august 13, 2018 attn: mr. philip lepine...2018/08/01 · august 13, 2018 snl construction re: 4380...

August 13, 2018

SNL Construction Re: 4380 Bullard Ave. 3333 New Hyde Park Rd., Suite 200 Bronx, NY Lake Success, N.Y. 11042 SMES Project #18-340 Attn: Mr. Philip Lepine [email protected] Dear Mr. Lepine: Forwarded herewith are supporting documents associated with soil waste characterization testing recently completed at the above referenced property, including: (i) Site Plan; (ii) tabulated sample summary and results of soil organic vapor screening; (iii) complete laboratory reports; (iv) laboratory chains of custody; and (v) sample Photo Log. Soil waste characterization samples were collected, on a continuous basis, from seven (7) geotechnical borehole locations to a depth of approximately 16 bgs (see Site Plan). All recovered soil samples were inspected for visual/olfactory evidence of contamination and screened for the presence of organic vapors, utilizing a photo ionization detector (PID - see Table #2). Based on the results of sample inspection and screening, discrete and homogenized composite soil samples were containerized for laboratory analysis from each borehole location (total 8 samples – see Tables #1 and #2). All sampling was conducted by qualified Soil Mechanics Environmental Services personnel in accordance with appropriate sampling protocols and in general conformance with the requirements of EWMI’s New Jersey facility, which requires one (1) discrete and one (1) 6 to 8-point composite soil sample for each 1,000 yds3 being considered for acceptance into their disposal facility. The discrete and composite samples were containerized into appropriate glassware, iced to 4 degrees centigrade, and hand delivered to Long Island Analytical Laboratories of Holbrook, NY (NYS certified), in accordance with appropriate Chain of Custody procedures. Analytical parameters for the samples containerized for testing included the following: (i) 1-point discrete samples (total 8 – see Table #2) EWMI Package A (natural soil)

or B (fill soil) VOCs; and

(ii) 6 to 8-point composite samples (total 8 – see Table #1) were as analyzed for EWMI Package A (natural soil) or B (fill soil) SVOCs, PCBs, herbicides, pesticides, EPH, and metals. Package B (fill soils) samples were further analyzed for TCLP 8-RCRA metals and pH.

Should you have any questions regarding the contents of this letter, please feel free to call our office.

Very truly yours, Soil Mechanics Environmental Services

Altan Gulum, C.P.G., P.G. Robert Cardinale, M.S., C.P.G., P.G. Project Manager Director of Environmental Services

Carl Vernick, P.E.

President

2

Table #1 Bullard Ave., Bronx, NY

South Half North Half

Sample WC-1 from Borings A, B, C (0.0’ – 4.0’ bgs)* Sample WC-4 from Borings D, E, F, G (0.0’ – 4.0’ bgs)* Sample WC-2 from Borings A, B, C (4.0’ – 8.0’ bgs)* Sample WC-5 from Borings D, E, F, G (4.0’ – 8.0’ bgs)* Sample W-3 from Borings A, B, C (8.0’ – 12.0’ bgs)** Sample WC-6 from Borings D, E, F, G (8.0’ – 12.0’ bgs)* Sample WC-8 from Borings A, B, C (12.0’ – 16.0” bgs)** Sample WC-7 from Borings D, E, F, G (12.0’ – 16.0’ bgs)**

* Historic Fill soil formation samples - Package B analysis consisting of ±6 to 8-point composite sample (except VOCs) ** Natural/native soil formation samples - Package A analysis consisting of ±6 to 8-point composite sample (except VOCs) Samples for VOC analysis are 1-point discrete samples selected for analysis based on PID readings (see Table #2)

Table #2 – Organic Vapor Screening - PID Readings (detection range 0.0-15000.0)

Sample Depth Boring A a/k/a B-1

Boring B a/k/a B-2

Boring C a/k/a B-3

Boring D a/k/a B-4

Boring E a/k/a B-5

Boring F a/k/a B-6

Boring G a/k/a B- 7

0’-2’ 0.0 0.0 0.0 0.0 50.3* 0.0 0.0 2’-4’ 0.0* 0.0 0.0 0.0 11.8 0.0 0.0

4’-6’ 0.0 0.0* 0.0 0.0 4.6 33.4 0.0 6’-8’ 0.0 0.0 11.1 0.0 23.7 51.9* 0.0

8’-10’ 0.0 0.0 0.0* 0.0 0.0 42.5* 0.0 10’-12’ 0.0 0.0 0.0 0.0 0.0 12.5 0.0

12’-14’ 0.0 NR below 12’

NR below 13’

NR Below 14’

0.0 6.4* 0.0

14’-16’ 0.0* NR NR NR 0.0 1.8 0.0

* Discrete sample (1-point) for VOC analysis acquired from this sampling interval Yellow Highlight Yellow - Fill Zone 6 to 8-point composite sample Green Highlighted Green – Natural/native soil zone 6 to 8-point composite sample ND Non-detect + Poor Recovery NR No recovery (refusal)

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Laboratory Report

LIAL# 8073111

August 14, 2018

Soil Mechanics

Robert J. Cardinale

3770 Merrick Road

Re: #18-340 Bullard Ave Bronx

Dear Robert J. Cardinale,

Enclosed please find the laboratory Analysis Report(s) for sample(s) received on July 31, 2018. Long Island Analytical

laboratories analyzed the samples on August 14, 2018 for the following:

Seaford, NY 11783

ANALYSIS SAMPLE ID

EPH 8015 D, Impact Comp BWC-1

EPA 8260CWC-1A


EPA 8260CWC-2A

EPH 8015 D, Impact Comp AWC-3

EPA 8260CWC-3A


EPA 8260CWC-8A


EPA 8260CWC-4A


EPA 8260CWC-5A


EPA 8260CWC-6A


EPA 8260CWC-7A

Samples received at 13.7 ° C

Holding time exceeded, analyze immediate parameter.1.C

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Long Island Analytical Laboratories, Inc. Michael Veraldi - Laboratory Director

If you have any questions or require further information, please call at your convenience. Long Island Analytical

Laboratories Inc. is a NELAP accredited laboratory. All reported results meet the requirements of the NELAP

standards unless noted. Report shall not be reproduced except in full without the written approval of the

laboratory. Results related only to items tested. Long Island Analytical Laboratories would like to thank you for

the opportunity to be of service to you.

Best Regards,

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Client: Soil Mechanics

Date (Time) Received: 07/31/2018 13:14

Matrix: Soil

Laboratory ID: 8073111-01

ELAP: #11693

Sample ID: WC-1

Client ID: #18-340 Bullard Ave Bronx

Date (Time) Collected: 07/31/2018 10:00

% Solid:83.78

Semivolatile AnalysisParameter LOQCAS No. Result Units Flag

1,2,4-Trichlorobenzene 120-82-1 <179 ug/kg dry179

2,2'-Oxybis(1-Chloropropane) 108-60-1 <179 ug/kg dry179

2,4,5-Trichlorophenol 95-95-4 <179 ug/kg dry179


2,4-Dichlorophenol 120-83-2 <179 ug/kg dry179

2,4-Dimethylphenol 105-67-9 <179 ug/kg dry179

2,4-Dinitrophenol 51-28-5 <358 ug/kg dry358

2,4-Dinitrotoluene 121-14-2 <179 ug/kg dry179


2-Chloronaphthalene 91-58-7 183 ug/kg dry179

2-Chlorophenol 95-57-8 <179 ug/kg dry179

2-Methylnaphthalene 91-57-6 <179 ug/kg dry179

2-Methylphenol 95-48-7 <358 ug/kg dry358

2-Nitroaniline 88-74-4 <179 ug/kg dry179

2-Nitrophenol 88-75-5 <179 ug/kg dry179

3,3'-Dichlorobenzidine 91-94-1 <358 ug/kg dry358

3/4-Methylphenol 108-39-4/106-44-5 <179 ug/kg dry179


4,6-Dinitro-2-methylphenol 534-52-1 <179 ug/kg dry179

4-Chloroaniline 106-47-8 <179 ug/kg dry179



Acenaphthene 83-32-9 194 ug/kg dry179

Acenaphthylene 208-96-8 <179 ug/kg dry179

Aniline 62-53-3 <179 ug/kg dry179

Anthracene 120-12-7 616 ug/kg dry179

Benzidine 92-87-5 <358 ug/kg dry358

Benzo(a)anthracene 56-55-3 1730 ug/kg dry179

Benzo(a)pyrene 50-32-8 1680 ug/kg dry179

Benzo(b)fluoranthene 205-99-2 2180 ug/kg dry358

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Parameter LOQCAS No. Result Units Flag

