ¼ inch polyethylene

tubing which extended approximately 18 inches beyond that needed to reach the surface. The

tubing was capped with a ¼ inch plastic end to prevent the infiltration of foreign particles into

the tube. Coarse sand was placed around the vapor implant to a height of approximately 1 foot

above the bottom of the implant. The remainder of the borehole was sealed with a bentonite

slurry to the surface.

Soil vapor sampling for the five soil vapor implants installed on April 2 and April 8, 2014, was

conducted on April 9 and April 17, 2014. Prior to sampling, each sampling location was tested to

ensure a proper surface seal had been obtained. In accordance with NYSDOH guidance

(NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February

2005), a tracer gas (helium) was used as a quality assurance/quality control device to verify the

integrity of the sampling point seal prior to collecting the samples. Prior to testing and collecting




Phone 631.504.6000 Fax 631.924.2870

samples, the surface immediately surrounding the polyethylene tubing of the vapor implant was

sealed using a 1 foot ft by 1 ft square sheet of 2 mil HDPE plastic firmly adhered to a wetted

layer of granular bentonite. The seal was then tested by enriching the air space above the seal

with a tracer gas (helium) while continuously monitoring air drawn from the implant with a

helium detector (Dielectric Model MGD-2002, Multi-Gas Detector) for a minimum of 15

minutes. The tracer gas test procedure was employed at all five soil vapor sampling locations. No

surface seal leaks were observed at any of the locations.

Following verification that the surface seal was tight, one to three volumes (i.e., the volume of

the sample probe and tube) of air was purged from the implant using a calibrated vacuum pump.

After purging, a 6-liter Summa® canister, fitted with a 2-hour flow regulator, was attached to the

surface tube of each of the five soil vapor implants. Prior to initiating sample collection, sample

identification, canister number, date and start time were recorded on tags attached to each

canister and in a bound field note book. Sampling then proceeded by fully opening the flow

control valve on each canister in turn. Immediately after opening the flow control valve on a

canister, the initial vacuum (inches of mercury) was recorded in the field book and on the sample

tag. When the vacuum level in the canister was between 5 and 8 inches of mercury (approx 2

hours), the flow controller valve was closed, and the final vacuum recorded in the field notebook

and on the sample tag.

The soil gas sample identification, date, start time, start vacuum, end time and end vacuum were

recorded on tags attached to each canister and on a sample log sheet (Attachment C). Samples

were submitted to Phoenix for laboratory analysis of VOCs EPA Method TO-15.

Chemical Analysis

Chemical analytical work presented in this RIR has been performed in the following manner:

Factor Description

Quality Assurance Officer The chemical analytical quality assurance is directed by Phoenix

Environmental Laboratories

Chemical Analytical

Laboratory

Chemical analytical laboratory(s) used in the RI is NYS ELAP

certified and was Phoenix Environmental Laboratories




Phone 631.504.6000 Fax 631.924.2870

Chemical Analytical

Methods

Soil and groundwater analytical methods:

TAL Metals by EPA Method 6010C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Soil vapor analytical methods:

VOCs by TO-15 VOC parameters.

Results of Chemical Analyses

Laboratory data for soil, groundwater, and soil vapor are summarized in Tables 2 through 11.

Laboratory data deliverables for all samples evaluated in this RIR are provided in digital form in

Attachment D.




Phone 631.504.6000 Fax 631.924.2870

5.0 ENVIRONMENTAL EVALUATION

5.1 Geological and Hydrogeological Conditions

Stratigraphy

The stratigraphy of Site E, from the surface down, consists of a layer of historic fill material that

varies from 2 to approximately 15ft below grade, underlain by a brown silty sand.

5.2 Soil Chemistry

Data collected during the RI performed in 2014 when combined with the data collected during

the 2004 Nova Phase III, and 2008 AKRF Phase II is sufficient to delineate the vertical and

horizontal distribution of contaminants in soil/fill at the Site. A summary table of data for

chemical analyses performed on soil samples is included in Tables 2a, 2b, 3a, 3b, 4 and 5.

Laboratory results from the 2014 EBC RI, 2004 Nova Phase III, and 2008 AKRF Phase II were

compared to NYSDEC Part 375 Table 375-6.8(a) and (b) Soil Cleanup Objectives (SCOs) for

Unrestricted Use and Restricted Residential Use. A copy of each of the laboratory reports for the

2014 EBC RI soil samples is provided in Attachment D. Figure 6 shows the location and posts

the values for soil/fill from both the 2014 EBC RI and 2008 AKRF Phase II that exceeds

UUSCOs and RRSCOs.

Soil/fill samples collected during the 2014 EBC RI, 2004 Nova Phase III, and 2008 AKRF Phase

II showed no VOCs above Unrestricted Use SCOs with the exception of acetone (68 micrograms

per kilogram [µg/Kg]). Naphthalene (maximum [max] of 430 µg/Kg) was detected in multiple

soil samples below Unrestricted Use SCOs. Eight SVOCs including benz(a)anthracene (max of

23,000 μg/Kg), benzo(a)pyrene (max of 20,000 μg/Kg), benzo(b)fluoranthene (max of 20,000

μg/Kg), benzo(k)fluoranthene (max of 20,000 μg/Kg), chrysene (max of 19,000 μg/Kg),

dibenz(a,h)anthracene (max of 8,600 μg/Kg), indeno(1,2,3-cd)pyrene (max of 18,000) and

phenanthrene (max of 160,000 μg/Kg) were detected above Unrestricted Use and Restricted

Residential Use SCOs within soil samples retained from the historic fill layer. Several metals

including arsenic (137 mg/Kg), cadmium (8.19 mg/kg), copper (max of 185 mg/Kg), lead (max

of 446 mg/Kg), mercury (max of 0.55 mg/Kg), nickel (39.6 mg/Kg), and zinc (max of 1,480

mg/Kg) were detected above Unrestricted Use SCOs. Of these metals, arsenic, cadmium and lead

also exceeded Restricted Residential Use SCOs within soil samples collected from the historic




Phone 631.504.6000 Fax 631.924.2870

fill layer. PCB-1254 (210 µg/Kg) was detected within one shallow soil sample at a concentration

above Unrestricted Use SCOs and within one shallow soil sample and PCB-1260 (maximum of

25 µg/Kg) was detected within two shallow soil samples at a concentration below Unrestricted

Use SCOs. The pesticides 4,4'-DDD (max of 15 µg/Kg) and 4,4'-DDT (max of 13 µg/Kg) were

detected within two shallow soil samples at a concentration above Unrestricted Use SCOs.

Neither the pesticides nor PCBs were detected within any of the deeper soil samples retained

from the same soil boring locations. Overall, the findings were consistent with observations for

historical fill sites in areas throughout NYC.

5.3 Groundwater Chemistry

Data collected during the RI performed in 2014 when combined with the data collected during

the 2008 AKRF Phase II is sufficient to delineate the distribution of contaminants in

groundwater at the Site. A summary table of data for chemical analyses performed on

groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II is included in

Tables 6 through 10. Figure 7 shows the location and posts the values for groundwater that

exceed the New York State 6NYCRR Part 703.5 Class GA Groundwater Quality Standards

(GQS) for the 2014 EBC RI and 2008 AKRF Phase II. A copy of the laboratory report for the

2014 RI groundwater samples is provided in Attachment D.

Groundwater samples collected during the 2014 EBC RI and 2008 AKRF Phase II showed no

detectable concentrations of pesticides or PCBs. The chlorinated VOCs cis-1,2-dichlorothene

(maximum of 5.56 µg/L), tetrachloroethene (maximum of 5.7 µg/L), and trichloroethene

(maximum of 27 µg/L) were detected within the groundwater samples collected by AKRF in

2008 and EBC in 2014 above GQS. The following VOCs were detected in one or more of the

groundwater samples at concentrations below GQS: 1,1-dichloroethene (1.7 µg/L), acetone

(maximum of 2.7 µg/L), carbon disulfide (0.90 µg/L), chloroform (1.5 µg/L), and methylene

chloride (0.38 µg/L). SVOCs detected above GQS included benzo(a)anthracene (max of 0.49

µg/L), benzo(b)fluoranthene (max of 0.48 µg/L), benzo(k)fluoranthene (0.08 µg/L), bis(2-

ethylhexyl)phthalate (max of 42 µg/L), chrysene (max. of 0.49 µg/L), and indeno(1,2,3-

cd)pyrene (3.7 µg/L) in one or more of the three groundwater samples collected by EBC in 2014

and the groundwater sample collected by AKRF in 2008. Dissolved metals present in

groundwater at levels above GQS included iron, lead, magnesium, manganese, selenium and




Phone 631.504.6000 Fax 631.924.2870

sodium. The presence of some of these metals in groundwater, specifically those that are

common salinity indicators, can be attributed to the proximity to the East River and the intrusion

of road salting.

5.4 Soil Vapor Chemistry

Data collected during the 2014 RI is sufficient to delineate the distribution of contaminants in

soil vapor at the Site. A summary table of data for chemical analyses performed on soil vapor

samples is included in Table 11. Soil vapor analytical results were compared to NYSDOH Final

Guidance on Soil Vapor Intrusion (October 2006) Matrix 1 and 2 guidance values. Figure 8

shows the location and posts the values for soil vapor samples with detected concentrations of

NYSDOH Matrix 1 and 2 compounds.

Soil vapor samples collected during the 2014 EBC RI indicated petroleum related VOCs and

chlorinated VOCs were present at low concentrations. Petroleum-related VOCs (BTEX) were

detected at a maximum concentration of 141.43 μg/m3. The highest reported concentration was

for acetone (maximum of 7693 μg/m3). Trichloroethylene (TCE) was detected in three of the five

soil vapor samples at a concentration ranging from 241 to 61.2 μg/m3. The New York State

Department of Health (NYSDOH) Final Guidance on Soil Vapor Intrusion (October 2006) notes

mitigation is the recommended action for a TCE concentrations above 250 μg/m3 in soil gas.

Tetrachloroethylene (PCE) was detected in all five soil vapor samples, and ranged in

concentration from 2.03 to 28.3 μg/m3. Carbon tetrachloride was detected within three of the five

soil vapor samples at a maximum concentration of 0.566 μg/m3, and 1,1,1-trichloethylene (TCA)

was detected in three of the five soil vapor samples at a maximum concentration of 3.54 μg/m3.

The PCE, carbon tetrachloride and TCA concentrations are below the monitoring level ranges

established within the NYSDOH Final Guidance on Soil Vapor Intrusion.

5.5 Prior Activity

Based on an evaluation of the data and information from the RIR, disposal of significant amounts

of hazardous waste is not suspected for Site E.

5.6 Impediments to Remedial Action

There are no known impediments to remedial action at this property.

TABLES

Table 1Former Domino Sugar Facility

Site E317-329 Kent Avenue, Brooklyn, NY

Soil Boring / Well Information

SB1 4/8/2014 40 2 Geoprobe - -SB2 4/2/2014 31 2 Geoprobe - -SB4 4/2/2014 20 2 Geoprobe - -SB5 4/2/2014 10 2 Geoprobe - -SB6 4/8/2014 20 2 Geoprobe - -SB7 4/8/2014 20 2 Geoprobe - -

MW1 4/8/2014 40 1 PVC 10.00 34.89MW2 Existing 40 1 PVC 10.00 30.43MW3 5/7/2014 30 1 PVC 10.00 22.47

SAMPLE ID Total Depth (ft) Diameter (in)DTW (ft)

Screen Length (ft)

DateConstruction

Materials

TABLE 2aSite E

Former Domino Sugar SiteBrooklyn, New York

Soil Analytical ResultsVolatile Organic Compounds

1,1,1,2-Tetrachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,1,1-Trichloroethane 680 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.82 U 0.78 U 0.83 U 0.87 U

1,1,2,2-Tetrachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.1 U 1.2 U 1.2 U

1,1,2-Trichloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.97 U 0.93 U 0.98 U 1 U

1,1-Dichloroethane 270 26,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.73 U 0.7 U 0.73 U 0.77 U

1,1-Dichloroethene 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.88 U 0.85 U 0.89 U 0.94 U

1,1-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2,3-Trichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2,3-Trichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2,4-Trichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2,4-Trimethylbenzene 3,600 52000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2,4,5-Trimethylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2-Dibromoethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2-Dichlorobenzene 1,100 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

1,2-Dichloroethane 20 3,100 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.2 U 1.2 U 1.3 U

1,2-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1 U 1.1 U 1.2 U

1,3,5-Trimethylbenzene 8,400 52000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -


1,3-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -


2,2-Dichloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

2-Chlorotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

2-Hexanone (Methyl Butyl Ketone) - - - - - - - - - - - - - - - - - - - - 2.9 U 2.8 U 3 U 3.1 U

4-Chlorotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Acetone 50 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2.6 U 2.5 U 2.6 U 2.8 U

Benzene 60 4,800 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U

Bromobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Bromochloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Bromodichloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.73 U 0.7 U 0.73 U 0.77 U

Bromoform BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.9 U 1.9 U 2 U 2.1 U

Bromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.7 U 1.6 U 1.7 U 1.8 U

Carbon Disulfide - - - - - - - - - - - - - - - - - - - - 0.59 U 0.57 U 0.6 U 0.63 U

Carbon tetrachloride 760 2,400 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U

Chlorobenzene 1,100 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.98 U 0.94 U 0.99 U 1 U

Chlorodibromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Chlorodifluoromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Chloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.4 U 1.4 U 1.4 U 1.5 U

Chloroform 370 49,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.59 U 0.57 U 0.6 U 0.63 U

Chloromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1.1 U 1.1 U 1.2 U

cis-1,2-Dichloroethene 250 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1 U 0.99 U 1 U 1.1 U

cis-1,3-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.69 U 0.67 U 0.7 U 0.74 U

Dibromochloromethane - - - - - - - - - - - - - - - - - - - - 1.2 U 1.1 U 1.2 U 1.3 U

Dibromochloropropane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Dibromomethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Dichlorodifluoromethane 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Ethylbenzene 1,000 41,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.79 U 0.76 U 0.8 U 0.84 U

Freon 113 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Hexachlorobutadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Isopropylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

m&p-Xylenes 260 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Methyl Ethyl Ketone (2-Butanone) 120 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3.8 U 3.6 U 3.8 U 4 U

Methyl Isobutyl Ketone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 15 U 3.3 U 8 U 16 U

Methylene chloride 50 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 15 U 3.3 U 8 U 16 U

Napthalene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL 18 BDL BDL BDL BDL BDL 34 BDL 65 74 BDL 21 BDL - - - -

n-Butylbenzene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

n-Propylbenzene 3,900 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

o-Xylene 260 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

p-Diethylbenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

p-Ethyltoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

p-Isopropyltoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

sec-Butylbenzene 11,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Styrene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.4 U 1.4 U 1.5 U 1.5 U

tert-ButylMethylEther BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

tert-Butylbenzene 5,900 100000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Tetrachloroethene 1,300 19,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.83 U 0.79 U 0.84 U 0.88 U

Toluene 700 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.66 U 0.63 U 0.67 U 0.7 U

Total Xylenes - - - - - - - - - - - - - - - - - - - - 2.7 U 2.6 U 2.8 U 2.9 U

trans-1,2-Dichloroethene 190 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1 U 1.1 U 1.1 U

trans-1,3-Dichloropropene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.2 U 1.1 U 1.2 U 1.3 U

Trichloroethene 470 21,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.1 U 1.1 U 1.1 U 1.2 U

Trichlorofluoromethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Vinyl Chloride 20 900 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.5 U 1.4 U 1.5 U 1.5 U

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

ND - Not-detected

BDL - Delow Detection Limit

Dash - Not Analyzed

J - The value is estimated. This flag is used: a) on form 1 when the compound is reported above the MDL, but below the PQL, and b) on the Tentatively Identified Compounds (TIC) form for all compounds identified.

S - This compound is a solvent that is used in the laboratory. Laboratory contamination is suspected if concentration is less than five times the reporting level.

N - The concentration is based on the response fo the nearest internal. This flag is used on the TIC form for all compounds identified.

U - The compound was anlayzed for but not detected at or above the MDL.

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value

Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

µg/Kg

NOVA Phase III

µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg µg/Kg

6/23/2004 6/23/2004 11/7/2008

(1-3')

11/7/2008

(27-29')

AKRF PhaseII

AKRF PhaseII

6/23/2004

(16-18')

AKRF PhaseII

AKRF PhaseII

11/7/20086/23/2004 6/23/2004 11/7/2008

(12-16')(8-12')

SB-13

(1-3')

NOVA Phase III

NOVA Phase III

B-5

(0-4') (4-8')

NOVA Phase III

NOVA Phase III

SB-12

µg/Kg

6/23/2004 6/23/2004

µg/Kg

6/23/2004

µg/Kg µg/Kgµg/Kg µg/Kg

6/23/2004 6/23/2004 6/23/2004

NOVA Phase III

NOVA Phase III

(4-8')

NOVA Phase III

NOVA Phase III

NOVA Phase III

(0-4')(16-20')

B-3

(12-16')

NOVA Phase III

(8-12')

B-4

NOVA Phase III

(8-12')(0-4')

B-1

6/23/2004

µg/Kg

6/23/2004 6/23/20046/23/2004 6/23/2004 6/23/2004

µg/Kg µg/Kg µg/Kg

COMPOUNDNYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives

NYDEC Part 375.6 Restricted Residential

Soil Cleanup Objectives*

(4-8')(12-16')

µg/Kg

NOVA Phase III

NOVA Phase III

(8-12')(4-8')(0-4')

µg/Kg

(8-12') (12-16')(0-4')

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

B-2

(4-8')

Results

6/23/2004


6/23/2004 6/23/2004

ResultsResultsResultsResultsResultsResults

Previous Investigations

ResultsResultsResults ResultsResultsResultsResultsResults ResultsResultsResultsResultsResultsResults ResultsResultsResults

TABLE 2bSite E


Soil Analytical ResultsVolatile Organic Compounds

Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL Results RL

1,1,1,2-Tetrachloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1,1-Trichloroethane 680 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1,2,2-Tetrachloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1,2-Trichloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1-Dichloroethane 270 26,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1-Dichloroethene 330 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,1-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2,3-Trichlorobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2,3-Trichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2,4-Trichlorobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2,4-Trimethylbenzene 3,600 52000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2,4,5-Trimethylbenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2-Dibromoethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2-Dichlorobenzene 1,100 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2-Dichloroethane 20 3,100 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,2-Dichloropropane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

1,3,5-Trimethylbenzene 8,400 52000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12





2-Chlorotoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

2-Hexanone (Methyl Butyl Ketone) < 47 47 < 29 29 < 41 41 < 40 40 < 40 40 < 34 34 < 49 49 < 45 45 < 27 27 < 36 36 < 36 36 < 61 61

2-Isorpropyltoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

4-Chlorotoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

4-Methyl-2-pentanone < 47 47 < 29 29 < 41 41 < 40 40 < 40 40 < 34 34 < 49 49 < 45 45 < 27 27 < 36 36 < 36 36 < 61 61

Acetone 50 100,000 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50 12 50 49 50 68 54 < 50 50 < 50 50 < 50 50

Acrylonitrile < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24

Benzene 60 4,800 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Bromobenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

Bromochloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Bromodichloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Bromoform < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Bromomethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Carbon Disulfide < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Carbon tetrachloride 760 2,400 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Chlorobenzene 1,100 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Chloroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Chloroform 370 49,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Chloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

cis-1,2-Dichloroethene 250 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

cis-1,3-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Dibromochloromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Dibromomethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Dichlorodifluoromethane 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Ethylbenzene 1,000 41,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Hexachlorobutadiene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

Isopropylbenzene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

m&p-Xylenes 260 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Methyl Ethyl Ketone (2-Butanone) 120 100,000 < 56 56 < 34 34 < 49 49 < 49 49 < 48 48 < 41 41 < 59 59 < 54 54 < 32 32 < 44 44 < 43 43 < 73 73

Methyl Isobutyl Ketone < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24

Methylene chloride 50 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Napthalene 12,000 100,000 < 9.3 9.3 < 5.7 5.7 430 310 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

n-Butylbenzene 12,000 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

n-Propylbenzene 3,900 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

o-Xylene 260 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

p-Isopropyltoluene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

sec-Butylbenzene 11,000 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

Styrene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

tert-Butylbenzene 5,900 100000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 280 280 < 280 280 < 7.3 7.3 < 7.2 7.2 < 12 12

Tetrachloroethene 1,300 19,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Tetrahydrofuran < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 18 18 < 11 11 < 15 15 < 14 14 < 24 24

Toluene 700 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

trans-1,2-Dichloroethene 190 100,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

trans-1,3-Dichloropropene < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

trans-1,4-dichloro-2-butene < 19 19 < 11 11 < 16 16 < 16 16 < 16 16 < 14 14 < 20 20 < 560 560 < 560 560 < 15 15 < 14 14 < 24 24

Trichloroethene 470 21,000 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Trichlorofluoromethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Trichlorotrifluoroethane < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12

Vinyl Chloride 20 900 < 9.3 9.3 < 5.7 5.7 < 8.2 8.2 < 8.1 8.1 < 8.0 8 < 6.9 6.9 < 9.8 9.8 < 8.9 8.9 < 5.4 5.4 < 7.3 7.3 < 7.2 7.2 < 12 12


ND - Not-detected




EBC RI EBC RI EBC RI

µg/Kg

4/8/2014

µg/Kg µg/Kg

4/2/2014 4/8/2014

EBC RI EBC RI

4/2/2014

EBC RI

4/2/2014 4/8/20144/2/2014 4/2/2014

µg/Kg

4/8/2014

(0-2')

µg/Kg µg/Kg

4/8/2014

EBC RIEBC RIEBC RI

4/8/2014

µg/Kg

EBC RICOMPOUND

NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives



4/8/2014

EBC RI

µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg

EBC RI

SB7

(0-2')

2014 Remedial Investigation

SB5 SB6

(12-14') (0-2') (15-17') (15-17')

SB4

(0-2')(29-31')(0-2')

SB1 SB2

(29-31') (0-2') (15-17')

TABLE 3aSite E


Soil Analytical ResultsSemi-Volatile Organic Compounds

1,2,4-Trichorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 59 U 620 U 65 U

1,2-Dichlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600 U 58 U 610 U 64 U

1,2-Diphenylhydrazine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -



2,2'-Oxybis (1-chloropropane) - - - - - - - - - - - - - - - - - - - - 710 U 69 U 720 U 76 U

2,4,5-Trichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 550 U 53 U 560 U 59 U

2,4,6-Trichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 58 U 610 U 65 U

2,4-Dichlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U

2,4-Dimethylphenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 490 U 47 U 490 U 52 U

2,4-Dinitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 4,100 U * 390 U * 4,100 U * 430 U *

2,4-Dinitrotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 570 U 55 U 580 U 61 U

2,6-Dinitrotoluene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 500 U 48 U 500 U 53 U

2-Chloronaphthalene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 640 U 62 U 650 U 68 U

2-Chlorophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 670 U 65 U 680 U 72 U

2-Methylnaphthalene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 710 1,500 1,400 BDL BDL BDL BDL 690 U 66 U 1300 J 73 U

2-Methylphenol (o-cresol) 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 540 U 52 U 550 U 58 U

2-Nitroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 590 U 57 U 600 U 63 U

2-Nitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 520 U 51 U 530 U 56 U

3&4-Methylphenol (p-cresol) BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

3,3'-Dichlorobenzidine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U


4,6-Dinitro-2-methylphenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 270 U 26 U 270 U 29 U

4-Bromophenyl phenyl ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 550 U 53 U 560 U 59 U

4-Chloro-3-methylphenol - - - - - - - - - - - - - - - - - - - - 540 U 52 U 550 U 58 U

4-Chloroaniline BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 490 U 47 U 490 U 52 U

4-Chlorophenyl phenyl ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 630 U 61 U 640 U 68 U

4-Methylphenol - - - - - - - - - - - - - - - - - - - - 720 U 69 U 730 U 76 U


4-Nitrophenol BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 670 U 65 U 680 U 72 U

Acenaphthene 20,000 100,000 BDL BDL BDL BDL BDL 330 BDL BDL BDL BDL BDL BDL BDL 2,500 2,900 2,400 BDL BDL BDL BDL 1,800 J 63 U 3,200 69 U

Acenaphthylene 100,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 740 J 66 U 700 U 73 U

Anthracene 100,000 100,000 BDL BDL BDL BDL BDL 1,200 BDL BDL BDL BDL 37 BDL BDL 8,300 8,300 13,000 800 BDL 690 BDL 5,700 64 U 7,200 71 U

Benz(a)anthracene 1,000 1,000 BDL BDL BDL BDL BDL 3,600 BDL 510 400 BDL 120 BDL BDL 21,000 16,000 23,000 3,200 490 540 BDL 17,000 54 U 12,000 59 U

Benzo(a)pyrene 1,000 1,000 BDL BDL BDL BDL BDL 3,000 BDL 1,400 430 BDL 140 BDL BDL 17,000 13,000 20,000 3,300 460 390 BDL 15,000 40 U 9,900 45 U

Benzo(b)fluoranthene 1,000 1,000 BDL BDL BDL BDL BDL 3,100 BDL 1,200 380 BDL 120 BDL BDL 16,000 13,000 20,000 3,100 420 360 BDL 18,000 51 U 11,000 57 U

Benzo(ghi)perylene 100,000 100,000 BDL BDL BDL BDL BDL 1,400 BDL 1,200 BDL BDL 86 BDL BDL 6,900 7,400 7,700 1,800 BDL 270 BDL 16,000 41 U 8,000 45 U

Benzo(k)fluoranthene 800 3,900 BDL BDL BDL BDL BDL 3,100 BDL 660 380 BDL 120 BDL BDL 16,000 13,000 20,000 3,100 420 360 BDL 6,200 46 U 3,700 51 U

Benzyl alcohol - - - - - - - - - - - - - - - - - - - - 520 U 50 U 530 U 56 U

Benzyl butyl phthalate BDL BDL BDL BDL BDL BDL BDL 1,200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 100 J 620 U 65 U

Bis(2-chloroethoxy)methane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 620 U 60 U 630 U 66 U

Bis(2-chloroethyl)ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 850 U 82 U 860 U 90 U

Bis(2-chloroisopropyl)ether BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL - - - -

Bis(2-ethylhexyl)phthalate BDL BDL 200 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 57 590 U 200 J 600 U 200 J Carbazole BDL BDL BDL BDL BDL 370 BDL BDL BDL BDL BDL BDL BDL 2,200 3,100 3,500 320 BDL BDL BDL 2,700 J 58 U 3,400 64 U

Chrysene 1,000 3,900 BDL BDL BDL BDL BDL 3,200 BDL 1,400 420 BDL 110 BDL BDL 18,000 15,000 19,000 3,000 480 610 BDL 17,000 61 U 12,000 68 U

Dibenz(a,h)anthracene 330 330 BDL BDL BDL BDL BDL 480 BDL BDL BDL BDL BDL BDL BDL 2,600 1,900 2,500 520 BDL BDL BDL 4,500 36 U 4,100 40 U

Dibenzofuran 7,000 59000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2,200 3,300 4,500 BDL BDL BDL BDL 1,300 J 63 U 2,800 J 70 U

Diethyl phthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 700 U 67 U 710 U 74 U

Dimethylphthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 630 U 61 U 640 U 68 U

Di-n-butylphthalate BDL BDL 45 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 700 U 68 U 710 U 75 U

Di-n-octylphthalate BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 530 U 51 U 540 U 56 U

Fluoranthene 100,000 100,000 BDL BDL BDL BDL BDL 7,700 550 2,500 520 540 210 BDL 400 53,000 27,000 41,000 6,000 740 1,800 BDL 37,000 64 U 29,000 71 U

Fluorene 30,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3,300 4,200 6,100 BDL BDL BDL BDL 1,600 J 66 U 3,400 73 U

Hexachlorobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 720 U 69 U 730 U 77 U

Hexachlorobutadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 640 U 61 U 650 U 68 U

Hexachlorocyclopentadiene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 930 U 90 U 940 U 99 U

Hexachloroethane BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 580 U 56 U 590 U 62 U

Indeno(1,2,3-cd)pyrene 500 500 BDL BDL BDL BDL BDL 1,300 BDL 730 BDL BDL BDL BDL BDL 6,900 7,900 7,700 1,500 300 270 BDL 18,000 40 U 8,900 44 U

Isophorone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 690 U 66 U 700 U 73 U

Naphthalene 12,000 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1,100 2,700 1,800 BDL BDL BDL BDL 820 J 63 U 3,100 70 U

Nitrobenzene BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 730 U 70 U 740 U 78 U

N-Nitrosodi-n-propylamine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 740 U 72 U 750 U 80 U

N-Nitrosodiphenylamine BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 600 U 58 U 610 U 64 U

Pentachlorophenol 800 6,700 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 370 U 36 U 370 U 39 U

Phenanthrene 100,000 100,000 BDL BDL BDL BDL BDL 5,200 440 2,500 610 360 160 BDL BDL 53,000 37,000 35,000 3,100 330 3,100 BDL 29,000 63 U 30,000 70 U

Phenol 330 100,000 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 610 U 59 U 620 U 66 U

Pyrene 100,000 100,000 BDL BDL BDL BDL BDL 6,800 410 3,100 890 530 190 BDL 450 46,000 35,000 41,000 5,900 780 1,400 BDL 34,000 71 U 23,000 79 U


Dash- Not Analyzed


ND - Not-detected







Results Results

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

Results

NOVA Phase III

Results Results Results Results

6/23/2004

(4-8')COMPOUND NYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives**

B-1 B-2

6/23/2004 6/23/2004

Results

NYDEC Part 375.6 Restricted

Residential Soil Cleanup

Objectives**

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

NOVA Phase III

(1-3')

NOVA Phase III

NOVA Phase III

(0-4')(4-8') (8-12') (12-16')

B-5 SB-12

(16-18')

AKRF PhaseII

(8-12')

SB-13

(0-4') (4-8') (8-12') (12-16') (16-20') (0-4') (4-8') (12-16') (27-29')

B-3 B-4

(8-12') (12-16') (0-4') (1-3')(8-12') (0-4') (4-8')

AKRF PhaseII

6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004 6/23/2004

NOVA Phase III

NOVA Phase III

6/23/2004 6/23/2004 6/23/2004 6/23/2004

AKRF PhaseII

NOVA Phase III

AKRF PhaseII

NOVA Phase III

NOVA Phase III

6/23/2004 6/23/2004 6/23/2004 11/7/20086/23/2004 6/23/2004

NOVA Phase III

NOVA Phase III

11/7/2008

µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg

6/23/2004

µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg µg/Kg µg/Kg

Results Results Results ResultsResults Results Results Results Results

µg/Kg µg/Kg

11/7/2008


µg/Kg

ResultsResults Results Results Results

11/7/2008

Results Results

TABLE 3bSite E


Soil Analytical ResultsSemi-Volatile Organic Compounds


1,2,4,5-Tetrachlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

1,2,4-Trichorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

1,2-Dichlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

1,2-Diphenylhydrazine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260



2,4,5-Trichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2,4,6-Trichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2,4-Dichlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2,4-Dimethylphenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2,4-Dinitrophenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

2,4-Dinitrotoluene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2,6-Dinitrotoluene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2-Chloronaphthalene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2-Chlorophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2-Methylnaphthalene < 250 250 < 240 240 550 540 < 240 240 < 270 270 < 250 250 < 500 500 180 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

2-Methylphenol (o-cresol) 330 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260

2-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

2-Nitrophenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

3&4-Methylphenol (p-cresol) < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

3,3'-Dichlorobenzidine < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750

3-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

4,6-Dinitro-2-methylphenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

4-Bromophenyl phenyl ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

4-Chloro-3-methylphenol < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

4-Chloroaniline < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750

4-Chlorophenyl phenyl ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

4-Nitroaniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

4-Nitrophenol < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

Acenaphthene 20,000 100,000 < 250 250 < 240 240 1,100 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Acenaphthylene 100,000 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 820 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Acetophenone < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Aniline < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

Anthracene 100,000 100,000 < 250 250 < 240 240 2,800 540 < 240 240 < 270 270 < 250 250 240 500 1,200 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Benz(a)anthracene 1,000 1,000 160 250 < 240 240 4,800 540 < 240 240 220 270 < 250 250 1,400 500 9,300 290 1,800 1,300 < 250 250 950 500 < 260 260

Benzidine < 710 710 < 680 680 < 1600 1,600 < 670 670 < 760 760 < 720 720 < 1400 1,400 < 830 830 < 3600 3,600 < 700 700 < 1400 1,400 < 750 750

Benzo(a)pyrene 1,000 1,000 140 250 < 240 240 3,700 540 < 240 240 180 270 < 250 250 1,200 500 8,300 290 1,800 1,300 < 250 250 790 500 < 260 260

Benzo(b)fluoranthene 1,000 1,000 190 250 < 240 240 5,000 540 < 240 240 260 270 < 250 250 1,800 500 11,000 290 2,300 1,300 < 250 250 1,000 500 < 260 260

Benzo(ghi)perylene 100,000 100,000 < 250 250 < 240 240 1,500 540 < 240 240 < 270 270 < 250 250 380 500 3,200 290 640 1,300 < 250 250 510 500 < 260 260

Benzo(k)fluoranthene 800 3,900 < 250 250 < 240 240 1,500 540 < 240 240 < 270 270 < 250 250 480 500 3,700 290 990 1,300 < 250 250 440 500 < 260 260

Benzoic Acid < 1800 1,800 < 1700 1,700 < 3900 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 < 2100 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

Benzyl butyl phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Bis(2-chloroethoxy)methane < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Bis(2-chloroethyl)ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Bis(2-chloroisopropyl)ether < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Bis(2-ethylhexyl)phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Carbazole < 1800 1,800 < 1700 1,700 1,000 3,900 < 1700 1,700 < 1900 1,900 < 1800 1,800 < 3500 3,500 690 2,100 < 8900 8,900 < 1800 1,800 < 3600 3,600 < 1900 1,900

Chrysene 1,000 3,900 160 250 < 240 240 4,200 540 < 240 240 240 270 < 250 250 1,300 500 8,600 290 1,800 1,300 < 250 250 920 500 < 260 260

Dibenz(a,h)anthracene 330 330 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260

Dibenzofuran 7,000 59000 < 250 250 < 240 240 1,200 540 < 240 240 < 270 270 < 250 250 < 500 500 200 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Diethyl phthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Dimethylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Di-n-butylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Di-n-octylphthalate < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Fluoranthene 100,000 100,000 240 250 < 240 240 9,900 540 < 240 240 340 270 < 250 250 2,100 500 18,000 290 2,400 1,300 < 250 250 1,900 500 < 260 260

Fluorene 30,000 100,000 < 250 250 < 240 240 1,400 540 < 240 240 < 270 270 < 250 250 < 500 500 230 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Hexachlorobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Hexachlorobutadiene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Hexachlorocyclopentadiene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Hexachloroethane < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Indeno(1,2,3-cd)pyrene 500 500 < 250 250 < 240 240 1,400 540 < 240 240 < 270 270 < 250 250 370 500 3,400 290 < 1300 1,300 < 250 250 460 500 < 260 260

Isophorone < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Naphthalene 12,000 100,000 < 250 250 < 240 240 870 540 < 240 240 < 270 270 < 250 250 < 500 500 590 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Nitrobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

N-Nitrosodimethylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

N-Nitrosodi-n-propylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

N-Nitrosodiphenylamine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Pentachloronitrobenzene < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Pentachlorophenol 800 6,700 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260

Phenanthrene 100,000 100,000 160 250 < 240 240 12,000 540 < 240 240 260 270 < 250 250 1,200 500 5,800 290 1,200 1,300 < 250 250 830 500 < 260 260

Phenol 330 100,000 < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 330 330 < 260 260

Pyrene 100,000 100,000 240 250 < 240 240 7,700 540 < 240 240 320 270 < 250 250 1,900 500 16,000 290 2,700 1,300 < 250 250 1,600 500 < 260 260

Pyridine < 250 250 < 240 240 < 540 540 < 240 240 < 270 270 < 250 250 < 500 500 < 290 290 < 1300 1,300 < 250 250 < 500 500 < 260 260


Dash- Not Analyzed


ND - Not-detected



µg/Kg µg/Kg

4/2/2014 4/2/2014 4/8/2014 4/8/2014 4/8/2014


(0-2') (15-17') (0-2') (15-17')

4/8/2014 4/8/2014

EBC RI EBC RI EBC RI EBC RI

4/2/2014

EBC RI EBC RI EBC RI EBC RI EBC RI

4/2/2014 4/8/2014 4/2/2014

µg/Kgµg/Kg µg/Kg µg/Kg µg/Kg


Residential Soil Cleanup Objectives*

COMPOUND NYSDEC Part 375.6 Unrestricted Use SoilCleanup Objectives*

SB1

(0-2') (29-31')

EBC RI EBC RI

4/8/2014

µg/Kg µg/Kg

2014 Remedial InvestigationSB2 SB4 SB5 SB6 SB7

(12-14')

EBC RI

(0-2')(0-2') (29-31') (0-2') (15-17')

TABLE 4Site E

Former Domino Sugar Site Brooklyn, New York

Soil Analytical ResultsPesticides / PCBs

Results RL Results RL Results RL Results RL Results RL Results RL Results RL

PCB-1016 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1221 100 1,000 1.2 U 1.2 U 1.2 U 1.3 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1232 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1242 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1248 100 1,000 5.1 U 4.9 U 5.2 U 5.5 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1254 100 1,000 1.7 U 1.6 U 1.7 U 1.8 U < 35 35 < 38 38 < 38 38 < 36 36 210 36 < 35 35 < 36 36

PCB-1260 100 1,000 25 3.7 U 7.7 J 4.1 U < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1262 100 1,000 - - - - < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

PCB-1268 100 1,000 - - - - < 35 35 < 38 38 < 38 38 < 36 36 < 36 36 < 35 35 < 36 36

4,4-DDD 3.3 13,000 7.3 0.64 15 0.7 < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 < 2.6 2.6 < 2.5 2.5 < 2.6 2.6

4,4-DDE 3.3 8,900 0.75 U 0.72 0.76 0.79 < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 < 2.6 2.6 < 2.5 2.5 < 2.6 2.6

4,4-DDT 3.3 7,900 13 0.87 9.3 0.96 U < 2.6 2.6 < 2.8 2.8 < 2.7 2.7 < 2.6 2.6 24 2.6 < 2.5 2.5 < 2.6 2.6

a-BHC 20 480 0.27 U 0.26 0.28 0.29 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

a-Chlordane 0.31 U 0.29 0.31 0.33 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Aldrin 5 97 0.20 U 0.19 0.2 0.21 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

b-BHC 36 360 0.42 U 0.4 0.61 0.44 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Chlordane - - - - < 21 21 < 23 23 < 23 23 < 22 22 < 22 22 < 21 21 < 22 22

d-BHC 40 100,000 0.41 U 0.39 0.41 0.43 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Dieldrin 5 200 0.64 U 0.61 0.64 U 0.68 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Endosulfan I 2,400 24,000 0.33 U 0.31 0.33 U 0.35 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Endosulfan II 2,400 24,000 0.69 U 0.67 2.9 J 0.74 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Endosulfan Sulfate 2,400 24,000 0.66 U 0.64 0.67 U 0.70 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Endrin 14 11,000 0.69 U 0.66 5.1 0.73 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Endrin aldehyde 10 0.44 14 0.48 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Endrin ketone 0.68 U 0.65 0.68 U 0.72 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

gamma-BHC 100 280 0.32 U 0.31 0.32 U 0.34 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

g-Chlordane 0.70 J 0.57 2 0.63 U < 3.5 3.5 < 3.8 3.8 < 3.8 3.8 < 3.6 3.6 < 3.6 3.6 < 3.5 3.5 < 3.6 3.6

Heptachlor 42 2,100 0.36 U 0.34 U 0.36 U 0.38 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Heptachlor epoxide 0.34 U 0.32 U 0.34 U 0.36 U < 1.8 1.8 < 1.9 1.9 < 1.9 1.9 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8 < 1.8 1.8

Methoxychlor 4.1 U 3.9 U 14 J 4.3 U < 7.1 7.1 < 92 92 < 7.6 7.6 < 22 22 < 7.3 7.3 < 7.0 7 < 18 18

Toxaphene 13 U 12 U 13 U 13 U < 180 180 < 190 190 < 190 190 < 180 180 < 180 180 < 180 180 < 180 180


ND - Not-detected

Dash - Not analyzed




(1-3')(16-18')

AKRF Phase IIAKRF Phase II



AKRF Phase II AKRF Phase IICOMPOUNDNYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives



(1-3')

Results

(27-29')

ResultsResultsResults

µg/Kg

11/7/2008

µg/Kg µg/Kgµg/Kg

11/7/2008 11/7/2008 11/7/2008

Previous Investigations 2014 Remedial Investigation

SB1 SB2 SB4 SB5 SB6 SB7SB-12 SB-13

EBC RI EBC RI

(0-2') (15-17')

EBC RI EBC RI

(0-2') (0-2')

µg/Kgµg/Kg µg/Kg

(0-2')(0-2') (0-2')

4/8/2014

EBC RIEBC RI EBC RI

µg/Kg µg/Kg

4/8/2014 4/8/20144/2/2014 4/2/2014

µg/Kg µg/Kg

4/8/2014 4/2/2014

TABLE 5Site E


Soil Analytical ResultsMetals

Aluminum - - - - - - - - 2,880 2,720 5,590 2,860Antimony - - - - - - - - 1.3 U 1.2 U 1.3 U 1.7 U

Arsenic 13 16 BDL 1.9 1.4 0.82 BDL BDL BDL BDL 5 J 1.8 J 10.2 0.87 U

Barium 350 400 49 74 36 47 87 110 26 45 53.7 25.3 95.6 18.7Beryllium 7.2 72 - - - - - - - - 0.24 J 0.22 U 0.39 J 0.31 U

