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B.TECH.-II (CHEMICAL) 3rd SEMESTER SCHEME FOR TEACHING AND EXAMINATION CS: Core Subject EIS: Elective Interdisciplinary Subject ES: Elective Subject (from Department) IS: Interdisciplinary Subject

Teaching Scheme Examination Scheme

Hours per Week Theory Practicals Sr. No. Course Code Credits

L Tu Pr Hr Sessional Tu End Sem

Sess ional

End Sem

Total Marks

1 Engineering Chemistry-II (IS-1)

CY 201 5 3 1 2 2 50 25 50 20 30 175

2 Engineering Mathematics-III (IS-2)

MH 210 5 4 1 0 2 50 25 50 --- --- 125

3 Solid Mechanics (IS-3)

AM 203 5 4 0 2 2 50 --- 50 20 30 150

4 Chemical Engineering Materials (CS-1)

CH 201 4 3 1 0 2 50 25 50 --- --- 125

5 Unit Processes (CS-2) CH 203 3 3 0 0 2 50 --- 50 --- --- 100 TOTAL 22 17 3 4 250 75 250 40 60 675

Total contact hours per week = 24 Total Credit = 22 Total marks = 675

B.TECH.-II (CHEMICAL) 4th SEMESTER SCHEME FOR TEACHING AND EXAMINATION Teaching Scheme Examination Scheme

Hours per Week Theory Practicals Sr. No. Course Code Credits

L Tu Pr Hr Sess ional Tu End Sem

Sess ional

End Sem

Total Marks

1 Electrical Technology (IS-1)

EE 214 4 3 0 2 2 50 --- 50 20 30 150

2 Engineering Chemistry-III (IS-2)

CY 202 5 3 1 2 2 50 25 50 20 30 175

3 Theory of Machines and Machine Design (IS-3)

ME 214 5 3 1 2 2 50 25 50 20 30 175

4 General Chemical Technology (CS-1)

CH 202 5 3 1 2 2 50 25 50 20 30 175

5 Process Calculations (CS-2)

CH 204 4 3 1 0 2 50 25 50 --- --- 125

TOTAL 23 15 4 8 250 100 250 80 120 800

Total contact hours per week = 27 Total Credit = 23 Total marks = 800

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B.Tech. II (CH), Semester III L T P C CY 201: ENGINEERING CHEMISTRY - II 3 1 2 5

SEPARATION METHODS (06 Hours)

Concepts of precipitation, fractional distillation, fractional crystallization, electrodeposition, electro-dialysis, reverse osmosis, distribution (partition co efficient), Chromatography Basic concepts; paper chromatography and thin layer chromatography with suitable examples.

CHEMICAL ANALYSIS OF WATER (04 Hours) Specifications of water; cooling water (Langelier Index and its treatment); tertiary waste water treatment; introduction to heavy water and rain water harvesting.

ORGANIC CHEMISTRY (11Hours) Preparation, properties and uses of alcohols (ethanol, ethylene glycol, glycerol).Carbohydrates structures, stereochemistry and reactions of monosaccharides (glucose and fructose), disaccharides (sucrose and maltose), polysaccharides (starch and cellulose). Peptides and proteins - general methods of protein structure determination with suitable examples; introduction to enzymes. Basic concepts of drug design; some drug types (antimalarials, antibiotics, antiseptic), structure and synthesis; antimalarials (4 and 8 anthraquinolines), antiseptics, antibiotics (chloramphenicol, peniclillin). Newer concepts of dyes development/high-tech dyes (Liquid crystalline,fluorescent, biomedicinal dyes), natural and photochromic dyes.

INSTRUMENTAL METHODS OF CHEMICAL ANALYSIS (06 Hours) Instrumental methods of chemical analysis (Basic concepts and relevant applications); Spectroscopic methods IR, UV- Visible, and fluorescence spectroscopy. TGA, DTA, DC polarography. Significant figures and expression of data.

POLYMERS (06 Hours) Engineering polymers, plastics, composites and their characterization. Novel functional polymers- processing and applications.

NEW APPROACH IN CHEMISTRY (06 Hours) Green chemical technology with few examples. Photochemical reactions: basic concepts and relevant Examples. Some aspects of supramolecular chemistry

REACTIONS AND MECHANISMS (06 Hours) Organic reactions and mechanisms: types of organic reactions; general methods of getting mechanisms, mechanism of ionic, free radical and isopolar reactions

(Total Contact Hours: 45) PRACTICALS:

1. Separation of SO42- from NO3- by BaSO4 precipitation. 2. Determination of total dissolved solids in a given water sample by Conductometric method. 3. Separation of Cu2+ from Ni2+ by Electrodeposition. 4. Spectrophotometric analysis of any two important impurities of water like Ca2+, Mg2+, Fe2+, NO3- ,

NO2-, PO4-3, CO3-2, Cl-, SO4-2 5. Organic spotting of Salicylic acid, Naphthalene, Aniline, Glycerol etc. 6. Electrogravimetric analysis of Cu in Non-ferrous alloys like brass. 7. Estimation of HCl and HAc using Conductometric acid base titration. 8. Coulometric titration of As2O3 by Internal generation of I2. 9. Separation of Amino acids by Paper Chromatography. 10. To determine the specific rotation of given substance using different concentration of sucrose.

BOOKS RECOMMENDED:

1. Chawla S., Text Book of Engineering Chemistry, Dhanpat Rai & Co. Pvt. Ltd., Delhi, 2003. 2. Sharma B. K., Engineering Chemistry, Krishna Prakashan Media (P) Ltd, Meerut.,2001 3. Ewing G. W., Instrumental Methods of Chemical Analysis, Tata-McGraw Hill., New Delhi, 2001. 4. Khopkar S. M., Basis Concept of Analytical Chemistry, New Age International Publishers, 1998. 5. Vogel A. I., A Text Book of Quantitative Chemical Analysis, ELBS UK, 5th Edition, 1996. 6. Billmeyer F. W., A Text Book of Polymer Science, Wiley Interscience, New York, 3rd ed., 1984.

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B. Tech. II (CH), Semester - III L T P C MH 210: ENGINEERING MATHEMATICS - III 4 1 0 5 ___________________________________________________________________________________________

CALCULUS, MULTIPLE INTEGRALS (08 Hours) Reorientation of concepts of integrals, Double and Triple integrals, evaluation techniques, change of order of Integration, change of variable, Application of double and triple integrals for evaluation of area, volume and mass.

BASIC CONCEPTS OF VECTOR CALCULUS (08 Hours)

Line Integrals, scalar and vector point function, differential operator, gradient, directional derivative, physical meaning of gradient, divergence, curl and Laplacian with their properties, Surface Integral, Volume integral, Greens ,Gauss and Stokes theorem & application.

FOURIER SERIES (06 Hours)

Definition, Fourier series with arbitrary period, in particular periodic function with period 2 . Fourier series of even and odd function, Half range Fourier series.

PARTIAL DIFFERENTIAL EQUATION (06 Hours)

Second order pde of mathematical physics (Heat, wave and Laplace equation, one dimensional with standard boundary conditions, solution by separation of variable method using Fourier series.

FOURIER INTEGRAL & TRANSFORM (06 Hours)

Fourier Integral theorem, Fourier sine and cosine integral complex form of integral, Inversion formula for Fourier transforms, Fourier transforms of the derivative of a function, Application of Fourier transforms to boundary value problems.

COMPLEX VARIABLES (08 Hours)

Basic mathematical concept, Analytic function, C R equations, Harmonic functions, its applications, Linear transformation of complex domain, some special transformation, bilinear transformations, conformal mapping and its application, complex integration including contour integration.

ELEMENTS OF STATISTICS & PROBABILITY (08 Hours) Correlation between two variable, application of correlation, evaluation of coefficients of correlation, Rank correlation, Regression, frequency distribution, Binomial, Poissons distribution and Normal distribution, application to industrial problem, Test of significance, Chi-square ( )2 test, students t Test, application of the t-test, F-distribution.

(Total Contact Hours: 50) __________________________________________________________________________________

BOOKS RECOMMENDED :

1. Kreyszing E., Advanced Engineering Mathematics, John Wiley & Sons, Singapore, Int. Student Ed. 1995. 2. Wiley C. R., Advanced Engineering Mathematics, McGraw Hill Inc., New York Ed. 1993. 3. ONeel Peter., Advanced Engg. Mathematics, Thompson, Singapore, Ind. Ed. 2002.

4. Greenbar Michael D., Advanced Engg. Mathematics, Pearson, Singapore, Ind. Ed. 2007. 5. Ramana D. V., Higher Engg. Mathematics, The MaGraw-Hill Inc., New Delhi, 2007.

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L T P CB. Tech. II (CH), Semester - III

AM 203 : Solid Mechanics 4 0 2 5

STRESSES AND STRAINS (Hours-06)

Concept of stresses and strains Types of stresses Hooks Law Lateral strain Poissons ratio Elongation due to own weight Tapering sections Varying cross sections Composite sections Relation between Modulus of Elasticity, Modulus of Rigidity and Bulk Modulus Thermal Stresses Eccentric load Limit of eccentricity Core /Kernel of the section.

SHEAR FORCE DIAGRAM AND BENDING MOMENT DIAGRAM (Hours-06) Types of beams Types of supports Types of loads shear force Bending moment Sign conventions Overhanging beams Point of contraflexure Varying loads Relation between SF and BM.