Benzo(g,h,i)perylene 191-24-2 1130 ug/kg dry179

Benzo(k)fluoranthene 207-08-9 850 ug/kg dry179

Benzoic Acid 65-85-0 <358 ug/kg dry358

Benzyl alcohol 100-51-6 <358 ug/kg dry358

Bis(2-Chloroethyl)ether 111-44-4 <179 ug/kg dry179

Bis(2-Ethylhexyl)phthalate 117-81-7 <179 ug/kg dry179

Butyl benzyl phthalate 85-68-7 <179 ug/kg dry179

Carbazole 86-74-8 320 ug/kg dry179

Chrysene 218-01-9 2050 ug/kg dry179

Dibenzo(a,h)anthracene 53-70-3 333 ug/kg dry179

Dibenzofuran 132-64-9 <179 ug/kg dry179

Diethyl phthalate 84-66-2 <179 ug/kg dry179

Dimethyl phthalate 131-11-3 <179 ug/kg dry179

Di-n-butyl phthalate 84-74-2 <358 ug/kg dry358

Di-n-octyl phthalate 117-84-0 <179 ug/kg dry179

Fluoranthene 206-44-0 3550 ug/kg dry179

Fluorene 86-73-7 211 ug/kg dry179

Hexachlorobenzene 118-74-1 <179 ug/kg dry179

Hexachlorobutadiene 87-68-3 <179 ug/kg dry179

Hexachlorocyclopentadiene 77-47-4 <358 ug/kg dry358

Hexachloroethane 67-72-1 <179 ug/kg dry179

Indeno(1,2,3-cd)pyrene 193-39-5 1000 ug/kg dry179

Isophorone 78-59-1 <358 ug/kg dry358

Nitrobenzene 98-95-3 <179 ug/kg dry179

N-Nitrosodimethylamine 62-75-9 <179 ug/kg dry179

N-Nitroso-di-n-propylamine 621-64-7 <179 ug/kg dry179

N-Nitrosodiphenylamine 86-30-6 <179 ug/kg dry179

Parathion (ethyl) 56-38-2 <179 ug/kg dry179

Pentachlorophenol 87-86-5 <179 ug/kg dry179

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78


Phenanthrene 85-01-8 2700 ug/kg dry179

Phenol 108-95-2 <179 ug/kg dry179

Pyrene 129-00-0 3310 ug/kg dry179

Surrogate CAS No. % Recovery Rec. Limits Flag

2-Fluorobiphenyl 321-60-8 49 32.6-96.2

2-Fluorophenol 367-12-4 47 32.8-95.8

Nitrobenzene-d5 4165-60-0 46 28.1-100

Phenol-d6 13127-88-3 51 31.2-102

Terphenyl-d14 1718-51-0 53 32.6-110

Internal Standard CAS No. FlagRec. Limits% Recovery

1,4-Dichlorobenzene-d4 50-2003855-82-1 93

Acenaphthene-d10 50-20015067-26-2 92

Chrysene-d12 50-2001719-03-5 75

Naphthalene-d8 50-2001146-65-2 92

Perylene-d12 50-2001520-96-3 77

Phenanthrene-d10 50-2001517-22-2 84

Date Prepared: 08/01/2018

Date Analyzed: 08/03/2018 Analytical Method: EPA 8270 D

Preparation Method: EPA 3545 A

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Additional Semivolatile AnalysisParameter LOQCAS No. Result Units Flag

1,1-Biphenyl 92-52-4 <179 ug/kg dry179

1,2-Diphenylhydrazine/Azobenzene 122-66-7/103-33-3 <179 ug/kg dry179

Acetophenone 989-86-2 <179 ug/kg dry179

Atrazine 1912-24-9 <179 ug/kg dry179

Benzaldehyde 100-52-7 <179 ug/kg dry179

Caprolactam 105-60-2 <179 ug/kg dry179


2,4,6-Tribromophenol 118-79-6 58 18.04-120.2

2-Fluorobiphenyl 321-60-8 49 34.39-110.73

2-Fluorophenol 367-12-4 47 22.98-107.57

Nitrobenzene-d5 4165-60-0 46 31-118.25

Phenol-d6 13127-88-3 51 35.55-111.39

Terphenyl-d14 1718-51-0 53 41.02-106



Acenaphthene-d10 50-20015067-26-2 92

Naphthalene-d8 50-2001146-65-2 92

Phenanthrene-d10 50-2001517-22-2 84




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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Pesticides AnalysisParameter LOQCAS No. Result Units Flag

4,4'-DDD 72-54-8 636 ug/kg dry3.58

4,4'-DDE 72-55-9 <3.58 ug/kg dry3.58

4,4'-DDT 50-29-3 <3.58 ug/kg dry3.58

Aldrin 309-00-2 <5.97 ug/kg dry5.97

alpha-BHC 319-84-6 449 ug/kg dry5.97

beta-BHC 319-85-7 <5.97 ug/kg dry5.97

Chlordane 12789-03-6 <17.9 ug/kg dry17.9

delta-BHC 319-86-8 <5.97 ug/kg dry5.97

Dieldrin 60-57-1 <5.97 ug/kg dry5.97

Endosulfan I 959-98-8 <5.97 ug/kg dry5.97

Endosulfan II 33213-65-9 <5.97 ug/kg dry5.97

Endosulfan Sulfate 1031-07-8 <5.97 ug/kg dry5.97

Endrin 72-20-8 84.5 ug/kg dry 4.N5.97

gamma-BHC 58-89-9 <5.97 ug/kg dry5.97

Heptachlor 76-44-8 <5.97 ug/kg dry5.97

Heptachlor Epoxide 1024-57-3 <5.97 ug/kg dry5.97

Methoxychlor 72-43-5 <5.97 ug/kg dry5.97

Toxaphene 8001-35-2 <119 ug/kg dry119


Decachlorobiphenyl 2051-24-3 4.D44 50.4-127

Tetrachloro-m-xylene 877-09-8 90 57.5-127


1-Bromo-2-Nitrobenzene 50-200108-31-6 106


Date Analyzed: 08/03/2018 Analytical Method: EPA 8081 B


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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

PCB/Aroclor AnalysisParameter LOQCAS No. Result Units Flag

Aroclor-1016 12674-11-2 <11.9 ug/kg dry 4.M11.9

Aroclor-1221 11104-28-2 <11.9 ug/kg dry11.9

Aroclor-1232 11141-16-5 <11.9 ug/kg dry11.9

Aroclor-1242 53469-21-9 <11.9 ug/kg dry11.9

Aroclor-1248 12672-29-6 <11.9 ug/kg dry11.9

Aroclor-1254 11097-69-1 <11.9 ug/kg dry11.9

Aroclor-1260 11096-82-5 <11.9 ug/kg dry11.9


Date Analyzed: 08/02/2018 Analytical Method: EPA 8082 A


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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Herbicide AnalysisParameter LOQCAS No. Result Units Flag

2,4,5-T 93-76-5 <30 ug/kg dry30

2,4,5-TP (Silvex) 93-72-1 <30 ug/kg dry30

2,4-D 94-75-7 <30 ug/kg dry30




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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Total Metals AnalysisParameter Result Units FlagDate Analyzed Method LOQ