Cadmium 2.5 c 4.3 1.2 0.8 BDL 0.77 1.1 1.7 BDL BDL 1.7 J 0.51 U 1.8 J 0.73 U

Calcium - - - - - - - - 122,000 874 59,100 6,400Chromium 30 c 180 - trivalent 10 20 11 14 6.8 9.4 8.8 11 6.3 6.1 12.6 6.3Cobalt - - - - - - - - 4 3.4 5.4 3.3Copper 50 270 - - - - - - - - 71.7 9.5 79.7 7.9Iron - - - - - - - - 9,740 7,090 25,000 6,990Lead 63 c 400 140 11 5.3 40 91 84 7.1 7.3 192 4.1 J 446 2.8 JMagnesium - - - - - - - - 81,200 1,390 3,900 3,280Manganese 1600 c 2,000 - - - - - - - - 215 283 242 211Mercury 0.18 c 0.81 0.12 0.022 0.032 0.076 0.11 0.052 0.0073 0.011 0.22 0.015 U 0.27 0.017 U

Nickel 30 310 - - - - - - - 19.1 11.1 13.2 6.4 JPotassium - - - - - - - 676 386 768 497Selenium 3.9c 180 BDL BDL BDL BDL BDL BDL BDL BDL 1 U 0.88 U 0.95 U 1.3 U

Silver 2 180 BDL BDL BDL BDL BDL BDL BDL BDL 0.31 U 0.27 U 0.3 U 0.39 U

Sodium - - - - - - - - 377 77.5 J 980 125 JThallium - - - - - - - - 3.4 U 3 U 3.3 U 4.3 U

Vanadium - - - - - - - - 31.5 8.9 23.2 8Zinc 109 c 10,000 - - - - - - - - 96.9 46.9 695 14.3 J


Aluminum 6,940 37 3,240 36 7,520 39 3,250 34 6,520 35 4,440 36 6,340 35 6,000 42 5,240 34 6,770 32 10,500 39 8,370 38

Antimony < 1.9 1.9 < 1.8 1.8 < 1.9 1.9 < 1.7 1.7 < 1.7 1.7 < 1.8 1.8 < 1.7 1.7 < 2.1 2.1 < 3.0 3 < 1.6 1.6 < 1.9 1.9 < 1.9 1.9

Arsenic 13 16 2.7 0.7 0.7 0.7 5.7 0.8 1.5 0.7 7.1 0.7 1.5 0.7 7.2 0.7 137 0.8 4.8 0.7 1.4 0.6 12.2 0.8 1.1 0.8

Barium 350 400 97.5 0.7 20.3 0.7 84.4 0.8 22.1 0.7 56 0.7 38.8 0.7 80.8 0.7 126 0.8 82.3 0.7 45.4 0.6 75.4 0.8 61.5 0.8

Beryllium 7.2 72 0.3 0.3 < 0.29 0.29 0.35 0.31 < 0.27 0.27 0.28 0.28 0.31 0.29 0.32 0.28 0.74 0.33 < 0.27 0.27 0.35 0.26 0.38 0.31 0.54 0.31

Cadmium 2.5 c 4.3 < 0.37 0.37 < 0.36 0.36 < 0.39 0.39 < 0.34 0.34 < 0.35 0.35 < 0.36 0.36 < 0.35 0.35 8.19 0.42 0.44 0.34 < 0.32 0.32 < 0.39 0.39 < 0.38 0.38

Calcium 18,100 37 2,030 3.6 36,500 39 11,100 34 44,300 35 15,200 36 37,400 35 21,400 42 50,400 34 2,730 3.2 62,000 39 2,050 3.8

Chromium 30 c 180 - trivalent 16.4 0.37 6.68 0.36 13.3 0.39 7.08 0.34 10.7 0.35 8.23 0.36 12.6 0.35 18.9 0.42 13.1 0.34 27.4 0.32 10.6 0.39 18.1 0.38

Cobalt 5.3 0.37 2.67 0.36 4.01 0.39 2.75 0.34 2.51 0.35 2.97 0.36 4.14 0.35 18.1 0.42 3.71 0.34 5.18 0.32 3.03 0.39 7.71 0.38

Copper 50 270 32 0.37 8.42 0.36 153 3.9 7.68 0.34 34.8 0.35 12.6 0.36 57 0.35 185 4.2 42.3 0.34 18.9 0.32 25.8 0.39 18.5 0.38

Iron 18,500 37 8,230 3.6 14,000 39 8,800 34 12,200 35 8,940 3.6 16,200 35 78,600 42 14,800 34 15,300 32 15,100 39 23,900 38

Lead 63 c 400 98.7 0.7 2.3 0.7 167 7.7 12.1 0.7 108 0.7 39 0.7 166 7 308 8.3 156 6.7 6.6 0.6 174 7.7 6.4 0.8

Magnesium 9,810 37 1,960 3.6 3,460 3.9 3,390 3.4 4,740 3.5 2,150 3.6 11,200 35 2,600 4.2 12,000 34 2,950 32 6,150 39 3,410 38

Manganese 1600 c 2,000 330 3.7 185 3.6 173 3.9 176 3.4 227 3.5 254 3.6 255 3.5 435 4.2 209 3.4 357 3.2 328 3.9 480 3.8

Mercury 0.18 c 0.81 0.55 0.06 < 0.08 0.08 0.14 0.09 < 0.06 0.06 0.09 0.07 < 0.08 0.08 0.28 0.06 0.23 0.1 0.34 0.06 < 0.06 0.06 0.14 0.07 < 0.09 0.09

Nickel 30 310 13.5 0.37 6.9 0.36 15.2 0.39 7.56 0.34 10.2 0.35 8.6 0.36 15.1 0.35 39.6 0.42 14 0.34 12.3 0.32 8.69 0.39 18.1 0.38

Potassium 2,070 7 756 7 1,140 8 767 7 905 7 997 7 938 7 1,330 8 966 7 1,480 6 1,230 8 2,490 8

Selenium 3.9c 180 < 1.5 1.5 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.5 1.5

Silver 2 180 < 0.37 0.37 < 0.36 0.36 < 0.39 0.39 < 0.34 0.34 < 0.35 0.35 < 0.36 0.36 < 0.35 0.35 < 0.42 0.42 < 0.34 0.34 < 0.32 0.32 < 0.39 0.39 < 0.38 0.38

Sodium 282 7 95 7 543 8 137 7 672 7 128 7 338 7 326 8 251 7 194 6 1,280 8 180 8

Thallium < 1.5 1.5 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.4 1.4 < 1.5 1.5 < 1.4 1.4 < 1.7 1.7 < 1.3 1.3 < 1.3 1.3 < 1.5 1.5 < 1.5 1.5

Vanadium 29.7 0.4 13.8 0.4 28.3 0.4 15.6 0.3 25.3 0.3 15.5 0.4 25.8 0.3 59 0.4 28.7 0.3 30.3 0.3 23.2 0.4 29.4 0.4

Zinc 109 c 10,000 77.7 0.7 14 0.7 87.1 0.8 13.5 0.7 116 0.7 22.2 0.7 121 0.7 1,480 8.3 130 0.7 25 0.6 104 0.8 32.2 0.8


ND - Not-detected

Dash - Not analyzed

BDL - Below Detection Limit



N - The concentration is based on the response for the nearest internal. This flag is used on the TIC form for all compounds identified.




6/23/2004 6/23/2004 6/23/2004 6/23/2004

SB-12

NOVA Phase III

B-5

(0-4') (4-8') (8-12') (12-16')

NOVA Phase III

(1-3') (16-18')

ResultsResultsResultsResults

SB-13

6/23/2004 6/23/2004

mg/Kg

11/7/2008 11/7/2008

mg/Kg mg/Kg

(1-3')

mg/Kg

(27-29')

11/7/2008

AKRF Phase II

11/7/2008

AKRF Phase II

ResultsResults

6/23/2004

mg/Kg mg/Kg

6/23/2004

mg/Kg mg/Kg

AKRF Phase II

COMPOUND

NYSDEC Part 375.6 Unrestricted Use

Soil Cleanup Objectives



Objectives*

EBC RI(0-2')

mg/Kg

EBC RI EBC RI EBC RI EBC RI EBC RI

COMPOUND

NYSDEC Part 375.6 Unrestricted Use

Soil Cleanup Objectives



Objectives*

mg/Kg

B-3

(0-4') (4-8') (8-12') (12-16')

NOVA Phase III

mg/Kg

NOVA Phase III

mg/Kg mg/Kg

NOVA Phase III NOVA Phase IIINOVA Phase III NOVA Phase III


2014 Remedial InvestigationSB1 SB2 SB4 SB5 SB6 SB7

Results

AKRF Phase II

(12-14') (0-2')(29-31') (0-2') (29-31') (0-2') (15-17')

ResultsResultsResults ResultsResults

(15-17') (0-2')(15-17') (0-2')

4/2/2014 4/2/2014 4/2/2014 4/2/20144/8/2014 4/8/2014 4/2/2014 4/8/2014

mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kgmg/Kg mg/Kgmg/Kg

EBC RI EBC RI

mg/Kg mg/Kg

4/8/2014 4/8/2014 4/8/20144/8/2014

EBC RI EBC RI EBC RI EBC RI

TABLE 6Site E


Groundwater Analytical ResultsVolatile Organic Compounds

SB-13

AKRF Phase II

11/7/2008

µg/L

Results

1,1,1,2-Tetrachlorothane 5 - < 1.0 1 < 1.0 1 < 1.0 1

1,1,1-Trichloroethane 5 0.69 U < 5.0 5 < 5.0 5 < 5.0 5

1,1,2,2-Tetrachloroethane 5 0.81 U < 1.0 1 < 1.0 1 < 1.0 1

1,1,2-Trichloroethane 1 0.65 U < 1.0 1 < 1.0 1 < 1.0 1

1,1-Dichloroethane 5 1.0 U < 5.0 5 < 5.0 5 < 5.0 5

1,1-Dichloroethene 5 1.7 J < 1.0 1 < 1.0 1 < 1.0 1

1,1-Dichloropropene - < 1.0 1 < 1.0 1 < 1.0 1

1,2,3-Trichlorobenzene - < 1.0 1 < 1.0 1 < 1.0 1

1,2,3-Trichloropropane 0.04 - < 1.0 1 < 1.0 1 < 1.0 1

1,2,4-Trichlorobenzene - < 1.0 1 < 1.0 1 < 1.0 1

1,2,4-Trimethylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

1,2-Dibromo-3-chloropropane 0.04 - < 1.0 1 < 1.0 1 < 1.0 1

1,2-Dibromoethane - < 1.0 1 < 1.0 1 < 1.0 1

1,2-Dichlorobenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

1,2-Dichloroethane 0.6 0.72 U < 2.0 2 < 2.0 2 < 2.0 2

1,2-Dichloropropane 0.94 0.71 U < 1.0 1 < 1.0 1 < 1.0 1

1,3,5-Trimethylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1


1,3-Dichloropropane 5 - < 1.0 1 < 1.0 1 < 1.0 1


2,2-Dichloropropane 5 - < 1.0 1 < 1.0 1 < 1.0 1

2-Chlorotoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1

2-Hexanone (Methyl Butyl Ketone) 1.1 U < 1.0 1 < 1.0 1 < 1.0 1

2-Isopropyltoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1

4-Chlorotoluene 5 - < 1.0 1 < 1.0 1 < 1.0 1

4-Methyl-2-Pentanone 0.38 U < 1.0 1 < 1.0 1 < 1.0 1

Acetone 2.4 J < 5.0 5 < 5.0 5 2.7 5

Acrolein - < 5.0 5 < 5.0 5 < 5.0 5

Acrylonitrile 5 - < 5.0 5 < 5.0 5 < 5.0 5

Benzene 1 0.74 U < 0.70 1 < 0.70 1 < 0.70 1

Bromobenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

Bromochloromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1

Bromodichloromethane 0.48 U < 1.0 1 < 1.0 1 < 1.0 1

Bromoform 0.46 U < 5.0 5 < 5.0 5 < 5.0 5

Bromomethane 5 2.1 U < 5.0 5 < 5.0 5 < 5.0 5

Carbon Disulfide 60 0.90 J < 1.0 1 < 1.0 1 < 1.0 1

Carbon tetrachloride 5 1.1 U < 1.0 1 < 1.0 1 < 1.0 1

Chlorobenzene 5 0.72 U < 5.0 5 < 5.0 5 < 5.0 5

Chloroethane 5 1.1 U < 5.0 5 < 5.0 5 < 5.0 5

Chloroform 7 1.5 J < 5.0 5 < 5.0 5 < 5.0 5

Chloromethane 60 1.1 U < 5.0 5 < 5.0 5 < 5.0 5

cis-1,2-Dichloroethene 5 5.5 4.7 1 3.6 1 < 1.0 1

cis-1,3-Dichloropropene 0.28 U < 0.40 0 < 0.40 0 < 0.40 0

Dibromochloromethane 0.55 U < 1.0 1 < 1.0 1 < 1.0 1

Dibromomethane 5 - < 1.0 1 < 1.0 1 < 1.0 1

Dichlorodifluoromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1

Ethylbenzene 5 0.87 U < 1.0 1 < 1.0 1 < 1.0 1

Hexachlorobutadiene 0.5 - < 1.0 1 < 1.0 1 < 1.0 1

Isopropylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

m&p-Xylenes 5 - < 1.0 1 < 1.0 1 < 1.0 1

Methyl Ethyl Ketone (2-Butanone) 50 1.1 U < 1.0 1 < 1.0 1 < 1.0 1

Methyl t-butyl ether (MTBE) 10 - < 1.0 1 < 1.0 1 < 1.0 1

Methylene chloride 5 0.78 U < 3.0 3 < 3.0 3 0.38 3

Naphthalene 10 - < 1.0 1 < 1.0 1 < 1.0 1

n-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

n-Propylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

o-Xylene 5 - < 1.0 1 < 1.0 1 < 1.0 1

p-Isopropyltoluene - < 1.0 1 < 1.0 1 < 1.0 1

sec-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

Styrene 5 0.64 U < 1.0 1 < 1.0 1 < 1.0 1

tert-Butylbenzene 5 - < 1.0 1 < 1.0 1 < 1.0 1

Tetrachloroethene 5 5.7 4.7 1 3.6 1 < 1.0 1

Tetrahydrofuran (THF) - < 5.0 5 < 5.0 5 < 5.0 5

Toluene 5 0.72 U < 1.0 1 < 1.0 1 < 1.0 1

Total Xylenes 2.3 U - - -

trans-1,2-Dichloroethene 5 0.76 U < 5.0 5 < 5.0 5 < 5.0 5

trans-1,3-Dichloropropene 0.4 0.57 U < 0.40 0 < 0.40 0 < 0.40 0

trans-1,4-dichloro-2-butene 5 - < 1.0 1 < 1.0 1 < 1.0 1

Trichloroethene 5 27 24 1 20 1 0.32 1

Trichlorofluoromethane 5 - < 1.0 1 < 1.0 1 < 1.0 1

Trichlorotrifluoroethane - < 1.0 1 < 1.0 1 < 1.0 1

Vinyl Chloride 2 0.99 U < 1.0 1 < 1.0 1 < 1.0 1

Notes:Dash - Not Analyzed



Bold/highlighted- Indicated exceedance of the NYSDEC Groundwater Standard


5/8/2014

µg/L µg/L µg/L

Results Results Results

4/9/2014 4/9/2014

COMPOUNDNYSDEC Groundwater

Quality Standards


E-MW1 E-MW2 E-MW3


TABLE 7Site E


Groundwater Analytical ResultsSemi-Volatile Organic Compounds

SB-13

AKRF Phase II

11/7/2008

µg/Lµg/L Results Result RL Result RL Result RL

1,2,4,5-Tetrachlorobenzene - < 1.5 1.5 < 1.9 1.9 < 0.50 0.5

1,2,4-Trichlorobenzene 0.65 U < 5.0 5 < 6.3 6.3 < 5.0 5

1,2-Dichlorobenzene 0.48 U < 1.0 1 < 1.3 1.3 < 1.0 1

1,2-Diphenylhdrazine - < 5.0 5 < 6.3 6.3 < 5.0 5



2,2'-Oxybis (1-chloropropane) 5 0.71 U - - -

2,4,5-Trichlorophenol 3 0.54 U < 1.0 1 < 1.3 1.3 < 1.0 1

2,4,6-Trichlorophenol 3 0.49 U < 1.0 1 < 1.3 1.3 < 1.0 1

2,4-Dichlorophenol 0.55 U < 1.0 1 < 1.3 1.3 < 1.0 1

2,4-Dimethylphenol 0.50 U < 1.0 1 < 1.3 1.3 < 1.0 1

2,4-Dinitrophenol 1.1 U < 1.0 1 < 1.3 1.3 < 1.0 1

2,4-Dinitrotoluene 5 0.30 U < 5.0 5 < 6.3 6.3 < 5.0 5

2,6-Dinitrotoluene 5 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5

2-Chloronaphthalene 10 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5

2-Chlorophenol 0.61 U < 1.0 1 < 1.3 1.3 < 1.0 1

2-Methylnaphthalene 0.47 U < 5.0 5 < 6.3 6.3 < 5.0 5

2-Methylphenol (o-cresol) 0.60 U < 1.0 1 < 1.3 1.3 < 1.0 1

2-Nitroaniline 5 0.53 U < 5.0 5 < 6.3 6.3 < 5.0 5

2-Nitrophenol 0.51 U < 1.0 1 < 1.3 1.3 < 1.0 1

3&4-Methylphenol (m&p-cresol) 0.39 U < 1.0 1 < 1.3 1.3 < 1.0 1

3,3'-Dichlorobenzidine 5 0.66 U < 5.0 5 < 6.3 6.3 < 5.0 5

3-Nitroaniline 5 0.37 U < 5.0 5 < 6.3 6.3 < 5.0 5

4,6-Dinitro-2-methylphenol 0.37 U < 1.0 1 < 1.3 1.3 < 1.0 1

4-Bromophenyl phenyl ether 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5

4-Chloro-3-methylphenol 1.3 U < 1.0 1 < 1.3 1.3 < 1.0 1

4-Chloroaniline 5 0.67 U < 3.5 3.5 < 4.4 4.4 < 3.5 3.5

4-Chlorophenyl phenyl ether 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5

4-Nitroaniline 5 0.28 U < 5.0 5 < 6.3 6.3 < 5.0 5

4-Nitrophenol 0.38 U < 1.0 1 < 1.3 1.3 < 1.0 1

Acenaphthene 20 0.38 U < 5.0 5 < 6.3 6.3 < 5.0 5

Acenaphthylene 0.47 U < 0.10 0.1 < 0.13 0.1 < 0.10 0.1

Acetophenone - < 5.0 5 < 6.3 6.3 < 5.0 5

Aniline - < 3.5 3.5 < 4.4 4.4 < 3.5 3.5

Anthracene 50 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5

Benzo(a)anthracene 0.002 0.49 J 0.03 0 0.19 0 0.06 0

Benzidine 5 < 10 10 < 5.6 5.6 < 4.5 4.5

Benzo(a)pyrene 0.38 J < 0.02 0 < 0.03 0 0.02 0

Benzo(b)fluoranthene 0.002 0.48 J < 0.02 0 0.29 0 0.04 0

Benzo(g,h,i)perylene 1.8 J < 0.02 0 < 0.03 0 0.02 0

Benzo(k)fluoranthene 0.002 0.43 U < 0.02 0 0.08 0 < 0.020 0

Benzoic Acid 0.39 U < 25 25 < 31 31 < 25 25

Benzyl Butyl phthalate 0.48 U < 5.0 5 < 6.3 6.3 < 5.0 5

Bis(2-chloroethoxy)methane 5 1.1 U < 5.0 5 < 6.3 6.3 < 5.0 5

Bis(2-chloroethyl)ether 1 1.0 U < 1.0 1 < 1.3 1.3 < 1.0 1

Bis(2-chloroisopropyl)ether - < 5.0 5 < 6.3 6.3 < 5.0 5

Bis(2-ethylhexyl)phthalate 5 42 < 1.6 1.6 4.1 2 < 1.0 1

Carbazole 0.35 U < 25 25 < 31 31 < 25 25

Chrysene 0.002 0.49 J 0.03 0 0.29 0 0.05 0

Dibenzo(a,h)anthracene 0.32 U < 0.02 0 0.04 0 < 0.020 0

Dibenzofuran 0.39 U < 5.0 5 < 6.3 6.3 < 5.0 5

Diethylphthalate 50 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5

Dimethylphthalate 50 0.33 U < 5.0 5 < 6.3 6.3 < 5.0 5

Di-n-butylphthalate 50 0.49 U < 5.0 5 < 6.3 6.3 < 5.0 5

Di-n-octylphthalate 50 0.45 U < 5.0 5 < 6.3 6.3 < 5.0 5

Fluoranthene 50 1.3 J < 5.0 5 < 6.3 6.3 < 5.0 5

Fluorene 50 0.48 U < 5.0 5 < 6.3 6.3 < 5.0 5

Hexachlorobenzene 0.04 0.48 U < 0.02 0 < 0.03 0 < 0.020 0

Hexachlorobutadiene 0.5 0.86 U - < 0 0 < 0.40 0.4

Hexachlorocyclopentadiene 5 0.75 U < 5.0 5 < 6.3 6.3 < 5.0 5

Hexachloroethane 5 0.52 U < 2.4 2.4 < 3.0 3 < 0.50 0.5

Indeno(1,2,3-cd)pyrene 0.002 3.7 J < 0.02 0 0.05 0 < 0.020 0

Isophorone 0.38 U < 5.0 5 < 6.3 6.3 < 5.0 5

Naphthalene 0.42 U < 5.0 5 < 6.3 6.3 < 5.0 5

Nitrobenzene 0.4 0.73 U - < 0.04 0 < 0.10 0.1

N-Nitrosodimethylamine - < 1.0 1 < 1.3 1.3 < 1.0 1

N-Nitrosodi-n-propylamine 0.41 U < 5.0 5 < 6.3 6.3 < 5.0 5

N-Nitrosodiphenylamine 50 0.35 U < 5.0 5 < 6.3 6.3 < 5.0 5

Pentachloronitrobenzene - < 0.10 0.1 < 0.13 0.1 < 0.10 0.1

Pentachlorophenol 1.2 U < 0.80 0.8 < 1.0 1 < 0.80 0.8

Phenanthrene 50 1.2 J < 0.10 0.1 0.49 0.1 0.23 0.1

Phenol 0.29 U < 1.0 1 < 1.3 1.3 < 1.0 1

Pyrene 50 1.0 J < 5.0 5 < 6.3 6.3 < 5.0 5

Pyridine - < 10 10 < 13 13 < 10 10







4/9/2014 4/9/2014 5/8/2014

µg/L µg/L µg/L

Compound NYSDEC Groundwater Quality Standards

E-MW1 E-MW2 E-MW3


TABLE 8Site E


Groundwater Analytical ResultsPesticides / PCBs

SB-13

AKRF Phase II

11/7/2008

µg/L

Results Result RL

PCB-1016 0.09 0.084 U < 0.069 0.069

PCB-1221 0.09 0.36 U < 0.069 0.069

PCB-1232 0.09 0.084 U < 0.069 0.069

PCB-1242 0.09 0.084 U < 0.069 0.069

PCB-1248 0.09 0.084 U < 0.069 0.069

PCB-1254 0.09 0.051 U < 0.069 0.069

PCB-1260 0.09 0.053 U < 0.069 0.069

PCB-1262 0.09 - < 0.069 0.069

PCB-1268 0.09 - < 0.069 0.069

4,4-DDD 0.3 0.012 U < 0.14 0.14

4,4-DDE 0.2 0.011 U < 0.14 0.14

4,4-DDT 0.11 0.016 U < 0.14 0.14

a-BHC 0.94 - < 0.069 0.069

a-Chlordane 1.94 0.0089 U < 0.14 0.14

Alachlor 0.0054 U < 1.0 1

Aldrin 0.0092 U < 0.021 0.021

b-BHC 0.04 0.0084 U < 0.069 0.069

Chlordane 0.05 - < 1.4 1.4

d-BHC 0.04 0.0064 U < 0.069 0.069

Dieldrin 0.004 0.011 U < 0.021 0.021

Endosulfan I 0.0052 U < 0.14 0.14

Endosulfan II 0.011 U < 0.14 0.14

Endosulfan Sulfate 0.015 U < 0.14 0.14

Endrin 0.016 U < 0.14 0.14

Endrin aldehyde 5 0.010 U < 0.14 0.14

Endrin ketone 0.012 U < 0.14 0.14

gamma-BHC 0.05 0.0060 U < 0.069 0.069

g-Chlordane 0.0054 U < 0.14 0.14

Heptachlor 0.04 0.0084 U < 0.14 0.14

Heptachlor epoxide 0.03 0.0065 U < 0.14 0.14

Methoxychlor 35 0.10 U < 1.4 1.4

Toxaphene 0.24 U < 3.5 3.5

Notes:U - The compound was anlayzed for but not detected at or above the MDL.

DASH - Not analyzed



Quality Standards

E-MW3

EBC RI

5/8/2014

µg/L

TABLE 9Site E


Groundwater Analytical ResultsMetals

SB-13

AKRF Phase II

11/7/2008

mg/L

Results Result RL Result RL

Aluminum NS 61 2.43 0.01 3.68 0.01

Antimony 0.003 0.0088 U < 0.003 0.003 < 0.003 0.003

Arsenic 0.025 0.04 < 0.004 0.004 < 0.004 0.004

Barium 1 0.59 0.126 0.01 0.128 0.01

Beryllium 0.003 0.0052 J < 0.001 0.001 < 0.001 0.001

Cadmium 0.005 0.0028 U < 0.004 0.004 < 0.004 0.004

Calcium NS 141 110 0.01 124 0.01

Chromium 0.05 0.5 0.004 0.001 0.008 0.001

Cobalt NS 0.099 < 0.005 0.005 < 0.005 0.005

Copper 0.2 0.58 0.007 0.005 0.014 0.005

Iron 0.5 178 2.89 0.01 3.89 0.01

Lead 0.025 0.16 < 0.002 0.002 0.031 0.002

Magnesium 35 65 31.2 0.01 30.9 0.01

Manganese 0.3 3 2.65 0.05 0.229 0.005

Mercury 7.00E-04 0.00009 U < 0.0002 2.00E-04 < 0.0002 2.00E-04

Nickel 0.1 0.39 0.014 0.004 0.005 0.004

Potassium NS 23 12.9 0.1 11.8 0.1

Selenium 0.01 0.0053 J 0.009 0.004 0.007 0.004

Silver 0.05 0.0013 U < 0.005 0.005 < 0.005 0.005

Sodium 2 213 237 1 249 1

Thallium 0.0005 0.008 U < 0.002 0.002 < 0.002 0.002

Vanadium NS 0.21 < 0.010 0.01 < 0.010 0.01

Zinc 2 8 < 0.010 0.01 0.031 0.01


U - The compound was anlayzed for but not detected at or above the MDL. NS - No Standard


mg/L


E-MW1 E-MW2

EBC RI EBC RI

4/9/2014 4/9/2014


Quality Standards

mg/L

TABLE 10Site E


Groundwater Analytical ResultsDissolved Metals

SB-13

AKRF Phase II

11/7/2008

mg/L

Results Result RL Result RL Result RL

Aluminum NS 0.047 U 0.9 0.01 0.39 0.01 0.39 0.01

Antimony 0.003 0.0088 U < 0.003 0.003 < 0.003 0.003 < 0.003 0.003

Arsenic 0.025 0.0044 U < 0.003 0.003 < 0.003 0.003 0.003 0.003

Barium 1 0.082 0.12 0.011 0.1 0.011 0.1 0.011

Beryllium 0.003 0.0011 U < 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Cadmium 0.005 0.0028 U < 0.004 0.004 < 0.004 0.004 0.001 0.004

Calcium NS 131 112 0.01 124 0.01 39.6 0.01

Chromium 0.05 0.001 U 0.001 0.001 < 0.001 0.001 0.005 0.001

Cobalt NS 0.014 < 0.005 0.005 < 0.005 0.005 < 0.005 0.005

Copper 0.2 0.0014 U < 0.005 0.005 < 0.005 0.005 0.003 0.005

Iron 0.5 1.8 0.88 0.01 0.18 0.01 0.38 0.01

Lead 0.025 0.003 U < 0.002 0.002 < 0.002 0.002 0.001 0.002

Magnesium 35 38.5 31.6 0.01 30.9 0.01 8.03 0.01

Manganese 0.3 0.63 2.89 0.053 0.137 0.005 0.019 0.005

Mercury 0.0007 0.00009 U < 0.0002 0.0002 < 0.0002 0.0002 < 0.0004 0.0004

Nickel 0.1 0.019 0.012 0.004 < 0.004 0.004 < 0.004 0.004

Potassium NS 9 13.6 0.1 13.1 0.1 12.5 0.1

Selenium 0.01 0.0058 J < 0.004 0.004 0.006 0.004 0.068 0.004

Silver 0.05 0.0013 U < 0.005 0.005 < 0.005 0.005 0.001 0.005

Sodium 2 211 255 1.1 247 1.1 87.5 1.1

Thallium 0.0005 0.008 U < 0.001 0.001 < 0.001 0.001 < 0.001 0.001

Vanadium NS 0.0012 U < 0.01 0.01 < 0.01 0.01 0.007 0.011

Zinc 2 0.25 < 0.011 0.011 < 0.011 0.011 0.008 0.011

Notes:Dash - Not AnalyzedNS - No Standard




4/9/2014 4/9/2014 5/8/2014

mg/L mg/L mg/L


Quality Standards

E-MW1 E-MW2 E-MW3


TABLE 11Site E


Soil Gas Analytical ResultsVolatile Organic Compounds

NYSDOH Soil OutdoorBackground Levels

(µg/m3) (a) (µg/m3) (b) Result RL Result RL Result RL Result RL Result RL

1,1,1,2-Tetrachloroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,1,1-Trichloroethane 100 <2.0 - 2.8 3.16 1 < 1.00 1 3.54 1 < 1.00 1 1.25 1

1,1,2,2-Tetrachloroethane <1.5 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,1,2-Trichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,1-Dichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,1-Dichloroethene <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2,4-Trichlorobenzene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2,4-Trimethylbenzene <1.0 < 1.00 1 34.5 1 24.5 1 24.3 1 17.8 1

1,2-Dibromoethane <1.5 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2-Dichlorobenzene <2.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2-Dichloroethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2-Dichloropropane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,2-Dichlorotetrafluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,3,5-Trimethylbenzene <1.0 < 1.00 1 9.28 1 6.78 1 6.58 1 6.29 1

1,3-Butadiene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,3-Dichlorobenzene <2.0 < 1.00 1 5.53 1 1.8 1 2.76 1 6.01 1

1,4-Dichlorobenzene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

1,4-Dioxane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

2-Hexanone 5.28 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

4-Ethyltoluene NA < 1.00 1 6.88 1 5.45 1 5.99 1 4.72 1

4-Isopropyltoluene < 1.00 1 < 1.00 1 1.26 1 < 1.00 1 < 1.00 1

4-Methyl-2-pentanone < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Acetone NA 254 1 387 1 769 1 268 1 610 1

Acrylonitrile < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Benzene <1.6 - 4.7 < 1.00 1 3.32 1 7.02 1 3.48 1 6.13 1

Benzyl Chloride NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Bromodichloromethane <5.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Bromoform <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Bromomethane <1.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Carbon Disulfide NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 5.63 1

Carbon Tetrachloride 5 <3.1 0.377 0.25 0.503 0.25 < 0.25 0.25 0.566 0.25 < 0.25 0.25

Chlorobenzene <2.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Chloroethane NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Chloroform <2.4 3.81 1 < 1.00 1 8.64 1 < 1.00 1 1.85 1

Chloromethane <1.0 - 1.4 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

cis-1,2-Dichloroethene <1.0 2.65 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

cis-1,3-Dichloropropene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Cyclohexane NA < 1.00 1 3.34 1 4.71 1 3.47 1 5.64 1

Dibromochloromethane <5.0 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Dichlorodifluromethane NA 1.63 1 2.57 1 2.37 1 2.92 1 2.47 1

Ethanol 9.4 1 52.3 1 58 1 49.3 1 56.9 1

Ethyl Acetate NA < 1.00 1 12.3 1 22.1 1 9 1 14.8 1

Ethylbenzene <4.3 < 1.00 1 15.6 1 11.8 1 13.4 1 14.1 1

Heptane NA 1.15 1 9.26 1 17.3 1 7.21 1 19.2 1

Hexachlorobutadiene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Hexane <1.5 < 1.00 1 5.88 1 13.4 1 5.11 1 18.5 1

Isopropylalcohol NA 4.86 1 2.97 1 4.52 1 4.84 1 3.86 1

Isopropylbenzene < 1.00 1 1.82 1 1.28 1 1.33 1 1.28 1

Xylene (m&p) <4.3 1.04 1 55.5 1 42.5 1 46.9 1 48.2 1

Methyl Ethyl Ketone 19.9 1 23.9 1 41.8 1 18.4 1 31.2 1

MTBE NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Methylene Chloride <3.4 1.6 1 1.25 1 < 1.00 1 1.42 1 1.14 1

n-Butylbenzene < 1.00 1 2.74 1 2.69 1 2.14 1 2.58 1

Xylene (o) <4.3 < 1.00 1 23.1 1 15.4 1 18.4 1 16.9 1

Propylene NA 5.21 1 2.24 1 23.7 1 2.03 1 50.9 1

sec-Butylbenzene < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Styrene <1.0 < 1.00 1 1.02 1 1.4 1 1.02 1 1.53 1

Tetrachloroethene 100 2.03 0.25 2.85 0.25 6.57 0.25 3.25 0.25 28.3 0.25

Tetrahydrofuran NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Toluene 1.0 - 6.1 1.81 1 41.8 1 50.1 1 36.8 1 56.1 1

trans-1,2-Dichloroethene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

trans-1,3-Dichloropropene NA < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Trichloroethene 5 <1.7 24.1 0.25 < 0.25 0.25 61.2 0.25 < 0.25 0.25 54.8 0.25

Trichlorofluoromethane NA 1.35 1 1.24 1 1.29 1 1.52 1 1.35 1

Trichlorotrifluoroethane < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1 < 1.00 1

Vinyl Chloride <1.0 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25 < 0.25 0.25

BTEX 2.85 139.32 126.82 118.98 141.43

Notes:NA No guidance value or standard available(a) Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York. October 2006. New York State Department of Health.(b) NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February 2005, Summary of Background Levels for Selected Compounds (NYSDOH Database, Outdoor values)Value detected above NYSDOH Air Guidance Value of 5 µg/m3, which according to Soil Vapor/Indoor Air Matrix 1 would require at a minimum, mitigation. Value detected above NYSDOH Air Guidance Value of 100 µg/m3, which according to Soil Vapor/Indoor Air Matrix 2 would require at a minimum, mitigation.

E-SG4(µg/m³)

E-SG5(µg/m³) COMPOUNDS

NYSDOH Maximum Sub-Slab Value

E-SG1(µg/m³)

E-SG2(µg/m³)

E-SG3(µg/m³)

FIGURES

EEBBCCEnvironmental Business Consultants Phone 631.504.6000

Fax1808 Middle Country Road. Ridge. NY 11961 631.924.2780

FORMER DOMINO SUGAR SITE E

FIGURE 1 Site Location Map

USGS Brooklyn Quadrangle 1995, Contour Interval = 10 feet

317-329 Kent Avenue, Brooklyn, NY

SITE LOCATION

EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

Site Name:

Site Address:

Drawing Title:

Figure No.2 317-329 Kent Avenue, Brooklyn, NY 11249

Domino Sugar Site - Site E

Site Boundary Map

1 Inch = 50 Feet

7525 50

Site Boundary

KEY:

0

SCALE:

KENT AVENUE

SO

UT

H 4

TH

ST

RE

ET

SID

EW

ALK

SO

UT

H 3

RD

ST

RE

ET

LOT 30

LOT 1

LOT 24

LO

T 26

LO

T 27

32

0'

180'

E

EEBB CC ENVIRONMENTAL BUSINESSS CONSULTANTS 1808 Middle Country Road, Ridge, New York 11961 Phone: (631) 504-6000 Fax: (631) 924-2870

FIGURE 4 SURROUNDING LAND USE MAP

SITE D 317-329 KENT AVENUE, BROOKLYN, NY

Source: http://www.oasisnyc.net/map.aspx

Site D

Site CSite E

Site F

Site B


Phone 631.504.6000Fax 631. 924 .2870

Site Name:

Site Address:

Drawing Title:



Site Sampling Locations

1 Inch = 50 Feet

7525 50

New Building Area

KEY:

0

SCALE:

KENT AVENUE

SO

UT

H 4

TH

ST

RE

ET

Existing Building

SB-13

SIDEWALK

SO

UT

H 3

RD

ST

RE

ET

LOT 30

LOT 1

LOT 24

LO

T 26

LO

T 27

E-MW1E-SB1

E-SB6

E-SB7

E-SB3

Soil Boring Location

GW Sampling Location

Soil Boring Location (AKRF Phase II 2008)

E-SB4 E-SB5

E-SG1

E-SG3

E-SG5

E-SG4

E-MW3

E-MW2

E-SB2

E-SG2

SG Sampling Location

REFUSALS 3-14'

NO SAMPLESALL C&D DEBRIS

RECOVERED

SB-12

E

Soil Boring Location (NOVA Phase III 2004)

B-5

B-3

B-4

B-1

B-2


Phone 631.504.6000Fax 631. 924 .2870

Site Name:

Site Address:

Drawing Title:



Soil Exceedences Map

1 Inch = 50 Feet

7525 50New Building Area

KEY:

0

SCALE:

KENT AVENUE

Existing Building

SIDEWALK

SO

UT

H 3

RD

ST

RE

ET

LOT 30 LOT 24

LO

T 26

LO

T 27

E-MW1

E-SB1

E-SB6

E-SB7

E-SB3




E-SB5

E-SG1

E-SG3

E-SG5

E-SG4

E-MW3

E-MW2E-SB2

E-SG2


REFUSALS 3-14'


RECOVERED

VOCs, SVOCs, Pesticides, PCBs ppb

Concentration above Unrestricted Use SCO

Concentration above Restricted Res SCO

Metals ppm

E-SB1 (0-2')

Lead 98.7

Mercury 0.55

E-SB2 (0-2')

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Chrysene

Indeno(1,2,3-cd)pyrene

Copper

Lead

Benzo(k)fluoranthene

3,700

5,000

4,800

1,400

4,200

153

167

1,500

E-SB4 (0-2')

Lead 108

Zinc 116

E-SB5 (0-2')

Benzo(a)anthracene

Benzo(a)pyrene 1,200

Benzo(b)fluoranthene 1,800

1,400

Indeno(1,2,3-cd)pyrene 3,400

Benzo(k)fluoranthene 3,700

Chrysene 8,600


Chrysene

Copper 57

1,300

Lead 166

Mercury 0.28

Zinc 121

E-SB5 (12-14')

Benzo(a)anthracene 9,300


Nickel 39.6

Lead 308

Mercury 0.23

Cadmium 8.19

Arsenic

Copper 185

Zinc 1,480

137

E-SB6 (0-2')

Acetone 68

Benzo(a)anthracene



1,800

Zinc 130

Chrysene

PCB-1254 210

1,800

4,4-DDT 24

Lead 156

Mercury 0.34

Benzo(k)fluoranthene 990

E-SB7 (0-2')

Lead 174



Chrysene 17,000


AKRF - SB-12 (1-3')



Copper

0.22

Lead71.7

Mercury

192

4,4'-DDD 7.33

Dibenz(a,h)anthracene

4,4'-DDT 13

18,000

4,500



Chrysene 12,000


AKRF - SB-13 (1-3')



Copper

0.27

Lead79.7

Mercury

446

4,4'-DDD 15


4,4'-DDT 9.3

8,900

4,100

695Zinc

E-SB4

BSoil Boring Location (NOVA Phase III 2004)

SB-13

SB-12

B-5

B-3

B-4

B-1

B-2


480


Chrysene 3,200


NOVA B-2 (0-4)



1,300



Chrysene 1,400


NOVA B-2 (8-12)


730

NOVA B-3 (0-4')

Lead 140


2,600


Chrysene 18,000


NOVA B-4 (0-4')



6,900



1,900


Chrysene 15,000


NOVA B-4 (4-8')



7,900



2,500


Chrysene 19,000


NOVA B-4 (8-12')



7,700



520


Chrysene 3,000


NOVA B-5 (0-4')


3,100

1,500


Benzo(b)fluoranthene

Lead 91

Lead 84

NOVA B-5 (4-8')


Phone 631.504.6000Fax 631. 924 .2870

Site Name:

Site Address:

Drawing Title:



Groundwater Exceedences Map

1 Inch = 50 Feet

7525 50

New Building Area

KEY:

0

SCALE:

KENT AVENUE

SO

UT

H 4

TH

ST

RE

ET

Existing Building

SB-13

SIDEWALK

SO

UT

H 3

RD

ST

RE

ET

LOT 30

LOT 1

LOT 24

LO

T 26

LO

T 27

E-MW1E-SB1

E-SB6

E-SB7

E-SB3




E-SB4

E-SB5

E-SG1

E-SG3

E-SG5

E-SG4

E-MW3

E-MW2E-SB2

E-SG2


REFUSALS 3-14'


RECOVERED

SB-12

E

E-MW1

Trichloroethylene 24

Chrysene 0.03

VOCs (ug/L)

SVOCs (ug/L)

Iron 0.88

Manganese 2.89

Dissolved Metals (mg/L)

Benzo(a)anthracene 0.03

E-MW2

Trichloroethylene 20

Benzo(b)fluoranthene 0.29

Benzo(k)fluoranthene 0.08

VOCs (ug/L)

SVOCs (ug/L)

Chrysene 0.29

Indeno(1,2,3-cd)pyrene 0.05


Sodium 255

Sodium 247


E-MW3


Chrysene 0.05

SVOCs (ug/L)

Selenium 0.068

Sodium 87.5



Iron 0.38

AKRF - SB-13

cis-1,2-Dichloroethene 5.5


Bis(2-ethylexyl)phthalate 42

VOCs (ug/L)

SVOCs (ug/L)

Chrysene 0.49

Indeno(1,2,3-cd)pyrene 3.7


Iron 1.8


Tetrachloroethene 5.7

Trichloroethene 27

Magnesium 38.5

Manganese 0.63

Sodium 211


Phone 631.504.6000Fax 631. 924 .2870

Site Name:

Site Address:

Drawing Title:



Soil Vapor Detections

1 Inch = 50 Feet

7525 50

New Building Area

KEY:

0

SCALE:

KENT AVENUE

SO

UT

H 4

TH

ST

RE

ET

Existing Building

SB-13

SIDEWALK

SO

UT

H 3

RD

ST

RE

ET

LOT 30

LOT 1

LOT 24

LOT

26

LOT

27

E-MW1E-SB1

E-SB6

E-SB7

E-SB3




E-SB4 E-SB5

E-SG1

E-SG3

E-SG5

E-SG4

E-MW3

E-MW2

E-SB2

E-SG2

SG Sampling LocationREFUSALS 3-14'


RECOVERED

SB-12

EE-SG5

Compound µg/m³

1,1,1-Trichloroethane

Carbon Tetrachloride

1.25

PCE 28.3

TCE 54.8

ND

E-SG4

Compound µg/m³



ND

PCE 3.25

TCE ND

0.566

E-SG2

Compound µg/m³



ND

PCE 2.85

TCE ND

0.503

E-SG1

Compound µg/m³



3.16

PCE 2.03

TCE 24.1

0.377

Value Detected Above NYSDOHAir Guidance Value

E-SG3

Compound µg/m³



3.54

PCE 6.57

TCE 61.2

ND

ATTACHMENT A

SOIL BORING LOGS

Geologic Boring Log Details

Site Elevation Datum

Site Name: TTM1401 DTW Ground Elevation

Drilling Company: Method:Eastern Environmental Solutions Geoprobe Well SpecificationsDate Started:

Installed E-MW1Completion Depth:40 feet D Mosca

DEPTH SAMPLES(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID

(in.) 6 in. (ppm)

0

5

10

15

20

25

30

35

36 0.0

26" - Tan coarse sand.