STRESSES IN BEAMS (Hours-06) Theory of simple bending Moment of Resistance Beam of Uniform strength Flitched beams Shear stress concept Derivation of shear stress Shear stress variation in rectangular, circular, T-section and I section

SPRINGS (Hours-04) Types of springs Close coiled helical spring subjected to axial load and twist Leaf springs Semi elliptical and Quarter elliptical leaf springs

PRINCIPAL STRESSES (Hours-02) Principal plane Principal stress Tangential and normal stress Derivation of Major and Minor principal stresses for different cases Mohrs circle graphical method

THEORIES OF FAILURE (Hours-02) THIN CYLINDERS (Hours-04)

Stresses in cylinders Thin cylinders and thin spheres Volumetric strain Wire wound thin cylinders. WELDED JOINTS (Hours -02)

TORSION (Hours-06) Basic theory of Torsion Solid shaft Hollow shaft Power transmitted by shaft Composite shafts

COLUMN AND STRUTS (Hours-06) Eulers theory for columns Different end conditions Rankines formula Limitations of Eulers theory

STRAIN ENERGY (Hours-04) Strain energy Resilience Strain energy due to Tension and compression - Strain energy due to freely falling load

PRACTICALS

1. Tension Test on MS and CI specimens 2. Torsion Test on MS Specimen 3. Charpy Impact Test 4. Transverse Test on Wooden beam 5. Spring Test 6. Compression test on CI Columns 7. Shear Strength Test 8. Hardness Test

BOOKS RECOMMENDED:

1. Timoshenko S & Young D H Elements of Strength of Materials, Tata Mc Graw Hill, New Delhi, 2006. 2. Ryder G H, Strength of Material, English Language Book Society, New Delhi,2006 3. Bhavikatti S S Strength of Materials, Vikas Publication House, New Delhi,2007 4. Egar P. Popov & Toader A . Balan Engineering Mechanics of Solids 2nd Edition, Prentice Hall of India

Pvt Ltd, New Delhi,2002 5. Beer F. P. & Johnston S J, Strength of Materials Tata Mc Graw Hill Publication, New Delhi,2004

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B.Tech. II (CH), Semester III L T P C CH 201: CHEMICAL ENGINEERING MATERIALS 3 1 0 4

CONCEPTS FROM PHYSICAL MATALLURGY (08 Hours) Structure of atoms and molecules, Bonding in solids, Crystal structure, Methods of determination of structures, Imperfection in crystals, Solid phases and phase diagrams, solid solutions, Ficks law.

MECHANICAL PROPERTIES (08 Hours) Structure of high polymers phase transformation, deformation of metals, creep, fracture, fatigue, radiation damage equilibrium diagrams, iron-carbon diagrams.

ENGINEERING PROPERTIES (04 Hours) Methods of fabrication of materials like timber, plastics, rubber, fibers and other polymeric materials.

FERROUS METALS (06 Hours) Pig iron, Cast iron, Wrought iron, Steel, Alloy steels, Effects of alloying elements.

NON-FERROUS METALS AND ALLOYS (04 Hours) Aluminum, Copper, Lead, Tin, Bearing metals, Zinc, Nickel.

INORGANIC, ORGANIC AND OTHER MATERIALS (07 Hours)

Crystalline and non-crystalline ceramic systems, Glass and porcelain enamels, Cement refractories, Ceramics.

CORROSION AND ITS PREVENTION (08 Hours) Protective coatings, chemical principles involved. Factors determining the choice of materials of construction in chemical industries.

(Total Contact Hours: 45) BOOKS RECOMMENDED:

1. ZasterZebski D., Nature and Properties of Engineering Materials, John Wiely & Sons, 2nd Edition, 1976. 2. Rumford F., Chemical Engineering Materials, Constable and Company Limited, 2nd Edition, 1987. 3. Vlack V., Elements of Material Science & Engineering Structures, Properties and Performance, Wesley

Publishing Company, 2nd Edition, 1964. 4. Chaudhry H., Chemical Engineering Materials Indian Book Distributing Company, 2nd Edition, Delhi, 1982. 5. Lee and Evans, Selecting Engineering Materials for Chemical and Process Plants, Business Works, 1978.

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B.Tech. II (CH), Semester-III L T P C CH 203: UNIT PROCESSES 3 0 0 3

INTRODUCTION (4 Hours) Definition and importance of Unit processes in Chemical Engg., Outlines of unit processes, and operations, Chemical process kinetics and Factors affecting it, Symbols used in Chem. Engg. Process flow diagram.

NITRATION (5 Hours)

Definition & scope of nitration reactions, Nitrating agents, Aromatic Nitration (schimid and Biazz; nitrators)mixed acid for nitration, D.V.S. value and nitric reaction, Comparison of batch Vs. Cont. nitration, Mfg. of Nitrobenzene, Dinitrobenzene, O-and P-Chloronitrobenzene.

AMINATION BY REDUCTION (6 Hours)

Definition & scope of Amination reactions, various methods of reductions and factors affecting it, Batch and Cont. process for manufacture of Aniline from Nitrobenzene, Cont. process for Mfg. of Aniline from nitrobenzene using catalytic fluidized bed reactor, M/c. in such processes.

HALOGENATION (6 Hours)

Definition and scope of various halogenation reactions, Halogenating agents Industrial halogenation with types of equipments and its materials M/c. MFG. of Chlorobenzene, Benzene hexa-chloride and vinyl chloride from Ethylene and Acetylene.

SULFONATION AND SULFATION (3 Hours)

Definition and scope of such reactions, sulfonating and sulfating agents and their applications, Chemical and physical factors affecting it. Industrial equipments and techniques for batch Vs. Cont. sulfonation, Mfg. of Benzene sulfonates, Sulfation of Dimethyl Ether and Lauryl Alcohol.

AMINATION BY AMMONOLYSIS (3 Hours)

Definition & types of reactions, Aminating agents, Physical and Chemical factors affecting it. Catalyst used in Ammonolysis, Mfg. of Aniline from chlorobenzene and Nitroaniline from Dichloro Nitro Aniline.

OXIDATION (5 Hours)

Definition and Types, Oxidizing agents, Liquid phase oxidation with oxidizing agents and oxygen. Oxidation of toluene with MnO2. Mfg. of Acetaldehyde from Acetic acid and mfg. of Acetic acid from Ethanol. Vapor phase oxidation of Methanol, Benzene and Naphthalene, Apparatus and its M/s. for oxidation reactions.

HYDROGENATION (5 Hours)

Definition and its scope, properties of hydrogen and sources of hydrogen, gas catalytic hydrogenation and hydrogenolysis, factors affecting it, Apparatus and M/c., Industrial hydrogenation of fat & oil, Mfg. of Methanol from CO2 & H2.

HYDROLYSIS (3 Hours)

Definition and types of hydrolysis, Hydrolyzing agents, equipments of hydrolysis, Industrial Hydrolysis of fat, hydrolysis of carbohydrates, starch to dextrose, Mfg. of ethanol from ethylene (shell process) Mfg. of phenol from benzene sulfonic.

POLYMERIZATION (5 Hours)

Introduction & chemistry of polymerization reactions, classifications of polymers methods of polymerization. (Total contact time : 45 Hours) BOOKS RECOMMENDED: 1. Groggins P. H., Unit Processing of Organic Synthesis, 5th edition, Tata-McGraw Hill, New Delhi, 2001. 2. Gopalarao. M. & Sitting M., Drydens Outlines of Chemical Tech., 2nd Ed., East-West Pub., New Delhi,

1997. 3. Austin G. T., Shreves Chemical Process Industries, 5th Ed. McGraw-Hill Pub., 1994. 4. Felder R.M., Rousseau R.W., "Elementary Principles of Chemical Processes", 3rd ed., John Wiley, New

York, 2000. 5. Kent J.A., Riggels Handbook of Industrial Chemistry, Van Nostrant Reinhold, 1974.

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B.Tech. II (CH), Semester IV L T P C EE 214: ELECTRICAL TECHNOLOGY 3 0 2 4

Construction, windings, EMF, torque and power equations, circuit model, Generating and Motoring modes, introduction to armature reaction, Types of generators and motors and their characteristics, Efficiency and Losses, Speed control of D C motors

D.C. MACHINES ( 08 Hours)

Review of equivalent circuit, no load and short circuit tests, per unit system, voltage regulation, Efficiency, Auto-transformer, three phase transformers, star and delta connection.

TRANSFORMERS (07 Hours)

Review of equivalent circuit, torque speed characteristics, No load and blocked rotor tests, load test, efficiency and losses , starting, Braking & speed control.

INDUCTION MACHINE ( 06 Hours)

SYNCHRONOUS-MACHINE (07Hours)

Construction and basic principals, EMF equation, Synchronous speed, armature reaction, synchronous reactance, voltage regulation, vector diagram for generating and motoring modes, synchronous motor starting, Synchronous condensers.

SPECIAL MACHINE (06

Hours) Theory, performance and applications of Servo motors, Stepper motors.

Cost of Generation and Supply (Tariff), Power factor and its effect on system economy, power factor improvement.

ELECTRICAL MEASUREMENT AND INSTRUMENTS (04 Hours) Principles of measurement of voltage, current, Power, Energy, Electrical parameters and measuring instruments.

PRINCIPLES OF ELECTRICAL POWER SYSTEMS (03 Hours)

Generation of Electrical power, transmission of Electrical power, distribution of Electrical power .

ECONOMIC ASPECTS OF POWER SYSTEM (04 Hours)

(Total Contact Hours: 45) PRACTICALS: 1. Speed control of D.C. shunt motor. 2. Speed Torque Characteristics of D.C. Shunt motor. 3. D.C. Series motor N.T. characteristics. 4. D.C. Generator Characteristics. 5. Efficiency and regulation of 1 phase Transformer from O.C. and S.C. test . 6. Load test on Induction motor. 7. Circle diagram. 8. Regulation of an alternator by synchronous impedance method. 9. V and inverted V curve . 10. Calibration of single phase energy meter. BOOKS RECOMMENDED: 1 Mehta, V.K.,Principles of Power System S. Chand & Co., New Delhi, 2005 2 Husain A., Fundamentals of Electrical Engineering, Dhanpat Rai & Co., Delhi, 2001 3. Bimbhra P.S., Electrical machinery ,Khanna Pub.,Delhi,1998 4. Mukherjee P.K., Chakravorti S. ,Electrical Machines Dhanpat Rai & Co., Delhi, 2001 5. Thereja B.L., & Thereja A.K., A Text Book of Electrical Technology, S. Chand & Co., New Delhi, 2005 7

B.Tech. II (CH), Semester IV L T P C CY 202: ENGINEERING CHEMISTRY - III 3 1 2 5

SEPARATION TECHNIQUES AND STRUCTURAL CHARACTERIZATION (10 Hours) Introductory discussion of mass, GC, HPLC, GC-MS, PMR, XRD, SEM, TEM.