3.Emg/kg dry10900Aluminum 08/02/2018 EPA 6010 C 114

mg/kg dry<1.90Antimony 08/02/2018 EPA 6010 C 1.90

mg/kg dry7.33Arsenic 08/02/2018 EPA 6010 C 1.90

mg/kg dry268Barium 08/02/2018 EPA 6010 C 1.90

mg/kg dry<1.90Beryllium 08/02/2018 EPA 6010 C 1.90

4.Jmg/kg dry<1.90Cadmium 08/02/2018 EPA 6010 C 1.90

4.Jmg/kg dry2870Calcium 08/02/2018 EPA 6010 C 11.4

mg/kg dry21.8Chromium 08/02/2018 EPA 6010 C 1.90

mg/kg dry8.41Cobalt 08/02/2018 EPA 6010 C 1.90

mg/kg dry169Copper 08/02/2018 EPA 6010 C 1.90

3.E, 4.Jmg/kg dry16000Iron 08/02/2018 EPA 6010 C 57.0

mg/kg dry359Lead 08/02/2018 EPA 6010 C 1.90

4.Jmg/kg dry2540Magnesium 08/02/2018 EPA 6010 C 5.70

mg/kg dry272Manganese 08/02/2018 EPA 6010 C 1.90

mg/kg dry25.4Nickel 08/02/2018 EPA 6010 C 1.90

4.J, 4.Nmg/kg dry1030Potassium 08/02/2018 EPA 6010 C 11.4

4.Jmg/kg dry<1.90Selenium 08/02/2018 EPA 6010 C 1.90

mg/kg dry<1.90Silver 08/02/2018 EPA 6010 C 1.90

4.Jmg/kg dry429Sodium 08/02/2018 EPA 6010 C 5.70

mg/kg dry<1.90Thallium 08/02/2018 EPA 6010 C 1.90

mg/kg dry25.7Vanadium 08/02/2018 EPA 6010 C 1.90

3.Emg/kg dry452Zinc 08/02/2018 EPA 6010 C 19.0

Date Prepared: 08/02/2018 Preparation Method: EPA 3050B

Parameter Result Units FlagDate Analyzed Method LOQ

mg/kg dry<0.561Hexavalent Chromium 08/09/2018 EPA 7196 A 0.561

Date Prepared: 08/08/2018 Preparation Method: EPA 3060A


mg/kg dry0.24Mercury 08/03/2018 EPA 7471 B 0.02

Date Prepared: 08/03/2018 Preparation Method: EPA 7471 B


mg/kg dry<0.24Cyanide 08/14/2018 EPA 9014 0.24

Date Prepared: 08/10/2018 Preparation Method: Distillation Prep

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Metals by EPA 1311 TCLP AnalysisParameter Result Units FlagDate Analyzed Method LOQ

mg/L<0.05Arsenic 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

mg/L1.55Barium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

1.00

mg/L<0.05Cadmium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

mg/L<0.05Chromium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

mg/L0.27Lead 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

mg/L<0.05Selenium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

mg/L<0.05Silver 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05

Date Leached: 08/02/2018 Leach Method: EPA 1311 Fluid #1Leach Batch: B831135

Date Prepared: 08/06/2018 Preparation Method: EPA 200.2


4.Mmg/L<0.02Mercury 08/07/2018 EPA 245.1 0.02



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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

Extractable Petroleum HydrocarbonsParameter LOQCAS No. Result Units Flag

Extractable Petroleum Hydrocarbons 8006-61-9/68334-30-5 667 mg/kg dry49.7


Date Analyzed: 08/03/2018 Analytical Method: EPA 8015 C

Preparation Method: [CALC]