10" - Saturated fine brown sand.

*Retained soil sample E-SB1(29-31')

30 0.0

30" - Medium brown sand and fine gravel.

32 0.0


to

22 0.0


to

21 0.0

21" - Medium brown sand.

to

25 0.0

7" - Top soil and gravel.

to18" - Medium brown sand.


4/8/2014 4/8/2014Geologist

E-SB1

(NTS)

Brooklyn, NY Groundwater depth

Date Completed:

30" - Saturated brown sand.

to

E-SB1Location: Performed at the northeast corner of the Site. Depth to Water

(ft. from grade.)Address: Date

1" PVC Set at 40' with 15' screen

to

to

30 0.0

EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS





NoneCompletion Depth:31 feet D Mosca


(in.) 6 in. (ppm)

0

5

10

15

20

25

31

E-SB2Location: Performed at the southeast corner of the Site. Depth to Water



Date Completed:4/8/2014 4/8/2014

Geologist

E-SB2

(NTS)

13 0.0

13" - Topsoil followed by concrete and brick.

to


12 0.0

12" - Concrete and brick.

to

8 0.0


to

0 0.0

No recovery, rock in shoe.

to

19 0.0

2" - Historic fill composed of coal and brick.

to

20" - Medium tan sand.

17" - Medium tan sand.

20 0.0to






Drilling Company: Method:C² Environmental Geoprobe Well SpecificationsDate Started:



(in.) 6 in. (ppm)

0

5

10

15

20

32 0.0

2" - Brick.

to30" - Medium sand and fine gravel.


28 0.0

18" - Brick and concrete.

to4" - Medium sand and broken brick.


0

No recovery.

to

30 0.0

6" - Topsoil and gravel.

to24" - Brick and concrete.


4/2/2014 4/2/2014Geologist

E-SB4

(NTS)


Date Completed:

E-SB4Location: Performed along South 4th Street approximately 140'

from the east property line.Depth to Water(ft. from grade.)

Address: Date








(in.) 6 in. (ppm)

0

5

10

14

3" - Red brick.

10" - Dark moist historic fill composed of coal, brick, and gravel.

4" - Moist brown silty sand.

*Retained soil sample A-SB5(11-14')

Refusal at 14'.

19 0.0


to

27 0.0

11" - Topsoil

to7" - Concrete.

9" - Red brick.


4/2/2014 4/2/2014Geologist

E-SB5

(NTS)


Date Completed:

to17 0.0

E-SB5Location: Performed along South 3rd Street approximately over

140' from the east property line.Depth to Water(ft. from grade.)

Address: Date








(in.) 6 in. (ppm)

0

5

10

15

20

E-SB6Location: Performed in the southwest corner within the bike park. Depth to Water




Geologist

E-SB6

(NTS)

to

20 0.0

4" - Top soil.

to


5" - Brown silty sand.

12 0.0


to


14 0.0

2" - Red brick.

to7" - Historic fill.

22 0.0

22" - Medium brown sand and gravel. Moist at the bottom 6".

22" - Historic fill composed of coal, brick, etc in a sandy matrix.

6" - Historic fill.






E-MW3Completion Depth:20 feet D Mosca


(in.) 6 in. (ppm)

0

5

10

15

20

1" PVC Set at 25' with 10' screen

E-SB7Location: Performed in the northeast corner of the Site. Depth to Water




Geologist

E-SB7

(NTS)

20 0.0

4" - Top soil.

to16" - Concrete and brick.


18 0.0


to

23 0.0

23" - Medium brown sand.

to

45 0.0

45" - Firm, moist brown sandy loam.

to



ATTACHMENT B GROUNDWATER SAMPLING LOGS

Well I.D.: E-MW1 Date: 4/9/2014

Well Depth (from TOC): 40 Equipment: Check Valve

Static Water Level (from TOC): 34.89 Field Personnel: Dominick Mosca

Height of Water in Well: 5.11

Gallons of Water per Well Volume: 0.2044

Approximate Flow Rate: 400ml/min.

Time Time (24Hr) ~ Flow RateGal.

RemovedpH Cond. (µS/cm) Temp. (ºF) DO (mg/L) Comments

0.00 8:11 400ml/min 0 turbid2.00 8:13 400ml/min 0.22 turbid4.00 8:15 400ml/min 0.44 clear6.00 8:17 400ml/min 0.66 clear8.00 8:19 400ml/min 0.88 clear

8:25 Collected Samples

Note 400 ml = 0.11 gallons

GROUNDWATER PURGE / SAMPLE LOGS

EBCEB C ENVIRONMENTAL BUSINESS CONSULTANTS







Time Time (24Hr) ~Flow RateGal.


0.00 8:34 400ml/min 0 turbid2.00 8:36 400ml/min 0.22 turbid4.00 8:38 400ml/min 0.44 turbid6.00 8:40 400ml/min 0.66 turbid8.00 8:42 400ml/min 0.88 clear10.00 8:44 400ml/min 1.1 clear12.00 8:46 400ml/min 1.32 clear14.00 8:48 400ml/min 1.54 clear16.00 8:50 400ml/min 1.76 clear











Time Time (24Hr) ~ Flow RateGal.


0.00 8:39 400ml/min 0 turbid2.00 8:41 400ml/min 0.22 turbid4.00 8:43 400ml/min 0.44 clear6.00 8:45 400ml/min 0.66 clear8.00 8:49 400ml/min 0.88 clear





ATTACHMENT C

SOIL GAS SAMPLING LOGS

ATTACHMENT D

LABORATORY REPORTS IN DIGITAL FORMAT

BG30367

Wednesday, May 07, 2014

Sample ID#s:

Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Project ID: DOMINO SUGAR SITE E

Sincerely yours,

Laboratory DirectorPhyllis Shiller

Enclosed are revised Analysis Report pages. Please replace and discard the original pages. If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

SDG CommentsMay 07, 2014

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GBG30363

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

04/08/14SWsee "By" below

Laboratory Data

E-SB6 15-17

Phoenix ID: BG30367

04/09/140:00

16:26

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 07, 2014

Date Time



SDG ID: GBG30363

Client ID:Project ID: DOMINO SUGAR SITE E

LOD/MDL

< 0.32Silver 0.32 04/11/14 LK SW6010mg/Kg0.196770Aluminum 32 04/11/14 LK SW6010mg/Kg6.51.4Arsenic 0.6 04/11/14 LK SW6010mg/Kg0.65

45.4Barium 0.6 04/11/14 LK SW6010mg/Kg0.130.35Beryllium 0.26 04/11/14 LK SW6010mg/Kg0.132730Calcium 3.2 04/11/14 LK SW6010mg/Kg3.0

< 0.32Cadmium 0.32 04/11/14 LK SW6010mg/Kg0.135.18Cobalt 0.32 04/11/14 LK SW6010mg/Kg0.1327.4Chromium 0.32 04/11/14 LK SW6010mg/Kg0.1318.9Copper 0.32 04/11/14 LK SW6010mg/kg0.26

15300Iron 32 04/11/14 LK SW6010mg/Kg B32< 0.06Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.041480Potassium 6 04/11/14 LK SW6010mg/Kg2.52950Magnesium 32 04/11/14 LK SW6010mg/Kg1.9357Manganese 3.2 04/11/14 LK SW6010mg/Kg1.3194Sodium 6 04/11/14 LK SW6010mg/Kg2.812.3Nickel 0.32 04/11/14 LK SW6010mg/Kg0.136.6Lead 0.6 04/11/14 LK SW6010mg/Kg0.19

< 1.6Antimony 1.6 04/11/14 LK SW6010mg/Kg0.65< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.330.3Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1325.0Zinc 0.6 04/11/14 LK SW6010mg/Kg0.3292Percent Solid 04/09/14 I E160.3%

CompletedSoil Extraction for PCB 05/01/14 JB SW3545CompletedSoil Extraction for Pesticide 05/01/14 JB/V SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471

Page 1 of 6 Ver 2

E-SB6 15-17Phoenix I.D.: BG30367

Client ID:DOMINO SUGAR SITE EProject ID:


LOD/MDL

CompletedTotal Metals Digest 04/09/14 CB/AG/WSW846 - 3050

CompletedField Extraction 04/08/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1221 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1232 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1242 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1248 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1254 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1260 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1262 35 05/02/14 AW SW 8082ug/Kg35NDPCB-1268 35 05/02/14 AW SW 8082ug/Kg35

QA/QC Surrogates97% DCBP 05/02/14 AW 30 - 150 %%82% TCMX 05/02/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDE 2.5 05/05/14 CE SW8081ug/Kg2.5ND4,4' -DDT 2.5 05/05/14 CE SW8081ug/Kg2.5NDa-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDAldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDChlordane 21 05/05/14 CE SW8081ug/Kg21NDd-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan II 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndosulfan sulfate 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin 1.8 05/05/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.5 05/05/14 CE SW8081ug/Kg3.5NDEndrin ketone 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 05/05/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.5 05/05/14 CE SW8081ug/Kg3.5NDHeptachlor 1.8 05/05/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 05/05/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.0 05/05/14 CE SW8081ug/Kg7.0NDToxaphene 180 05/05/14 CE SW8081ug/Kg180

QA/QC Surrogates101% DCBP 05/05/14 CE 30 - 150 %%90% TCMX 05/05/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.2ND1,1,1-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg1.5ND1,1,2,2-Tetrachloroethane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,1,2-Trichloroethane 7.3 04/11/14 U SW8260ug/Kg0.71ND1,1-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg1.4

Page 2 of 6 Ver 2




LOD/MDL

ND1,1-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6ND1,1-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.4ND1,2,3-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,3-Trichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.5ND1,2,4-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg1.0ND1,2-Dibromo-3-chloropropane 7.3 04/11/14 U SW8260ug/Kg2.0ND1,2-Dibromoethane 7.3 04/11/14 U SW8260ug/Kg1.9ND1,2-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg0.80ND1,2-Dichloroethane 7.3 04/11/14 U SW8260ug/Kg0.64ND1,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.0ND1,3,5-Trimethylbenzene 7.3 04/11/14 U SW8260ug/Kg0.96ND1,3-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1ND1,3-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg0.77ND1,4-Dichlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.2ND2,2-Dichloropropane 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg1.2ND2-Hexanone 36 04/11/14 U SW8260ug/Kg3.3ND2-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg 11.0ND4-Chlorotoluene 7.3 04/11/14 U SW8260ug/Kg0.84ND4-Methyl-2-pentanone 36 04/11/14 U SW8260ug/Kg1.7NDAcetone 50 04/11/14 U SW8260ug/Kg7.2NDAcrylonitrile 15 04/11/14 U SW8260ug/Kg4.1NDBenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDBromobenzene 7.3 04/11/14 U SW8260ug/Kg0.95NDBromochloromethane 7.3 04/11/14 U SW8260ug/Kg1.1NDBromodichloromethane 7.3 04/11/14 U SW8260ug/Kg0.90NDBromoform 7.3 04/11/14 U SW8260ug/Kg1.0NDBromomethane 7.3 04/11/14 U SW8260ug/Kg5.6NDCarbon Disulfide 7.3 04/11/14 U SW8260ug/Kg1.2NDCarbon tetrachloride 7.3 04/11/14 U SW8260ug/Kg0.84NDChlorobenzene 7.3 04/11/14 U SW8260ug/Kg1.1NDChloroethane 7.3 04/11/14 U SW8260ug/Kg1.7NDChloroform 7.3 04/11/14 U SW8260ug/Kg1.3NDChloromethane 7.3 04/11/14 U SW8260ug/Kg3.8NDcis-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.6NDcis-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg0.79NDDibromochloromethane 7.3 04/11/14 U SW8260ug/Kg0.82NDDibromomethane 7.3 04/11/14 U SW8260ug/Kg0.92NDDichlorodifluoromethane 7.3 04/11/14 U SW8260ug/Kg1.9NDEthylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDHexachlorobutadiene 7.3 04/11/14 U SW8260ug/Kg1.5NDIsopropylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDm&p-Xylene 7.3 04/11/14 U SW8260ug/Kg2.9NDMethyl Ethyl Ketone 44 04/11/14 U SW8260ug/Kg6.3NDMethyl t-butyl ether (MTBE) 15 04/11/14 U SW8260ug/Kg2.0NDMethylene chloride 7.3 04/11/14 U SW8260ug/Kg1.2NDNaphthalene 7.3 04/11/14 U SW8260ug/Kg2.0NDn-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3

Page 3 of 6 Ver 2




LOD/MDL

NDn-Propylbenzene 7.3 04/11/14 U SW8260ug/Kg1.3NDo-Xylene 7.3 04/11/14 U SW8260ug/Kg2.8NDp-Isopropyltoluene 7.3 04/11/14 U SW8260ug/Kg1.0NDsec-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.4NDStyrene 7.3 04/11/14 U SW8260ug/Kg2.1NDtert-Butylbenzene 7.3 04/11/14 U SW8260ug/Kg1.2NDTetrachloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTetrahydrofuran (THF) 15 04/11/14 U SW8260ug/Kg 16.6NDToluene 7.3 04/11/14 U SW8260ug/Kg1.2NDtrans-1,2-Dichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,3-Dichloropropene 7.3 04/11/14 U SW8260ug/Kg1.5NDtrans-1,4-dichloro-2-butene 15 04/11/14 U SW8260ug/Kg14NDTrichloroethene 7.3 04/11/14 U SW8260ug/Kg1.5NDTrichlorofluoromethane 7.3 04/11/14 U SW8260ug/Kg1.6NDTrichlorotrifluoroethane 7.3 04/11/14 U SW8260ug/Kg1.1NDVinyl chloride 7.3 04/11/14 U SW8260ug/Kg2.4

QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%100% Bromofluorobenzene 04/11/14 U 70 - 130 %%114% Dibromofluoromethane 04/11/14 U 70 - 130 %%100% Toluene-d8 04/11/14 U 70 - 130 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 250 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 250 04/10/14 DD SW 8270ug/Kg110ND1,2-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg99ND1,2-Diphenylhydrazine 250 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 250 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 250 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 250 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 250 04/10/14 DD SW 8270ug/Kg87ND2,4-Dinitrophenol 1800 04/10/14 DD SW 8270ug/Kg250ND2,4-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg140ND2,6-Dinitrotoluene 250 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Chlorophenol 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylnaphthalene 250 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 250 04/10/14 DD SW 8270ug/Kg170ND2-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg360ND2-Nitrophenol 250 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 250 04/10/14 DD SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 700 04/10/14 DD SW 8270ug/Kg170ND3-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg760ND4,6-Dinitro-2-methylphenol 1800 04/10/14 DD SW 8270ug/Kg380ND4-Bromophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 250 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 700 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 250 04/10/14 DD SW 8270ug/Kg120

Page 4 of 6 Ver 2




LOD/MDL

ND4-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/10/14 DD SW 8270ug/Kg98NDAcetophenone 250 04/10/14 DD SW 8270ug/Kg110NDAniline 1800 04/10/14 DD SW 8270ug/Kg710NDAnthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenz(a)anthracene 250 04/10/14 DD SW 8270ug/Kg120NDBenzidine 700 04/10/14 DD SW 8270ug/Kg210NDBenzo(a)pyrene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 250 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/10/14 DD SW 8270ug/Kg 1700NDBenzyl butyl phthalate 250 04/10/14 DD SW 8270ug/Kg91NDBis(2-chloroethoxy)methane 250 04/10/14 DD SW 8270ug/Kg97NDBis(2-chloroethyl)ether 250 04/10/14 DD SW 8270ug/Kg95NDBis(2-chloroisopropyl)ether 250 04/10/14 DD SW 8270ug/Kg 198NDBis(2-ethylhexyl)phthalate 250 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/10/14 DD SW 8270ug/Kg270NDChrysene 250 04/10/14 DD SW 8270ug/Kg120NDDibenz(a,h)anthracene 250 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 250 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/10/14 DD SW 8270ug/Kg94NDDi-n-octylphthalate 250 04/10/14 DD SW 8270ug/Kg91NDFluoranthene 250 04/10/14 DD SW 8270ug/Kg110NDFluorene 250 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/10/14 DD SW 8270ug/Kg120NDIsophorone 250 04/10/14 DD SW 8270ug/Kg98NDNaphthalene 250 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 250 04/10/14 DD SW 8270ug/Kg99NDN-Nitrosodi-n-propylamine 250 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 250 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 250 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 250 04/10/14 DD SW 8270ug/Kg100NDPhenol 250 04/10/14 DD SW 8270ug/Kg110NDPyrene 250 04/10/14 DD SW 8270ug/Kg120NDPyridine 250 04/10/14 DD SW 8270ug/Kg86

QA/QC Surrogates80% 2,4,6-Tribromophenol 04/10/14 DD 30 - 130 %%55% 2-Fluorobiphenyl 04/10/14 DD 30 - 130 %%

Page 5 of 6 Ver 2




LOD/MDL

77% 2-Fluorophenol 04/10/14 DD 30 - 130 %%51% Nitrobenzene-d5 04/10/14 DD 30 - 130 %%82% Phenol-d5 04/10/14 DD 30 - 130 %%56% Terphenyl-d14 04/10/14 DD 30 - 130 %%

Comments:

TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.



Phyllis Shiller, Laboratory DirectorMay 07, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Greg Lawrence, Assistant Lab Director

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

Page 6 of 6 Ver 2

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportMay 07, 2014



SDG I.D.: GBG30363

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 271080, QC Sample No: BG30143 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)

ICP Metals - SoilNC NCAluminum BRL NC11314.7 105 7.3 75 - 125 306310 7310

87.2 88.8Antimony BRL 1.884.5NC 80.6 4.7 75 - 125 301.1 <4.3

89.5 93.2Arsenic BRL 4.198.9NC 94.4 4.7 75 - 125 301.4 1.59

104 109Barium BRL 4.710310.5 97.4 5.6 75 - 125 3017.1 19.0

95.3 98.6Beryllium BRL 3.4103NC 98.6 4.4 75 - 125 300.22 0.22 B

87.8 90.5Cadmium BRL 3.095.1NC 90.2 5.3 75 - 125 30<0.39 <0.43

NC NCCalcium BRL NC1017.30 99.9 1.1 75 - 125 30798 742

97.6 102Chromium BRL 4.41067.50 100 5.8 75 - 125 309.16 9.87

94.4 97.9Cobalt BRL 3.61031.30 97.3 5.7 75 - 125 303.00 2.96

99.7 104Copper BRL 4.21042.10 100 3.9 75 - 125 306.36 6.23

NC NCIron 9.3 NC1212.70 113 6.8 75 - 125 3011100 10800

92.4 95.9Lead BRL 3.798.6NC 95.8 2.9 75 - 125 303.8 4.68

NC NCMagnesium BRL NC1091.50 102 6.6 75 - 125 301310 1330

104 107Manganese BRL 2.810712.1 102 4.8 75 - 125 3065.8 58.3

95.2 98.9Nickel BRL 3.81033.70 98.3 4.7 75 - 125 306.99 7.25

>130 >130Potassium BRL NC1211.70 112 7.7 m75 - 125 30474 466

79.1 83.0Selenium BRL 4.885.8NC 80.9 5.9 75 - 125 30<1.6 <1.7

93.9 97.3Silver BRL 3.6103NC 94.0 9.1 75 - 125 30<0.39 <0.43

NC NCSodium BRL NC1221.70 114 6.8 75 - 125 301140 1160

88.7 92.1Thallium BRL 3.898.1NC 91.1 7.4 75 - 125 30<3.5 <3.8

98.8 104Vanadium BRL 5.11061.80 102 3.8 75 - 125 3016.5 16.2

101 100Zinc BRL 1.098.65.00 93.3 5.5 75 - 125 3018.3 17.4

QA/QC Batch 271124, QC Sample No: BG30354 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)107 92.5Mercury - Soil BRL 14.598.5NC 97.2 1.3 70 - 130 300.13 0.10

Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%.

Comment:

QA/QC Batch 271068, QC Sample No: BG30370 (BG30370)


91.9 93.3Antimony BRL 1.5113NC 113 0.0 75 - 125 30<1.7 <1.7

88.4 89.6Arsenic BRL 1.394.2NC 92.8 1.5 75 - 125 30<0.7 0.76

101 102Barium BRL 1.010310.2 100 3.0 75 - 125 3021.4 23.7

94.8 95.2Beryllium BRL 0.4101NC 100 1.0 75 - 125 30<0.27 <0.26

87.8 88.1Cadmium BRL 0.395.9NC 94.8 1.2 75 - 125 30<0.33 <0.33


96.2 96.8Chromium BRL 0.61045.50 100 3.9 75 - 125 307.78 8.22

93.3 93.9Cobalt BRL 0.699.313.1 98.4 0.9 75 - 125 302.92 3.33

99.0 99.1Copper BRL 0.11051.70 102 2.9 75 - 125 309.10 9.26

NC NCIron 8.4 NC1123.60 110 1.8 75 - 125 309380 9720

90.6 91.6Lead BRL 1.194.9NC 92.6 2.5 75 - 125 302.2 2.94

Page 1 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

NC NCMagnesium BRL NC10327.0 99.6 3.4 75 - 125 302270 2980

109 94.9Manganese BRL 13.810327.1 101 2.0 75 - 125 30201 264

92.8 93.6Nickel BRL 0.999.84.70 98.2 1.6 75 - 125 307.62 7.27


77.4 77.7Selenium BRL 0.482.8NC 81.4 1.7 75 - 125 30<1.3 <1.3

92.9 93.3Silver BRL 0.496.4NC 95.1 1.4 75 - 125 30<0.33 <0.33

129 129Sodium BRL 0.0117NC 115 1.7 m75 - 125 30124 117

88.7 89.3Thallium BRL 0.794.6NC 94.9 0.3 75 - 125 30<1.3 <1.3

100 98.0Vanadium BRL 2.010320.8 103 0.0 75 - 125 3012.5 15.4

87.9 89.8Zinc BRL 2.194.817.4 92.8 2.1 75 - 125 3014.7 17.5

QA/QC Batch 271125, QC Sample No: BG30370 (BG30370)104 101Mercury - Soil BRL 2.996.6NC 92.1 4.8 70 - 130 30<0.07 <0.08


Comment:

m = This parameter is outside laboratory ms/msd specified recovery limits.

Page 2 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportMay 07, 2014



SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 271077, QC Sample No: BG30355 (BG30363, BG30366, BG30368)

Pesticides - Solid107 834,4' -DDD ND 25.395 108 12.8 40 - 140 30

90 714,4' -DDE ND 23.689 90 1.1 40 - 140 30

82 644,4' -DDT ND 24.784 84 0.0 40 - 140 30

92 87a-BHC ND 5.681 93 13.8 40 - 140 30

93 80a-Chlordane ND 15.092 93 1.1 40 - 140 30

86 69Aldrin ND 21.981 73 10.4 40 - 140 30

98 91b-BHC ND 7.497 94 3.1 40 - 140 30

NA NAChlordane ND NCNA NA NC 40 - 140 30

77 71d-BHC ND 8.181 77 5.1 40 - 140 30

93 82Dieldrin ND 12.686 87 1.2 40 - 140 30

94 86Endosulfan I ND 8.983 91 9.2 40 - 140 30

93 80Endosulfan II ND 15.043 65 40.7 r40 - 140 30

88 79Endosulfan sulfate ND 10.860 65 8.0 40 - 140 30

96 85Endrin ND 12.294 93 1.1 40 - 140 30

85 78Endrin aldehyde ND 8.647 70 39.3 r40 - 140 30

103 95Endrin ketone ND 8.187 86 1.2 40 - 140 30

111 103g-BHC ND 7.594 93 1.1 40 - 140 30

99 82g-Chlordane ND 18.899 97 2.0 40 - 140 30

101 82Heptachlor ND 20.8103 99 4.0 40 - 140 30

103 93Heptachlor epoxide ND 10.292 93 1.1 40 - 140 30

121 102Methoxychlor ND 17.088 89 1.1 40 - 140 30

NA NAToxaphene ND NCNA NA NC 40 - 140 30

83 88% DCBP 93 5.886 95 9.9 30 - 150 30

83 81% TCMX 88 2.486 90 4.5 30 - 150 30

Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, LCSD, MS and MSD.

Comment:


Polychlorinated Biphenyls - Solid92 98PCB-1016 ND 6.375 95 23.5 40 - 140 30

PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

92 101PCB-1260 ND 9.399 91 8.4 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30

89 87% DCBP (Surrogate Rec) 87 2.3100 90 10.5 30 - 150 30

92 90% TCMX (Surrogate Rec) 81 2.299 92 7.3 30 - 150 30

Page 3 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 271323, QC Sample No: BG30364 (BG30363, BG30364 (91, 1X) , BG30365, BG30366, BG30367, BG30368, BG30369, BG30370, BG30371 (50X) , BG30372)

Volatiles - Solid101 1041,1,1,2-Tetrachloroethane ND 2.999 101 2.0 70 - 130 30

101 1001,1,1-Trichloroethane ND 1.092 94 2.2 70 - 130 30

92 931,1,2,2-Tetrachloroethane ND 1.190 92 2.2 70 - 130 30


95 971,1-Dichloroethane ND 2.190 97 7.5 70 - 130 30

94 951,1-Dichloroethene ND 1.185 92 7.9 70 - 130 30

100 971,1-Dichloropropene ND 3.092 95 3.2 70 - 130 30

98 981,2,3-Trichlorobenzene ND 0.090 95 5.4 70 - 130 30

95 951,2,3-Trichloropropane ND 0.095 97 2.1 70 - 130 30


102 1011,2,4-Trimethylbenzene ND 1.099 102 3.0 70 - 130 30

93 891,2-Dibromo-3-chloropropane ND 4.497 96 1.0 70 - 130 30

101 1011,2-Dibromoethane ND 0.0100 105 4.9 70 - 130 30

99 1001,2-Dichlorobenzene ND 1.092 94 2.2 70 - 130 30


95 981,2-Dichloropropane ND 3.193 98 5.2 70 - 130 30






97 972-Chlorotoluene ND 0.090 97 7.5 70 - 130 30

84 892-Hexanone ND 5.8121 127 4.8 70 - 130 30

102 1022-Isopropyltoluene ND 0.096 99 3.1 70 - 130 30


101 1044-Methyl-2-pentanone ND 2.9127 133 4.6 l70 - 130 30

67 66Acetone ND 1.575 84 11.3 m70 - 130 30

93 93Acrylonitrile ND 0.091 102 11.4 70 - 130 30

97 98Benzene ND 1.094 97 3.1 70 - 130 30

98 99Bromobenzene ND 1.093 94 1.1 70 - 130 30

96 95Bromochloromethane ND 1.095 96 1.0 70 - 130 30

104 102Bromodichloromethane ND 1.994 95 1.1 70 - 130 30

100 101Bromoform ND 1.097 102 5.0 70 - 130 30

80 81Bromomethane ND 1.294 100 6.2 70 - 130 30

87 89Carbon Disulfide ND 2.387 92 5.6 70 - 130 30

100 102Carbon tetrachloride ND 2.094 94 0.0 70 - 130 30

99 99Chlorobenzene ND 0.097 96 1.0 70 - 130 30

82 83Chloroethane ND 1.290 93 3.3 70 - 130 30

102 102Chloroform ND 0.093 98 5.2 70 - 130 30

77 80Chloromethane ND 3.890 95 5.4 70 - 130 30

96 101cis-1,2-Dichloroethene ND 5.189 99 10.6 70 - 130 30

101 101cis-1,3-Dichloropropene ND 0.096 101 5.1 70 - 130 30

101 101Dibromochloromethane ND 0.0100 101 1.0 70 - 130 30

100 103Dibromomethane ND 3.097 99 2.0 70 - 130 30

72 70Dichlorodifluoromethane ND 2.888 92 4.4 70 - 130 30

99 98Ethylbenzene ND 1.097 95 2.1 70 - 130 30

97 101Hexachlorobutadiene ND 4.088 93 5.5 70 - 130 30

99 101Isopropylbenzene ND 2.092 98 6.3 70 - 130 30

100 99m&p-Xylene ND 1.097 98 1.0 70 - 130 30

Page 4 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

85 88Methyl ethyl ketone ND 3.5105 112 6.5 70 - 130 30

108 106Methyl t-butyl ether (MTBE) ND 1.993 96 3.2 70 - 130 30

90 89Methylene chloride ND 1.186 91 5.6 70 - 130 30

96 99Naphthalene ND 3.198 100 2.0 70 - 130 30

102 101n-Butylbenzene ND 1.098 101 3.0 70 - 130 30

94 95n-Propylbenzene ND 1.196 98 2.1 70 - 130 30

100 105o-Xylene ND 4.995 96 1.0 70 - 130 30

100 101p-Isopropyltoluene ND 1.097 97 0.0 70 - 130 30

97 98sec-Butylbenzene ND 1.091 92 1.1 70 - 130 30

103 104Styrene ND 1.095 97 2.1 70 - 130 30

98 99tert-Butylbenzene ND 1.094 96 2.1 70 - 130 30

98 95Tetrachloroethene ND 3.192 98 6.3 70 - 130 30

97 96Tetrahydrofuran (THF) ND 1.094 101 7.2 70 - 130 30

98 98Toluene ND 0.094 96 2.1 70 - 130 30

94 97trans-1,2-Dichloroethene ND 3.186 92 6.7 70 - 130 30

107 103trans-1,3-Dichloropropene ND 3.894 100 6.2 70 - 130 30

91 92trans-1,4-dichloro-2-butene ND 1.198 100 2.0 70 - 130 30

96 100Trichloroethene ND 4.195 98 3.1 70 - 130 30

62 63Trichlorofluoromethane ND 1.689 95 6.5 m70 - 130 30

99 101Trichlorotrifluoroethane ND 2.093 95 2.1 70 - 130 30

74 76Vinyl chloride ND 2.785 94 10.1 70 - 130 30

102 100% 1,2-dichlorobenzene-d4 102 2.099 97 2.0 70 - 130 30

103 102% Bromofluorobenzene 98 1.0102 100 2.0 70 - 130 30

103 103% Dibromofluoromethane 104 0.099 103 4.0 70 - 130 30

99 98% Toluene-d8 100 1.0101 101 0.0 70 - 130 30

Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%.

Comment:

QA/QC Batch 271082, QC Sample No: BG30364 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369, BG30370)

Semivolatiles - Solid84 881,2,4,5-Tetrachlorobenzene ND 4.770 78 10.8 30 - 130 30



92 981,2-Diphenylhydrazine ND 6.376 85 11.2 30 - 130 30



100 1022,4,5-Trichlorophenol ND 2.081 91 11.6 30 - 130 30


77 942,4-Dichlorophenol ND 19.975 84 11.3 30 - 130 30

45 552,4-Dimethylphenol ND 20.045 50 10.5 30 - 130 30

36 272,4-Dinitrophenol ND 28.618 33 58.8 l,m,r30 - 130 30

93 992,4-Dinitrotoluene ND 6.376 87 13.5 30 - 130 30


91 942-Chloronaphthalene ND 3.277 84 8.7 30 - 130 30

86 902-Chlorophenol ND 4.573 82 11.6 30 - 130 30

85 892-Methylnaphthalene ND 4.672 80 10.5 30 - 130 30

80 792-Methylphenol (o-cresol) ND 1.369 77 11.0 30 - 130 30

114 1192-Nitroaniline ND 4.385 103 19.1 30 - 130 30

75 892-Nitrophenol ND 17.169 79 13.5 30 - 130 30

85 903&4-Methylphenol (m&p-cresol) ND 5.772 81 11.8 30 - 130 30

116 1173,3'-Dichlorobenzidine ND 0.9108 115 6.3 30 - 130 30

93 893-Nitroaniline ND 4.480 91 12.9 30 - 130 30

Page 5 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

96 994,6-Dinitro-2-methylphenol ND 3.152 76 37.5 r30 - 130 30

92 964-Bromophenyl phenyl ether ND 4.379 87 9.6 30 - 130 30

91 984-Chloro-3-methylphenol ND 7.477 87 12.2 30 - 130 30

55 524-Chloroaniline ND 5.654 57 5.4 30 - 130 30

92 944-Chlorophenyl phenyl ether ND 2.275 83 10.1 30 - 130 30

97 994-Nitroaniline ND 2.079 89 11.9 30 - 130 30

103 1034-Nitrophenol ND 0.083 101 19.6 30 - 130 30

86 90Acenaphthene ND 4.572 81 11.8 30 - 130 30

90 92Acenaphthylene ND 2.274 83 11.5 30 - 130 30

88 93Acetophenone ND 5.573 83 12.8 30 - 130 30

81 80Aniline ND 1.273 77 5.3 30 - 130 30

92 96Anthracene ND 4.376 87 13.5 30 - 130 30

93 97Benz(a)anthracene ND 4.278 86 9.8 30 - 130 30

142 135Benzidine ND 5.1174 >200 NC l,m30 - 130 30

81 86Benzo(a)pyrene ND 6.069 77 11.0 30 - 130 30

88 93Benzo(b)fluoranthene ND 5.576 85 11.2 30 - 130 30

93 103Benzo(ghi)perylene ND 10.277 87 12.2 30 - 130 30

92 97Benzo(k)fluoranthene ND 5.374 83 11.5 30 - 130 30

89 98Benzyl butyl phthalate ND 9.683 86 3.6 30 - 130 30

72 87Bis(2-chloroethoxy)methane ND 18.970 76 8.2 30 - 130 30

81 85Bis(2-chloroethyl)ether ND 4.867 76 12.6 30 - 130 30

86 88Bis(2-chloroisopropyl)ether ND 2.370 78 10.8 30 - 130 30

91 99Bis(2-ethylhexyl)phthalate ND 8.483 85 2.4 30 - 130 30

96 99Carbazole ND 3.176 90 16.9 30 - 130 30

92 97Chrysene ND 5.378 87 10.9 30 - 130 30

95 103Dibenz(a,h)anthracene ND 8.178 89 13.2 30 - 130 30

90 95Dibenzofuran ND 5.474 84 12.7 30 - 130 30

92 97Diethyl phthalate ND 5.377 84 8.7 30 - 130 30

90 92Dimethylphthalate ND 2.276 83 8.8 30 - 130 30

89 94Di-n-butylphthalate ND 5.581 86 6.0 30 - 130 30

91 99Di-n-octylphthalate ND 8.481 88 8.3 30 - 130 30

93 96Fluoranthene ND 3.278 87 10.9 30 - 130 30

94 97Fluorene ND 3.176 85 11.2 30 - 130 30

86 93Hexachlorobenzene ND 7.878 84 7.4 30 - 130 30


71 70Hexachlorocyclopentadiene ND 1.454 64 16.9 30 - 130 30

80 83Hexachloroethane ND 3.768 76 11.1 30 - 130 30

94 102Indeno(1,2,3-cd)pyrene ND 8.278 87 10.9 30 - 130 30

77 92Isophorone ND 17.874 82 10.3 30 - 130 30

82 87Naphthalene ND 5.970 78 10.8 30 - 130 30

85 88Nitrobenzene ND 3.570 79 12.1 30 - 130 30

83 86N-Nitrosodimethylamine ND 3.669 76 9.7 30 - 130 30

88 92N-Nitrosodi-n-propylamine ND 4.472 81 11.8 30 - 130 30

98 101N-Nitrosodiphenylamine ND 3.080 90 11.8 30 - 130 30

93 96Pentachloronitrobenzene ND 3.280 86 7.2 30 - 130 30

92 93Pentachlorophenol ND 1.160 75 22.2 30 - 130 30

92 97Phenanthrene ND 5.378 87 10.9 30 - 130 30

89 92Phenol ND 3.374 83 11.5 30 - 130 30

94 97Pyrene ND 3.177 89 14.5 30 - 130 30

70 69Pyridine ND 1.462 65 4.7 30 - 130 30

84 92% 2,4,6-Tribromophenol 80 9.175 77 2.6 30 - 130 30

56 57% 2-Fluorobiphenyl 55 1.847 50 6.2 30 - 130 30

78 82% 2-Fluorophenol 81 5.066 71 7.3 30 - 130 30

Page 6 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

54 55% Nitrobenzene-d5 52 1.844 49 10.8 30 - 130 30

82 85% Phenol-d5 81 3.669 75 8.3 30 - 130 30

64 65% Terphenyl-d14 62 1.653 59 10.7 30 - 130 30

Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%)

Comment:


Pesticides - Solid92 954,4' -DDD ND 3.256 40 - 140 30

96 994,4' -DDE ND 3.189 40 - 140 30

94 984,4' -DDT ND 4.287 40 - 140 30

95 94a-BHC ND 1.182 40 - 140 30

97 97a-Chlordane ND 0.083 40 - 140 30

84 87Aldrin ND 3.579 40 - 140 30

100 98b-BHC ND 2.085 40 - 140 30

92 94Chlordane ND 2.283 40 - 140 30

79 78d-BHC ND 1.367 40 - 140 30

96 97Dieldrin ND 1.086 40 - 140 30

92 94Endosulfan I ND 2.282 40 - 140 30

103 106Endosulfan II ND 2.994 40 - 140 30

73 75Endosulfan sulfate ND 2.759 40 - 140 30

97 97Endrin ND 0.086 40 - 140 30

80 82Endrin aldehyde ND 2.548 40 - 140 30

92 93Endrin ketone ND 1.179 40 - 140 30

94 93g-BHC ND 1.180 40 - 140 30

92 94g-Chlordane ND 2.283 40 - 140 30

88 92Heptachlor ND 4.479 40 - 140 30

96 96Heptachlor epoxide ND 0.085 40 - 140 30

102 106Methoxychlor ND 3.891 40 - 140 30

NA NAToxaphene ND NCNA 40 - 140 30

97 94% DCBP 95 3.194 30 - 150 30

89 86% TCMX 86 3.487 30 - 150 30

Alpha and gamma chlordane were spiked and analyzed instead of technical chlordane. Gamma chlordane recovery is reported in theLCS, MS and MSD.

Comment:



PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

94 79PCB-1260 ND 17.388 81 8.3 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30



QA/QC Batch 271482, QC Sample No: BG30788 (BG30366 (71X) )

Volatiles - Solid99 971,2,3-Trichlorobenzene ND 2.0100 106 5.8 70 - 130 30

Page 7 of 8

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits












99 98Bromobenzene ND 1.0100 102 2.0 70 - 130 30



105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30










Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

May 07, 2014MS Dup - Matrix Spike Duplicate

RPD - Relative Percent Difference

LCS - Laboratory Control SampleLCSD - Laboratory Control Sample Duplicate

NC - No Criteria

Intf - Interference

Page 8 of 8

Sample Criteria Exceedences ReportWednesday, May 07, 2014 Page 1 of 2

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GBG30363 - EBCCriteria: NY: 375, 375RRS, 375RS

RLCriteria

State: NY

HG-SM Mercury 0.180.55 0.06 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 6398.7 0.7 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260MADPR Acetone 5068 54 ug/KgBG30366 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8270SMRDP Phenol 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Pentachlorophenol 800ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800990 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$PCB_SMRDP PCB-1254 100210 36 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR 4,4' -DDT 3.324 2.6 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.34 0.06 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63156 6.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109130 0.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 109

PB-SMDP Lead 63174 7.7 mg/KgBG30368 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Benzene 60ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50

Sample Criteria Exceedences ReportWednesday, May 07, 2014 Page 2 of 2


UnitsCriteria


RLCriteria

State: NY

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

NY Temperature NarrationMay 07, 2014



SDG I.D.: GBG30363

The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)

Page 1 of 1

1

Sarah - Phoenixlabs

From: Sarah - Phoenixlabs [[email protected]]Sent: Wednesday, April 30, 2014 11:10 AMTo: 'Shannon - Phoenixlabs'Subject: Can you take off hold BG30367Attachments: GBG30363-ChainofCustody-1.pdf

Importance: High

Please run per Dominick BG30367 for PCB and Pest. I will scan to COC

mailto:[email protected]

BG31851 - BG31853

Monday, April 21, 2014

Sample ID#s:



Sincerely yours,


If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.