CHEMICAL KINETICS (04 Hours)

Chemical equilibrium, determination of rate and order of reaction, ultra fast processes, kinetics of enzyme catalysis

THERMODYNAMICS (04 Hours)

Laws of thermodynamics, Clapeyron clausius equation, carnot cycle

SURFACE CHEMISTRY (05 Hours) Roughness and friction lubricants, absorption adsorption isotherms, catalysis, surface characterization, organic assemblies; synthesis, structure, property and application of nanoparticles

A.FUELS (10 Hours)

Classification, characteristics, combustion, calorific value and its determination by Bomb and Bouys calorimeters, theoretical calculations by Dulong formula, analysis of coal and fuel gases, fuel cells, H2 as fuel and biofuels

B.NUCLEAR CHEMISTRY Nuclear fission and fusion, nuclear energy, nuclear reactors, disposal of nuclear waste, radiation measurement and contentment

COORDINATION COMPOUNDS AND ORGANOMETALLICS (06 Hours)

Structure and bonding, its application in catalysis; biological role of iron, magnesium and manganese (hemoglobin and chlorophyll)

CORROSION AND ITS CONTROL (06 Hours)

Pourbiax diagram, boiler corrosion, intergranular corrosion and bio-corrosion. Selection of material like SS, Ti/Zr alloy and design for corrosion control, corrosion inhibitors, cathodic and anodic protection

(Total Contact Hours: 45)

PRACTICALS:

1. Rate determination of chemical reactions. 2. Conductometric rate determination of esterification reaction. 3. Potentiometric estimation of Cu+2 by titration with EDTA. 4. Photometric estimation of Ti. 5. Estimation of Cu+2 by iodimetric titration. 6. Viscosity measurement. 7. Study of Corrosion of Steel at different concentration of Sulfuric Acid OR Study of effect of inhibitors on corrosion of steel in sulphuric acid.

8. Demo: 1. Effects of removal of DO on corrosion. 9. Demo: 2. Anodic protection of steel in sulphuric acid. BOOKS RECOMMENDED:

1. Atkins P. & de Paula J., Physical chemistry, Oxford University Press, UK, 2002. 2. Chawla S., Text Book of Engineering Chemistry, Dhanpat Rai & Co., Delhi, 2003. 3. Dara S. S., A Text Book of Enginering Chemistry, S Chand & Sons., New Delhi, 2004. 4. Fontana M. G., Corrosion Engineering., Tata-McGraw Hill, New Delhi,1988. 5. Skoog, West & Holler,Analytical Chemistry: An Introduction, 6th edition, Saunders College Publishing,

1994.

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B. Tech. II (CH) Semester-IV L T P C

ME 214: THEORY OF MACHINES AND MACHINE DESIGN 3 1 2 5

THEORY OF MACHINES:

INTRODUCTION TO MACHINES AND MECHANISMS (07 Hours) Introduction, Mechanism and machine, Rigid and Resistant body, Link, Kinematic pair, Types of motion, Degrees of Freedom (Mobility), Classification of Kinematic pairs, Kinematic Chain, Linkage, Kinematic Inversion, Inversions of Slider-Crank Chain, Double Slider-Crank Chain.

CAMS (06 Hours)

Introduction, Types of Cams, Types of Followers, Cam Terminology, Displacement Diagrams, Motions of the Follower, Drawing of Cam Profile.

GEARS (05Hours) Different Types of Motion Transmitting Elements, Advantages and Disadvantages, Types of Gears and Gear trains, Gear Terminology and classification.

FRICTION (05 Hours) Introduction to Friction, Significance of Friction, its Merits and Demerits, Application of Friction to Screw Jack, Bearings, Breaks, Clutches etc.

MACHINE DESIGN:

DESIGN PROCESS, MATERIAL SELECTION, FACTOR OF SAFETY, FAILURES & THEIR CAUSES (07 Hours) Introduction, Types of Load, Design Process, Material Selection, Factor of Safety, Failure and Their Causes, Introduction to Corrosion (Design Aspect).

DESIGN OF JOINTS (07 Hours) Introduction, Different types of Joints and Their Applications, Design of Bolts and Rivets joints, Design of Screw Joint, Design of Welded Joints (Efficiency & Strength).

DESIGN OF POWER TRANSMISSION ELEMENTS (08 Hours) Introduction, Stresses Induced in the Shaft Under Different Conditions, Selection of Keys, Selection of Bearings, Power Rating of Spur/Helical Gears, Power Transmitting Capacity of Flat & V Belt.

(Total Contact Hours: 45)

PRACTICALS:

Design and Drawing of various machine elements using conventional methods and few drawing sheets will be prepared using CAD software.

BOOKS RECOMMENDED:

1. Rattan, S.S.: Theory of Machines, Tata McGraw-Hill Publishing Co. Ltd., New Delhi, 1984. 2. Rao, J.S., and Dukkipati, R.V.: Mechanism and Machine Theory, Wiley Eastern Ltd., 1992. 3. Green, W.G.: Theory of Machines, 2nd Ed., Balckie, London, 1992. 4. Bhandari, V.B.: Design of Machine Elements, Tata McGraw-Hill Publishing Co. Ltd., 1984. 5. Shigley, J.: Mechanical Engineering Design, McGraw Hill Book Co., 1989.

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B.Tech. II (CH), Semester-IV L T P C CH 202: GENERAL CHEMICAL TECHNOLOGY 3 1 2 5

CHLOR-ALKALI INDUSTRY ( 4 Hours) Manufacture of soda ash, Caustic Soda, Chlorine, hydrogen and Hydrochloric acid. CEMENT & GLASS MANUFACTURE (4 Hours)

Portland cements, other cements, Methods and manufacture of special Glasses SULFURIC ACID MANUFACTURE (2 Hours) PULP & PAPER INDUSTRY (3 Hours)

Cellulose derivatives, pulp , paper & board. SUGAR & STARCH INDUSTRY (3 Hours)

Sugar, starches and related products OIL, FATS, SOAPS AND DETERGENTS (3 Hours)

Vegetable Oils, animal fats, their nature, analysis& extracted methods, Hydrogenations oil, Fatty acids and alcohol, waxes, soap, synthetic detergent.

POLYMER INDUSTRY: (4 Hours) Manufacture of Phenol and Urea Formaldehyde resin, PVC, Polyethylene, Synthetic rubber etc.

SYNTHETIC FIBER INDUSTRY: (4 Hours) Nylon, Polyester, Acrylics, and Rayons. FINE CHEMICALS AND DRUGS (5 Hours)

Classifications of pharmaceuticals, manufacture of important drugs and pharmaceuticals, salicylic acid, Methyl salicylate, Aspirin, Anti-biotics, Vitamins.

INTRODUCTION TO N & P FERTILIZERS. (3 Hours) INTRODUCTION TO PETROLEUM REFINING & PETROCHEMICAL INDUSTRY (10 Hours)

(Total Contact Hours: 45) PRACTICALS

1. Preparation of Boric acid by acidified solution of Borax (Na2B4O7). 2. Preparation of CaCl2 from HCl and lime (CaCO3). 3. Preparation of detergent. 4. Preparation of nitro naphthalene from given chemicals. 5. Preparation of polystyrene from styrene monomer. 6. Preparation of Potash alum from Aluminium Sulphate and Potassium sulphate. 7. Preparation of soap from KOH and coconut oil 8. Determination of the kinematic viscosity of given oil sample using Engler viscometer& Red Wood

Viscometer. 9. Determination of the aniline point of diesel using proper instruments. 10. Determination of the smoke point of kerosene and diesel. 11. Measurement of the softening point of grease sample. 12. Determination of the penetration index using pentrometer. 13. Determination of flash point and fire point of kerosene using Pensky Martin apparatus. 14. ASTM Distillation of gasoline.

BOOKS RECOMMENDED: 1. Austin G. T., Shreves Chemical Process Industries, 5th Ed. McGraw-Hill Pub., 1994. 2. Gopalarao M. & Sitting M., Drydens Outlines of Chemical Tech., 2nd Ed., East-West Pub., New

Delhi,1997 3. Rao B.K.B., Modern Petroleum Refining Processes, 4th ed.,Oxford & IBH Publishing Co. Pvt. Ltd., New

Delhi, 2002. 4. Nelson, W.L., Petroleum Refinry Engineering, 4th ed. (International student edition), McGraw-Hill

Kogakusha, Ltd., Tokyo, 1958. 5. Mall I.D., Petrochemicals Process Technology, Macmillan India Ltd, New Delhi, 2006.

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B.Tech. II (CH), Semester-IV L T P C CH 204: PROCESS CALCULATIONS 3 1 0 4

INTRODUCTION (4 Hours) Dimension and Units, Fundamental and derived quantities, Mathematical techniques in chemical

engineering.

BASIC CHEMICAL CALCULATIONS (6 Hours) Gas laws and phase equilibria, Humidity, saturation and crystallization.

COMBUSTION (8 Hours) Combustion and chemical processes.

MATERIAL BALANCE (9 Hours) Material balances involving recycle, bypass and purge systems.

THERMOPHYSICS (8 Hours) Heat capacity calculations. Enthalpy changes of reactions, dissolution and laws of thermochemistry. Effect

of pressure and temperature on heat of reactions.

MATERIAL AND ENERGY BALANCE (10 Hours) Combined material and energy balances for single stage processes. Material and energy balance calculations for

industrial processes.