Diesel Range Organics (C10-C28) 68334-30-5 667 mg/kg dry 4.F19.9


p-Terphenyl-d14 1718-51-0 84 45.8-130


Date Analyzed: 08/03/2018 Analytical Method: EPA 8015 D DRO



Gasoline Range Organics(C6-C10) 8006-61-9 <29.8 mg/kg dry29.8


Naphthalene-d8 1146-65-2 27 20.7-168


Date Analyzed: 08/02/2018 Analytical Method: EPA 8015 D GRO


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Matrix: Soil


ELAP: #11693

Sample ID: WC-1



% Solid:83.78

General Chemistry ParametersParameter Result Units FlagDate Analyzed Method LOQ

pH 7.81 1.C, 2.BEPA 9045C08/07/2018 09:49 NA units

Temperature @ pH in C 21.90 1.C, 2.BEPA 9045C08/07/2018 09:49 NA units

Date Prepared: 08/07/2018 Preparation Method: pH- No Preparation

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1A



% Solid:84.21

Volatiles Low Level AnalysisParameter LOQCAS No. Result Units Flag

1,1,1,2-Tetrachloroethane 630-20-6 <11.8 ug/kg dry11.8

1,1,1-Trichloroethane 71-55-6 <11.8 ug/kg dry11.8


1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 <11.8 ug/kg dry 4.M11.8


1,1-Dichloroethane 75-34-3 <11.8 ug/kg dry11.8

1,1-Dichloroethylene 75-35-4 <11.8 ug/kg dry 4.M11.8

1,2,3-Trichloropropane 96-18-4 <11.8 ug/kg dry11.8

1,2,4-Trimethylbenzene 95-63-6 <11.8 ug/kg dry11.8

1,2-Dibromo-3-chloropropane 96-12-8 <11.8 ug/kg dry11.8

1,2-Dibromoethane 106-93-4 <11.8 ug/kg dry11.8

1,2-Dichlorobenzene 95-50-1 <11.8 ug/kg dry11.8


1,2-Dichloropropane 78-87-5 <11.8 ug/kg dry11.8





1,4-Dioxane 123-91-1 <59.1 ug/kg dry 4.J59.1

2,2-Dichloropropane 594-20-7 <11.8 ug/kg dry 4.J11.8

2-Chlorotoluene 95-49-8 <11.8 ug/kg dry11.8

4-Isopropyltoluene 99-87-6 <11.8 ug/kg dry11.8

4-Methyl-2-Pentanone 108-10-1 <23.7 ug/kg dry 4.J23.7

Acetone 67-64-1 79.9 ug/kg dry 4.M47.3

Acrylonitrile 107-13-1 <11.8 ug/kg dry 4.M11.8

Benzene 71-43-2 <11.8 ug/kg dry11.8

Bromochloromethane 74-97-5 <11.8 ug/kg dry11.8

Bromodichloromethane 75-27-4 <11.8 ug/kg dry11.8

Bromoform 75-25-2 <11.8 ug/kg dry11.8

Bromomethane 74-83-9 <11.8 ug/kg dry 4.J11.8

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1A



% Solid:84.21


Carbon disulfide 75-15-0 <11.8 ug/kg dry 4.M11.8

Carbon Tetrachloride 56-23-5 <11.8 ug/kg dry11.8

Chlorobenzene 108-90-7 <11.8 ug/kg dry11.8

Chloroethane 75-00-3 <11.8 ug/kg dry11.8

Chloroform 67-66-3 <11.8 ug/kg dry11.8

Chloromethane 74-87-3 <11.8 ug/kg dry 4.J11.8

cis-1,2-Dichloroethylene 156-59-2 <11.8 ug/kg dry11.8

cis-1,3-Dichloropropylene 10061-01-5 <11.8 ug/kg dry11.8

Dibromochloromethane 124-48-1 <11.8 ug/kg dry11.8

Dibromomethane 74-95-3 <11.8 ug/kg dry11.8

Dichlorodifluoromethane 75-71-8 <11.8 ug/kg dry11.8

Ethylbenzene 100-41-4 <11.8 ug/kg dry11.8

Isopropylbenzene (Cumene) 98-82-8 <11.8 ug/kg dry11.8

m,p-Xylenes 108-38-3/106-42-3 <23.7 ug/kg dry23.7

Methyl Butyl Ketone (2-Hexanone) 591-78-6 <11.8 ug/kg dry 4.J11.8

Methyl Ethyl Ketone (2-Butanone) 78-93-3 <23.7 ug/kg dry 4.J23.7

Methylene Chloride 75-09-2 <11.8 ug/kg dry 4.M, 4.K11.8

Methyl-tert-Butyl Ether 1634-04-4 <11.8 ug/kg dry 4.J11.8

Naphthalene 91-20-3 <11.8 ug/kg dry11.8

n-Butylbenzene 104-51-8 <11.8 ug/kg dry11.8

n-Propylbenzene 103-65-1 <11.8 ug/kg dry11.8

o-Xylene 95-47-6 <11.8 ug/kg dry11.8

sec-Butylbenzene 135-98-8 <11.8 ug/kg dry11.8

Styrene 100-42-5 <11.8 ug/kg dry11.8

tert-Butyl alcohol 75-65-0 <11.8 ug/kg dry 4.M11.8

tert-Butylbenzene 98-06-6 <11.8 ug/kg dry11.8

Tetrachloroethylene 127-18-4 <11.8 ug/kg dry11.8

Toluene 108-88-3 <11.8 ug/kg dry11.8

trans-1,2-Dichloroethylene 156-60-5 <11.8 ug/kg dry11.8

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Matrix: Soil


ELAP: #11693

Sample ID: WC-1A



% Solid:84.21


trans-1,3-Dichloropropylene 10061-02-6 <11.8 ug/kg dry11.8

Trichloroethylene 79-01-6 <11.8 ug/kg dry11.8

Trichlorofluoromethane 75-69-4 <11.8 ug/kg dry 4.M11.8

Vinyl chloride 75-01-4 <11.8 ug/kg dry 4.K, 4.M11.8


1,2-Dichloroethane-d4 10706-07-0 109 71.6-131

4-Bromofluorobenzene 460-00-4 114 75.4-133

Dibromofluoromethane 1868-53-7 4.E160 75.6-135

Toluene-d8 2037-26-5 91 79.9-123



1,4-Difluorobenzene 50-200540-36-3 71

Chlorobenzene-d5 50-2003114-55-4 72

Pentafluorobenzene 50-200363-72-4 59



Preparation Method: EPA 5035A-L

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Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05











2-Chloronaphthalene 91-58-7 <165 ug/kg dry165













Acenaphthene 83-32-9 <165 ug/kg dry165



Anthracene 120-12-7 <165 ug/kg dry165


Benzo(a)anthracene 56-55-3 <165 ug/kg dry165

Benzo(a)pyrene 50-32-8 174 ug/kg dry165

Benzo(b)fluoranthene 205-99-2 <329 ug/kg dry329

of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


Benzo(g,h,i)perylene 191-24-2 <165 ug/kg dry165

Benzo(k)fluoranthene 207-08-9 <165 ug/kg dry165






Carbazole 86-74-8 <165 ug/kg dry165


Dibenzo(a,h)anthracene 53-70-3 <165 ug/kg dry165







Fluorene 86-73-7 <165 ug/kg dry165





Indeno(1,2,3-cd)pyrene 193-39-5 <165 ug/kg dry165








of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


Phenanthrene 85-01-8 <165 ug/kg dry165

Phenol 108-95-2 <165 ug/kg dry165

Pyrene 129-00-0 257 ug/kg dry165


2-Fluorobiphenyl 321-60-8 53 32.6-96.2

2-Fluorophenol 367-12-4 50 32.8-95.8

Nitrobenzene-d5 4165-60-0 49 28.1-100

Phenol-d6 13127-88-3 52 31.2-102

Terphenyl-d14 1718-51-0 55 32.6-110



Acenaphthene-d10 50-20015067-26-2 90

Chrysene-d12 50-2001719-03-5 74

Naphthalene-d8 50-2001146-65-2 90

Perylene-d12 50-2001520-96-3 75

Phenanthrene-d10 50-2001517-22-2 84




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05









2,4,6-Tribromophenol 118-79-6 60 18.04-120.2

2-Fluorobiphenyl 321-60-8 53 34.39-110.73

2-Fluorophenol 367-12-4 50 22.98-107.57

Nitrobenzene-d5 4165-60-0 49 31-118.25

Phenol-d6 13127-88-3 52 35.55-111.39

Terphenyl-d14 1718-51-0 55 41.02-106



Acenaphthene-d10 50-20015067-26-2 90

Naphthalene-d8 50-2001146-65-2 90

Phenanthrene-d10 50-2001517-22-2 84




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


4,4'-DDD 72-54-8 <3.29 ug/kg dry3.29

4,4'-DDE 72-55-9 <3.29 ug/kg dry3.29

4,4'-DDT 50-29-3 9.20 ug/kg dry3.29

Aldrin 309-00-2 <5.49 ug/kg dry5.49

alpha-BHC 319-84-6 30.7 ug/kg dry5.49

beta-BHC 319-85-7 <5.49 ug/kg dry5.49







Endrin 72-20-8 <5.49 ug/kg dry 4.N5.49


Heptachlor 76-44-8 14.3 ug/kg dry5.49












of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05



Aroclor-1221 11104-28-2 <11.0 ug/kg dry11.0

Aroclor-1232 11141-16-5 <11.0 ug/kg dry11.0

Aroclor-1242 53469-21-9 <11.0 ug/kg dry11.0

Aroclor-1248 12672-29-6 <11.0 ug/kg dry11.0

Aroclor-1254 11097-69-1 <11.0 ug/kg dry11.0

Aroclor-1260 11096-82-5 <11.0 ug/kg dry11.0




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


2,4,5-T 93-76-5 <27 ug/kg dry27


2,4-D 94-75-7 <27 ug/kg dry27




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


3.E, 4.Gmg/kg dry11800Aluminum 08/02/2018 EPA 6010 C 105



mg/kg dry53.0Barium 08/02/2018 EPA 6010 C 1.75






mg/kg dry18.4Copper 08/02/2018 EPA 6010 C 1.75

3.E, 4.G, 4.Jmg/kg dry14700Iron 08/02/2018 EPA 6010 C 52.5

mg/kg dry16.4Lead 08/02/2018 EPA 6010 C 1.75


4.H, 4.Tmg/kg dry264Manganese 08/02/2018 EPA 6010 C 1.75








mg/kg dry41.2Zinc 08/02/2018 EPA 6010 C 1.75






mg/kg dry<0.02Mercury 08/03/2018 EPA 7471 B 0.02





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05



4.4(1994)

0.05

mg/L<1.00Barium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

1.00


4.4(1994)

0.05


4.4(1994)

0.05

mg/L<0.05Lead 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05


4.4(1994)

0.05


4.4(1994)

0.05




4.Mmg/L<0.02Mercury 08/07/2018 EPA 245.1 0.02



of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05


Extractable Petroleum Hydrocarbons 8006-61-9/68334-30-5 <45.8 mg/kg dry45.8





Diesel Range Organics (C10-C28) 68334-30-5 <18.3 mg/kg dry18.3


p-Terphenyl-d14 1718-51-0 70 45.8-130







Naphthalene-d8 1146-65-2 82 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2