GROUND WATEREBC72 Hour


Laboratory Data

E-MW1

Phoenix ID: BG31851

04/11/140:00

17:36



Analysis ReportApril 21, 2014

Date Time



SDG ID: GBG31851


LOD/MDL

< 0.005Silver 0.005 04/12/14 LK SW6010mg/L0.00062.43Aluminum 0.010 04/12/14 LK SW6010mg/L0.0024

< 0.004Arsenic - LDL 0.004 04/12/14 LK SW6010mg/L0.0010.126Barium 0.010 04/12/14 LK SW6010mg/L0.0003

< 0.001Beryllium 0.001 04/12/14 LK SW6010mg/L0.001110Calcium 0.010 04/12/14 LK SW6010mg/L0.003

< 0.004Cadmium 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt 0.005 04/12/14 LK SW6010mg/L0.00030.004Chromium 0.001 04/12/14 LK SW6010mg/L0.00090.007Copper 0.005 04/12/14 LK SW6010mg/L0.001

< 0.005Silver (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00060.90Aluminum (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0026

< 0.003Arsenic, (Dissolved) 0.003 04/12/14 LK SW6010mg/L0.0010.120Barium (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.0003

< 0.001Beryllium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.001112Calcium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.003

< 0.004Cadmium (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00030.001Chromium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.0010

< 0.005Copper, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.0010.88Iron, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.005

< 0.0002Mercury (Dissolved) 0.0002 04/14/14 RS SW7470mg/L0.0001513.6Potassium (Dissolved) 0.1 04/12/14 LK SW6010mg/L0.131.6Magnesium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0012.89Manganese, (Dissolved) 0.053 04/12/14 LK SW6010mg/L0.011255Sodium (Dissolved) 1.1 04/12/14 LK SW6010mg/L1.1

0.012Nickel, (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead (Dissolved) 0.002 04/12/14 LK SW6010mg/L0.001

Page 1 of 15 Ver 1

E-MW1Phoenix I.D.: BG31851



LOD/MDL

< 0.003Antimony, (Dissolved) 0.003 04/15/14 RS 7010mg/L0.003< 0.004Selenium, (Dissolved) 0.004 04/14/14 E/R 7010mg/L0.002< 0.001Thallium , (Dissolved) 0.001 04/12/14 TH 7010mg/L0.001< 0.01Vanadium, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.001< 0.011Zinc, (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.001

2.89Iron 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury 0.0002 04/14/14 RS SW7470mg/L0.00015

12.9Potassium 0.1 04/12/14 LK SW6010mg/L0.131.2Magnesium 0.01 04/12/14 LK SW6010mg/L0.0012.65Manganese 0.050 04/12/14 LK SW6010mg/L0.010237Sodium 1.0 04/12/14 LK SW6010mg/L1.0

0.014Nickel 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead 0.002 04/12/14 LK SW6010mg/L0.001< 0.003Antimony 0.003 04/15/14 RS 7010mg/L0.0020.009Selenium 0.004 04/16/14 RS 7010mg/L0.002

< 0.002Thallium - LDL 0.002 04/16/14 RS 7010mg/L0.001< 0.010Vanadium 0.010 04/12/14 LK SW6010mg/L0.001< 0.010Zinc 0.010 04/12/14 LK SW6010mg/L0.001

CompletedFiltration 04/11/14 AG 0.45um Filter

CompletedDissolved Mercury Digestion 04/14/14 I/I SW7470CompletedMercury Digestion 04/14/14 I/I SW7470CompletedSemi-Volatile Extraction 04/11/14 e/D/D SW3520CompletedDissolved Metals Preparation 04/11/14 AG SW846-3005CompletedTotal Metals Digestion 04/11/14 AG SW846 - 3050

VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21

Page 2 of 15 Ver 1




LOD/MDL

ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.214.7cis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.234.7Tetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.4524Trichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14

QA/QC Surrogates98% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%

Page 3 of 15 Ver 1




LOD/MDL

102% Bromofluorobenzene 04/12/14 RM 70 - 130 %%95% Dibromofluoromethane 04/12/14 RM 70 - 130 %%98% Toluene-d8 04/12/14 RM 70 - 130 %%

SemivolatilesND1,2,4-Trichlorobenzene 5.0 04/16/14 DD SW 8270ug/L1.5ND1,2-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.4ND1,2-Diphenylhydrazine 5.0 04/16/14 DD SW 8270ug/L1.6ND1,3-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.5ND1,4-Dichlorobenzene 1.0 04/16/14 DD SW 8270ug/L1.5ND2,4,5-Trichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4,6-Trichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dichlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dimethylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dinitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2,4-Dinitrotoluene 5.0 04/16/14 DD SW 8270ug/L2.0ND2,6-Dinitrotoluene 5.0 04/16/14 DD SW 8270ug/L1.6ND2-Chloronaphthalene 5.0 04/16/14 DD SW 8270ug/L1.4ND2-Chlorophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND2-Methylnaphthalene 5.0 04/16/14 DD SW 8270ug/L1.5ND2-Methylphenol (o-cresol) 1.0 04/16/14 DD SW 8270ug/L1.0ND2-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L5.0ND2-Nitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0ND3&4-Methylphenol (m&p-cresol) 1.0 04/16/14 DD SW 8270ug/L1.0ND3,3'-Dichlorobenzidine 5.0 04/16/14 DD SW 8270ug/L2.4ND3-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L5.0ND4,6-Dinitro-2-methylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND4-Bromophenyl phenyl ether 5.0 04/16/14 DD SW 8270ug/L1.5ND4-Chloro-3-methylphenol 1.0 04/16/14 DD SW 8270ug/L1.0ND4-Chloroaniline 3.5 04/16/14 DD SW 8270ug/L2.3ND4-Chlorophenyl phenyl ether 5.0 04/16/14 DD SW 8270ug/L1.7ND4-Nitroaniline 5.0 04/16/14 DD SW 8270ug/L1.7ND4-Nitrophenol 1.0 04/16/14 DD SW 8270ug/L1.0NDAcenaphthene 5.0 04/16/14 DD SW 8270ug/L1.5NDAcetophenone 5.0 04/16/14 DD SW 8270ug/L1.6NDAniline 3.5 04/16/14 DD SW 8270ug/L5.0NDAnthracene 5.0 04/16/14 DD SW 8270ug/L1.6NDBenzidine 10 04/16/14 DD SW 8270ug/L2.9NDBenzoic acid 25 04/16/14 DD SW 8270ug/L10NDBenzyl butyl phthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDBis(2-chloroethoxy)methane 5.0 04/16/14 DD SW 8270ug/L1.4NDBis(2-chloroethyl)ether 1.0 04/16/14 DD SW 8270ug/L1.0NDBis(2-chloroisopropyl)ether 5.0 04/16/14 DD SW 8270ug/L1.4NDCarbazole 25 04/16/14 DD SW 8270ug/L3.8NDDibenzofuran 5.0 04/16/14 DD SW 8270ug/L1.5NDDiethyl phthalate 5.0 04/16/14 DD SW 8270ug/L1.6NDDimethylphthalate 5.0 04/16/14 DD SW 8270ug/L1.6NDDi-n-butylphthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDDi-n-octylphthalate 5.0 04/16/14 DD SW 8270ug/L1.3NDFluoranthene 5.0 04/16/14 DD SW 8270ug/L1.6

Page 4 of 15 Ver 1




LOD/MDL

NDFluorene 5.0 04/16/14 DD SW 8270ug/L1.7NDHexachlorobutadiene 1.0 04/16/14 DD SW 8270ug/L1.8NDHexachlorocyclopentadiene 5.0 04/16/14 DD SW 8270ug/L1.5NDIsophorone 5.0 04/16/14 DD SW 8270ug/L1.4NDNaphthalene 5.0 04/16/14 DD SW 8270ug/L1.4NDNitrobenzene 1.0 04/16/14 DD SW 8270ug/L1.8NDN-Nitrosodimethylamine 1.0 04/16/14 DD SW 8270ug/L1.0NDN-Nitrosodi-n-propylamine 5.0 04/16/14 DD SW 8270ug/L1.6NDN-Nitrosodiphenylamine 5.0 04/16/14 DD SW 8270ug/L1.9NDPhenol 1.0 04/16/14 DD SW 8270ug/L1.6NDPyrene 5.0 04/16/14 DD SW 8270ug/L1.7NDPyridine 10 04/16/14 DD SW 8270ug/L1.2

QA/QC Surrogates90% 2,4,6-Tribromophenol 04/16/14 DD 15 - 110 %%78% 2-Fluorobiphenyl 04/16/14 DD 30 - 130 %%48% 2-Fluorophenol 04/16/14 DD 15 - 110 %%82% Nitrobenzene-d5 04/16/14 DD 30 - 130 %%47% Phenol-d5 04/16/14 DD 15 - 110 %%64% Terphenyl-d14 04/16/14 DD 30 - 130 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 1.5 04/15/14 DD SW8270 (SIM)ug/L1.5NDAcenaphthylene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.100.03Benz(a)anthracene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(a)pyrene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(b)fluoranthene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(ghi)perylene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBenzo(k)fluoranthene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDBis(2-ethylhexyl)phthalate 1.6 04/15/14 DD SW8270 (SIM)ug/L1.40.03Chrysene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDDibenz(a,h)anthracene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDHexachlorobenzene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDHexachloroethane 2.4 04/15/14 DD SW8270 (SIM)ug/L1.5NDIndeno(1,2,3-cd)pyrene 0.02 04/15/14 DD SW8270 (SIM)ug/L0.02NDPentachloronitrobenzene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.10NDPentachlorophenol 0.80 04/15/14 DD SW8270 (SIM)ug/L0.80NDPhenanthrene 0.10 04/15/14 DD SW8270 (SIM)ug/L0.10


Page 5 of 15 Ver 1




LOD/MDL

Comments:


Phyllis Shiller, Laboratory DirectorApril 21, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.


Reviewed and Released by: Bobbi Aloisa, Vice President


Page 6 of 15 Ver 1





Laboratory Data

E-MW2

Phoenix ID: BG31852

04/11/140:00

17:36




Date Time



SDG ID: GBG31851


LOD/MDL

< 0.005Silver 0.005 04/12/14 LK SW6010mg/L0.00063.68Aluminum 0.010 04/12/14 LK SW6010mg/L0.0024

< 0.004Arsenic - LDL 0.004 04/12/14 LK SW6010mg/L0.0010.128Barium 0.010 04/12/14 LK SW6010mg/L0.0003

< 0.001Beryllium 0.001 04/12/14 LK SW6010mg/L0.001124Calcium 0.010 04/12/14 LK SW6010mg/L0.003

< 0.004Cadmium 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt 0.005 04/12/14 LK SW6010mg/L0.00030.008Chromium 0.001 04/12/14 LK SW6010mg/L0.00090.014Copper 0.005 04/12/14 LK SW6010mg/L0.001

< 0.005Silver (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.00060.39Aluminum (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0026

< 0.003Arsenic, (Dissolved) 0.003 04/12/14 LK SW6010mg/L0.0010.100Barium (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.0003

< 0.001Beryllium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.001124Calcium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.003

< 0.004Cadmium (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0002< 0.005Cobalt, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.0003< 0.001Chromium (Dissolved) 0.001 04/12/14 LK SW6010mg/L0.0010< 0.005Copper, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.001

0.18Iron, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury (Dissolved) 0.0002 04/14/14 RS SW7470mg/L0.00015

13.1Potassium (Dissolved) 0.1 04/12/14 LK SW6010mg/L0.130.9Magnesium (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.0010.137Manganese, (Dissolved) 0.005 04/12/14 LK SW6010mg/L0.001247Sodium (Dissolved) 1.1 04/12/14 LK SW6010mg/L1.1

< 0.004Nickel, (Dissolved) 0.004 04/12/14 LK SW6010mg/L0.0005< 0.002Lead (Dissolved) 0.002 04/12/14 LK SW6010mg/L0.001

Page 7 of 15 Ver 1




LOD/MDL

< 0.003Antimony, (Dissolved) 0.003 04/15/14 RS 7010mg/L0.0030.006Selenium, (Dissolved) 0.004 04/14/14 E/R 7010mg/L0.002

< 0.001Thallium , (Dissolved) 0.001 04/12/14 TH 7010mg/L0.001< 0.01Vanadium, (Dissolved) 0.01 04/12/14 LK SW6010mg/L0.001< 0.011Zinc, (Dissolved) 0.011 04/12/14 LK SW6010mg/L0.001

3.89Iron 0.01 04/12/14 LK SW6010mg/L0.005< 0.0002Mercury 0.0002 04/14/14 RS SW7470mg/L0.00015

11.8Potassium 0.1 04/12/14 LK SW6010mg/L0.130.9Magnesium 0.01 04/12/14 LK SW6010mg/L0.0010.229Manganese 0.005 04/12/14 LK SW6010mg/L0.001249Sodium 1.0 04/12/14 LK SW6010mg/L1.0

0.005Nickel 0.004 04/12/14 LK SW6010mg/L0.00050.031Lead 0.002 04/12/14 LK SW6010mg/L0.001

< 0.003Antimony 0.003 04/15/14 RS 7010mg/L0.0020.007Selenium 0.004 04/15/14 E/R 7010mg/L0.001

< 0.002Thallium - LDL 0.002 04/16/14 RS 7010mg/L0.001< 0.010Vanadium 0.010 04/12/14 LK SW6010mg/L0.0010.031Zinc 0.010 04/12/14 LK SW6010mg/L0.001


CompletedDissolved Mercury Digestion 04/14/14 I/I SW7470CompletedMercury Digestion 04/14/14 I/I SW7470CompletedSemi-Volatile Extraction 04/16/14 E/K SW3520CompletedDissolved Metals Preparation 04/11/14 AG SW846-3005CompletedTotal Metals Digestion 04/11/14 AG SW846 - 3050

VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21

Page 8 of 15 Ver 1




LOD/MDL

ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.213.6cis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.233.6Tetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.4520Trichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14

QA/QC Surrogates99% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%

Page 9 of 15 Ver 1




LOD/MDL

98% Bromofluorobenzene 04/12/14 RM 70 - 130 %%96% Dibromofluoromethane 04/12/14 RM 70 - 130 %%101% Toluene-d8 04/12/14 RM 70 - 130 %%

SemivolatilesND1,2,4-Trichlorobenzene 6.3 04/17/14 DD SW 8270ug/L1.9ND1,2-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.8ND1,2-Diphenylhydrazine 6.3 04/17/14 DD SW 8270ug/L2.0ND1,3-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.9ND1,4-Dichlorobenzene 1.3 04/17/14 DD SW 8270ug/L1.9ND2,4,5-Trichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4,6-Trichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dichlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dimethylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dinitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2,4-Dinitrotoluene 6.3 04/17/14 DD SW 8270ug/L2.5ND2,6-Dinitrotoluene 6.3 04/17/14 DD SW 8270ug/L2.0ND2-Chloronaphthalene 6.3 04/17/14 DD SW 8270ug/L1.8ND2-Chlorophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND2-Methylnaphthalene 6.3 04/17/14 DD SW 8270ug/L1.9ND2-Methylphenol (o-cresol) 1.3 04/17/14 DD SW 8270ug/L1.3ND2-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L6.3ND2-Nitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3ND3&4-Methylphenol (m&p-cresol) 1.3 04/17/14 DD SW 8270ug/L1.3ND3,3'-Dichlorobenzidine 6.3 04/17/14 DD SW 8270ug/L3.0ND3-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L6.3ND4,6-Dinitro-2-methylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND4-Bromophenyl phenyl ether 6.3 04/17/14 DD SW 8270ug/L1.8ND4-Chloro-3-methylphenol 1.3 04/17/14 DD SW 8270ug/L1.3ND4-Chloroaniline 4.4 04/17/14 DD SW 8270ug/L2.9ND4-Chlorophenyl phenyl ether 6.3 04/17/14 DD SW 8270ug/L2.1ND4-Nitroaniline 6.3 04/17/14 DD SW 8270ug/L2.1ND4-Nitrophenol 1.3 04/17/14 DD SW 8270ug/L1.3NDAcenaphthene 6.3 04/17/14 DD SW 8270ug/L1.9NDAcetophenone 6.3 04/17/14 DD SW 8270ug/L2.0NDAniline 4.4 04/17/14 DD SW 8270ug/L6.3NDAnthracene 6.3 04/17/14 DD SW 8270ug/L2.1NDBenzidine 5.6 04/17/14 DD SW 8270ug/L3.7NDBenzoic acid 31 04/17/14 DD SW 8270ug/L13NDBenzyl butyl phthalate 6.3 04/17/14 DD SW 8270ug/L1.6NDBis(2-chloroethoxy)methane 6.3 04/17/14 DD SW 8270ug/L1.7NDBis(2-chloroethyl)ether 1.3 04/17/14 DD SW 8270ug/L1.3NDBis(2-chloroisopropyl)ether 6.3 04/17/14 DD SW 8270ug/L1.7NDCarbazole 31 04/17/14 DD SW 8270ug/L4.7NDDibenzofuran 6.3 04/17/14 DD SW 8270ug/L1.8NDDiethyl phthalate 6.3 04/17/14 DD SW 8270ug/L2.0NDDimethylphthalate 6.3 04/17/14 DD SW 8270ug/L1.9NDDi-n-butylphthalate 6.3 04/17/14 DD SW 8270ug/L1.7NDDi-n-octylphthalate 6.3 04/17/14 DD SW 8270ug/L1.6NDFluoranthene 6.3 04/17/14 DD SW 8270ug/L2.0

Page 10 of 15 Ver 1




LOD/MDL

NDFluorene 6.3 04/17/14 DD SW 8270ug/L2.1NDHexachlorocyclopentadiene 6.3 04/17/14 DD SW 8270ug/L1.9NDIsophorone 6.3 04/17/14 DD SW 8270ug/L1.8NDNaphthalene 6.3 04/17/14 DD SW 8270ug/L1.8NDN-Nitrosodimethylamine 1.3 04/17/14 DD SW 8270ug/L1.3NDN-Nitrosodi-n-propylamine 6.3 04/17/14 DD SW 8270ug/L2.0NDN-Nitrosodiphenylamine 6.3 04/17/14 DD SW 8270ug/L2.4NDPhenol 1.3 04/17/14 DD SW 8270ug/L2.0NDPyrene 6.3 04/17/14 DD SW 8270ug/L2.2NDPyridine 13 04/17/14 DD SW 8270ug/L1.5


SemivolatilesND1,2,4,5-Tetrachlorobenzene 1.9 04/17/14 DD SW8270 (SIM)ug/LNDAcenaphthylene 0.13 04/17/14 DD SW8270 (SIM)ug/L0.19Benz(a)anthracene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDBenzo(a)pyrene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.29Benzo(b)fluoranthene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDBenzo(ghi)perylene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.08Benzo(k)fluoranthene 0.03 04/17/14 DD SW8270 (SIM)ug/L4.1Bis(2-ethylhexyl)phthalate 2.0 04/17/14 DD SW8270 (SIM)ug/L

0.29Chrysene 0.03 04/17/14 DD SW8270 (SIM)ug/L0.04Dibenz(a,h)anthracene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDHexachlorobenzene 0.03 04/17/14 DD SW8270 (SIM)ug/LNDHexachlorobutadiene 0 04/17/14 DD SW8270 (SIM)ug/LNDHexachloroethane 3.0 04/17/14 DD SW8270 (SIM)ug/L0.05Indeno(1,2,3-cd)pyrene 0 04/17/14 DD SW8270 (SIM)ug/LNDNitrobenzene 0.04 04/17/14 DD SW8270 (SIM)ug/LNDPentachloronitrobenzene 0.13 04/17/14 DD SW8270 (SIM)ug/LNDPentachlorophenol 1.0 04/17/14 DD SW8270 (SIM)ug/L0.49Phenanthrene 0.13 04/17/14 DD SW8270 (SIM)ug/L


Page 11 of 15 Ver 1




LOD/MDL

Comments:







Page 12 of 15 Ver 1





Laboratory Data

TRIP BLANK

Phoenix ID: BG31853

04/11/140:00

17:36




Date Time



SDG ID: GBG31851


LOD/MDL

VolatilesND1,1,1,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 04/12/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 04/12/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 04/12/14 RM SW8260ug/L0.23ND1,1-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 04/12/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 04/12/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 04/12/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 04/12/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 04/12/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 04/12/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 04/12/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 04/12/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L 10.21ND4-Chlorotoluene 1.0 04/12/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 04/12/14 RM SW8260ug/L0.19

Page 13 of 15 Ver 1

TRIP BLANKPhoenix I.D.: BG31853



LOD/MDL

NDAcetone 5.0 04/12/14 RM SW8260ug/L0.31NDAcrolein 5.0 04/12/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 04/12/14 RM SW8260ug/L0.17NDBenzene 0.70 04/12/14 RM SW8260ug/L0.19NDBromobenzene 1.0 04/12/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 04/12/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 04/12/14 RM SW8260ug/L0.16NDBromoform 5.0 04/12/14 RM SW8260ug/L0.10NDBromomethane 5.0 04/12/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 04/12/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 04/12/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 04/12/14 RM SW8260ug/L0.20NDChloroethane 5.0 04/12/14 RM SW8260ug/L0.24NDChloroform 5.0 04/12/14 RM SW8260ug/L0.22NDChloromethane 5.0 04/12/14 RM SW8260ug/L0.21NDcis-1,2-Dichloroethene 1.0 04/12/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 04/12/14 RM SW8260ug/L0.15NDDibromomethane 1.0 04/12/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 04/12/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 04/12/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 04/12/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 04/12/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 04/12/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 04/12/14 RM SW8260ug/L0.19NDMethylene chloride 3.0 04/12/14 RM SW8260ug/L0.16NDNaphthalene 1.0 04/12/14 RM SW8260ug/L0.19NDn-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 04/12/14 RM SW8260ug/L0.20NDo-Xylene 1.0 04/12/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 04/12/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.22NDStyrene 1.0 04/12/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 04/12/14 RM SW8260ug/L0.23NDTetrachloroethene 1.0 04/12/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 04/12/14 RM SW8260ug/L 10.51NDToluene 1.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 04/12/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 04/12/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 04/12/14 RM SW8260ug/L0.45NDTrichloroethene 1.0 04/12/14 RM SW8260ug/L0.18NDTrichlorofluoromethane 1.0 04/12/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 04/12/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 04/12/14 RM SW8260ug/L0.14

QA/QC Surrogates98% 1,2-dichlorobenzene-d4 04/12/14 RM 70 - 130 %%96% Bromofluorobenzene 04/12/14 RM 70 - 130 %%94% Dibromofluoromethane 04/12/14 RM 70 - 130 %%

Page 14 of 15 Ver 1

TRIP BLANKPhoenix I.D.: BG31853



LOD/MDL

99% Toluene-d8 04/12/14 RM 70 - 130 %%

Comments:

TRIP BLANK INCLUDED.






Page 15 of 15 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

QA/QC ReportApril 21, 2014



SDG I.D.: GBG31851

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 271115, QC Sample No: BG29684 (BG31851, BG31852)113 114Antimony (Dissolved) BRL 0.9109NC 107 1.9<0.003 <0.003

99.6 104Selenium (Dissolved) BRL 4.3101NC 103 2.0<0.004 <0.004

79.6 78.0Thallium (Dissolved) BRL 2.096.0NC 98.2 2.3 75 - 125 20<0.002 <0.002

QA/QC Batch 270936, QC Sample No: BG29684 (BG31851, BG31852)32.2 <30Antimony - Water BRL NC109NC 111 1.8 m75 - 125 20<0.003 <0.003

52.9 52.2Selenium - Water BRL 1.3110NC 107 2.8 m75 - 125 20<0.004 <0.010

78.1 75.0Thallium - Water BRL 4.0108NC 108 0.0 75 - 125 20<0.002 <0.002

QA/QC Batch 271425, QC Sample No: BG31458 (BG31851, BG31852)

ICP Metals - Aqueous93.5 91.9Aluminum BRL 1.799.2NC 98.9 0.3 75 - 125 200.081 0.049

103 104Arsenic BRL 1.0103NC 104 1.0 75 - 125 20<0.004 <0.004

100 101Barium BRL 1.01033.90 102 1.0 75 - 125 200.026 0.025

104 104Beryllium BRL 0.0105NC 104 1.0 75 - 125 20<0.001 <0.001

101 102Cadmium BRL 1.0104NC 104 0.0 75 - 125 20<0.004 <0.001

NC NCCalcium BRL NC1040.80 105 1.0 75 - 125 2012.1 12.0

99.1 100Chromium BRL 0.9101NC 102 1.0 75 - 125 20<0.001 <0.001

104 105Cobalt BRL 1.0107NC 107 0.0 75 - 125 20<0.002 <0.002

100 101Copper BRL 1.0102NC 102 0.0 75 - 125 200.001 <0.005

100 101Iron BRL 1.0104NC 103 1.0 75 - 125 200.024 0.022

100 101Lead BRL 1.0103NC 103 0.0 75 - 125 20<0.002 <0.002

NC NCMagnesium BRL NC1041.50 104 0.0 75 - 125 207.60 7.49

89.7 90.8Manganese BRL 1.21041.30 103 1.0 75 - 125 201.56 1.54

102 103Nickel BRL 1.0105NC 105 0.0 75 - 125 200.001 0.001 B

100 99.9Potassium BRL 0.11010 100 1.0 75 - 125 204.3 4.3

99.2 99.2Silver BRL 0.0100NC 101 1.0 75 - 125 20<0.001 <0.001

NC NCSodium BRL NC1030.20 103 0.0 75 - 125 2060.2 60.3

101 101Vanadium BRL 0.0102NC 103 1.0 75 - 125 20<0.002 <0.002

102 103Zinc BRL 1.0104NC 103 1.0 75 - 125 200.005 0.005

QA/QC Batch 271471, QC Sample No: BG31486 (BG31851, BG31852)105 103Mercury - Water BRL 1.998.3NC 100 1.7 70 - 130 20<0.0002 <0.0002


Comment:


ICP Metals - Dissolved99.3 96.6Aluminum BRL 2.898.753.3 99.4 0.7 r75 - 125 200.11 0.19

105 102Arsenic BRL 2.9102NC 102 0.0 75 - 125 20<0.003 <0.003

100 96.9Barium BRL 3.11061.10 107 0.9 75 - 125 200.092 0.091

103 100Beryllium BRL 3.0103NC 103 0.0 75 - 125 20<0.001 <0.001

99.4 96.0Cadmium BRL 3.5104NC 104 0.0 75 - 125 20<0.004 <0.004

NC NCCalcium BRL NC1051.50 105 0.0 75 - 125 2061.4 60.5

100 96.7Chromium BRL 3.4102NC 102 0.0 75 - 125 20<0.001 <0.001

Page 1 of 6

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG31851

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

104 101Cobalt BRL 2.91079.50 107 0.0 75 - 125 200.011 0.010

103 100Copper BRL 3.0103NC 103 0.0 75 - 125 200.009 0.011

101 97.4Iron BRL 3.61062.90 106 0.0 75 - 125 200.276 0.284

100 96.5Lead BRL 3.6103NC 103 0.0 75 - 125 20<0.002 <0.002

NC NCMagnesium BRL NC1062.00 106 0.0 75 - 125 2015.4 15.1

96.4 93.0Manganese BRL 3.61042.20 104 0.0 75 - 125 201.41 1.38

101 98.4Nickel BRL 2.61050 105 0.0 75 - 125 200.028 0.028

106 102Potassium BRL 3.899.81.80 101 1.2 75 - 125 205.5 5.4

89.3 86.2Silver BRL 3.599.9NC 100 0.1 75 - 125 20<0.005 <0.005


102 99.6Vanadium BRL 2.4104NC 104 0.0 75 - 125 20<0.002 <0.002

102 98.7Zinc BRL 3.31013.10 102 1.0 75 - 125 200.033 0.032

m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

Page 2 of 6

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG31851

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


Semivolatiles - Ground Water1,2,4,5-Tetrachlorobenzene ND 106 98 7.8 30 - 130 20

1,2,4-Trichlorobenzene ND 102 95 7.1 30 - 130 20

1,2-Dichlorobenzene ND 92 86 6.7 30 - 130 20

1,2-Diphenylhydrazine ND 105 97 7.9 30 - 130 20



2,4,5-Trichlorophenol ND 115 110 4.4 30 - 130 20

2,4,6-Trichlorophenol ND 116 110 5.3 30 - 130 20

2,4-Dichlorophenol ND 110 103 6.6 30 - 130 20

2,4-Dimethylphenol ND 66 62 6.3 30 - 130 20

2,4-Dinitrophenol ND 115 122 5.9 30 - 130 20

2,4-Dinitrotoluene ND 109 101 7.6 30 - 130 20

2,6-Dinitrotoluene ND 108 101 6.7 30 - 130 20

2-Chloronaphthalene ND 104 99 4.9 30 - 130 20

2-Chlorophenol ND 94 89 5.5 30 - 130 20

2-Methylnaphthalene ND 98 93 5.2 30 - 130 20

2-Methylphenol (o-cresol) ND 87 82 5.9 30 - 130 20

2-Nitroaniline ND 159 158 0.6 l30 - 130 20

2-Nitrophenol ND 108 101 6.7 30 - 130 20

3&4-Methylphenol (m&p-cresol) ND 93 88 5.5 30 - 130 20

3,3'-Dichlorobenzidine ND >200 191 NC l30 - 130 20

3-Nitroaniline ND 186 184 1.1 l30 - 130 20

4,6-Dinitro-2-methylphenol ND 122 123 0.8 30 - 130 20

4-Bromophenyl phenyl ether ND 108 100 7.7 30 - 130 20

4-Chloro-3-methylphenol ND 114 108 5.4 30 - 130 20

4-Chloroaniline ND 81 76 6.4 30 - 130 20

4-Chlorophenyl phenyl ether ND 111 103 7.5 30 - 130 20

4-Nitroaniline ND 113 108 4.5 30 - 130 20

4-Nitrophenol ND 120 119 0.8 15 - 130 20

Acenaphthene ND 101 94 7.2 30 - 130 20

Acenaphthylene ND 100 96 4.1 30 - 130 20

Acetophenone ND 100 95 5.1 30 - 130 20

Aniline ND 74 70 5.6 30 - 130 20

Anthracene ND 104 100 3.9 30 - 130 20

Benz(a)anthracene ND 105 100 4.9 30 - 130 20

Benzidine ND >200 >200 NC l30 - 130 20

Benzo(a)pyrene ND 96 91 5.3 30 - 130 20

Benzo(b)fluoranthene ND 112 104 7.4 30 - 130 20

Benzo(ghi)perylene ND 102 103 1.0 30 - 130 20

Benzo(k)fluoranthene ND 107 102 4.8 30 - 130 20

Benzoic acid ND 59 66 11.2 30 - 130 20

Page 3 of 6

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG31851

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Benzyl butyl phthalate ND 102 95 7.1 30 - 130 20

Bis(2-chloroethoxy)methane ND 101 94 7.2 30 - 130 20

Bis(2-chloroethyl)ether ND 84 79 6.1 30 - 130 20

Bis(2-chloroisopropyl)ether ND 96 89 7.6 30 - 130 20

Bis(2-ethylhexyl)phthalate ND 113 104 8.3 30 - 130 20

Carbazole ND 153 149 2.6 l30 - 130 20

Chrysene ND 102 97 5.0 30 - 130 20

Dibenz(a,h)anthracene ND 109 108 0.9 30 - 130 20

Dibenzofuran ND 104 98 5.9 30 - 130 20

Diethyl phthalate ND 109 100 8.6 30 - 130 20

Dimethylphthalate ND 106 99 6.8 30 - 130 20

Di-n-butylphthalate ND 112 105 6.5 30 - 130 20

Di-n-octylphthalate ND 110 98 11.5 30 - 130 20

Fluoranthene ND 106 103 2.9 30 - 130 20

Fluorene ND 109 104 4.7 30 - 130 20

Hexachlorobenzene ND 104 95 9.0 30 - 130 20

Hexachlorobutadiene ND 99 91 8.4 30 - 130 20

Hexachlorocyclopentadiene ND 72 68 5.7 30 - 130 20

Hexachloroethane ND 92 86 6.7 30 - 130 20

Indeno(1,2,3-cd)pyrene ND 107 105 1.9 30 - 130 20

Isophorone ND 109 101 7.6 30 - 130 20

Naphthalene ND 99 92 7.3 30 - 130 20

Nitrobenzene ND 96 90 6.5 30 - 130 20

N-Nitrosodimethylamine ND 71 72 1.4 30 - 130 20

N-Nitrosodi-n-propylamine ND 96 94 2.1 30 - 130 20

N-Nitrosodiphenylamine ND 121 113 6.8 30 - 130 20

Pentachloronitrobenzene ND 111 101 9.4 30 - 130 20

Pentachlorophenol ND 150 146 2.7 l30 - 130 20

Phenanthrene ND 107 101 5.8 30 - 130 20

Phenol ND 78 74 5.3 15 - 130 20

Pyrene ND 105 104 1.0 30 - 130 20

Pyridine ND 43 42 2.4 30 - 130 20

% 2,4,6-Tribromophenol 96 110 101 8.5 15 - 110 20

% 2-Fluorobiphenyl 70 97 91 6.4 30 - 130 20

% 2-Fluorophenol 81 71 66 7.3 15 - 110 20

% Nitrobenzene-d5 82 94 89 5.5 30 - 130 20

% Phenol-d5 85 72 69 4.3 15 - 110 20

% Terphenyl-d14 81 110 108 1.8 30 - 130 20


Comment:


Volatiles - Ground Water1,1,1,2-Tetrachloroethane ND 94 96 2.1 70 - 130 30

1,1,1-Trichloroethane ND 90 93 3.3 70 - 130 30

1,1,2,2-Tetrachloroethane ND 87 92 5.6 70 - 130 30

1,1,2-Trichloroethane ND 90 103 13.5 70 - 130 30

1,1-Dichloroethane ND 95 98 3.1 70 - 130 30

1,1-Dichloroethene ND 96 97 1.0 70 - 130 30

1,1-Dichloropropene ND 93 95 2.1 70 - 130 30


1,2,3-Trichloropropane ND 93 98 5.2 70 - 130 30

Page 4 of 6

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG31851

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


1,2,4-Trimethylbenzene ND 103 106 2.9 70 - 130 30

1,2-Dibromo-3-chloropropane ND 83 93 11.4 70 - 130 30

1,2-Dibromoethane ND 89 95 6.5 70 - 130 30


1,2-Dichloroethane ND 86 92 6.7 70 - 130 30

1,2-Dichloropropane ND 93 96 3.2 70 - 130 30

1,3,5-Trimethylbenzene ND 100 100 0.0 70 - 130 30





2-Chlorotoluene ND 101 101 0.0 70 - 130 30

2-Hexanone ND 80 93 15.0 70 - 130 30

2-Isopropyltoluene ND 100 103 3.0 70 - 130 30

4-Chlorotoluene ND 103 102 1.0 70 - 130 30

4-Methyl-2-pentanone ND 74 84 12.7 70 - 130 30

Acetone ND 84 81 3.6 70 - 130 30

Acrolein ND 113 124 9.3 70 - 130 30

Acrylonitrile ND 87 98 11.9 70 - 130 30

Benzene ND 95 99 4.1 70 - 130 30

Bromobenzene ND 98 99 1.0 70 - 130 30

Bromochloromethane ND 91 95 4.3 70 - 130 30

Bromodichloromethane ND 90 93 3.3 70 - 130 30

Bromoform ND 88 97 9.7 70 - 130 30

Bromomethane ND 109 113 3.6 70 - 130 30

Carbon Disulfide ND 98 99 1.0 70 - 130 30

Carbon tetrachloride ND 88 88 0.0 70 - 130 30

Chlorobenzene ND 97 100 3.0 70 - 130 30

Chloroethane ND 105 110 4.7 70 - 130 30

Chloroform ND 90 94 4.3 70 - 130 30

Chloromethane ND 110 118 7.0 70 - 130 30

cis-1,2-Dichloroethene ND 94 100 6.2 70 - 130 30

cis-1,3-Dichloropropene ND 88 91 3.4 70 - 130 30

Dibromochloromethane ND 89 99 10.6 70 - 130 30

Dibromomethane ND 92 96 4.3 70 - 130 30

Dichlorodifluoromethane ND 116 119 2.6 70 - 130 30

Ethylbenzene ND 99 100 1.0 70 - 130 30

Hexachlorobutadiene ND 86 89 3.4 70 - 130 30

Isopropylbenzene ND 103 105 1.9 70 - 130 30

m&p-Xylene ND 99 101 2.0 70 - 130 30

Methyl ethyl ketone ND 71 84 16.8 70 - 130 30

Methyl t-butyl ether (MTBE) ND 86 97 12.0 70 - 130 30

Methylene chloride ND 80 82 2.5 70 - 130 30

Naphthalene ND 104 119 13.5 70 - 130 30

n-Butylbenzene ND 95 98 3.1 70 - 130 30

n-Propylbenzene ND 108 109 0.9 70 - 130 30

o-Xylene ND 99 102 3.0 70 - 130 30

p-Isopropyltoluene ND 94 99 5.2 70 - 130 30

sec-Butylbenzene ND 90 95 5.4 70 - 130 30

Styrene ND 100 102 2.0 70 - 130 30

tert-Butylbenzene ND 98 98 0.0 70 - 130 30

Tetrachloroethene ND 98 100 2.0 70 - 130 30

Page 5 of 6

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG31851

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

Tetrahydrofuran (THF) ND 86 99 14.1 70 - 130 30

Toluene ND 98 98 0.0 70 - 130 30

trans-1,2-Dichloroethene ND 95 96 1.0 70 - 130 30

trans-1,3-Dichloropropene ND 88 91 3.4 70 - 130 30

trans-1,4-dichloro-2-butene ND 94 101 7.2 70 - 130 30

Trichloroethene ND 98 99 1.0 70 - 130 30

Trichlorofluoromethane ND 91 92 1.1 70 - 130 30

Trichlorotrifluoroethane ND 91 89 2.2 70 - 130 30

Vinyl chloride ND 109 113 3.6 70 - 130 30

% 1,2-dichlorobenzene-d4 98 98 99 1.0 70 - 130 30

% Bromofluorobenzene 94 97 101 4.0 70 - 130 30

% Dibromofluoromethane 96 92 94 2.2 70 - 130 30

% Toluene-d8 101 100 98 2.0 70 - 130 30

A blank MS/MSD was analyzed with this batch.


Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.