(Total Contact Hours: 45) BOOKS RECOMMENDED:

1. Bhatt B.I. & Vora S.M., "Stoichiometry, 4th Ed., Tata-McGraw-Hill, New Delhi, 2004 2. Hougen O.A., Watson K.M. & Ragatz R.A., Chemical Process Principals: Part-I, 2nd Ed., CBS Publishers and Distributors, New Delhi, 1995. 3. Himmelblau D.M., Basics Principles and Calculations in Chemical Engineering 6th Ed., Prentice-Hall India,1996. 4. Whitwell J.C. & Jone R.K., Conservation of Mass and Energy, McGraw-Hill, Singapore, 1973. 5. Process Calculation for Chemical Engineering, Second Revised Edition, Chemical Engineering Education Development Centre, I.I.T., Madras, 1981.

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B.TECH.-III (CHEMICAL) 5th SEMESTER SCHEME FOR TEACHING AND EXAMINATION CS: Core Subject EIS: Elective Interdisciplinary Subject

ES: Elective Subject (from Department) IS: Interdisciplinary Subject Teaching Scheme Examination Scheme Hours per Week Theory Practicals Sr.

No. Course Code Credits L Tu Pr Hr Sess ional Tu End Sem

Sess ional

End Sem

Total Marks

1 Chemical Engineering Thermodynamics-I (CS-1)

CH 301 4 3 1 0 2 50 25 50 --- --- 125

2 Heat Transfer Operations (CS-2)

CH 303 5 3 1 2 2 50 25 50 20 30 175

3 Mass Transfer Operations-I (CS-3)

CH 305 5 3 1 2 2 50 25 50 20 30 175

4 Mechanical Operations (CS-4)

CH 307 5 3 1 2 2 50 25 50 20 30 175

5 EIS-1* 3 3 0 0 2 50 --- 50 --- --- 100 TOTAL 22 15 4 6 250 100 250 60 90 750 Total contact hours per week = 25 Total Credit = 22 Total marks = 750

B.TECH.-III (CHEMICAL) 6th SEMESTER SCHEME FOR TEACHING AND EXAMINATION Teaching Scheme Examination Scheme

Hours per Week Theory Practicals Sr. No. Course Code Credits

L Tu Pr Hr Sess ional Tu End Sem

Sess ional

End Sem

Total Marks

1 Chemical Engineering Thermodynamics-II (CS-1)

CH 302 4 3 1 0 2 50 25 50 --- --- 125

2 Chemical Reaction Engineering -I (CS-2)

CH 304 5 3 1 2 2 50 25 50 20 30 175

3 Fluid Flow Operations (CS-3)

CH 306 5 3 1 2 2 50 25 50 20 30 175

4 Mass Transfer Operations-II (CS-4)

CH 308 5 3 1 2 2 50 25 50 20 30 175

5 EIS-2* 3 3 0 0 2 50 --- 50 --- --- 100 TOTAL 22 15 4 6 250 100 250 60 90 750 Total contact hours per week = 25 Total Credit = 22 Total marks = 750

* Students have to opt for one subject from each Elective Interdisciplinary Subject Group-1 & 2 as listed below: EIS: Elective Interdisciplinary Subjects (Group-1)# EIS: Elective Interdisciplinary Subjects (Group-2)# CH 309: Bioprocess Engineering CH 311: Energy Technology CH 313: Fertilizer Technology CH 315: Fuels and Combustion CH 317: Polymer Science and Engineering

CH 312: Bioseparations CH 314: Cleaner Technologies in Chemical Process Industries CH 316: Introduction to Industrial Biotechnology CH 318 Petrochemical Technology CH 322: Petroleum Refinery Engineering

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B.Tech.-IV (CHEMICAL) 7th SEMESTER SCHEME FOR TEACHING AND EXAMINATION CS: Core Subject ES: Elective Subject (from Department)

Teaching Scheme Examination Scheme

Hours per Week Theory Practicals

Sr. No. Course Code Credits

L Tu Pr Hr Sess ional Tu End Sem

Sess ional

End Sem

Total Marks

1 Chemical Reaction Engineering-II (CS-1)

CH 401 3 3 0 0 2 50 --- 50 --- --- 100

2 Instrumentation and Process Control (CS-2)

CH 403 5 3 1 2 2 50 25 50 20 30 175

3 Process Equipment Design and Drawing (CS-3)

CH 405 5 3 1 2 2 50 25 50 20 30 175

4 Transport Phenomena (CS-4) CH 407 4 3 1 0 2 50 25 50 --- --- 125

5 ES-1** 3 3 0 0 2 50 --- 50 --- --- 100 6 Seminar CH 409 1 0 0 2 --- --- --- --- 20 30 50 7 Project Preliminaries CH 411 2 0 0 4 --- --- --- --- 40 60 100 8 Training CH 413 1 0 0 0 --- --- --- --- --- 50 50 TOTAL 24 15 3 10 250 75 250 100 200 875 Total contact hours per week = 28 Total Credit = 24 Total marks = 875

B.Tech.-IV (CHEMICAL) 8th SEMESTER SCHEME FOR TEACHING AND EXAMINATION

Teaching Scheme Examination Scheme Hours per Week Theory Practicals Sr.

No. Course Code Credits L Tu Pr Hr Sess ional Tu End Sem

Sess ional

End Sem

Total Marks

1 Chemical Engineering Plant Design and Economics (CS-1)

CH 402 3 3 0 0 2 50 --- 50 --- --- 100

2 Chemical Systems Modeling (CS-2)

CH 404 3 3 0 0 2 50 --- 50 --- --- 100

3 Computer Aided Design in Chemical Engineering (CS-3)

CH 406 5 3 1 2 2 50 25 50 20 30 175

4 Safety and Pollution Control in Chemical Process Industries (CS-4)

CH 408 4 3 0 2 2 50 --- 50 20 30 150

5 ES-2** 3 3 0 0 2 50 --- 50 --- --- 100 6 Project CH 412 4 0 0 8 --- --- --- --- 80 120 200 TOTAL 22 15 1 12 250 25 250 120 180 825 Total contact hours per week = 28 Total Credit = 22 Total marks = 825

** Students have to opt for one subject from each Elective Subjects Group-1 & 2 as listed below:

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ES: Elective Subjects (Group-1)# ES: Elective Subjects (Group-2)# CH 415: Fundamentals of Biochemical Engineering CH 417: Fundamentals of Colloid and Interface Science CH 419: Fundamentals of Rheology of Materials CH 421: Industrial Waste Management and Control CH 423: Reaction Engineering for Pollution Prevention CH 425: Sustainability and Green Chemistry

CH 414: Advances in Chemical Engineering CH 416: Catalysis and Reactor Design CH 418: Fluidization Engineering CH 422: Introduction to Nanotechnology in Chemical Engineering CH 424: New Separation Techniques CH 426: Numerical Techniques and Optimization in Engineering

B.Tech. III (CH), Semester-V L T P C CH 301: CHEMICAL ENGINEERING THERMODYNAMICS - I 3 1 0 4

INTRODUCTION ( 6 Hours) Conservation of energy and first law of thermodynamics, application to steady state flow process, enthalpy, internal energy, equilibrium state, phase rule, reversible and irreversible processes, heat capacity specific heat.

PROPERTIES OF PURE SUBSTANCES ( 8 Hours) P-V-T behavior, ideal and non-ideal gases, different equations of state for real gases.

HEAT EFFECTS ( 5 Hours) Heat capacities of gases as a function of temperature of liquids and solids, heat of vaporization, heat of fusion, heat of sublimation, etc.

SECOND AND THIRD LAW OF THERMODYNAMICS ( 7 Hours) Thermodynamic temperature scale, ideal gas temperature scale, concept of entropy, entropy change and irreversibility, third law of thermodynamics.

THERMODYNAMIC PROPERTIES OF FLUID ( 8 Hours) Mathematical relation among thermodynamic functions, Mexwells relations, Interrelation between H, S, U, G, Cp, Cv, properties of single and two phase system. Types of thermodynamic diagrams.

THERMODYNAMICS OF FLOW PROCESS ( 6 Hours) Fundamental relation for flow in pipes, maximum velocity in pipe flow, throttling process, flow through nozzles, single stage and multi stage compressors.

REFRIGERATION AND LIQUEFACTION: ( 5 Hours) Carnot refrigeration cycle, air refrigeration cycle, absorption refrigeration, heat pump, choice of refrigeration, liquefaction processes.

(Total contact time: 45 hours) BOOKS RECOMMENDED: 1. Smith J. M., Van Ness H. C., M.M. Abbott, Introduction to Chemical Engineering Thermodynamics, 6th Ed., McGraw-Hill, New York, 2001 2. Dodge B. F., Chemical Engineering Thermodynamics, McGraw-Hill Book Co., New York, 1960. 3. Rao Y. V. C., Chemical Engineering Thermodynamics, Universities Press Limited, Heydrabad, 1997. 4. Kyle, B.G., "Chemical and Process Thermodynamics, 2nd Ed., Prentice-Hall of India, New Delhi,1990. 5. Sandler, S.I., "Chemical and Engineering Thermodynamics", 2nd Ed., Wiley, New York, 1989.

3

L T P C 3 1 2 5

B. Tech. III (CH), Semester V CH 303: HEAT TRANSFER OPERATIONS

INTRODUCTION (02 Hours) Modes of Heat Transfer: Conduction, Convection and Radiation

CONDUCTION (05 Hours) Fourier conduction equation, General conduction equation in Cartesian, Cylindrical and Spherical co-ordinates, Steady state and transient conduction equation.

FORCED CONVECTION (10 Hours) Heat transfer in fluids without phase change, Forced convection, Dimensional analysis, Heat transfer in laminar and turbulent flows inside and outside tubes. Concept of thermal boundary layer, Overall heat transfer coefficient, LMTD, Fouling factors, Transfer units, Flow over flat plates with heat transfer, Empirical correlations.

NATURAL CONVECTION (04 Hours) Qualitative description of free convection flows, Hear transfer correlations for free convection.

BOILING AND CONDENSATION (04 Hours) Boiling phenomena: Regimes of boiling etc, Condensation: Film and drop condensation etc.