% Solid:91.05





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2A



% Solid:83.81
















1,3,5-Trimethylbenzene 108-67-8 <13.2 ug/kg dry 4.K13.2








4-Methyl-2-Pentanone 108-10-1 <26.4 ug/kg dry26.4

Acetone 67-64-1 <52.8 ug/kg dry 4.M52.8







of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2A



% Solid:83.81


Carbon disulfide 75-15-0 <13.2 ug/kg dry 4.M, 4.K13.2





Chloromethane 74-87-3 <13.2 ug/kg dry13.2




Dibromomethane 74-95-3 <13.2 ug/kg dry 4.K13.2


Ethylbenzene 100-41-4 <13.2 ug/kg dry 4.K13.2


m,p-Xylenes 108-38-3/106-42-3 <26.4 ug/kg dry 4.K26.4

Methyl Butyl Ketone (2-Hexanone) 591-78-6 <13.2 ug/kg dry13.2


Methylene Chloride 75-09-2 <13.2 ug/kg dry 4.M13.2

Methyl-tert-Butyl Ether 1634-04-4 <13.2 ug/kg dry 4.K13.2




o-Xylene 95-47-6 <13.2 ug/kg dry13.2


Styrene 100-42-5 <13.2 ug/kg dry13.2



Tetrachloroethylene 127-18-4 <13.2 ug/kg dry 4.K13.2

Toluene 108-88-3 <13.2 ug/kg dry13.2


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-2A



% Solid:83.81





Vinyl chloride 75-01-4 <13.2 ug/kg dry 4.M, 4.J13.2





Toluene-d8 2037-26-5 95 79.9-123









of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76






























Benzo(a)pyrene 50-32-8 <165 ug/kg dry165


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76










Chrysene 218-01-9 <165 ug/kg dry165







Fluoranthene 206-44-0 <165 ug/kg dry165














of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76



Phenol 108-95-2 <165 ug/kg dry165

Pyrene 129-00-0 <165 ug/kg dry165


2-Fluorobiphenyl 321-60-8 52 32.6-96.2

2-Fluorophenol 367-12-4 51 32.8-95.8

Nitrobenzene-d5 4165-60-0 51 28.1-100

Phenol-d6 13127-88-3 52 31.2-102

Terphenyl-d14 1718-51-0 61 32.6-110



Acenaphthene-d10 50-20015067-26-2 102

Chrysene-d12 50-2001719-03-5 84

Naphthalene-d8 50-2001146-65-2 101

Perylene-d12 50-2001520-96-3 84

Phenanthrene-d10 50-2001517-22-2 97




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76









2,4,6-Tribromophenol 118-79-6 58 18.04-120.2

2-Fluorobiphenyl 321-60-8 52 34.39-110.73

2-Fluorophenol 367-12-4 51 22.98-107.57

Nitrobenzene-d5 4165-60-0 51 31-118.25

Phenol-d6 13127-88-3 52 35.55-111.39

Terphenyl-d14 1718-51-0 61 41.02-106



Acenaphthene-d10 50-20015067-26-2 102

Naphthalene-d8 50-2001146-65-2 101

Phenanthrene-d10 50-2001517-22-2 97




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76


4,4'-DDD 72-54-8 39.6 ug/kg dry3.31

4,4'-DDE 72-55-9 <3.31 ug/kg dry3.31

4,4'-DDT 50-29-3 <3.31 ug/kg dry3.31

Aldrin 309-00-2 <5.51 ug/kg dry5.51

alpha-BHC 319-84-6 <5.51 ug/kg dry5.51

beta-BHC 319-85-7 <5.51 ug/kg dry5.51







Endrin 72-20-8 <5.51 ug/kg dry 4.N5.51














of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76



Aroclor-1221 11104-28-2 <11.0 ug/kg dry11.0

Aroclor-1232 11141-16-5 <11.0 ug/kg dry11.0

Aroclor-1242 53469-21-9 <11.0 ug/kg dry11.0

Aroclor-1248 12672-29-6 <11.0 ug/kg dry11.0

Aroclor-1254 11097-69-1 <11.0 ug/kg dry11.0

Aroclor-1260 11096-82-5 <11.0 ug/kg dry11.0




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76


2,4,5-T 93-76-5 <28 ug/kg dry28


2,4-D 94-75-7 <28 ug/kg dry28




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76


mg/kg16.5Chromium, Trivalent 08/09/2018 Calculation 2.17

Date Prepared: 08/08/2018 Preparation Method: [CALC]












4.Jmg/kg dry14300Iron 08/02/2018 EPA 6010 C 54.0

















mg/kg dry0.03Mercury 08/03/2018 EPA 7471 B 0.02





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76









p-Terphenyl-d14 1718-51-0 90 45.8-130







Naphthalene-d8 1146-65-2 77 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3



% Solid:90.76





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3A



% Solid:89.93
































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3A



% Solid:89.93


















Methylene Chloride 75-09-2 17.3 ug/kg dry 4.K, 4.M12.1





o-Xylene 95-47-6 <12.1 ug/kg dry12.1


Styrene 100-42-5 <12.1 ug/kg dry12.1




Toluene 108-88-3 <12.1 ug/kg dry12.1


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-3A



% Solid:89.93










Toluene-d8 2037-26-5 91 79.9-123









of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88
































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88



Phenol 108-95-2 <177 ug/kg dry177

Pyrene 129-00-0 <177 ug/kg dry177


2-Fluorobiphenyl 321-60-8 56 32.6-96.2

2-Fluorophenol 367-12-4 56 32.8-95.8

Nitrobenzene-d5 4165-60-0 55 28.1-100

Phenol-d6 13127-88-3 57 31.2-102

Terphenyl-d14 1718-51-0 62 32.6-110



Acenaphthene-d10 50-20015067-26-2 106

Chrysene-d12 50-2001719-03-5 91

Naphthalene-d8 50-2001146-65-2 105

Perylene-d12 50-2001520-96-3 88

Phenanthrene-d10 50-2001517-22-2 103




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88









2,4,6-Tribromophenol 118-79-6 66 18.04-120.2

2-Fluorobiphenyl 321-60-8 56 34.39-110.73

2-Fluorophenol 367-12-4 56 22.98-107.57

Nitrobenzene-d5 4165-60-0 55 31-118.25

Phenol-d6 13127-88-3 57 35.55-111.39

Terphenyl-d14 1718-51-0 62 41.02-106



Acenaphthene-d10 50-20015067-26-2 106

Naphthalene-d8 50-2001146-65-2 105

Phenanthrene-d10 50-2001517-22-2 103




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88


4,4'-DDD 72-54-8 <166 ug/kg dry 3.A166

4,4'-DDE 72-55-9 <166 ug/kg dry 3.A166

4,4'-DDT 50-29-3 <166 ug/kg dry 3.A166

Aldrin 309-00-2 <276 ug/kg dry 3.A276

alpha-BHC 319-84-6 <276 ug/kg dry 3.A276

beta-BHC 319-85-7 <276 ug/kg dry 3.A276

Chlordane 12789-03-6 <828 ug/kg dry 3.A828

delta-BHC 319-86-8 <276 ug/kg dry 3.A276

Dieldrin 60-57-1 <276 ug/kg dry 3.A276

Endosulfan I 959-98-8 <276 ug/kg dry 3.A276

Endosulfan II 33213-65-9 <276 ug/kg dry 3.A276

Endosulfan Sulfate 1031-07-8 <276 ug/kg dry 3.A276

Endrin 72-20-8 849 ug/kg dry 3.E276

gamma-BHC 58-89-9 <276 ug/kg dry 3.A276

Heptachlor 76-44-8 <276 ug/kg dry 3.A276

Heptachlor Epoxide 1024-57-3 <276 ug/kg dry 3.A276

Methoxychlor 72-43-5 <276 ug/kg dry 3.A276

Toxaphene 8001-35-2 <5520 ug/kg dry 3.A5520


Decachlorobiphenyl 2051-24-3 3.E72 50.4-127

Tetrachloro-m-xylene 877-09-8 3.E71 57.5-127






of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88


Aroclor-1016 12674-11-2 <884 ug/kg dry 3.A884

Aroclor-1221 11104-28-2 <884 ug/kg dry884

Aroclor-1232 11141-16-5 <884 ug/kg dry884

Aroclor-1242 53469-21-9 <884 ug/kg dry884

Aroclor-1248 12672-29-6 <884 ug/kg dry884

Aroclor-1254 11097-69-1 <884 ug/kg dry884

Aroclor-1260 11096-82-5 60700 ug/kg dry 3.E884




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88


2,4,5-T 93-76-5 <29 ug/kg dry29


2,4-D 94-75-7 <29 ug/kg dry29




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88





mg/kg dry7060Aluminum 08/02/2018 EPA 6010 C 11.8



mg/kg dry143Barium 08/02/2018 EPA 6010 C 1.97



3.E, 4.Jmg/kg dry22600Calcium 08/02/2018 EPA 6010 C 118










4.Jmg/kg dry2.07Selenium 08/02/2018 EPA 6010 C 1.97





mg/kg dry198Zinc 08/02/2018 EPA 6010 C 1.97






3.Emg/kg dry2.19Mercury 08/03/2018 EPA 7471 B 0.23





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88







Diesel Range Organics (C10-C28) 68334-30-5 1240 mg/kg dry19.6


p-Terphenyl-d14 1718-51-0 68 45.8-130







Naphthalene-d8 1146-65-2 22 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8