April 21, 2014MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 6 of 6

Sample Criteria Exceedences ReportMonday, April 21, 2014 Page 1 of 3


UnitsCriteria

GBG31851 - EBCCriteria: NY: GW

RLCriteria

State: NY

$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R Trichloroethene 524 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMF Nitrobenzene 0.4ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.4$DP8270-SIMF Hexachlorobutadiene 0.5ND 1.0 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.5$DP8270-SIMF Benzidine 5ND 10 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.03 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.02 ug/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.12.43 0.010 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.90 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.88 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3DMN-WMDP Manganese, (Dissolved) 0.32.89 0.053 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 20255 1.1 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.32.89 0.01 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3MN-WMDP Manganese 0.32.65 0.050 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20237 1.0 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 20TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31851 NY / TOGS - Water Quality / GA Criteria 0.0005

$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TAGM - Volatile Organics / Groundwater Standards 5$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R Trichloroethene 520 1.0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF Phenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethyl)ether 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Chlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1



UnitsCriteria


RLCriteria

State: NY

$DP8270-SIMF 2-Methylphenol (o-cresol) 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4-Dimethylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Bis(2-chloroethoxy)methane 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4-Dichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Chloro-3-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Hexachlorocyclopentadiene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4,6-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 1$DP8270-SIMF 2,4,5-Trichlorophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 4-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,6-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 3-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 2,4-Dinitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Dibenzofuran 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2,4-Dinitrotoluene 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4-Nitrophenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 5$DP8270-SIMF 2-Nitroaniline 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 4,6-Dinitro-2-methylphenol 1ND 1.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 1$DP8270-SIMF Benzidine 5ND 5.6 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMF 3,3'-Dichlorobenzidine 5ND 6.3 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 5$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.19 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.29 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.0020.08 0.03 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(a)pyrene 0.002ND 0.03 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.0020.05 0 ug/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.002AL-WM Aluminum 0.13.68 0.010 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.1D-NA Sodium (Dissolved) 20247 1.1 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005FE-WMDP Iron 0.33.89 0.01 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.3NA-WM Sodium 20249 1.0 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 20



UnitsCriteria


RLCriteria

State: NY

PB-WM Lead 0.0250.031 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.025TL-WMDP Thallium - LDL 0.0005BRL 0.002 mg/LBG31852 NY / TOGS - Water Quality / GA Criteria 0.0005

$8260DP25R Hexachlorobutadiene 0.5ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.5$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,3-Dichlorobenzene 3ND 5.0 ug/LBG31853 NY / TOGS - Water Quality / GA Criteria 3


NY Temperature NarrationApril 21, 2014



SDG I.D.: GBG31851


Page 1 of 1

BG30363 - BG30372

Wednesday, April 16, 2014

Sample ID#s:



Sincerely yours,










SDG CommentsApril 16, 2014



SDG I.D.: GBG30363




SOLIDEBC72 Hour


Laboratory Data

E-SB1 0-2

Phoenix ID: BG30363

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL


97.5Barium 0.7 04/11/14 LK SW6010mg/Kg0.150.30Beryllium 0.30 04/11/14 LK SW6010mg/Kg0.15

18100Calcium 37 04/11/14 LK SW6010mg/Kg34< 0.37Cadmium 0.37 04/11/14 LK SW6010mg/Kg0.155.30Cobalt 0.37 04/11/14 LK SW6010mg/Kg0.1516.4Chromium 0.37 04/11/14 LK SW6010mg/Kg0.1532.0Copper 0.37 04/11/14 LK SW6010mg/kg0.30

18500Iron 37 04/11/14 LK SW6010mg/Kg B370.55Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.042070Potassium 7 04/11/14 LK SW6010mg/Kg2.99810Magnesium 37 04/11/14 LK SW6010mg/Kg2.2330Manganese 3.7 04/11/14 LK SW6010mg/Kg1.5282Sodium 7 04/11/14 LK SW6010mg/Kg3.213.5Nickel 0.37 04/11/14 LK SW6010mg/Kg0.1598.7Lead 0.7 04/11/14 LK SW6010mg/Kg0.22< 1.9Antimony 1.9 04/11/14 LK SW6010mg/Kg0.74< 1.5Selenium 1.5 04/11/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 04/11/14 LK SW6010mg/Kg1.529.7Vanadium 0.4 04/11/14 LK SW6010mg/Kg0.1577.7Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3792Percent Solid 04/09/14 I E160.3%

CompletedSoil Extraction for PCB 04/09/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/09/14 BB SW3545CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471

Page 1 of 49 Ver 1




LOD/MDL

CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050







Page 2 of 49 Ver 1




LOD/MDL


Page 3 of 49 Ver 1




LOD/MDL




Page 4 of 49 Ver 1




LOD/MDL

ND4-Nitroaniline 1800 04/10/14 DD SW 8270ug/Kg120ND4-Nitrophenol 1800 04/10/14 DD SW 8270ug/Kg160NDAcenaphthene 250 04/10/14 DD SW 8270ug/Kg110NDAcenaphthylene 250 04/10/14 DD SW 8270ug/Kg100NDAcetophenone 250 04/10/14 DD SW 8270ug/Kg110NDAniline 1800 04/10/14 DD SW 8270ug/Kg720NDAnthracene 250 04/10/14 DD SW 8270ug/Kg120160Benz(a)anthracene 250 04/10/14 DD SW 8270ug/Kg120JNDBenzidine 710 04/10/14 DD SW 8270ug/Kg210140Benzo(a)pyrene 250 04/10/14 DD SW 8270ug/Kg120J190Benzo(b)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120JNDBenzo(ghi)perylene 250 04/10/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 250 04/10/14 DD SW 8270ug/Kg120NDBenzoic acid 1800 04/10/14 DD SW 8270ug/Kg 1710NDBenzyl butyl phthalate 250 04/10/14 DD SW 8270ug/Kg92NDBis(2-chloroethoxy)methane 250 04/10/14 DD SW 8270ug/Kg98NDBis(2-chloroethyl)ether 250 04/10/14 DD SW 8270ug/Kg96NDBis(2-chloroisopropyl)ether 250 04/10/14 DD SW 8270ug/Kg 199NDBis(2-ethylhexyl)phthalate 250 04/10/14 DD SW 8270ug/Kg100NDCarbazole 1800 04/10/14 DD SW 8270ug/Kg270160Chrysene 250 04/10/14 DD SW 8270ug/Kg120JNDDibenz(a,h)anthracene 250 04/10/14 DD SW 8270ug/Kg120NDDibenzofuran 250 04/10/14 DD SW 8270ug/Kg100NDDiethyl phthalate 250 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 250 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 250 04/10/14 DD SW 8270ug/Kg95NDDi-n-octylphthalate 250 04/10/14 DD SW 8270ug/Kg92240Fluoranthene 250 04/10/14 DD SW 8270ug/Kg120JNDFluorene 250 04/10/14 DD SW 8270ug/Kg120NDHexachlorobenzene 250 04/10/14 DD SW 8270ug/Kg100NDHexachlorobutadiene 250 04/10/14 DD SW 8270ug/Kg130NDHexachlorocyclopentadiene 250 04/10/14 DD SW 8270ug/Kg110NDHexachloroethane 250 04/10/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 250 04/10/14 DD SW 8270ug/Kg120NDIsophorone 250 04/10/14 DD SW 8270ug/Kg100NDNaphthalene 250 04/10/14 DD SW 8270ug/Kg100NDNitrobenzene 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 250 04/10/14 DD SW 8270ug/Kg100NDN-Nitrosodi-n-propylamine 250 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 250 04/10/14 DD SW 8270ug/Kg140NDPentachloronitrobenzene 250 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 250 04/10/14 DD SW 8270ug/Kg130160Phenanthrene 250 04/10/14 DD SW 8270ug/Kg100JNDPhenol 250 04/10/14 DD SW 8270ug/Kg110240Pyrene 250 04/10/14 DD SW 8270ug/Kg120JNDPyridine 250 04/10/14 DD SW 8270ug/Kg87


Page 5 of 49 Ver 1




LOD/MDL


Comments:









Page 6 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB1 29-31

Phoenix ID: BG30364

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL


20.3Barium 0.7 04/11/14 LK SW6010mg/Kg0.14< 0.29Beryllium 0.29 04/11/14 LK SW6010mg/Kg0.142030Calcium 3.6 04/11/14 LK SW6010mg/Kg3.3

< 0.36Cadmium 0.36 04/11/14 LK SW6010mg/Kg0.142.67Cobalt 0.36 04/11/14 LK SW6010mg/Kg0.146.68Chromium 0.36 04/11/14 LK SW6010mg/Kg0.148.42Copper 0.36 04/11/14 LK SW6010mg/kg0.298230Iron 3.6 04/11/14 LK SW6010mg/Kg B3.6

< 0.08Mercury 0.08 04/10/14 RS SW-7471mg/Kg0.05756Potassium 7 04/11/14 LK SW6010mg/Kg2.8

1960Magnesium 3.6 04/11/14 LK SW6010mg/Kg0.21185Manganese 3.6 04/11/14 LK SW6010mg/Kg1.495Sodium 7 04/11/14 LK SW6010mg/Kg3.1

6.90Nickel 0.36 04/11/14 LK SW6010mg/Kg0.142.3Lead 0.7 04/11/14 LK SW6010mg/Kg0.21


CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG/W SW846 - 3050


Page 7 of 49 Ver 1




LOD/MDL

VolatilesND1,1,1,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.94ND1,1,1-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,1,2-Trichloroethane 5.7 04/11/14 U SW8260ug/Kg0.56ND1,1-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,2,4-Trichlorobenzene 5.7 04/11/14 U SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.82ND1,2-Dibromo-3-chloropropane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dibromoethane 5.7 04/11/14 U SW8260ug/Kg1.5ND1,2-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.63ND1,2-Dichloroethane 5.7 04/11/14 U SW8260ug/Kg0.50ND1,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.81ND1,3,5-Trimethylbenzene 5.7 04/11/14 U SW8260ug/Kg0.76ND1,3-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85ND1,3-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.61ND1,4-Dichlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.90ND2,2-Dichloropropane 5.7 04/11/14 U SW8260ug/Kg0.96ND2-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.92ND2-Hexanone 29 04/11/14 U SW8260ug/Kg2.6ND2-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg 10.79ND4-Chlorotoluene 5.7 04/11/14 U SW8260ug/Kg0.66ND4-Methyl-2-pentanone 29 04/11/14 U SW8260ug/Kg1.4NDAcetone 50 04/11/14 U SW8260ug/Kg5.7NDAcrylonitrile 11 04/11/14 U SW8260ug/Kg3.2NDBenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDBromobenzene 5.7 04/11/14 U SW8260ug/Kg0.74NDBromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.84NDBromodichloromethane 5.7 04/11/14 U SW8260ug/Kg0.71NDBromoform 5.7 04/11/14 U SW8260ug/Kg0.80NDBromomethane 5.7 04/11/14 U SW8260ug/Kg4.4NDCarbon Disulfide 5.7 04/11/14 U SW8260ug/Kg0.93NDCarbon tetrachloride 5.7 04/11/14 U SW8260ug/Kg0.66NDChlorobenzene 5.7 04/11/14 U SW8260ug/Kg0.85NDChloroethane 5.7 04/11/14 U SW8260ug/Kg1.3NDChloroform 5.7 04/11/14 U SW8260ug/Kg1.0NDChloromethane 5.7 04/11/14 U SW8260ug/Kg3.0NDcis-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg0.62NDDibromochloromethane 5.7 04/11/14 U SW8260ug/Kg0.64NDDibromomethane 5.7 04/11/14 U SW8260ug/Kg0.72NDDichlorodifluoromethane 5.7 04/11/14 U SW8260ug/Kg1.5NDEthylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDHexachlorobutadiene 5.7 04/11/14 U SW8260ug/Kg1.2NDIsopropylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1

Page 8 of 49 Ver 1




LOD/MDL

NDm&p-Xylene 5.7 04/11/14 U SW8260ug/Kg2.3NDMethyl Ethyl Ketone 34 04/11/14 U SW8260ug/Kg5.0NDMethyl t-butyl ether (MTBE) 11 04/11/14 U SW8260ug/Kg1.6NDMethylene chloride 5.7 04/11/14 U SW8260ug/Kg0.94NDNaphthalene 5.7 04/11/14 U SW8260ug/Kg1.5NDn-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDn-Propylbenzene 5.7 04/11/14 U SW8260ug/Kg1.0NDo-Xylene 5.7 04/11/14 U SW8260ug/Kg2.2NDp-Isopropyltoluene 5.7 04/11/14 U SW8260ug/Kg0.82NDsec-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg1.1NDStyrene 5.7 04/11/14 U SW8260ug/Kg1.6NDtert-Butylbenzene 5.7 04/11/14 U SW8260ug/Kg0.92NDTetrachloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTetrahydrofuran (THF) 11 04/11/14 U SW8260ug/Kg 15.1NDToluene 5.7 04/11/14 U SW8260ug/Kg0.90NDtrans-1,2-Dichloroethene 5.7 04/11/14 U SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.7 04/11/14 U SW8260ug/Kg1.2NDtrans-1,4-dichloro-2-butene 11 04/11/14 U SW8260ug/Kg11NDTrichloroethene 5.7 04/11/14 U SW8260ug/Kg1.2NDTrichlorofluoromethane 5.7 04/11/14 U SW8260ug/Kg1.3NDTrichlorotrifluoroethane 5.7 04/11/14 U SW8260ug/Kg0.89NDVinyl chloride 5.7 04/11/14 U SW8260ug/Kg1.9


SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 04/10/14 DD SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg96ND1,2-Diphenylhydrazine 240 04/10/14 DD SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND1,4-Dichlorobenzene 240 04/10/14 DD SW 8270ug/Kg100ND2,4,5-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg190ND2,4,6-Trichlorophenol 240 04/10/14 DD SW 8270ug/Kg110ND2,4-Dichlorophenol 240 04/10/14 DD SW 8270ug/Kg120ND2,4-Dimethylphenol 240 04/10/14 DD SW 8270ug/Kg84ND2,4-Dinitrophenol 1700 04/10/14 DD SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg130ND2,6-Dinitrotoluene 240 04/10/14 DD SW 8270ug/Kg110ND2-Chloronaphthalene 240 04/10/14 DD SW 8270ug/Kg97ND2-Chlorophenol 240 04/10/14 DD SW 8270ug/Kg97ND2-Methylnaphthalene 240 04/10/14 DD SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 04/10/14 DD SW 8270ug/Kg160ND2-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg340ND2-Nitrophenol 240 04/10/14 DD SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 240 04/10/14 DD SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 680 04/10/14 DD SW 8270ug/Kg160

Page 9 of 49 Ver 1




LOD/MDL

ND3-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg740ND4,6-Dinitro-2-methylphenol 1700 04/10/14 DD SW 8270ug/Kg370ND4-Bromophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg100ND4-Chloro-3-methylphenol 240 04/10/14 DD SW 8270ug/Kg120ND4-Chloroaniline 680 04/10/14 DD SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 04/10/14 DD SW 8270ug/Kg110ND4-Nitroaniline 1700 04/10/14 DD SW 8270ug/Kg110ND4-Nitrophenol 1700 04/10/14 DD SW 8270ug/Kg150NDAcenaphthene 240 04/10/14 DD SW 8270ug/Kg100NDAcenaphthylene 240 04/10/14 DD SW 8270ug/Kg95NDAcetophenone 240 04/10/14 DD SW 8270ug/Kg110NDAniline 1700 04/10/14 DD SW 8270ug/Kg690NDAnthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenz(a)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDBenzidine 680 04/10/14 DD SW 8270ug/Kg200NDBenzo(a)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 04/10/14 DD SW 8270ug/Kg120NDBenzo(ghi)perylene 240 04/10/14 DD SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDBenzoic acid 1700 04/10/14 DD SW 8270ug/Kg 1680NDBenzyl butyl phthalate 240 04/10/14 DD SW 8270ug/Kg88NDBis(2-chloroethoxy)methane 240 04/10/14 DD SW 8270ug/Kg94NDBis(2-chloroethyl)ether 240 04/10/14 DD SW 8270ug/Kg92NDBis(2-chloroisopropyl)ether 240 04/10/14 DD SW 8270ug/Kg 195NDBis(2-ethylhexyl)phthalate 240 04/10/14 DD SW 8270ug/Kg98NDCarbazole 1700 04/10/14 DD SW 8270ug/Kg260NDChrysene 240 04/10/14 DD SW 8270ug/Kg110NDDibenz(a,h)anthracene 240 04/10/14 DD SW 8270ug/Kg110NDDibenzofuran 240 04/10/14 DD SW 8270ug/Kg99NDDiethyl phthalate 240 04/10/14 DD SW 8270ug/Kg110NDDimethylphthalate 240 04/10/14 DD SW 8270ug/Kg110NDDi-n-butylphthalate 240 04/10/14 DD SW 8270ug/Kg91NDDi-n-octylphthalate 240 04/10/14 DD SW 8270ug/Kg88NDFluoranthene 240 04/10/14 DD SW 8270ug/Kg110NDFluorene 240 04/10/14 DD SW 8270ug/Kg110NDHexachlorobenzene 240 04/10/14 DD SW 8270ug/Kg99NDHexachlorobutadiene 240 04/10/14 DD SW 8270ug/Kg120NDHexachlorocyclopentadiene 240 04/10/14 DD SW 8270ug/Kg100NDHexachloroethane 240 04/10/14 DD SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 04/10/14 DD SW 8270ug/Kg110NDIsophorone 240 04/10/14 DD SW 8270ug/Kg95NDNaphthalene 240 04/10/14 DD SW 8270ug/Kg98NDNitrobenzene 240 04/10/14 DD SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 04/10/14 DD SW 8270ug/Kg96NDN-Nitrosodi-n-propylamine 240 04/10/14 DD SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 04/10/14 DD SW 8270ug/Kg130NDPentachloronitrobenzene 240 04/10/14 DD SW 8270ug/Kg130NDPentachlorophenol 240 04/10/14 DD SW 8270ug/Kg130NDPhenanthrene 240 04/10/14 DD SW 8270ug/Kg97

Page 10 of 49 Ver 1




LOD/MDL

NDPhenol 240 04/10/14 DD SW 8270ug/Kg110NDPyrene 240 04/10/14 DD SW 8270ug/Kg120NDPyridine 240 04/10/14 DD SW 8270ug/Kg84


Comments:









Page 11 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB2 29-31

Phoenix ID: BG30365

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL


22.1Barium 0.7 04/11/14 LK SW6010mg/Kg0.14< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.1411100Calcium 34 04/11/14 LK SW6010mg/Kg31< 0.34Cadmium 0.34 04/11/14 LK SW6010mg/Kg0.142.75Cobalt 0.34 04/11/14 LK SW6010mg/Kg0.147.08Chromium 0.34 04/11/14 LK SW6010mg/Kg0.147.68Copper 0.34 04/11/14 LK SW6010mg/kg0.278800Iron 34 04/11/14 LK SW6010mg/Kg B34


3390Magnesium 3.4 04/11/14 LK SW6010mg/Kg0.20176Manganese 3.4 04/11/14 LK SW6010mg/Kg1.4137Sodium 7 04/11/14 LK SW6010mg/Kg2.97.56Nickel 0.34 04/11/14 LK SW6010mg/Kg0.1412.1Lead 0.7 04/11/14 LK SW6010mg/Kg0.20< 1.7Antimony 1.7 04/11/14 LK SW6010mg/Kg0.68< 1.4Selenium 1.4 04/11/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 04/11/14 LK SW6010mg/Kg1.415.6Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.1413.5Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3497Percent Solid 04/09/14 I E160.3%



Page 12 of 49 Ver 1




LOD/MDL


Page 13 of 49 Ver 1




LOD/MDL




Page 14 of 49 Ver 1




LOD/MDL


Page 15 of 49 Ver 1




LOD/MDL



Comments:









Page 16 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB6 0-2

Phoenix ID: BG30366

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL


82.3Barium 0.7 04/11/14 LK SW6010mg/Kg0.13< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.1350400Calcium 34 04/11/14 LK SW6010mg/Kg310.44Cadmium 0.34 04/11/14 LK SW6010mg/Kg0.133.71Cobalt 0.34 04/11/14 LK SW6010mg/Kg0.1313.1Chromium 0.34 04/11/14 LK SW6010mg/Kg0.1342.3Copper 0.34 04/11/14 LK SW6010mg/kg0.27

14800Iron 34 04/11/14 LK SW6010mg/Kg B340.34Mercury 0.06 04/10/14 RS SW-7471mg/Kg0.04966Potassium 7 04/11/14 LK SW6010mg/Kg2.6

12000Magnesium 34 04/11/14 LK SW6010mg/Kg2.0209Manganese 3.4 04/11/14 LK SW6010mg/Kg1.3251Sodium 7 04/11/14 LK SW6010mg/Kg2.914.0Nickel 0.34 04/11/14 LK SW6010mg/Kg0.13156Lead 6.7 04/11/14 LK SW6010mg/Kg2.0

< 3.0Antimony 3.0 04/11/14 LK SW6010mg/Kg3.0< 1.3Selenium 1.3 04/11/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 04/11/14 LK SW6010mg/Kg1.328.7Vanadium 0.3 04/11/14 LK SW6010mg/Kg0.13130Zinc 0.7 04/11/14 LK SW6010mg/Kg0.3491Percent Solid 04/09/14 I E160.3%


Page 17 of 49 Ver 1




LOD/MDL



Polychlorinated BiphenylsNDPCB-1016 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1221 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1232 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1242 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1248 36 04/10/14 AW SW 8082ug/Kg36210PCB-1254 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1260 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1262 36 04/10/14 AW SW 8082ug/Kg36NDPCB-1268 36 04/10/14 AW SW 8082ug/Kg36


Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6244,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.3 04/14/14 CE SW8081ug/Kg7.3NDToxaphene 180 04/14/14 CE SW8081ug/Kg180


VolatilesND1,1,1,2-Tetrachloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.88ND1,1,1-Trichloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.76ND1,1,2-Trichloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.53ND1,1-Dichloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.1

Page 18 of 49 Ver 1




LOD/MDL

ND1,1-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.2ND1,1-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichlorobenzene 280 04/11/14 JLI SW8260ug/Kg56ND1,2,3-Trichloropropane 280 04/11/14 JLI SW8260ug/Kg40ND1,2,4-Trichlorobenzene 280 04/11/14 JLI SW8260ug/Kg56ND1,2,4-Trimethylbenzene 280 04/11/14 JLI SW8260ug/Kg41ND1,2-Dibromo-3-chloropropane 280 04/11/14 JLI SW8260ug/Kg76ND1,2-Dibromoethane 5.4 04/11/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg31ND1,2-Dichloroethane 5.4 04/11/14 JLI SW8260ug/Kg0.47ND1,2-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.76ND1,3,5-Trimethylbenzene 280 04/11/14 JLI SW8260ug/Kg37ND1,3-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg42ND1,3-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.57ND1,4-Dichlorobenzene 280 04/11/14 JLI SW8260ug/Kg45ND2,2-Dichloropropane 5.4 04/11/14 JLI SW8260ug/Kg0.90ND2-Chlorotoluene 280 04/11/14 JLI SW8260ug/Kg45ND2-Hexanone 27 04/11/14 JLI SW8260ug/Kg2.4ND2-Isopropyltoluene 280 04/11/14 JLI SW8260ug/Kg 139ND4-Chlorotoluene 280 04/11/14 JLI SW8260ug/Kg33ND4-Methyl-2-pentanone 27 04/11/14 JLI SW8260ug/Kg1.368Acetone 54 04/11/14 JLI SW8260ug/Kg5.4NDAcrylonitrile 11 04/11/14 JLI SW8260ug/Kg3.0NDBenzene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDBromobenzene 280 04/11/14 JLI SW8260ug/Kg37NDBromochloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.79NDBromodichloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.67NDBromoform 5.4 04/11/14 JLI SW8260ug/Kg0.75NDBromomethane 5.4 04/11/14 JLI SW8260ug/Kg4.1NDCarbon Disulfide 5.4 04/11/14 JLI SW8260ug/Kg0.87NDCarbon tetrachloride 5.4 04/11/14 JLI SW8260ug/Kg0.62NDChlorobenzene 5.4 04/11/14 JLI SW8260ug/Kg0.80NDChloroethane 5.4 04/11/14 JLI SW8260ug/Kg1.3NDChloroform 5.4 04/11/14 JLI SW8260ug/Kg0.98NDChloromethane 5.4 04/11/14 JLI SW8260ug/Kg2.8NDcis-1,2-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg0.58NDDibromochloromethane 5.4 04/11/14 JLI SW8260ug/Kg0.60NDDibromomethane 5.4 04/11/14 JLI SW8260ug/Kg0.68NDDichlorodifluoromethane 5.4 04/11/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.4 04/11/14 JLI SW8260ug/Kg0.98NDHexachlorobutadiene 280 04/11/14 JLI SW8260ug/Kg59NDIsopropylbenzene 280 04/11/14 JLI SW8260ug/Kg54NDm&p-Xylene 5.4 04/11/14 JLI SW8260ug/Kg2.1NDMethyl Ethyl Ketone 32 04/11/14 JLI SW8260ug/Kg4.7NDMethyl t-butyl ether (MTBE) 11 04/11/14 JLI SW8260ug/Kg1.5NDMethylene chloride 5.4 04/11/14 JLI SW8260ug/Kg0.88NDNaphthalene 280 04/11/14 JLI SW8260ug/Kg76NDn-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg51

Page 19 of 49 Ver 1




LOD/MDL

NDn-Propylbenzene 280 04/11/14 JLI SW8260ug/Kg51NDo-Xylene 5.4 04/11/14 JLI SW8260ug/Kg2.1NDp-Isopropyltoluene 280 04/11/14 JLI SW8260ug/Kg41NDsec-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg53NDStyrene 5.4 04/11/14 JLI SW8260ug/Kg1.6NDtert-Butylbenzene 280 04/11/14 JLI SW8260ug/Kg45NDTetrachloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 11 04/11/14 JLI SW8260ug/Kg 14.8NDToluene 5.4 04/11/14 JLI SW8260ug/Kg0.85NDtrans-1,2-Dichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 560 04/11/14 JLI SW8260ug/Kg520NDTrichloroethene 5.4 04/11/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.4 04/11/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.4 04/11/14 JLI SW8260ug/Kg0.84NDVinyl chloride 5.4 04/11/14 JLI SW8260ug/Kg1.7

QA/QC Surrogates101% 1,2-dichlorobenzene-d4 04/11/14 JLI 70 - 130 %%97% Bromofluorobenzene 04/11/14 JLI 70 - 130 %%102% Dibromofluoromethane 04/11/14 JLI 70 - 130 %%96% Toluene-d8 04/11/14 JLI 70 - 130 %%


Page 20 of 49 Ver 1




LOD/MDL

ND4-Nitroaniline 8900 04/11/14 DD SW 8270ug/Kg600ND4-Nitrophenol 8900 04/11/14 DD SW 8270ug/Kg810NDAcenaphthene 1300 04/11/14 DD SW 8270ug/Kg540NDAcenaphthylene 1300 04/11/14 DD SW 8270ug/Kg500NDAcetophenone 1300 04/11/14 DD SW 8270ug/Kg560NDAniline 8900 04/11/14 DD SW 8270ug/Kg3600NDAnthracene 1300 04/11/14 DD SW 8270ug/Kg590

1800Benz(a)anthracene 1300 04/11/14 DD SW 8270ug/Kg600NDBenzidine 3600 04/11/14 DD SW 8270ug/Kg1100

1800Benzo(a)pyrene 1300 04/11/14 DD SW 8270ug/Kg5802300Benzo(b)fluoranthene 1300 04/11/14 DD SW 8270ug/Kg610640Benzo(ghi)perylene 1300 04/11/14 DD SW 8270ug/Kg580J990Benzo(k)fluoranthene 1300 04/11/14 DD SW 8270ug/Kg590JNDBenzoic acid 8900 04/11/14 DD SW 8270ug/Kg 13600NDBenzyl butyl phthalate 1300 04/11/14 DD SW 8270ug/Kg460NDBis(2-chloroethoxy)methane 1300 04/11/14 DD SW 8270ug/Kg490NDBis(2-chloroethyl)ether 1300 04/11/14 DD SW 8270ug/Kg480NDBis(2-chloroisopropyl)ether 1300 04/11/14 DD SW 8270ug/Kg 1500NDBis(2-ethylhexyl)phthalate 1300 04/11/14 DD SW 8270ug/Kg510NDCarbazole 8900 04/11/14 DD SW 8270ug/Kg1400

1800Chrysene 1300 04/11/14 DD SW 8270ug/Kg600NDDibenz(a,h)anthracene 1300 04/11/14 DD SW 8270ug/Kg580NDDibenzofuran 1300 04/11/14 DD SW 8270ug/Kg520NDDiethyl phthalate 1300 04/11/14 DD SW 8270ug/Kg560NDDimethylphthalate 1300 04/11/14 DD SW 8270ug/Kg550NDDi-n-butylphthalate 1300 04/11/14 DD SW 8270ug/Kg480NDDi-n-octylphthalate 1300 04/11/14 DD SW 8270ug/Kg460

2400Fluoranthene 1300 04/11/14 DD SW 8270ug/Kg580NDFluorene 1300 04/11/14 DD SW 8270ug/Kg590NDHexachlorobenzene 1300 04/11/14 DD SW 8270ug/Kg520NDHexachlorobutadiene 1300 04/11/14 DD SW 8270ug/Kg650NDHexachlorocyclopentadiene 1300 04/11/14 DD SW 8270ug/Kg550NDHexachloroethane 1300 04/11/14 DD SW 8270ug/Kg540NDIndeno(1,2,3-cd)pyrene 1300 04/11/14 DD SW 8270ug/Kg590NDIsophorone 1300 04/11/14 DD SW 8270ug/Kg500NDNaphthalene 1300 04/11/14 DD SW 8270ug/Kg510NDNitrobenzene 1300 04/11/14 DD SW 8270ug/Kg630NDN-Nitrosodimethylamine 1300 04/11/14 DD SW 8270ug/Kg500NDN-Nitrosodi-n-propylamine 1300 04/11/14 DD SW 8270ug/Kg580NDN-Nitrosodiphenylamine 1300 04/11/14 DD SW 8270ug/Kg690NDPentachloronitrobenzene 1300 04/11/14 DD SW 8270ug/Kg660NDPentachlorophenol 1300 04/11/14 DD SW 8270ug/Kg680

1200Phenanthrene 1300 04/11/14 DD SW 8270ug/Kg510JNDPhenol 1300 04/11/14 DD SW 8270ug/Kg570

2700Pyrene 1300 04/11/14 DD SW 8270ug/Kg610NDPyridine 1300 04/11/14 DD SW 8270ug/Kg440


Page 21 of 49 Ver 1




LOD/MDL


Comments:




Semi-Volatile Comment:Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, a dilution was required resulting in an elevated RL for the semivolatile analysis.

Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.

For Pesticides, due to matrix interference caused by the presence of PCBs in the samples an elevated MDL was reported.







Page 22 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB6 15-17

Phoenix ID: BG30367

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL








Page 23 of 49 Ver 1




LOD/MDL


Page 24 of 49 Ver 1




LOD/MDL




Page 25 of 49 Ver 1




LOD/MDL


Page 26 of 49 Ver 1




LOD/MDL



Comments:










Page 27 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB7 0-2

Phoenix ID: BG30368

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL

< 0.39Silver 0.39 04/11/14 LK SW6010mg/Kg0.2310500Aluminum 39 04/11/14 LK SW6010mg/Kg7.712.2Arsenic 0.8 04/11/14 LK SW6010mg/Kg0.7775.4Barium 0.8 04/11/14 LK SW6010mg/Kg0.150.38Beryllium 0.31 04/11/14 LK SW6010mg/Kg0.15


15100Iron 39 04/11/14 LK SW6010mg/Kg B390.14Mercury 0.07 04/10/14 RS SW-7471mg/Kg0.041230Potassium 8 04/11/14 LK SW6010mg/Kg3.06150Magnesium 39 04/11/14 LK SW6010mg/Kg2.3328Manganese 3.9 04/11/14 LK SW6010mg/Kg1.5

1280Sodium 8 04/11/14 LK SW6010mg/Kg3.38.69Nickel 0.39 04/11/14 LK SW6010mg/Kg0.15174Lead 7.7 04/11/14 LK SW6010mg/Kg2.3



Page 28 of 49 Ver 1




LOD/MDL





Pesticides - SoilND4,4' -DDD 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 04/14/14 CE SW8081ug/Kg2.6ND4,4' -DDT 2.6 04/14/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDAldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDChlordane 22 04/14/14 CE SW8081ug/Kg22NDd-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin 1.8 04/14/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 04/14/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 04/14/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 04/14/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 04/14/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 04/14/14 CE SW8081ug/Kg1.8NDMethoxychlor 18 04/14/14 CE SW8081ug/Kg18NDToxaphene 180 04/14/14 CE SW8081ug/Kg180



Page 29 of 49 Ver 1




LOD/MDL


Page 30 of 49 Ver 1




LOD/MDL




Page 31 of 49 Ver 1




LOD/MDL

ND4-Nitroaniline 3600 04/10/14 DD SW 8270ug/Kg240ND4-Nitrophenol 3600 04/10/14 DD SW 8270ug/Kg330NDAcenaphthene 500 04/10/14 DD SW 8270ug/Kg220NDAcenaphthylene 500 04/10/14 DD SW 8270ug/Kg200NDAcetophenone 500 04/10/14 DD SW 8270ug/Kg220NDAniline 3600 04/10/14 DD SW 8270ug/Kg1500NDAnthracene 500 04/10/14 DD SW 8270ug/Kg240950Benz(a)anthracene 500 04/10/14 DD SW 8270ug/Kg240NDBenzidine 1400 04/10/14 DD SW 8270ug/Kg420790Benzo(a)pyrene 500 04/10/14 DD SW 8270ug/Kg230

1000Benzo(b)fluoranthene 500 04/10/14 DD SW 8270ug/Kg250510Benzo(ghi)perylene 500 04/10/14 DD SW 8270ug/Kg230440Benzo(k)fluoranthene 500 04/10/14 DD SW 8270ug/Kg240JNDBenzoic acid 3600 04/10/14 DD SW 8270ug/Kg 11400NDBenzyl butyl phthalate 500 04/10/14 DD SW 8270ug/Kg190NDBis(2-chloroethoxy)methane 500 04/10/14 DD SW 8270ug/Kg200NDBis(2-chloroethyl)ether 500 04/10/14 DD SW 8270ug/Kg190NDBis(2-chloroisopropyl)ether 500 04/10/14 DD SW 8270ug/Kg 1200NDBis(2-ethylhexyl)phthalate 500 04/10/14 DD SW 8270ug/Kg210NDCarbazole 3600 04/10/14 DD SW 8270ug/Kg550920Chrysene 500 04/10/14 DD SW 8270ug/Kg240NDDibenz(a,h)anthracene 330 04/10/14 DD SW 8270ug/Kg230NDDibenzofuran 500 04/10/14 DD SW 8270ug/Kg210NDDiethyl phthalate 500 04/10/14 DD SW 8270ug/Kg230NDDimethylphthalate 500 04/10/14 DD SW 8270ug/Kg220NDDi-n-butylphthalate 500 04/10/14 DD SW 8270ug/Kg190NDDi-n-octylphthalate 500 04/10/14 DD SW 8270ug/Kg190

1900Fluoranthene 500 04/10/14 DD SW 8270ug/Kg230NDFluorene 500 04/10/14 DD SW 8270ug/Kg240NDHexachlorobenzene 500 04/10/14 DD SW 8270ug/Kg210NDHexachlorobutadiene 500 04/10/14 DD SW 8270ug/Kg260NDHexachlorocyclopentadiene 500 04/10/14 DD SW 8270ug/Kg220NDHexachloroethane 500 04/10/14 DD SW 8270ug/Kg220460Indeno(1,2,3-cd)pyrene 500 04/10/14 DD SW 8270ug/Kg240JNDIsophorone 500 04/10/14 DD SW 8270ug/Kg200NDNaphthalene 500 04/10/14 DD SW 8270ug/Kg210NDNitrobenzene 500 04/10/14 DD SW 8270ug/Kg250NDN-Nitrosodimethylamine 500 04/10/14 DD SW 8270ug/Kg200NDN-Nitrosodi-n-propylamine 500 04/10/14 DD SW 8270ug/Kg230NDN-Nitrosodiphenylamine 500 04/10/14 DD SW 8270ug/Kg280NDPentachloronitrobenzene 500 04/10/14 DD SW 8270ug/Kg270NDPentachlorophenol 500 04/10/14 DD SW 8270ug/Kg270830Phenanthrene 500 04/10/14 DD SW 8270ug/Kg210NDPhenol 330 04/10/14 DD SW 8270ug/Kg230



Page 32 of 49 Ver 1




LOD/MDL


Comments:





Due to a matrix interference and/or the presence of a large amount of non-target material in the sample, an elevated RL was reported for the pesticide analysis.







Page 33 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB7 15-17

Phoenix ID: BG30369

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL








Page 34 of 49 Ver 1




LOD/MDL

VolatilesND1,1,1,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg2.0ND1,1,1-Trichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1,2,2-Tetrachloroethane 12 04/11/14 U SW8260ug/Kg1.7ND1,1,2-Trichloroethane 12 04/11/14 U SW8260ug/Kg1.2ND1,1-Dichloroethane 12 04/11/14 U SW8260ug/Kg2.4ND1,1-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7ND1,1-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,3-Trichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,2,4-Trichlorobenzene 12 04/11/14 U SW8260ug/Kg2.4ND1,2,4-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,2-Dibromo-3-chloropropane 12 04/11/14 U SW8260ug/Kg3.3ND1,2-Dibromoethane 12 04/11/14 U SW8260ug/Kg3.2ND1,2-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichloroethane 12 04/11/14 U SW8260ug/Kg1.1ND1,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.7ND1,3,5-Trimethylbenzene 12 04/11/14 U SW8260ug/Kg1.6ND1,3-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.8ND1,3-Dichloropropane 12 04/11/14 U SW8260ug/Kg1.3ND1,4-Dichlorobenzene 12 04/11/14 U SW8260ug/Kg1.9ND2,2-Dichloropropane 12 04/11/14 U SW8260ug/Kg2.0ND2-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.9ND2-Hexanone 61 04/11/14 U SW8260ug/Kg5.5ND2-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg 11.7ND4-Chlorotoluene 12 04/11/14 U SW8260ug/Kg1.4ND4-Methyl-2-pentanone 61 04/11/14 U SW8260ug/Kg2.9NDAcetone 50 04/11/14 U SW8260ug/Kg12NDAcrylonitrile 24 04/11/14 U SW8260ug/Kg6.8NDBenzene 12 04/11/14 U SW8260ug/Kg2.4NDBromobenzene 12 04/11/14 U SW8260ug/Kg1.6NDBromochloromethane 12 04/11/14 U SW8260ug/Kg1.8NDBromodichloromethane 12 04/11/14 U SW8260ug/Kg1.5NDBromoform 12 04/11/14 U SW8260ug/Kg1.7NDBromomethane 12 04/11/14 U SW8260ug/Kg9.4NDCarbon Disulfide 12 04/11/14 U SW8260ug/Kg2.0NDCarbon tetrachloride 12 04/11/14 U SW8260ug/Kg1.4NDChlorobenzene 12 04/11/14 U SW8260ug/Kg1.8NDChloroethane 12 04/11/14 U SW8260ug/Kg2.8NDChloroform 12 04/11/14 U SW8260ug/Kg2.2NDChloromethane 12 04/11/14 U SW8260ug/Kg6.4NDcis-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.7NDcis-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg1.3NDDibromochloromethane 12 04/11/14 U SW8260ug/Kg1.4NDDibromomethane 12 04/11/14 U SW8260ug/Kg1.5NDDichlorodifluoromethane 12 04/11/14 U SW8260ug/Kg3.2NDEthylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDHexachlorobutadiene 12 04/11/14 U SW8260ug/Kg2.6NDIsopropylbenzene 12 04/11/14 U SW8260ug/Kg2.3

Page 35 of 49 Ver 1




LOD/MDL

NDm&p-Xylene 12 04/11/14 U SW8260ug/Kg4.8NDMethyl Ethyl Ketone 73 04/11/14 U SW8260ug/Kg11NDMethyl t-butyl ether (MTBE) 24 04/11/14 U SW8260ug/Kg3.4NDMethylene chloride 12 04/11/14 U SW8260ug/Kg2.0NDNaphthalene 12 04/11/14 U SW8260ug/Kg3.3NDn-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDn-Propylbenzene 12 04/11/14 U SW8260ug/Kg2.2NDo-Xylene 12 04/11/14 U SW8260ug/Kg4.6NDp-Isopropyltoluene 12 04/11/14 U SW8260ug/Kg1.8NDsec-Butylbenzene 12 04/11/14 U SW8260ug/Kg2.3NDStyrene 12 04/11/14 U SW8260ug/Kg3.5NDtert-Butylbenzene 12 04/11/14 U SW8260ug/Kg1.9NDTetrachloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTetrahydrofuran (THF) 24 04/11/14 U SW8260ug/Kg 111NDToluene 12 04/11/14 U SW8260ug/Kg1.9NDtrans-1,2-Dichloroethene 12 04/11/14 U SW8260ug/Kg2.4NDtrans-1,3-Dichloropropene 12 04/11/14 U SW8260ug/Kg2.5NDtrans-1,4-dichloro-2-butene 24 04/11/14 U SW8260ug/Kg23NDTrichloroethene 12 04/11/14 U SW8260ug/Kg2.6NDTrichlorofluoromethane 12 04/11/14 U SW8260ug/Kg2.7NDTrichlorotrifluoroethane 12 04/11/14 U SW8260ug/Kg1.9NDVinyl chloride 12 04/11/14 U SW8260ug/Kg3.9



Page 36 of 49 Ver 1




LOD/MDL


Page 37 of 49 Ver 1




LOD/MDL



Comments:










Page 38 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

SOIL DUPLICATE 2

Phoenix ID: BG30370

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL

< 0.33Silver 0.33 04/11/14 LK SW6010mg/Kg0.203800Aluminum 33 04/10/14 LK SW6010mg/Kg6.7< 0.7Arsenic 0.7 04/11/14 LK SW6010mg/Kg0.6721.4Barium 0.7 04/11/14 LK SW6010mg/Kg0.13

< 0.27Beryllium 0.27 04/11/14 LK SW6010mg/Kg0.133010Calcium 3.3 04/11/14 LK SW6010mg/Kg3.1

< 0.33Cadmium 0.33 04/11/14 LK SW6010mg/Kg0.132.92Cobalt 0.33 04/11/14 LK SW6010mg/Kg0.137.78Chromium 0.33 04/11/14 LK SW6010mg/Kg0.139.10Copper 0.33 04/11/14 LK SW6010mg/kg0.279380Iron 33 04/10/14 LK SW6010mg/Kg B33


2270Magnesium 3.3 04/11/14 LK SW6010mg/Kg0.20201Manganese 3.3 04/10/14 LK SW6010mg/Kg1.3142Sodium 7 04/11/14 LK SW6010mg/Kg2.97.62Nickel 0.33 04/11/14 LK SW6010mg/Kg0.132.2Lead 0.7 04/11/14 LK SW6010mg/Kg0.20


CompletedSoil Extraction for SVOA 04/09/14 JJ/FV SW3545CompletedMercury Digestion 04/10/14 I/I SW7471CompletedTotal Metals Digest 04/09/14 CB/AG SW846 - 3050


Page 39 of 49 Ver 1

SOIL DUPLICATE 2Phoenix I.D.: BG30370



LOD/MDL


Page 40 of 49 Ver 1




LOD/MDL




Page 41 of 49 Ver 1




LOD/MDL


Page 42 of 49 Ver 1




LOD/MDL



Comments:










Page 43 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

TRIP BLANK HIGH

Phoenix ID: BG30371

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL

100Percent Solid 1 04/08/14 E160.3%

VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29

Page 44 of 49 Ver 1

TRIP BLANK HIGHPhoenix I.D.: BG30371



LOD/MDL

ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81

QA/QC Surrogates105% 1,2-dichlorobenzene-d4 04/10/14 U 70 - 130 %%95% Bromofluorobenzene 04/10/14 U 70 - 130 %%103% Dibromofluoromethane 04/10/14 U 70 - 130 %%

Page 45 of 49 Ver 1




LOD/MDL

101% Toluene-d8 04/10/14 U 70 - 130 %%

Comments:


This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.