EVAPORATION AND CRYSTALIZATION (06 Hours) Single effect and Multi-effect evaporation, Forward and backward feed system.

Equilibrium in crystallization, operation and equipment. HEAT EXCHANGERS (06 Hours)

Double pipe heat exchanger and Shell-and-tube heat exchanger, its applications and design RADIATION HEAT TRANSFER (04 Hours)

Basic concepts of radiation heat transfer, Radiative heat exchange between surfaces, Radiation shield. EXTENDED SURFACES (04 Hours)

Heat transfer from extended surfaces, fin efficiency (Total contact time: 45 hours)

PRACTICALS: 1. Experiment on Heat transfer through composite wall at different temperature 2. Experiment on Thermal conductivity of insulating powder (Asbestos powder) 3. Experiment on Heat transfer in double pipe heat exchanger in laminar flow 4. Experiment on Heat transfer in turbulent flow 5. Experiment on Heat transfer by forced convection 6. Experiment on Heat transfer coefficient in natural convection 7. Experiment on Extended surface heat transfer 8. Experiment on Shell and tube heat exchanger 9. Experiment on Heat transfer by radiation: Stefan-Boltzmann Law BOOKS RECOMMENDED: 1. McCabe W.L., Smith J.C., Harrott P., Unit Operations of Chemical Engineering, 6th & 7th Eds. McGraw-Hill, New York, 2001 & 2005. 2. Kern D. Q., Process Heat Transfer, McGraw-Hill, New York, 1950. 3. Hollman J. P., Heat Transfer Basic approach, McGraw-Hill, New York, 1985. 4. Gebhart B. U., Heat Transfer, Tata McGraw-Hill, New York, 1961. 5. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Chemical Engineering Vol. 1. 6th Ed. Elservier, New Delhi, 2004.

4

B. Tech. III (CH), Semester-V L T P C

CH 305: MASS TRANSFER OPERATIONS-I 3 1 2 5

INTRODUCTION ( 02 Hours) Introduction to Mass Transfer Operation: classification & method.

DIFFUSION AND MASS TRANSFER ( 08 Hours) Molecular diffusion in fluids, steady state diffusion (both gases & liquids), diffusivity of liquids & gases.

MASS TRANFER COEFFICIENTS ( 03 Hours)

Mass Transfer co-efficient in laminar & turbulent flow, Mass, Heat and Momentum transfer analogies

DIFFUSION IN SOLIDS ( 06 Hours)

Introduction to diffusion in solids, Ficks law, types of solid diffusion

INTER PHASE MASS TRANSFER ( 04 Hours) Equilibrium, diffusion between phases, material balance, stages

DISTILLATION ( 16 Hours)

VLE data, flash, differential and continuous distillation, McCabe-Thiele and Ponchon-Savarit method, Azeotropic, Extractive, Reactive, Molecular and Multicomponent distillation, Equipment for gas-liquid operation

HUMIDIFICATION ( 06 Hours) Vapor-gas mixtures, vapor-liquid equilibrium,gas-liquid contact operations, adiabatic & non-adiabatic operations. (Total contact time: 45 hours)

PRACTICALS 1. Humidification and dehumidification 2. Mass transfer coefficient 3. Crystallization 4. Azeotropic distillation 5. Diffusion coefficient 6. Latent heat of vaporization 7. Cooling tower 8. Packed distillation

BOOKS RECOMMENDED:

1. Treybal R.E., Mass-Transfer Operations, 3rd Ed., McGraw-Hill, New York, 1981. 2. McCabe W.L, Smith J.C., Harriott P., Unit Operations in Chemical Engineering, 6th & 7th Eds., McGraw-Hill, New York,2001 & 2005. 3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Chemical Engineering Vol. 1. 6th Ed. Elservier, New Delhi, 2004. 4. Sherwood, T.K., Pigford, R.L., Wilke, C.R., Mass Transfer, McGraw-Hill, New York, 1976. 5. Cussler E.L.,Diffusion: Mass Transfer in Fluid Systems, 2nd Ed., Cambridge University Press, Cambridge, 1997.

5

B. Tech. III (CH), Semester V L T P C

CH 307: MECHANICAL OPERATIONS 3 1 2 5

INTRODUCTION (03 Hours) Solids, Storage, Transportation and Handling of Solis, Liquid and Gases, characteristics of solid particles

SIZE REDUCTION (05 Hours)

Size reduction and enlargement, crushers, grinders, disintegrates for coarse & intermediate & fine grinding, energy and power requirements, law of crushers, work index, etc.

SCREENING AND OTHER SEPARATION METHODS (10 Hours)

Screening and other separation methods: screen analysis, estimation of particle size, surface area and particle population based on screen analysis, ideal and actual screens, principles of elutriation, flotation, jigging, electrostatics, and magnetic separation processes, Cyclones, Hydroclones, Centrifugal Decanter.

SEDIMENTATION (05 Hours)

Sedimentation, Settling velocity, flocculation, Thickener, Sedimentation zones.

FILTRATION (10 Hours) Filtration, filter media, filter aids, batch & cont. filtration, filtration equipment, filter press, leaf, cartridge, vacuum filter, rotary drum filters.

MIXING AND AGITATION (09 Hours) Equipments for agitation, agitation of liquids, types of impellers, power consumption in agitated vessels etc.

CONVEYERS (03Hours)

Mechanical and Pneumatic conveying, elevators, Bins, silos etc. (Total contact time: 45 hours)

PRACTICALS: 1. Determination of the optimum speed and critical speed of a ball mill. 2. Calculation of the overall effectiveness of screen. 3. Analysis of solid powder sample. 4. Study of Roll crusher 5. Finding characteristic constants of Jaw crusher 6. Obtaining the collection efficiency of cyclone 7. Obtaining settling rates of slurry as function of solid concentration 8. Study of pressure drop as function of superficial velocity BOOKS RECOMMENDED: 1. McCabe W.L., Smith J.C., Harriott P., Unit Operations of Chemical Engineering, 6th & 7th Eds., McGraw-Hill, New York, 2001 & 2005. 2. Foust A.S., Wenzel L.A., Clump C.W., Maus L., Anderson L.B. Principles of Unit Operations, John Wiley & Sons, New York, 1980. 3. Brown G.G., Unit Operations, John Wiley & Sons, New York, 1953. 4. Badger W.L., Banchero J.T., Introduction to Chemical Engineering, McGraw Hill, New York, 1997. 5. Coulson J.M., Richardson J.F., Chemical Engineering, Vol. 2, 5th Ed., Elservier, New Delhi, 2002.

6

B.Tech. III (CH), Semester-VI L T P C CH 302: CHEMICAL ENGINEERING THERMODYNAMICS - II 3 1 0 4

THERMODYNAMIC PROPERTIES OF FLUIDS (12 Hours)

Partial molar properties, chemical potential, non-ideal solution, fugacity, and fugacity co- efficient, for pure components and for mixture of gases, and for liquids. Lewis randall rule, Henrys law, excess property, activity and activity co-efficient.

PHASE EQUILIBRIUM (15 Hours)

Phase rule, Duhem theory, miscible system, immiscible system, partially immiscible system, testing of vapor-liquid equilibrium data, Gibbs-Duhem equation, Van Laar equation. Margules equation, Redlich-Kister equation, P-X-Y, T-X-Y, & X-Y Diagram, vapor-liquid equilibrium of ideal and non-ideal solution, Roults law & Henrys law.

CHEMICAL EQUILIBRIUM (10 Hours)

Criteria, equilibrium conversion (X), constant (K), effect of Temp. & Pressure on K, evaluation of K, evaluation of equilibrium conversion for gas phase reaction.

INTRODUCTION TO STATISTICAL THERMODYNAMICS ( 8Hours)

Stefen-Boltzman, Bose-Einstein and Fermi-Dirac distributions, corrected boltzman statistics, partition function etc.

(Total contact time: 45 hours) BOOKS RECOMMENDED: 1. Smith J. M. Van Ness H. C., Abbott M.M., Introduction to Chemical Engineering Thermodynamics, 6th & 7th Eds., McGraw-Hill, New York, 2001 & 2005. 2. Dodge B. F., Chemical Engineering Thermodynamics, McGraw-Hill, New York, 1960. 3. Rao Y. V. C., Chemical Engineering Thermodynamics, Universities Press Limited, Heydrabad, 1997. 4. Sonntag R.E., Van Wylen G.J., Fundamentals of Statistical Thermodynamics, John Wiley & Sons, Singapore, 1991. 5. Sandler, S.I., Chemical and Engineering Thermodynamics, 2nd Ed., Wiley, New York, 1989.