% Solid:84.88





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8A



% Solid:88.29
















1,3,5-Trimethylbenzene 108-67-8 <11.1 ug/kg dry 4.K11.1








4-Methyl-2-Pentanone 108-10-1 <22.2 ug/kg dry22.2








of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8A



% Solid:88.29


Carbon disulfide 75-15-0 <11.1 ug/kg dry 4.K, 4.M11.1





Chloromethane 74-87-3 <11.1 ug/kg dry11.1




Dibromomethane 74-95-3 <11.1 ug/kg dry 4.K11.1


Ethylbenzene 100-41-4 <11.1 ug/kg dry 4.K11.1


m,p-Xylenes 108-38-3/106-42-3 <22.2 ug/kg dry 4.K22.2

Methyl Butyl Ketone (2-Hexanone) 591-78-6 <11.1 ug/kg dry11.1


Methylene Chloride 75-09-2 <11.1 ug/kg dry 4.M11.1

Methyl-tert-Butyl Ether 1634-04-4 <11.1 ug/kg dry 4.K11.1




o-Xylene 95-47-6 <11.1 ug/kg dry11.1


Styrene 100-42-5 <11.1 ug/kg dry11.1



Tetrachloroethylene 127-18-4 <11.1 ug/kg dry 4.K11.1

Toluene 108-88-3 <11.1 ug/kg dry11.1


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-8A



% Solid:88.29





Vinyl chloride 75-01-4 <11.1 ug/kg dry 4.M, 4.J11.1




Dibromofluoromethane 1868-53-7 124 75.6-135

Toluene-d8 2037-26-5 95 79.9-123









of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54











2-Chloronaphthalene 91-58-7 <8870 ug/kg dry 3.E8870







3/4-Methylphenol 108-39-4/106-44-5 1210 ug/kg dry887














of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54



Phenol 108-95-2 <887 ug/kg dry887

Pyrene 129-00-0 <887 ug/kg dry887


2-Fluorobiphenyl 321-60-8 4.D29 32.6-96.2

2-Fluorophenol 367-12-4 4.D29 32.8-95.8

Nitrobenzene-d5 4165-60-0 4.D28 28.1-100

Phenol-d6 13127-88-3 4.D30 31.2-102

Terphenyl-d14 1718-51-0 4.D30 32.6-110



Acenaphthene-d10 50-20015067-26-2 105

Chrysene-d12 50-2001719-03-5 86

Naphthalene-d8 50-2001146-65-2 106

Perylene-d12 50-2001520-96-3 88

Phenanthrene-d10 50-2001517-22-2 98




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54









2,4,6-Tribromophenol 118-79-6 29 18.04-120.2

2-Fluorobiphenyl 321-60-8 4.D29 34.39-110.73

2-Fluorophenol 367-12-4 29 22.98-107.57

Nitrobenzene-d5 4165-60-0 4.D28 31-118.25

Phenol-d6 13127-88-3 4.D30 35.55-111.39

Terphenyl-d14 1718-51-0 4.D30 41.02-106



Acenaphthene-d10 50-20015067-26-2 105

Naphthalene-d8 50-2001146-65-2 106

Phenanthrene-d10 50-2001517-22-2 98




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54


4,4'-DDD 72-54-8 <166 ug/kg dry 3.A166

4,4'-DDE 72-55-9 <166 ug/kg dry 3.A166

4,4'-DDT 50-29-3 <166 ug/kg dry 3.A166

Aldrin 309-00-2 <277 ug/kg dry 3.A277









Endrin 72-20-8 <277 ug/kg dry 3.A277







Decachlorobiphenyl 2051-24-3 3.E71 50.4-127

Tetrachloro-m-xylene 877-09-8 3.E102 57.5-127






of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54



Aroclor-1221 11104-28-2 <887 ug/kg dry887

Aroclor-1232 11141-16-5 <887 ug/kg dry887

Aroclor-1242 53469-21-9 <887 ug/kg dry887

Aroclor-1248 12672-29-6 <887 ug/kg dry887

Aroclor-1254 11097-69-1 <887 ug/kg dry887





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54


2,4,5-T 93-76-5 <30 ug/kg dry30


2,4-D 94-75-7 <30 ug/kg dry30




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54


































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54



4.4(1994)

0.05


4.4(1994)

1.00

mg/L0.07Cadmium 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05


4.4(1994)

0.05

mg/L0.11Lead 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05


4.4(1994)

0.05


4.4(1994)

0.05




4.Mmg/L<0.02Mercury 08/07/2018 EPA 245.1 0.02



of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54









p-Terphenyl-d14 1718-51-0 57 45.8-130







Naphthalene-d8 1146-65-2 4.D13 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4