Page 46 of 49 Ver 1



SOLIDEBC72 Hour


Laboratory Data

TRIP BLANK LOW

Phoenix ID: BG30372

04/09/140:00

16:26




Date Time



SDG ID: GBG30363


LOD/MDL

100Percent Solid 1 04/08/14 E160.3%CompletedField Extraction 04/08/14 SW5035

VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/11/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/11/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/11/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/11/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/11/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/11/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/11/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg 10.69

Page 47 of 49 Ver 1

TRIP BLANK LOWPhoenix I.D.: BG30372



LOD/MDL

ND4-Chlorotoluene 5.0 04/11/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/11/14 U SW8260ug/Kg1.2NDAcetone 50 04/11/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/11/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/11/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/11/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/11/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/11/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/11/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/11/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/11/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/11/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/11/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/11/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/11/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/11/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/11/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/11/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/11/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/11/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/11/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/11/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/11/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/11/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/11/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/11/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/11/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/11/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/11/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/11/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/11/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/11/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/11/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/11/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/11/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/11/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/11/14 U SW8260ug/Kg1.6

QA/QC Surrogates103% 1,2-dichlorobenzene-d4 04/11/14 U 70 - 130 %%93% Bromofluorobenzene 04/11/14 U 70 - 130 %%

Page 48 of 49 Ver 1




LOD/MDL

91% Dibromofluoromethane 04/11/14 U 70 - 130 %%102% Toluene-d8 04/11/14 U 70 - 130 %%

Comments:








Page 49 of 49 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG30363

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 271080, QC Sample No: BG30143 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)


87.2 88.8Antimony BRL 1.884.5NC 80.6 4.7 75 - 125 301.1 <4.3

89.5 93.2Arsenic BRL 4.198.9NC 94.4 4.7 75 - 125 301.4 1.59

104 109Barium BRL 4.710310.5 97.4 5.6 75 - 125 3017.1 19.0

95.3 98.6Beryllium BRL 3.4103NC 98.6 4.4 75 - 125 300.22 0.22 B

87.8 90.5Cadmium BRL 3.095.1NC 90.2 5.3 75 - 125 30<0.39 <0.43


97.6 102Chromium BRL 4.41067.50 100 5.8 75 - 125 309.16 9.87

94.4 97.9Cobalt BRL 3.61031.30 97.3 5.7 75 - 125 303.00 2.96

99.7 104Copper BRL 4.21042.10 100 3.9 75 - 125 306.36 6.23

NC NCIron 9.3 NC1212.70 113 6.8 75 - 125 3011100 10800

92.4 95.9Lead BRL 3.798.6NC 95.8 2.9 75 - 125 303.8 4.68

NC NCMagnesium BRL NC1091.50 102 6.6 75 - 125 301310 1330

104 107Manganese BRL 2.810712.1 102 4.8 75 - 125 3065.8 58.3

95.2 98.9Nickel BRL 3.81033.70 98.3 4.7 75 - 125 306.99 7.25


79.1 83.0Selenium BRL 4.885.8NC 80.9 5.9 75 - 125 30<1.6 <1.7

93.9 97.3Silver BRL 3.6103NC 94.0 9.1 75 - 125 30<0.39 <0.43


88.7 92.1Thallium BRL 3.898.1NC 91.1 7.4 75 - 125 30<3.5 <3.8

98.8 104Vanadium BRL 5.11061.80 102 3.8 75 - 125 3016.5 16.2

101 100Zinc BRL 1.098.65.00 93.3 5.5 75 - 125 3018.3 17.4

QA/QC Batch 271124, QC Sample No: BG30354 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369)107 92.5Mercury - Soil BRL 14.598.5NC 97.2 1.3 70 - 130 300.13 0.10


Comment:



91.9 93.3Antimony BRL 1.5113NC 113 0.0 75 - 125 30<1.7 <1.7

88.4 89.6Arsenic BRL 1.394.2NC 92.8 1.5 75 - 125 30<0.7 0.76

101 102Barium BRL 1.010310.2 100 3.0 75 - 125 3021.4 23.7

94.8 95.2Beryllium BRL 0.4101NC 100 1.0 75 - 125 30<0.27 <0.26

87.8 88.1Cadmium BRL 0.395.9NC 94.8 1.2 75 - 125 30<0.33 <0.33


96.2 96.8Chromium BRL 0.61045.50 100 3.9 75 - 125 307.78 8.22

93.3 93.9Cobalt BRL 0.699.313.1 98.4 0.9 75 - 125 302.92 3.33

99.0 99.1Copper BRL 0.11051.70 102 2.9 75 - 125 309.10 9.26

NC NCIron 8.4 NC1123.60 110 1.8 75 - 125 309380 9720

90.6 91.6Lead BRL 1.194.9NC 92.6 2.5 75 - 125 302.2 2.94

Page 1 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

NC NCMagnesium BRL NC10327.0 99.6 3.4 75 - 125 302270 2980

109 94.9Manganese BRL 13.810327.1 101 2.0 75 - 125 30201 264

92.8 93.6Nickel BRL 0.999.84.70 98.2 1.6 75 - 125 307.62 7.27


77.4 77.7Selenium BRL 0.482.8NC 81.4 1.7 75 - 125 30<1.3 <1.3

92.9 93.3Silver BRL 0.496.4NC 95.1 1.4 75 - 125 30<0.33 <0.33

129 129Sodium BRL 0.0117NC 115 1.7 m75 - 125 30124 117

88.7 89.3Thallium BRL 0.794.6NC 94.9 0.3 75 - 125 30<1.3 <1.3

100 98.0Vanadium BRL 2.010320.8 103 0.0 75 - 125 3012.5 15.4

87.9 89.8Zinc BRL 2.194.817.4 92.8 2.1 75 - 125 3014.7 17.5

QA/QC Batch 271125, QC Sample No: BG30370 (BG30370)104 101Mercury - Soil BRL 2.996.6NC 92.1 4.8 70 - 130 30<0.07 <0.08


Comment:

m = This parameter is outside laboratory ms/msd specified recovery limits.

Page 2 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits



90 714,4' -DDE ND 23.689 90 1.1 40 - 140 30

82 644,4' -DDT ND 24.784 84 0.0 40 - 140 30

92 87a-BHC ND 5.681 93 13.8 40 - 140 30

93 80a-Chlordane ND 15.092 93 1.1 40 - 140 30

86 69Aldrin ND 21.981 73 10.4 40 - 140 30

98 91b-BHC ND 7.497 94 3.1 40 - 140 30


77 71d-BHC ND 8.181 77 5.1 40 - 140 30

93 82Dieldrin ND 12.686 87 1.2 40 - 140 30

94 86Endosulfan I ND 8.983 91 9.2 40 - 140 30

93 80Endosulfan II ND 15.043 65 40.7 r40 - 140 30


96 85Endrin ND 12.294 93 1.1 40 - 140 30

85 78Endrin aldehyde ND 8.647 70 39.3 r40 - 140 30

103 95Endrin ketone ND 8.187 86 1.2 40 - 140 30

111 103g-BHC ND 7.594 93 1.1 40 - 140 30

99 82g-Chlordane ND 18.899 97 2.0 40 - 140 30

101 82Heptachlor ND 20.8103 99 4.0 40 - 140 30


121 102Methoxychlor ND 17.088 89 1.1 40 - 140 30


83 88% DCBP 93 5.886 95 9.9 30 - 150 30

83 81% TCMX 88 2.486 90 4.5 30 - 150 30


Comment:



PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

92 101PCB-1260 ND 9.399 91 8.4 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30



Page 3 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

QA/QC Batch 271323, QC Sample No: BG30364 (BG30363, BG30364 (91, 1X) , BG30365, BG30366, BG30367, BG30368, BG30369, BG30370, BG30371 (50X) , BG30372)























84 892-Hexanone ND 5.8121 127 4.8 70 - 130 30




67 66Acetone ND 1.575 84 11.3 m70 - 130 30


97 98Benzene ND 1.094 97 3.1 70 - 130 30

98 99Bromobenzene ND 1.093 94 1.1 70 - 130 30



100 101Bromoform ND 1.097 102 5.0 70 - 130 30

80 81Bromomethane ND 1.294 100 6.2 70 - 130 30




82 83Chloroethane ND 1.290 93 3.3 70 - 130 30

102 102Chloroform ND 0.093 98 5.2 70 - 130 30







99 98Ethylbenzene ND 1.097 95 2.1 70 - 130 30



100 99m&p-Xylene ND 1.097 98 1.0 70 - 130 30

Page 4 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits




96 99Naphthalene ND 3.198 100 2.0 70 - 130 30



100 105o-Xylene ND 4.995 96 1.0 70 - 130 30



103 104Styrene ND 1.095 97 2.1 70 - 130 30




98 98Toluene ND 0.094 96 2.1 70 - 130 30





62 63Trichlorofluoromethane ND 1.689 95 6.5 m70 - 130 30






99 98% Toluene-d8 100 1.0101 101 0.0 70 - 130 30


Comment:

QA/QC Batch 271082, QC Sample No: BG30364 (BG30363, BG30364, BG30365, BG30366, BG30367, BG30368, BG30369, BG30370)











36 272,4-Dinitrophenol ND 28.618 33 58.8 l,m,r30 - 130 30




86 902-Chlorophenol ND 4.573 82 11.6 30 - 130 30



114 1192-Nitroaniline ND 4.385 103 19.1 30 - 130 30

75 892-Nitrophenol ND 17.169 79 13.5 30 - 130 30



93 893-Nitroaniline ND 4.480 91 12.9 30 - 130 30

Page 5 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

96 994,6-Dinitro-2-methylphenol ND 3.152 76 37.5 r30 - 130 30





97 994-Nitroaniline ND 2.079 89 11.9 30 - 130 30

103 1034-Nitrophenol ND 0.083 101 19.6 30 - 130 30

86 90Acenaphthene ND 4.572 81 11.8 30 - 130 30


88 93Acetophenone ND 5.573 83 12.8 30 - 130 30

81 80Aniline ND 1.273 77 5.3 30 - 130 30

92 96Anthracene ND 4.376 87 13.5 30 - 130 30


142 135Benzidine ND 5.1174 >200 NC l,m30 - 130 30

81 86Benzo(a)pyrene ND 6.069 77 11.0 30 - 130 30









96 99Carbazole ND 3.176 90 16.9 30 - 130 30

92 97Chrysene ND 5.378 87 10.9 30 - 130 30


90 95Dibenzofuran ND 5.474 84 12.7 30 - 130 30





93 96Fluoranthene ND 3.278 87 10.9 30 - 130 30

94 97Fluorene ND 3.176 85 11.2 30 - 130 30






77 92Isophorone ND 17.874 82 10.3 30 - 130 30

82 87Naphthalene ND 5.970 78 10.8 30 - 130 30

85 88Nitrobenzene ND 3.570 79 12.1 30 - 130 30






92 97Phenanthrene ND 5.378 87 10.9 30 - 130 30

89 92Phenol ND 3.374 83 11.5 30 - 130 30

94 97Pyrene ND 3.177 89 14.5 30 - 130 30

70 69Pyridine ND 1.462 65 4.7 30 - 130 30

84 92% 2,4,6-Tribromophenol 80 9.175 77 2.6 30 - 130 30

56 57% 2-Fluorobiphenyl 55 1.847 50 6.2 30 - 130 30

78 82% 2-Fluorophenol 81 5.066 71 7.3 30 - 130 30

Page 6 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG30363

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits

54 55% Nitrobenzene-d5 52 1.844 49 10.8 30 - 130 30

82 85% Phenol-d5 81 3.669 75 8.3 30 - 130 30

64 65% Terphenyl-d14 62 1.653 59 10.7 30 - 130 30


Comment:


Volatiles - Solid99 971,2,3-Trichlorobenzene ND 2.0100 106 5.8 70 - 130 30












99 98Bromobenzene ND 1.0100 102 2.0 70 - 130 30



105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30










Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.






NC - No Criteria

Intf - Interference

Page 7 of 7

Sample Criteria Exceedences ReportWednesday, April 16, 2014 Page 1 of 2


UnitsCriteria


RLCriteria

State: NY

HG-SM Mercury 0.180.55 0.06 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 6398.7 0.7 mg/KgBG30363 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260MADPR Acetone 5068 54 ug/KgBG30366 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8270SMRDP Phenol 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Pentachlorophenol 800ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10002300 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 800990 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001800 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 1300 ug/KgBG30366 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$PCB_SMRDP PCB-1254 100210 36 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 100$PESTSMDPR 4,4' -DDT 3.324 2.6 ug/KgBG30366 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3HG-SM Mercury 0.180.34 0.06 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63156 6.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109130 0.7 mg/KgBG30366 NY / 375-6.8 Metals / Unrestricted Use Soil 109

PB-SMDP Lead 63174 7.7 mg/KgBG30368 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Benzene 60ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG30371 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50

Sample Criteria Exceedences ReportWednesday, April 16, 2014 Page 2 of 2


UnitsCriteria


RLCriteria

State: NY





SDG I.D.: GBG30363


Page 1 of 1

BG43036

Friday, May 16, 2014

Sample ID#s:



Sincerely yours,













Laboratory Data

E-MW 3

Phoenix ID: BG43036

05/09/140:00

16:47



Analysis ReportMay 16, 2014

Date Time



SDG ID: GBG43036


LOD/MDL

0.001Silver (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.001B0.39Aluminum (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.00260.003Arsenic, (Dissolved) 0.003 05/09/14 LK SW6010mg/L0.001B*0.100Barium (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001

< 0.001Beryllium (Dissolved) 0.001 05/09/14 LK SW6010mg/L0.00139.6Calcium (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.0030.001Cadmium (Dissolved) 0.004 05/09/14 LK SW6010mg/L0.0005B

< 0.005Cobalt, (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.0010.005Chromium (Dissolved) 0.001 05/09/14 LK SW6010mg/L0.0010.003Copper, (Dissolved) 0.005 05/12/14 LK SW6010mg/L0.001B*0.38Iron, (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.01

< 0.0004Mercury (Dissolved) 0.0004 05/12/14 RS SW7470mg/L0.000312.5Potassium (Dissolved) 0.1 05/09/14 LK SW6010mg/L0.18.03Magnesium (Dissolved) 0.01 05/09/14 LK SW6010mg/L0.0010.019Manganese, (Dissolved) 0.005 05/09/14 LK SW6010mg/L0.00187.5Sodium (Dissolved) 1.1 05/09/14 LK SW6010mg/L1.1

< 0.004Nickel, (Dissolved) 0.004 05/09/14 LK SW6010mg/L0.0010.001Lead (Dissolved) 0.002 05/09/14 LK SW6010mg/L0.001B

< 0.003Antimony, (Dissolved) 0.003 05/12/14 RS 7010mg/L0.0030.068Selenium, (Dissolved) 0.004 05/13/14 TH 7010mg/L0.002

< 0.001Thallium , (Dissolved) 0.001 05/12/14 RS 7010mg/L0.0010.007Vanadium, (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001B0.008Zinc, (Dissolved) 0.011 05/09/14 LK SW6010mg/L0.001B


CompletedDissolved Mercury Digestion 05/12/14 I/I SW7470CompletedPCB Extraction (2 Liter) 05/09/14 L SW3510CompletedExtraction for Pest (2 Liter) 05/09/14 L SW3510CompletedSemi-Volatile Extraction 05/09/14 E/X SW3520

Page 1 of 6 Ver 1

E-MW 3Phoenix I.D.: BG43036



LOD/MDL

CompletedDissolved Metals Preparation 05/09/14 AG SW846-3005

PesticidesND4,4' -DDD 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDE 0.14 05/13/14 CE SW8081ug/L0.14ND4,4' -DDT 0.14 05/13/14 CE SW8081ug/L0.14NDa-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDa-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDAlachlor 1.0 05/13/14 CE SW8081ug/L 11.0NDAldrin 0.021 05/13/14 CE SW8081ug/L0.021NDb-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDChlordane 1.4 05/13/14 CE SW8081ug/L1.4NDd-BHC 0.069 05/13/14 CE SW8081ug/L0.069NDDieldrin 0.021 05/13/14 CE SW8081ug/L0.021NDEndosulfan I 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan II 0.14 05/13/14 CE SW8081ug/L0.14NDEndosulfan Sulfate 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin Aldehyde 0.14 05/13/14 CE SW8081ug/L0.14NDEndrin ketone 0.14 05/13/14 CE SW8081ug/L0.14NDg-BHC (Lindane) 0.069 05/13/14 CE SW8081ug/L0.069NDg-chlordane 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor 0.14 05/13/14 CE SW8081ug/L0.14NDHeptachlor epoxide 0.14 05/13/14 CE SW8081ug/L0.14NDMethoxychlor 1.4 05/13/14 CE SW8081ug/L1.4NDToxaphene 3.5 05/13/14 CE SW8081ug/L3.5

QA/QC SurrogatesDiluted Out%DCBP (Surrogate Rec) 05/13/14 CE SW8081%Diluted Out%TCMX (Surrogate Rec) 05/13/14 CE SW8081%

Polychlorinated BiphenylsNDPCB-1016 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1221 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1232 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1242 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1248 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1254 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1260 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1262 0.069 05/12/14 AW 608/ 8082ug/L0.069NDPCB-1268 0.069 05/12/14 AW 608/ 8082ug/L0.069

QA/QC Surrogates53% DCBP 05/12/14 AW 608/ 8082%67% TCMX 05/12/14 AW 608/ 8082%

VolatilesND1,1,1,2-Tetrachloroethane 1.0 05/14/14 RM SW8260ug/L0.19ND1,1,1-Trichloroethane 5.0 05/14/14 RM SW8260ug/L0.19ND1,1,2,2-Tetrachloroethane 1.0 05/14/14 RM SW8260ug/L0.15ND1,1,2-Trichloroethane 1.0 05/14/14 RM SW8260ug/L0.20ND1,1-Dichloroethane 5.0 05/14/14 RM SW8260ug/L0.23

Page 2 of 6 Ver 1




LOD/MDL

ND1,1-Dichloroethene 1.0 05/14/14 RM SW8260ug/L0.24ND1,1-Dichloropropene 1.0 05/14/14 RM SW8260ug/L0.20ND1,2,3-Trichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.20ND1,2,3-Trichloropropane 1.0 05/14/14 RM SW8260ug/L0.21ND1,2,4-Trichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.18ND1,2,4-Trimethylbenzene 1.0 05/14/14 RM SW8260ug/L0.18ND1,2-Dibromo-3-chloropropane 1.0 05/14/14 RM SW8260ug/L0.36ND1,2-Dibromoethane 1.0 05/14/14 RM SW8260ug/L0.20ND1,2-Dichlorobenzene 1.0 05/14/14 RM SW8260ug/L0.16ND1,2-Dichloroethane 2.0 05/14/14 RM SW8260ug/L0.20ND1,2-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.18ND1,3,5-Trimethylbenzene 1.0 05/14/14 RM SW8260ug/L0.21ND1,3-Dichlorobenzene 5.0 05/14/14 RM SW8260ug/L0.19ND1,3-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.22ND1,4-Dichlorobenzene 5.0 05/14/14 RM SW8260ug/L0.19ND2,2-Dichloropropane 1.0 05/14/14 RM SW8260ug/L0.16ND2-Chlorotoluene 1.0 05/14/14 RM SW8260ug/L0.23ND2-Hexanone 1.0 05/14/14 RM SW8260ug/L0.27ND2-Isopropyltoluene 1.0 05/14/14 RM SW8260ug/L 10.21ND4-Chlorotoluene 1.0 05/14/14 RM SW8260ug/L0.16ND4-Methyl-2-pentanone 1.0 05/14/14 RM SW8260ug/L0.192.7Acetone 5.0 05/14/14 RM SW8260ug/L0.31JSNDAcrolein 5.0 05/14/14 RM SW8260ug/L0.95NDAcrylonitrile 5.0 05/14/14 RM SW8260ug/L0.17NDBenzene 0.70 05/14/14 RM SW8260ug/L0.19NDBromobenzene 1.0 05/14/14 RM SW8260ug/L0.20NDBromochloromethane 1.0 05/14/14 RM SW8260ug/L0.22NDBromodichloromethane 1.0 05/14/14 RM SW8260ug/L0.16NDBromoform 5.0 05/14/14 RM SW8260ug/L0.10NDBromomethane 5.0 05/14/14 RM SW8260ug/L0.25NDCarbon Disulfide 1.0 05/14/14 RM SW8260ug/L0.24NDCarbon tetrachloride 1.0 05/14/14 RM SW8260ug/L0.23NDChlorobenzene 5.0 05/14/14 RM SW8260ug/L0.20NDChloroethane 5.0 05/14/14 RM SW8260ug/L0.24NDChloroform 5.0 05/14/14 RM SW8260ug/L0.22NDChloromethane 5.0 05/14/14 RM SW8260ug/L0.21NDcis-1,2-Dichloroethene 1.0 05/14/14 RM SW8260ug/L0.23NDcis-1,3-Dichloropropene 0.40 05/14/14 RM SW8260ug/L0.15NDDibromochloromethane 1.0 05/14/14 RM SW8260ug/L0.15NDDibromomethane 1.0 05/14/14 RM SW8260ug/L0.23NDDichlorodifluoromethane 1.0 05/14/14 RM SW8260ug/L0.26NDEthylbenzene 1.0 05/14/14 RM SW8260ug/L0.19NDHexachlorobutadiene 1.0 05/14/14 RM SW8260ug/L0.13NDIsopropylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDm&p-Xylene 1.0 05/14/14 RM SW8260ug/L0.42NDMethyl ethyl ketone 1.0 05/14/14 RM SW8260ug/L0.50NDMethyl t-butyl ether (MTBE) 1.0 05/14/14 RM SW8260ug/L0.190.38Methylene chloride 3.0 05/14/14 RM SW8260ug/L0.16JSNDNaphthalene 1.0 05/14/14 RM SW8260ug/L0.19

Page 3 of 6 Ver 1




LOD/MDL

NDn-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDn-Propylbenzene 1.0 05/14/14 RM SW8260ug/L0.20NDo-Xylene 1.0 05/14/14 RM SW8260ug/L0.45NDp-Isopropyltoluene 1.0 05/14/14 RM SW8260ug/L0.21NDsec-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.22NDStyrene 1.0 05/14/14 RM SW8260ug/L0.41NDtert-Butylbenzene 1.0 05/14/14 RM SW8260ug/L0.23NDTetrachloroethene 1.0 05/14/14 RM SW8260ug/L0.24NDTetrahydrofuran (THF) 5.0 05/14/14 RM SW8260ug/L 10.51NDToluene 1.0 05/14/14 RM SW8260ug/L0.20NDtrans-1,2-Dichloroethene 5.0 05/14/14 RM SW8260ug/L0.20NDtrans-1,3-Dichloropropene 0.40 05/14/14 RM SW8260ug/L0.14NDtrans-1,4-dichloro-2-butene 1.0 05/14/14 RM SW8260ug/L0.450.32Trichloroethene 1.0 05/14/14 RM SW8260ug/L0.18JNDTrichlorofluoromethane 1.0 05/14/14 RM SW8260ug/L0.23NDTrichlorotrifluoroethane 1.0 05/14/14 RM SW8260ug/L0.23NDVinyl chloride 1.0 05/14/14 RM SW8260ug/L0.14

QA/QC Surrogates98% 1,2-dichlorobenzene-d4 05/14/14 RM 70 - 121 %%94% Bromofluorobenzene 05/14/14 RM 59 - 113 %%98% Dibromofluoromethane 05/14/14 RM 70 - 130 %%99% Toluene-d8 05/14/14 RM 84 - 138 %%

SemivolatilesND1,2,4-Trichlorobenzene 5.0 05/14/14 KCA SW 8270ug/L1.5ND1,2-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.4ND1,2-Diphenylhydrazine 5.0 05/14/14 KCA SW 8270ug/L1.6ND1,3-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.5ND1,4-Dichlorobenzene 1.0 05/14/14 KCA SW 8270ug/L1.5ND2,4,5-Trichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4,6-Trichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dichlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dimethylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dinitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2,4-Dinitrotoluene 5.0 05/14/14 KCA SW 8270ug/L2.0ND2,6-Dinitrotoluene 5.0 05/14/14 KCA SW 8270ug/L1.6ND2-Chloronaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.4ND2-Chlorophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND2-Methylnaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.5ND2-Methylphenol (o-cresol) 1.0 05/14/14 KCA SW 8270ug/L1.0ND2-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L5.0ND2-Nitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND3&4-Methylphenol (m&p-cresol) 1.0 05/14/14 KCA SW 8270ug/L1.0ND3,3'-Dichlorobenzidine 5.0 05/14/14 KCA SW 8270ug/L2.4ND3-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L5.0ND4,6-Dinitro-2-methylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND4-Bromophenyl phenyl ether 5.0 05/14/14 KCA SW 8270ug/L1.5ND4-Chloro-3-methylphenol 1.0 05/14/14 KCA SW 8270ug/L1.0ND4-Chloroaniline 3.5 05/14/14 KCA SW 8270ug/L2.3ND4-Chlorophenyl phenyl ether 5.0 05/14/14 KCA SW 8270ug/L1.7

Page 4 of 6 Ver 1




LOD/MDL

ND4-Nitroaniline 5.0 05/14/14 KCA SW 8270ug/L1.7ND4-Nitrophenol 1.0 05/14/14 KCA SW 8270ug/L1.0NDAcenaphthene 5.0 05/14/14 KCA SW 8270ug/L1.5NDAcetophenone 5.0 05/14/14 KCA SW 8270ug/L1.6NDAniline 3.5 05/14/14 KCA SW 8270ug/L5.0NDAnthracene 5.0 05/14/14 KCA SW 8270ug/L1.6NDBenzidine 4.5 05/14/14 KCA SW 8270ug/L2.9NDBenzoic acid 25 05/14/14 KCA SW 8270ug/L10NDBenzyl butyl phthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDBis(2-chloroethoxy)methane 5.0 05/14/14 KCA SW 8270ug/L1.4NDBis(2-chloroethyl)ether 1.0 05/14/14 KCA SW 8270ug/L1.0NDBis(2-chloroisopropyl)ether 5.0 05/14/14 KCA SW 8270ug/L1.4NDCarbazole 25 05/14/14 KCA SW 8270ug/L3.8NDDibenzofuran 5.0 05/14/14 KCA SW 8270ug/L1.5NDDiethyl phthalate 5.0 05/14/14 KCA SW 8270ug/L1.6NDDimethylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.6NDDi-n-butylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDDi-n-octylphthalate 5.0 05/14/14 KCA SW 8270ug/L1.3NDFluoranthene 5.0 05/14/14 KCA SW 8270ug/L1.6NDFluorene 5.0 05/14/14 KCA SW 8270ug/L1.7NDHexachlorocyclopentadiene 5.0 05/14/14 KCA SW 8270ug/L1.5NDIsophorone 5.0 05/14/14 KCA SW 8270ug/L1.4NDNaphthalene 5.0 05/14/14 KCA SW 8270ug/L1.4NDN-Nitrosodimethylamine 1.0 05/14/14 KCA SW 8270ug/L1.0NDN-Nitrosodi-n-propylamine 5.0 05/14/14 KCA SW 8270ug/L1.6NDN-Nitrosodiphenylamine 5.0 05/14/14 KCA SW 8270ug/L1.9NDPhenol 1.0 05/14/14 KCA SW 8270ug/L1.6NDPyrene 5.0 05/14/14 KCA SW 8270ug/L1.7NDPyridine 10 05/14/14 KCA SW 8270ug/L1.2

QA/QC Surrogates117% 2,4,6-Tribromophenol 05/14/14 KCA 19 - 122 %%77% 2-Fluorobiphenyl 05/14/14 KCA 30 - 115 %%76% 2-Fluorophenol 05/14/14 KCA 25 - 121 %%84% Nitrobenzene-d5 05/14/14 KCA 23 - 120 %%53% Phenol-d5 05/14/14 KCA 24 - 113 %%79% Terphenyl-d14 05/14/14 KCA 18 - 137 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 0.50 05/12/14 KCA SW8270 (SIM)ug/L0.50NDAcenaphthylene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10

0.060Benz(a)anthracene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.020Benzo(a)pyrene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.040Benzo(b)fluoranthene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.0200.020Benzo(ghi)perylene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDBenzo(k)fluoranthene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDBis(2-ethylhexyl)phthalate 1.0 05/12/14 KCA SW8270 (SIM)ug/L1.0

0.050Chrysene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDDibenz(a,h)anthracene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDHexachlorobenzene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDHexachlorobutadiene 0.40 05/12/14 KCA SW8270 (SIM)ug/L0.40

Page 5 of 6 Ver 1




LOD/MDL

NDHexachloroethane 0.50 05/12/14 KCA SW8270 (SIM)ug/L0.50NDIndeno(1,2,3-cd)pyrene 0.020 05/12/14 KCA SW8270 (SIM)ug/L0.020NDNitrobenzene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10NDPentachloronitrobenzene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10NDPentachlorophenol 0.80 05/12/14 KCA SW8270 (SIM)ug/L0.800.23Phenanthrene 0.10 05/12/14 KCA SW8270 (SIM)ug/L0.10

QA/QC Surrogates124% 2,4,6-Tribromophenol 05/12/14 KCA 19 - 122 %% 3

94% 2-Fluorobiphenyl 05/12/14 KCA 30 - 115 %%77% 2-Fluorophenol 05/12/14 KCA 25 - 121 %%91% Nitrobenzene-d5 05/12/14 KCA 23 - 120 %%81% Phenol-d5 05/12/14 KCA 24 - 113 %%88% Terphenyl-d14 05/12/14 KCA 18 - 137 %%

Comments:



Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.3 = This parameter exceeds laboratory specified limits.




Page 6 of 6 Ver 1

Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 1 of 2


UnitsCriteria


RLCriteria

State: NY

$8260DP25R 1,2-Dibromo-3-chloropropane 0.04ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$8260DP25R 1,2-Dibromoethane 0.0006ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.0006$8260DP25R 1,2-Dichloroethane 0.6ND 2.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.6$8260DP25R 1,2,3-Trichloropropane 0.04ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Chrysene 0.0020.050 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.040 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(a)pyrene 0.0020.020 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.060 0.020 ug/LBG43036 NY / TAGM - Semi-Volatiles / Groundwater Standards 0.002$DP8270-SIMR Benzo(b)fluoranthene 0.0020.040 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Chrysene 0.0020.050 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benz(a)anthracene 0.0020.060 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Indeno(1,2,3-cd)pyrene 0.002ND 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DP8270-SIMR Benzo(k)fluoranthene 0.002ND 0.020 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.002$DPPEST_GA Aldrin 0.01ND 0.021 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA a-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA a-BHC 0.01ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.01$DPPEST_GA b-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA b-BHC 0.04ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA d-BHC 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA d-BHC 0.04ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA g-BHC (Lindane) 0.05ND 0.069 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.05$DPPEST_GA g-BHC (Lindane) 0.05ND 0.069 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.05$DPPEST_GA Chlordane 0.1ND 1.4 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Chlordane 0.05ND 1.4 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.05$DPPEST_GA 4,4' -DDD 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA 4,4' -DDE 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA 4,4' -DDT 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Dieldrin 0.01ND 0.021 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Dieldrin 0.004ND 0.021 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.004$DPPEST_GA Endosulfan I 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endosulfan II 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endosulfan Sulfate 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1$DPPEST_GA Endrin 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor 0.04ND 0.14 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.04$DPPEST_GA Heptachlor epoxide 0.01ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.01$DPPEST_GA Heptachlor epoxide 0.03ND 0.14 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.03$DPPEST_GA Alachlor 0.5ND 1.0 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.5$DPPEST_GA Toxaphene 0.06ND 3.5 ug/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.06$DPPEST_GA g-chlordane 0.1ND 0.14 ug/LBG43036 NY / TAGM - Pest/Herb/PCBs / Groundwater Standards 0.1

Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 2 of 2


UnitsCriteria


RLCriteria

State: NY

D-AL Aluminum (Dissolved) 0.10.39 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.1DFE-WMDP Iron, (Dissolved) 0.30.38 0.01 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.3D-NA Sodium (Dissolved) 2087.5 1.1 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 20DSE-WMDP Selenium, (Dissolved) 0.010.068 0.004 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.01DTL-WMDP Thallium , (Dissolved) 0.0005BRL 0.001 mg/LBG43036 NY / TOGS - Water Quality / GA Criteria 0.0005


NY Temperature NarrationMay 16, 2014



SDG I.D.: GBG43036


Page 1 of 1

BG31847 - BG31850

Friday, April 18, 2014

Sample ID#s:



Sincerely yours,











AIREBC72 Hour


DM

Laboratory Data

E-SG2

Phoenix ID: BG31847

04/11/1410:4517:36

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference



Date Time



SDG ID: GBG31847


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.00ND1,1,1-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.007.021,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1534.5 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.891,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO159.28 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.921,3-Dichlorobenzene 0.166 04/15/14 KCA TO155.53 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.44-Ethyltoluene 0.204 04/15/14 KCA TO156.88 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00163Acetone 0.421 04/15/14 KCA TO15387 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.04Benzene 0.313 04/15/14 KCA TO153.32 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00

Page 1 of 12 Ver 1

E-SG2Phoenix I.D.: BG31847


Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.000.08Carbon Tetrachloride 0.040 04/15/14 KCA TO150.503 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.00NDChloroform 0.205 04/15/14 KCA TO15ND 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.000.97Cyclohexane 0.291 04/15/14 KCA TO153.34 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.52Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.57 1.0027.8Ethanol 0.531 04/15/14 KCA TO1552.3 11.003.42Ethyl acetate 0.278 04/15/14 KCA TO1512.3 11.003.6Ethylbenzene 0.230 04/15/14 KCA TO1515.6 1.00

2.26Heptane 0.244 04/15/14 KCA TO159.26 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.001.67Hexane 0.284 04/15/14 KCA TO155.88 1.001.21Isopropylalcohol 0.407 04/15/14 KCA TO152.97 1.000.37Isopropylbenzene 0.204 04/15/14 KCA TO151.82 1.0012.8m,p-Xylene 0.230 04/15/14 KCA TO1555.5 1.008.1Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1523.9 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.36Methylene Chloride 0.288 04/15/14 KCA TO151.25 1.000.5n-Butylbenzene 0.182 04/15/14 KCA TO152.74 11.00

5.32o-Xylene 0.230 04/15/14 KCA TO1523.1 1.001.3Propylene 0.581 04/15/14 KCA TO152.24 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.24Styrene 0.235 04/15/14 KCA TO151.02 1.000.42Tetrachloroethene 0.037 04/15/14 KCA TO152.85 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0011.1Toluene 0.266 04/15/14 KCA TO1541.8 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.00NDTrichloroethene 0.047 04/15/14 KCA TO15ND 0.250.22Trichlorofluoromethane 0.178 04/15/14 KCA TO151.24 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25

QA/QC Surrogates104% Bromofluorobenzene % 04/15/14 KCA TO15104 %

Page 2 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:





RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level

Page 3 of 12 Ver 1



AIREBC72 Hour


DM

Laboratory Data

E-SG3

Phoenix ID: BG31848

04/11/1410:4317:36

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG31847


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.000.651,1,1-Trichloroethane 0.183 04/15/14 KCA TO153.54 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.004.981,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1524.5 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.381,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.78 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.31,3-Dichlorobenzene 0.166 04/15/14 KCA TO151.80 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.114-Ethyltoluene 0.204 04/15/14 KCA TO155.45 11.000.234-Isopropyltoluene 0.182 04/15/14 KCA TO151.26 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00324Acetone 0.421 04/15/14 KCA TO15769 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.002.2Benzene 0.313 04/15/14 KCA TO157.02 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00

Page 4 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.00NDCarbon Tetrachloride 0.040 04/15/14 KCA TO15ND 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.001.77Chloroform 0.205 04/15/14 KCA TO158.64 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.37Cyclohexane 0.291 04/15/14 KCA TO154.71 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.48Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.37 1.0030.8Ethanol 0.531 04/15/14 KCA TO1558.0 11.006.13Ethyl acetate 0.278 04/15/14 KCA TO1522.1 11.002.72Ethylbenzene 0.230 04/15/14 KCA TO1511.8 1.004.23Heptane 0.244 04/15/14 KCA TO1517.3 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.003.8Hexane 0.284 04/15/14 KCA TO1513.4 1.00

1.84Isopropylalcohol 0.407 04/15/14 KCA TO154.52 1.000.26Isopropylbenzene 0.204 04/15/14 KCA TO151.28 1.009.8m,p-Xylene 0.230 04/15/14 KCA TO1542.5 1.00

14.2Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1541.8 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.00NDMethylene Chloride 0.288 04/15/14 KCA TO15ND 1.000.49n-Butylbenzene 0.182 04/15/14 KCA TO152.69 11.003.55o-Xylene 0.230 04/15/14 KCA TO1515.4 1.0013.8Propylene 0.581 04/15/14 KCA TO1523.7 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.33Styrene 0.235 04/15/14 KCA TO151.40 1.000.97Tetrachloroethene 0.037 04/15/14 KCA TO156.57 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0013.3Toluene 0.266 04/15/14 KCA TO1550.1 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.0011.4Trichloroethene 0.047 04/15/14 KCA TO1561.2 0.250.23Trichlorofluoromethane 0.178 04/15/14 KCA TO151.29 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25


Page 5 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 6 of 12 Ver 1



AIREBC72 Hour


DM

Laboratory Data

E-SG4

Phoenix ID: BG31849

04/11/1410:4617:36

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG31847


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.00ND1,1,1-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.004.941,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1524.3 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.341,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.58 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.000.461,3-Dichlorobenzene 0.166 04/15/14 KCA TO152.76 1.00ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.001.224-Ethyltoluene 0.204 04/15/14 KCA TO155.99 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00113Acetone 0.421 04/15/14 KCA TO15268 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.09Benzene 0.313 04/15/14 KCA TO153.48 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00

Page 7 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/15/14 KCA TO15ND 1.000.09Carbon Tetrachloride 0.040 04/15/14 KCA TO150.566 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.00NDChloroform 0.205 04/15/14 KCA TO15ND 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.01Cyclohexane 0.291 04/15/14 KCA TO153.47 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.59Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.92 1.0026.2Ethanol 0.531 04/15/14 KCA TO1549.3 11.002.5Ethyl acetate 0.278 04/15/14 KCA TO159.00 11.00

3.08Ethylbenzene 0.230 04/15/14 KCA TO1513.4 1.001.76Heptane 0.244 04/15/14 KCA TO157.21 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.001.45Hexane 0.284 04/15/14 KCA TO155.11 1.001.97Isopropylalcohol 0.407 04/15/14 KCA TO154.84 1.000.27Isopropylbenzene 0.204 04/15/14 KCA TO151.33 1.0010.8m,p-Xylene 0.230 04/15/14 KCA TO1546.9 1.006.23Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1518.4 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.41Methylene Chloride 0.288 04/15/14 KCA TO151.42 1.000.39n-Butylbenzene 0.182 04/15/14 KCA TO152.14 11.004.23o-Xylene 0.230 04/15/14 KCA TO1518.4 1.001.18Propylene 0.581 04/15/14 KCA TO152.03 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.24Styrene 0.235 04/15/14 KCA TO151.02 1.000.48Tetrachloroethene 0.037 04/15/14 KCA TO153.25 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.009.76Toluene 0.266 04/15/14 KCA TO1536.8 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.00NDTrichloroethene 0.047 04/15/14 KCA TO15ND 0.250.27Trichlorofluoromethane 0.178 04/15/14 KCA TO151.52 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25


Page 8 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 9 of 12 Ver 1



AIREBC72 Hour


DM

Laboratory Data

E-SG5

Phoenix ID: BG31850

04/11/1410:2517:36

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG31847


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 11.000.231,1,1-Trichloroethane 0.183 04/15/14 KCA TO151.25 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/15/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/15/14 KCA TO15ND 1.003.631,2,4-Trimethylbenzene 0.204 04/15/14 KCA TO1517.8 1.00ND1,2-Dibromoethane(EDB) 0.130 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/15/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/15/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/15/14 KCA TO15ND 1.001.281,3,5-Trimethylbenzene 0.204 04/15/14 KCA TO156.29 1.00ND1,3-Butadiene 0.452 04/15/14 KCA TO15ND 1.0011,3-Dichlorobenzene 0.166 04/15/14 KCA TO156.01 1.00

ND1,4-Dichlorobenzene 0.166 04/15/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/15/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 04/15/14 KCA TO15ND 11.000.964-Ethyltoluene 0.204 04/15/14 KCA TO154.72 11.00ND4-Isopropyltoluene 0.182 04/15/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/15/14 KCA TO15ND 1.00257Acetone 0.421 04/15/14 KCA TO15610 1.00NDAcrylonitrile 0.461 04/15/14 KCA TO15ND 1.001.92Benzene 0.313 04/15/14 KCA TO156.13 1.00NDBenzyl chloride 0.193 04/15/14 KCA TO15ND 1.00

Page 10 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 04/15/14 KCA TO15ND 1.00NDBromoform 0.097 04/15/14 KCA TO15ND 1.00NDBromomethane 0.258 04/15/14 KCA TO15ND 1.001.81Carbon Disulfide 0.321 04/15/14 KCA TO155.63 1.00NDCarbon Tetrachloride 0.040 04/15/14 KCA TO15ND 0.25NDChlorobenzene 0.217 04/15/14 KCA TO15ND 1.00NDChloroethane 0.379 04/15/14 KCA TO15ND 1.000.38Chloroform 0.205 04/15/14 KCA TO151.85 1.00NDChloromethane 0.484 04/15/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.001.64Cyclohexane 0.291 04/15/14 KCA TO155.64 1.00NDDibromochloromethane 0.117 04/15/14 KCA TO15ND 1.000.5Dichlorodifluoromethane 0.202 04/15/14 KCA TO152.47 1.00

30.2Ethanol 0.531 04/15/14 KCA TO1556.9 11.004.12Ethyl acetate 0.278 04/15/14 KCA TO1514.8 11.003.25Ethylbenzene 0.230 04/15/14 KCA TO1514.1 1.004.7Heptane 0.244 04/15/14 KCA TO1519.2 1.00NDHexachlorobutadiene 0.094 04/15/14 KCA TO15ND 1.005.25Hexane 0.284 04/15/14 KCA TO1518.5 1.001.57Isopropylalcohol 0.407 04/15/14 KCA TO153.86 1.000.26Isopropylbenzene 0.204 04/15/14 KCA TO151.28 1.0011.1m,p-Xylene 0.230 04/15/14 KCA TO1548.2 1.0010.6Methyl Ethyl Ketone 0.339 04/15/14 KCA TO1531.2 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/15/14 KCA TO15ND 1.000.33Methylene Chloride 0.288 04/15/14 KCA TO151.14 1.000.47n-Butylbenzene 0.182 04/15/14 KCA TO152.58 11.003.9o-Xylene 0.230 04/15/14 KCA TO1516.9 1.00

29.6Propylene 0.581 04/15/14 KCA TO1550.9 11.00NDsec-Butylbenzene 0.182 04/15/14 KCA TO15ND 11.000.36Styrene 0.235 04/15/14 KCA TO151.53 1.004.18Tetrachloroethene 0.037 04/15/14 KCA TO1528.3 0.25NDTetrahydrofuran 0.339 04/15/14 KCA TO15ND 11.0014.9Toluene 0.266 04/15/14 KCA TO1556.1 1.00NDTrans-1,2-Dichloroethene 0.252 04/15/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/15/14 KCA TO15ND 1.0010.2Trichloroethene 0.047 04/15/14 KCA TO1554.8 0.250.24Trichlorofluoromethane 0.178 04/15/14 KCA TO151.35 1.00NDTrichlorotrifluoroethane 0.130 04/15/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/15/14 KCA TO15ND 0.25


Page 11 of 12 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 12 of 12 Ver 1

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD




SDG I.D.: GBG31847

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

QA/QC Batch 271636, QC Sample No: BG32377 (BG31847, BG31848, BG31849, BG31850)

VolatilesND ND1,1,1,2-Tetrachloroethane ND NC121 ND ND 70 - 130 20ND

ND ND1,1,1-Trichloroethane ND NC109 ND ND 70 - 130 20ND

ND ND1,1,2,2-Tetrachloroethane ND NC107 ND ND 70 - 130 20ND


ND ND1,1-Dichloroethane ND NC98 ND ND 70 - 130 20ND

ND ND1,1-Dichloroethene ND NC96 ND ND 70 - 130 20ND

ND ND1,2,4-Trichlorobenzene ND NC111 ND ND 70 - 130 20ND

1.03 11,2,4-Trimethylbenzene ND 3.0107 5.06 4.91 70 - 130 20ND

ND ND1,2-Dibromoethane(EDB) ND NC113 ND ND 70 - 130 20ND

ND ND1,2-Dichlorobenzene ND NC108 ND ND 70 - 130 20ND


ND ND1,2-dichloropropane ND NC109 ND ND 70 - 130 20ND

ND ND1,2-Dichlorotetrafluoroethane ND NC117 ND ND 70 - 130 20ND

ND ND1,3,5-Trimethylbenzene ND NC104 ND ND 70 - 130 20ND

ND ND1,3-Butadiene ND NC102 ND ND 70 - 130 20ND

1.09 1.191,3-Dichlorobenzene ND 8.8109 6.55 7.15 70 - 130 20ND


ND ND1,4-Dioxane ND NC115 ND ND 70 - 130 20ND

ND ND2-Hexanone(MBK) ND NC114 ND ND 70 - 130 20ND

ND ND4-Ethyltoluene ND NC106 ND ND 70 - 130 20ND

ND ND4-Isopropyltoluene ND NC107 ND ND 70 - 130 20ND

ND ND4-Methyl-2-pentanone(MIBK) ND NC119 ND ND 70 - 130 20ND

49.3 58Acetone ND 16.299 117 138 70 - 130 20ND

ND NDAcrylonitrile ND NC105 ND ND 70 - 130 20ND

4.78 5.61Benzene ND 16.0108 15.3 17.9 70 - 130 20ND

ND NDBenzyl chloride ND NC136 ND ND l70 - 130 20ND

ND NDBromodichloromethane ND NC112 ND ND 70 - 130 20ND

ND NDBromoform ND NC126 ND ND 70 - 130 20ND

ND NDBromomethane ND NC100 ND ND 70 - 130 20ND

5.7 6.61Carbon Disulfide ND 14.8100 17.7 20.6 70 - 130 20ND

0.52 0.58Carbon Tetrachloride ND 10.9114 3.27 3.65 70 - 130 20ND

ND NDChlorobenzene ND NC104 ND ND 70 - 130 20ND

ND NDChloroethane ND NC100 ND ND 70 - 130 20ND

ND NDChloroform ND NC100 ND ND 70 - 130 20ND

0.49 0.59Chloromethane ND 18.5102 1.01 1.22 70 - 130 20ND

ND NDCis-1,2-Dichloroethene ND NC86 ND ND 70 - 130 20ND

ND NDcis-1,3-Dichloropropene ND NC113 ND ND 70 - 130 20ND

1.92 2.22Cyclohexane ND 14.5109 6.60 7.64 70 - 130 20ND

ND NDDibromochloromethane ND NC119 ND ND 70 - 130 20ND

0.66 0.64Dichlorodifluoromethane ND 3.1108 3.26 3.16 70 - 130 20ND

33.1 38.1Ethanol ND 14.0102 62.3 71.7 70 - 130 20ND

Page 1 of 2

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBG31847

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

1.4 1.31Ethyl acetate ND 6.6113 5.04 4.72 70 - 130 20ND

0.98 0.91Ethylbenzene ND 7.4107 4.25 3.95 70 - 130 20ND

4.87 4.98Heptane ND 2.2104 19.9 20.4 70 - 130 20ND

ND NDHexachlorobutadiene ND NC89 ND ND 70 - 130 20ND

13.1 12.8Hexane ND 2.3103 46.1 45.1 70 - 130 20ND

1.88 2.17Isopropylalcohol ND 14.3110 4.62 5.33 70 - 130 20ND

ND NDIsopropylbenzene ND NC109 ND ND 70 - 130 20ND

4.05 3.79m,p-Xylene ND 6.6109 17.6 16.4 70 - 130 20ND

7.87 9.32Methyl Ethyl Ketone ND 16.996 23.2 27.5 70 - 130 20ND

ND NDMethyl tert-butyl ether(MTBE) ND NC102 ND ND 70 - 130 20ND

ND NDMethylene Chloride ND NC87 ND ND 70 - 130 20ND

ND NDn-Butylbenzene ND NC113 ND ND 70 - 130 20ND

1.48 1.36o-Xylene ND 8.5106 6.42 5.90 70 - 130 20ND

36.2 45.8Propylene ND 23.4111 62.3 78.8 70 - 130 20ND

ND NDsec-Butylbenzene ND NC106 ND ND 70 - 130 20ND

ND NDStyrene ND NC113 ND ND 70 - 130 20ND

0.62 0.63Tetrachloroethene ND 1.6110 4.20 4.27 70 - 130 20ND

3.96 4.61Tetrahydrofuran ND 15.2115 11.7 13.6 70 - 130 20ND

3.83 4.05Toluene ND 5.6110 14.4 15.2 70 - 130 20ND

ND NDTrans-1,2-Dichloroethene ND NC100 ND ND 70 - 130 20ND

ND NDtrans-1,3-Dichloropropene ND NC120 ND ND 70 - 130 20ND

ND NDTrichloroethene ND NC106 ND ND 70 - 130 20ND

2.47 2.83Trichlorofluoromethane ND 13.6102 13.9 15.9 70 - 130 20ND

ND NDTrichlorotrifluoroethane ND NC96 ND ND 70 - 130 20ND

ND NDVinyl Chloride ND NC100 ND ND 70 - 130 20ND

108 109% Bromofluorobenzene 101 0.9102 108 109 70 - 130 20101

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.