7

B. Tech. III (CH), Semester-VI L T P C

CH 304: CHEMICAL REACTION ENGINEERING - I 3 1 2 5

INTRODUCTION (01 Hour) Chemical kinetics, Classification of reactions, Variables affecting the rate of reaction, Reaction rate

KINETICS OF HOMOGENEOUS REACTIONS (06 Hours) Concentration dependent term and temperature dependent terms of rate equation, Single and multiple reactions, Elementary and non-elementary reactions, Molecularity and order of reaction, Rate constant, Representation of reaction rate, Kinetic models, Temperature dependency from Arrhenius law, thermodynamics, various theories, Activation energy, Searching for the reaction mechanism

INTERPRETATION OF BATCH REACTOR DATA (08 Hours) Constant volume batch reactor, Variable volume batch reactor, Integral method and differential method of analysis of kinetic data, Temperature and reaction rate

INTRODUCTION TO REACTOR DESIGN (03 Hours) Types of reactors, PFR, CSTR etc., Material & energy balances single ideal reactor, Space-time and space-velocity, Holding time, Introduction of non-ideal flow

DESIGN FOR SINGLE REACTIONS (08 Hours) Size comparison of single reactors, General graphical comparison, Multiple reactor system, Recycle

reactor, Autocatalytic reactions DESIGN FOR MULTIPLE REACTIONS SYSTEMS (08 Hours)

Reaction in parallel, Reaction in series, Series-parallel reaction and applications TEMPERATURE & PRESSURE EFFECTS (04 Hours) Single & multiple reactions, Heats of reaction from thermodynamics, Product distribution INDUSTRIAL APPLICATIONS (04 Hours)

Types of reactors used in industries, Advanced chemical reactors. INTRODUCTION TO BIOCHEMICAL REACTION ENGINEERING (03 Hours)

Types of bio-reactors, Design, scale-up, operation and control of bio-reactors, Kinetics of biochemical reactions

(Total contact time: 45 hours) PRACTICALS: 1. Integral method of analysis of kinetic data 2. Differential method of analysis of kinetic data 3. Activation energy and frequency factor 4. Half-life method 5. Pseudo first order reaction 6. Study of kinetics of the reaction in presence of DC current 7. Study of membrane reactor 8. Study of spiral coiled reactor 9. Study of annulus flow reactor 10. Study of specific reaction/reactor system BOOKS RECOMMENDED: 1. Levenspiel O., Chemical Reaction Engineering, 3rd Ed., John Wiley & Sons, Singapore, 1998. 2. Fogler H.S., Elements of Chemical Reaction Engineering, 4th Ed., Prentice-Hall, NJ, 2006. 3. Smith J. M., Chemical Engineering Kinetics, 3rd Ed., McGraw-Hill, New York, 1981. 4. Froment G.F., Bischoff K.B., Chemical Reactor Analysis and Design, 2nd Ed., John Wiley & Sons, Singapore, 1990. 5. Inamdar S.T.A., Biochemical Engineering Principles and Concepts, Prentice-Hall of India, New Delhi, 2007. 6. Shuler M.L., Kargi F., Bioprocess Engineering Basic Concepts, 2nd Ed., Prentice-Hall of India, New Delhi, 2006.

8

B. Tech. III (CH), Semester VI L T P C

CH 306: FLUID DYNAMICS 3 1 2 5

INTRODUCTION (4 hours) Definitions of Unit operations, Basic concepts of fluids and its application area, Properties of fluids, Unit systems, Standards, Conversion on units, Units and equations, Dimension analysis, Dimension and units, Dimensional homogeneity, Dimensionless equations, Buckingham theorem, Common groups, examples.

FLUID STATIC & ITS APPLICATIONS (3 hours) Nature of fluids: Incompressible and compressible fluids, Pressure concepts, Hydrostatic equilibrium in gravitational and centrifugal field, Manometers, Inclined manometer, Continuous gravity and centrifugal decanter.

FLUID FLOW PHENOMENA (4 hours) Types of flow, potential flow, one dimensional flow, laminar flow, Reynolds number, Newtonian and non-Newtonian fluids, Velocity gradient and Rate of shear, Viscosity of gases and liquids, Turbulent flow, Nature of turbulence, Eddy viscosity, Eddy diffusivity of momentum, Flow in boundary layers, Laminar and turbulent flow in boundary layers, Boundary layer formation in straight tube and flat plates, Boundary layer thickness, Boundary layer separation and wake formation.

BASIC EQUATIONS OF FLUID FLOW (6 hours) Stream line and stream tubes, Average velocity, Mass velocity, Momentum balance, Bernoullis equation without friction, Correction of Bernoullis equation for fluid friction, Pump work in Bernoullis equation.

FLOW OF INCOMPRESSIBLE FLOW AND ITS APPLICATIONS IN CONDUITS AND THIN LAYERS (6 hours) Flow of incompressible fluids in pipes, Friction factor, Laminar flow of Newtonian and non-Newtonian fluids, Turbulent flow in pipes and closed channels, Effect of roughness, Friction factor chart, Drag reduction in turbulent flow Friction factor in Flow through channels of noncircular cross section, Friction from changes in velocity or direction, Effect of fittings and valves, Practical use of velocity heads in design, Minimization expansion and contraction losses.

FLOW OF COMPRESSIBLE FLUIDS AND ITS APPLICATIONS (4 hours)

Continuity equations, Velocity of sound, Stagnation temperature, Processes of compressible flow.

FLUID FLOW MEASUREMENTS (8 hours) Fluid flow measurement: venture meter, Orifice meter, Rotameter, Pitot tubes etc,

APPLICATIONS OF FLUID MECHANICS (10 hours) Transportation and metering of fluids: Pipe, fitting and valves, Pumps, compressor, blowers and fans, Flow past immersed bodies: Drag, Drag coefficients, Flow through beds of solids, Particle motion, Terminal velocity, Hindered settling, Settling and rise of bubbles and drops, Fluidization, Introduction to computational fluid dynamics (CFD). (Total contact time: 45 hours)

9

PRACTICALS 1. Experiment on Viscosity by Stokes law 2. Experiment on Reynolds number 3. Experiment on Friction in circular pipe 4. Experiment on Friction in annulus 5. Experiment on Calibration of venturimeter 6. Experiment on Orifice meter 7. Experiment on Characteristics of centrifugal pump 8. Experiment on Equivalent length of pipe fittings BOOKS RECOMMENDED 1. McCabe W.L., Smith J.C., Harriott P., Unit Operations of Chemical Engineering, 6th & 7th Eds., McGraw-Hill, New York, 2001 & 2005. 2. Coulson & Richardsons Chemical Engineering, Vol. 2, 5th Ed., Elesevier, New Delhi, 2005. 3. Coulson & Richardsons Chemical Engineering, Vol. 4, 2nd Ed., Elesevier, New Delhi, 2001. 4. Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006. 5. de Nevers N., Fluid Mechanics for Chemical Engineers, 2nd Ed., McGraw-Hill, New York, 1991.

10

B. Tech. III (CH), Semester-VI L T P C

CH 308: MASS TRANSFER OPERATIONS-II 3 1 2 5

ABSORPTION ( 10 Hours) Equilibrium, material balance for single component transfer, multi-stage & packed tower operation, multicomponent system, non-isothermal operation, absorption with chemical reaction

LIQUID EXTRACTION ( 08 Hours)

Liquid equilibria, stage wise extraction, stage type extractor, differential extractor

ADSORPTION AND ION-EXCHANGE ( 06 Hours) Adsorption equilibria, stage wise and continuous operations

DRYING ( 06 Hours) Equilibrium, batch drying, mechanism, continuous

LEACHING ( 04 Hours) Steady state & unsteady state operations, methods of calculation

CRYSTALLIZATION ( 03 Hours) Equilibrium, operations and equipment

INTRODUCTION TO RECENT SEPARATION TECHNIQUE ( 08 Hours) Ultrafiltration, reverse osmosis, nanofiltration, liquid membrane

(Total contact time: 45 hours)

PRACTICALS

1. Leaching 2. Liquid-liquid extraction 3. Freundlich isotherm 4. Ternary diagram 5. Drying 6. Fluidization apparatus 7. Cooling tower 8. Fluid bed dryer 9. Evaporator BOOKS RECOMMENDED: 1. Treybal R.E., Mass-Transfer Operations, 3rd Ed., McGraw-Hill, Singapore, 1981. 2. McCabe W.L, Smith J.C., Harriott P., Unit Operations in Chemical Engineering, 6th &7th Eds., McGraw-Hill, New York, 2001 & 2005. 3. Coulson J.M., Richardson J.F., Backhurst J. R., Harker J.H. Coulson & Richardson's Chemical Engineering, Vol. 1, 6th Ed., Elservier, New Delhi, 2004. 4. Chopey N.P., Handbook of Chemical Engineering Calculations, 3rd Ed., McGraw-Hill, New York, 2004. 5. Suryanarayana A., Mass Transfer Operations, New Age International, New Delhi, 2002.

11

B. Tech. IV (CH) Semester-VII L T P C

CH 401: CHEMICAL REACTION ENGINEERING - II 3 0 0 3

INTRODUCTION TO RTD (03 Hours) Non ideal flow in reactors, RTD of fluid in reactors, Age distribution, F curve, C curve and E curve, Intensity Function, Effects of RTD on performance of Chemical Process Equipment

KINETICS AND DESIGN FOR NONCATALYSED HETEROGENEOUS SYSTEM (06 Hours) Selection of a model, Determination of rate controlling step, Application to design, Application to fluidized bed,

FLUID- FLUID REACTIONS (05 Hours) The rate equation, Kinetic regimes for mass transfer and reaction, fast reaction, intermediate reaction, slow reaction, Slurry reaction kinetics, Application to design

FLUID SOLID NON-CATALYTIC REACTIONS (06 Hours) Particles of single size, plug flow of solids, Mixture of particles of different and unchanging sizes, mixed flow of particles of a single unchanging size,

CATALYTIC REACTORS (06 Hours) ion kinetics, External and Internal Diffusional Resistances, Effects of Heat Generation/Absorption, Effectiveness Factors, Fixed Bed, Fluid Bed, Trickle bed, Slurry Reactors,

CATALYSIS (05 Hours) Typical Catalysts used in chemical processes, Catalyst Characterizations, Catalyst Deactivation and Regeneration, Metal recovery from the Spent Catalysts

ZEOLITE CATALYSTS (05 Hours) Applications, Rise of Acidity, Modifications, Shape Selectivity

ENVIRONMENTAL CATALYSIS (03 Hours) Importance, Applications

MONOLITHIC REACTORS (03 Hours) Configurations, Preparation, Hydrodynamics and Applications, Accelerated Deactivation of catalysts, Laboratory reactors, Oscillatory motion of reactants in catalyst pores, Microreactors.

INDUSTRIAL CASE STUDIES ON CATALYSIS AND CATALYTIC REACTORS (03 Hours)

(Total Contact Time: 45 Hours) BOOKS RECOMMENDED: 1. Fogler H.S., Elements of Chemical Reaction Engineering, 4th Ed., Prentice Hall, NJ, 2006. 2. Levenspiel O., Chemical Reaction Engineering, 3rd Ed., John Wiley & Sons, Singapore, 1998. 3. Smith J. M., Chemical Engineering Kinetics, 3rd Edition, McGraw Hill, N Y, 1981. 4. Davis M.E., Davis R.J., Fundamentals of Chemical Reaction Engineering, McGraw-Hill, New York,2003. 5. Froment G.F., Bischoff K.B., Chemical Reactor Analysis and Design, 2nd Ed., John Wiley & Sons, Singapore, 1990.