% Solid:84.54





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4A



% Solid:81.86


1,1,1,2-Tetrachloroethane 630-20-6 <339 ug/kg dry339

1,1,1-Trichloroethane 71-55-6 <339 ug/kg dry339


1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 <339 ug/kg dry 4.M339


1,1-Dichloroethane 75-34-3 <339 ug/kg dry339

1,1-Dichloroethylene 75-35-4 <339 ug/kg dry 4.M339

1,2,3-Trichloropropane 96-18-4 <339 ug/kg dry339

1,2,4-Trimethylbenzene 95-63-6 <339 ug/kg dry339

1,2-Dibromo-3-chloropropane 96-12-8 <339 ug/kg dry339

1,2-Dibromoethane 106-93-4 <339 ug/kg dry339

1,2-Dichlorobenzene 95-50-1 <339 ug/kg dry339


1,2-Dichloropropane 78-87-5 <339 ug/kg dry339

1,3,5-Trimethylbenzene 108-67-8 <339 ug/kg dry 4.K339




1,4-Dioxane 123-91-1 <1700 ug/kg dry 4.J1700


2-Chlorotoluene 95-49-8 <339 ug/kg dry339

4-Isopropyltoluene 99-87-6 <339 ug/kg dry339

4-Methyl-2-Pentanone 108-10-1 <679 ug/kg dry679

Acetone 67-64-1 2330 ug/kg dry 4.M1360

Acrylonitrile 107-13-1 <339 ug/kg dry 4.M339

Benzene 71-43-2 <339 ug/kg dry339

Bromochloromethane 74-97-5 <339 ug/kg dry339

Bromodichloromethane 75-27-4 <339 ug/kg dry339

Bromoform 75-25-2 <339 ug/kg dry339

Bromomethane 74-83-9 <339 ug/kg dry 4.J339

of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4A



% Solid:81.86


Carbon disulfide 75-15-0 <339 ug/kg dry 4.K, 4.M339

Carbon Tetrachloride 56-23-5 <339 ug/kg dry339

Chlorobenzene 108-90-7 <339 ug/kg dry339

Chloroethane 75-00-3 <339 ug/kg dry339

Chloroform 67-66-3 <339 ug/kg dry339

Chloromethane 74-87-3 <339 ug/kg dry339

cis-1,2-Dichloroethylene 156-59-2 <339 ug/kg dry339

cis-1,3-Dichloropropylene 10061-01-5 <339 ug/kg dry339

Dibromochloromethane 124-48-1 <339 ug/kg dry339

Dibromomethane 74-95-3 <339 ug/kg dry 4.K339

Dichlorodifluoromethane 75-71-8 <339 ug/kg dry339

Ethylbenzene 100-41-4 <339 ug/kg dry 4.K339

Isopropylbenzene (Cumene) 98-82-8 <339 ug/kg dry339

m,p-Xylenes 108-38-3/106-42-3 <679 ug/kg dry 4.K679

Methyl Butyl Ketone (2-Hexanone) 591-78-6 <339 ug/kg dry339

Methyl Ethyl Ketone (2-Butanone) 78-93-3 <679 ug/kg dry 4.J679

Methylene Chloride 75-09-2 <339 ug/kg dry 4.M339

Methyl-tert-Butyl Ether 1634-04-4 <339 ug/kg dry 4.K339

Naphthalene 91-20-3 68400 ug/kg dry339

n-Butylbenzene 104-51-8 <339 ug/kg dry339

n-Propylbenzene 103-65-1 <339 ug/kg dry339

o-Xylene 95-47-6 <339 ug/kg dry339

sec-Butylbenzene 135-98-8 <339 ug/kg dry339

Styrene 100-42-5 <339 ug/kg dry339

tert-Butyl alcohol 75-65-0 <339 ug/kg dry 4.M339

tert-Butylbenzene 98-06-6 <339 ug/kg dry339

Tetrachloroethylene 127-18-4 <339 ug/kg dry 4.K339

Toluene 108-88-3 <339 ug/kg dry339

trans-1,2-Dichloroethylene 156-60-5 <339 ug/kg dry339

of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-4A



% Solid:81.86


trans-1,3-Dichloropropylene 10061-02-6 <339 ug/kg dry339

Trichloroethylene 79-01-6 <339 ug/kg dry339

Trichlorofluoromethane 75-69-4 <339 ug/kg dry 4.M339

Vinyl chloride 75-01-4 <339 ug/kg dry 4.M, 4.J339





Toluene-d8 2037-26-5 86 79.9-123









of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41







2,4-Dimethylphenol 105-67-9 232 ug/kg dry174




2-Chloronaphthalene 91-58-7 5830 ug/kg dry 3.E3470







3/4-Methylphenol 108-39-4/106-44-5 674 ug/kg dry174











Benzo(a)anthracene 56-55-3 183 ug/kg dry174



of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41


Phenanthrene 85-01-8 205 ug/kg dry174

Phenol 108-95-2 <174 ug/kg dry174

Pyrene 129-00-0 402 ug/kg dry174


2-Fluorobiphenyl 321-60-8 50 32.6-96.2

2-Fluorophenol 367-12-4 46 32.8-95.8

Nitrobenzene-d5 4165-60-0 46 28.1-100

Phenol-d6 13127-88-3 51 31.2-102

Terphenyl-d14 1718-51-0 48 32.6-110



Acenaphthene-d10 50-20015067-26-2 99

Chrysene-d12 50-2001719-03-5 81

Naphthalene-d8 50-2001146-65-2 99

Perylene-d12 50-2001520-96-3 85

Phenanthrene-d10 50-2001517-22-2 90




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41









2,4,6-Tribromophenol 118-79-6 55 18.04-120.2

2-Fluorobiphenyl 321-60-8 50 34.39-110.73

2-Fluorophenol 367-12-4 46 22.98-107.57

Nitrobenzene-d5 4165-60-0 46 31-118.25

Phenol-d6 13127-88-3 51 35.55-111.39

Terphenyl-d14 1718-51-0 48 41.02-106



Acenaphthene-d10 50-20015067-26-2 99

Naphthalene-d8 50-2001146-65-2 99

Phenanthrene-d10 50-2001517-22-2 90




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41


4,4'-DDD 72-54-8 <163 ug/kg dry 3.A163

4,4'-DDE 72-55-9 <163 ug/kg dry 3.A163

4,4'-DDT 50-29-3 <163 ug/kg dry 3.A163

Aldrin 309-00-2 <271 ug/kg dry 3.A271









Endrin 72-20-8 <271 ug/kg dry 3.A271







Decachlorobiphenyl 2051-24-3 3.A, 3.E70 50.4-127

Tetrachloro-m-xylene 877-09-8 3.A, 3.E79 57.5-127






of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41



Aroclor-1221 11104-28-2 <868 ug/kg dry868

Aroclor-1232 11141-16-5 <868 ug/kg dry868

Aroclor-1242 53469-21-9 <868 ug/kg dry868

Aroclor-1248 12672-29-6 <868 ug/kg dry868

Aroclor-1254 11097-69-1 <868 ug/kg dry868





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41


2,4,5-T 93-76-5 <29 ug/kg dry29


2,4-D 94-75-7 <29 ug/kg dry29




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41


































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41



4.4(1994)

0.05


4.4(1994)

1.00


4.4(1994)

0.05


4.4(1994)

0.05

mg/L0.98Lead 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05


4.4(1994)

0.05


4.4(1994)

0.05




4.Mmg/L<0.02Mercury 08/07/2018 EPA 245.1 0.02



of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41









p-Terphenyl-d14 1718-51-0 62 45.8-130







Naphthalene-d8 1146-65-2 56 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5