Page 2 of 2

Sample Criteria Exceedences ReportFriday, April 18, 2014 Page 1 of 1


UnitsCriteria

GBG31847 - EBCCriteria: None

RLCriteria

State: NY

#Error*** No Data to Display ***


BG29068 - BG29075

Tuesday, April 15, 2014

Sample ID#s:


Project ID: DOMINO SUGAR SITE

Sincerely yours,










SDG CommentsApril 15, 2014



SDG I.D.: GBG29068




SOLIDEBC72 Hour


Laboratory Data

E-SB2 0-2

Phoenix ID: BG29068

04/07/140:00

17:33




Date Time



SDG ID: GBG29068

Client ID:Project ID: DOMINO SUGAR SITE

LOD/MDL



36500Calcium 39 04/08/14 LK SW6010mg/Kg36< 0.39Cadmium 0.39 04/09/14 LK SW6010mg/Kg0.154.01Cobalt 0.39 04/09/14 LK SW6010mg/Kg0.1513.3Chromium 0.39 04/09/14 LK SW6010mg/Kg0.15153Copper 3.9 04/08/14 LK SW6010mg/kg3.1

14000Iron 39 04/08/14 LK SW6010mg/Kg B390.14Mercury 0.09 04/08/14 RS SW-7471mg/Kg0.051140Potassium 8 04/09/14 LK SW6010mg/Kg3.03460Magnesium 3.9 04/09/14 LK SW6010mg/Kg0.23173Manganese 3.9 04/08/14 LK SW6010mg/Kg1.5543Sodium 8 04/09/14 LK SW6010mg/Kg B3.315.2Nickel 0.39 04/09/14 LK SW6010mg/Kg0.15167Lead 7.7 04/08/14 LK SW6010mg/Kg2.3


CompletedSoil Extraction for PCB 04/07/14 BB/V SW3545CompletedSoil Extraction for Pesticide 04/07/14 BB SW3545CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471

Page 1 of 40 Ver 1


Client ID:DOMINO SUGAR SITEProject ID:


LOD/MDL

CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050





QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%

78% TCMX 04/09/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.4ND1,1,1-Trichloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,1,2,2-Tetrachloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,1,2-Trichloroethane 8.2 04/10/14 JLI SW8260ug/Kg0.81ND1,1-Dichloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.6

Page 2 of 40 Ver 1




LOD/MDL

ND1,1-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.8ND1,1-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,3-Trichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,3-Trichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,2,4-Trichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6ND1,2,4-Trimethylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.2 04/10/14 JLI SW8260ug/Kg2.2ND1,2-Dibromoethane 8.2 04/10/14 JLI SW8260ug/Kg2.2ND1,2-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg0.91ND1,2-Dichloroethane 8.2 04/10/14 JLI SW8260ug/Kg0.72ND1,2-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,3,5-Trimethylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2ND1,3-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg0.87ND1,4-Dichlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.3ND2,2-Dichloropropane 8.2 04/10/14 JLI SW8260ug/Kg1.4ND2-Chlorotoluene 8.2 04/10/14 JLI SW8260ug/Kg1.3ND2-Hexanone 41 04/10/14 JLI SW8260ug/Kg3.7ND2-Isopropyltoluene 8.2 04/10/14 JLI SW8260ug/Kg 11.1ND4-Chlorotoluene 8.2 04/10/14 JLI SW8260ug/Kg0.96ND4-Methyl-2-pentanone 41 04/10/14 JLI SW8260ug/Kg2.0NDAcetone 50 04/10/14 JLI SW8260ug/Kg8.2NDAcrylonitrile 16 04/10/14 JLI SW8260ug/Kg4.6NDBenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDBromobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.1NDBromochloromethane 8.2 04/10/14 JLI SW8260ug/Kg1.2NDBromodichloromethane 8.2 04/10/14 JLI SW8260ug/Kg1.0NDBromoform 8.2 04/10/14 JLI SW8260ug/Kg1.2NDBromomethane 8.2 04/10/14 JLI SW8260ug/Kg6.3NDCarbon Disulfide 8.2 04/10/14 JLI SW8260ug/Kg1.3NDCarbon tetrachloride 8.2 04/10/14 JLI SW8260ug/Kg0.96NDChlorobenzene 8.2 04/10/14 JLI SW8260ug/Kg1.2NDChloroethane 8.2 04/10/14 JLI SW8260ug/Kg1.9NDChloroform 8.2 04/10/14 JLI SW8260ug/Kg1.5NDChloromethane 8.2 04/10/14 JLI SW8260ug/Kg4.3NDcis-1,2-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.8NDcis-1,3-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg0.89NDDibromochloromethane 8.2 04/10/14 JLI SW8260ug/Kg0.92NDDibromomethane 8.2 04/10/14 JLI SW8260ug/Kg1.0NDDichlorodifluoromethane 8.2 04/10/14 JLI SW8260ug/Kg2.2NDEthylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDHexachlorobutadiene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDIsopropylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDm&p-Xylene 8.2 04/10/14 JLI SW8260ug/Kg3.2NDMethyl Ethyl Ketone 49 04/10/14 JLI SW8260ug/Kg7.1NDMethyl t-butyl ether (MTBE) 16 04/10/14 JLI SW8260ug/Kg2.3NDMethylene chloride 8.2 04/10/14 JLI SW8260ug/Kg1.4430Naphthalene 310 04/11/14 JLI SW8260ug/Kg82NDn-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5

Page 3 of 40 Ver 1




LOD/MDL

NDn-Propylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDo-Xylene 8.2 04/10/14 JLI SW8260ug/Kg3.1NDp-Isopropyltoluene 8.2 04/10/14 JLI SW8260ug/Kg1.2NDsec-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.5NDStyrene 8.2 04/10/14 JLI SW8260ug/Kg2.4NDtert-Butylbenzene 8.2 04/10/14 JLI SW8260ug/Kg1.3NDTetrachloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDTetrahydrofuran (THF) 16 04/10/14 JLI SW8260ug/Kg 17.4NDToluene 8.2 04/10/14 JLI SW8260ug/Kg1.3NDtrans-1,2-Dichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.6NDtrans-1,3-Dichloropropene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDtrans-1,4-dichloro-2-butene 16 04/10/14 JLI SW8260ug/Kg15NDTrichloroethene 8.2 04/10/14 JLI SW8260ug/Kg1.7NDTrichlorofluoromethane 8.2 04/10/14 JLI SW8260ug/Kg1.8NDTrichlorotrifluoroethane 8.2 04/10/14 JLI SW8260ug/Kg1.3NDVinyl chloride 8.2 04/10/14 JLI SW8260ug/Kg2.7

QA/QC Surrogates111% 1,2-dichlorobenzene-d4 04/10/14 JLI 70 - 130 %%86% Bromofluorobenzene 04/10/14 JLI 70 - 130 %%98% Dibromofluoromethane 04/10/14 JLI 70 - 130 %%102% Toluene-d8 04/10/14 JLI 70 - 130 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 540 04/08/14 DD SW 8270ug/Kg270ND1,2,4-Trichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND1,2-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg220ND1,2-Diphenylhydrazine 540 04/08/14 DD SW 8270ug/Kg250ND1,3-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND1,4-Dichlorobenzene 540 04/08/14 DD SW 8270ug/Kg230ND2,4,5-Trichlorophenol 540 04/08/14 DD SW 8270ug/Kg430ND2,4,6-Trichlorophenol 540 04/08/14 DD SW 8270ug/Kg250ND2,4-Dichlorophenol 540 04/08/14 DD SW 8270ug/Kg270ND2,4-Dimethylphenol 540 04/08/14 DD SW 8270ug/Kg190ND2,4-Dinitrophenol 3900 04/08/14 DD SW 8270ug/Kg540ND2,4-Dinitrotoluene 540 04/08/14 DD SW 8270ug/Kg310ND2,6-Dinitrotoluene 540 04/08/14 DD SW 8270ug/Kg250ND2-Chloronaphthalene 540 04/08/14 DD SW 8270ug/Kg220ND2-Chlorophenol 540 04/08/14 DD SW 8270ug/Kg2205502-Methylnaphthalene 540 04/08/14 DD SW 8270ug/Kg230ND2-Methylphenol (o-cresol) 540 04/08/14 DD SW 8270ug/Kg360ND2-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg780ND2-Nitrophenol 540 04/08/14 DD SW 8270ug/Kg490ND3&4-Methylphenol (m&p-cresol) 540 04/08/14 DD SW 8270ug/Kg 1310ND3,3'-Dichlorobenzidine 1600 04/08/14 DD SW 8270ug/Kg370ND3-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg1700ND4,6-Dinitro-2-methylphenol 3900 04/08/14 DD SW 8270ug/Kg840ND4-Bromophenyl phenyl ether 540 04/08/14 DD SW 8270ug/Kg230ND4-Chloro-3-methylphenol 540 04/08/14 DD SW 8270ug/Kg270ND4-Chloroaniline 1600 04/08/14 DD SW 8270ug/Kg360ND4-Chlorophenyl phenyl ether 540 04/08/14 DD SW 8270ug/Kg260

Page 4 of 40 Ver 1




LOD/MDL

ND4-Nitroaniline 3900 04/08/14 DD SW 8270ug/Kg260ND4-Nitrophenol 3900 04/08/14 DD SW 8270ug/Kg350

1100Acenaphthene 540 04/08/14 DD SW 8270ug/Kg240NDAcenaphthylene 540 04/08/14 DD SW 8270ug/Kg220NDAcetophenone 540 04/08/14 DD SW 8270ug/Kg240NDAniline 3900 04/08/14 DD SW 8270ug/Kg1600

2800Anthracene 540 04/08/14 DD SW 8270ug/Kg2504800Benz(a)anthracene 540 04/08/14 DD SW 8270ug/Kg260NDBenzidine 1600 04/08/14 DD SW 8270ug/Kg460

3700Benzo(a)pyrene 540 04/08/14 DD SW 8270ug/Kg2505000Benzo(b)fluoranthene 540 04/08/14 DD SW 8270ug/Kg2701500Benzo(ghi)perylene 540 04/08/14 DD SW 8270ug/Kg2501500Benzo(k)fluoranthene 540 04/08/14 DD SW 8270ug/Kg260NDBenzoic acid 3900 04/08/14 DD SW 8270ug/Kg 11600NDBenzyl butyl phthalate 540 04/08/14 DD SW 8270ug/Kg200NDBis(2-chloroethoxy)methane 540 04/08/14 DD SW 8270ug/Kg210NDBis(2-chloroethyl)ether 540 04/08/14 DD SW 8270ug/Kg210NDBis(2-chloroisopropyl)ether 540 04/08/14 DD SW 8270ug/Kg 1220NDBis(2-ethylhexyl)phthalate 540 04/08/14 DD SW 8270ug/Kg220

1000Carbazole 3900 04/08/14 DD SW 8270ug/Kg590J4200Chrysene 540 04/08/14 DD SW 8270ug/Kg260NDDibenz(a,h)anthracene 540 04/08/14 DD SW 8270ug/Kg250

1200Dibenzofuran 540 04/08/14 DD SW 8270ug/Kg230NDDiethyl phthalate 540 04/08/14 DD SW 8270ug/Kg250NDDimethylphthalate 540 04/08/14 DD SW 8270ug/Kg240NDDi-n-butylphthalate 540 04/08/14 DD SW 8270ug/Kg210NDDi-n-octylphthalate 540 04/08/14 DD SW 8270ug/Kg200

9900Fluoranthene 540 04/08/14 DD SW 8270ug/Kg2501400Fluorene 540 04/08/14 DD SW 8270ug/Kg260NDHexachlorobenzene 540 04/08/14 DD SW 8270ug/Kg230NDHexachlorobutadiene 540 04/08/14 DD SW 8270ug/Kg280NDHexachlorocyclopentadiene 540 04/08/14 DD SW 8270ug/Kg240NDHexachloroethane 540 04/08/14 DD SW 8270ug/Kg230

1400Indeno(1,2,3-cd)pyrene 540 04/08/14 DD SW 8270ug/Kg260NDIsophorone 540 04/08/14 DD SW 8270ug/Kg220870Naphthalene 540 04/08/14 DD SW 8270ug/Kg220NDNitrobenzene 540 04/08/14 DD SW 8270ug/Kg270NDN-Nitrosodimethylamine 540 04/08/14 DD SW 8270ug/Kg220NDN-Nitrosodi-n-propylamine 540 04/08/14 DD SW 8270ug/Kg250NDN-Nitrosodiphenylamine 540 04/08/14 DD SW 8270ug/Kg300NDPentachloronitrobenzene 540 04/08/14 DD SW 8270ug/Kg290NDPentachlorophenol 540 04/08/14 DD SW 8270ug/Kg290

12000Phenanthrene 540 04/08/14 DD SW 8270ug/Kg220NDPhenol 540 04/08/14 DD SW 8270ug/Kg250



Page 5 of 40 Ver 1




LOD/MDL


Comments:











Page 6 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB4 0-2

Phoenix ID: BG29069

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL





4740Magnesium 3.5 04/09/14 LK SW6010mg/Kg0.21227Manganese 3.5 04/08/14 LK SW6010mg/Kg1.4672Sodium 7 04/09/14 LK SW6010mg/Kg B3.010.2Nickel 0.35 04/09/14 LK SW6010mg/Kg0.14108Lead 0.7 04/09/14 LK SW6010mg/Kg0.21



Page 7 of 40 Ver 1




LOD/MDL






QA/QC SurrogatesInterference% DCBP 04/09/14 CE 30 - 150 %%

91% TCMX 04/09/14 CE 30 - 150 %%


Page 8 of 40 Ver 1




LOD/MDL


Page 9 of 40 Ver 1




LOD/MDL




Page 10 of 40 Ver 1




LOD/MDL

ND4-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg130ND4-Nitrophenol 1900 04/08/14 DD SW 8270ug/Kg170NDAcenaphthene 270 04/08/14 DD SW 8270ug/Kg120NDAcenaphthylene 270 04/08/14 DD SW 8270ug/Kg110NDAcetophenone 270 04/08/14 DD SW 8270ug/Kg120NDAniline 1900 04/08/14 DD SW 8270ug/Kg770NDAnthracene 270 04/08/14 DD SW 8270ug/Kg120220Benz(a)anthracene 270 04/08/14 DD SW 8270ug/Kg130JNDBenzidine 760 04/08/14 DD SW 8270ug/Kg220180Benzo(a)pyrene 270 04/08/14 DD SW 8270ug/Kg120J260Benzo(b)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130JNDBenzo(ghi)perylene 270 04/08/14 DD SW 8270ug/Kg120NDBenzo(k)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130NDBenzoic acid 1900 04/08/14 DD SW 8270ug/Kg 1760NDBenzyl butyl phthalate 270 04/08/14 DD SW 8270ug/Kg98NDBis(2-chloroethoxy)methane 270 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 270 04/08/14 DD SW 8270ug/Kg100NDBis(2-chloroisopropyl)ether 270 04/08/14 DD SW 8270ug/Kg 1110NDBis(2-ethylhexyl)phthalate 270 04/08/14 DD SW 8270ug/Kg110NDCarbazole 1900 04/08/14 DD SW 8270ug/Kg290240Chrysene 270 04/08/14 DD SW 8270ug/Kg130JNDDibenz(a,h)anthracene 270 04/08/14 DD SW 8270ug/Kg120NDDibenzofuran 270 04/08/14 DD SW 8270ug/Kg110NDDiethyl phthalate 270 04/08/14 DD SW 8270ug/Kg120NDDimethylphthalate 270 04/08/14 DD SW 8270ug/Kg120NDDi-n-butylphthalate 270 04/08/14 DD SW 8270ug/Kg100NDDi-n-octylphthalate 270 04/08/14 DD SW 8270ug/Kg98340Fluoranthene 270 04/08/14 DD SW 8270ug/Kg120NDFluorene 270 04/08/14 DD SW 8270ug/Kg130NDHexachlorobenzene 270 04/08/14 DD SW 8270ug/Kg110NDHexachlorobutadiene 270 04/08/14 DD SW 8270ug/Kg140NDHexachlorocyclopentadiene 270 04/08/14 DD SW 8270ug/Kg120NDHexachloroethane 270 04/08/14 DD SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 270 04/08/14 DD SW 8270ug/Kg130NDIsophorone 270 04/08/14 DD SW 8270ug/Kg110NDNaphthalene 270 04/08/14 DD SW 8270ug/Kg110NDNitrobenzene 270 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 270 04/08/14 DD SW 8270ug/Kg110NDN-Nitrosodi-n-propylamine 270 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 270 04/08/14 DD SW 8270ug/Kg150NDPentachloronitrobenzene 270 04/08/14 DD SW 8270ug/Kg140NDPentachlorophenol 270 04/08/14 DD SW 8270ug/Kg140260Phenanthrene 270 04/08/14 DD SW 8270ug/Kg110JNDPhenol 270 04/08/14 DD SW 8270ug/Kg120320Pyrene 270 04/08/14 DD SW 8270ug/Kg130NDPyridine 270 04/08/14 DD SW 8270ug/Kg94


Page 11 of 40 Ver 1




LOD/MDL


Comments:









Page 12 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB4 15-17

Phoenix ID: BG29070

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL



15200Calcium 36 04/08/14 LK SW6010mg/Kg33< 0.36Cadmium 0.36 04/09/14 LK SW6010mg/Kg0.152.97Cobalt 0.36 04/09/14 LK SW6010mg/Kg0.158.23Chromium 0.36 04/09/14 LK SW6010mg/Kg0.1512.6Copper 0.36 04/09/14 LK SW6010mg/kg0.298940Iron 3.6 04/09/14 LK SW6010mg/Kg B3.6


2150Magnesium 3.6 04/09/14 LK SW6010mg/Kg0.22254Manganese 3.6 04/08/14 LK SW6010mg/Kg1.5128Sodium 7 04/09/14 LK SW6010mg/Kg B3.18.60Nickel 0.36 04/09/14 LK SW6010mg/Kg0.1539.0Lead 0.7 04/09/14 LK SW6010mg/Kg0.22< 1.8Antimony 1.8 04/09/14 LK SW6010mg/Kg0.73< 1.5Selenium 1.5 04/09/14 LK SW6010mg/Kg1.2< 1.5Thallium 1.5 04/09/14 LK SW6010mg/Kg1.515.5Vanadium 0.4 04/09/14 LK SW6010mg/Kg0.1522.2Zinc 0.7 04/10/14 LK SW6010mg/Kg0.3693Percent Solid 04/07/14 I E160.3%

CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050


Page 13 of 40 Ver 1




LOD/MDL


Page 14 of 40 Ver 1




LOD/MDL




Page 15 of 40 Ver 1




LOD/MDL


Page 16 of 40 Ver 1




LOD/MDL



Comments:









Page 17 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB5 0-2

Phoenix ID: BG29071

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL





11200Magnesium 35 04/08/14 LK SW6010mg/Kg2.1255Manganese 3.5 04/08/14 LK SW6010mg/Kg1.4338Sodium 7 04/09/14 LK SW6010mg/Kg B3.015.1Nickel 0.35 04/09/14 LK SW6010mg/Kg0.14166Lead 7.0 04/08/14 LK SW6010mg/Kg2.1



Page 18 of 40 Ver 1




LOD/MDL








Page 19 of 40 Ver 1




LOD/MDL

ND1,1-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1ND1,1-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.9ND1,2,3-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,3-Trichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2,4-Trichlorobenzene 9.8 04/10/14 U SW8260ug/Kg2.0ND1,2,4-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.4ND1,2-Dibromo-3-chloropropane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dibromoethane 9.8 04/10/14 U SW8260ug/Kg2.6ND1,2-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.1ND1,2-Dichloroethane 9.8 04/10/14 U SW8260ug/Kg0.87ND1,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.4ND1,3,5-Trimethylbenzene 9.8 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5ND1,3-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.0ND1,4-Dichlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.6ND2,2-Dichloropropane 9.8 04/10/14 U SW8260ug/Kg1.7ND2-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.6ND2-Hexanone 49 04/10/14 U SW8260ug/Kg4.4ND2-Isopropyltoluene 9.8 04/10/14 U SW8260ug/Kg 11.4ND4-Chlorotoluene 9.8 04/10/14 U SW8260ug/Kg1.1ND4-Methyl-2-pentanone 49 04/10/14 U SW8260ug/Kg2.312Acetone 50 04/10/14 U SW8260ug/Kg9.8JSNDAcrylonitrile 20 04/10/14 U SW8260ug/Kg5.5NDBenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDBromobenzene 9.8 04/10/14 U SW8260ug/Kg1.3NDBromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.4NDBromodichloromethane 9.8 04/10/14 U SW8260ug/Kg1.2NDBromoform 9.8 04/10/14 U SW8260ug/Kg1.4NDBromomethane 9.8 04/10/14 U SW8260ug/Kg7.6NDCarbon Disulfide 9.8 04/10/14 U SW8260ug/Kg1.6NDCarbon tetrachloride 9.8 04/10/14 U SW8260ug/Kg1.1NDChlorobenzene 9.8 04/10/14 U SW8260ug/Kg1.5NDChloroethane 9.8 04/10/14 U SW8260ug/Kg2.3NDChloroform 9.8 04/10/14 U SW8260ug/Kg1.8NDChloromethane 9.8 04/10/14 U SW8260ug/Kg5.2NDcis-1,2-Dichloroethene 9.8 04/10/14 U SW8260ug/Kg2.1NDcis-1,3-Dichloropropene 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromochloromethane 9.8 04/10/14 U SW8260ug/Kg1.1NDDibromomethane 9.8 04/10/14 U SW8260ug/Kg1.2NDDichlorodifluoromethane 9.8 04/10/14 U SW8260ug/Kg2.6NDEthylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8NDHexachlorobutadiene 9.8 04/10/14 U SW8260ug/Kg2.1NDIsopropylbenzene 9.8 04/10/14 U SW8260ug/Kg1.9NDm&p-Xylene 9.8 04/10/14 U SW8260ug/Kg3.9NDMethyl Ethyl Ketone 59 04/10/14 U SW8260ug/Kg8.5NDMethyl t-butyl ether (MTBE) 20 04/10/14 U SW8260ug/Kg2.7NDMethylene chloride 9.8 04/10/14 U SW8260ug/Kg1.6NDNaphthalene 9.8 04/10/14 U SW8260ug/Kg2.6NDn-Butylbenzene 9.8 04/10/14 U SW8260ug/Kg1.8

Page 20 of 40 Ver 1




LOD/MDL




Page 21 of 40 Ver 1




LOD/MDL

ND4-Nitroaniline 3500 04/08/14 DD SW 8270ug/Kg240ND4-Nitrophenol 3500 04/08/14 DD SW 8270ug/Kg320NDAcenaphthene 500 04/08/14 DD SW 8270ug/Kg220NDAcenaphthylene 500 04/08/14 DD SW 8270ug/Kg200NDAcetophenone 500 04/08/14 DD SW 8270ug/Kg220NDAniline 3500 04/08/14 DD SW 8270ug/Kg1400240Anthracene 500 04/08/14 DD SW 8270ug/Kg230J

1400Benz(a)anthracene 500 04/08/14 DD SW 8270ug/Kg240NDBenzidine 1400 04/08/14 DD SW 8270ug/Kg420

1200Benzo(a)pyrene 500 04/08/14 DD SW 8270ug/Kg2301800Benzo(b)fluoranthene 500 04/08/14 DD SW 8270ug/Kg240380Benzo(ghi)perylene 500 04/08/14 DD SW 8270ug/Kg230J480Benzo(k)fluoranthene 500 04/08/14 DD SW 8270ug/Kg240JNDBenzoic acid 3500 04/08/14 DD SW 8270ug/Kg 11400NDBenzyl butyl phthalate 500 04/08/14 DD SW 8270ug/Kg180NDBis(2-chloroethoxy)methane 500 04/08/14 DD SW 8270ug/Kg200NDBis(2-chloroethyl)ether 500 04/08/14 DD SW 8270ug/Kg190NDBis(2-chloroisopropyl)ether 500 04/08/14 DD SW 8270ug/Kg 1200NDBis(2-ethylhexyl)phthalate 500 04/08/14 DD SW 8270ug/Kg200NDCarbazole 3500 04/08/14 DD SW 8270ug/Kg540

1300Chrysene 500 04/08/14 DD SW 8270ug/Kg240NDDibenz(a,h)anthracene 500 04/08/14 DD SW 8270ug/Kg230NDDibenzofuran 500 04/08/14 DD SW 8270ug/Kg210NDDiethyl phthalate 500 04/08/14 DD SW 8270ug/Kg220NDDimethylphthalate 500 04/08/14 DD SW 8270ug/Kg220NDDi-n-butylphthalate 500 04/08/14 DD SW 8270ug/Kg190NDDi-n-octylphthalate 500 04/08/14 DD SW 8270ug/Kg180

2100Fluoranthene 500 04/08/14 DD SW 8270ug/Kg230NDFluorene 500 04/08/14 DD SW 8270ug/Kg230NDHexachlorobenzene 500 04/08/14 DD SW 8270ug/Kg210NDHexachlorobutadiene 500 04/08/14 DD SW 8270ug/Kg260NDHexachlorocyclopentadiene 500 04/08/14 DD SW 8270ug/Kg220NDHexachloroethane 500 04/08/14 DD SW 8270ug/Kg210370Indeno(1,2,3-cd)pyrene 500 04/08/14 DD SW 8270ug/Kg240JNDIsophorone 500 04/08/14 DD SW 8270ug/Kg200NDNaphthalene 500 04/08/14 DD SW 8270ug/Kg200NDNitrobenzene 500 04/08/14 DD SW 8270ug/Kg250NDN-Nitrosodimethylamine 500 04/08/14 DD SW 8270ug/Kg200NDN-Nitrosodi-n-propylamine 500 04/08/14 DD SW 8270ug/Kg230NDN-Nitrosodiphenylamine 500 04/08/14 DD SW 8270ug/Kg270NDPentachloronitrobenzene 500 04/08/14 DD SW 8270ug/Kg260NDPentachlorophenol 500 04/08/14 DD SW 8270ug/Kg270




Page 22 of 40 Ver 1




LOD/MDL


Comments:











Page 23 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

E-SB5 12-14

Phoenix ID: BG29072

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL

< 0.42Silver 0.42 04/09/14 LK SW6010mg/Kg0.256000Aluminum 42 04/09/14 LK SW6010mg/Kg8.3137Arsenic 0.8 04/09/14 LK SW6010mg/Kg0.83126Barium 0.8 04/09/14 LK SW6010mg/Kg0.170.74Beryllium 0.33 04/09/14 LK SW6010mg/Kg0.17

21400Calcium 42 04/09/14 LK SW6010mg/Kg388.19Cadmium 0.42 04/09/14 LK SW6010mg/Kg0.1718.1Cobalt 0.42 04/09/14 LK SW6010mg/Kg0.1718.9Chromium 0.42 04/09/14 LK SW6010mg/Kg0.17185Copper 4.2 04/09/14 LK SW6010mg/kg3.3



CompletedSoil Extraction for SVOA 04/07/14 BB/FV SW3545CompletedMercury Digestion 04/08/14 I/I SW7471CompletedTotal Metals Digest 04/07/14 CB/AG/D SW846 - 3050


Page 24 of 40 Ver 1




LOD/MDL

VolatilesND1,1,1,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.5ND1,1,1-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1,2,2-Tetrachloroethane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,1,2-Trichloroethane 8.9 04/10/14 U SW8260ug/Kg0.88ND1,1-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg1.8ND1,1-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,3-Trichloropropane 280 04/11/14 U SW8260ug/Kg40ND1,2,4-Trichlorobenzene 280 04/11/14 U SW8260ug/Kg56ND1,2,4-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg41ND1,2-Dibromo-3-chloropropane 280 04/11/14 U SW8260ug/Kg75ND1,2-Dibromoethane 8.9 04/10/14 U SW8260ug/Kg2.4ND1,2-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg31ND1,2-Dichloroethane 8.9 04/10/14 U SW8260ug/Kg0.79ND1,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.3ND1,3,5-Trimethylbenzene 280 04/11/14 U SW8260ug/Kg37ND1,3-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg42ND1,3-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg0.95ND1,4-Dichlorobenzene 280 04/11/14 U SW8260ug/Kg44ND2,2-Dichloropropane 8.9 04/10/14 U SW8260ug/Kg1.5ND2-Chlorotoluene 280 04/11/14 U SW8260ug/Kg45ND2-Hexanone 45 04/10/14 U SW8260ug/Kg4.0ND2-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg 139ND4-Chlorotoluene 280 04/11/14 U SW8260ug/Kg33ND4-Methyl-2-pentanone 45 04/10/14 U SW8260ug/Kg2.149Acetone 50 04/10/14 U SW8260ug/Kg8.9JS'NDAcrylonitrile 18 04/10/14 U SW8260ug/Kg5.0NDBenzene 8.9 04/10/14 U SW8260ug/Kg1.8NDBromobenzene 280 04/11/14 U SW8260ug/Kg37NDBromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.3NDBromodichloromethane 8.9 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.9 04/10/14 U SW8260ug/Kg1.3NDBromomethane 8.9 04/10/14 U SW8260ug/Kg6.9NDCarbon Disulfide 8.9 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.9 04/10/14 U SW8260ug/Kg1.0NDChlorobenzene 8.9 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.9 04/10/14 U SW8260ug/Kg2.1NDChloroform 8.9 04/10/14 U SW8260ug/Kg1.6NDChloromethane 8.9 04/10/14 U SW8260ug/Kg4.7NDcis-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg0.97NDDibromochloromethane 8.9 04/10/14 U SW8260ug/Kg1.0NDDibromomethane 8.9 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.9 04/10/14 U SW8260ug/Kg2.4NDEthylbenzene 8.9 04/10/14 U SW8260ug/Kg1.6NDHexachlorobutadiene 280 04/11/14 U SW8260ug/Kg59NDIsopropylbenzene 280 04/11/14 U SW8260ug/Kg54

Page 25 of 40 Ver 1




LOD/MDL

NDm&p-Xylene 8.9 04/10/14 U SW8260ug/Kg3.5NDMethyl Ethyl Ketone 54 04/10/14 U SW8260ug/Kg7.8NDMethyl t-butyl ether (MTBE) 18 04/10/14 U SW8260ug/Kg2.5NDMethylene chloride 8.9 04/10/14 U SW8260ug/Kg1.5NDNaphthalene 280 04/11/14 U SW8260ug/Kg75NDn-Butylbenzene 280 04/11/14 U SW8260ug/Kg51NDn-Propylbenzene 280 04/11/14 U SW8260ug/Kg51NDo-Xylene 8.9 04/10/14 U SW8260ug/Kg3.4NDp-Isopropyltoluene 280 04/11/14 U SW8260ug/Kg41NDsec-Butylbenzene 280 04/11/14 U SW8260ug/Kg53NDStyrene 8.9 04/10/14 U SW8260ug/Kg2.6NDtert-Butylbenzene 280 04/11/14 U SW8260ug/Kg45NDTetrachloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTetrahydrofuran (THF) 18 04/10/14 U SW8260ug/Kg 18.0NDToluene 8.9 04/10/14 U SW8260ug/Kg1.4NDtrans-1,2-Dichloroethene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,3-Dichloropropene 8.9 04/10/14 U SW8260ug/Kg1.8NDtrans-1,4-dichloro-2-butene 560 04/11/14 U SW8260ug/Kg520NDTrichloroethene 8.9 04/10/14 U SW8260ug/Kg1.9NDTrichlorofluoromethane 8.9 04/10/14 U SW8260ug/Kg2.0NDTrichlorotrifluoroethane 8.9 04/10/14 U SW8260ug/Kg1.4NDVinyl chloride 8.9 04/10/14 U SW8260ug/Kg2.9


SemivolatilesND1,2,4,5-Tetrachlorobenzene 290 04/08/14 DD SW 8270ug/Kg150ND1,2,4-Trichlorobenzene 290 04/08/14 DD SW 8270ug/Kg130ND1,2-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND1,2-Diphenylhydrazine 290 04/08/14 DD SW 8270ug/Kg140ND1,3-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND1,4-Dichlorobenzene 290 04/08/14 DD SW 8270ug/Kg120ND2,4,5-Trichlorophenol 290 04/08/14 DD SW 8270ug/Kg230ND2,4,6-Trichlorophenol 290 04/08/14 DD SW 8270ug/Kg130ND2,4-Dichlorophenol 290 04/08/14 DD SW 8270ug/Kg150ND2,4-Dimethylphenol 290 04/08/14 DD SW 8270ug/Kg100ND2,4-Dinitrophenol 2100 04/08/14 DD SW 8270ug/Kg290ND2,4-Dinitrotoluene 290 04/08/14 DD SW 8270ug/Kg160ND2,6-Dinitrotoluene 290 04/08/14 DD SW 8270ug/Kg130ND2-Chloronaphthalene 290 04/08/14 DD SW 8270ug/Kg120ND2-Chlorophenol 290 04/08/14 DD SW 8270ug/Kg1201802-Methylnaphthalene 290 04/08/14 DD SW 8270ug/Kg120JND2-Methylphenol (o-cresol) 290 04/08/14 DD SW 8270ug/Kg200ND2-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg420ND2-Nitrophenol 290 04/08/14 DD SW 8270ug/Kg260ND3&4-Methylphenol (m&p-cresol) 290 04/08/14 DD SW 8270ug/Kg 1160ND3,3'-Dichlorobenzidine 830 04/08/14 DD SW 8270ug/Kg200

Page 26 of 40 Ver 1




LOD/MDL

ND3-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg900ND4,6-Dinitro-2-methylphenol 2100 04/08/14 DD SW 8270ug/Kg450ND4-Bromophenyl phenyl ether 290 04/08/14 DD SW 8270ug/Kg120ND4-Chloro-3-methylphenol 290 04/08/14 DD SW 8270ug/Kg150ND4-Chloroaniline 830 04/08/14 DD SW 8270ug/Kg190ND4-Chlorophenyl phenyl ether 290 04/08/14 DD SW 8270ug/Kg140ND4-Nitroaniline 2100 04/08/14 DD SW 8270ug/Kg140ND4-Nitrophenol 2100 04/08/14 DD SW 8270ug/Kg190NDAcenaphthene 290 04/08/14 DD SW 8270ug/Kg130820Acenaphthylene 290 04/08/14 DD SW 8270ug/Kg120NDAcetophenone 290 04/08/14 DD SW 8270ug/Kg130NDAniline 2100 04/08/14 DD SW 8270ug/Kg840


8300Benzo(a)pyrene 290 04/08/14 DD SW 8270ug/Kg14011000Benzo(b)fluoranthene 290 04/08/14 DD SW 8270ug/Kg1403200Benzo(ghi)perylene 290 04/08/14 DD SW 8270ug/Kg1303700Benzo(k)fluoranthene 290 04/08/14 DD SW 8270ug/Kg140NDBenzoic acid 2100 04/08/14 DD SW 8270ug/Kg 1830NDBenzyl butyl phthalate 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethoxy)methane 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 290 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroisopropyl)ether 290 04/08/14 DD SW 8270ug/Kg 1120NDBis(2-ethylhexyl)phthalate 290 04/08/14 DD SW 8270ug/Kg120690Carbazole 2100 04/08/14 DD SW 8270ug/Kg320J

8600Chrysene 290 04/08/14 DD SW 8270ug/Kg140NDDibenz(a,h)anthracene 290 04/08/14 DD SW 8270ug/Kg130200Dibenzofuran 290 04/08/14 DD SW 8270ug/Kg120JNDDiethyl phthalate 290 04/08/14 DD SW 8270ug/Kg130NDDimethylphthalate 290 04/08/14 DD SW 8270ug/Kg130NDDi-n-butylphthalate 290 04/08/14 DD SW 8270ug/Kg110NDDi-n-octylphthalate 290 04/08/14 DD SW 8270ug/Kg110

18000Fluoranthene 290 04/08/14 DD SW 8270ug/Kg130230Fluorene 290 04/08/14 DD SW 8270ug/Kg140JNDHexachlorobenzene 290 04/08/14 DD SW 8270ug/Kg120NDHexachlorobutadiene 290 04/08/14 DD SW 8270ug/Kg150NDHexachlorocyclopentadiene 290 04/08/14 DD SW 8270ug/Kg130NDHexachloroethane 290 04/08/14 DD SW 8270ug/Kg120

3400Indeno(1,2,3-cd)pyrene 290 04/08/14 DD SW 8270ug/Kg140NDIsophorone 290 04/08/14 DD SW 8270ug/Kg120590Naphthalene 290 04/08/14 DD SW 8270ug/Kg120NDNitrobenzene 290 04/08/14 DD SW 8270ug/Kg150NDN-Nitrosodimethylamine 290 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodi-n-propylamine 290 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodiphenylamine 290 04/08/14 DD SW 8270ug/Kg160NDPentachloronitrobenzene 290 04/08/14 DD SW 8270ug/Kg150NDPentachlorophenol 290 04/08/14 DD SW 8270ug/Kg160

5800Phenanthrene 290 04/08/14 DD SW 8270ug/Kg120

Page 27 of 40 Ver 1




LOD/MDL

NDPhenol 290 04/08/14 DD SW 8270ug/Kg13016000Pyrene 290 04/08/14 DD SW 8270ug/Kg140

NDPyridine 290 04/08/14 DD SW 8270ug/Kg100


Comments:



Volatile Comment:There was a suppression of the last internal standard in the low level analysis, all affected compounds are reported from the methanol preserved high level analysis which did not exhibit this interference.