12

B. Tech. IV (CH), Semester VII L T P C

CH 403: INSTRUMENTATION AND PROCESS CONTROL 3 1 2 5

INTRODUCTION (02 Hours) Steady and unsteady state design equation for an agitated heated tank. Introduction to P, PI, PID controls.

DYNAMICS OF FIRST ORDER SYSTEMS (04 Hours)

Dynamics of first order systems subjected to various disturbances like step, ramp, impulse & sinusoidal e.g. liquid level tanks, mixing process, thermometer etc. response of first order system in series.

DYNAMICS OF SECOND ORDER SYSTEMS (06 Hours)

Dynamics of second order systems subjected to various disturbances like step, impulse, sinusoidal.

LINEAR CLOSE LOOP SYSTEM (03 Hours) Linear close loop system, Servo and Regulator problem.

CLOSED LOOP TRANSFER FUNCTION (05 Hours)

Closed loop transfer function, block diagrams for various simple systems, Transient response of the control system.

STABILITY OF CONTROL SYSTEM (04 Hours)

Stability of control system, Routh test criterion, Concept of Root Locus, frequency analysis, Bode diagrams for simple order system (first order system, second order system, P, PI, PD controllers)

ADVANCED CONTROL (05 Hours)

Cascade Control, Feed forward Control, Ratio control, Split Range Control, Auctioneering Control and Multivariable Control.

CONTROLLERS AND CONTROL ELEMENTS (02 Hours) Controller, control elements, control valves.

DISTRIBUTED CONTROL SYSTEM (02 Hours)

Distributed control system (DCS), Programmable Logical Control System (PLC).

FLOW, LEVEL, PRESSURE AND TEMPERATURE MESUREMENT (04 Hours) Construction, working principle, selection criteria and application of the measurement devices

LOGIC STRUCTURE, COMBINATIONAL LOGICS (03 Hours)

KARNAUGH MAPS, ASSEMBLY LANGUAGE PROGRAMMING (02 Hours) SENSOR AND TRANSDUCER, INSTRUCTION PANELS,INTERFACE (03 Hours)

(Total Contact Time: 45 Hours)

13

PRACTICALS: 1. Dynamics of First Order Liquid Level System. 2. Dynamics of Non Interacting Tanks. 3. Simulation of Heat Exchanger 4. Simulation of Catalytic Reformer 5. Simulation of Binary Distillation 6. Study of Temperature Control Trainer 7. Study of Pressure Control Trainer 8. Study of Flow Control Trainer 9. Study of Level Control Trainer 10. Dissolved Oxygen Meter 11. Thermocouple Calibration BOOKS RECOMMENDED: 1. Coughanowr D.R., Process Systems Analysis and Control, 2nd Ed., McGraw-Hill, New York, 1991. 2. Stephanopoulos G., Chemical Process Control, Prentice-Hall of India, New Delhi, 2001. 3. Luben W.L., Luben M.L., Essentials of Process Control, McGraw-Hill, New York, 1997. 4. Kopell L.B., Coughanowr D.R., Process Systems Analysis and Control, McGraw-Hill, New York, 1986. 5. Eckman D.P., Industrial Instrumentation, Dhanpat Rai and Sons, New Delhi, 1999. 6. Morris M. M., Kime C.R., Logic and Computer Design Fundamentals, Prentice-all, PLACE2000. 7. Considine D.M., Process Industrial Instruments and Control Handbook, McGraw-Hill, New York, 2001.

14

B. Tech. IV (CH) Semester - VII L T P C CH 405 : PROCESS EQUIPMENT DESIGN & DRAWING 3 1 2 5

INTRODUCTION (02 Hours)

Introduction to Chemical Engineering Design, Process design, Mechanical aspects of process equipment design, General design procedure, Equipment classifications, Design codes and standards (IS, ASTM and BS)

CRITERIA IN VESSEL DESIGN (03 Hours) Properties of materials, Material of construction for various equipments and services, Material specifications, Fabrication techniques

DESIGN OF PRESSURE VESSELS (12 Hours) Design of pressure vessels under internal pressure, Construction features, Pressure vessel code, Design of shell, various types of heads, nozzles, flanges for pressure vessel, Design and construction features of thick-walled pressure vessels, Various types of jackets and coils for reactors, Auxiliary process vessels

SUPPORTS FOR VESSELS (04 Hours) Design consideration for supports for process equipments, Design of brackets support, leg support skirt, support, saddle support.

DESIGN OF STORAGE VESSEL (03 Hours) Storage of nonvolatile and volatile liquids and gases, Codes for storage vessel design, Bottom, Roof and Shell designs.

DESIGN OF VESSELS UNDER EXTERNAL PRESSURE (03 Hours) Design criteria for external design pressure, vessels operated under vacuum, Use of stiffeners, Design of covers, pipes and tubes

DESIGN OF HEAT EXCHANGERS (08 Hours) Types of heat exchangers, Selection criteria, Design of heat exchangers- shell, tube, baffles, closures, channels, tube sheets etc.

DESIGN OF DISTILLATION AND ABSORPTION COLUMNS (08 Hours) Basic features of tall vertical equipments/ towers, Towers/Column Internal, Design of tower shell and internals, supports etc.

PROCESS HAZARDS & SAFETY, MEASURES IN EQUIPMENT DESIGN (02 Hours) Equipment testing, Analysis of hazards, Pressure relief devices. Safety measures in process equipment design (Total contact time: 45 hours)

PRACTICALS 1. Design & drawing of Pressure Vessels 2. Design & drawing of Heat Exchangers 3. Design & drawing of Distillation Columns 4. Design & drawing of Reactors 5. Design & drawing of Storage Vessels 6. Design & drawing of specific equipments: Evaporators/ Crystallizers/ Dryers, etc. 7. Sketches of equipment accessories such as covers for pressure vessels, flanges, flange facing,

supports, roofs for storage vessel, jackets, coils, tube sheet for heat exchangers, baffles in head exchangers, trays for distillation columns, packing for distillation towers, liquid distributors etc.

8. AutoCAD: Flange, Hub, 3-D Pressure vessel, 3-D Flange

15

BOOKS RECOMMENDED: 1. Joshi M.V., Mahajani V.V., Process Equipment Design, 3rd Ed., MacMillan, Delhi, 1996. 2. IS Code: 2825 (1969). 3. Bhattacharyya B.C., Introduction to Chemical Equipment Design: Mechanical Aspects, 5th Ed., CBS Publishers, New Delhi, 2008. 4. Soares C., Process Engineering Equipment Handbook, McGraw-Hill, New York, 2002. 5. Cheremisinoff N.P., Handbook of Chemical Processing Equipment, Butterworth Heinemann, Oxford, 2000. 6. Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elesevier, New Delhi, 2006. 7. Kern D.Q., Process Heat Transfer, McGraw-Hill, New York, 1965. 8. Brownell L.E., Young E.H., Process Equipment Design, Wiley Eastern, Delhi, 1977. 9. Branan C.R., Rules of Thumb for Chemical Engineers, 4th Ed., Elsevier, Oxford, 2005.

16

B. Tech. IV (CH), Semester VII L T P C

CH 407: TRANSPORT PHENOMENA 3 1 0 4

INTRODUCTION (01 Hour) TRANSPORT BY MOLECULAR MOTION (14 Hours)

Momentum transport by viscosity and momentum-flux. Energy transport by thermal conductivity and heat-flux. Mass transport by diffusivity and mass-flux.

TRANSPORT IN ONE DIMENSION (SHELL BALANCE METHODS) (17 Hours) Shell momentum balances and velocity distributions. Shell energy balances and temperature distributions. Shell mass balances and concentration distributions.

USE OF GENERAL TRANSPORT EQUATIONS (6 Hours) Equations of change and their use in momentum transport (isothermal).

VELOCITY DISTRIBUTIONS IN TURBULENT FLOW (1 Hour) Comparisons of laminar and turbulent flows. Time-smoothed equations of change for incompressible fluids.

INTERPHASE TRANSPORT IN ISOTHERMAL SYSTEMS (04 Hours) Friction factors for flow in tubes, flow around spheres, and packed columns.

MACROSCOPIC BALANCES FOR ISOTHERMAL FLOW SYSTEMS (02 Hours) Macroscopic mass balance for steady and unsteady-state problems.

(Total contact hours : 45)

____________________________________________________________________________________

BOOKS RECOMMENDED:

1. Bird R.B., Stewart W.E., Lightfoot E.N., Transport Phenomena, 1st & 2nd Eds., John Wiley & Sons, Singapore, 1960 & 2002. 2. Thomson, W.J., Introduction to Transport Phenomena Pearson Education Asia, Singapore, 2000. 3. Brodkey R.S. and Hershey H.C., Transport Phenomena: A Unified Approach McGraw-Hill, New York, 1988. 4. Plawsky J.L., Transport Phenomena Fundamentals, Marcel Dekker, New York, 2001. 5. Slattery J.C., Sagis L., Oh E-S., Interfacial Transport Phenomena, 2nd Ed., Springer, New York, 2007.

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B. Tech. IV (CH), Semester-VIII L T P C

CH 402: CHEM. ENGG. PLANT DESIGN AND ECONOMICS 3 0 0 3

INTRODUCTION ( 02 Hours) Basic consideration in chem. Engg. plant design, project identification, preliminary techno-economic feasibility. .

PROCESS DESIGN ASPECTS ( 04 Hours) Selection of process, factors affecting process selection, types of flow diagrams.

SELECTION OF PROCESS EQUIPMENT ( 02 Hours)

Standard versus special equipment, materials of construction, selection criteria etc.