% Solid:86.41





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5A



% Solid:72.76





1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 <344 ug/kg dry 4.M344



1,1-Dichloroethylene 75-35-4 <344 ug/kg dry 4.M344

1,2,3-Trichloropropane 96-18-4 <344 ug/kg dry344

1,2,4-Trimethylbenzene 95-63-6 <344 ug/kg dry344

1,2-Dibromo-3-chloropropane 96-12-8 <344 ug/kg dry344

1,2-Dibromoethane 106-93-4 <344 ug/kg dry344




1,3,5-Trimethylbenzene 108-67-8 <344 ug/kg dry 4.K344




1,4-Dioxane 123-91-1 <1720 ug/kg dry 4.J1720


2-Chlorotoluene 95-49-8 <344 ug/kg dry344

4-Isopropyltoluene 99-87-6 <344 ug/kg dry344

4-Methyl-2-Pentanone 108-10-1 <687 ug/kg dry687

Acetone 67-64-1 <1370 ug/kg dry 4.M1370

Acrylonitrile 107-13-1 <344 ug/kg dry 4.M344

Benzene 71-43-2 <344 ug/kg dry344

Bromochloromethane 74-97-5 <344 ug/kg dry344

Bromodichloromethane 75-27-4 <344 ug/kg dry344

Bromoform 75-25-2 <344 ug/kg dry344

Bromomethane 74-83-9 <344 ug/kg dry 4.J344

of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5A



% Solid:72.76


Carbon disulfide 75-15-0 <344 ug/kg dry 4.K, 4.M344

Carbon Tetrachloride 56-23-5 <344 ug/kg dry344

Chlorobenzene 108-90-7 <344 ug/kg dry344

Chloroethane 75-00-3 <344 ug/kg dry344

Chloroform 67-66-3 <344 ug/kg dry344

Chloromethane 74-87-3 <344 ug/kg dry344

cis-1,2-Dichloroethylene 156-59-2 <344 ug/kg dry344

cis-1,3-Dichloropropylene 10061-01-5 <344 ug/kg dry344

Dibromochloromethane 124-48-1 <344 ug/kg dry344

Dibromomethane 74-95-3 <344 ug/kg dry 4.K344

Dichlorodifluoromethane 75-71-8 <344 ug/kg dry344

Ethylbenzene 100-41-4 <344 ug/kg dry 4.K344

Isopropylbenzene (Cumene) 98-82-8 <344 ug/kg dry344

m,p-Xylenes 108-38-3/106-42-3 <687 ug/kg dry 4.K687

Methyl Butyl Ketone (2-Hexanone) 591-78-6 <344 ug/kg dry344

Methyl Ethyl Ketone (2-Butanone) 78-93-3 <687 ug/kg dry 4.J687

Methylene Chloride 75-09-2 <344 ug/kg dry 4.M344

Methyl-tert-Butyl Ether 1634-04-4 <344 ug/kg dry 4.K344

Naphthalene 91-20-3 34300 ug/kg dry344

n-Butylbenzene 104-51-8 <344 ug/kg dry344

n-Propylbenzene 103-65-1 <344 ug/kg dry344

o-Xylene 95-47-6 <344 ug/kg dry344

sec-Butylbenzene 135-98-8 <344 ug/kg dry344

Styrene 100-42-5 <344 ug/kg dry344

tert-Butyl alcohol 75-65-0 <344 ug/kg dry 4.M344

tert-Butylbenzene 98-06-6 <344 ug/kg dry344

Tetrachloroethylene 127-18-4 <344 ug/kg dry 4.K344

Toluene 108-88-3 <344 ug/kg dry344

trans-1,2-Dichloroethylene 156-60-5 <344 ug/kg dry344

of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-5A



% Solid:72.76


trans-1,3-Dichloropropylene 10061-02-6 <344 ug/kg dry344

Trichloroethylene 79-01-6 <344 ug/kg dry344

Trichlorofluoromethane 75-69-4 <344 ug/kg dry 4.M344

Vinyl chloride 75-01-4 <344 ug/kg dry 4.M, 4.J344





Toluene-d8 2037-26-5 4.E75 79.9-123




Chlorobenzene-d5 50-2003114-55-4 106





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17











2-Chloronaphthalene 91-58-7 464 ug/kg dry166





















of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17



Phenol 108-95-2 <166 ug/kg dry166

Pyrene 129-00-0 <166 ug/kg dry166


2-Fluorobiphenyl 321-60-8 49 32.6-96.2

2-Fluorophenol 367-12-4 49 32.8-95.8

Nitrobenzene-d5 4165-60-0 49 28.1-100

Phenol-d6 13127-88-3 48 31.2-102

Terphenyl-d14 1718-51-0 50 32.6-110



Acenaphthene-d10 50-20015067-26-2 97

Chrysene-d12 50-2001719-03-5 83

Naphthalene-d8 50-2001146-65-2 95

Perylene-d12 50-2001520-96-3 84

Phenanthrene-d10 50-2001517-22-2 93




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17









2,4,6-Tribromophenol 118-79-6 52 18.04-120.2

2-Fluorobiphenyl 321-60-8 49 34.39-110.73

2-Fluorophenol 367-12-4 49 22.98-107.57

Nitrobenzene-d5 4165-60-0 49 31-118.25

Phenol-d6 13127-88-3 48 35.55-111.39

Terphenyl-d14 1718-51-0 50 41.02-106



Acenaphthene-d10 50-20015067-26-2 97

Naphthalene-d8 50-2001146-65-2 95

Phenanthrene-d10 50-2001517-22-2 93




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17


4,4'-DDD 72-54-8 <3.33 ug/kg dry3.33

4,4'-DDE 72-55-9 <3.33 ug/kg dry3.33

4,4'-DDT 50-29-3 <3.33 ug/kg dry3.33

Aldrin 309-00-2 <5.54 ug/kg dry5.54

alpha-BHC 319-84-6 239 ug/kg dry5.54

beta-BHC 319-85-7 <5.54 ug/kg dry5.54







Endrin 72-20-8 <5.54 ug/kg dry 4.N5.54








Tetrachloro-m-xylene 877-09-8 4.D55 57.5-127






of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17



Aroclor-1221 11104-28-2 <11.1 ug/kg dry11.1

Aroclor-1232 11141-16-5 <11.1 ug/kg dry11.1

Aroclor-1242 53469-21-9 <11.1 ug/kg dry11.1

Aroclor-1248 12672-29-6 <11.1 ug/kg dry11.1

Aroclor-1254 11097-69-1 <11.1 ug/kg dry11.1

Aroclor-1260 11096-82-5 <11.1 ug/kg dry11.1




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17


2,4,5-T 93-76-5 <28 ug/kg dry28


2,4-D 94-75-7 <28 ug/kg dry28




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17


































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17



4.4(1994)

0.05


4.4(1994)

1.00


4.4(1994)

0.05


4.4(1994)

0.05

mg/L<0.05Lead 08/06/2018 EPA 200.7, Rev.

4.4(1994)

0.05


4.4(1994)

0.05


4.4(1994)

0.05




4.Mmg/L<0.02Mercury 08/07/2018 EPA 245.1 0.02



of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17









p-Terphenyl-d14 1718-51-0 85 45.8-130







Naphthalene-d8 1146-65-2 74 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6



% Solid:90.17





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6A



% Solid:84.81

























Acetone 67-64-1 116 ug/kg dry 4.M47.2







of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6A



% Solid:84.81


















Methylene Chloride 75-09-2 <11.8 ug/kg dry 4.K, 4.M11.8


Naphthalene 91-20-3 199 ug/kg dry11.8



o-Xylene 95-47-6 <11.8 ug/kg dry11.8


Styrene 100-42-5 <11.8 ug/kg dry11.8




Toluene 108-88-3 <11.8 ug/kg dry11.8


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-6A



% Solid:84.81










Toluene-d8 2037-26-5 82 79.9-123




Chlorobenzene-d5 50-2003114-55-4 147





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09
































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09



Phenol 108-95-2 <166 ug/kg dry166

Pyrene 129-00-0 <166 ug/kg dry166


2-Fluorobiphenyl 321-60-8 56 32.6-96.2

2-Fluorophenol 367-12-4 56 32.8-95.8

Nitrobenzene-d5 4165-60-0 54 28.1-100

Phenol-d6 13127-88-3 57 31.2-102

Terphenyl-d14 1718-51-0 64 32.6-110



Acenaphthene-d10 50-20015067-26-2 97

Chrysene-d12 50-2001719-03-5 85

Naphthalene-d8 50-2001146-65-2 97

Perylene-d12 50-2001520-96-3 83

Phenanthrene-d10 50-2001517-22-2 95




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09









2,4,6-Tribromophenol 118-79-6 63 18.04-120.2

2-Fluorobiphenyl 321-60-8 56 34.39-110.73

2-Fluorophenol 367-12-4 56 22.98-107.57

Nitrobenzene-d5 4165-60-0 54 31-118.25

Phenol-d6 13127-88-3 57 35.55-111.39

Terphenyl-d14 1718-51-0 64 41.02-106



Acenaphthene-d10 50-20015067-26-2 97

Naphthalene-d8 50-2001146-65-2 97

Phenanthrene-d10 50-2001517-22-2 95




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09


4,4'-DDD 72-54-8 <3.33 ug/kg dry3.33

4,4'-DDE 72-55-9 <3.33 ug/kg dry3.33

4,4'-DDT 50-29-3 <3.33 ug/kg dry3.33

Aldrin 309-00-2 <5.55 ug/kg dry5.55

alpha-BHC 319-84-6 12.5 ug/kg dry5.55

beta-BHC 319-85-7 <5.55 ug/kg dry5.55







Endrin 72-20-8 <5.55 ug/kg dry 4.N5.55














of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09



Aroclor-1221 11104-28-2 <11.1 ug/kg dry11.1

Aroclor-1232 11141-16-5 <11.1 ug/kg dry11.1

Aroclor-1242 53469-21-9 <11.1 ug/kg dry11.1

Aroclor-1248 12672-29-6 <11.1 ug/kg dry11.1

Aroclor-1254 11097-69-1 <11.1 ug/kg dry11.1

Aroclor-1260 11096-82-5 <11.1 ug/kg dry11.1




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09


2,4,5-T 93-76-5 <28 ug/kg dry28


2,4-D 94-75-7 <28 ug/kg dry28




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09







mg/kg dry<1.84Arsenic 08/02/2018 EPA 6010 C 1.84






























of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09









p-Terphenyl-d14 1718-51-0 90 45.8-130







Naphthalene-d8 1146-65-2 47 20.7-168




of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7



% Solid:90.09





of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7A



% Solid:90.36
































of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7A



% Solid:90.36


















Methylene Chloride 75-09-2 <11.7 ug/kg dry 4.K, 4.M11.7


Naphthalene 91-20-3 50.4 ug/kg dry11.7



o-Xylene 95-47-6 <11.7 ug/kg dry11.7


Styrene 100-42-5 <11.7 ug/kg dry11.7




Toluene 108-88-3 <11.7 ug/kg dry11.7


of 111



Matrix: Soil


ELAP: #11693

Sample ID: WC-7A



% Solid:90.36










Toluene-d8 2037-26-5 81 79.9-123




Chlorobenzene-d5 50-2003114-55-4 132





Data Qualifiers Key Reference:

1.C Holding time exceeded, analyze immediate parameter.

2.B Parameter not certifiable by NELAP.

3.A Reporting limit raised due to matrix interference.

3.E Compound reported at a dilution factor.

4.D Surrogate recovery has failed low.

4.E Surrogate recovery has failed high.

4.F Spike recovery does not meet QC criteria due to high target compound concentration.

4.G Spike recovery out of range due to matrix interference.

4.H Batch spike recovery out of range due to matrix inconsistency.

4.J Continuing Calibration Verification (CCV) quality control levels failed low, values are considered to be estimated.

4.K Continuing Calibration Verification (CCV) quality control levels failed high, values are considered to be estimated.

4.M LCS recovery was above QC acceptance limit.

4.N LCS recovery was below QC acceptance limit.

4.T Sample Matrix Spike/Spike Dup RPD is above acceptable range.

4.Y Blank Spike/Blank Spike Dup RPD is above acceptable range.

Minimum Detection LimitMDL

LOQ Limit of Quantitation

august 13, 2018 attn: mr. philip lepine...2018/08/01 · august 13, 2018 snl construction re: 4380...

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