Page 28 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

SOIL DUPLICATE 1

Phoenix ID: BG29073

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL

< 0.36Silver 0.36 04/09/14 LK SW6010mg/Kg0.227570Aluminum 36 04/09/14 LK SW6010mg/Kg7.25.2Arsenic 0.7 04/09/14 LK SW6010mg/Kg0.72110Barium 0.7 04/09/14 LK SW6010mg/Kg0.140.39Beryllium 0.29 04/09/14 LK SW6010mg/Kg0.14





Page 29 of 40 Ver 1




LOD/MDL








Page 30 of 40 Ver 1




LOD/MDL

ND1,1-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9ND1,1-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,3-Trichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2,4-Trichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.7ND1,2,4-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.2ND1,2-Dibromo-3-chloropropane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dibromoethane 8.5 04/10/14 U SW8260ug/Kg2.3ND1,2-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg0.94ND1,2-Dichloroethane 8.5 04/10/14 U SW8260ug/Kg0.75ND1,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.2ND1,3,5-Trimethylbenzene 8.5 04/10/14 U SW8260ug/Kg1.1ND1,3-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND1,3-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg0.90ND1,4-Dichlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3ND2,2-Dichloropropane 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg1.4ND2-Hexanone 43 04/10/14 U SW8260ug/Kg3.8ND2-Isopropyltoluene 8.5 04/10/14 U SW8260ug/Kg 11.2ND4-Chlorotoluene 8.5 04/10/14 U SW8260ug/Kg0.99ND4-Methyl-2-pentanone 43 04/10/14 U SW8260ug/Kg2.030Acetone 50 04/10/14 U SW8260ug/Kg8.5JSNDAcrylonitrile 17 04/10/14 U SW8260ug/Kg4.8NDBenzene 8.5 04/10/14 U SW8260ug/Kg1.7NDBromobenzene 8.5 04/10/14 U SW8260ug/Kg1.1NDBromochloromethane 8.5 04/10/14 U SW8260ug/Kg1.2NDBromodichloromethane 8.5 04/10/14 U SW8260ug/Kg1.1NDBromoform 8.5 04/10/14 U SW8260ug/Kg1.2NDBromomethane 8.5 04/10/14 U SW8260ug/Kg6.6NDCarbon Disulfide 8.5 04/10/14 U SW8260ug/Kg1.4NDCarbon tetrachloride 8.5 04/10/14 U SW8260ug/Kg0.99NDChlorobenzene 8.5 04/10/14 U SW8260ug/Kg1.3NDChloroethane 8.5 04/10/14 U SW8260ug/Kg2.0NDChloroform 8.5 04/10/14 U SW8260ug/Kg1.5NDChloromethane 8.5 04/10/14 U SW8260ug/Kg4.5NDcis-1,2-Dichloroethene 8.5 04/10/14 U SW8260ug/Kg1.9NDcis-1,3-Dichloropropene 8.5 04/10/14 U SW8260ug/Kg0.92NDDibromochloromethane 8.5 04/10/14 U SW8260ug/Kg0.95NDDibromomethane 8.5 04/10/14 U SW8260ug/Kg1.1NDDichlorodifluoromethane 8.5 04/10/14 U SW8260ug/Kg2.3NDEthylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5NDHexachlorobutadiene 8.5 04/10/14 U SW8260ug/Kg1.8NDIsopropylbenzene 8.5 04/10/14 U SW8260ug/Kg1.6NDm&p-Xylene 8.5 04/10/14 U SW8260ug/Kg3.4NDMethyl Ethyl Ketone 51 04/10/14 U SW8260ug/Kg7.4NDMethyl t-butyl ether (MTBE) 17 04/10/14 U SW8260ug/Kg2.3NDMethylene chloride 8.5 04/10/14 U SW8260ug/Kg1.4390Naphthalene 320 04/11/14 U SW8260ug/Kg84NDn-Butylbenzene 8.5 04/10/14 U SW8260ug/Kg1.5

Page 31 of 40 Ver 1




LOD/MDL



SemivolatilesND1,2,4,5-Tetrachlorobenzene 270 04/08/14 DD SW 8270ug/Kg140ND1,2,4-Trichlorobenzene 270 04/08/14 DD SW 8270ug/Kg120ND1,2-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,2-Diphenylhydrazine 270 04/08/14 DD SW 8270ug/Kg130ND1,3-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND1,4-Dichlorobenzene 270 04/08/14 DD SW 8270ug/Kg110ND2,4,5-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg210ND2,4,6-Trichlorophenol 270 04/08/14 DD SW 8270ug/Kg120ND2,4-Dichlorophenol 270 04/08/14 DD SW 8270ug/Kg140ND2,4-Dimethylphenol 270 04/08/14 DD SW 8270ug/Kg95ND2,4-Dinitrophenol 1900 04/08/14 DD SW 8270ug/Kg270ND2,4-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg150ND2,6-Dinitrotoluene 270 04/08/14 DD SW 8270ug/Kg120ND2-Chloronaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Chlorophenol 270 04/08/14 DD SW 8270ug/Kg1103302-Methylnaphthalene 270 04/08/14 DD SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 270 04/08/14 DD SW 8270ug/Kg180ND2-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg390ND2-Nitrophenol 270 04/08/14 DD SW 8270ug/Kg240ND3&4-Methylphenol (m&p-cresol) 270 04/08/14 DD SW 8270ug/Kg 1150ND3,3'-Dichlorobenzidine 770 04/08/14 DD SW 8270ug/Kg180ND3-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg840ND4,6-Dinitro-2-methylphenol 1900 04/08/14 DD SW 8270ug/Kg410ND4-Bromophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg110ND4-Chloro-3-methylphenol 270 04/08/14 DD SW 8270ug/Kg140ND4-Chloroaniline 770 04/08/14 DD SW 8270ug/Kg180ND4-Chlorophenyl phenyl ether 270 04/08/14 DD SW 8270ug/Kg130

Page 32 of 40 Ver 1




LOD/MDL

ND4-Nitroaniline 1900 04/08/14 DD SW 8270ug/Kg130ND4-Nitrophenol 1900 04/08/14 DD SW 8270ug/Kg170690Acenaphthene 270 04/08/14 DD SW 8270ug/Kg120NDAcenaphthylene 270 04/08/14 DD SW 8270ug/Kg110NDAcetophenone 270 04/08/14 DD SW 8270ug/Kg120NDAniline 1900 04/08/14 DD SW 8270ug/Kg780


2500Benzo(a)pyrene 270 04/08/14 DD SW 8270ug/Kg1303700Benzo(b)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130940Benzo(ghi)perylene 270 04/08/14 DD SW 8270ug/Kg120

1200Benzo(k)fluoranthene 270 04/08/14 DD SW 8270ug/Kg130NDBenzoic acid 1900 04/08/14 DD SW 8270ug/Kg 1770NDBenzyl butyl phthalate 270 04/08/14 DD SW 8270ug/Kg99NDBis(2-chloroethoxy)methane 270 04/08/14 DD SW 8270ug/Kg110NDBis(2-chloroethyl)ether 270 04/08/14 DD SW 8270ug/Kg100NDBis(2-chloroisopropyl)ether 270 04/08/14 DD SW 8270ug/Kg 1110NDBis(2-ethylhexyl)phthalate 270 04/08/14 DD SW 8270ug/Kg110610Carbazole 1900 04/08/14 DD SW 8270ug/Kg290J

2800Chrysene 270 04/08/14 DD SW 8270ug/Kg130NDDibenz(a,h)anthracene 270 04/08/14 DD SW 8270ug/Kg120690Dibenzofuran 270 04/08/14 DD SW 8270ug/Kg110NDDiethyl phthalate 270 04/08/14 DD SW 8270ug/Kg120NDDimethylphthalate 270 04/08/14 DD SW 8270ug/Kg120NDDi-n-butylphthalate 270 04/08/14 DD SW 8270ug/Kg100NDDi-n-octylphthalate 270 04/08/14 DD SW 8270ug/Kg99

6000Fluoranthene 270 04/08/14 DD SW 8270ug/Kg120840Fluorene 270 04/08/14 DD SW 8270ug/Kg130NDHexachlorobenzene 270 04/08/14 DD SW 8270ug/Kg110NDHexachlorobutadiene 270 04/08/14 DD SW 8270ug/Kg140NDHexachlorocyclopentadiene 270 04/08/14 DD SW 8270ug/Kg120NDHexachloroethane 270 04/08/14 DD SW 8270ug/Kg120890Indeno(1,2,3-cd)pyrene 270 04/08/14 DD SW 8270ug/Kg130NDIsophorone 270 04/08/14 DD SW 8270ug/Kg110560Naphthalene 270 04/08/14 DD SW 8270ug/Kg110NDNitrobenzene 270 04/08/14 DD SW 8270ug/Kg130NDN-Nitrosodimethylamine 270 04/08/14 DD SW 8270ug/Kg110NDN-Nitrosodi-n-propylamine 270 04/08/14 DD SW 8270ug/Kg120NDN-Nitrosodiphenylamine 270 04/08/14 DD SW 8270ug/Kg150NDPentachloronitrobenzene 270 04/08/14 DD SW 8270ug/Kg140NDPentachlorophenol 270 04/08/14 DD SW 8270ug/Kg150




Page 33 of 40 Ver 1




LOD/MDL


Comments:










Page 34 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

TRIP BLANK HIGH

Phoenix ID: BG29074

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL


VolatilesND1,1,1,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg41ND1,1,1-Trichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 04/10/14 U SW8260ug/Kg36ND1,1,2-Trichloroethane 250 04/10/14 U SW8260ug/Kg25ND1,1-Dichloroethane 250 04/10/14 U SW8260ug/Kg50ND1,1-Dichloroethene 250 04/10/14 U SW8260ug/Kg55ND1,1-Dichloropropene 250 04/10/14 U SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,3-Trichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 04/10/14 U SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dibromoethane 250 04/10/14 U SW8260ug/Kg67ND1,2-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg28ND1,2-Dichloroethane 250 04/10/14 U SW8260ug/Kg22ND1,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 04/10/14 U SW8260ug/Kg33ND1,3-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg37ND1,3-Dichloropropane 250 04/10/14 U SW8260ug/Kg27ND1,4-Dichlorobenzene 250 04/10/14 U SW8260ug/Kg40ND2,2-Dichloropropane 250 04/10/14 U SW8260ug/Kg42ND2-Chlorotoluene 250 04/10/14 U SW8260ug/Kg40ND2-Hexanone 1300 04/10/14 U SW8260ug/Kg110ND2-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg 135

Page 35 of 40 Ver 1




LOD/MDL

ND4-Chlorotoluene 250 04/10/14 U SW8260ug/Kg29ND4-Methyl-2-pentanone 1300 04/10/14 U SW8260ug/Kg60NDAcetone 2500 04/10/14 U SW8260ug/Kg250NDAcrylonitrile 500 04/10/14 U SW8260ug/Kg140NDBenzene 250 04/10/14 U SW8260ug/Kg50NDBromobenzene 250 04/10/14 U SW8260ug/Kg33NDBromochloromethane 250 04/10/14 U SW8260ug/Kg37NDBromodichloromethane 250 04/10/14 U SW8260ug/Kg31NDBromoform 250 04/10/14 U SW8260ug/Kg35NDBromomethane 250 04/10/14 U SW8260ug/Kg190NDCarbon Disulfide 250 04/10/14 U SW8260ug/Kg41NDCarbon tetrachloride 250 04/10/14 U SW8260ug/Kg29NDChlorobenzene 250 04/10/14 U SW8260ug/Kg37NDChloroethane 250 04/10/14 U SW8260ug/Kg59NDChloroform 250 04/10/14 U SW8260ug/Kg46NDChloromethane 250 04/10/14 U SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg27NDDibromochloromethane 250 04/10/14 U SW8260ug/Kg28NDDibromomethane 250 04/10/14 U SW8260ug/Kg32NDDichlorodifluoromethane 250 04/10/14 U SW8260ug/Kg67NDEthylbenzene 250 04/10/14 U SW8260ug/Kg46NDHexachlorobutadiene 250 04/10/14 U SW8260ug/Kg53NDIsopropylbenzene 250 04/10/14 U SW8260ug/Kg48NDm&p-Xylene 250 04/10/14 U SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 04/10/14 U SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 04/10/14 U SW8260ug/Kg69NDMethylene chloride 250 04/10/14 U SW8260ug/Kg41NDNaphthalene 250 04/10/14 U SW8260ug/Kg67NDn-Butylbenzene 250 04/10/14 U SW8260ug/Kg46NDn-Propylbenzene 250 04/10/14 U SW8260ug/Kg45NDo-Xylene 250 04/10/14 U SW8260ug/Kg96NDp-Isopropyltoluene 250 04/10/14 U SW8260ug/Kg36NDsec-Butylbenzene 250 04/10/14 U SW8260ug/Kg47NDStyrene 250 04/10/14 U SW8260ug/Kg72NDtert-Butylbenzene 250 04/10/14 U SW8260ug/Kg40NDTetrachloroethene 250 04/10/14 U SW8260ug/Kg53NDTetrahydrofuran (THF) 500 04/10/14 U SW8260ug/Kg 1230NDToluene 250 04/10/14 U SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 04/10/14 U SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 04/10/14 U SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 04/10/14 U SW8260ug/Kg460NDTrichloroethene 250 04/10/14 U SW8260ug/Kg53NDTrichlorofluoromethane 250 04/10/14 U SW8260ug/Kg56NDTrichlorotrifluoroethane 250 04/10/14 U SW8260ug/Kg39NDVinyl chloride 250 04/10/14 U SW8260ug/Kg81


Page 36 of 40 Ver 1




LOD/MDL


Comments:


This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.







Page 37 of 40 Ver 1



SOLIDEBC72 Hour


Laboratory Data

TRIP BLANK LOW

Phoenix ID: BG29075

04/07/140:00

17:33




Date Time



SDG ID: GBG29068


LOD/MDL


VolatilesND1,1,1,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 04/10/14 U SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 04/10/14 U SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 04/10/14 U SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 04/10/14 U SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 04/10/14 U SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 04/10/14 U SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.80ND2-Hexanone 25 04/10/14 U SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg 10.69

Page 38 of 40 Ver 1




LOD/MDL

ND4-Chlorotoluene 5.0 04/10/14 U SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 04/10/14 U SW8260ug/Kg1.2NDAcetone 50 04/10/14 U SW8260ug/Kg5.0NDAcrylonitrile 10 04/10/14 U SW8260ug/Kg2.8NDBenzene 5.0 04/10/14 U SW8260ug/Kg0.99NDBromobenzene 5.0 04/10/14 U SW8260ug/Kg0.65NDBromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.73NDBromodichloromethane 5.0 04/10/14 U SW8260ug/Kg0.62NDBromoform 5.0 04/10/14 U SW8260ug/Kg0.70NDBromomethane 5.0 04/10/14 U SW8260ug/Kg3.9NDCarbon Disulfide 5.0 04/10/14 U SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 04/10/14 U SW8260ug/Kg0.58NDChlorobenzene 5.0 04/10/14 U SW8260ug/Kg0.74NDChloroethane 5.0 04/10/14 U SW8260ug/Kg1.2NDChloroform 5.0 04/10/14 U SW8260ug/Kg0.91NDChloromethane 5.0 04/10/14 U SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg0.54NDDibromochloromethane 5.0 04/10/14 U SW8260ug/Kg0.56NDDibromomethane 5.0 04/10/14 U SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 04/10/14 U SW8260ug/Kg1.3NDEthylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 04/10/14 U SW8260ug/Kg1.1NDIsopropylbenzene 5.0 04/10/14 U SW8260ug/Kg0.96NDm&p-Xylene 5.0 04/10/14 U SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 04/10/14 U SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 04/10/14 U SW8260ug/Kg1.4NDMethylene chloride 5.0 04/10/14 U SW8260ug/Kg0.82NDNaphthalene 5.0 04/10/14 U SW8260ug/Kg1.3NDn-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.91NDn-Propylbenzene 5.0 04/10/14 U SW8260ug/Kg0.90NDo-Xylene 5.0 04/10/14 U SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 04/10/14 U SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.94NDStyrene 5.0 04/10/14 U SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 04/10/14 U SW8260ug/Kg0.80NDTetrachloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 04/10/14 U SW8260ug/Kg 14.5NDToluene 5.0 04/10/14 U SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 04/10/14 U SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 04/10/14 U SW8260ug/Kg9.3NDTrichloroethene 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 04/10/14 U SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 04/10/14 U SW8260ug/Kg0.78NDVinyl chloride 5.0 04/10/14 U SW8260ug/Kg1.6


Page 39 of 40 Ver 1




LOD/MDL


Comments:








Page 40 of 40 Ver 1

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG29068

LCS%

DupRPD

LCSD%

LCSRPD

%Rec

Limits

%RPD

LimitsSampleResult

DupResult

QA/QC Batch 270840, QC Sample No: BG28884 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)113 114Mercury - Soil BRL 0.9103NC 104 1.0 70 - 130 30<0.07 <0.08


Comment:

QA/QC Batch 270800, QC Sample No: BG29062 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)


93.0 95.1Antimony BRL 2.296.5NC 101 4.6 75 - 125 30<1.9 <1.9

93.9 94.0Arsenic BRL 0.195.3NC 96.8 1.6 75 - 125 303.3 2.78

98.0 110Barium BRL 11.512015.4 101 17.2 75 - 125 3047.5 40.7

97.4 98.8Beryllium BRL 1.4101NC 101 0.0 75 - 125 30<0.31 <0.31

89.8 91.0Cadmium BRL 1.397.0NC 94.0 3.1 75 - 125 30<0.39 <0.39

NC NCCalcium BRL NC93.744.8 92.3 1.5 r75 - 125 3027400 43200

95.9 96.0Chromium BRL 0.11038.00 103 0.0 75 - 125 3019.5 18.0

93.3 93.9Cobalt BRL 0.6101NC 98.8 2.2 75 - 125 301.94 1.77

86.3 85.6Copper BRL 0.810613.1 104 1.9 75 - 125 30203 178

NC NCIron 9.7 NC1068.10 108 1.9 75 - 125 306900 7480

90.1 92.2Lead BRL 2.310122.6 96.9 4.1 75 - 125 3049.8 39.7

NC NCMagnesium BRL NC101116 101 0.0 r75 - 125 302200 8330

93.0 94.7Manganese BRL 1.810316.1 100 3.0 75 - 125 3084.5 99.3

91.7 91.8Nickel BRL 0.11023.90 99.1 2.9 75 - 125 3010.5 10.1

128 >130Potassium BRL NC10929.7 113 3.6 m75 - 125 301320 979

82.3 82.7Selenium BRL 0.586.8NC 84.3 2.9 75 - 125 30<1.6 <1.6

99.6 100Silver BRL 0.498.2NC 99.5 1.3 75 - 125 30<0.39 <0.39

>130 >130Sodium 5.6 NC1133.80 112 0.9 m75 - 125 30234 243

94.8 95.8Thallium BRL 1.098.4NC 96.1 2.4 75 - 125 30<1.6 <1.6

99.0 100Vanadium BRL 1.010416.6 102 1.9 75 - 125 309.4 11.1

NC NCZinc BRL NC99.256.9 95.6 3.7 r75 - 125 30117 210

m = This parameter is outside laboratory ms/msd specified recovery limits.r = This parameter is outside laboratory rpd specified recovery limits.

Page 1 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD




SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits



85 984,4' -DDE ND 14.2100 86 15.1 40 - 140 30

102 1094,4' -DDT ND 6.6106 91 15.2 40 - 140 30

96 102a-BHC ND 6.197 84 14.4 40 - 140 30

96 100a-Chlordane ND 4.1102 89 13.6 40 - 140 30

87 89Aldrin ND 2.397 84 14.4 40 - 140 30

96 106b-BHC ND 9.998 87 11.9 40 - 140 30


74 80d-BHC ND 7.875 65 14.3 40 - 140 30

87 96Dieldrin ND 9.898 84 15.4 40 - 140 30

100 105Endosulfan I ND 4.9101 90 11.5 40 - 140 30

100 105Endosulfan II ND 4.971 80 11.9 40 - 140 30


101 110Endrin ND 8.5102 90 12.5 40 - 140 30

85 101Endrin aldehyde ND 17.278 79 1.3 40 - 140 30

100 107Endrin ketone ND 6.8102 90 12.5 40 - 140 30

100 108g-BHC ND 7.7101 88 13.8 40 - 140 30

93 97g-Chlordane ND 4.299 86 14.1 40 - 140 30

94 96Heptachlor ND 2.1101 88 13.8 40 - 140 30


104 111Methoxychlor ND 6.5111 98 12.4 40 - 140 30


90 98% DCBP 104 8.597 83 15.6 30 - 150 30

87 90% TCMX 94 3.493 78 17.5 30 - 150 30


Comment:

QA/QC Batch 270799, QC Sample No: BG29065 (BG29068, BG29069, BG29070, BG29071, BG29072, BG29073)











2.8 3.02,4-Dinitrophenol ND 6.9<10 <10 NC l,m30 - 130 30


Page 2 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits



88 862-Chlorophenol ND 2.379 78 1.3 30 - 130 30



108 1192-Nitroaniline ND 9.7105 104 1.0 30 - 130 30

83 862-Nitrophenol ND 3.668 67 1.5 30 - 130 30



89 893-Nitroaniline ND 0.089 89 0.0 30 - 130 30

78 844,6-Dinitro-2-methylphenol ND 7.422 23 4.4 l30 - 130 30





96 984-Nitroaniline ND 2.189 84 5.8 30 - 130 30

107 1084-Nitrophenol ND 0.992 90 2.2 30 - 130 30

83 83Acenaphthene ND 0.076 76 0.0 30 - 130 30


86 87Acetophenone ND 1.280 78 2.5 30 - 130 30

79 78Aniline ND 1.380 77 3.8 30 - 130 30

91 91Anthracene ND 0.082 82 0.0 30 - 130 30


141 136Benzidine ND 3.6>200 >200 NC l,m30 - 130 30

80 82Benzo(a)pyrene ND 2.573 73 0.0 30 - 130 30









100 98Carbazole ND 2.087 88 1.1 30 - 130 30

90 91Chrysene ND 1.181 82 1.2 30 - 130 30


88 88Dibenzofuran ND 0.080 81 1.2 30 - 130 30





94 92Fluoranthene ND 2.284 86 2.4 30 - 130 30

87 90Fluorene ND 3.482 82 0.0 30 - 130 30






88 88Isophorone ND 0.081 80 1.2 30 - 130 30

82 82Naphthalene ND 0.075 75 0.0 30 - 130 30

84 84Nitrobenzene ND 0.078 76 2.6 30 - 130 30



Page 3 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits




91 91Phenanthrene ND 0.082 83 1.2 30 - 130 30

90 90Phenol ND 0.083 80 3.7 30 - 130 30

96 95Pyrene ND 1.085 87 2.3 30 - 130 30

66 65Pyridine ND 1.568 66 3.0 30 - 130 30

87 96% 2,4,6-Tribromophenol 63 9.878 76 2.6 30 - 130 30

55 54% 2-Fluorobiphenyl 54 1.849 48 2.1 30 - 130 30

80 79% 2-Fluorophenol 77 1.370 69 1.4 30 - 130 30

54 54% Nitrobenzene-d5 53 0.049 48 2.1 30 - 130 30

83 83% Phenol-d5 81 0.075 73 2.7 30 - 130 30

67 66% Terphenyl-d14 60 1.558 60 3.4 30 - 130 30


Comment:



PCB-1221 ND 40 - 140 30

PCB-1232 ND 40 - 140 30

PCB-1242 ND 40 - 140 30

PCB-1248 ND 40 - 140 30

PCB-1254 ND 40 - 140 30

102 96PCB-1260 ND 6.198 95 3.1 40 - 140 30

PCB-1262 ND 40 - 140 30

PCB-1268 ND 40 - 140 30

























Page 4 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


119 1102-Hexanone ND 7.9131 118 10.4 l70 - 130 30




67 63Acetone ND 6.291 85 6.8 m70 - 130 30


98 99Benzene ND 1.099 93 6.3 70 - 130 30

100 100Bromobenzene ND 0.099 92 7.3 70 - 130 30



98 104Bromoform ND 5.9101 99 2.0 70 - 130 30

100 104Bromomethane ND 3.995 85 11.1 70 - 130 30




90 92Chloroethane ND 2.295 91 4.3 70 - 130 30

95 97Chloroform ND 2.196 91 5.3 70 - 130 30







93 99Ethylbenzene ND 6.396 90 6.5 70 - 130 30



95 100m&p-Xylene ND 5.199 93 6.3 70 - 130 30




100 99Naphthalene ND 1.0103 99 4.0 70 - 130 30



103 106o-Xylene ND 2.998 90 8.5 70 - 130 30



99 104Styrene ND 4.9103 94 9.1 70 - 130 30




94 99Toluene ND 5.299 97 2.0 70 - 130 30





90 91Trichlorofluoromethane ND 1.194 88 6.6 70 - 130 30






99 101% Toluene-d8 102 2.0100 101 1.0 70 - 130 30

Page 5 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


Comment:

QA/QC Batch 271311, QC Sample No: BG29079 (BG29070, BG29071, BG29072 (50, 1X) , BG29073 (63, 1X) , BG29074 (50X) , BG29075)























76 762-Hexanone ND 0.098 107 8.8 70 - 130 30



89 894-Methyl-2-pentanone ND 0.0102 114 11.1 70 - 130 30

82 81Acetone ND 1.2126 109 14.5 70 - 130 30


97 96Benzene ND 1.090 93 3.3 70 - 130 30

97 95Bromobenzene ND 2.192 94 2.2 70 - 130 30



88 92Bromoform ND 4.489 97 8.6 70 - 130 30

110 88Bromomethane ND 22.2108 91 17.1 70 - 130 30




96 100Chloroethane ND 4.196 102 6.1 70 - 130 30

99 98Chloroform ND 1.090 95 5.4 70 - 130 30







99 97Ethylbenzene ND 2.090 93 3.3 70 - 130 30


Page 6 of 7

QA/QC Data

Parameter BlankMS%

MSD%

MSRPD

SDG I.D.: GBG29068

LCS%

LCSD%

LCSRPD

%Rec

Limits

%RPD

Limits


98 95m&p-Xylene ND 3.190 94 4.3 70 - 130 30




94 80Naphthalene ND 16.194 88 6.6 70 - 130 30



98 96o-Xylene ND 2.191 95 4.3 70 - 130 30



95 94Styrene ND 1.194 96 2.1 70 - 130 30




98 95Toluene ND 3.190 94 4.3 70 - 130 30





106 105Trichlorofluoromethane ND 0.996 103 7.0 70 - 130 30






99 99% Toluene-d8 99 0.099 100 1.0 70 - 130 30


Comment:


Volatiles - Solid105 102Naphthalene ND 2.9100 105 4.9 70 - 130 30


Comment:

l = This parameter is outside laboratory lcs/lcsd specified recovery limits.m = This parameter is outside laboratory ms/msd specified recovery limits.






NC - No Criteria

Intf - Interference

Page 7 of 7

Sample Criteria Exceedences ReportTuesday, April 15, 2014 Page 1 of 3


UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Phenol 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10004800 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 39004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 10004200 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10005000 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10001500 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8001500 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10003700 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5001400 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential 330$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 540 ug/KgBG29068 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330CU-SM Copper 50153 3.9 mg/kgBG29068 NY / 375-6.8 Metals / Unrestricted Use Soil 50PB-SMDP Lead 63167 7.7 mg/KgBG29068 NY / 375-6.8 Metals / Unrestricted Use Soil 63

PB-SMDP Lead 63108 0.7 mg/KgBG29069 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109116 0.7 mg/KgBG29069 NY / 375-6.8 Metals / Unrestricted Use Soil 109

$8270SMRDP Phenol 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP 2-Methylphenol (o-cresol) 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10001400 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10001300 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10001300 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10001800 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10001200 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential 330



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Residential Restricted 330$8270SMRDP Dibenz(a,h)anthracene 330ND 500 ug/KgBG29071 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 330CU-SM Copper 5057.0 0.35 mg/kgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 50HG-SM Mercury 0.180.28 0.06 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18PB-SMDP Lead 63166 7.0 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 109121 0.7 mg/KgBG29071 NY / 375-6.8 Metals / Unrestricted Use Soil 109

$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10009300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 39008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 3900$8270SMRDP Chrysene 10008600 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 100011000 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10003700 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8003700 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10008300 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 5003400 290 ug/KgBG29072 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500AS-SM Arsenic 16137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Residential 16AS-SM Arsenic 16137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Residential Restricted 16AS-SM Arsenic 13137 0.8 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 13CD-SM Cadmium 2.58.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Residential 2.5CD-SM Cadmium 4.38.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Residential Restricted 4.3CD-SM Cadmium 2.58.19 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 2.5CU-SM Copper 50185 4.2 mg/kgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 50HG-SM Mercury 0.180.23 0.10 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 0.18NI-SM Nickel 3039.6 0.42 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 30PB-SMDP Lead 63308 8.3 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 63ZN-SMDP Zinc 1091480 8.3 mg/KgBG29072 NY / 375-6.8 Metals / Unrestricted Use Soil 109

$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benz(a)anthracene 10003300 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Chrysene 10002800 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Chrysene 10002800 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000



UnitsCriteria


RLCriteria

State: NY

$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(b)fluoranthene 10003700 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Benzo(k)fluoranthene 10001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(k)fluoranthene 8001200 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 800$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 1000$8270SMRDP Benzo(a)pyrene 10002500 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 1000$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Residential Restricted 500$8270SMRDP Indeno(1,2,3-cd)pyrene 500890 270 ug/KgBG29073 NY / 375-6.8 Semivolatiles / Unrestricted Use Soil 500CU-SM Copper 5051.2 0.36 mg/kgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 50PB-SMDP Lead 63156 7.2 mg/KgBG29073 NY / 375-6.8 Metals / Unrestricted Use Soil 63

$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR Acetone 50ND 2500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Benzene 60ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Methylene chloride 50ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG29074 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190





SDG I.D.: GBG29068


Page 1 of 1

BG34092

Tuesday, April 22, 2014

Sample ID#s:



Sincerely yours,











AIREBC72 Hour


DM

Laboratory Data

E-SG1

Phoenix ID: BG34092

04/17/1411:1217:15

Parameterppbv

ResultppbvRL




Date Time



SDG ID: GBG34092


ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 04/18/14 KCA TO15ND 11.000.581,1,1-Trichloroethane 0.183 04/18/14 KCA TO153.16 1.00ND1,1,2,2-Tetrachloroethane 0.146 04/18/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 04/18/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 04/18/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 04/18/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 04/18/14 KCA TO15ND 1.00ND1,2,4-Trimethylbenzene 0.204 04/18/14 KCA TO15ND 1.00ND1,2-Dibromoethane(EDB) 0.130 04/18/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 04/18/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 04/18/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 04/18/14 KCA TO15ND 1.00ND1,3,5-Trimethylbenzene 0.204 04/18/14 KCA TO15ND 1.00ND1,3-Butadiene 0.452 04/18/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 04/18/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 04/18/14 KCA TO15ND 1.001.292-Hexanone(MBK) 0.244 04/18/14 KCA TO155.28 11.00ND4-Ethyltoluene 0.204 04/18/14 KCA TO15ND 11.00ND4-Isopropyltoluene 0.182 04/18/14 KCA TO15ND 11.00ND4-Methyl-2-pentanone(MIBK) 0.244 04/18/14 KCA TO15ND 1.00107Acetone 0.421 04/18/14 KCA TO15254 1.00NDAcrylonitrile 0.461 04/18/14 KCA TO15ND 1.00NDBenzene 0.313 04/18/14 KCA TO15ND 1.00NDBenzyl chloride 0.193 04/18/14 KCA TO15ND 1.00

Page 1 of 3 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

NDBromodichloromethane 0.149 04/18/14 KCA TO15ND 1.00NDBromoform 0.097 04/18/14 KCA TO15ND 1.00NDBromomethane 0.258 04/18/14 KCA TO15ND 1.00NDCarbon Disulfide 0.321 04/18/14 KCA TO15ND 1.000.06Carbon Tetrachloride 0.040 04/18/14 KCA TO150.377 0.25NDChlorobenzene 0.217 04/18/14 KCA TO15ND 1.00NDChloroethane 0.379 04/18/14 KCA TO15ND 1.000.78Chloroform 0.205 04/18/14 KCA TO153.81 1.00NDChloromethane 0.484 04/18/14 KCA TO15ND 1.000.67Cis-1,2-Dichloroethene 0.252 04/18/14 KCA TO152.65 1.00NDcis-1,3-Dichloropropene 0.220 04/18/14 KCA TO15ND 1.00NDCyclohexane 0.291 04/18/14 KCA TO15ND 1.00NDDibromochloromethane 0.117 04/18/14 KCA TO15ND 1.000.33Dichlorodifluoromethane 0.202 04/18/14 KCA TO151.63 1.004.99Ethanol 0.531 04/18/14 KCA TO159.40 11.00NDEthyl acetate 0.278 04/18/14 KCA TO15ND 11.00NDEthylbenzene 0.230 04/18/14 KCA TO15ND 1.000.28Heptane 0.244 04/18/14 KCA TO151.15 1.00NDHexachlorobutadiene 0.094 04/18/14 KCA TO15ND 1.00NDHexane 0.284 04/18/14 KCA TO15ND 1.001.98Isopropylalcohol 0.407 04/18/14 KCA TO154.86 1.00NDIsopropylbenzene 0.204 04/18/14 KCA TO15ND 1.000.24m,p-Xylene 0.230 04/18/14 KCA TO151.04 1.006.74Methyl Ethyl Ketone 0.339 04/18/14 KCA TO1519.9 1.00NDMethyl tert-butyl ether(MTBE) 0.278 04/18/14 KCA TO15ND 1.000.46Methylene Chloride 0.288 04/18/14 KCA TO151.60 1.00NDn-Butylbenzene 0.182 04/18/14 KCA TO15ND 11.00NDo-Xylene 0.230 04/18/14 KCA TO15ND 1.003.03Propylene 0.581 04/18/14 KCA TO155.21 11.00NDsec-Butylbenzene 0.182 04/18/14 KCA TO15ND 11.00NDStyrene 0.235 04/18/14 KCA TO15ND 1.000.3Tetrachloroethene 0.037 04/18/14 KCA TO152.03 0.25NDTetrahydrofuran 0.339 04/18/14 KCA TO15ND 11.000.48Toluene 0.266 04/18/14 KCA TO151.81 1.00NDTrans-1,2-Dichloroethene 0.252 04/18/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 04/18/14 KCA TO15ND 1.004.49Trichloroethene 0.047 04/18/14 KCA TO1524.1 0.250.24Trichlorofluoromethane 0.178 04/18/14 KCA TO151.35 1.00NDTrichlorotrifluoroethane 0.130 04/18/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 04/18/14 KCA TO15ND 0.25


Page 2 of 3 Ver 1



Parameterppbv

ResultppbvRL


ug/m3RL

Comments:






Page 3 of 3 Ver 1

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD




SDG I.D.: GBG34092

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3


VolatilesND ND1,1,1,2-Tetrachloroethane ND NC110 ND ND 70 - 130 20ND

0.58 0.481,1,1-Trichloroethane ND 18.9101 3.16 2.62 70 - 130 20ND

ND ND1,1,2,2-Tetrachloroethane ND NC104 ND ND 70 - 130 20ND



ND ND1,1-Dichloroethene ND NC94 ND ND 70 - 130 20ND

ND ND1,2,4-Trichlorobenzene ND NC109 ND ND 70 - 130 20ND


ND ND1,2-Dibromoethane(EDB) ND NC104 ND ND 70 - 130 20ND



ND ND1,2-dichloropropane ND NC101 ND ND 70 - 130 20ND

ND ND1,2-Dichlorotetrafluoroethane ND NC114 ND ND 70 - 130 20ND


ND ND1,3-Butadiene ND NC99 ND ND 70 - 130 20ND



ND ND1,4-Dioxane ND NC104 ND ND 70 - 130 20ND

1.29 1.022-Hexanone(MBK) ND 23.4104 5.28 4.18 70 - 130 20ND

ND ND4-Ethyltoluene ND NC105 ND ND 70 - 130 20ND

ND ND4-Isopropyltoluene ND NC107 ND ND 70 - 130 20ND

ND ND4-Methyl-2-pentanone(MIBK) ND NC103 ND ND 70 - 130 20ND

111 83.3Acetone ND 28.596 264 198 70 - 130 20ND

ND NDAcrylonitrile ND NC98 ND ND 70 - 130 20ND

ND NDBenzene ND NC102 ND ND 70 - 130 20ND

ND NDBenzyl chloride ND NC124 ND ND 70 - 130 20ND

ND NDBromodichloromethane ND NC101 ND ND 70 - 130 20ND

ND NDBromoform ND NC115 ND ND 70 - 130 20ND

ND NDBromomethane ND NC96 ND ND 70 - 130 20ND

ND NDCarbon Disulfide ND NC97 ND ND 70 - 130 20ND

0.06 0.05Carbon Tetrachloride ND 18.2104 0.377 0.314 70 - 130 20ND

ND NDChlorobenzene ND NC99 ND ND 70 - 130 20ND

ND NDChloroethane ND NC95 ND ND 70 - 130 20ND

0.78 0.7Chloroform ND 10.888 3.81 3.42 70 - 130 20ND

ND NDChloromethane ND NC95 ND ND 70 - 130 20ND

0.67 0.55Cis-1,2-Dichloroethene ND 19.798 2.65 2.18 70 - 130 20ND

ND NDcis-1,3-Dichloropropene ND NC102 ND ND 70 - 130 20ND

ND NDCyclohexane ND NC102 ND ND 70 - 130 20ND

ND NDDibromochloromethane ND NC109 ND ND 70 - 130 20ND

0.33 0.38Dichlorodifluoromethane ND 14.1104 1.63 1.88 70 - 130 20ND

4.99 4.74Ethanol ND 5.191 9.40 8.92 70 - 130 20ND

Page 1 of 2

QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBG34092

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

ND NDEthyl acetate ND NC102 ND ND 70 - 130 20ND

ND NDEthylbenzene ND NC105 ND ND 70 - 130 20ND

0.28 0.31Heptane ND 10.297 1.15 1.27 70 - 130 20ND

ND NDHexachlorobutadiene ND NC88 ND ND 70 - 130 20ND

ND NDHexane ND NC87 ND ND 70 - 130 20ND

1.98 1.5Isopropylalcohol ND 27.6101 4.86 3.68 70 - 130 20ND

ND NDIsopropylbenzene ND NC106 ND ND 70 - 130 20ND

0.24 NDm,p-Xylene ND NC106 1.04 ND 70 - 130 20ND

6.74 5.31Methyl Ethyl Ketone ND 23.7100 19.9 15.6 70 - 130 20ND

ND NDMethyl tert-butyl ether(MTBE) ND NC103 ND ND 70 - 130 20ND

0.46 0.29Methylene Chloride ND 45.386 1.60 1.01 70 - 130 20ND

ND NDn-Butylbenzene ND NC113 ND ND 70 - 130 20ND

ND NDo-Xylene ND NC105 ND ND 70 - 130 20ND

3.03 2.08Propylene ND 37.2105 5.21 3.58 70 - 130 20ND

ND NDsec-Butylbenzene ND NC106 ND ND 70 - 130 20ND

ND NDStyrene ND NC108 ND ND 70 - 130 20ND

0.3 0.24Tetrachloroethene ND 22.2103 2.03 1.63 70 - 130 20ND

ND NDTetrahydrofuran ND NC108 ND ND 70 - 130 20ND

0.48 0.39Toluene ND 20.7103 1.81 1.47 70 - 130 20ND

ND NDTrans-1,2-Dichloroethene ND NC97 ND ND 70 - 130 20ND

ND NDtrans-1,3-Dichloropropene ND NC105 ND ND 70 - 130 20ND

4.49 4.51Trichloroethene ND 0.498 24.1 24.2 70 - 130 20ND

0.24 0.19Trichlorofluoromethane ND 23.398 1.35 1.07 70 - 130 20ND

ND NDTrichlorotrifluoroethane ND NC94 ND ND 70 - 130 20ND

ND NDVinyl Chloride ND NC96 ND ND 70 - 130 20ND

108 102% Bromofluorobenzene 104 5.7100 108 102 70 - 130 20104







Page 2 of 2



UnitsCriteria

GBG34092 - EBCCriteria: None

RLCriteria

State: NY

#Error*** No Data to Display ***


ATTACHMENT E EHI 2004 PHASE I REPORT

ATTACHMENT F Emteque 2012 PHASE I REPORT

ATTACHMENT G NOVA 2004 Phase II Report

ATTACHMENT H AKRF 2009 Phase II Report

brooklyn, new york remedial investigation report · brooklyn, new york remedial investigation...

Documents