PROCESS AUXILIARIES ( 04 Hours) Piping design, layout, support for piping insulation, types of valves, process control & instrumentation control system design.

PROCESS UTILITIES ( 06 Hours) Process water, boiler feed water, water treatment & disposal, steam, oil heating system, chilling plant, compressed air and vacuum system.

PLANT LOCATION AND LAYOUT ( 04 Hours) Factors affecting plant location, use of scale models.

COST ESTIMATION ( 06 Hours) Factors involved in project cost estimation, total fixed & working capital, types & methods of estimation of total capital investment, estimation of total product cost, factors involved.

DEPRECIATION ( 03 Hours) Types and methods of determination, evaluation.

PROFITABILITY ( 04 Hours) Alternative investment & replacement methods for profitability evaluation, economic consideration in process and equipment design, inventory control.

OPTIMUM DESIGN ( 02 Hours) General products rates in plant operation, optimum conditions etc.

PRODUCTION, PLANNING, SCHEDULING AND CONTROL (08 Hours) Introduction, PERTS & CPM

(Total contact time: 45 hours)

BOOKS RECOMMENDED: 1. Peters M.S., Timmerhaus, K.D., Plant Design and Economics for Chemical Engineers, 4th Ed., McGraw-Hill, Singapore, 1991. 2. Vilbrant F.C., Dryden, C.E., Chemical Engineering and Plant Design, 4th Ed., McGraw-Hill, New York, 1959. 3. Pant J.C. CPM and PERT with Linear Programming, Jain Brothers, New Delhi, 1986. 4. Davis, G.S, "Chemical Engineering Economics and Decision Analysis", CENDC, I.I.T., Madras, 1981. 5. Holland, F.A., Watson, F.A and Wilkinson, J.K., "Introduction to Process Economics", Wiley, New York, 1974.

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B. Tech. IV (CH), Semester VIII L T P C

CH 404: CHEMICAL SYSTEMS MODELING 3 0 0 3

INTRODUCTION (3 hours) Physical and mathematical modeling, Principles of similarity, Independent variables, Dependent variables, Parameters and boundary conditions.

SOLUTIONS OF THE MODEL EQUATIONS (15 hours) Laplace Transforms: Thermometer systems, mixing tanks, fixed bed reactor formulation. Partial differential equations and finite differences, Numerical Methods: Direct solutions of linear equations, roots of nonlinear equations.

MATHEMATICAL MODELING OF CHEMICAL ENGINEERING SYSTEM (8 hours) Principle of formulations, Mathematical consistency of model, Continuity equations, Component continuity equations, Energy equations, Equations of motion, Transport equations, Equilibrium, Chemical Kinetics with examples.

APPLICATIONS IN CHEMICAL ENGINEERING SYSTEMS (12 hours) Single, Two and n-stage extraction steady state mass transfer processes. Unsteady state formulation of a single stage extraction, Steady state heat conduction through hollow cylindrical pipe using various boundary condition, Unsteady process of steam heating of a liquid, Heat transfer through extended surface, Steady state counter current cooling of a tank diffusion with Chemical Reaction in a turbulent reactor, Batch distillation, pH systems etc.

TREATMENT OF EXPERIMENTAL RESULTS (3 hours) Curve fitting, Numerical differentiation and integration etc

INDUSTRIAL SIMULATORS (4 hours) Introduction and applications (Total contact time: 45 hours)

BOOKS RECOMMENDED 1. Mickley H. S., Sherwood T. S., Reed C. E., Application of Mathematical Modeling in Chemical Engineering, Tata-McGraw-Hill, New Delhi, 2002. 2. Jensen V.G., Jeffreys G.V., Mathematical Methods in Chemical Engineering, 2nd Ed., Academic Press, London, 1978. 3. Salariya R. S., Numerical Methods, Tata-McGraw Hill, New Delhi, 2002. 4. Lubyen W. L., Process Modeling, Simulation and Control for Chemical Engineers, 2nd Ed., McGraw-Hill, New York, 1989. 5. Pushpavanam S., Mathematical Methods in Chemical Engineering, Prentice-Hall of India, New Delhi, 2001.

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B. Tech. IV (CH), Semester VIII L T P C

CH 406: CAD IN CHEMICAL ENGINEERING 3 1 2 5 INTRODUCTION (3 hours)

Introduction to Computer aided design in chemical engineering, Mathematical modeling, Steady state and dynamic Simulation, Process simulation program (ASPEN PLUS).

CAD IN CHEMICAL PROCESSES (4 hours) Computer aided design of chemical process equipments, concepts of modular design, optimum design, parameter optimization etc.

COMPUTER AIDED FLOW SHEETING (6 hours)

Spread sheeting, Process synthesis, Flow sheeting software, Equation solution with recycle.

INPUT OUTPUT STRUCTURE (4 hours) Decision for the input output structure, Flow sheet alternatives: guidelines, Number of product streams, Gas recycle and purge.

APPLICATION OF CAD IN HEAT EXCHANGER NETWORK DESIGN (8 hours) Pinch technology, Heat integration, and Optimum number of heat exchanger.

APPLICATION OF CAD IN HEAT INTEGRATION OF DISTILLATION COLUMN(8 hours) Characteristics, Appropriate placement of column, Distillation across pinch, Grand composite curve, Design of simple distillation column to improve heat integration.

APPLICATION OF CAD IN HEAT INTEGRATION OF REACTORS (6 hours) Characteristics, Adiabatic operations, Indirect heat transfer, Appropriate placement of reactors.

APPLICATIONS OF CAD IN OTHER AREAS (6 hours) Neural network, Artificial neural network, Knowledge based system etc (Total contact time: 45 hours)

PRACTICALS 1. Simulation by ASPEN PLUS for Single distillation column 2. Simulation by ASPEN PLUS for REDFRAC 3. Simulation by ASPEN PLUS for Heat Exchanger 4. Simulation by ASPEN PLUS for Reactors ( CSTR, PFR Etc) 5. Simulation by ASPEN PLUS for Cumin Production system 6. Simulation by ASPEN PLUS for Plant Optimization 7. Simulation by ASPEN PLUS for Property Estimation 8. Simulation by ASPEN PLUS for Methanol- Water System

BOOKS RECOMMENDED

1. Sinnott R. K., Coulson & Richardsons Chemical Engineering, Vol. 6, 4th Ed., Elsevier, 2005. 2. Edgar T. F., Himmelblau D. M., Lasdon L. S., Optimization of Chemical Processes, 2nd Ed., McGraw-Hill, New York, 2001. 3. Smith R., Chemical Process Design, McGraw-Hill, New York, 2000. 4. Biegler L. T., Grossmann E. I., Westerberg A. W., Systematic Methods of Chemical Process Design, Prentice-Hall , New Jersey, 1997. 5. Douglas J., Conceptual Design of Chemical Processes, McGraw-Hill, New York, 1989.

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21

B. Tech. IV (CH), Semester - VIII L T P C CH 408: SAFETY AND POLLUTION CONTROL IN CHEMICAL PROCESS INDUSTRIES

3 - 2 4

ENVIRONMENTAL AND POLLUTION IN CHEMICAL INDUSTRIES (02 Hours) Definitions, scope and importance, need for public awareness, sources of pollution from Chemical industries

ENVIRONMENTAL LAWS AND STANDARDS (03 Hours) Laws related to solid, liquid and gases effluents, standards and legislations, Health and environmental effects, case studies for specific industries like petrochemicals, fertilizers, desalination, petroleum refining.

POLLUTION PREVENTION THROUGH PROCESS MODIFICATION (10 Hours) Recovery of by-products, Energy recovery, Waste utilization and recycle and reuse and waste generation minimization

AIR POLLUTION CONTROL (05 Hours) Air pollution control through mechanical separation, adsorption, etc.

WATER POLLUTION CONTROL (05 Hours) Water pollution control by physical, chemical and biochemical methods.

DESIGN OF CONTROL EQUIPMENT AND SYSTEMS (06 Hours) Designs to prevent fires and explosions, fire triangles, fault tree analysis, case studies

SOLID WASTE TREATMENT AND DISPOSAL (04 Hours) Types of solid waste, generation, onsite handling, storage & processing, Disposal techniques, recovery of resources, conversion products and energy.

SAFETY IN CHEMICAL PROCESS INDUSTRIES (10 Hours) Safety and loss prevention, safety systems, Hazardus properties of chemicals, characterization of chemical processes, the nature and impact of chemical plant accidents, occupational safety and industrial hygiene, Toxicology, toxic release, case studies (Total contact time: 45 hours)

PRACTICALS 1. Determination of Dissolved Oxygen (DO) 2. Determination of Biochemical Oxygen Demand (BOD) 3. Determination of Chemical Oxygen Demand (COD) 4. Determination of Oil and Grease 5. Determination of Alkalinity 6. Determination of Acidity 7. Determination of Chloride Ion Concentration 8. Determinations of Total Suspended Solids (TSS) 9. Calorific value 10. Sampling Programs 11. Atomic Absorption Spectrophotometer Method BOOKS RECOMMENDED: 1. Crowl D. A., Louvar J. F., Chemical Process Safety, Prantice-Hall, 2nd Ed., New York, 2002. 2. Metcalf & Eddy, Waste Water Engineering: Treatment, Disposal and Reuse, Tata-McGraw-Hill, New Delhi, 2002. 3. MaCarty S., Chemistry for Environmental Engineering, Tata-McGraw-Hill, New Delhi, 2004. 4. Rao C.S., Environmental Engineering, Wiley Eastern Limited, New Delhi, 1995. 5. Sanders R E., Chemical Process Safety, Butterworth-Heinemann, New Delhi, 2005. 6. Masters G.M., Introduction to Environmental Engineering and Science, Prentice-Hall, New Delhi, 1997.

Scheme & Syllabus B.Tech_II_12-05-2008_ChEDScheme & Syllabus__B.Tech._III & IV_Passed in 16th Senate meeting held on 19-07-2008_Corrected_29-8-08